· ANALYTICAL RESULTS Prepared by: Lancaster Laboratories 2425 New Holland Pike Lancaster, PA 17605-2425 Prepared for: CDM Federal Programs Corp. 14420 Albemarle Point Place Suite

ANALYTICAL RESULTS

Prepared by:

Lancaster Laboratories2425 New Holland Pike

Lancaster, PA 17605-2425

Prepared for:

CDM Federal Programs Corp.14420 Albemarle Point Place

Suite 210Chantilly VA 20151

June 21, 2011

Project: SSFL Area IV Collocated Soil Sampling

Submittal Date: 05/17/2011Group Number: 1247140

SDG: DE151PO Number: 1203-004-008-AL

Release Number: TRACKING #12090State of Sample Origin: CA

Client Sample Description Lancaster Labs (LLI) #SL-042-SA5A-SB-3.5-4.5 Soil 6288929SL-042-SA5A-SB-3.5-4.5MS Soil 6288930SL-042-SA5A-SB-3.5-4.5MSD Soil 6288931SL-042-SA5A-SB-3.5-4.5DUP Soil 6288932DUP-17-SA5A-QC-051611 Soil 6288933SL-167-SA5A-SB-1.0-2.0 Soil 6288934EB15-SA5A-SB-051611 Water 6288935SL-002-SA5DN-SB-4.0-5.0 Soil 6288936SL-002-SA5DN-SB-9.0-10.0 Soil 6288937SL-003-SA5DN-SB-0.5-1.5 Soil 6288938SL-003-SA5DN-SB-8.0-9.0 Soil 6288939SL-004-SA5DN-SB-3.5-4.5 Soil 6288940SL-004-SA5DN-SB-9.0-10.0 Soil 6288941TB-051611 Water 6288942

The specific methodologies used in obtaining the enclosed analytical results are indicated on theLaboratory Sample Analysis Record.

ELECTRONICCOPY TO

CDM Federal Services Program Attn: Todd Burgesser

1 COPY TO Data Package Group

Questions? Contact your Client Services RepresentativeNicole L Maljovec at (717) 656-2300 Ext. 1537

Respectfully Submitted,

Page 1 of 7

LLI Sample # SW 6288929LLI Group # 1247140Account # 13013

Sample Description: SL-042-SA5A-SB-3.5-4.5 Soil SSFL Area IV Collocated Soil Sampling SL-042-SA5A-SB-3.5-4.5 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40

CDM Federal Programs Corp.

Reported: 06/21/2011 13:43

14420 Albemarle Point PlaceSuite 210Chantilly VA 20151

SL042 SDG#: DE151-01BKG

DryLimit ofQuantitation

DryMethodDetection Limit*

DryResultAnalysis Name CAS Number

ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B7.4 J 0.9467-64-106192 7.1 8.5Acetone0.11 U 0.9471-43-206192 0.11 4.3Benzene0.14 U 0.94108-86-106192 0.14 4.3Bromobenzene0.35 U 0.9474-97-506192 0.35 4.3Bromochloromethane0.09 U 0.9475-27-406192 0.09 4.3Bromodichloromethane0.43 U 0.9475-25-206192 0.43 4.3Bromoform0.27 U 0.9474-83-906192 0.27 4.3Bromomethane1.3 U 0.9478-93-306192 1.3 8.52-Butanone0.13 U 0.94104-51-806192 0.13 4.3n-Butylbenzene0.06 U 0.94135-98-806192 0.06 4.3sec-Butylbenzene0.17 U 0.9498-06-606192 0.17 4.3tert-Butylbenzene0.15 U 0.9456-23-506192 0.15 4.3Carbon Tetrachloride0.12 U 0.94108-90-706192 0.12 4.3Chlorobenzene0.14 U 0.9475-00-306192 0.14 4.3Chloroethane0.32 U 0.94110-75-806192 0.32 4.32-Chloroethyl Vinyl Ether0.13 U 0.9467-66-306192 0.13 4.3Chloroform0.35 U 0.9474-87-306192 0.35 4.3Chloromethane0.15 U 0.9495-49-806192 0.15 4.32-Chlorotoluene0.15 U 0.94106-43-406192 0.15 4.34-Chlorotoluene0.53 U 0.9479-38-906192 0.53 5.3Chlorotrifluoroethene0.75 U 0.9496-12-806192 0.75 4.31,2-Dibromo-3-chloropropane0.21 U 0.94124-48-106192 0.21 4.3Dibromochloromethane0.18 U 0.94106-93-406192 0.18 4.31,2-Dibromoethane0.26 U 0.9474-95-306192 0.26 4.3Dibromomethane0.1 U 0.9495-50-106192 0.1 4.31,2-Dichlorobenzene0.13 U 0.94541-73-106192 0.13 4.31,3-Dichlorobenzene0.17 U 0.94106-46-706192 0.17 4.31,4-Dichlorobenzene0.13 U 0.9475-71-806192 0.13 4.3Dichlorodifluoromethane0.11 U 0.9475-34-306192 0.11 4.31,1-Dichloroethane0.16 U 0.94107-06-206192 0.16 4.31,2-Dichloroethane0.42 U 0.9475-35-406192 0.42 4.31,1-Dichloroethene0.20 U 0.94156-59-206192 0.20 4.3cis-1,2-Dichloroethene0.13 U 0.94156-60-506192 0.13 4.3trans-1,2-Dichloroethene0.18 U 0.9478-87-506192 0.18 4.31,2-Dichloropropane0.09 U 0.94142-28-906192 0.09 4.31,3-Dichloropropane0.18 U 0.94594-20-706192 0.18 4.32,2-Dichloropropane0.14 U 0.94563-58-606192 0.14 4.31,1-Dichloropropene0.17 U 0.9410061-01-506192 0.17 4.3cis-1,3-Dichloropropene0.18 U 0.9410061-02-606192 0.18 4.3trans-1,3-Dichloropropene0.06 U 0.94100-41-406192 0.06 4.3Ethylbenzene0.12 U 0.9476-13-106192 0.12 4.3Freon 1130.53 U 0.9475-88-706192 0.53 5.3Freon 133a0.15 U 0.9487-68-306192 0.15 4.3Hexachlorobutadiene1.7 U 0.94591-78-606192 1.7 8.52-Hexanone0.06 U 0.9498-82-806192 0.06 4.3Isopropylbenzene0.12 U 0.9499-87-606192 0.12 4.3p-Isopropyltoluene0.22 U 0.941634-04-406192 0.22 4.3Methyl Tertiary Butyl Ether0.42 U 0.94108-10-106192 0.42 8.54-Methyl-2-pentanone3.7 J 0.9475-09-206192 0.26 4.3Methylene Chloride0.08 U 0.94103-65-106192 0.08 4.3n-Propylbenzene

*=This limit was used in the evaluation of the final resultShaded result = The results or reporting limit exceeded the client-provided action limit.

Page 2 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B0.11 U 0.94100-42-506192 0.11 4.3Styrene0.12 U 0.94630-20-606192 0.12 4.31,1,1,2-Tetrachloroethane0.25 U 0.9479-34-506192 0.25 4.31,1,2,2-Tetrachloroethane0.21 U 0.94127-18-406192 0.21 4.3Tetrachloroethene0.12 J 0.94108-88-306192 0.09 4.3Toluene0.15 U 0.9487-61-606192 0.15 4.31,2,3-Trichlorobenzene0.19 U 0.94120-82-106192 0.19 4.31,2,4-Trichlorobenzene0.21 U 0.9471-55-606192 0.21 4.31,1,1-Trichloroethane0.29 U 0.9479-00-506192 0.29 4.31,1,2-Trichloroethane0.16 U 0.9479-01-606192 0.16 4.3Trichloroethene0.31 U 0.9475-69-406192 0.31 4.3Trichlorofluoromethane0.35 U 0.9496-18-406192 0.35 4.31,2,3-Trichloropropane0.43 U 0.9495-63-606192 0.43 4.31,2,4-Trimethylbenzene0.11 U 0.94108-67-806192 0.11 4.31,3,5-Trimethylbenzene0.21 U 0.9475-01-406192 0.21 4.3Vinyl Chloride0.18 U 0.94179601-23-106192 0.18 4.3m+p-Xylene0.18 U 0.9495-47-606192 0.18 4.3o-Xylene

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B SIM4.9 U 21.66123-91-110326 4.9 151,4-Dioxane

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C190 U 162-53-304688 190 560Aniline1,300 U 192-87-504688 1,300 3,800Benzidine190 U 165-85-004688 190 560Benzoic acid190 U 1100-51-604688 190 560Benzyl alcohol19 U 1101-55-304688 19 1904-Bromophenyl-phenylether19 U 186-74-804688 19 190Carbazole38 U 159-50-704688 38 1904-Chloro-3-methylphenol75 U 1106-47-804688 75 1904-Chloroaniline19 U 1111-91-104688 19 190bis(2-Chloroethoxy)methane19 U 1111-44-404688 19 190bis(2-Chloroethyl)ether19 U 139638-32-904688 19 190bis(2-Chloroisopropyl)ether19 U 191-58-704688 19 1902-Chloronaphthalene19 U 195-57-804688 19 1902-Chlorophenol38 U 17005-72-304688 38 1904-Chlorophenyl-phenylether19 U 1132-64-904688 19 190Dibenzofuran19 U 195-50-104688 19 1901,2-Dichlorobenzene19 U 1541-73-104688 19 1901,3-Dichlorobenzene19 U 1106-46-704688 19 1901,4-Dichlorobenzene110 U 191-94-104688 110 3803,3'-Dichlorobenzidine19 U 1120-83-204688 19 1902,4-Dichlorophenol38 U 1105-67-904688 38 1902,4-Dimethylphenol38 U 1108-68-904688 38 1903,5-Dimethylphenol190 U 1534-52-104688 190 5604,6-Dinitro-2-methylphenol380 U 151-28-504688 380 1,1002,4-Dinitrophenol38 U 1121-14-204688 38 1902,4-Dinitrotoluene19 U 1606-20-204688 19 1902,6-Dinitrotoluene19 U 1122-66-704688 19 1901,2-Diphenylhydrazine


Page 3 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C19 U 1118-74-104688 19 190Hexachlorobenzene75 U 187-68-304688 75 190Hexachlorobutadiene190 U 177-47-404688 190 560Hexachlorocyclopentadiene19 U 167-72-104688 19 190Hexachloroethane19 U 178-59-104688 19 190Isophorone38 U 195-48-704688 38 1902-Methylphenol38 U 1106-44-504688 38 1904-Methylphenol

3-Methylphenol and 4-methylphenol cannot be resolved under thechromatographic conditions used for sample analysis. The result reportedfor 4-methylphenol represents the combined total of both compounds.

19 U 188-74-404688 19 1902-Nitroaniline38 U 199-09-204688 38 1903-Nitroaniline75 U 1100-01-604688 75 1904-Nitroaniline19 U 198-95-304688 19 190Nitrobenzene19 U 188-75-504688 19 1902-Nitrophenol190 U 1100-02-704688 190 5604-Nitrophenol19 U 1621-64-704688 19 190N-Nitroso-di-n-propylamine19 U 186-30-604688 19 190N-Nitrosodiphenylamine

N-nitrosodiphenylamine decomposes in the GC inlet formingdiphenylamine. The result reported for N-nitrosodiphenylaminerepresents the combined total of both compounds.

190 U 187-86-504688 190 560Pentachlorophenol19 U 1108-95-204688 19 190Phenol19 U 1120-82-104688 19 1901,2,4-Trichlorobenzene38 U 195-95-404688 38 1902,4,5-Trichlorophenol38 U 188-06-204688 38 1902,4,6-Trichlorophenol

The LCS and/or LCSD recoveries are outside the stated QC windowbut within the marginal exceedance allowance of +/- 4 standarddeviations as defined in the NELAC Standards. The followinganalytes are accepted based on this allowance:2,4-dinitrophenol4,6-dinitro-2-methylphenol

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.76 U 183-32-910138 0.76 1.9Acenaphthene0.38 U 1208-96-810138 0.38 1.9Acenaphthylene0.38 U 1120-12-710138 0.38 1.9Anthracene0.76 U 156-55-310138 0.76 1.9Benzo(a)anthracene0.76 U 150-32-810138 0.76 1.9Benzo(a)pyrene0.76 U 1205-99-210138 0.76 1.9Benzo(b)fluoranthene0.76 U 1191-24-210138 0.76 1.9Benzo(g,h,i)perylene0.76 U 1207-08-910138 0.76 1.9Benzo(k)fluoranthene6.8 U 185-68-710138 6.8 20Butylbenzylphthalate6.8 U 184-74-210138 6.8 20Di-n-butylphthalate0.38 U 1218-01-910138 0.38 1.9Chrysene0.76 U 153-70-310138 0.76 1.9Dibenz(a,h)anthracene6.8 U 184-66-210138 6.8 20Diethylphthalate6.8 U 1131-11-310138 6.8 20Dimethylphthalate6.8 U 1117-81-710138 6.8 20Bis(2-Ethylhexyl)phthalate0.76 U 1206-44-010138 0.76 1.9Fluoranthene


Page 4 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.76 U 186-73-710138 0.76 1.9Fluorene0.76 U 1193-39-510138 0.76 1.9Indeno(1,2,3-cd)pyrene0.76 U 190-12-010138 0.76 1.91-Methylnaphthalene0.76 U 191-57-610138 0.76 1.92-Methylnaphthalene0.76 U 191-20-310138 0.76 1.9Naphthalene0.76 U 162-75-910138 0.76 1.9N-Nitrosodimethylamine6.8 U 1117-84-010138 6.8 20Di-n-octylphthalate0.76 U 185-01-810138 0.76 1.9Phenanthrene0.76 U 1129-00-010138 0.76 1.9Pyrene

ug/kgug/kgug/kg ug/kgPesticides/PCBs SW-846 80821.1 U 163496-31-110225 1.1 3.7Aroclor 54321.1 U 112642-23-810225 1.1 3.7Aroclor 54421.5 J 111126-42-410225 1.1 3.7Aroclor 54600.37 U 112674-11-210225 0.37 1.9PCB-10160.37 U 111104-28-210225 0.37 1.9PCB-12210.37 U 111141-16-510225 0.37 1.9PCB-12320.37 U 153469-21-910225 0.37 1.9PCB-12420.37 U 112672-29-610225 0.37 1.9PCB-12483.2 111097-69-110225 0.37 1.9PCB-12540.44 U 111096-82-510225 0.44 1.9PCB-12600.37 U 137324-23-510225 0.37 1.9PCB-12620.37 U 111100-14-410225 0.37 1.9PCB-1268

mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B33,800 17429-90-501643 5.51 21.9Aluminum8.21 17440-42-807914 0.975 5.48Boron3,050 17440-70-201650 6.71 21.9Calcium28,200 17439-89-601654 5.16 21.9Iron32.1 17439-93-201656 0.24 2.2Lithium5,730 17439-95-401657 2.78 11.0Magnesium252 17439-96-506958 0.0854 0.548Manganese322 17723-14-010145 0.613 11.0Phosphorus1,810 17440-09-701662 19.7 54.8Potassium112 17440-23-501667 40.8 110Sodium22.9 17440-24-607968 0.0679 0.548Strontium3.40 J 17440-31-506969 1.10 11.0Tin1,450 17440-32-606970 0.416 1.10Titanium5.24 J 17440-67-710146 0.920 5.48Zirconium

mg/kgmg/kgmg/kg mg/kgSW-846 60200.312 27440-36-006124 0.0677 0.226Antimony

Due to the nature of the EPA Method 3050B digestion procedure forICP-MS, the Laboratory Control Standard and Matrix Spike(s) may exhibitlow recoveries for antimony.

9.05 27440-38-206125 0.0902 0.451Arsenic120 27440-39-306126 0.122 0.451Barium1.11 27440-41-706127 0.0180 0.113Beryllium0.0923 J 27440-43-906128 0.0451 0.113Cadmium


Page 5 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

mg/kgmg/kgmg/kg mg/kgMetals SW-846 602028.3 27440-47-306131 0.135 0.451Chromium9.21 27440-48-406132 0.0226 0.113Cobalt11.1 27440-50-806133 0.0744 0.451Copper8.57 27439-92-106135 0.0117 0.226Lead1.50 27439-98-706138 0.0564 0.113Molybdenum18.9 27440-02-006139 0.113 0.451Nickel0.248 J 27782-49-206141 0.0451 0.451Selenium0.833 27440-22-406142 0.0135 0.113Silver0.295 27440-28-006145 0.0338 0.113Thallium55.1 27440-62-206148 0.0248 0.113Vanadium52.4 27440-66-606149 0.631 3.38Zinc

mg/kgmg/kgmg/kg mg/kgSW-846 7471A0.0032 U 17439-97-600159 0.0032 0.110Mercury

mg/kgmg/kgmg/kg mg/kgWet Chemistry EPA 300.00.91 U 116984-48-807332 0.91 1.111a Anions by 300.0 - Fluoride

ug/kgug/kgug/kg ug/kgEPA 314.010.3 U 114797-73-010147 10.3 34.27a Perchlorate EPA 314.0

mg/kgmg/kgmg/kg mg/kgSW-846 71990.58 J 118540-29-905892 0.23 1.13a Cr VI by EPA 7199

mVmVmV mVASTM D1498389 1n.a.01821 10.0 10.032a OR Potential

The oxidation-reduction potential is reported in mV as referred to thestandard hydrogen scale.

Std. UnitsStd. UnitsStd. Units Std.Units

SW-846 9045C modified

6.53 1n.a.00394 0.0100 0.010018a pH by 9045C

%%% %Wet Chemistry EPA 160.3 modified12.2 1n.a.11624 0.50 0.50Moisture Content by 160.3

"Moisture" represents the loss in weight of the sample after oven drying at103 - 105 degrees Celsius. The moisture result reported above is on anas-received basis.

General Sample CommentsState of California Lab Certification No. 2501The volatile analysis was performed on soil from SL-042-SA5A-SB-4.0. All QC is compliant unless otherwise noted. Please refer to the QualityControl Summary for overall QC performance data and associated samples.


Page 6 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43



MethodAnalysis NameCATNo.

AnalysisDate and Time

Batch#Trial# Dilution Factor

Analyst

Laboratory Sample Analysis Record

0.94Chelsea B Eastep05/20/2011 16:56B111401AA1SW-846 8260B1a Volatile Organics EPA8260B

06192

21.66Jason M Long05/18/2011 15:28E111381AA1SW-846 8260B SIM14a 1,4-Dioxane by 8260BSIM

10326

n.a.Lois E Hiltz05/17/2011 19:072011137244351SW-846 5035GC/MS - HL Encore Prep08390n.a.Lois E Hiltz05/17/2011 20:042011137244351SW-846 5035GC/MS - LL DIH2O Encore

Prep07320

n.a.Lois E Hiltz05/17/2011 20:052011137244352SW-846 5035GC/MS - LL DIH2O EncorePrep

07320

n.a.Lois E Hiltz05/17/2011 19:052011137244351SW-846 5035GC/MS-HL Encore Prep-NC075781Brian K Graham05/24/2011 05:1711139SLH0261SW-846 8270C5a Semivolatiles by EPA

8270C04688

1Gregory JDrahovsky

05/20/2011 18:1711139SLG0261SW-846 8270C SIM4a Select SVOC EPA 8270SIM10138

1Sherry L Morrow05/20/2011 03:3011139SLG0261SW-846 3550BBNA Soil Extraction SIM104791Sherry L Morrow05/20/2011 03:3011139SLH0261SW-846 3550BBNA Soil Sonication003811Sarah M Snyder05/25/2011 12:03111380023A1SW-846 80828a PCBs/PCTs by 8082102251Roman Kuropatkin05/19/2011 05:15111380023A1SW-846 3550BSolid Sample Pesticide

Extract00819

1Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BCalcium016501Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 06:311113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:06111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Cobalt061322Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:06111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:06111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:06111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 07:54111371026001A1SW-846 6020Zinc06149


Page 7 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






Analyst


1Damary Valentin05/18/2011 06:251113757110021SW-846 7471AMercury001591Annamaria

Stipkovits05/17/2011 20:501113757080021SW-846 3050BSW SW846 ICP Digest05708

1AnnamariaStipkovits

05/17/2011 21:121113710260011SW-846 3050BSW SW846 ICP-MS Digest11026


05/18/2011 01:001113757110021SW-846 7471Amodified

SW SW846 Hg Digest05711

1Ashley M Adams05/22/2011 13:1011141621202B1EPA 300.011a Anions by 300.0 -Fluoride

07332

1William L HamakerJr

05/21/2011 11:5311141621201A1EPA 314.07a Perchlorate EPA 314.010147

1Parker D Lindstrom05/23/2011 19:5611140243201A2SW-846 71993a Cr VI by EPA 719905892


05/21/2011 11:5511141621202B1EPA 300.011a Anions by 300.0 -Extract.

01352


05/21/2011 09:5011141621201A1EPA 314.07a Perchlorate EPA 314.0Prep.

10129

1Michele L Graham05/19/2011 14:4511139182102A1ASTM D149832a OR Potential018211Michele L Graham05/19/2011 14:4511139039402A1SW-846 9045C

modified18a pH by 9045C00394

1Luz M Groff05/20/2011 17:2011140243201A1SW-846 3060A3a Cr VI by EPA 7199 - Ext.02432

1Scott W Freisher05/24/2011 17:3211144162401A1EPA 160.3 modifiedMoisture Content by 160.311624


Page 1 of 7


Sample Description: SL-042-SA5A-SB-3.5-4.5MS Soil SSFL Area IV Collocated Soil Sampling SL-042-SA5A-SB-3.5-4.5 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL042 SDG#: DE151-01MS




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B200 0.9667-64-106192 7.3 8.7Acetone25 0.9671-43-206192 0.11 4.4Benzene24 0.96108-86-106192 0.14 4.4Bromobenzene29 0.9674-97-506192 0.36 4.4Bromochloromethane22 0.9675-27-406192 0.09 4.4Bromodichloromethane21 0.9675-25-206192 0.44 4.4Bromoform15 0.9674-83-906192 0.27 4.4Bromomethane180 0.9678-93-306192 1.3 8.72-Butanone22 0.96104-51-806192 0.13 4.4n-Butylbenzene25 0.96135-98-806192 0.06 4.4sec-Butylbenzene24 0.9698-06-606192 0.17 4.4tert-Butylbenzene26 0.9656-23-506192 0.15 4.4Carbon Tetrachloride23 0.96108-90-706192 0.12 4.4Chlorobenzene14 0.9675-00-306192 0.14 4.4Chloroethane19 0.96110-75-806192 0.33 4.42-Chloroethyl Vinyl Ether24 0.9667-66-306192 0.13 4.4Chloroform17 0.9674-87-306192 0.36 4.4Chloromethane23 0.9695-49-806192 0.15 4.42-Chlorotoluene22 0.96106-43-406192 0.15 4.44-Chlorotoluene16 0.8679-38-906192 0.49 4.9Chlorotrifluoroethene17 0.9696-12-806192 0.76 4.41,2-Dibromo-3-chloropropane22 0.96124-48-106192 0.22 4.4Dibromochloromethane21 0.96106-93-406192 0.19 4.41,2-Dibromoethane21 0.9674-95-306192 0.26 4.4Dibromomethane21 0.9695-50-106192 0.1 4.41,2-Dichlorobenzene23 0.96541-73-106192 0.13 4.41,3-Dichlorobenzene22 0.96106-46-706192 0.17 4.41,4-Dichlorobenzene17 0.9675-71-806192 0.13 4.4Dichlorodifluoromethane25 0.9675-34-306192 0.11 4.41,1-Dichloroethane22 0.96107-06-206192 0.16 4.41,2-Dichloroethane20 0.9675-35-406192 0.42 4.41,1-Dichloroethene23 0.96156-59-206192 0.21 4.4cis-1,2-Dichloroethene24 0.96156-60-506192 0.13 4.4trans-1,2-Dichloroethene24 0.9678-87-506192 0.19 4.41,2-Dichloropropane21 0.96142-28-906192 0.09 4.41,3-Dichloropropane23 0.96594-20-706192 0.19 4.42,2-Dichloropropane25 0.96563-58-606192 0.14 4.41,1-Dichloropropene21 0.9610061-01-506192 0.17 4.4cis-1,3-Dichloropropene19 0.9610061-02-606192 0.19 4.4trans-1,3-Dichloropropene23 0.96100-41-406192 0.06 4.4Ethylbenzene22 0.9676-13-106192 0.12 4.4Freon 11317 0.8675-88-706192 0.49 4.9Freon 133a24 0.9687-68-306192 0.15 4.4Hexachlorobutadiene110 0.96591-78-606192 1.7 8.72-Hexanone24 0.9698-82-806192 0.06 4.4Isopropylbenzene24 0.9699-87-606192 0.12 4.4p-Isopropyltoluene19 0.961634-04-406192 0.23 4.4Methyl Tertiary Butyl Ether91 0.96108-10-106192 0.42 8.74-Methyl-2-pentanone22 0.9675-09-206192 0.26 4.4Methylene Chloride25 0.96103-65-106192 0.08 4.4n-Propylbenzene


Page 2 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B21 0.96100-42-506192 0.11 4.4Styrene23 0.96630-20-606192 0.12 4.41,1,1,2-Tetrachloroethane20 0.9679-34-506192 0.25 4.41,1,2,2-Tetrachloroethane27 0.96127-18-406192 0.22 4.4Tetrachloroethene24 0.96108-88-306192 0.09 4.4Toluene18 0.9687-61-606192 0.15 4.41,2,3-Trichlorobenzene17 0.96120-82-106192 0.20 4.41,2,4-Trichlorobenzene25 0.9671-55-606192 0.22 4.41,1,1-Trichloroethane21 0.9679-00-506192 0.29 4.41,1,2-Trichloroethane24 0.9679-01-606192 0.16 4.4Trichloroethene19 0.9675-69-406192 0.32 4.4Trichlorofluoromethane21 0.9696-18-406192 0.36 4.41,2,3-Trichloropropane23 0.9695-63-606192 0.44 4.41,2,4-Trimethylbenzene24 0.96108-67-806192 0.11 4.41,3,5-Trimethylbenzene17 0.9675-01-406192 0.22 4.4Vinyl Chloride46 0.96179601-23-106192 0.19 4.4m+p-Xylene22 0.9695-47-606192 0.19 4.4o-Xylene

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B SIM240 23.02123-91-110326 5.2 161,4-Dioxane

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C1,800 183-32-904688 19 190Acenaphthene1,800 1208-96-804688 19 190Acenaphthylene1,600 162-53-304688 190 560Aniline1,800 1120-12-704688 19 190Anthracene3,000 J 192-87-504688 1,300 3,800Benzidine1,800 156-55-304688 19 190Benzo(a)anthracene1,700 150-32-804688 19 190Benzo(a)pyrene1,800 1205-99-204688 19 190Benzo(b)fluoranthene1,600 1191-24-204688 19 190Benzo(g,h,i)perylene1,800 1207-08-904688 19 190Benzo(k)fluoranthene1,200 165-85-004688 190 560Benzoic acid1,800 1100-51-604688 190 560Benzyl alcohol1,700 1101-55-304688 19 1904-Bromophenyl-phenylether1,800 185-68-704688 19 190Butylbenzylphthalate1,700 184-74-204688 19 190Di-n-butylphthalate1,700 186-74-804688 19 190Carbazole1,800 159-50-704688 38 1904-Chloro-3-methylphenol1,400 1106-47-804688 75 1904-Chloroaniline1,800 1111-91-104688 19 190bis(2-Chloroethoxy)methane1,700 1111-44-404688 19 190bis(2-Chloroethyl)ether1,700 139638-32-904688 19 190bis(2-Chloroisopropyl)ether1,700 191-58-704688 19 1902-Chloronaphthalene1,800 195-57-804688 19 1902-Chlorophenol1,800 17005-72-304688 38 1904-Chlorophenyl-phenylether1,700 1218-01-904688 19 190Chrysene1,600 153-70-304688 19 190Dibenz(a,h)anthracene1,800 1132-64-904688 19 190Dibenzofuran


Page 3 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C1,600 195-50-104688 19 1901,2-Dichlorobenzene1,600 1541-73-104688 19 1901,3-Dichlorobenzene1,600 1106-46-704688 19 1901,4-Dichlorobenzene1,300 191-94-104688 110 3803,3'-Dichlorobenzidine1,800 1120-83-204688 19 1902,4-Dichlorophenol1,700 184-66-204688 19 190Diethylphthalate1,800 1105-67-904688 38 1902,4-Dimethylphenol1,900 1108-68-904688 38 1903,5-Dimethylphenol1,800 1131-11-304688 19 190Dimethylphthalate1,000 1534-52-104688 190 5604,6-Dinitro-2-methylphenol1,100 J 151-28-504688 380 1,1002,4-Dinitrophenol1,800 1121-14-204688 38 1902,4-Dinitrotoluene1,800 1606-20-204688 19 1902,6-Dinitrotoluene1,800 1122-66-704688 19 1901,2-Diphenylhydrazine1,700 1117-81-704688 19 380bis(2-Ethylhexyl)phthalate1,800 1206-44-004688 19 190Fluoranthene1,700 186-73-704688 19 190Fluorene1,800 1118-74-104688 19 190Hexachlorobenzene1,600 187-68-304688 75 190Hexachlorobutadiene3,300 177-47-404688 190 560Hexachlorocyclopentadiene1,500 167-72-104688 19 190Hexachloroethane1,600 1193-39-504688 19 190Indeno(1,2,3-cd)pyrene1,800 178-59-104688 19 190Isophorone1,800 190-12-004688 19 1901-Methylnaphthalene1,600 191-57-604688 19 1902-Methylnaphthalene1,800 195-48-704688 38 1902-Methylphenol1,900 1106-44-504688 38 1904-Methylphenol


1,700 191-20-304688 19 190Naphthalene1,800 188-74-404688 19 1902-Nitroaniline1,700 199-09-204688 38 1903-Nitroaniline1,500 1100-01-604688 75 1904-Nitroaniline1,800 198-95-304688 19 190Nitrobenzene1,800 188-75-504688 19 1902-Nitrophenol1,600 1100-02-704688 190 5604-Nitrophenol1,800 162-75-904688 38 190N-Nitrosodimethylamine1,600 1621-64-704688 19 190N-Nitroso-di-n-propylamine1,800 186-30-604688 19 190N-Nitrosodiphenylamine


1,800 1117-84-004688 19 190Di-n-octylphthalate1,300 187-86-504688 190 560Pentachlorophenol1,800 185-01-804688 19 190Phenanthrene1,800 1108-95-204688 19 190Phenol1,900 1129-00-004688 19 190Pyrene1,700 1120-82-104688 19 1901,2,4-Trichlorobenzene1,800 195-95-404688 38 1902,4,5-Trichlorophenol


Page 4 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C1,800 188-06-204688 38 1902,4,6-Trichlorophenol


ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM35 183-32-910138 0.76 1.9Acenaphthene34 1208-96-810138 0.38 1.9Acenaphthylene36 1120-12-710138 0.38 1.9Anthracene38 156-55-310138 0.76 1.9Benzo(a)anthracene38 150-32-810138 0.76 1.9Benzo(a)pyrene42 1205-99-210138 0.76 1.9Benzo(b)fluoranthene42 1191-24-210138 0.76 1.9Benzo(g,h,i)perylene38 1207-08-910138 0.76 1.9Benzo(k)fluoranthene42 185-68-710138 6.8 20Butylbenzylphthalate41 184-74-210138 6.8 20Di-n-butylphthalate37 1218-01-910138 0.38 1.9Chrysene42 153-70-310138 0.76 1.9Dibenz(a,h)anthracene38 184-66-210138 6.8 20Diethylphthalate37 1131-11-310138 6.8 20Dimethylphthalate50 1117-81-710138 6.8 20Bis(2-Ethylhexyl)phthalate39 1206-44-010138 0.76 1.9Fluoranthene37 186-73-710138 0.76 1.9Fluorene42 1193-39-510138 0.76 1.9Indeno(1,2,3-cd)pyrene37 190-12-010138 0.76 1.91-Methylnaphthalene33 191-57-610138 0.76 1.92-Methylnaphthalene37 191-20-310138 0.76 1.9Naphthalene33 162-75-910138 0.76 1.9N-Nitrosodimethylamine47 1117-84-010138 6.8 20Di-n-octylphthalate35 185-01-810138 0.76 1.9Phenanthrene37 1129-00-010138 0.76 1.9Pyrene

Naphthalene was detected in the method blank at a concentration of 1.1 ug/l.The blank value was not subtracted from the analytical result.

ug/kgug/kgug/kg ug/kgPesticides/PCBs SW-846 80821.1 U 163496-31-110225 1.1 3.8Aroclor 54321.1 U 112642-23-810225 1.1 3.8Aroclor 54421.1 U 111126-42-410225 1.1 3.8Aroclor 546018 112674-11-210225 0.38 1.9PCB-10160.38 U 111104-28-210225 0.38 1.9PCB-12210.38 U 111141-16-510225 0.38 1.9PCB-12320.38 U 153469-21-910225 0.38 1.9PCB-12420.38 U 112672-29-610225 0.38 1.9PCB-12486.1 111097-69-110225 0.38 1.9PCB-125421 111096-82-510225 0.44 1.9PCB-12600.38 U 137324-23-510225 0.38 1.9PCB-12620.38 U 111100-14-410225 0.38 1.9PCB-1268


Page 5 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B42,500 17429-90-501643 5.51 21.9Aluminum216 17440-42-807914 0.975 5.48Boron3,510 17440-70-201650 6.71 21.9Calcium30,600 57439-89-601654 25.8 110Iron146 17439-93-201656 0.24 2.2Lithium6,270 17439-95-401657 2.78 11.0Magnesium333 17439-96-506958 0.0854 0.548Manganese427 17723-14-010145 0.613 11.0Phosphorus3,010 17440-09-701662 19.7 54.8Potassium1,210 17440-23-501667 40.8 110Sodium135 17440-24-607968 0.0679 0.548Strontium380 17440-31-506969 1.10 11.0Tin1,720 17440-32-606970 0.416 1.10Titanium108 17440-67-710146 0.920 5.48Zirconium



13.6 27440-38-206125 0.0876 0.438Arsenic147 27440-39-306126 0.118 0.438Barium2.24 27440-41-706127 0.0175 0.110Beryllium1.39 27440-43-906128 0.0438 0.110Cadmium46.9 27440-47-306131 0.131 0.438Chromium78.9 27440-48-406132 0.0219 0.110Cobalt24.5 27440-50-806133 0.0723 0.438Copper14.2 27439-92-106135 0.0114 0.219Lead16.5 27439-98-706138 0.0548 0.110Molybdenum35.2 27440-02-006139 0.110 0.438Nickel2.82 27782-49-206141 0.0438 0.438Selenium14.4 27440-22-406142 0.0131 0.110Silver0.814 27440-28-006145 0.0329 0.110Thallium79.2 27440-62-206148 0.0241 0.110Vanadium57.1 27440-66-606149 0.613 3.29Zinc

mg/kgmg/kgmg/kg mg/kgSW-846 7471A0.172 17439-97-600159 0.0031 0.108Mercury

mg/kgmg/kgmg/kg mg/kgWet Chemistry EPA 300.04.0 116984-48-807332 0.91 1.111a Anions by 300.0 - Fluoride

ug/kgug/kgug/kg ug/kgEPA 314.0508 114797-73-010147 10.3 34.27a Perchlorate EPA 314.0

mg/kgmg/kgmg/kg mg/kgSW-846 719942.5 518540-29-905892 1.1 5.73a Cr VI by EPA 7199


Page 6 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.






Analyst



06192


06192


10326


Prep07320


07320


8270C04688

1Gregory JDrahovsky



Extract00819

1Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BCalcium016505Joanne M Gates05/18/2011 11:421113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BTitanium06970


Page 7 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






Analyst


1Tara L Snyder05/18/2011 06:421113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:15111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Cobalt061322Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:15111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:15111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:15111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 07:59111371026001A1SW-846 6020Zinc061491Damary Valentin05/18/2011 06:311113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified



07332






01352



10129




Page 1 of 7


Sample Description: SL-042-SA5A-SB-3.5-4.5MSD Soil SSFL Area IV Collocated Soil Sampling SL-042-SA5A-SB-3.5-4.5 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL042 SDG#: DE151-01MSD




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B180 0.9367-64-106192 7.1 8.5Acetone24 0.9371-43-206192 0.11 4.3Benzene23 0.93108-86-106192 0.14 4.3Bromobenzene27 0.9374-97-506192 0.35 4.3Bromochloromethane22 0.9375-27-406192 0.09 4.3Bromodichloromethane21 0.9375-25-206192 0.43 4.3Bromoform14 0.9374-83-906192 0.27 4.3Bromomethane170 0.9378-93-306192 1.3 8.52-Butanone22 0.93104-51-806192 0.13 4.3n-Butylbenzene24 0.93135-98-806192 0.06 4.3sec-Butylbenzene23 0.9398-06-606192 0.17 4.3tert-Butylbenzene25 0.9356-23-506192 0.15 4.3Carbon Tetrachloride22 0.93108-90-706192 0.12 4.3Chlorobenzene13 0.9375-00-306192 0.14 4.3Chloroethane18 0.93110-75-806192 0.32 4.32-Chloroethyl Vinyl Ether23 0.9367-66-306192 0.13 4.3Chloroform17 0.9374-87-306192 0.35 4.3Chloromethane22 0.9395-49-806192 0.15 4.32-Chlorotoluene21 0.93106-43-406192 0.15 4.34-Chlorotoluene20 1.0979-38-906192 0.62 6.2Chlorotrifluoroethene18 0.9396-12-806192 0.74 4.31,2-Dibromo-3-chloropropane21 0.93124-48-106192 0.21 4.3Dibromochloromethane20 0.93106-93-406192 0.18 4.31,2-Dibromoethane20 0.9374-95-306192 0.26 4.3Dibromomethane21 0.9395-50-106192 0.1 4.31,2-Dichlorobenzene22 0.93541-73-106192 0.13 4.31,3-Dichlorobenzene21 0.93106-46-706192 0.17 4.31,4-Dichlorobenzene17 0.9375-71-806192 0.13 4.3Dichlorodifluoromethane24 0.9375-34-306192 0.11 4.31,1-Dichloroethane21 0.93107-06-206192 0.16 4.31,2-Dichloroethane18 0.9375-35-406192 0.41 4.31,1-Dichloroethene23 0.93156-59-206192 0.20 4.3cis-1,2-Dichloroethene23 0.93156-60-506192 0.13 4.3trans-1,2-Dichloroethene23 0.9378-87-506192 0.18 4.31,2-Dichloropropane21 0.93142-28-906192 0.09 4.31,3-Dichloropropane22 0.93594-20-706192 0.18 4.32,2-Dichloropropane24 0.93563-58-606192 0.14 4.31,1-Dichloropropene21 0.9310061-01-506192 0.17 4.3cis-1,3-Dichloropropene19 0.9310061-02-606192 0.18 4.3trans-1,3-Dichloropropene22 0.93100-41-406192 0.06 4.3Ethylbenzene21 0.9376-13-106192 0.12 4.3Freon 11321 1.0975-88-706192 0.62 6.2Freon 133a24 0.9387-68-306192 0.15 4.3Hexachlorobutadiene100 0.93591-78-606192 1.7 8.52-Hexanone23 0.9398-82-806192 0.06 4.3Isopropylbenzene23 0.9399-87-606192 0.12 4.3p-Isopropyltoluene19 0.931634-04-406192 0.22 4.3Methyl Tertiary Butyl Ether91 0.93108-10-106192 0.41 8.54-Methyl-2-pentanone21 0.9375-09-206192 0.26 4.3Methylene Chloride24 0.93103-65-106192 0.07 4.3n-Propylbenzene


Page 2 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B20 0.93100-42-506192 0.11 4.3Styrene22 0.93630-20-606192 0.12 4.31,1,1,2-Tetrachloroethane20 0.9379-34-506192 0.24 4.31,1,2,2-Tetrachloroethane26 0.93127-18-406192 0.21 4.3Tetrachloroethene23 0.93108-88-306192 0.09 4.3Toluene19 0.9387-61-606192 0.15 4.31,2,3-Trichlorobenzene18 0.93120-82-106192 0.19 4.31,2,4-Trichlorobenzene23 0.9371-55-606192 0.21 4.31,1,1-Trichloroethane21 0.9379-00-506192 0.29 4.31,1,2-Trichloroethane23 0.9379-01-606192 0.16 4.3Trichloroethene18 0.9375-69-406192 0.31 4.3Trichlorofluoromethane21 0.9396-18-406192 0.35 4.31,2,3-Trichloropropane22 0.9395-63-606192 0.43 4.31,2,4-Trimethylbenzene23 0.93108-67-806192 0.11 4.31,3,5-Trimethylbenzene17 0.9375-01-406192 0.21 4.3Vinyl Chloride44 0.93179601-23-106192 0.18 4.3m+p-Xylene21 0.9395-47-606192 0.18 4.3o-Xylene

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B SIM240 23.63123-91-110326 5.4 161,4-Dioxane

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C1,800 183-32-904688 19 190Acenaphthene1,900 1208-96-804688 19 190Acenaphthylene1,400 162-53-304688 190 560Aniline1,800 1120-12-704688 19 190Anthracene2,100 J 192-87-504688 1,300 3,800Benzidine1,800 156-55-304688 19 190Benzo(a)anthracene1,800 150-32-804688 19 190Benzo(a)pyrene1,800 1205-99-204688 19 190Benzo(b)fluoranthene1,700 1191-24-204688 19 190Benzo(g,h,i)perylene1,800 1207-08-904688 19 190Benzo(k)fluoranthene980 165-85-004688 190 560Benzoic acid1,700 1100-51-604688 190 560Benzyl alcohol1,800 1101-55-304688 19 1904-Bromophenyl-phenylether1,800 185-68-704688 19 190Butylbenzylphthalate1,700 184-74-204688 19 190Di-n-butylphthalate1,800 186-74-804688 19 190Carbazole1,700 159-50-704688 38 1904-Chloro-3-methylphenol1,300 1106-47-804688 75 1904-Chloroaniline1,700 1111-91-104688 19 190bis(2-Chloroethoxy)methane1,700 1111-44-404688 19 190bis(2-Chloroethyl)ether1,600 139638-32-904688 19 190bis(2-Chloroisopropyl)ether1,700 191-58-704688 19 1902-Chloronaphthalene1,800 195-57-804688 19 1902-Chlorophenol1,800 17005-72-304688 38 1904-Chlorophenyl-phenylether1,800 1218-01-904688 19 190Chrysene1,700 153-70-304688 19 190Dibenz(a,h)anthracene1,800 1132-64-904688 19 190Dibenzofuran


Page 3 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C1,500 195-50-104688 19 1901,2-Dichlorobenzene1,400 1541-73-104688 19 1901,3-Dichlorobenzene1,500 1106-46-704688 19 1901,4-Dichlorobenzene1,200 191-94-104688 110 3803,3'-Dichlorobenzidine1,800 1120-83-204688 19 1902,4-Dichlorophenol1,700 184-66-204688 19 190Diethylphthalate1,700 1105-67-904688 38 1902,4-Dimethylphenol1,900 1108-68-904688 38 1903,5-Dimethylphenol1,800 1131-11-304688 19 190Dimethylphthalate730 1534-52-104688 190 5604,6-Dinitro-2-methylphenol670 J 151-28-504688 380 1,1002,4-Dinitrophenol1,800 1121-14-204688 38 1902,4-Dinitrotoluene1,800 1606-20-204688 19 1902,6-Dinitrotoluene1,900 1122-66-704688 19 1901,2-Diphenylhydrazine1,700 1117-81-704688 19 380bis(2-Ethylhexyl)phthalate1,800 1206-44-004688 19 190Fluoranthene1,800 186-73-704688 19 190Fluorene1,800 1118-74-104688 19 190Hexachlorobenzene1,600 187-68-304688 75 190Hexachlorobutadiene3,300 177-47-404688 190 560Hexachlorocyclopentadiene1,400 167-72-104688 19 190Hexachloroethane1,700 1193-39-504688 19 190Indeno(1,2,3-cd)pyrene1,700 178-59-104688 19 190Isophorone1,700 190-12-004688 19 1901-Methylnaphthalene1,600 191-57-604688 19 1902-Methylnaphthalene1,700 195-48-704688 38 1902-Methylphenol1,800 1106-44-504688 38 1904-Methylphenol


1,600 191-20-304688 19 190Naphthalene1,900 188-74-404688 19 1902-Nitroaniline1,800 199-09-204688 38 1903-Nitroaniline1,500 1100-01-604688 75 1904-Nitroaniline1,700 198-95-304688 19 190Nitrobenzene1,800 188-75-504688 19 1902-Nitrophenol1,600 1100-02-704688 190 5604-Nitrophenol1,700 162-75-904688 38 190N-Nitrosodimethylamine1,600 1621-64-704688 19 190N-Nitroso-di-n-propylamine1,800 186-30-604688 19 190N-Nitrosodiphenylamine


1,900 1117-84-004688 19 190Di-n-octylphthalate1,100 187-86-504688 190 560Pentachlorophenol1,800 185-01-804688 19 190Phenanthrene1,800 1108-95-204688 19 190Phenol2,000 1129-00-004688 19 190Pyrene1,700 1120-82-104688 19 1901,2,4-Trichlorobenzene1,800 195-95-404688 38 1902,4,5-Trichlorophenol


Page 4 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C1,800 188-06-204688 38 1902,4,6-Trichlorophenol


ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM35 183-32-910138 0.76 1.9Acenaphthene33 1208-96-810138 0.38 1.9Acenaphthylene36 1120-12-710138 0.38 1.9Anthracene39 156-55-310138 0.76 1.9Benzo(a)anthracene39 150-32-810138 0.76 1.9Benzo(a)pyrene42 1205-99-210138 0.76 1.9Benzo(b)fluoranthene43 1191-24-210138 0.76 1.9Benzo(g,h,i)perylene39 1207-08-910138 0.76 1.9Benzo(k)fluoranthene44 185-68-710138 6.8 20Butylbenzylphthalate41 184-74-210138 6.8 20Di-n-butylphthalate40 1218-01-910138 0.38 1.9Chrysene43 153-70-310138 0.76 1.9Dibenz(a,h)anthracene36 184-66-210138 6.8 20Diethylphthalate36 1131-11-310138 6.8 20Dimethylphthalate51 1117-81-710138 6.8 20Bis(2-Ethylhexyl)phthalate40 1206-44-010138 0.76 1.9Fluoranthene36 186-73-710138 0.76 1.9Fluorene42 1193-39-510138 0.76 1.9Indeno(1,2,3-cd)pyrene35 190-12-010138 0.76 1.91-Methylnaphthalene31 191-57-610138 0.76 1.92-Methylnaphthalene32 191-20-310138 0.76 1.9Naphthalene30 162-75-910138 0.76 1.9N-Nitrosodimethylamine47 1117-84-010138 6.8 20Di-n-octylphthalate36 185-01-810138 0.76 1.9Phenanthrene38 1129-00-010138 0.76 1.9Pyrene

Naphthalene was detected in the method blank at a concentration of 1.1 ug/l.The blank value was not subtracted from the analytical result.

ug/kgug/kgug/kg ug/kgPesticides/PCBs SW-846 80821.1 U 163496-31-110225 1.1 3.7Aroclor 54321.1 U 112642-23-810225 1.1 3.7Aroclor 54421.1 U 111126-42-410225 1.1 3.7Aroclor 546019 112674-11-210225 0.38 1.9PCB-10160.38 U 111104-28-210225 0.38 1.9PCB-12210.38 U 111141-16-510225 0.38 1.9PCB-12320.38 U 153469-21-910225 0.38 1.9PCB-12420.38 U 112672-29-610225 0.38 1.9PCB-12486.3 111097-69-110225 0.38 1.9PCB-125422 111096-82-510225 0.44 1.9PCB-12600.38 U 137324-23-510225 0.38 1.9PCB-12620.38 U 111100-14-410225 0.38 1.9PCB-1268


Page 5 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B40,800 17429-90-501643 5.67 22.6Aluminum226 17440-42-807914 1.00 5.64Boron3,570 17440-70-201650 6.91 22.6Calcium29,800 17439-89-601654 5.31 22.6Iron148 17439-93-201656 0.25 2.3Lithium6,200 17439-95-401657 2.86 11.3Magnesium334 17439-96-506958 0.0880 0.564Manganese420 17723-14-010145 0.631 11.3Phosphorus2,950 17440-09-701662 20.3 56.4Potassium1,240 17440-23-501667 42.1 113Sodium137 17440-24-607968 0.0699 0.564Strontium398 17440-31-506969 1.13 11.3Tin1,720 17440-32-606970 0.429 1.13Titanium112 17440-67-710146 0.947 5.64Zirconium



13.9 27440-38-206125 0.0902 0.451Arsenic151 27440-39-306126 0.122 0.451Barium2.38 27440-41-706127 0.0180 0.113Beryllium1.49 27440-43-906128 0.0451 0.113Cadmium44.7 27440-47-306131 0.135 0.451Chromium75.5 27440-48-406132 0.0226 0.113Cobalt24.3 27440-50-806133 0.0744 0.451Copper14.5 27439-92-106135 0.0117 0.226Lead16.2 27439-98-706138 0.0564 0.113Molybdenum35.0 27440-02-006139 0.113 0.451Nickel2.80 27782-49-206141 0.0451 0.451Selenium14.2 27440-22-406142 0.0135 0.113Silver0.860 27440-28-006145 0.0338 0.113Thallium78.7 27440-62-206148 0.0248 0.113Vanadium56.3 27440-66-606149 0.631 3.38Zinc




Page 6 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43







Analyst



06192


06192


10326


Prep07320


07320


8270C04688

1Gregory JDrahovsky



Extract00819

1Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BCalcium016501Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 06:451113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:18111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Cobalt06132


Page 7 of 7



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






Analyst


2Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:18111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:18111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:18111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 08:01111371026001A1SW-846 6020Zinc061491Damary Valentin05/18/2011 06:321113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified




Page 1 of 3


Sample Description: SL-042-SA5A-SB-3.5-4.5DUP Soil SSFL Area IV Collocated Soil Sampling SL-042-SA5A-SB-3.5-4.5 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL042 SDG#: DE151-01DUP




ActionLimit

DilutionFactor

CATNo.

mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B35,300 17429-90-501643 5.62 22.3Aluminum8.66 17440-42-807914 0.994 5.58Boron2,950 17440-70-201650 6.84 22.3Calcium27,900 17439-89-601654 5.26 22.3Iron31.5 17439-93-201656 0.25 2.2Lithium5,460 17439-95-401657 2.84 11.2Magnesium196 17439-96-506958 0.0871 0.558Manganese291 17723-14-010145 0.625 11.2Phosphorus1,420 17440-09-701662 20.1 55.8Potassium109 J 17440-23-501667 41.6 112Sodium22.6 17440-24-607968 0.0692 0.558Strontium3.28 J 17440-31-506969 1.12 11.2Tin1,370 17440-32-606970 0.424 1.12Titanium5.63 17440-67-710146 0.938 5.58Zirconium



8.57 27440-38-206125 0.0876 0.438Arsenic97.2 27440-39-306126 0.118 0.438Barium0.986 27440-41-706127 0.0175 0.110Beryllium0.0438 U 27440-43-906128 0.0438 0.110Cadmium25.6 27440-47-306131 0.131 0.438Chromium6.33 27440-48-406132 0.0219 0.110Cobalt7.82 27440-50-806133 0.0723 0.438Copper7.77 27439-92-106135 0.0114 0.219Lead1.70 27439-98-706138 0.0548 0.110Molybdenum15.5 27440-02-006139 0.110 0.438Nickel0.232 J 27782-49-206141 0.0438 0.438Selenium0.186 27440-22-406142 0.0131 0.110Silver0.237 27440-28-006145 0.0329 0.110Thallium50.3 27440-62-206148 0.0241 0.110Vanadium43.1 27440-66-606149 0.613 3.29Zinc

mg/kgmg/kgmg/kg mg/kgSW-846 7471A0.0050 J 17439-97-600159 0.0032 0.112Mercury





Page 2 of 3



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

mVmVmV mVWet Chemistry ASTM D1498400 1n.a.01821 10.0 10.032a OR Potential




6.48 1n.a.00394 0.0100 0.010018a pH by 9045C

%%% %Wet Chemistry EPA 160.3 modified12.0 1n.a.11626 0.50 0.5028a Moisture Content by 160.3

The duplicate moisture value is provided to assess the precision of themoisture test. For comparability purposes, the initial moisturedetermination is the value used to perform dry weight calculations.

12.2 1n.a.11625 0.50 0.50Moisture Content by 160.3

General Sample CommentsState of California Lab Certification No. 2501 All QC is compliant unless otherwise noted. Please refer to the QualityControl Summary for overall QC performance data and associated samples.




Analyst


1Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BCalcium016501Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 06:381113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:12111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Cobalt06132


Page 3 of 3



Collected: 05/16/2011 11:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






Analyst


2Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:12111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:12111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:12111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 07:58111371026001A1SW-846 6020Zinc061491Damary Valentin05/18/2011 06:301113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified



07332






01352



10129




1Scott W Freisher05/24/2011 17:3211144162401A1EPA 160.3 modified28a Moisture Content by160.3

11626



Page 1 of 7


Sample Description: DUP-17-SA5A-QC-051611 Soil SSFL Area IV Collocated Soil Sampling DUP-17-SA5A-QC-051611 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 11:37

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


DUP17 SDG#: DE151-02FD




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B7.4 U 0.9767-64-106192 7.4 8.8Acetone0.11 U 0.9771-43-206192 0.11 4.4Benzene0.14 U 0.97108-86-106192 0.14 4.4Bromobenzene0.36 U 0.9774-97-506192 0.36 4.4Bromochloromethane0.09 U 0.9775-27-406192 0.09 4.4Bromodichloromethane0.44 U 0.9775-25-206192 0.44 4.4Bromoform0.28 U 0.9774-83-906192 0.28 4.4Bromomethane1.3 U 0.9778-93-306192 1.3 8.82-Butanone0.13 U 0.97104-51-806192 0.13 4.4n-Butylbenzene0.07 U 0.97135-98-806192 0.07 4.4sec-Butylbenzene0.18 U 0.9798-06-606192 0.18 4.4tert-Butylbenzene0.15 U 0.9756-23-506192 0.15 4.4Carbon Tetrachloride0.12 U 0.97108-90-706192 0.12 4.4Chlorobenzene0.14 U 0.9775-00-306192 0.14 4.4Chloroethane0.33 U 0.97110-75-806192 0.33 4.42-Chloroethyl Vinyl Ether0.13 U 0.9767-66-306192 0.13 4.4Chloroform0.36 U 0.9774-87-306192 0.36 4.4Chloromethane0.15 U 0.9795-49-806192 0.15 4.42-Chlorotoluene0.15 U 0.97106-43-406192 0.15 4.44-Chlorotoluene0.55 U 0.9779-38-906192 0.55 5.5Chlorotrifluoroethene0.77 U 0.9796-12-806192 0.77 4.41,2-Dibromo-3-chloropropane0.22 U 0.97124-48-106192 0.22 4.4Dibromochloromethane0.19 U 0.97106-93-406192 0.19 4.41,2-Dibromoethane0.26 U 0.9774-95-306192 0.26 4.4Dibromomethane0.1 U 0.9795-50-106192 0.1 4.41,2-Dichlorobenzene0.13 U 0.97541-73-106192 0.13 4.41,3-Dichlorobenzene0.18 U 0.97106-46-706192 0.18 4.41,4-Dichlorobenzene0.13 U 0.9775-71-806192 0.13 4.4Dichlorodifluoromethane0.11 U 0.9775-34-306192 0.11 4.41,1-Dichloroethane0.17 U 0.97107-06-206192 0.17 4.41,2-Dichloroethane0.43 U 0.9775-35-406192 0.43 4.41,1-Dichloroethene0.21 U 0.97156-59-206192 0.21 4.4cis-1,2-Dichloroethene0.13 U 0.97156-60-506192 0.13 4.4trans-1,2-Dichloroethene0.19 U 0.9778-87-506192 0.19 4.41,2-Dichloropropane0.09 U 0.97142-28-906192 0.09 4.41,3-Dichloropropane0.19 U 0.97594-20-706192 0.19 4.42,2-Dichloropropane0.14 U 0.97563-58-606192 0.14 4.41,1-Dichloropropene0.18 U 0.9710061-01-506192 0.18 4.4cis-1,3-Dichloropropene0.19 U 0.9710061-02-606192 0.19 4.4trans-1,3-Dichloropropene0.07 U 0.97100-41-406192 0.07 4.4Ethylbenzene0.12 U 0.9776-13-106192 0.12 4.4Freon 1130.55 U 0.9775-88-706192 0.55 5.5Freon 133a0.15 U 0.9787-68-306192 0.15 4.4Hexachlorobutadiene1.8 U 0.97591-78-606192 1.8 8.82-Hexanone0.07 U 0.9798-82-806192 0.07 4.4Isopropylbenzene0.12 U 0.9799-87-606192 0.12 4.4p-Isopropyltoluene0.23 U 0.971634-04-406192 0.23 4.4Methyl Tertiary Butyl Ether0.43 U 0.97108-10-106192 0.43 8.84-Methyl-2-pentanone4.1 J 0.9775-09-206192 0.26 4.4Methylene Chloride0.08 U 0.97103-65-106192 0.08 4.4n-Propylbenzene


Page 2 of 7



Collected: 05/16/2011 11:37

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.





Page 3 of 7



Collected: 05/16/2011 11:37

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.









Page 4 of 7



Collected: 05/16/2011 11:37

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.75 U 186-73-710138 0.75 1.9Fluorene0.75 U 1193-39-510138 0.75 1.9Indeno(1,2,3-cd)pyrene0.75 U 190-12-010138 0.75 1.91-Methylnaphthalene0.75 U 191-57-610138 0.75 1.92-Methylnaphthalene0.75 U 191-20-310138 0.75 1.9Naphthalene0.75 U 162-75-910138 0.75 1.9N-Nitrosodimethylamine6.8 U 1117-84-010138 6.8 20Di-n-octylphthalate0.75 U 185-01-810138 0.75 1.9Phenanthrene0.75 U 1129-00-010138 0.75 1.9Pyrene

ug/kgug/kgug/kg ug/kgPesticides/PCBs SW-846 80821.1 U 163496-31-110225 1.1 3.7Aroclor 54321.1 U 112642-23-810225 1.1 3.7Aroclor 54421.3 J 111126-42-410225 1.1 3.7Aroclor 54600.37 U 112674-11-210225 0.37 1.9PCB-10160.37 U 111104-28-210225 0.37 1.9PCB-12210.37 U 111141-16-510225 0.37 1.9PCB-12320.37 U 153469-21-910225 0.37 1.9PCB-12420.37 U 112672-29-610225 0.37 1.9PCB-12481.7 J 111097-69-110225 0.37 1.9PCB-12541.9 111096-82-510225 0.44 1.9PCB-12600.37 U 137324-23-510225 0.37 1.9PCB-12620.37 U 111100-14-410225 0.37 1.9PCB-1268

The surrogate data is outside the QC limits. Results from thereextraction are within the limits. The hold time had expired prior tothe reextraction therefore, all results are reported from the originalextract. Similar results were obtained in both extracts.

mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B29,600 17429-90-501643 5.54 22.0Aluminum8.74 17440-42-807914 0.981 5.51Boron2,780 17440-70-201650 6.76 22.0Calcium26,800 17439-89-601654 5.19 22.0Iron32.4 17439-93-201656 0.24 2.2Lithium5,650 17439-95-401657 2.80 11.0Magnesium304 17439-96-506958 0.0860 0.551Manganese322 17723-14-010145 0.617 11.0Phosphorus2,180 17440-09-701662 19.8 55.1Potassium108 J 17440-23-501667 41.1 110Sodium21.9 17440-24-607968 0.0683 0.551Strontium3.31 J 17440-31-506969 1.10 11.0Tin1,520 17440-32-606970 0.419 1.10Titanium4.56 J 17440-67-710146 0.926 5.51Zirconium




Page 5 of 7



Collected: 05/16/2011 11:37

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

mg/kgmg/kgmg/kg mg/kgMetals SW-846 60206.91 27440-38-206125 0.0882 0.441Arsenic114 27440-39-306126 0.119 0.441Barium0.849 27440-41-706127 0.0176 0.110Beryllium0.0742 J 27440-43-906128 0.0441 0.110Cadmium20.9 27440-47-306131 0.132 0.441Chromium8.87 27440-48-406132 0.0220 0.110Cobalt8.59 27440-50-806133 0.0727 0.441Copper6.44 27439-92-106135 0.0115 0.220Lead0.918 27439-98-706138 0.0551 0.110Molybdenum15.2 27440-02-006139 0.110 0.441Nickel0.207 J 27782-49-206141 0.0441 0.441Selenium0.391 27440-22-406142 0.0132 0.110Silver0.306 27440-28-006145 0.0331 0.110Thallium43.0 27440-62-206148 0.0242 0.110Vanadium54.4 27440-66-606149 0.617 3.31Zinc









6.43 1n.a.00394 0.0100 0.010018a pH by 9045C




Page 6 of 7



Collected: 05/16/2011 11:37

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43







Analyst



06192


10326


Prep07320


07320


8270C04688

1Gregory JDrahovsky


1Sherry L Morrow05/20/2011 03:3011139SLG0261SW-846 3550BBNA Soil Extraction SIM104791Sherry L Morrow05/20/2011 03:3011139SLH0261SW-846 3550BBNA Soil Sonication003811Richard A Shober05/25/2011 12:59111380023A1SW-846 80828a PCBs/PCTs by 8082102251Roman Kuropatkin05/19/2011 05:15111380023A1SW-846 3550BSolid Sample Pesticide

Extract00819

1Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BCalcium016501Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 07:371113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:27111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Cobalt061322Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:27111371026001C1SW-846 6020Molybdenum06138


Page 7 of 7



Collected: 05/16/2011 11:37

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






Analyst


2Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:27111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:27111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 08:05111371026001A1SW-846 6020Zinc061491Damary Valentin05/18/2011 06:331113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified



07332






01352



10129






Page 1 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B7.4 U 1.0267-64-106192 7.4 8.9Acetone0.11 U 1.0271-43-206192 0.11 4.4Benzene0.14 U 1.02108-86-106192 0.14 4.4Bromobenzene0.37 U 1.0274-97-506192 0.37 4.4Bromochloromethane0.09 U 1.0275-27-406192 0.09 4.4Bromodichloromethane0.44 U 1.0275-25-206192 0.44 4.4Bromoform0.28 U 1.0274-83-906192 0.28 4.4Bromomethane1.4 U 1.0278-93-306192 1.4 8.92-Butanone0.13 U 1.02104-51-806192 0.13 4.4n-Butylbenzene0.07 U 1.02135-98-806192 0.07 4.4sec-Butylbenzene0.18 U 1.0298-06-606192 0.18 4.4tert-Butylbenzene0.15 U 1.0256-23-506192 0.15 4.4Carbon Tetrachloride0.12 U 1.02108-90-706192 0.12 4.4Chlorobenzene0.14 U 1.0275-00-306192 0.14 4.4Chloroethane0.33 U 1.02110-75-806192 0.33 4.42-Chloroethyl Vinyl Ether0.13 U 1.0267-66-306192 0.13 4.4Chloroform0.37 U 1.0274-87-306192 0.37 4.4Chloromethane0.15 U 1.0295-49-806192 0.15 4.42-Chlorotoluene0.15 U 1.02106-43-406192 0.15 4.44-Chlorotoluene0.55 U 1.0279-38-906192 0.55 5.5Chlorotrifluoroethene0.78 U 1.0296-12-806192 0.78 4.41,2-Dibromo-3-chloropropane0.22 U 1.02124-48-106192 0.22 4.4Dibromochloromethane0.19 U 1.02106-93-406192 0.19 4.41,2-Dibromoethane0.27 U 1.0274-95-306192 0.27 4.4Dibromomethane0.1 U 1.0295-50-106192 0.1 4.41,2-Dichlorobenzene0.13 U 1.02541-73-106192 0.13 4.41,3-Dichlorobenzene0.18 U 1.02106-46-706192 0.18 4.41,4-Dichlorobenzene0.13 U 1.0275-71-806192 0.13 4.4Dichlorodifluoromethane0.11 U 1.0275-34-306192 0.11 4.41,1-Dichloroethane0.17 U 1.02107-06-206192 0.17 4.41,2-Dichloroethane0.43 U 1.0275-35-406192 0.43 4.41,1-Dichloroethene0.21 U 1.02156-59-206192 0.21 4.4cis-1,2-Dichloroethene0.13 U 1.02156-60-506192 0.13 4.4trans-1,2-Dichloroethene0.19 U 1.0278-87-506192 0.19 4.41,2-Dichloropropane0.09 U 1.02142-28-906192 0.09 4.41,3-Dichloropropane0.19 U 1.02594-20-706192 0.19 4.42,2-Dichloropropane0.14 U 1.02563-58-606192 0.14 4.41,1-Dichloropropene0.18 U 1.0210061-01-506192 0.18 4.4cis-1,3-Dichloropropene0.19 U 1.0210061-02-606192 0.19 4.4trans-1,3-Dichloropropene0.07 U 1.02100-41-406192 0.07 4.4Ethylbenzene0.12 U 1.0276-13-106192 0.12 4.4Freon 1130.55 U 1.0275-88-706192 0.55 5.5Freon 133a0.15 U 1.0287-68-306192 0.15 4.4Hexachlorobutadiene1.8 U 1.02591-78-606192 1.8 8.92-Hexanone0.66 J 1.0298-82-806192 0.07 4.4Isopropylbenzene0.12 U 1.0299-87-606192 0.12 4.4p-Isopropyltoluene0.23 U 1.021634-04-406192 0.23 4.4Methyl Tertiary Butyl Ether0.43 U 1.02108-10-106192 0.43 8.94-Methyl-2-pentanone6.2 1.0275-09-206192 0.27 4.4Methylene Chloride0.08 U 1.02103-65-106192 0.08 4.4n-Propylbenzene


Page 2 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




ActionLimit

DilutionFactor

CATNo.



ng/kgng/kgng/kg ng/kgGC/MS Semivolatiles EPA 1625C18.0 U 162-75-911622 18.0 36.0N-Nitrosodimethylamine

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C180 U 162-53-304688 180 540Aniline1,300 U 192-87-504688 1,300 3,600Benzidine180 U 165-85-004688 180 540Benzoic acid180 U 1100-51-604688 180 540Benzyl alcohol18 U 1101-55-304688 18 1804-Bromophenyl-phenylether18 U 186-74-804688 18 180Carbazole36 U 159-50-704688 36 1804-Chloro-3-methylphenol72 U 1106-47-804688 72 1804-Chloroaniline18 U 1111-91-104688 18 180bis(2-Chloroethoxy)methane18 U 1111-44-404688 18 180bis(2-Chloroethyl)ether18 U 139638-32-904688 18 180bis(2-Chloroisopropyl)ether18 U 191-58-704688 18 1802-Chloronaphthalene18 U 195-57-804688 18 1802-Chlorophenol36 U 17005-72-304688 36 1804-Chlorophenyl-phenylether18 U 1132-64-904688 18 180Dibenzofuran18 U 195-50-104688 18 1801,2-Dichlorobenzene18 U 1541-73-104688 18 1801,3-Dichlorobenzene18 U 1106-46-704688 18 1801,4-Dichlorobenzene110 U 191-94-104688 110 3603,3'-Dichlorobenzidine18 U 1120-83-204688 18 1802,4-Dichlorophenol36 U 1105-67-904688 36 1802,4-Dimethylphenol36 U 1108-68-904688 36 1803,5-Dimethylphenol180 U 1534-52-104688 180 5404,6-Dinitro-2-methylphenol360 U 151-28-504688 360 1,1002,4-Dinitrophenol


Page 3 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C36 U 1121-14-204688 36 1802,4-Dinitrotoluene18 U 1606-20-204688 18 1802,6-Dinitrotoluene18 U 1122-66-704688 18 1801,2-Diphenylhydrazine18 J 1117-81-704688 18 360bis(2-Ethylhexyl)phthalate18 U 1118-74-104688 18 180Hexachlorobenzene72 U 187-68-304688 72 180Hexachlorobutadiene180 U 177-47-404688 180 540Hexachlorocyclopentadiene18 U 167-72-104688 18 180Hexachloroethane18 U 178-59-104688 18 180Isophorone36 U 195-48-704688 36 1802-Methylphenol36 U 1106-44-504688 36 1804-Methylphenol






ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.72 U 183-32-910138 0.72 1.8Acenaphthene0.36 U 1208-96-810138 0.36 1.8Acenaphthylene0.66 J 1120-12-710138 0.36 1.8Anthracene1.0 J 156-55-310138 0.72 1.8Benzo(a)anthracene1.4 J 150-32-810138 0.72 1.8Benzo(a)pyrene2.0 1205-99-210138 0.72 1.8Benzo(b)fluoranthene1.2 J 1191-24-210138 0.72 1.8Benzo(g,h,i)perylene0.98 J 1207-08-910138 0.72 1.8Benzo(k)fluoranthene6.5 U 185-68-710138 6.5 19Butylbenzylphthalate6.5 U 184-74-210138 6.5 19Di-n-butylphthalate1.2 J 1218-01-910138 0.36 1.8Chrysene0.72 U 153-70-310138 0.72 1.8Dibenz(a,h)anthracene


Page 4 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM6.5 U 184-66-210138 6.5 19Diethylphthalate6.5 U 1131-11-310138 6.5 19Dimethylphthalate0.83 J 1206-44-010138 0.72 1.8Fluoranthene0.72 U 186-73-710138 0.72 1.8Fluorene0.98 J 1193-39-510138 0.72 1.8Indeno(1,2,3-cd)pyrene0.72 U 190-12-010138 0.72 1.81-Methylnaphthalene0.72 U 191-57-610138 0.72 1.82-Methylnaphthalene0.72 U 191-20-310138 0.72 1.8Naphthalene0.72 U 162-75-910138 0.72 1.8N-Nitrosodimethylamine6.5 U 1117-84-010138 6.5 19Di-n-octylphthalate0.72 U 185-01-810138 0.72 1.8Phenanthrene0.76 J 1129-00-010138 0.72 1.8Pyrene

mg/kgmg/kgmg/kg mg/kgGC Volatiles TPH GRO SW-846 8015Bmod

0.2 U 26.43n.a.05551 0.2 1.19a TPH by EPA 8015B Gas C5-C12

ug/kgug/kgug/kg ug/kgExplosives SW-846 8330A62 U 119406-51-010132 62 120 1000000

04-Amino-2,6-Dinitrotoluene

42 U 135572-78-210132 42 120 10000000


83 U 159229-75-310132 83 250 10000000

2,6-Diamino-4-nitrotoluene

83 U 16629-29-410132 83 250 10000000


42 U 199-65-010132 42 120 10000000

1,3-Dinitrobenzene

42 U 1121-14-210132 42 120 10000000

2,4-Dinitrotoluene

42 U 1606-20-210132 42 120 10000000

2,6-Dinitrotoluene

100 U 12691-41-010132 100 310 10000000

HMX

42 U 198-95-310132 42 120 10000000

Nitrobenzene

830 U 155-63-010132 830 2,500 10000000

Nitroglycerin

83 U 188-72-210132 83 120 10000000

2-Nitrotoluene

100 U 199-08-110132 100 120 10000000

3-Nitrotoluene

83 U 199-99-010132 83 120 10000000

4-Nitrotoluene

830 U 178-11-510132 830 2,500 10000000

PETN

52 U 1121-82-410132 52 120 10000000

RDX


Page 5 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




ActionLimit

DilutionFactor

CATNo.


0Tetryl

42 U 199-35-410132 42 120 10000000

1,3,5-Trinitrobenzene

42 U 1118-96-710132 42 120 10000000

2,4,6-Trinitrotoluene

The LCSD recovery for 2,4-diamino-6-nitrotoluene and 2,6-diamino-4-nitrotolueneis outside the QC limits. Results from the reextraction are within the limits.The hold time had expired prior to the reextraction so all results are reportedfrom the original extract. Similar results were obtained in both extracts.

ug/kgug/kgug/kg ug/kgHPLC Organics SW-846 8315A680 J 150-00-004173 650 1,60025a Formaldehyde 8315A

ug/kgug/kgug/kg ug/kgPesticides/PCBs SW-846 80821.1 U 163496-31-110225 1.1 3.6Aroclor 54321.1 U 112642-23-810225 1.1 3.6Aroclor 54421.1 U 111126-42-410225 1.1 3.6Aroclor 54600.36 U 112674-11-210225 0.36 1.8PCB-10160.36 U 111104-28-210225 0.36 1.8PCB-12210.36 U 111141-16-510225 0.36 1.8PCB-12320.36 U 153469-21-910225 0.36 1.8PCB-12420.36 U 112672-29-610225 0.36 1.8PCB-12480.36 U 111097-69-110225 0.36 1.8PCB-12540.42 U 111096-82-510225 0.42 1.8PCB-12600.36 U 137324-23-510225 0.36 1.8PCB-12620.36 U 111100-14-410225 0.36 1.8PCB-1268

mg/kgmg/kgmg/kg mg/kgGC Extractable TPH SW-846 8015B modified

0.43 U 1n.a.10199 0.43 1.3EFH (C12-C14)0.43 U 1n.a.10199 0.43 1.3EFH (C15-C20)1.9 1n.a.10199 0.43 1.3EFH (C21-C30)5.2 1n.a.10199 0.43 1.3EFH (C30 - C40)0.43 U 1n.a.10199 0.43 1.3EFH (C8-C11)

ug/kgug/kgug/kg ug/kgGC Miscellaneous SW-846 8015B110 U 164-17-510501 110 540Ethanol110 U 167-63-010501 110 540Isopropanol110 U 167-56-110501 110 540Methanol

mg/kgmg/kgmg/kg mg/kgGC Miscellaneous SW-846 8015B modified

5.4 U 1111-46-608283 5.4 11Diethylene glycol5.4 U 1107-21-108283 5.4 11Ethylene glycol5.4 U 157-55-608283 5.4 11Propylene glycol


Page 6 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




ActionLimit

DilutionFactor

CATNo.

mg/kgmg/kgmg/kg mg/kgTerphenyls SW-846 8015B1.6 U 192-06-810318 1.6 3.8m-Terphenyl1.6 U 184-15-110318 1.6 3.8o-Terphenyl1.6 U 192-94-410318 1.6 3.8p-Terphenyl

mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B12,500 17429-90-501643 5.23 20.8Aluminum7.69 17440-42-807914 0.926 5.20Boron2,710 17440-70-201650 6.38 20.8Calcium20,000 17439-89-601654 4.90 20.8Iron18.8 17439-93-201656 0.23 2.1Lithium4,390 17439-95-401657 2.64 10.4Magnesium269 17439-96-506958 0.0812 0.520Manganese340 17723-14-010145 0.583 10.4Phosphorus2,160 17440-09-701662 18.7 52.0Potassium88.9 J 17440-23-501667 38.8 104Sodium17.3 17440-24-607968 0.0645 0.520Strontium2.92 J 17440-31-506969 1.04 10.4Tin1,120 17440-32-606970 0.395 1.04Titanium2.97 J 17440-67-710146 0.874 5.20Zirconium



7.02 27440-38-206125 0.0841 0.420Arsenic90.4 27440-39-306126 0.113 0.420Barium0.749 27440-41-706127 0.0168 0.105Beryllium0.191 27440-43-906128 0.0420 0.105Cadmium20.7 27440-47-306131 0.126 0.420Chromium7.70 27440-48-406132 0.0210 0.105Cobalt27.4 27440-50-806133 0.0693 0.420Copper10.3 27439-92-106135 0.0109 0.210Lead0.573 27439-98-706138 0.0525 0.105Molybdenum14.3 27440-02-006139 0.105 0.420Nickel0.154 J 27782-49-206141 0.0420 0.420Selenium1.47 27440-22-406142 0.0126 0.105Silver0.322 27440-28-006145 0.0315 0.105Thallium41.4 27440-62-206148 0.0231 0.105Vanadium64.5 27440-66-606149 0.588 3.15Zinc


mg/kgmg/kgmg/kg mg/kgWet Chemistry EPA 300.01.7 116984-48-807332 0.87 1.111a Anions by 300.0 - Fluoride0.92 J 114797-55-807336 0.87 1.611a Anions by 300.0 - Nitrate


Page 7 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgWet Chemistry EPA 314.09.7 U 114797-73-010147 9.7 32.57a Perchlorate EPA 314.0


mg/kgmg/kgmg/kg mg/kgSW-846 9012B0.19 U 157-12-505895 0.19 0.5417a Cyanide by 9012B





6.59 1n.a.00394 0.0100 0.010018a pH by 9045C







Analyst



06192


10326


Prep07320


07320

n.a.Lois E Hiltz05/17/2011 19:252011137244351SW-846 5035GC/MS-HL Encore Prep-NC075781Matthew S Woods06/08/2011 17:4611146SLE0261EPA 1625C15a NDMA by 1625C11622


Page 8 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




Analyst


1Brian K Graham05/24/2011 06:5811139SLH0261SW-846 8270C5a Semivolatiles by EPA8270C

04688

1Gregory JDrahovsky


1Olivia I Santiago05/27/2011 14:3011146SLE0262SW-846 3546NDMA Soil Microwave116301Sherry L Morrow05/20/2011 03:3011139SLG0261SW-846 3550BBNA Soil Extraction SIM104791Sherry L Morrow05/20/2011 03:3011139SLH0261SW-846 3550BBNA Soil Sonication0038126.43Elizabeth J Marin05/23/2011 15:3911139A34A1TPH GRO SW-846

8015B mod9a TPH by EPA 8015B Gas C5-C12

05551

n.a.Lois E Hiltz05/17/2011 19:242011137244351SW-846 5035GC - 5 g HL Encore Prep061301James H Place05/27/2011 02:04111450004A1SW-846 8330A16a Energetics by 8330A101321Michele D Hamilton05/23/2011 19:06111400002A1SW-846 8315A25a Formaldehyde 8315A04173

1Sarah M Snyder05/25/2011 13:17111380023A1SW-846 80828a PCBs/PCTs by 8082102251Roman Kuropatkin05/19/2011 05:15111380023A1SW-846 3550BSolid Sample Pesticide

Extract00819

1Wanda F Oswald05/20/2011 13:30111400002A1SW-846 8315AFormaldehyde SolidExtraction

05876

1Kelli M Barto05/25/2011 18:30111450004A1SW-846 8330Energetics Extraction111371Tracy A Cole05/25/2011 06:36111380034A1SW-846 8015B

modified9a TPH by EPA 8015BOil/Diesel

10199

1Tyler O Griffin05/19/2011 23:48111390030A1SW-846 8015B19a Alcohols by 8015B105011Dustin A

Underkoffler05/20/2011 18:26111370018A1SW-846 8015B

modified21a Glycols by 8015B08283

1Melissa McDermott05/24/2011 19:18111390019A1SW-846 8015B20a Terphenyls by 8015B103181Kerrie A Freeburn05/19/2011 09:00111380034A1SW-846 3550BEFH Extraction - Soils112381Sherry L Morrow05/20/2011 03:30111390019A1SW-846 3550BTerphenyls soil prep103031Tyler O Griffin05/19/2011 16:45111390030A1SW-846 8015BSolids Extraction for

Alcohols00380

1Dustin AUnderkoffler

05/20/2011 12:00111370018A1SW-846 8015Bmodified

Solids Glycol Extraction11551

1Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BCalcium016501Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 07:471113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:37111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Cadmium06128


Page 9 of 9



Collected: 05/16/2011 16:17

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


SL167 SDG#: DE151-03




Analyst


2Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Cobalt061322Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:37111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:37111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:37111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 08:10111371026001A1SW-846 6020Zinc061495Damary Valentin05/18/2011 06:461113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified



07332

1Ashley M Adams05/22/2011 14:0911141621202B1EPA 300.011a Anions by 300.0 -Nitrate

07336




1K RobertCaulfeild-James

05/25/2011 10:5511144102201A1SW-846 9012B17a Cyanide by 9012B05895



01352



10129

1Nancy J Shoop05/24/2011 09:1011144102201A1SW-846 9012BCyanide Solid Distillation058961Michele L Graham05/19/2011 14:4511139182102A1ASTM D149832a OR Potential018211Michele L Graham05/19/2011 14:4511139039402A1SW-846 9045C





Page 1 of 6

LLI Sample # WW 6288935LLI Group # 1247140Account # 13013

Sample Description: EB15-SA5A-SB-051611 Water SSFL Area IV Collocated Soil Sampling EB15-SA5A-SB-051611 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 14:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


EB-15 SDG#: DE151-04EB

As ReceivedLimit ofQuantitation

As ReceivedMethodDetection Limit*

As ReceivedResultAnalysis Name CAS Number

ActionLimit

DilutionFactor

CATNo.

ug/lug/lug/l ug/lGC/MS Volatiles SW-846 8260B6 U 167-64-110904 6 20Acetone0.5 U 171-43-210904 0.5 5Benzene1 U 1108-86-110904 1 5Bromobenzene1 U 174-97-510904 1 5Bromochloromethane1 U 175-27-410904 1 5Bromodichloromethane1 U 175-25-210904 1 5Bromoform1 U 174-83-910904 1 5Bromomethane3 U 178-93-310904 3 102-Butanone1 U 1104-51-810904 1 5n-Butylbenzene1 U 1135-98-810904 1 5sec-Butylbenzene1 U 198-06-610904 1 5tert-Butylbenzene1 U 156-23-510904 1 5Carbon Tetrachloride0.8 U 1108-90-710904 0.8 5Chlorobenzene1 U 175-00-310904 1 5Chloroethane2 U 1110-75-810904 2 102-Chloroethyl Vinyl Ether

2-Chloroethyl vinyl ether may not be recovered if acid was used topreserve this sample.

0.8 U 167-66-310904 0.8 5Chloroform1 U 174-87-310904 1 5Chloromethane1 U 195-49-810904 1 52-Chlorotoluene1 U 1106-43-410904 1 54-Chlorotoluene2 U 179-38-910904 2 5Chlorotrifluoroethene2 U 196-12-810904 2 51,2-Dibromo-3-chloropropane1 U 1124-48-110904 1 5Dibromochloromethane1 U 1106-93-410904 1 51,2-Dibromoethane1 U 174-95-310904 1 5Dibromomethane1 U 195-50-110904 1 51,2-Dichlorobenzene1 U 1541-73-110904 1 51,3-Dichlorobenzene1 U 1106-46-710904 1 51,4-Dichlorobenzene2 U 175-71-810904 2 5Dichlorodifluoromethane1 U 175-34-310904 1 51,1-Dichloroethane1 U 1107-06-210904 1 51,2-Dichloroethane0.8 U 175-35-410904 0.8 51,1-Dichloroethene0.8 U 1156-59-210904 0.8 5cis-1,2-Dichloroethene0.8 U 1156-60-510904 0.8 5trans-1,2-Dichloroethene1 U 178-87-510904 1 51,2-Dichloropropane1 U 1142-28-910904 1 51,3-Dichloropropane1 U 1594-20-710904 1 52,2-Dichloropropane1 U 1563-58-610904 1 51,1-Dichloropropene1 U 110061-01-510904 1 5cis-1,3-Dichloropropene1 U 110061-02-610904 1 5trans-1,3-Dichloropropene0.8 U 1100-41-410904 0.8 5Ethylbenzene2 U 176-13-110904 2 10Freon 1132 U 175-88-710904 2 5Freon 133a2 U 187-68-310904 2 5Hexachlorobutadiene3 U 1591-78-610904 3 102-Hexanone1 U 198-82-810904 1 5Isopropylbenzene1 U 199-87-610904 1 5p-Isopropyltoluene0.5 U 11634-04-410904 0.5 5Methyl Tertiary Butyl Ether3 U 1108-10-110904 3 104-Methyl-2-pentanone


Page 2 of 6



Collected: 05/16/2011 14:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/lug/lug/l ug/lGC/MS Volatiles SW-846 8260B2 U 175-09-210904 2 5Methylene Chloride1 U 1103-65-110904 1 5n-Propylbenzene1 U 1100-42-510904 1 5Styrene1 U 1630-20-610904 1 51,1,1,2-Tetrachloroethane1 U 179-34-510904 1 51,1,2,2-Tetrachloroethane0.8 U 1127-18-410904 0.8 5Tetrachloroethene0.7 U 1108-88-310904 0.7 5Toluene1 U 187-61-610904 1 51,2,3-Trichlorobenzene1 U 1120-82-110904 1 51,2,4-Trichlorobenzene0.8 U 171-55-610904 0.8 51,1,1-Trichloroethane0.8 U 179-00-510904 0.8 51,1,2-Trichloroethane1 U 179-01-610904 1 5Trichloroethene2 U 175-69-410904 2 5Trichlorofluoromethane1 U 196-18-410904 1 51,2,3-Trichloropropane1 U 195-63-610904 1 51,2,4-Trimethylbenzene1 U 1108-67-810904 1 51,3,5-Trimethylbenzene1 U 175-01-410904 1 5Vinyl Chloride0.8 U 1179601-23-110904 0.8 5m+p-Xylene0.8 U 195-47-610904 0.8 5o-Xylene

ug/lug/lug/l ug/lGC/MS Volatiles SW-846 8260B SIM0.5 U 1123-91-100527 0.5 2.01,4-Dioxane

ug/lug/lug/l ug/lGC/MS Semivolatiles SW-846 8270C1 U 162-53-304678 1 6Aniline22 U 192-87-504678 22 67Benzidine7 U 165-85-004678 7 17Benzoic acid6 U 1100-51-604678 6 17Benzyl alcohol1 U 1101-55-304678 1 64-Bromophenyl-phenylether1 U 186-74-804678 1 6Carbazole1 U 159-50-704678 1 64-Chloro-3-methylphenol1 U 1106-47-804678 1 64-Chloroaniline1 U 1111-91-104678 1 6bis(2-Chloroethoxy)methane1 U 1111-44-404678 1 6bis(2-Chloroethyl)ether1 U 139638-32-904678 1 6bis(2-Chloroisopropyl)ether2 U 191-58-704678 2 62-Chloronaphthalene1 U 195-57-804678 1 62-Chlorophenol2 U 17005-72-304678 2 64-Chlorophenyl-phenylether1 U 1132-64-904678 1 6Dibenzofuran1 U 195-50-104678 1 61,2-Dichlorobenzene1 U 1541-73-104678 1 61,3-Dichlorobenzene1 U 1106-46-704678 1 61,4-Dichlorobenzene2 U 191-94-104678 2 63,3'-Dichlorobenzidine1 U 1120-83-204678 1 62,4-Dichlorophenol3 U 1105-67-904678 3 112,4-Dimethylphenol3 U 1108-68-904678 3 113,5-Dimethylphenol6 U 1534-52-104678 6 174,6-Dinitro-2-methylphenol11 U 151-28-504678 11 332,4-Dinitrophenol1 U 1121-14-204678 1 62,4-Dinitrotoluene


Page 3 of 6



Collected: 05/16/2011 14:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/lug/lug/l ug/lGC/MS Semivolatiles SW-846 8270C1 U 1606-20-204678 1 62,6-Dinitrotoluene1 U 1122-66-704678 1 61,2-Diphenylhydrazine1 U 1118-74-104678 1 6Hexachlorobenzene1 U 187-68-304678 1 6Hexachlorobutadiene6 U 177-47-404678 6 17Hexachlorocyclopentadiene1 U 167-72-104678 1 6Hexachloroethane1 U 178-59-104678 1 6Isophorone1 U 195-48-704678 1 62-Methylphenol2 U 1106-44-504678 2 64-Methylphenol





The LCS and/or LCSD recoveries are outside the stated QC windowbut within the marginal exceedance allowance of +/- 4 standarddeviations as defined in the NELAC Standards. The followinganalytes are accepted based on this allowance:4-methylphenol

ug/lug/lug/l ug/lGC/MS Semivolatiles SW-846 8270C SIM0.011 U 183-32-910137 0.011 0.054Acenaphthene0.011 U 1208-96-810137 0.011 0.054Acenaphthylene0.011 U 1120-12-710137 0.011 0.054Anthracene0.011 U 156-55-310137 0.011 0.054Benzo(a)anthracene0.011 U 150-32-810137 0.011 0.054Benzo(a)pyrene0.011 U 1205-99-210137 0.011 0.054Benzo(b)fluoranthene0.011 U 1191-24-210137 0.011 0.054Benzo(g,h,i)perylene0.011 U 1207-08-910137 0.011 0.054Benzo(k)fluoranthene0.054 U 185-68-710137 0.054 1.1Butylbenzylphthalate0.054 U 184-74-210137 0.054 1.1Di-n-butylphthalate0.011 U 1218-01-910137 0.011 0.054Chrysene0.011 U 153-70-310137 0.011 0.054Dibenz(a,h)anthracene0.054 U 184-66-210137 0.054 1.1Diethylphthalate0.054 U 1131-11-310137 0.054 1.1Dimethylphthalate0.054 U 1117-81-710137 0.054 1.1Bis(2-Ethylhexyl)phthalate


Page 4 of 6



Collected: 05/16/2011 14:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

ug/lug/lug/l ug/lGC/MS Semivolatiles SW-846 8270C SIM0.011 U 1206-44-010137 0.011 0.054Fluoranthene0.011 U 186-73-710137 0.011 0.054Fluorene0.011 U 1193-39-510137 0.011 0.054Indeno(1,2,3-cd)pyrene0.031 J 190-12-010137 0.011 0.0541-Methylnaphthalene0.033 J 191-57-610137 0.011 0.0542-Methylnaphthalene0.22 191-20-310137 0.032 0.054Naphthalene0.030 J 162-75-910137 0.011 0.054N-Nitrosodimethylamine0.054 U 1117-84-010137 0.054 1.1Di-n-octylphthalate0.011 U 185-01-810137 0.011 0.054Phenanthrene0.011 U 1129-00-010137 0.011 0.054Pyrene

Reporting limits were raised due to limited sample volume.

ug/lug/lug/l ug/lPesticides/PCBs SW-846 80820.10 U 163496-31-110227 0.10 0.52Aroclor 54320.10 U 112642-23-810227 0.10 0.52Aroclor 54420.10 U 111126-42-410227 0.10 0.52Aroclor 54600.10 U 112674-11-210227 0.10 0.52PCB-10160.10 U 111104-28-210227 0.10 0.52PCB-12210.21 U 111141-16-510227 0.21 0.52PCB-12320.10 U 153469-21-910227 0.10 0.52PCB-12420.10 U 112672-29-610227 0.10 0.52PCB-12480.10 U 111097-69-110227 0.10 0.52PCB-12540.16 U 111096-82-510227 0.16 0.52PCB-12600.21 U 137324-23-510227 0.21 0.52PCB-12620.17 U 111100-14-410227 0.17 0.52PCB-1268

mg/lmg/lmg/l mg/lMetals SW-846 6010B0.0834 U 17429-90-501743 0.0834 0.200Aluminum0.0195 J 17440-42-808014 0.0138 0.0500Boron0.0702 U 17440-70-201750 0.0702 0.200Calcium0.0522 U 17439-89-601754 0.0522 0.200Iron0.0024 U 17439-93-201756 0.0024 0.0200Lithium0.0172 U 17439-95-401757 0.0172 0.100Magnesium0.00084 U 17439-96-507058 0.00084 0.0050Manganese0.0089 U 17723-14-010143 0.0089 0.100Phosphorus0.239 U 17440-09-701762 0.239 0.500Potassium0.433 U 17440-23-501767 0.433 1.00Sodium0.00089 U 17440-24-608068 0.00089 0.0050Strontium0.0098 U 17440-31-507069 0.0098 0.0200Tin0.0038 U 17440-32-607070 0.0038 0.0100Titanium0.0206 U 17440-67-710144 0.0206 0.0500Zirconium

mg/lmg/lmg/l mg/lSW-846 60200.00030 U 17440-36-006024 0.00030 0.0010Antimony0.00095 U 17440-38-206025 0.00095 0.0020Arsenic0.00053 U 17440-39-306026 0.00053 0.0020Barium0.00013 U 17440-41-706027 0.00013 0.00050Beryllium0.00020 U 17440-43-906028 0.00020 0.00050Cadmium0.00060 U 17440-47-306031 0.00060 0.0020Chromium


Page 5 of 6



Collected: 05/16/2011 14:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






ActionLimit

DilutionFactor

CATNo.

mg/lmg/lmg/l mg/lMetals SW-846 60200.00010 U 17440-48-406032 0.00010 0.00050Cobalt0.00038 U 17440-50-806033 0.00038 0.0020Copper0.000052 U 17439-92-106035 0.000052 0.0010Lead0.00025 U 17439-98-706038 0.00025 0.00050Molybdenum0.00050 U 17440-02-006039 0.00050 0.0020Nickel0.00025 U 17782-49-206041 0.00025 0.0020Selenium0.000080 U 17440-22-406042 0.000080 0.00050Silver0.00015 U 17440-28-006045 0.00015 0.00050Thallium0.00016 U 17440-62-206048 0.00016 0.00050Vanadium0.0040 U 17440-66-606049 0.0040 0.0150Zinc

mg/lmg/lmg/l mg/lSW-846 7470A0.000046 U 17439-97-600259 0.000046 0.00020Mercury

mg/lmg/lmg/l mg/lWet Chemistry EPA 300.00.080 U 116984-48-801504 0.080 0.1011b Anions by 300.0 - Fluoride

ug/lug/lug/l ug/lEPA 314.00.70 U 114797-73-006019 0.70 2.07b Perchlorate EPA 314.0

ug/lug/lug/l ug/lSW-846 71995.0 U 118540-29-906467 5.0 10.03b Cr VI by EPA 7199


SW-846 9040B

5.6 1n.a.00200 0.010 0.01018b pH by 9040B





Analyst


1Kevin A Sposito05/17/2011 23:51L111372AA1SW-846 8260B1b Volatile OrganicsEPA8260

10904

1Jason M Long05/17/2011 13:32E111371AA1SW-846 8260B SIM14b 1,4-Dioxane by 8260BSIM

00527

1Jason M Long05/17/2011 13:32E111371AA1SW-846 5030BGC/MS VOA Water Prep011631Kevin A Sposito05/17/2011 23:51L111372AA2SW-846 5030BGC/MS VOA Water Prep011631Brian K Graham05/21/2011 07:2211138WAD0261SW-846 8270C5b Semivolatiles by EPA

8270C04678


Page 6 of 6



Collected: 05/16/2011 14:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43






Analyst


1Gregory JDrahovsky

05/19/2011 23:3611138WAG0261SW-846 8270C SIM4b Select SVOC EPA 8270SIM10137

1Timothy JAttenberger

05/18/2011 15:2011138WAD0261SW-846 3510CBNA Water Extraction00813

1Timothy JAttenberger

05/18/2011 15:2011138WAG0261SW-846 3510CBNA Water Extraction SIM10466

1Sarah M Snyder05/20/2011 21:42111380016A1SW-846 80828b PCBs/PCTs by 8082102271Sherry L Morrow05/19/2011 02:00111380016A1SW-846 3510CPCB Waters Extraction111171John P Hook05/19/2011 18:541113818480021SW-846 6010BAluminum017431John P Hook05/19/2011 18:541113818480021SW-846 6010BBoron080141John P Hook05/19/2011 18:541113818480021SW-846 6010BCalcium017501John P Hook05/19/2011 18:541113818480021SW-846 6010BIron017541John P Hook05/19/2011 18:541113818480021SW-846 6010BLithium017561John P Hook05/19/2011 18:541113818480021SW-846 6010BMagnesium017571John P Hook05/19/2011 18:541113818480021SW-846 6010BManganese070581John P Hook05/19/2011 18:541113818480021SW-846 6010BPhosphorus101431John P Hook05/19/2011 18:541113818480021SW-846 6010BPotassium017621John P Hook05/19/2011 18:541113818480021SW-846 6010BSodium017671John P Hook05/19/2011 18:541113818480021SW-846 6010BStrontium080681John P Hook05/19/2011 18:541113818480021SW-846 6010BTin070691John P Hook05/19/2011 18:541113818480021SW-846 6010BTitanium070701John P Hook05/19/2011 18:541113818480021SW-846 6010BZirconium101441Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Antimony060241Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Arsenic060251Choon Y Tian05/20/2011 11:40111386050002D1SW-846 6020Barium060261Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Beryllium060271Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Cadmium060281Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Chromium060311Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Cobalt060321Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Copper060331Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Lead060351Choon Y Tian05/20/2011 11:40111386050002C1SW-846 6020Molybdenum060381Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Nickel060391Choon Y Tian05/20/2011 11:40111386050002B1SW-846 6020Selenium060411Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Silver060421Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Thallium060451Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Vanadium060481Choon Y Tian05/20/2011 11:40111386050002A1SW-846 6020Zinc060491Damary Valentin05/19/2011 09:311113857130021SW-846 7470AMercury002591Denise K Conners05/19/2011 09:101113818480021SW-846 3005AWW SW846 ICP Digest (tot

rec)01848

1Denise K Conners05/19/2011 09:081113860500021SW-846 3020AICP/MS SW-846 Water Digest060501Damary Valentin05/19/2011 04:301113857130021SW-846 7470AWW SW846 Hg Digest057131Ashley M Adams05/20/2011 07:4811139196902B1EPA 300.011b Anions by 300.0 -

Fluoride01504


06/03/2011 14:0311154621701A1EPA 314.07b Perchlorate EPA 314.006019

1Ashley M Adams05/17/2011 11:2411137196401A1SW-846 71993b Cr VI by EPA 7199064671Luz M Groff05/17/2011 20:0011137020001A1SW-846 9040B18b pH by 9040B00200


Page 1 of 7


Sample Description: SL-002-SA5DN-SB-4.0-5.0 Soil SSFL Area IV Collocated Soil Sampling SL-002-SA5DN-SB-4.0-5.0 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 15:48

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0024 SDG#: DE151-05




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B6.7 U 0.8767-64-106192 6.7 8.0Acetone0.1 U 0.8771-43-206192 0.1 4.0Benzene0.13 U 0.87108-86-106192 0.13 4.0Bromobenzene0.33 U 0.8774-97-506192 0.33 4.0Bromochloromethane0.08 U 0.8775-27-406192 0.08 4.0Bromodichloromethane0.40 U 0.8775-25-206192 0.40 4.0Bromoform0.25 U 0.8774-83-906192 0.25 4.0Bromomethane1.2 U 0.8778-93-306192 1.2 8.02-Butanone0.12 U 0.87104-51-806192 0.12 4.0n-Butylbenzene0.06 U 0.87135-98-806192 0.06 4.0sec-Butylbenzene0.16 U 0.8798-06-606192 0.16 4.0tert-Butylbenzene0.14 U 0.8756-23-506192 0.14 4.0Carbon Tetrachloride0.11 U 0.87108-90-706192 0.11 4.0Chlorobenzene0.13 U 0.8775-00-306192 0.13 4.0Chloroethane0.30 U 0.87110-75-806192 0.30 4.02-Chloroethyl Vinyl Ether0.12 U 0.8767-66-306192 0.12 4.0Chloroform0.33 U 0.8774-87-306192 0.33 4.0Chloromethane0.14 U 0.8795-49-806192 0.14 4.02-Chlorotoluene0.14 U 0.87106-43-406192 0.14 4.04-Chlorotoluene0.50 U 0.8779-38-906192 0.50 5.0Chlorotrifluoroethene0.70 U 0.8796-12-806192 0.70 4.01,2-Dibromo-3-chloropropane0.20 U 0.87124-48-106192 0.20 4.0Dibromochloromethane0.17 U 0.87106-93-406192 0.17 4.01,2-Dibromoethane0.24 U 0.8774-95-306192 0.24 4.0Dibromomethane0.09 U 0.8795-50-106192 0.09 4.01,2-Dichlorobenzene0.12 U 0.87541-73-106192 0.12 4.01,3-Dichlorobenzene0.16 U 0.87106-46-706192 0.16 4.01,4-Dichlorobenzene0.12 U 0.8775-71-806192 0.12 4.0Dichlorodifluoromethane0.1 U 0.8775-34-306192 0.1 4.01,1-Dichloroethane0.15 U 0.87107-06-206192 0.15 4.01,2-Dichloroethane0.39 U 0.8775-35-406192 0.39 4.01,1-Dichloroethene0.19 U 0.87156-59-206192 0.19 4.0cis-1,2-Dichloroethene0.12 U 0.87156-60-506192 0.12 4.0trans-1,2-Dichloroethene0.17 U 0.8778-87-506192 0.17 4.01,2-Dichloropropane0.08 U 0.87142-28-906192 0.08 4.01,3-Dichloropropane0.17 U 0.87594-20-706192 0.17 4.02,2-Dichloropropane0.13 U 0.87563-58-606192 0.13 4.01,1-Dichloropropene0.16 U 0.8710061-01-506192 0.16 4.0cis-1,3-Dichloropropene0.17 U 0.8710061-02-606192 0.17 4.0trans-1,3-Dichloropropene0.06 U 0.87100-41-406192 0.06 4.0Ethylbenzene0.11 U 0.8776-13-106192 0.11 4.0Freon 1130.50 U 0.8775-88-706192 0.50 5.0Freon 133a0.14 U 0.8787-68-306192 0.14 4.0Hexachlorobutadiene1.6 U 0.87591-78-606192 1.6 8.02-Hexanone0.06 U 0.8798-82-806192 0.06 4.0Isopropylbenzene0.11 U 0.8799-87-606192 0.11 4.0p-Isopropyltoluene0.21 U 0.871634-04-406192 0.21 4.0Methyl Tertiary Butyl Ether0.39 U 0.87108-10-106192 0.39 8.04-Methyl-2-pentanone4.5 0.8775-09-206192 0.24 4.0Methylene Chloride0.07 U 0.87103-65-106192 0.07 4.0n-Propylbenzene


Page 2 of 7



Collected: 05/16/2011 15:48

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0024 SDG#: DE151-05




ActionLimit

DilutionFactor

CATNo.





Page 3 of 7



Collected: 05/16/2011 15:48

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0024 SDG#: DE151-05




ActionLimit

DilutionFactor

CATNo.









Page 4 of 7



Collected: 05/16/2011 15:48

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0024 SDG#: DE151-05




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.75 U 186-73-710138 0.75 1.9Fluorene0.75 U 1193-39-510138 0.75 1.9Indeno(1,2,3-cd)pyrene0.75 U 190-12-010138 0.75 1.91-Methylnaphthalene0.75 U 191-57-610138 0.75 1.92-Methylnaphthalene0.75 U 191-20-310138 0.75 1.9Naphthalene0.75 U 162-75-910138 0.75 1.9N-Nitrosodimethylamine8.9 J 1117-84-010138 6.8 20Di-n-octylphthalate0.75 U 185-01-810138 0.75 1.9Phenanthrene0.75 U 1129-00-010138 0.75 1.9Pyrene


mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B34,000 17429-90-501643 5.77 23.0Aluminum15.5 17440-42-807914 1.02 5.74Boron13,300 17440-70-201650 7.04 23.0Calcium33,800 57439-89-601654 27.0 115Iron28.4 17439-93-201656 0.25 2.3Lithium7,000 17439-95-401657 2.92 11.5Magnesium515 17439-96-506958 0.0896 0.574Manganese167 17723-14-010145 0.643 11.5Phosphorus3,130 17440-09-701662 20.7 57.4Potassium659 17440-23-501667 42.8 115Sodium61.6 17440-24-607968 0.0712 0.574Strontium3.05 J 17440-31-506969 1.15 11.5Tin1,100 17440-32-606970 0.436 1.15Titanium5.51 J 17440-67-710146 0.964 5.74Zirconium



8.95 27440-38-206125 0.0883 0.442Arsenic196 27440-39-306126 0.119 0.442Barium1.19 27440-41-706127 0.0177 0.110Beryllium0.216 27440-43-906128 0.0442 0.110Cadmium


Page 5 of 7



Collected: 05/16/2011 15:48

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0024 SDG#: DE151-05




ActionLimit

DilutionFactor

CATNo.

mg/kgmg/kgmg/kg mg/kgMetals SW-846 602039.9 27440-47-306131 0.132 0.442Chromium14.9 27440-48-406132 0.0221 0.110Cobalt18.6 27440-50-806133 0.0729 0.442Copper13.0 27439-92-106135 0.0115 0.221Lead0.423 27439-98-706138 0.0552 0.110Molybdenum32.7 27440-02-006139 0.110 0.442Nickel0.0763 J 27782-49-206141 0.0442 0.442Selenium0.0765 J 27440-22-406142 0.0132 0.110Silver0.402 27440-28-006145 0.0331 0.110Thallium75.4 27440-62-206148 0.0243 0.110Vanadium58.2 27440-66-606149 0.618 3.31Zinc




mg/kgmg/kgmg/kg mg/kgSW-846 71990.23 U 118540-29-905892 0.23 1.13a Cr VI by EPA 7199





7.92 1n.a.00394 0.0100 0.010018a pH by 9045C



General Sample CommentsState of California Lab Certification No. 2501The volatile analysis was performed on soil from SL-002-SA5DN-SB-4.5. All QC is compliant unless otherwise noted. Please refer to the QualityControl Summary for overall QC performance data and associated samples.


Page 6 of 7



Collected: 05/16/2011 15:48

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0024 SDG#: DE151-05




Analyst



06192


10326


Prep07320


07320


8270C04688

1Gregory JDrahovsky



Extract00819

1Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BCalcium016505Joanne M Gates05/18/2011 11:461113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 07:511113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:40111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Cobalt061322Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:40111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:40111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:40111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 08:12111371026001A1SW-846 6020Zinc06149


Page 7 of 7



Collected: 05/16/2011 15:48

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0024 SDG#: DE151-05




Analyst


1Damary Valentin05/18/2011 06:361113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified



07332






01352



10129






Page 1 of 5



Collected: 05/16/2011 15:52

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0029 SDG#: DE151-06




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C190 U 162-53-304688 190 570Aniline1,300 U 192-87-504688 1,300 3,800Benzidine190 U 165-85-004688 190 570Benzoic acid190 U 1100-51-604688 190 570Benzyl alcohol19 U 1101-55-304688 19 1904-Bromophenyl-phenylether19 U 186-74-804688 19 190Carbazole38 U 159-50-704688 38 1904-Chloro-3-methylphenol76 U 1106-47-804688 76 1904-Chloroaniline19 U 1111-91-104688 19 190bis(2-Chloroethoxy)methane19 U 1111-44-404688 19 190bis(2-Chloroethyl)ether19 U 139638-32-904688 19 190bis(2-Chloroisopropyl)ether19 U 191-58-704688 19 1902-Chloronaphthalene19 U 195-57-804688 19 1902-Chlorophenol38 U 17005-72-304688 38 1904-Chlorophenyl-phenylether19 U 1132-64-904688 19 190Dibenzofuran19 U 195-50-104688 19 1901,2-Dichlorobenzene19 U 1541-73-104688 19 1901,3-Dichlorobenzene19 U 1106-46-704688 19 1901,4-Dichlorobenzene110 U 191-94-104688 110 3803,3'-Dichlorobenzidine19 U 1120-83-204688 19 1902,4-Dichlorophenol38 U 1105-67-904688 38 1902,4-Dimethylphenol38 U 1108-68-904688 38 1903,5-Dimethylphenol190 U 1534-52-104688 190 5704,6-Dinitro-2-methylphenol380 U 151-28-504688 380 1,1002,4-Dinitrophenol38 U 1121-14-204688 38 1902,4-Dinitrotoluene19 U 1606-20-204688 19 1902,6-Dinitrotoluene19 U 1122-66-704688 19 1901,2-Diphenylhydrazine35 J 1117-81-704688 19 380bis(2-Ethylhexyl)phthalate19 U 1118-74-104688 19 190Hexachlorobenzene76 U 187-68-304688 76 190Hexachlorobutadiene190 U 177-47-404688 190 570Hexachlorocyclopentadiene19 U 167-72-104688 19 190Hexachloroethane19 U 178-59-104688 19 190Isophorone38 U 195-48-704688 38 1902-Methylphenol38 U 1106-44-504688 38 1904-Methylphenol




190 U 187-86-504688 190 570Pentachlorophenol


Page 2 of 5



Collected: 05/16/2011 15:52

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0029 SDG#: DE151-06




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C19 U 1108-95-204688 19 190Phenol19 U 1120-82-104688 19 1901,2,4-Trichlorobenzene38 U 195-95-404688 38 1902,4,5-Trichlorophenol38 U 188-06-204688 38 1902,4,6-Trichlorophenol


ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.76 U 183-32-910138 0.76 1.9Acenaphthene0.38 U 1208-96-810138 0.38 1.9Acenaphthylene0.38 U 1120-12-710138 0.38 1.9Anthracene0.76 U 156-55-310138 0.76 1.9Benzo(a)anthracene0.76 U 150-32-810138 0.76 1.9Benzo(a)pyrene0.76 U 1205-99-210138 0.76 1.9Benzo(b)fluoranthene0.76 U 1191-24-210138 0.76 1.9Benzo(g,h,i)perylene0.76 U 1207-08-910138 0.76 1.9Benzo(k)fluoranthene6.8 U 185-68-710138 6.8 21Butylbenzylphthalate6.8 U 184-74-210138 6.8 21Di-n-butylphthalate0.38 U 1218-01-910138 0.38 1.9Chrysene0.76 U 153-70-310138 0.76 1.9Dibenz(a,h)anthracene6.8 U 184-66-210138 6.8 21Diethylphthalate6.8 U 1131-11-310138 6.8 21Dimethylphthalate0.76 U 1206-44-010138 0.76 1.9Fluoranthene0.76 U 186-73-710138 0.76 1.9Fluorene0.76 U 1193-39-510138 0.76 1.9Indeno(1,2,3-cd)pyrene0.76 U 190-12-010138 0.76 1.91-Methylnaphthalene0.76 U 191-57-610138 0.76 1.92-Methylnaphthalene0.76 U 191-20-310138 0.76 1.9Naphthalene0.76 U 162-75-910138 0.76 1.9N-Nitrosodimethylamine6.8 U 1117-84-010138 6.8 21Di-n-octylphthalate0.76 U 185-01-810138 0.76 1.9Phenanthrene0.76 U 1129-00-010138 0.76 1.9Pyrene

ug/kgug/kgug/kg ug/kgPesticides/PCBs SW-846 80821.1 U 163496-31-110225 1.1 3.8Aroclor 54321.1 U 112642-23-810225 1.1 3.8Aroclor 54421.1 U 111126-42-410225 1.1 3.8Aroclor 54600.38 U 112674-11-210225 0.38 1.9PCB-10160.38 U 111104-28-210225 0.38 1.9PCB-12210.38 U 111141-16-510225 0.38 1.9PCB-12320.38 U 153469-21-910225 0.38 1.9PCB-12420.38 U 112672-29-610225 0.38 1.9PCB-12480.38 U 111097-69-110225 0.38 1.9PCB-12540.45 U 111096-82-510225 0.45 1.9PCB-12600.38 U 137324-23-510225 0.38 1.9PCB-1262


Page 3 of 5



Collected: 05/16/2011 15:52

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0029 SDG#: DE151-06




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgPesticides/PCBs SW-846 80820.38 U 111100-14-410225 0.38 1.9PCB-1268

mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B29,300 17429-90-501643 5.71 22.7Aluminum15.0 17440-42-807914 1.01 5.68Boron12,000 17440-70-201650 6.96 22.7Calcium35,000 57439-89-601654 26.7 114Iron28.3 17439-93-201656 0.25 2.3Lithium6,960 17439-95-401657 2.88 11.4Magnesium517 17439-96-506958 0.0886 0.568Manganese256 17723-14-010145 0.636 11.4Phosphorus3,300 17440-09-701662 20.4 56.8Potassium739 17440-23-501667 42.4 114Sodium55.0 17440-24-607968 0.0704 0.568Strontium3.20 J 17440-31-506969 1.14 11.4Tin1,390 17440-32-606970 0.431 1.14Titanium7.08 17440-67-710146 0.954 5.68Zirconium



10.4 27440-38-206125 0.0882 0.441Arsenic165 27440-39-306126 0.119 0.441Barium1.10 27440-41-706127 0.0176 0.110Beryllium0.243 27440-43-906128 0.0441 0.110Cadmium35.2 27440-47-306131 0.132 0.441Chromium10.5 27440-48-406132 0.0221 0.110Cobalt19.8 27440-50-806133 0.0728 0.441Copper10.5 27439-92-106135 0.0115 0.221Lead0.651 27439-98-706138 0.0551 0.110Molybdenum25.6 27440-02-006139 0.110 0.441Nickel0.0860 J 27782-49-206141 0.0441 0.441Selenium0.0385 J 27440-22-406142 0.0132 0.110Silver0.425 27440-28-006145 0.0331 0.110Thallium70.7 27440-62-206148 0.0243 0.110Vanadium66.5 27440-66-606149 0.618 3.31Zinc





Page 4 of 5



Collected: 05/16/2011 15:52

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0029 SDG#: DE151-06




ActionLimit

DilutionFactor

CATNo.

mg/kgmg/kgmg/kg mg/kgWet Chemistry SW-846 71990.23 U 118540-29-905892 0.23 1.13a Cr VI by EPA 7199





8.31 1n.a.00394 0.0100 0.010018a pH by 9045C







Analyst



04688

1Gregory JDrahovsky



Extract00819

1Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BCalcium016505Joanne M Gates05/18/2011 11:491113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BSodium01667


Page 5 of 5



Collected: 05/16/2011 15:52

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0029 SDG#: DE151-06




Analyst


1Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 07:541113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:43111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Cobalt061322Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:43111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:43111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:43111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 08:14111371026001A1SW-846 6020Zinc061491Damary Valentin05/18/2011 06:371113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified



07332






01352



10129






Page 1 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B22 0.8767-64-106192 7.0 8.4Acetone0.21 J 0.8771-43-206192 0.10 4.2Benzene0.14 U 0.87108-86-106192 0.14 4.2Bromobenzene0.35 U 0.8774-97-506192 0.35 4.2Bromochloromethane0.08 U 0.8775-27-406192 0.08 4.2Bromodichloromethane0.42 U 0.8775-25-206192 0.42 4.2Bromoform0.26 U 0.8774-83-906192 0.26 4.2Bromomethane3.9 J 0.8778-93-306192 1.3 8.42-Butanone0.13 U 0.87104-51-806192 0.13 4.2n-Butylbenzene0.06 U 0.87135-98-806192 0.06 4.2sec-Butylbenzene0.17 U 0.8798-06-606192 0.17 4.2tert-Butylbenzene0.15 U 0.8756-23-506192 0.15 4.2Carbon Tetrachloride0.12 U 0.87108-90-706192 0.12 4.2Chlorobenzene0.14 U 0.8775-00-306192 0.14 4.2Chloroethane0.31 U 0.87110-75-806192 0.31 4.22-Chloroethyl Vinyl Ether0.13 U 0.8767-66-306192 0.13 4.2Chloroform0.35 U 0.8774-87-306192 0.35 4.2Chloromethane0.15 U 0.8795-49-806192 0.15 4.22-Chlorotoluene0.15 U 0.87106-43-406192 0.15 4.24-Chlorotoluene0.52 U 0.8779-38-906192 0.52 5.2Chlorotrifluoroethene0.73 U 0.8796-12-806192 0.73 4.21,2-Dibromo-3-chloropropane0.21 U 0.87124-48-106192 0.21 4.2Dibromochloromethane0.18 U 0.87106-93-406192 0.18 4.21,2-Dibromoethane0.25 U 0.8774-95-306192 0.25 4.2Dibromomethane0.09 U 0.8795-50-106192 0.09 4.21,2-Dichlorobenzene0.13 U 0.87541-73-106192 0.13 4.21,3-Dichlorobenzene0.17 U 0.87106-46-706192 0.17 4.21,4-Dichlorobenzene0.13 U 0.8775-71-806192 0.13 4.2Dichlorodifluoromethane0.10 U 0.8775-34-306192 0.10 4.21,1-Dichloroethane0.16 U 0.87107-06-206192 0.16 4.21,2-Dichloroethane0.41 U 0.8775-35-406192 0.41 4.21,1-Dichloroethene0.20 U 0.87156-59-206192 0.20 4.2cis-1,2-Dichloroethene0.13 U 0.87156-60-506192 0.13 4.2trans-1,2-Dichloroethene0.18 U 0.8778-87-506192 0.18 4.21,2-Dichloropropane0.08 U 0.87142-28-906192 0.08 4.21,3-Dichloropropane0.18 U 0.87594-20-706192 0.18 4.22,2-Dichloropropane0.14 U 0.87563-58-606192 0.14 4.21,1-Dichloropropene0.17 U 0.8710061-01-506192 0.17 4.2cis-1,3-Dichloropropene0.18 U 0.8710061-02-606192 0.18 4.2trans-1,3-Dichloropropene0.06 U 0.87100-41-406192 0.06 4.2Ethylbenzene0.12 U 0.8776-13-106192 0.12 4.2Freon 1130.52 U 0.8775-88-706192 0.52 5.2Freon 133a0.15 U 0.8787-68-306192 0.15 4.2Hexachlorobutadiene1.7 U 0.87591-78-606192 1.7 8.42-Hexanone0.06 U 0.8798-82-806192 0.06 4.2Isopropylbenzene0.12 U 0.8799-87-606192 0.12 4.2p-Isopropyltoluene0.22 U 0.871634-04-406192 0.22 4.2Methyl Tertiary Butyl Ether0.41 U 0.87108-10-106192 0.41 8.44-Methyl-2-pentanone5.1 0.8775-09-206192 0.25 4.2Methylene Chloride0.07 U 0.87103-65-106192 0.07 4.2n-Propylbenzene


Page 2 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




ActionLimit

DilutionFactor

CATNo.



ng/kgng/kgng/kg ng/kgGC/MS Semivolatiles EPA 1625C199 U 1062-75-911622 199 399N-Nitrosodimethylamine

The internal standard peak areas were outside of the QC limits for both theinitial injection and the re-injection. The values here are from the initialinjection of the sample. Reporting limits were raised due to interference from the sample matrix.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C200 U 162-53-304688 200 590Aniline1,400 U 192-87-504688 1,400 3,900Benzidine200 U 165-85-004688 200 590Benzoic acid200 U 1100-51-604688 200 590Benzyl alcohol20 U 1101-55-304688 20 2004-Bromophenyl-phenylether20 U 186-74-804688 20 200Carbazole39 U 159-50-704688 39 2004-Chloro-3-methylphenol79 U 1106-47-804688 79 2004-Chloroaniline20 U 1111-91-104688 20 200bis(2-Chloroethoxy)methane20 U 1111-44-404688 20 200bis(2-Chloroethyl)ether20 U 139638-32-904688 20 200bis(2-Chloroisopropyl)ether20 U 191-58-704688 20 2002-Chloronaphthalene20 U 195-57-804688 20 2002-Chlorophenol39 U 17005-72-304688 39 2004-Chlorophenyl-phenylether20 U 1132-64-904688 20 200Dibenzofuran20 U 195-50-104688 20 2001,2-Dichlorobenzene20 U 1541-73-104688 20 2001,3-Dichlorobenzene20 U 1106-46-704688 20 2001,4-Dichlorobenzene120 U 191-94-104688 120 3903,3'-Dichlorobenzidine


Page 3 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C20 U 1120-83-204688 20 2002,4-Dichlorophenol39 U 1105-67-904688 39 2002,4-Dimethylphenol39 U 1108-68-904688 39 2003,5-Dimethylphenol200 U 1534-52-104688 200 5904,6-Dinitro-2-methylphenol390 U 151-28-504688 390 1,2002,4-Dinitrophenol39 U 1121-14-204688 39 2002,4-Dinitrotoluene20 U 1606-20-204688 20 2002,6-Dinitrotoluene20 U 1122-66-704688 20 2001,2-Diphenylhydrazine20 U 1118-74-104688 20 200Hexachlorobenzene79 U 187-68-304688 79 200Hexachlorobutadiene200 U 177-47-404688 200 590Hexachlorocyclopentadiene20 U 167-72-104688 20 200Hexachloroethane20 U 178-59-104688 20 200Isophorone39 U 195-48-704688 39 2002-Methylphenol39 U 1106-44-504688 39 2004-Methylphenol






ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.79 U 183-32-910138 0.79 2.0Acenaphthene0.39 U 1208-96-810138 0.39 2.0Acenaphthylene0.39 U 1120-12-710138 0.39 2.0Anthracene0.79 U 156-55-310138 0.79 2.0Benzo(a)anthracene0.79 U 150-32-810138 0.79 2.0Benzo(a)pyrene0.79 U 1205-99-210138 0.79 2.0Benzo(b)fluoranthene0.79 U 1191-24-210138 0.79 2.0Benzo(g,h,i)perylene0.79 U 1207-08-910138 0.79 2.0Benzo(k)fluoranthene


Page 4 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM7.1 U 185-68-710138 7.1 21Butylbenzylphthalate7.1 U 184-74-210138 7.1 21Di-n-butylphthalate0.39 U 1218-01-910138 0.39 2.0Chrysene0.79 U 153-70-310138 0.79 2.0Dibenz(a,h)anthracene7.1 U 184-66-210138 7.1 21Diethylphthalate7.1 U 1131-11-310138 7.1 21Dimethylphthalate7.1 U 1117-81-710138 7.1 21Bis(2-Ethylhexyl)phthalate0.79 U 1206-44-010138 0.79 2.0Fluoranthene0.79 U 186-73-710138 0.79 2.0Fluorene0.79 U 1193-39-510138 0.79 2.0Indeno(1,2,3-cd)pyrene0.79 U 190-12-010138 0.79 2.01-Methylnaphthalene0.79 U 191-57-610138 0.79 2.02-Methylnaphthalene0.79 U 191-20-310138 0.79 2.0Naphthalene0.79 U 162-75-910138 0.79 2.0N-Nitrosodimethylamine7.1 U 1117-84-010138 7.1 21Di-n-octylphthalate0.79 U 185-01-810138 0.79 2.0Phenanthrene0.79 U 1129-00-010138 0.79 2.0Pyrene





48 U 135572-78-210132 48 140 10000000


96 U 159229-75-310132 96 290 10000000


96 U 16629-29-410132 96 290 10000000


48 U 199-65-010132 48 140 10000000

1,3-Dinitrobenzene

48 U 1121-14-210132 48 140 10000000

2,4-Dinitrotoluene

48 U 1606-20-210132 48 140 10000000

2,6-Dinitrotoluene

120 U 12691-41-010132 120 360 10000000

HMX

48 U 198-95-310132 48 140 10000000

Nitrobenzene

960 U 155-63-010132 960 2,900 10000000

Nitroglycerin

96 U 188-72-210132 96 140 10000000

2-Nitrotoluene

120 U 199-08-110132 120 140 10000000

3-Nitrotoluene

96 U 199-99-010132 96 140 10000000

4-Nitrotoluene


Page 5 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgExplosives SW-846 8330A960 U 178-11-510132 960 2,900 1000000

0PETN

60 U 1121-82-410132 60 140 10000000

RDX

73 U 1479-45-810132 73 140 10000000

Tetryl

48 U 199-35-410132 48 140 10000000


48 U 1118-96-710132 48 140 10000000


ug/kgug/kgug/kg ug/kgHPLC Organics SW-846 8315A6,600 150-00-004173 710 1,80025a Formaldehyde 8315A

ug/kgug/kgug/kg ug/kgPerchlorate SW-846 6850 1/20072.5 U 114797-73-006557 2.5 6.06a Perchlorate EPA 6850



0.96 U 2n.a.10199 0.96 2.9EFH (C12-C14)1.8 J 2n.a.10199 0.96 2.9EFH (C15-C20)11 2n.a.10199 0.96 2.9EFH (C21-C30)68 2n.a.10199 0.96 2.9EFH (C30 - C40)0.96 U 2n.a.10199 0.96 2.9EFH (C8-C11)

ug/kgug/kgug/kg ug/kgGC Miscellaneous SW-846 8015B120 U 164-17-510501 120 600Ethanol120 U 167-63-010501 120 600Isopropanol230 J 167-56-110501 120 600Methanol


6.0 U 1111-46-608283 6.0 12Diethylene glycol


Page 6 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




ActionLimit

DilutionFactor

CATNo.


6.0 U 1107-21-108283 6.0 12Ethylene glycol6.0 U 157-55-608283 6.0 12Propylene glycol








Page 7 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




ActionLimit

DilutionFactor

CATNo.









7.70 1n.a.00394 0.0100 0.010018a pH by 9045C







Analyst



06192


10326

n.a.Lois E Hiltz05/17/2011 19:372011137244351SW-846 5035GC/MS - HL Encore Prep08390


Page 8 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




Analyst



07320


07320

n.a.Lois E Hiltz05/17/2011 19:352011137244351SW-846 5035GC/MS-HL Encore Prep-NC0757810Matthew S Woods06/10/2011 16:0311146SLE0261EPA 1625C15a NDMA by 1625C116221Brian K Graham05/24/2011 08:1311139SLH0261SW-846 8270C5a Semivolatiles by EPA

8270C04688

1Gregory JDrahovsky




05551

n.a.Lois E Hiltz05/17/2011 19:342011137244351SW-846 5035GC - 5 g HL Encore Prep061301Michele D Hamilton06/01/2011 07:16111430006A1SW-846 8330A16a Energetics by 8330A10132

1Michele D Hamilton05/23/2011 19:16111400002A1SW-846 8315A25a Formaldehyde 8315A04173

1Richard A Shober05/19/2011 18:34111390003A1SW-846 6850 1/20076a Perchlorate EPA 685006557


Extract00819

1Maria Davenport05/19/2011 09:15111390003A1SW-846 6850 1/2007Perchlorate Soil Prep06568


05876

1Wanda F Oswald05/23/2011 15:30111430006A1SW-846 8330Energetics Extraction111372Tracy A Cole05/25/2011 09:55111380034A1SW-846 8015B


10199




1Heather E Williams06/01/2011 06:48111460029A1SW-846 8015B20a Terphenyls by 8015B10318

1Kerrie A Freeburn05/19/2011 09:00111380034A1SW-846 3550BEFH Extraction - Soils112381Joseph S Feister05/27/2011 07:30111460029A2SW-846 3550BTerphenyls soil prep103031Tyler O Griffin05/19/2011 16:45111390030A1SW-846 8015BSolids Extraction for

Alcohols00380


05/20/2011 12:00111370018A1SW-846 8015Bmodified


1Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BCalcium016505Joanne M Gates05/18/2011 11:531113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BManganese06958


Page 9 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




Analyst


1Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 07:581113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:46111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Cobalt061322Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:46111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:46111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:46111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 08:15111371026001A1SW-846 6020Zinc061491Damary Valentin05/18/2011 06:381113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified



07332


07336








01352



10129

1Nancy J Shoop05/24/2011 09:1011144102201A1SW-846 9012BCyanide Solid Distillation058961Michele L Graham05/19/2011 14:4511139182102B1ASTM D149832a OR Potential018211Michele L Graham05/19/2011 14:4511139039402B1SW-846 9045C




Page 10 of 10



Collected: 05/16/2011 10:43

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0030 SDG#: DE151-07




Analyst


1Scott W Freisher06/07/2011 21:2411158162401B1EPA 160.3 modifiedMoisture Content by 160.311624


Page 1 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




ActionLimit

DilutionFactor

CATNo.



Page 2 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




ActionLimit

DilutionFactor

CATNo.






Page 3 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C37 U 1121-14-204688 37 1802,4-Dinitrotoluene18 U 1606-20-204688 18 1802,6-Dinitrotoluene18 U 1122-66-704688 18 1801,2-Diphenylhydrazine18 U 1118-74-104688 18 180Hexachlorobenzene74 U 187-68-304688 74 180Hexachlorobutadiene180 U 177-47-404688 180 550Hexachlorocyclopentadiene18 U 167-72-104688 18 180Hexachloroethane18 U 178-59-104688 18 180Isophorone37 U 195-48-704688 37 1802-Methylphenol37 U 1106-44-504688 37 1804-Methylphenol






ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.74 U 183-32-910138 0.74 1.8Acenaphthene0.37 U 1208-96-810138 0.37 1.8Acenaphthylene0.37 U 1120-12-710138 0.37 1.8Anthracene0.74 U 156-55-310138 0.74 1.8Benzo(a)anthracene0.74 U 150-32-810138 0.74 1.8Benzo(a)pyrene0.74 U 1205-99-210138 0.74 1.8Benzo(b)fluoranthene0.74 U 1191-24-210138 0.74 1.8Benzo(g,h,i)perylene0.74 U 1207-08-910138 0.74 1.8Benzo(k)fluoranthene6.7 U 185-68-710138 6.7 20Butylbenzylphthalate6.7 U 184-74-210138 6.7 20Di-n-butylphthalate0.37 U 1218-01-910138 0.37 1.8Chrysene0.74 U 153-70-310138 0.74 1.8Dibenz(a,h)anthracene6.7 U 184-66-210138 6.7 20Diethylphthalate


Page 4 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM6.7 U 1131-11-310138 6.7 20Dimethylphthalate6.7 U 1117-81-710138 6.7 20Bis(2-Ethylhexyl)phthalate0.74 U 1206-44-010138 0.74 1.8Fluoranthene0.74 U 186-73-710138 0.74 1.8Fluorene0.74 U 1193-39-510138 0.74 1.8Indeno(1,2,3-cd)pyrene0.74 U 190-12-010138 0.74 1.81-Methylnaphthalene0.74 U 191-57-610138 0.74 1.82-Methylnaphthalene0.74 U 191-20-310138 0.74 1.8Naphthalene0.74 U 162-75-910138 0.74 1.8N-Nitrosodimethylamine6.7 U 1117-84-010138 6.7 20Di-n-octylphthalate0.74 U 185-01-810138 0.74 1.8Phenanthrene0.74 U 1129-00-010138 0.74 1.8Pyrene





43 U 135572-78-210132 43 130 10000000


86 U 159229-75-310132 86 260 10000000


86 U 16629-29-410132 86 260 10000000


43 U 199-65-010132 43 130 10000000

1,3-Dinitrobenzene

43 U 1121-14-210132 43 130 10000000

2,4-Dinitrotoluene

43 U 1606-20-210132 43 130 10000000

2,6-Dinitrotoluene

110 U 12691-41-010132 110 320 10000000

HMX

43 U 198-95-310132 43 130 10000000

Nitrobenzene

860 U 155-63-010132 860 2,600 10000000

Nitroglycerin

86 U 188-72-210132 86 130 10000000

2-Nitrotoluene

110 U 199-08-110132 110 130 10000000

3-Nitrotoluene

86 U 199-99-010132 86 130 10000000

4-Nitrotoluene

860 U 178-11-510132 860 2,600 10000000

PETN

54 U 1121-82-410132 54 130 10000000

RDX


Page 5 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




ActionLimit

DilutionFactor

CATNo.


0Tetryl

43 U 199-35-410132 43 130 10000000


43 U 1118-96-710132 43 130 10000000



ug/kgug/kgug/kg ug/kgHPLC Organics SW-846 8315A660 U 150-00-004173 660 1,60025a Formaldehyde 8315A

ug/kgug/kgug/kg ug/kgPesticides/PCBs SW-846 80821.1 U 163496-31-110225 1.1 3.7Aroclor 54321.1 U 112642-23-810225 1.1 3.7Aroclor 54421.1 U 111126-42-410225 1.1 3.7Aroclor 54600.37 U 112674-11-210225 0.37 1.9PCB-10160.37 U 111104-28-210225 0.37 1.9PCB-12210.37 U 111141-16-510225 0.37 1.9PCB-12320.86 J 153469-21-910225 0.37 1.9PCB-12420.37 U 112672-29-610225 0.37 1.9PCB-12480.37 U 111097-69-110225 0.37 1.9PCB-12540.43 U 111096-82-510225 0.43 1.9PCB-12600.37 U 137324-23-510225 0.37 1.9PCB-12620.37 U 111100-14-410225 0.37 1.9PCB-1268


0.89 U 2n.a.10199 0.89 2.7EFH (C12-C14)1.0 J 2n.a.10199 0.89 2.7EFH (C15-C20)9.0 2n.a.10199 0.89 2.7EFH (C21-C30)47 2n.a.10199 0.89 2.7EFH (C30 - C40)0.89 U 2n.a.10199 0.89 2.7EFH (C8-C11)





Page 6 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




ActionLimit

DilutionFactor

CATNo.


mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B22,300 17429-90-501643 5.46 21.7Aluminum10.9 17440-42-807914 0.965 5.42Boron34,500 17440-70-201650 6.65 21.7Calcium34,400 57439-89-601654 25.5 108Iron28.6 17439-93-201656 0.24 2.2Lithium6,350 17439-95-401657 2.76 10.8Magnesium237 17439-96-506958 0.0846 0.542Manganese523 17723-14-010145 0.607 10.8Phosphorus2,650 17440-09-701662 19.5 54.2Potassium676 17440-23-501667 40.5 108Sodium52.6 17440-24-607968 0.0673 0.542Strontium3.25 J 17440-31-506969 1.08 10.8Tin1,400 17440-32-606970 0.412 1.08Titanium5.09 J 17440-67-710146 0.911 5.42Zirconium




mg/kgmg/kgmg/kg mg/kgSW-846 7471A0.0306 J 17439-97-600159 0.0030 0.104Mercury

mg/kgmg/kgmg/kg mg/kgWet Chemistry EPA 300.05.8 116984-48-807332 0.89 1.111a Anions by 300.0 - Fluoride7.8 114797-55-807336 0.89 1.711a Anions by 300.0 - Nitrate


Page 7 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




ActionLimit

DilutionFactor

CATNo.








8.36 1n.a.00394 0.0100 0.010018a pH by 9045C







Analyst



06192


10326


Prep07320


07320



Page 8 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




Analyst



04688

1Gregory JDrahovsky




05551



Extract00819


05876



10199





Alcohols00380


05/20/2011 12:00111370018A1SW-846 8015Bmodified


1Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BCalcium016505Joanne M Gates05/18/2011 11:561113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 08:021113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:49111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:49111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:49111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:49111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:49111371026001A1SW-846 6020Cadmium06128


Page 9 of 9



Collected: 05/16/2011 10:50

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0038 SDG#: DE151-08




Analyst







05/18/2011 01:001113757110021SW-846 7471Amodified



07332


07336








01352



10129






Page 1 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B15 0.8467-64-106192 6.7 8.0Acetone0.17 J 0.8471-43-206192 0.10 4.0Benzene0.13 U 0.84108-86-106192 0.13 4.0Bromobenzene0.33 U 0.8474-97-506192 0.33 4.0Bromochloromethane0.08 U 0.8475-27-406192 0.08 4.0Bromodichloromethane0.40 U 0.8475-25-206192 0.40 4.0Bromoform0.25 U 0.8474-83-906192 0.25 4.0Bromomethane3.2 J 0.8478-93-306192 1.2 8.02-Butanone0.12 U 0.84104-51-806192 0.12 4.0n-Butylbenzene0.06 U 0.84135-98-806192 0.06 4.0sec-Butylbenzene0.16 U 0.8498-06-606192 0.16 4.0tert-Butylbenzene0.14 U 0.8456-23-506192 0.14 4.0Carbon Tetrachloride0.11 U 0.84108-90-706192 0.11 4.0Chlorobenzene0.13 U 0.8475-00-306192 0.13 4.0Chloroethane0.30 U 0.84110-75-806192 0.30 4.02-Chloroethyl Vinyl Ether0.12 U 0.8467-66-306192 0.12 4.0Chloroform0.33 U 0.8474-87-306192 0.33 4.0Chloromethane0.14 U 0.8495-49-806192 0.14 4.02-Chlorotoluene0.14 U 0.84106-43-406192 0.14 4.04-Chlorotoluene0.50 U 0.8479-38-906192 0.50 5.0Chlorotrifluoroethene0.70 U 0.8496-12-806192 0.70 4.01,2-Dibromo-3-chloropropane0.20 U 0.84124-48-106192 0.20 4.0Dibromochloromethane0.17 U 0.84106-93-406192 0.17 4.01,2-Dibromoethane0.24 U 0.8474-95-306192 0.24 4.0Dibromomethane0.09 U 0.8495-50-106192 0.09 4.01,2-Dichlorobenzene0.12 U 0.84541-73-106192 0.12 4.01,3-Dichlorobenzene0.16 U 0.84106-46-706192 0.16 4.01,4-Dichlorobenzene0.12 U 0.8475-71-806192 0.12 4.0Dichlorodifluoromethane0.10 U 0.8475-34-306192 0.10 4.01,1-Dichloroethane0.15 U 0.84107-06-206192 0.15 4.01,2-Dichloroethane0.39 U 0.8475-35-406192 0.39 4.01,1-Dichloroethene0.19 U 0.84156-59-206192 0.19 4.0cis-1,2-Dichloroethene0.12 U 0.84156-60-506192 0.12 4.0trans-1,2-Dichloroethene0.17 U 0.8478-87-506192 0.17 4.01,2-Dichloropropane0.08 U 0.84142-28-906192 0.08 4.01,3-Dichloropropane0.17 U 0.84594-20-706192 0.17 4.02,2-Dichloropropane0.13 U 0.84563-58-606192 0.13 4.01,1-Dichloropropene0.16 U 0.8410061-01-506192 0.16 4.0cis-1,3-Dichloropropene0.17 U 0.8410061-02-606192 0.17 4.0trans-1,3-Dichloropropene0.06 U 0.84100-41-406192 0.06 4.0Ethylbenzene0.11 U 0.8476-13-106192 0.11 4.0Freon 1130.50 U 0.8475-88-706192 0.50 5.0Freon 133a0.14 U 0.8487-68-306192 0.14 4.0Hexachlorobutadiene1.6 U 0.84591-78-606192 1.6 8.02-Hexanone0.06 U 0.8498-82-806192 0.06 4.0Isopropylbenzene0.11 U 0.8499-87-606192 0.11 4.0p-Isopropyltoluene0.21 U 0.841634-04-406192 0.21 4.0Methyl Tertiary Butyl Ether0.39 U 0.84108-10-106192 0.39 8.04-Methyl-2-pentanone0.88 J 0.8475-09-206192 0.24 4.0Methylene Chloride0.07 U 0.84103-65-106192 0.07 4.0n-Propylbenzene


Page 2 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




ActionLimit

DilutionFactor

CATNo.



ng/kgng/kgng/kg ng/kgGC/MS Semivolatiles EPA 1625C287 J 1062-75-911622 200 399N-Nitrosodimethylamine



Page 3 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




ActionLimit

DilutionFactor

CATNo.







ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.80 U 183-32-910138 0.80 2.0Acenaphthene0.40 U 1208-96-810138 0.40 2.0Acenaphthylene0.40 U 1120-12-710138 0.40 2.0Anthracene0.80 U 156-55-310138 0.80 2.0Benzo(a)anthracene0.80 U 150-32-810138 0.80 2.0Benzo(a)pyrene0.80 U 1205-99-210138 0.80 2.0Benzo(b)fluoranthene0.80 U 1191-24-210138 0.80 2.0Benzo(g,h,i)perylene0.80 U 1207-08-910138 0.80 2.0Benzo(k)fluoranthene7.2 U 185-68-710138 7.2 22Butylbenzylphthalate7.2 U 184-74-210138 7.2 22Di-n-butylphthalate0.40 U 1218-01-910138 0.40 2.0Chrysene0.80 U 153-70-310138 0.80 2.0Dibenz(a,h)anthracene7.2 U 184-66-210138 7.2 22Diethylphthalate


Page 4 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM7.2 U 1131-11-310138 7.2 22Dimethylphthalate7.2 U 1117-81-710138 7.2 22Bis(2-Ethylhexyl)phthalate0.86 J 1206-44-010138 0.80 2.0Fluoranthene0.80 U 186-73-710138 0.80 2.0Fluorene0.80 U 1193-39-510138 0.80 2.0Indeno(1,2,3-cd)pyrene0.80 U 190-12-010138 0.80 2.01-Methylnaphthalene0.80 U 191-57-610138 0.80 2.02-Methylnaphthalene0.96 J 191-20-310138 0.80 2.0Naphthalene0.80 U 162-75-910138 0.80 2.0N-Nitrosodimethylamine7.2 U 1117-84-010138 7.2 22Di-n-octylphthalate1.0 J 185-01-810138 0.80 2.0Phenanthrene0.80 U 1129-00-010138 0.80 2.0Pyrene





46 U 135572-78-210132 46 140 10000000


92 U 159229-75-310132 92 280 10000000


92 U 16629-29-410132 92 280 10000000


46 U 199-65-010132 46 140 10000000

1,3-Dinitrobenzene

46 U 1121-14-210132 46 140 10000000

2,4-Dinitrotoluene

46 U 1606-20-210132 46 140 10000000

2,6-Dinitrotoluene

120 U 12691-41-010132 120 350 10000000

HMX

46 U 198-95-310132 46 140 10000000

Nitrobenzene

920 U 155-63-010132 920 2,800 10000000

Nitroglycerin

92 U 188-72-210132 92 140 10000000

2-Nitrotoluene

120 U 199-08-110132 120 140 10000000

3-Nitrotoluene

92 U 199-99-010132 92 140 10000000

4-Nitrotoluene

920 U 178-11-510132 920 2,800 10000000

PETN

58 U 1121-82-410132 58 140 10000000

RDX


Page 5 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




ActionLimit

DilutionFactor

CATNo.


0Tetryl

46 U 199-35-410132 46 140 10000000


46 U 1118-96-710132 46 140 10000000






0.48 U 1n.a.10199 0.48 1.4EFH (C12-C14)0.48 U 1n.a.10199 0.48 1.4EFH (C15-C20)0.48 U 1n.a.10199 0.48 1.4EFH (C21-C30)0.93 J 1n.a.10199 0.48 1.4EFH (C30 - C40)0.48 U 1n.a.10199 0.48 1.4EFH (C8-C11)

ug/kgug/kgug/kg ug/kgGC Miscellaneous SW-846 8015B120 U 164-17-510501 120 600Ethanol120 U 167-63-010501 120 600Isopropanol630 167-56-110501 120 600Methanol




Page 6 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




ActionLimit

DilutionFactor

CATNo.









Page 7 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




ActionLimit

DilutionFactor

CATNo.








6.96 1n.a.00394 0.0100 0.010018a pH by 9045C







Analyst



06192


10326


Prep07320


07320



Page 8 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




Analyst



04688

1Gregory JDrahovsky

05/24/2011 23:2911143SLE0261SW-846 8270C SIM4a Select SVOC EPA 8270SIM10138

1Olivia I Santiago05/27/2011 14:3011146SLE0262SW-846 3546NDMA Soil Microwave116301Katheryne V

Sponheimer05/24/2011 08:0011143SLE0262SW-846 3550BBNA Soil Extraction SIM10479

1Sherry L Morrow05/20/2011 03:3011139SLH0261SW-846 3550BBNA Soil Sonication0038124.18Elizabeth J Marin05/23/2011 17:2911139A34A1TPH GRO SW-846


05551



Extract00819


05876



10199





Alcohols00380


05/20/2011 12:00111370018A1SW-846 8015Bmodified


1Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BBoron079141Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BCalcium016505Joanne M Gates05/18/2011 12:001113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 08:061113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:52111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Beryllium06127


Page 9 of 9



Collected: 05/16/2011 12:39

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0043 SDG#: DE151-09




Analyst


2Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Cadmium061282Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Chromium061312Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Cobalt061322Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Copper061332Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Lead061352Choon Y Tian05/18/2011 09:52111371026001C1SW-846 6020Molybdenum061382Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Nickel061392Choon Y Tian05/18/2011 09:52111371026001B1SW-846 6020Selenium061412Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Silver061422Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Thallium061452Choon Y Tian05/18/2011 09:52111371026001A1SW-846 6020Vanadium061482Choon Y Tian05/19/2011 08:19111371026001A1SW-846 6020Zinc061491Damary Valentin05/18/2011 06:431113757110021SW-846 7471AMercury001591Annamaria





05/18/2011 01:001113757110021SW-846 7471Amodified



07332


07336








01352



10129






Page 1 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




ActionLimit

DilutionFactor

CATNo.



Page 2 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Volatiles SW-846 8260B0.1 U 0.87100-42-506192 0.1 3.9Styrene0.11 U 0.87630-20-606192 0.11 3.91,1,1,2-Tetrachloroethane0.23 U 0.8779-34-506192 0.23 3.91,1,2,2-Tetrachloroethane0.20 U 0.87127-18-406192 0.20 3.9Tetrachloroethene0.08 U 0.87108-88-306192 0.08 3.9Toluene0.14 U 0.8787-61-606192 0.14 3.91,2,3-Trichlorobenzene0.18 U 0.87120-82-106192 0.18 3.91,2,4-Trichlorobenzene0.20 U 0.8771-55-606192 0.20 3.91,1,1-Trichloroethane0.27 U 0.8779-00-506192 0.27 3.91,1,2-Trichloroethane0.15 U 0.8779-01-606192 0.15 3.9Trichloroethene0.29 U 0.8775-69-406192 0.29 3.9Trichlorofluoromethane0.33 U 0.8796-18-406192 0.33 3.91,2,3-Trichloropropane0.39 U 0.8795-63-606192 0.39 3.91,2,4-Trimethylbenzene0.1 U 0.87108-67-806192 0.1 3.91,3,5-Trimethylbenzene0.20 U 0.8775-01-406192 0.20 3.9Vinyl Chloride0.17 U 0.87179601-23-106192 0.17 3.9m+p-Xylene0.17 U 0.8795-47-606192 0.17 3.9o-Xylene





Page 3 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




ActionLimit

DilutionFactor

CATNo.







ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM0.75 U 183-32-910138 0.75 1.9Acenaphthene0.37 U 1208-96-810138 0.37 1.9Acenaphthylene0.37 U 1120-12-710138 0.37 1.9Anthracene0.75 U 156-55-310138 0.75 1.9Benzo(a)anthracene0.75 U 150-32-810138 0.75 1.9Benzo(a)pyrene0.75 U 1205-99-210138 0.75 1.9Benzo(b)fluoranthene0.75 U 1191-24-210138 0.75 1.9Benzo(g,h,i)perylene0.75 U 1207-08-910138 0.75 1.9Benzo(k)fluoranthene6.7 U 185-68-710138 6.7 20Butylbenzylphthalate6.7 U 184-74-210138 6.7 20Di-n-butylphthalate0.61 J 1218-01-910138 0.37 1.9Chrysene0.75 U 153-70-310138 0.75 1.9Dibenz(a,h)anthracene6.7 U 184-66-210138 6.7 20Diethylphthalate


Page 4 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




ActionLimit

DilutionFactor

CATNo.

ug/kgug/kgug/kg ug/kgGC/MS Semivolatiles SW-846 8270C SIM6.7 U 1131-11-310138 6.7 20Dimethylphthalate6.7 U 1117-81-710138 6.7 20Bis(2-Ethylhexyl)phthalate0.75 U 1206-44-010138 0.75 1.9Fluoranthene0.75 U 186-73-710138 0.75 1.9Fluorene0.75 U 1193-39-510138 0.75 1.9Indeno(1,2,3-cd)pyrene0.75 U 190-12-010138 0.75 1.91-Methylnaphthalene0.81 J 191-57-610138 0.75 1.92-Methylnaphthalene0.75 U 191-20-310138 0.75 1.9Naphthalene0.75 U 162-75-910138 0.75 1.9N-Nitrosodimethylamine6.7 U 1117-84-010138 6.7 20Di-n-octylphthalate0.75 U 185-01-810138 0.75 1.9Phenanthrene0.75 U 1129-00-010138 0.75 1.9Pyrene


0.2 U 21.74n.a.05551 0.2 19a TPH by EPA 8015B Gas C5-C12



44 U 135572-78-210132 44 130 10000000


89 U 159229-75-310132 89 270 10000000


89 U 16629-29-410132 89 270 10000000


44 U 199-65-010132 44 130 10000000

1,3-Dinitrobenzene

44 U 1121-14-210132 44 130 10000000

2,4-Dinitrotoluene

44 U 1606-20-210132 44 130 10000000

2,6-Dinitrotoluene

110 U 12691-41-010132 110 330 10000000

HMX

44 U 198-95-310132 44 130 10000000

Nitrobenzene

890 U 155-63-010132 890 2,700 10000000

Nitroglycerin

89 U 188-72-210132 89 130 10000000

2-Nitrotoluene

110 U 199-08-110132 110 130 10000000

3-Nitrotoluene

89 U 199-99-010132 89 130 10000000

4-Nitrotoluene

890 U 178-11-510132 890 2,700 10000000

PETN

56 U 1121-82-410132 56 130 10000000

RDX


Page 5 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




ActionLimit

DilutionFactor

CATNo.


0Tetryl

44 U 199-35-410132 44 130 10000000


44 U 1118-96-710132 44 130 10000000






0.45 U 1n.a.10199 0.45 1.4EFH (C12-C14)0.45 U 1n.a.10199 0.45 1.4EFH (C15-C20)2.2 1n.a.10199 0.45 1.4EFH (C21-C30)17 1n.a.10199 0.45 1.4EFH (C30 - C40)0.45 U 1n.a.10199 0.45 1.4EFH (C8-C11)





Page 6 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




ActionLimit

DilutionFactor

CATNo.


mg/kgmg/kgmg/kg mg/kgMetals SW-846 6010B27,800 17429-90-501643 5.54 22.0Aluminum12.7 17440-42-807914 0.980 5.50Boron67,600 57440-70-201650 33.7 110Calcium23,800 17439-89-601654 5.18 22.0Iron25.5 17439-93-201656 0.24 2.2Lithium5,230 17439-95-401657 2.80 11.0Magnesium174 17439-96-506958 0.0859 0.550Manganese208 17723-14-010145 0.616 11.0Phosphorus2,640 17440-09-701662 19.8 55.0Potassium581 17440-23-501667 41.1 110Sodium86.1 17440-24-607968 0.0682 0.550Strontium2.81 J 17440-31-506969 1.10 11.0Tin1,190 17440-32-606970 0.418 1.10Titanium5.21 J 17440-67-710146 0.925 5.50Zirconium





mg/kgmg/kgmg/kg mg/kgWet Chemistry EPA 300.06.7 116984-48-807332 0.91 1.111a Anions by 300.0 - Fluoride7.9 114797-55-807336 0.91 1.711a Anions by 300.0 - Nitrate


Page 7 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




ActionLimit

DilutionFactor

CATNo.








7.97 1n.a.00394 0.0100 0.010018a pH by 9045C







Analyst



06192


10326


Prep07320


07320



Page 8 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




Analyst



04688

1Gregory JDrahovsky




05551



Extract00819


05876



10199





Alcohols00380


05/20/2011 12:00111370018A1SW-846 8015Bmodified


1Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BAluminum016431Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BBoron079145Joanne M Gates05/18/2011 12:031113757080021SW-846 6010BCalcium016501Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BIron016541Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BLithium016561Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BMagnesium016571Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BManganese069581Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BPhosphorus101451Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BPotassium016621Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BSodium016671Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BStrontium079681Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BTin069691Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BTitanium069701Tara L Snyder05/18/2011 08:091113757080021SW-846 6010BZirconium101462Choon Y Tian05/18/2011 09:55111371026001A1SW-846 6020Antimony061242Choon Y Tian05/18/2011 09:55111371026001A1SW-846 6020Arsenic061252Choon Y Tian05/18/2011 09:55111371026001D1SW-846 6020Barium061262Choon Y Tian05/18/2011 09:55111371026001A1SW-846 6020Beryllium061272Choon Y Tian05/18/2011 09:55111371026001A1SW-846 6020Cadmium06128


Page 9 of 9



Collected: 05/16/2011 12:47

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


S0049 SDG#: DE151-10




Analyst







05/18/2011 01:001113757110021SW-846 7471Amodified



07332


07336








01352



10129






Page 1 of 2


Sample Description: TB-051611 Water SSFL Area IV Collocated Soil Sampling TB-051611 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 16:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


TB516 SDG#: DE151-11TB*




ActionLimit

DilutionFactor

CATNo.

ug/lug/lug/l ug/lGC/MS Volatiles SW-846 8260B6 U 167-64-110904 6 20Acetone0.5 U 171-43-210904 0.5 5Benzene1 U 1108-86-110904 1 5Bromobenzene1 U 174-97-510904 1 5Bromochloromethane1 U 175-27-410904 1 5Bromodichloromethane1 U 175-25-210904 1 5Bromoform1 U 174-83-910904 1 5Bromomethane3 U 178-93-310904 3 102-Butanone1 U 1104-51-810904 1 5n-Butylbenzene1 U 1135-98-810904 1 5sec-Butylbenzene1 U 198-06-610904 1 5tert-Butylbenzene1 U 156-23-510904 1 5Carbon Tetrachloride0.8 U 1108-90-710904 0.8 5Chlorobenzene1 U 175-00-310904 1 5Chloroethane2 U 1110-75-810904 2 102-Chloroethyl Vinyl Ether

2-Chloroethyl vinyl ether may not be recovered if acid was used topreserve this sample.

0.8 U 167-66-310904 0.8 5Chloroform1 U 174-87-310904 1 5Chloromethane1 U 195-49-810904 1 52-Chlorotoluene1 U 1106-43-410904 1 54-Chlorotoluene2 U 179-38-910904 2 5Chlorotrifluoroethene2 U 196-12-810904 2 51,2-Dibromo-3-chloropropane1 U 1124-48-110904 1 5Dibromochloromethane1 U 1106-93-410904 1 51,2-Dibromoethane1 U 174-95-310904 1 5Dibromomethane1 U 195-50-110904 1 51,2-Dichlorobenzene1 U 1541-73-110904 1 51,3-Dichlorobenzene1 U 1106-46-710904 1 51,4-Dichlorobenzene2 U 175-71-810904 2 5Dichlorodifluoromethane1 U 175-34-310904 1 51,1-Dichloroethane1 U 1107-06-210904 1 51,2-Dichloroethane0.8 U 175-35-410904 0.8 51,1-Dichloroethene0.8 U 1156-59-210904 0.8 5cis-1,2-Dichloroethene0.8 U 1156-60-510904 0.8 5trans-1,2-Dichloroethene1 U 178-87-510904 1 51,2-Dichloropropane1 U 1142-28-910904 1 51,3-Dichloropropane1 U 1594-20-710904 1 52,2-Dichloropropane1 U 1563-58-610904 1 51,1-Dichloropropene1 U 110061-01-510904 1 5cis-1,3-Dichloropropene1 U 110061-02-610904 1 5trans-1,3-Dichloropropene0.8 U 1100-41-410904 0.8 5Ethylbenzene2 U 176-13-110904 2 10Freon 1132 U 175-88-710904 2 5Freon 133a2 U 187-68-310904 2 5Hexachlorobutadiene3 U 1591-78-610904 3 102-Hexanone1 U 198-82-810904 1 5Isopropylbenzene1 U 199-87-610904 1 5p-Isopropyltoluene0.5 U 11634-04-410904 0.5 5Methyl Tertiary Butyl Ether3 U 1108-10-110904 3 104-Methyl-2-pentanone


Page 2 of 2


Sample Description: TB-051611 Water SSFL Area IV Collocated Soil Sampling TB-051611 Project Name: SSFL Area IV Collocated Soil Sampling

Collected: 05/16/2011 16:30

Submitted: 05/17/2011 09:40


Reported: 06/21/2011 13:43


TB516 SDG#: DE151-11TB*




ActionLimit

DilutionFactor

CATNo.

ug/lug/lug/l ug/lGC/MS Volatiles SW-846 8260B2 U 175-09-210904 2 5Methylene Chloride1 U 1103-65-110904 1 5n-Propylbenzene1 U 1100-42-510904 1 5Styrene1 U 1630-20-610904 1 51,1,1,2-Tetrachloroethane1 U 179-34-510904 1 51,1,2,2-Tetrachloroethane0.8 U 1127-18-410904 0.8 5Tetrachloroethene0.7 U 1108-88-310904 0.7 5Toluene1 U 187-61-610904 1 51,2,3-Trichlorobenzene1 U 1120-82-110904 1 51,2,4-Trichlorobenzene0.8 U 171-55-610904 0.8 51,1,1-Trichloroethane0.8 U 179-00-510904 0.8 51,1,2-Trichloroethane1 U 179-01-610904 1 5Trichloroethene2 U 175-69-410904 2 5Trichlorofluoromethane1 U 196-18-410904 1 51,2,3-Trichloropropane1 U 195-63-610904 1 51,2,4-Trimethylbenzene1 U 1108-67-810904 1 51,3,5-Trimethylbenzene1 U 175-01-410904 1 5Vinyl Chloride0.8 U 1179601-23-110904 0.8 5m+p-Xylene0.8 U 195-47-610904 0.8 5o-Xylene

ug/lug/lug/l ug/lGC/MS Volatiles SW-846 8260B SIM0.5 U 1123-91-100527 0.5 2.01,4-Dioxane

ug/lug/lug/l ug/lGC Volatiles TPH GRO SW-8015B20 U 1n.a.08229 20 50TPH-GRO S.CA water C5-C12





Analyst


1Kevin A Sposito05/18/2011 00:12L111372AA1SW-846 8260B1b Volatile OrganicsEPA8260

10904

1Jason M Long05/17/2011 13:52E111371AA1SW-846 8260B SIM14b 1,4-Dioxane by 8260BSIM

00527

1Jason M Long05/17/2011 13:52E111371AA1SW-846 5030BGC/MS VOA Water Prep011631Kevin A Sposito05/18/2011 00:12L111372AA2SW-846 5030BGC/MS VOA Water Prep011631Carrie E Miller05/23/2011 23:0111143A20A1TPH GRO SW-8015B9b TPH by EPA 8015B Gas C5-

C1208229

1Carrie E Miller05/23/2011 23:0111143A20A1SW-846 5030BGC VOA Water Prep01146


Page 1 of 24

Quality Control Summary

Client Name: CDM Federal Programs Corp. Group Number: 1247140Reported: 06/21/11 at 01:43 PM

*- Outside of specification**-This limit was used in the evaluation of the final result for the blank(1) The result for one or both determinations was less than five times the LOQ.(2) The unspiked result was more than four times the spike added.

Matrix QC may not be reported if site-specific QC samples were notsubmitted. In these situations, to demonstrate precision and accuracy ata batch level, a LCS/LCSD was performed, unless otherwise specified in themethod.

Laboratory Compliance Quality Control

Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max

Batch number: B111401AA Sample number(s): 6288929-6288931,6288933-6288934,6288936,6288938-6288941Acetone 6.7 U 6.7 8.0 ug/kg 136 32-209Benzene 0.10 U 0.10 4.0 ug/kg 103 80-120Bromobenzene 0.13 U 0.13 4.0 ug/kg 103 79-120Bromochloromethane 0.33 U 0.33 4.0 ug/kg 125* 79-124Bromodichloromethane 0.08 U 0.08 4.0 ug/kg 100 78-120Bromoform 0.40 U 0.40 4.0 ug/kg 104 70-120Bromomethane 0.25 U 0.25 4.0 ug/kg 65 32-1622-Butanone 1.2 U 1.2 8.0 ug/kg 127 46-153n-Butylbenzene 0.12 U 0.12 4.0 ug/kg 98 72-120sec-Butylbenzene 0.06 U 0.06 4.0 ug/kg 105 75-120tert-Butylbenzene 0.16 U 0.16 4.0 ug/kg 97 75-120Carbon Tetrachloride 0.14 U 0.14 4.0 ug/kg 106 69-122Chlorobenzene 0.11 U 0.11 4.0 ug/kg 100 80-120Chloroethane 0.13 U 0.13 4.0 ug/kg 61 37-1542-Chloroethyl Vinyl Ether 0.30 U 0.30 4.0 ug/kg 94 43-146Chloroform 0.12 U 0.12 4.0 ug/kg 101 80-120Chloromethane 0.33 U 0.33 4.0 ug/kg 68 54-1322-Chlorotoluene 0.14 U 0.14 4.0 ug/kg 99 78-1204-Chlorotoluene 0.14 U 0.14 4.0 ug/kg 96 79-120Chlorotrifluoroethene 0.50 U 0.50 5.0 ug/kg 74 22-1311,2-Dibromo-3-chloropropane 0.70 U 0.70 4.0 ug/kg 96 58-120Dibromochloromethane 0.20 U 0.20 4.0 ug/kg 103 77-1201,2-Dibromoethane 0.17 U 0.17 4.0 ug/kg 100 80-120Dibromomethane 0.24 U 0.24 4.0 ug/kg 100 80-1201,2-Dichlorobenzene 0.09 U 0.09 4.0 ug/kg 100 79-1201,3-Dichlorobenzene 0.12 U 0.12 4.0 ug/kg 102 78-1201,4-Dichlorobenzene 0.16 U 0.16 4.0 ug/kg 100 79-120Dichlorodifluoromethane 0.12 U 0.12 4.0 ug/kg 66 20-1201,1-Dichloroethane 0.10 U 0.10 4.0 ug/kg 102 80-1201,2-Dichloroethane 0.15 U 0.15 4.0 ug/kg 100 71-1291,1-Dichloroethene 0.39 U 0.39 4.0 ug/kg 77 73-123cis-1,2-Dichloroethene 0.19 U 0.19 4.0 ug/kg 99 80-120trans-1,2-Dichloroethene 0.12 U 0.12 4.0 ug/kg 98 79-1201,2-Dichloropropane 0.17 U 0.17 4.0 ug/kg 102 80-1201,3-Dichloropropane 0.08 U 0.08 4.0 ug/kg 99 80-1202,2-Dichloropropane 0.17 U 0.17 4.0 ug/kg 91 72-1231,1-Dichloropropene 0.13 U 0.13 4.0 ug/kg 101 77-120cis-1,3-Dichloropropene 0.16 U 0.16 4.0 ug/kg 97 80-120trans-1,3-Dichloropropene 0.17 U 0.17 4.0 ug/kg 91 77-120Ethylbenzene 0.06 U 0.06 4.0 ug/kg 96 80-120Freon 113 0.11 U 0.11 4.0 ug/kg 85 61-126Freon 133a 0.50 U 0.50 5.0 ug/kg 81 78-120Hexachlorobutadiene 0.14 U 0.14 4.0 ug/kg 114 57-1202-Hexanone 1.6 U 1.6 8.0 ug/kg 115 45-155Isopropylbenzene 0.06 U 0.06 4.0 ug/kg 101 76-120p-Isopropyltoluene 0.11 U 0.11 4.0 ug/kg 103 75-120

Page 2 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD MaxMethyl Tertiary Butyl Ether 0.21 U 0.21 4.0 ug/kg 92 74-1214-Methyl-2-pentanone 0.39 U 0.39 8.0 ug/kg 101 61-134Methylene Chloride 0.39 J 0.24 4.0 ug/kg 77 76-124n-Propylbenzene 0.07 U 0.07 4.0 ug/kg 104 77-120Styrene 0.10 U 0.10 4.0 ug/kg 94 76-1201,1,1,2-Tetrachloroethane 0.11 U 0.11 4.0 ug/kg 104 80-1201,1,2,2-Tetrachloroethane 0.23 U 0.23 4.0 ug/kg 96 71-123Tetrachloroethene 0.20 U 0.20 4.0 ug/kg 117 77-120Toluene 0.08 U 0.08 4.0 ug/kg 98 80-1201,2,3-Trichlorobenzene 0.14 U 0.14 4.0 ug/kg 104 64-1201,2,4-Trichlorobenzene 0.18 U 0.18 4.0 ug/kg 94 68-1201,1,1-Trichloroethane 0.20 U 0.20 4.0 ug/kg 101 71-1251,1,2-Trichloroethane 0.27 U 0.27 4.0 ug/kg 98 80-120Trichloroethene 0.15 U 0.15 4.0 ug/kg 100 80-120Trichlorofluoromethane 0.29 U 0.29 4.0 ug/kg 78 58-1331,2,3-Trichloropropane 0.33 U 0.33 4.0 ug/kg 101 71-1231,2,4-Trimethylbenzene 0.40 U 0.40 4.0 ug/kg 100 79-1201,3,5-Trimethylbenzene 0.10 U 0.10 4.0 ug/kg 100 78-120Vinyl Chloride 0.20 U 0.20 4.0 ug/kg 68 53-120m+p-Xylene 0.17 U 0.17 4.0 ug/kg 98 80-120o-Xylene 0.17 U 0.17 4.0 ug/kg 96 80-120

Batch number: E111371AA Sample number(s): 6288935,62889421,4-Dioxane 0.5 U 0.5 2.0 ug/l 110 109 80-123 1 30

Batch number: E111381AA Sample number(s): 6288929-6288931,6288933-6288934,6288936,6288938-62889411,4-Dioxane 5.0 U 5.0 15 ug/kg 104 106 70-130 2 30

Batch number: L111372AA Sample number(s): 6288935,6288942Acetone 6 U 6. 20 ug/l 90 85 49-234 5 30Benzene 0.5 U 0.5 5 ug/l 99 96 79-120 3 30Bromobenzene 1 U 1. 5 ug/l 94 89 80-120 5 30Bromochloromethane 1 U 1. 5 ug/l 96 90 80-120 6 30Bromodichloromethane 1 U 1. 5 ug/l 90 87 80-120 4 30Bromoform 1 U 1. 5 ug/l 81 78 61-120 4 30Bromomethane 1 U 1. 5 ug/l 117 113 44-120 3 302-Butanone 3 U 3. 10 ug/l 91 87 66-151 4 30n-Butylbenzene 1 U 1. 5 ug/l 99 95 74-120 4 30sec-Butylbenzene 1 U 1. 5 ug/l 96 91 78-120 5 30tert-Butylbenzene 1 U 1. 5 ug/l 93 91 80-120 2 30Carbon Tetrachloride 1 U 1. 5 ug/l 92 87 75-123 6 30Chlorobenzene 0.8 U 0.8 5 ug/l 94 91 80-120 4 30Chloroethane 1 U 1. 5 ug/l 110 106 49-129 4 302-Chloroethyl Vinyl Ether 2 U 2. 10 ug/l 93 90 56-129 4 30Chloroform 0.8 U 0.8 5 ug/l 96 92 77-122 4 30Chloromethane 1 U 1. 5 ug/l 109 104 60-129 4 302-Chlorotoluene 1 U 1. 5 ug/l 95 93 80-120 3 304-Chlorotoluene 1 U 1. 5 ug/l 97 93 80-120 4 30Chlorotrifluoroethene 2 U 2. 5 ug/l 54 55 38-136 1 301,2-Dibromo-3-chloropropane 2 U 2. 5 ug/l 87 84 56-126 4 30Dibromochloromethane 1 U 1. 5 ug/l 88 84 80-120 5 301,2-Dibromoethane 1 U 1. 5 ug/l 96 92 80-120 5 30Dibromomethane 1 U 1. 5 ug/l 92 87 80-120 5 301,2-Dichlorobenzene 1 U 1. 5 ug/l 95 91 80-120 5 301,3-Dichlorobenzene 1 U 1. 5 ug/l 94 91 80-120 3 301,4-Dichlorobenzene 1 U 1. 5 ug/l 95 91 80-120 5 30Dichlorodifluoromethane 2 U 2. 5 ug/l 93 89 47-120 5 301,1-Dichloroethane 1 U 1. 5 ug/l 97 94 79-120 4 30

Page 3 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max1,2-Dichloroethane 1 U 1. 5 ug/l 95 92 70-130 4 301,1-Dichloroethene 0.8 U 0.8 5 ug/l 97 95 74-123 2 30cis-1,2-Dichloroethene 0.8 U 0.8 5 ug/l 95 92 80-120 4 30trans-1,2-Dichloroethene 0.8 U 0.8 5 ug/l 97 93 80-120 4 301,2-Dichloropropane 1 U 1. 5 ug/l 96 93 78-120 4 301,3-Dichloropropane 1 U 1. 5 ug/l 96 92 80-120 5 302,2-Dichloropropane 1 U 1. 5 ug/l 93 88 77-124 5 301,1-Dichloropropene 1 U 1. 5 ug/l 95 93 80-120 3 30cis-1,3-Dichloropropene 1 U 1. 5 ug/l 91 89 80-120 3 30trans-1,3-Dichloropropene 1 U 1. 5 ug/l 91 86 79-120 5 30Ethylbenzene 0.8 U 0.8 5 ug/l 98 93 79-120 5 30Freon 113 2 U 2. 10 ug/l 100 92 69-128 8 30Freon 133a 2 U 2. 5 ug/l 95 93 77-120 2 30Hexachlorobutadiene 2 U 2. 5 ug/l 85 82 58-120 4 302-Hexanone 3 U 3. 10 ug/l 91 87 65-136 5 30Isopropylbenzene 1 U 1. 5 ug/l 98 93 77-120 5 30p-Isopropyltoluene 1 U 1. 5 ug/l 92 89 80-120 4 30Methyl Tertiary Butyl Ether 0.5 U 0.5 5 ug/l 94 89 76-120 5 304-Methyl-2-pentanone 3 U 3. 10 ug/l 90 87 70-121 4 30Methylene Chloride 2 U 2. 5 ug/l 98 93 80-120 5 30n-Propylbenzene 1 U 1. 5 ug/l 94 92 80-120 3 30Styrene 1 U 1. 5 ug/l 94 90 80-120 5 301,1,1,2-Tetrachloroethane 1 U 1. 5 ug/l 93 88 80-120 6 301,1,2,2-Tetrachloroethane 1 U 1. 5 ug/l 101 96 71-120 5 30Tetrachloroethene 0.8 U 0.8 5 ug/l 93 87 80-121 6 30Toluene 0.7 U 0.7 5 ug/l 98 94 79-120 5 301,2,3-Trichlorobenzene 1 U 1. 5 ug/l 90 89 65-120 2 301,2,4-Trichlorobenzene 1 U 1. 5 ug/l 87 83 67-120 4 301,1,1-Trichloroethane 0.8 U 0.8 5 ug/l 92 89 75-127 3 301,1,2-Trichloroethane 0.8 U 0.8 5 ug/l 95 92 80-120 4 30Trichloroethene 1 U 1. 5 ug/l 93 90 80-120 4 30Trichlorofluoromethane 2 U 2. 5 ug/l 106 102 64-129 4 301,2,3-Trichloropropane 1 U 1. 5 ug/l 96 90 80-120 7 301,2,4-Trimethylbenzene 1 U 1. 5 ug/l 97 94 74-120 4 301,3,5-Trimethylbenzene 1 U 1. 5 ug/l 96 92 75-120 5 30Vinyl Chloride 1 U 1. 5 ug/l 109 106 65-125 3 30m+p-Xylene 0.8 U 0.8 5 ug/l 96 91 80-120 5 30o-Xylene 0.8 U 0.8 5 ug/l 94 91 80-120 3 30

Batch number: 11138WAD026 Sample number(s): 6288935Aniline 1 U 1. 5 ug/l 72 80 49-101 11 30Benzidine 20 U 20. 60 ug/l 68 72 34-117 4 30Benzoic acid 6 U 6. 15 ug/l 25 34 10-69 31* 30Benzyl alcohol 5 U 5. 15 ug/l 71 85 66-97 17 304-Bromophenyl-phenylether 1 U 1. 5 ug/l 90 95 82-117 5 30Carbazole 1 U 1. 5 ug/l 92 93 81-114 2 304-Chloro-3-methylphenol 1 U 1. 5 ug/l 92 94 70-123 2 304-Chloroaniline 1 U 1. 5 ug/l 82 85 42-124 4 30bis(2-Chloroethoxy)methane 1 U 1. 5 ug/l 88 92 74-124 4 30bis(2-Chloroethyl)ether 1 U 1. 5 ug/l 82 84 77-108 3 30bis(2-Chloroisopropyl)ether 1 U 1. 5 ug/l 79 82 62-127 5 302-Chloronaphthalene 2 U 2. 5 ug/l 85 90 54-132 6 302-Chlorophenol 1 U 1. 5 ug/l 85 88 77-108 4 304-Chlorophenyl-phenylether 2 U 2. 5 ug/l 94 101 82-111 7 30Dibenzofuran 1 U 1. 5 ug/l 90 94 83-108 5 301,2-Dichlorobenzene 1 U 1. 5 ug/l 85 86 55-118 1 301,3-Dichlorobenzene 1 U 1. 5 ug/l 84 87 50-119 4 301,4-Dichlorobenzene 1 U 1. 5 ug/l 82 85 53-119 4 30

Page 4 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max3,3'-Dichlorobenzidine 2 U 2. 5 ug/l 64 71 49-111 11 302,4-Dichlorophenol 1 U 1. 5 ug/l 94 96 80-109 2 302,4-Dimethylphenol 3 U 3. 10 ug/l 86 89 72-110 4 303,5-Dimethylphenol 3 U 3. 10 ug/l 91 95 70-130 5 304,6-Dinitro-2-methylphenol 5 U 5. 15 ug/l 96 98 78-119 2 302,4-Dinitrophenol 10 U 10. 30 ug/l 79 85 52-131 7 302,4-Dinitrotoluene 1 U 1. 5 ug/l 95 100 81-115 5 302,6-Dinitrotoluene 1 U 1. 5 ug/l 92 93 85-115 1 301,2-Diphenylhydrazine 1 U 1. 5 ug/l 83 85 78-116 2 30Hexachlorobenzene 1 U 1. 5 ug/l 98 101 81-118 3 30Hexachlorobutadiene 1 U 1. 5 ug/l 93 94 57-124 0 30Hexachlorocyclopentadiene 5 U 5. 15 ug/l 67 72 36-118 7 30Hexachloroethane 1 U 1. 5 ug/l 76 78 52-113 2 30Isophorone 1 U 1. 5 ug/l 90 91 74-117 1 302-Methylphenol 1 U 1. 5 ug/l 74 81 64-101 10 304-Methylphenol 2 U 2. 5 ug/l 60* 66 61-103 9 302-Nitroaniline 1 U 1. 5 ug/l 91 90 83-116 1 303-Nitroaniline 1 U 1. 5 ug/l 92 95 74-113 3 304-Nitroaniline 1 U 1. 5 ug/l 80 82 59-100 3 30Nitrobenzene 1 U 1. 5 ug/l 87 91 75-109 4 302-Nitrophenol 1 U 1. 5 ug/l 88 89 86-120 2 304-Nitrophenol 10 U 10. 30 ug/l 25 31 16-78 20 30N-Nitroso-di-n-propylamine 1 U 1. 5 ug/l 82 88 69-110 7 30N-Nitrosodiphenylamine 2 U 2. 5 ug/l 86 88 67-136 3 30Pentachlorophenol 3 U 3. 15 ug/l 77 76 53-110 2 30Phenol 1 U 1. 5 ug/l 33 40 21-67 20 301,2,4-Trichlorobenzene 1 U 1. 5 ug/l 91 94 71-112 3 302,4,5-Trichlorophenol 1 U 1. 5 ug/l 86 89 79-107 3 302,4,6-Trichlorophenol 1 U 1. 5 ug/l 87 89 81-113 2 30

Batch number: 11138WAG026 Sample number(s): 6288935Acenaphthene 0.010 U 0.010 0.050 ug/l 98 97 74-109 2 30Acenaphthylene 0.010 U 0.010 0.050 ug/l 95 95 70-110 0 30Anthracene 0.010 U 0.010 0.050 ug/l 102 101 66-111 1 30Benzo(a)anthracene 0.010 U 0.010 0.050 ug/l 106 105 72-114 1 30Benzo(a)pyrene 0.010 U 0.010 0.050 ug/l 107 109 60-127 1 30Benzo(b)fluoranthene 0.010 U 0.010 0.050 ug/l 122 124* 69-123 1 30Benzo(g,h,i)perylene 0.010 U 0.010 0.050 ug/l 107 105 57-131 2 30Benzo(k)fluoranthene 0.010 U 0.010 0.050 ug/l 105 109 59-130 4 30Butylbenzylphthalate 0.050 U 0.050 1.0 ug/l 94 90 40-138 4 30Di-n-butylphthalate 0.050 U 0.050 1.0 ug/l 101 97 74-131 4 30Chrysene 0.010 U 0.010 0.050 ug/l 104 103 76-116 1 30Dibenz(a,h)anthracene 0.010 U 0.010 0.050 ug/l 107 108 55-134 2 30Diethylphthalate 0.050 U 0.050 1.0 ug/l 99 99 57-134 1 30Dimethylphthalate 0.050 U 0.050 1.0 ug/l 88 88 40-119 0 30Bis(2-Ethylhexyl)phthalate 0.050 U 0.050 1.0 ug/l 118 107 57-154 10 30Fluoranthene 0.010 U 0.010 0.050 ug/l 102 106 75-116 3 30Fluorene 0.010 U 0.010 0.050 ug/l 104 103 75-114 1 30Indeno(1,2,3-cd)pyrene 0.010 U 0.010 0.050 ug/l 105 107 69-124 2 301-Methylnaphthalene 0.010 U 0.010 0.050 ug/l 101 100 71-117 1 302-Methylnaphthalene 0.010 U 0.010 0.050 ug/l 90 89 75-115 2 30Naphthalene 0.030 U 0.030 0.050 ug/l 96 96 72-109 0 30N-Nitrosodimethylamine 0.010 U 0.010 0.050 ug/l 48 50 36-89 5 30Di-n-octylphthalate 0.050 U 0.050 1.0 ug/l 117 124 57-145 6 30Phenanthrene 0.010 U 0.010 0.050 ug/l 98 97 76-111 0 30Pyrene 0.010 U 0.010 0.050 ug/l 100 98 69-118 2 30

Batch number: 11139SLG026 Sample number(s): 6288929-6288931,6288933-6288934,6288936-6288939,6288941

Page 5 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD MaxAcenaphthene 0.67 U 0.67 1.7 ug/kg 100 63-120Acenaphthylene 0.33 U 0.33 1.7 ug/kg 92 60-120Anthracene 0.33 U 0.33 1.7 ug/kg 96 55-120Benzo(a)anthracene 0.67 U 0.67 1.7 ug/kg 104 74-120Benzo(a)pyrene 0.67 U 0.67 1.7 ug/kg 103 58-129Benzo(b)fluoranthene 0.67 U 0.67 1.7 ug/kg 112 63-143Benzo(g,h,i)perylene 0.67 U 0.67 1.7 ug/kg 116 44-138Benzo(k)fluoranthene 0.67 U 0.67 1.7 ug/kg 107 54-142Butylbenzylphthalate 6.0 U 6.0 18 ug/kg 114 65-131Di-n-butylphthalate 6.0 U 6.0 18 ug/kg 113 75-137Chrysene 0.33 U 0.33 1.7 ug/kg 104 73-114Dibenz(a,h)anthracene 0.67 U 0.67 1.7 ug/kg 117 53-138Diethylphthalate 6.0 U 6.0 18 ug/kg 103 68-125Dimethylphthalate 6.0 U 6.0 18 ug/kg 104 79-121Bis(2-Ethylhexyl)phthalate 6.0 U 6.0 18 ug/kg 136 67-143Fluoranthene 0.67 U 0.67 1.7 ug/kg 107 64-120Fluorene 0.67 U 0.67 1.7 ug/kg 109 71-120Indeno(1,2,3-cd)pyrene 0.67 U 0.67 1.7 ug/kg 115 56-1341-Methylnaphthalene 0.67 U 0.67 1.7 ug/kg 106 72-1202-Methylnaphthalene 0.67 U 0.67 1.7 ug/kg 94 62-120Naphthalene 1.1 J 0.67 1.7 ug/kg 104 67-120N-Nitrosodimethylamine 0.67 U 0.67 1.7 ug/kg 96 55-118Di-n-octylphthalate 6.0 U 6.0 18 ug/kg 124 55-176Phenanthrene 0.67 U 0.67 1.7 ug/kg 100 75-120Pyrene 0.67 U 0.67 1.7 ug/kg 102 56-121

Batch number: 11139SLH026 Sample number(s): 6288929-6288931,6288933-6288934,6288936-6288941Acenaphthene 17 U 17. 170 ug/kg 96 76-111Acenaphthylene 17 U 17. 170 ug/kg 98 75-122Aniline 170

U170. 500 ug/kg 71 34-94

Anthracene 17 U 17. 170 ug/kg 97 76-112Benzidine 1,200

U1,200. 3,300 ug/kg 50 15-121

Benzo(a)anthracene 17 U 17. 170 ug/kg 98 73-112Benzo(a)pyrene 17 U 17. 170 ug/kg 99 69-122Benzo(b)fluoranthene 17 U 17. 170 ug/kg 96 61-127Benzo(g,h,i)perylene 17 U 17. 170 ug/kg 89 65-122Benzo(k)fluoranthene 17 U 17. 170 ug/kg 105 67-125Benzoic acid 170

U170. 500 ug/kg 69 62-113

Benzyl alcohol 170U

170. 500 ug/kg 96 68-111

4-Bromophenyl-phenylether 17 U 17. 170 ug/kg 97 79-117Butylbenzylphthalate 17 U 17. 170 ug/kg 98 75-115Di-n-butylphthalate 17 U 17. 170 ug/kg 91 79-112Carbazole 17 U 17. 170 ug/kg 94 77-1134-Chloro-3-methylphenol 33 U 33. 170 ug/kg 93 74-1194-Chloroaniline 67 U 67. 170 ug/kg 42 10-110bis(2-Chloroethoxy)methane 17 U 17. 170 ug/kg 97 70-118bis(2-Chloroethyl)ether 17 U 17. 170 ug/kg 91 70-104bis(2-Chloroisopropyl)ether 17 U 17. 170 ug/kg 87 68-1312-Chloronaphthalene 17 U 17. 170 ug/kg 87 49-1282-Chlorophenol 17 U 17. 170 ug/kg 98 72-1124-Chlorophenyl-phenylether 33 U 33. 170 ug/kg 95 79-110Chrysene 17 U 17. 170 ug/kg 96 76-113Dibenz(a,h)anthracene 17 U 17. 170 ug/kg 90 70-128Dibenzofuran 17 U 17. 170 ug/kg 95 79-108

Page 6 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max1,2-Dichlorobenzene 17 U 17. 170 ug/kg 87 79-1021,3-Dichlorobenzene 17 U 17. 170 ug/kg 86 70-981,4-Dichlorobenzene 17 U 17. 170 ug/kg 87 74-1063,3'-Dichlorobenzidine 100

U100. 330 ug/kg 44 24-101

2,4-Dichlorophenol 17 U 17. 170 ug/kg 101 75-111Diethylphthalate 17 U 17. 170 ug/kg 93 76-1112,4-Dimethylphenol 33 U 33. 170 ug/kg 93 72-1113,5-Dimethylphenol 33 U 33. 170 ug/kg 104 70-130Dimethylphthalate 17 U 17. 170 ug/kg 95 77-1094,6-Dinitro-2-methylphenol 170

U170. 500 ug/kg 44* 53-110

2,4-Dinitrophenol 330U

330. 1,000 ug/kg 24* 37-120

2,4-Dinitrotoluene 33 U 33. 170 ug/kg 96 73-1152,6-Dinitrotoluene 17 U 17. 170 ug/kg 99 79-1151,2-Diphenylhydrazine 17 U 17. 170 ug/kg 99 77-111bis(2-Ethylhexyl)phthalate 17 U 17. 330 ug/kg 92 75-117Fluoranthene 17 U 17. 170 ug/kg 96 78-116Fluorene 17 U 17. 170 ug/kg 96 75-116Hexachlorobenzene 17 U 17. 170 ug/kg 94 78-116Hexachlorobutadiene 67 U 67. 170 ug/kg 89 70-112Hexachlorocyclopentadiene 170

U170. 500 ug/kg 84 46-115

Hexachloroethane 17 U 17. 170 ug/kg 88 68-105Indeno(1,2,3-cd)pyrene 17 U 17. 170 ug/kg 89 64-119Isophorone 17 U 17. 170 ug/kg 92 69-1101-Methylnaphthalene 17 U 17. 170 ug/kg 94 74-1052-Methylnaphthalene 17 U 17. 170 ug/kg 90 76-1052-Methylphenol 33 U 33. 170 ug/kg 96 66-1104-Methylphenol 33 U 33. 170 ug/kg 101 66-117Naphthalene 17 U 17. 170 ug/kg 92 73-1062-Nitroaniline 17 U 17. 170 ug/kg 97 78-1163-Nitroaniline 33 U 33. 170 ug/kg 88 62-1094-Nitroaniline 67 U 67. 170 ug/kg 70 49-98Nitrobenzene 17 U 17. 170 ug/kg 94 71-1042-Nitrophenol 17 U 17. 170 ug/kg 93 81-1144-Nitrophenol 170

U170. 500 ug/kg 84 56-118

N-Nitroso-di-n-propylamine 17 U 17. 170 ug/kg 88 63-107N-Nitrosodimethylamine 33 U 33. 170 ug/kg 92 60-106N-Nitrosodiphenylamine 17 U 17. 170 ug/kg 99 67-141Di-n-octylphthalate 17 U 17. 170 ug/kg 105 68-130Pentachlorophenol 170

U170. 500 ug/kg 66 51-117

Phenanthrene 17 U 17. 170 ug/kg 96 77-113Phenol 17 U 17. 170 ug/kg 98 58-112Pyrene 17 U 17. 170 ug/kg 104 75-1151,2,4-Trichlorobenzene 17 U 17. 170 ug/kg 97 73-1082,4,5-Trichlorophenol 33 U 33. 170 ug/kg 95 76-1072,4,6-Trichlorophenol 33 U 33. 170 ug/kg 98 78-111

Batch number: 11143SLE026 Sample number(s): 6288940Acenaphthene 0.67 U 0.67 1.7 ug/kg 97 63-120Acenaphthylene 0.33 U 0.33 1.7 ug/kg 93 60-120Anthracene 0.33 U 0.33 1.7 ug/kg 100 55-120Benzo(a)anthracene 0.67 U 0.67 1.7 ug/kg 104 74-120Benzo(a)pyrene 0.67 U 0.67 1.7 ug/kg 106 58-129

Page 7 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD MaxBenzo(b)fluoranthene 0.67 U 0.67 1.7 ug/kg 104 63-143Benzo(g,h,i)perylene 0.67 U 0.67 1.7 ug/kg 123 44-138Benzo(k)fluoranthene 0.67 U 0.67 1.7 ug/kg 104 54-142Butylbenzylphthalate 6.0 U 6.0 18 ug/kg 100 65-131Di-n-butylphthalate 6.0 U 6.0 18 ug/kg 109 75-137Chrysene 0.33 U 0.33 1.7 ug/kg 101 73-114Dibenz(a,h)anthracene 0.67 U 0.67 1.7 ug/kg 123 53-138Diethylphthalate 6.0 U 6.0 18 ug/kg 95 68-125Dimethylphthalate 6.0 U 6.0 18 ug/kg 97 79-121Bis(2-Ethylhexyl)phthalate 6.0 U 6.0 18 ug/kg 116 67-143Fluoranthene 0.67 U 0.67 1.7 ug/kg 112 64-120Fluorene 0.67 U 0.67 1.7 ug/kg 104 71-120Indeno(1,2,3-cd)pyrene 0.67 U 0.67 1.7 ug/kg 122 56-1341-Methylnaphthalene 0.67 U 0.67 1.7 ug/kg 94 72-1202-Methylnaphthalene 0.67 U 0.67 1.7 ug/kg 89 62-120Naphthalene 0.67 U 0.67 1.7 ug/kg 93 67-120N-Nitrosodimethylamine 0.67 U 0.67 1.7 ug/kg 89 55-118Di-n-octylphthalate 6.0 U 6.0 18 ug/kg 114 55-176Phenanthrene 0.67 U 0.67 1.7 ug/kg 96 75-120Pyrene 0.67 U 0.67 1.7 ug/kg 98 56-121

Batch number: 11146SLE026 Sample number(s): 6288934,6288938-6288941N-Nitrosodimethylamine 16.7 U 16.7 33.3 ng/kg 83 70-130

Batch number: 11139A34A Sample number(s): 6288934,6288938-62889419a TPH by EPA 8015B Gas C5-C12 0.2 U 0.2 1.0 mg/kg 71 73 67-119 2 30

Batch number: 11143A20A Sample number(s): 6288942TPH-GRO S.CA water C5-C12 20 U 20. 50 ug/l 109 109 75-135 0 30

Batch number: 111430006A Sample number(s): 62889384-Amino-2,6-Dinitrotoluene 60 U 60. 120 ug/kg 119 80-1202-Amino-4,6-Dinitrotoluene 40 U 40. 120 ug/kg 126* 80-1202,6-Diamino-4-nitrotoluene 80 U 80. 240 ug/kg 100 107 54-134 7 302,4-Diamino-6-nitrotoluene 80 U 80. 240 ug/kg 99 107 54-134 7 301,3-Dinitrobenzene 40 U 40. 120 ug/kg 129 51-1712,4-Dinitrotoluene 40 U 40. 120 ug/kg 119 72-1352,6-Dinitrotoluene 40 U 40. 120 ug/kg 112 80-120HMX 100

U100. 300 ug/kg 108 74-130

Nitrobenzene 40 U 40. 120 ug/kg 145* 80-120Nitroglycerin 800

U800. 2,400 ug/kg 105 80-120

2-Nitrotoluene 80 U 80. 120 ug/kg 115 78-1283-Nitrotoluene 100

U100. 120 ug/kg 119 73-127

4-Nitrotoluene 80 U 80. 120 ug/kg 113 80-120PETN 800

U800. 2,400 ug/kg 132* 80-120

RDX 50 U 50. 120 ug/kg 116 75-131Tetryl 61 U 61. 120 ug/kg 82 70-1681,3,5-Trinitrobenzene 40 U 40. 120 ug/kg 119 77-1372,4,6-Trinitrotoluene 40 U 40. 120 ug/kg 121* 80-120

Batch number: 111450004A Sample number(s): 6288934,6288939-62889414-Amino-2,6-Dinitrotoluene 60 U 60. 120 ug/kg 112 80-1202-Amino-4,6-Dinitrotoluene 40 U 40. 120 ug/kg 115 80-1202,6-Diamino-4-nitrotoluene 80 U 80. 240 ug/kg 95 0* 54-134 200* 30

Page 8 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max2,4-Diamino-6-nitrotoluene 80 U 80. 240 ug/kg 95 0* 54-134 200* 301,3-Dinitrobenzene 40 U 40. 120 ug/kg 119 51-1712,4-Dinitrotoluene 40 U 40. 120 ug/kg 109 72-1352,6-Dinitrotoluene 40 U 40. 120 ug/kg 105 80-120HMX 100

U100. 300 ug/kg 101 74-130

Nitrobenzene 40 U 40. 120 ug/kg 132* 80-120Nitroglycerin 800

U800. 2,400 ug/kg 97 80-120

2-Nitrotoluene 80 U 80. 120 ug/kg 106 78-1283-Nitrotoluene 100

U100. 120 ug/kg 109 73-127

4-Nitrotoluene 80 U 80. 120 ug/kg 105 80-120PETN 800

U800. 2,400 ug/kg 123* 80-120

RDX 50 U 50. 120 ug/kg 106 75-131Tetryl 61 U 61. 120 ug/kg 72 70-1681,3,5-Trinitrobenzene 40 U 40. 120 ug/kg 109 77-1372,4,6-Trinitrotoluene 40 U 40. 120 ug/kg 108 80-120

Batch number: 111400002A Sample number(s): 6288934,6288938-628894125a Formaldehyde 8315A 600

U600. 1,500 ug/kg 92 80-126

Batch number: 111390003A Sample number(s): 62889386a Perchlorate EPA 6850 2.1 U 2.1 5.0 ug/kg 103 70-130

Batch number: 111380016A Sample number(s): 6288935Aroclor 5432 0.10 U 0.10 0.50 ug/lAroclor 5442 0.10 U 0.10 0.50 ug/l 88* 94* 35-84 7 30Aroclor 5460 0.10 U 0.10 0.50 ug/lPCB-1016 0.10 U 0.10 0.50 ug/l 98 104 51-128 6 30PCB-1221 0.10 U 0.10 0.50 ug/lPCB-1232 0.20 U 0.20 0.50 ug/lPCB-1242 0.10 U 0.10 0.50 ug/lPCB-1248 0.10 U 0.10 0.50 ug/lPCB-1254 0.10 U 0.10 0.50 ug/lPCB-1260 0.15 U 0.15 0.50 ug/l 82 100 56-135 20 30PCB-1262 0.20 U 0.20 0.50 ug/lPCB-1268 0.16 U 0.16 0.50 ug/l

Batch number: 111380023A Sample number(s): 6288929-6288931,6288933-6288934,6288936-6288941Aroclor 5432 1.0 U 1.0 3.3 ug/kgAroclor 5442 1.0 U 1.0 3.3 ug/kg 103 99 36-106 3 30Aroclor 5460 1.0 U 1.0 3.3 ug/kgPCB-1016 0.33 U 0.33 1.7 ug/kg 110 72-120PCB-1221 0.33 U 0.33 1.7 ug/kgPCB-1232 0.33 U 0.33 1.7 ug/kgPCB-1242 0.33 U 0.33 1.7 ug/kgPCB-1248 0.33 U 0.33 1.7 ug/kgPCB-1254 0.33 U 0.33 1.7 ug/kgPCB-1260 0.39 U 0.39 1.7 ug/kg 119 65-137PCB-1262 0.33 U 0.33 1.7 ug/kgPCB-1268 0.33 U 0.33 1.7 ug/kg

Batch number: 111380034A Sample number(s): 6288934,6288938-6288941EFH (C12-C14) 0.40 U 0.40 1.2 mg/kg 80 71-118EFH (C15-C20) 0.40 U 0.40 1.2 mg/kg 82 76-122

Page 9 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD MaxEFH (C21-C30) 0.40 U 0.40 1.2 mg/kg 85 69-132EFH (C30 - C40) 0.40 U 0.40 1.2 mg/kg 75 67-127EFH (C8-C11) 0.40 U 0.40 1.2 mg/kg 67 54-107

Batch number: 111370018A Sample number(s): 6288934,6288938-6288941Diethylene glycol 5.0 U 5.0 10 mg/kg 90 75-125Ethylene glycol 5.0 U 5.0 10 mg/kg 91 65-122Propylene glycol 5.0 U 5.0 10 mg/kg 91 75-125

Batch number: 111390030A Sample number(s): 6288934,6288938-6288941Ethanol 100

U100. 500 ug/kg 93 71-129

Isopropanol 100U

100. 500 ug/kg 92 75-125

Methanol 100U

100. 500 ug/kg 97 68-129

Batch number: 111390019A Sample number(s): 6288934,6288939-6288941m-Terphenyl 1.5 U 1.5 3.5 mg/kg 85 75-125o-Terphenyl 1.5 U 1.5 3.5 mg/kg 99 75-125p-Terphenyl 1.5 U 1.5 3.5 mg/kg 93 75-125

Batch number: 111460029A Sample number(s): 6288938m-Terphenyl 1.5 U 1.5 3.5 mg/kg 84 75-125o-Terphenyl 1.5 U 1.5 3.5 mg/kg 96 75-125p-Terphenyl 1.5 U 1.5 3.5 mg/kg 91 75-125

Batch number: 111371026001A Sample number(s): 6288929-6288934,6288936-6288941Antimony 0.0600 U 0.0600 0.200 mg/kg 149 27-181Arsenic 0.0800 U 0.0800 0.400 mg/kg 101 83-113Beryllium 0.0160 U 0.0160 0.100 mg/kg 102 86-111Cadmium 0.0400 U 0.0400 0.100 mg/kg 99 82-118Chromium 0.120 U 0.120 0.400 mg/kg 114 80-120Cobalt 0.0200 U 0.0200 0.100 mg/kg 102 82-118Copper 0.0827 J 0.0660 0.400 mg/kg 98 83-110Lead 0.0381 J 0.0104 0.200 mg/kg 100 83-110Nickel 0.100 U 0.100 0.400 mg/kg 100 81-110Silver 0.0120 U 0.0120 0.100 mg/kg 100 81-111Thallium 0.0300 U 0.0300 0.100 mg/kg 100 83-110Vanadium 0.0220 U 0.0220 0.100 mg/kg 106 84-116Zinc 0.560 U 0.560 3.00 mg/kg 100 81-112

Batch number: 111371026001B Sample number(s): 6288929-6288934,6288936-6288941Selenium 0.0400 U 0.0400 0.400 mg/kg 104 83-111

Batch number: 111371026001C Sample number(s): 6288929-6288934,6288936-6288941Molybdenum 0.0500 U 0.0500 0.100 mg/kg 111 78-122

Batch number: 111371026001D Sample number(s): 6288929-6288934,6288936-6288941Barium 0.108 U 0.108 0.400 mg/kg 100 81-111

Batch number: 111375708002 Sample number(s): 6288929-6288934,6288936-6288941Aluminum 5.03 U 5.03 20.0 mg/kg 97 61-110Boron 0.890 U 0.890 5.00 mg/kg 92 78-110Calcium 6.13 U 6.13 20.0 mg/kg 98 88-110Iron 4.71 U 4.71 20.0 mg/kg 102 61-110Lithium 0.22 U 0.22 2.0 mg/kg 105 80-120Magnesium 2.54 U 2.54 10.0 mg/kg 99 82-110

Page 10 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD MaxManganese 0.0780 U 0.0780 0.500 mg/kg 100 89-112Phosphorus 1.24 J 0.560 10.0 mg/kg 105 80-120Potassium 18.0 U 18.0 50.0 mg/kg 99 78-110Sodium 37.3 U 37.3 100 mg/kg 97 87-110Strontium 0.0620 U 0.0620 0.500 mg/kg 99 86-110Tin 1.54 J 1.00 10.0 mg/kg 105 90-114Titanium 0.380 U 0.380 1.00 mg/kg 102 80-120Zirconium 0.840 U 0.840 5.00 mg/kg 102 80-120

Batch number: 111375711002 Sample number(s): 6288929-6288934,6288936-6288941Mercury 0.0028 U 0.0028 0.0974 mg/kg 102 88-123

Batch number: 111381848002 Sample number(s): 6288935Aluminum 0.0834 U 0.0834 0.200 mg/l 99 96 90-112 3 20Boron 0.0181 J 0.0138 0.0500 mg/l 98 96 89-110 2 20Calcium 0.0702 U 0.0702 0.200 mg/l 110 109 90-112 1 20Iron 0.0522 U 0.0522 0.200 mg/l 111 108 90-112 3 20Lithium 0.0024 U 0.0024 0.0200 mg/l 100 99 80-120 1 20Magnesium 0.0172 U 0.0172 0.100 mg/l 101 100 89-110 1 20Manganese 0.00084 U 0.00084 0.0050 mg/l 106 103 90-110 3 20Phosphorus 0.0089 U 0.0089 0.100 mg/l 104 102 80-120 2 20Potassium 0.239 U 0.239 0.500 mg/l 98 96 85-115 2 20Sodium 0.433 U 0.433 1.00 mg/l 98 97 87-114 1 20Strontium 0.00089 U 0.00089 0.0050 mg/l 104 102 90-110 2 20Tin 0.0098 U 0.0098 0.0200 mg/l 102 99 90-110 2 20Titanium 0.0038 U 0.0038 0.0100 mg/l 104 102 90-113 3 20Zirconium 0.0206 U 0.0206 0.0500 mg/l 103 102 80-120 1 20

Batch number: 111385713002 Sample number(s): 6288935Mercury 0.000046

U0.000046

0.00020 mg/l 103 103 80-120 1 20

Batch number: 111386050002A Sample number(s): 6288935Antimony 0.00030 U 0.00030 0.0010 mg/l 101 95 87-110 6 20Arsenic 0.00095 U 0.00095 0.0020 mg/l 102 105 86-111 3 20Beryllium 0.00013 U 0.00013 0.00050 mg/l 104 104 90-113 0 20Cadmium 0.00020 U 0.00020 0.00050 mg/l 101 107 90-114 6 20Chromium 0.00060 U 0.00060 0.0020 mg/l 102 107 90-118 5 20Cobalt 0.00010 U 0.00010 0.00050 mg/l 96 100 87-113 4 20Copper 0.00038 U 0.00038 0.0020 mg/l 97 101 90-113 5 20Lead 0.000052

U0.000052

0.0010 mg/l 101 102 90-115 1 20

Nickel 0.00050 U 0.00050 0.0020 mg/l 103 108 90-113 5 20Silver 0.000080

U0.000080

0.00050 mg/l 100 105 90-115 5 20

Thallium 0.00015 U 0.00015 0.00050 mg/l 97 107 89-116 10 20Vanadium 0.00016 U 0.00016 0.00050 mg/l 99 105 89-116 6 20Zinc 0.0040 U 0.0040 0.0150 mg/l 95 104 90-116 10 20

Batch number: 111386050002B Sample number(s): 6288935Selenium 0.00025 U 0.00025 0.0020 mg/l 104 107 85-114 3 20

Batch number: 111386050002C Sample number(s): 6288935Molybdenum 0.00025 U 0.00025 0.00050 mg/l 98 103 89-115 6 20

Batch number: 111386050002D Sample number(s): 6288935Barium 0.00053 U 0.00053 0.0020 mg/l 100 108 88-113 8 20

Page 11 of 24




Blank Blank Blank Report LCS LCSD LCS/LCSDAnalysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD MaxBatch number: 11137196401A Sample number(s): 62889353b Cr VI by EPA 7199 5.0 U 5.0 10.0 ug/l 102 103 90-110 1 20

Batch number: 11139196902B Sample number(s): 628893511b Anions by 300.0 - Fluoride 0.080 U 0.080 0.10 mg/l 96 96 90-110 0 20

Batch number: 11140243201A Sample number(s): 6288929-6288930,6288932-6288934,6288936-62889413a Cr VI by EPA 7199 0.20 U 0.20 1.0 mg/kg 91 80-120

Batch number: 11141621201A Sample number(s): 6288929-6288930,6288932-6288934,6288936-62889417a Perchlorate EPA 314.0 9.0 U 9.0 30.0 ug/kg 94 85-115

Batch number: 11141621202B Sample number(s): 6288929-6288930,6288932-6288934,6288936-628894111a Anions by 300.0 - Fluoride 0.80 U 0.80 1.0 mg/kg 90 90-11011a Anions by 300.0 - Nitrate 0.80 U 0.80 1.5 mg/kg 102 90-110

Batch number: 11144102201A Sample number(s): 6288934,6288938-628894117a Cyanide by 9012B 0.18 U 0.18 0.50 mg/kg 95 80-120

Batch number: 11154621701A Sample number(s): 62889357b Perchlorate EPA 314.0 0.70 U 0.70 2.0 ug/l 98 99 85-115 0 20

Batch number: 11137020001A Sample number(s): 628893518b pH by 9040B 100 100 90-110 0 3

Batch number: 11139039402A Sample number(s): 6288929,6288932-6288934,6288936-628893718a pH by 9045C 100 95-105

Batch number: 11139039402B Sample number(s): 6288938-628894118a pH by 9045C 100 95-105

Batch number: 11139182102A Sample number(s): 6288929,6288932-6288934,6288936-628893732a OR Potential 98 98-102

Batch number: 11139182102B Sample number(s): 6288938-628894132a OR Potential 98 98-102

Batch number: 11144162401A Sample number(s): 6288929-6288933,6288936-628893728a Moisture Content by 160.3 100 80-120Moisture Content by 160.3 100 80-120Moisture Content by 160.3 100 80-120

Batch number: 11158162401B Sample number(s): 6288938Moisture Content by 160.3 100 80-120

Batch number: 11160162401A Sample number(s): 6288934,6288939-6288941Moisture Content by 160.3 100 80-120

Sample Matrix Quality ControlUnspiked (UNSPK) = the sample used in conjunction with the matrix spikeBackground (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD

Page 12 of 24




Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: B111401AA Sample number(s): 6288929-6288931,6288933-6288934,6288936,6288938-6288941 UNSPK:6288929

Acetone 118 110 15-210 9 30Benzene 113 110 55-143 4 30Bromobenzene 109 108 43-139 2 30Bromochloromethane 132 126 60-137 7 30Bromodichloromethane 103 101 53-136 4 30Bromoform 97 97 38-124 2 30Bromomethane 68 65 42-168 8 302-Butanone 110 106 37-163 6 30n-Butylbenzene 103 102 30-146 3 30sec-Butylbenzene 115 114 33-157 3 30tert-Butylbenzene 108 107 41-152 3 30Carbon Tetrachloride 122 117 45-153 6 30Chlorobenzene 105 104 49-135 4 30Chloroethane 65 60 39-152 10 302-Chloroethyl Vinyl Ether 85 86 32-139 1 30Chloroform 110 107 61-142 5 30Chloromethane 79 79 51-163 2 302-Chlorotoluene 107 104 42-146 5 304-Chlorotoluene 102 100 39-145 4 30Chlorotrifluoroethene 81 81 70-130 23 301,2-Dibromo-3-chloropropane 79 82 30-139 2 30Dibromochloromethane 103 100 51-128 5 301,2-Dibromoethane 95 95 54-129 2 30Dibromomethane 96 96 57-130 3 301,2-Dichlorobenzene 98 98 36-133 2 301,3-Dichlorobenzene 104 103 34-134 3 301,4-Dichlorobenzene 100 101 35-136 2 30Dichlorodifluoromethane 79 79 26-151 2 301,1-Dichloroethane 114 111 63-142 5 301,2-Dichloroethane 101 100 68-131 3 301,1-Dichloroethene 92 86 61-149 9 30cis-1,2-Dichloroethene 107 106 60-136 4 30trans-1,2-Dichloroethene 112 108 59-142 6 301,2-Dichloropropane 109 107 62-135 4 301,3-Dichloropropane 97 97 58-129 3 302,2-Dichloropropane 106 102 53-147 7 301,1-Dichloropropene 116 112 54-145 6 30cis-1,3-Dichloropropene 98 98 51-131 2 30trans-1,3-Dichloropropene 89 90 49-129 1 30Ethylbenzene 104 103 44-141 4 30Freon 113 101 96 56-156 7 30Freon 133a 85 85 61-131 23 30Hexachlorobutadiene 109 112 10-155 0 302-Hexanone 98 97 32-160 3 30Isopropylbenzene 109 106 38-144 5 30p-Isopropyltoluene 110 109 29-152 3 30Methyl Tertiary Butyl Ether 88 87 55-129 3 304-Methyl-2-pentanone 83 86 46-139 1 30Methylene Chloride 82 79 61-141 5 30n-Propylbenzene 113 111 39-157 4 30Styrene 97 95 35-134 5 301,1,1,2-Tetrachloroethane 107 104 52-130 4 301,1,2,2-Tetrachloroethane 91 92 40-152 2 30Tetrachloroethene 126 122 42-149 6 30Toluene 109 106 50-146 5 301,2,3-Trichlorobenzene 84 89 10-140 4 30

Page 13 of 24





MS MSD MS/MSD RPD BKG DUP DUP Dup RPDAnalysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___1,2,4-Trichlorobenzene 80 85 10-136 5 301,1,1-Trichloroethane 113 110 64-142 5 301,1,2-Trichloroethane 98 97 54-139 3 30Trichloroethene 109 106 53-144 5 30Trichlorofluoromethane 89 85 47-163 7 301,2,3-Trichloropropane 95 96 45-154 1 301,2,4-Trimethylbenzene 105 103 37-149 4 301,3,5-Trimethylbenzene 108 107 38-150 4 30Vinyl Chloride 79 80 50-154 2 30m+p-Xylene 106 103 44-137 5 30o-Xylene 101 99 42-137 4 30

Batch number: E111381AA Sample number(s): 6288929-6288931,6288933-6288934,6288936,6288938-6288941 UNSPK:6288929

1,4-Dioxane 90 89 70-130 1 30

Batch number: 11139SLG026 Sample number(s): 6288929-6288931,6288933-6288934,6288936-6288939,6288941 UNSPK:6288929

Acenaphthene 93 92 63-105 2 30Acenaphthylene 90 86 67-114 4 30Anthracene 94 94 60-122 0 30Benzo(a)anthracene 100 103 59-128 3 30Benzo(a)pyrene 99 103 45-138 4 30Benzo(b)fluoranthene 111 111 43-155 1 30Benzo(g,h,i)perylene 110 113 33-141 3 30Benzo(k)fluoranthene 101 103 42-144 1 30Butylbenzylphthalate 112 115 57-173 3 30Di-n-butylphthalate 107 110 65-148 2 30Chrysene 99 104 48-134 6 30Dibenz(a,h)anthracene 111 113 22-133 2 30Diethylphthalate 101 96 70-136 5 30Dimethylphthalate 99 96 74-118 3 30Bis(2-Ethylhexyl)phthalate 132 136 39-167 3 30Fluoranthene 103 107 26-166 4 30Fluorene 99 96 66-122 3 30Indeno(1,2,3-cd)pyrene 110 112 21-143 2 301-Methylnaphthalene 98 92 72-123 6 302-Methylnaphthalene 87 82 64-103 6 30Naphthalene 97 85 61-102 12 30N-Nitrosodimethylamine 87 79 48-113 11 30Di-n-octylphthalate 124 123 40-192 0 30Phenanthrene 93 96 12-165 3 30Pyrene 97 99 15-153 2 30

Batch number: 11139SLH026 Sample number(s): 6288929-6288931,6288933-6288934,6288936-6288941 UNSPK: 6288929Acenaphthene 94 97 75-115 3 30Acenaphthylene 97 99 81-110 2 30Aniline 83 76 35-95 9 30Anthracene 95 97 75-115 2 30Benzidine 32* 22* 35-141 36* 30Benzo(a)anthracene 96 98 65-122 1 30Benzo(a)pyrene 92 96 57-126 4 30Benzo(b)fluoranthene 95 97 59-125 2 30

Page 14 of 24





MS MSD MS/MSD RPD BKG DUP DUP Dup RPDAnalysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___Benzo(g,h,i)perylene 83 90 59-127 8 30Benzo(k)fluoranthene 94 95 56-132 2 30Benzoic acid 62 52 10-173 18 30Benzyl alcohol 95 93 67-115 3 304-Bromophenyl-phenylether 93 98 67-129 6 30Butylbenzylphthalate 95 96 73-134 1 30Di-n-butylphthalate 90 91 67-123 0 30Carbazole 93 95 64-120 2 304-Chloro-3-methylphenol 94 91 76-110 3 304-Chloroaniline 73 67 23-95 8 30bis(2-Chloroethoxy)methane 95 93 75-104 3 30bis(2-Chloroethyl)ether 93 91 60-116 2 30bis(2-Chloroisopropyl)ether 90 85 55-142 5 302-Chloronaphthalene 89 90 50-141 2 302-Chlorophenol 96 94 73-121 2 304-Chlorophenyl-phenylether 93 98 80-109 5 30Chrysene 91 96 62-128 5 30Dibenz(a,h)anthracene 87 91 65-125 4 30Dibenzofuran 96 98 71-112 2 301,2-Dichlorobenzene 86 82 66-108 5 301,3-Dichlorobenzene 84 77 63-109 8 301,4-Dichlorobenzene 85 79 70-100 8 303,3'-Dichlorobenzidine 68 63 16-119 8 302,4-Dichlorophenol 98 97 78-117 0 30Diethylphthalate 91 92 66-118 1 302,4-Dimethylphenol 94 91 78-110 3 303,5-Dimethylphenol 103 102 70-130 1 30Dimethylphthalate 94 95 64-118 1 304,6-Dinitro-2-methylphenol 56 39 24-116 35* 302,4-Dinitrophenol 29 18* 20-143 48* 302,4-Dinitrotoluene 98 96 73-113 2 302,6-Dinitrotoluene 96 97 69-123 0 301,2-Diphenylhydrazine 98 100 71-129 2 30bis(2-Ethylhexyl)phthalate 90 91 63-122 1 30Fluoranthene 94 96 73-112 2 30Fluorene 93 95 77-111 2 30Hexachlorobenzene 95 94 77-114 2 30Hexachlorobutadiene 86 84 62-120 2 30Hexachlorocyclopentadiene 87 88 10-153 1 30Hexachloroethane 79 73 57-109 8 30Indeno(1,2,3-cd)pyrene 83 89 61-126 7 30Isophorone 94 92 73-102 2 301-Methylnaphthalene 93 91 73-112 3 302-Methylnaphthalene 87 87 76-114 0 302-Methylphenol 94 92 75-111 2 304-Methylphenol 100 97 71-111 3 30Naphthalene 89 88 72-116 2 302-Nitroaniline 98 99 67-125 1 303-Nitroaniline 93 94 59-122 1 304-Nitroaniline 81 78 52-112 4 30Nitrobenzene 93 91 72-106 3 302-Nitrophenol 93 93 74-115 0 304-Nitrophenol 83 83 54-113 0 30

Page 15 of 24





MS MSD MS/MSD RPD BKG DUP DUP Dup RPDAnalysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___N-Nitroso-di-n-propylamine 87 86 60-116 1 30N-Nitrosodimethylamine 95 88 47-116 8 30N-Nitrosodiphenylamine 97 97 86-145 0 30Di-n-octylphthalate 98 100 56-126 1 30Pentachlorophenol 69 60 28-127 15 30Phenanthrene 94 97 65-125 3 30Phenol 97 95 58-126 2 30Pyrene 103 105 74-126 2 301,2,4-Trichlorobenzene 92 89 72-115 4 302,4,5-Trichlorophenol 94 94 78-109 1 302,4,6-Trichlorophenol 96 98 77-115 2 30

Batch number: 11143SLE026 Sample number(s): 6288940 UNSPK: P293457Acenaphthene 92 92 63-105 0 30Acenaphthylene 91 99 67-114 8 30Anthracene 103 102 60-122 1 30Benzo(a)anthracene 108 103 59-128 5 30Benzo(a)pyrene 111 105 45-138 5 30Benzo(b)fluoranthene 117 112 43-155 4 30Benzo(g,h,i)perylene 60 55 33-141 9 30Benzo(k)fluoranthene 115 112 42-144 2 30Butylbenzylphthalate 106 947* 57-173 160* 30Di-n-butylphthalate 93 91 65-148 2 30Chrysene 101 95 48-134 5 30Dibenz(a,h)anthracene 76 71 22-133 6 30Diethylphthalate 95 94 70-136 2 30Dimethylphthalate 93 101 74-118 9 30Bis(2-Ethylhexyl)phthalate 127 101 39-167 19 30Fluoranthene 125 122 26-166 2 30Fluorene 95 99 66-122 4 30Indeno(1,2,3-cd)pyrene 74 68 21-143 8 301-Methylnaphthalene 93 95 72-123 3 302-Methylnaphthalene 84 86 64-103 2 30Naphthalene 90 86 61-102 4 30N-Nitrosodimethylamine 94 88 48-113 6 30Di-n-octylphthalate 104 119 40-192 11 30Phenanthrene 96 94 12-165 2 30Pyrene 89 85 15-153 5 30

Batch number: 11146SLE026 Sample number(s): 6288934,6288938-6288941 UNSPK: P296047N-Nitrosodimethylamine 24* 24* 70-130 1 30

Batch number: 111430006A Sample number(s): 6288938 UNSPK: P2919994-Amino-2,6-Dinitrotoluene 95 104 80-127 10 502-Amino-4,6-Dinitrotoluene 97 106 80-137 11 501,3-Dinitrobenzene 104 111 38-166 9 502,4-Dinitrotoluene 93 102 80-131 11 502,6-Dinitrotoluene 93 99 80-127 9 50HMX 83 91 63-128 12 50Nitrobenzene 115 125 80-125 10 50Nitroglycerin 92 99 80-120 10 502-Nitrotoluene 94 101 80-122 9 503-Nitrotoluene 97 104 72-119 9 50

Page 16 of 24





MS MSD MS/MSD RPD BKG DUP DUP Dup RPDAnalysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___4-Nitrotoluene 93 100 80-125 9 50PETN 109 118 80-121 10 50RDX 80 90 75-129 13 50Tetryl 60 69 55-174 15 501,3,5-Trinitrobenzene 90 101 82-126 13 502,4,6-Trinitrotoluene 91 100 82-130 11 50

Batch number: 111450004A Sample number(s): 6288934,6288939-6288941 UNSPK: P2907544-Amino-2,6-Dinitrotoluene 109 109 80-127 0 502-Amino-4,6-Dinitrotoluene 113 113 80-137 0 501,3-Dinitrobenzene 117 117 38-166 0 502,4-Dinitrotoluene 107 107 80-131 0 502,6-Dinitrotoluene 106 106 80-127 0 50HMX 99 99 63-128 0 50Nitrobenzene 128* 128* 80-125 0 50Nitroglycerin 106 106 80-120 0 502-Nitrotoluene 105 105 80-122 1 503-Nitrotoluene 107 107 72-119 0 504-Nitrotoluene 104 104 80-125 0 50PETN 126* 125* 80-121 1 50RDX 96 97 75-129 1 50Tetryl 74 73 55-174 0 501,3,5-Trinitrobenzene 107 106 82-126 0 502,4,6-Trinitrotoluene 108 107 82-130 0 50

Batch number: 111400002A Sample number(s): 6288934,6288938-6288941 UNSPK: P29199925a Formaldehyde 8315A 90 89 80-120 1 50

Batch number: 111390003A Sample number(s): 6288938 UNSPK: P2850366a Perchlorate EPA 6850 100 102 80-120 2 20

Batch number: 111380023A Sample number(s): 6288929-6288931,6288933-6288934,6288936-6288941 UNSPK: 6288929PCB-1016 96 98 29-146 2 50PCB-1260 113 114 39-149 0 50

Batch number: 111380034A Sample number(s): 6288934,6288938-6288941 UNSPK: P281100EFH (C12-C14) 70 73 49-123 3 20EFH (C15-C20) 86 90 49-123 3 20EFH (C21-C30) 101 104 49-123 2 20EFH (C30 - C40) 64 71 49-123 7 20EFH (C8-C11) 70 67 49-123 5 20

Batch number: 111370018A Sample number(s): 6288934,6288938-6288941 UNSPK: 6288934Diethylene glycol 40* 44* 59-109 9 20Ethylene glycol 71 80 63-107 12 20Propylene glycol 78 87 63-107 11 20

Batch number: 111390030A Sample number(s): 6288934,6288938-6288941 UNSPK: P291999Ethanol 42* 33* 48-130 24* 20Isopropanol 66 64 12-149 3 20Methanol 55 52 43-138 5 20

Batch number: 111390019A Sample number(s): 6288934,6288939-6288941 UNSPK: 6288934

Page 17 of 24





MS MSD MS/MSD RPD BKG DUP DUP Dup RPDAnalysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___m-Terphenyl 0* 0* 75-125 0 20o-Terphenyl 96 100 75-125 4 20p-Terphenyl 0* 92 75-125 200* 20

Batch number: 111460029A Sample number(s): 6288938 UNSPK: P294833m-Terphenyl 84 84 75-125 1 20o-Terphenyl 99 100 75-125 1 20p-Terphenyl 95 97 75-125 2 20

Batch number: 111371026001A Sample number(s): 6288929-6288934,6288936-6288941 UNSPK: 6288929 BKG: 6288929Antimony 64* 68* 75-125 7 20 0.274 0.210 27* (1) 20Arsenic 208 (2) 216 (2) 75-125 2 20 7.95 7.53 5 20Beryllium 129* 141* 75-125 6 20 0.974 0.865 12 20Cadmium 119 124 75-125 7 20 0.0810 J 0.0385 U 200* (1) 20Chromium 170* 145* 75-125 5 20 24.9 22.5 10 20Cobalt 127* 118 75-125 4 20 8.09 5.56 37* 20Copper 122 117 75-125 1 20 9.75 6.87 35* 20Lead 171* 174* 75-125 2 20 7.52 6.82 10 20Nickel 148* 142* 75-125 0 20 16.6 13.6 20 20Silver 124 119 75-125 1 20 0.731 0.163 127* (1) 20Thallium 118 125 75-125 6 20 0.259 0.208 22* (1) 20Vanadium 220 (2) 210 (2) 75-125 1 20 48.3 44.2 9 20Zinc 42 (2) 34 (2) 75-125 1 20 46.0 37.9 19 20

Batch number: 111371026001B Sample number(s): 6288929-6288934,6288936-6288941 UNSPK: 6288929 BKG: 6288929Selenium 117 113 75-125 1 20 0.217 J 0.203 J 7 (1) 20

Batch number: 111371026001C Sample number(s): 6288929-6288934,6288936-6288941 UNSPK: 6288929 BKG: 6288929Molybdenum 137* 130* 75-125 2 20 1.32 1.50 13 20

Batch number: 111371026001D Sample number(s): 6288929-6288934,6288936-6288941 UNSPK: 6288929 BKG: 6288929Barium 248 (2) 282 (2) 75-125 3 20 105 85.3 21* 20

Batch number: 111375708002 Sample number(s): 6288929-6288934,6288936-6288941 UNSPK: 6288929 BKG: 6288929Aluminum 3976

(2)3125(2)

75-125 4 20 29,600 31,000 4 20

Boron 95 96 84-115 4 20 7.21 7.60 5 (1) 20Calcium 104 (2) 115 (2) 75-125 2 20 2,680 2,590 4 20Iron 2168

(2)1389(2)

75-125 3 20 24,700 24,500 1 20

Lithium 104 102 82-114 1 20 28.2 27.6 2 20Magnesium 243 (2) 209 (2) 75-125 1 20 5,030 4,790 5 20Manganese 147 (2) 144 (2) 75-125 0 20 221 172 25* 20Phosphorus 96 87 75-125 2 20 283 255 10 20Potassium 109 101 75-125 2 20 1,590 1,250 24* 20Sodium 100 100 75-125 2 20 98.7 95.6 J 3 (1) 20Strontium 102 101 75-115 1 20 20.1 19.9 1 20Tin 86 88 80-110 5 20 2.98 J 2.88 J 4 (1) 20Titanium 249 (2) 243 (2) 75-125 0 20 1,270 1,200 6 20Zirconium 94 94 75-125 3 20 4.60 J 4.94 7 (1) 20

Batch number: 111375711002 Sample number(s): 6288929-6288934,6288936-6288941 UNSPK: 6288929 BKG: 6288929Mercury 96 103 65-135 11 20 0.0028 U 0.0044 J 200* (1) 20

Page 18 of 24





MS MSD MS/MSD RPD BKG DUP DUP Dup RPDAnalysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: 11140243201A Sample number(s): 6288929-6288930,6288932-6288934,6288936-6288941 UNSPK: 6288929BKG: 6288929

3a Cr VI by EPA 7199 91 75-125 0.51 J 0.57 J 10 (1) 20

Batch number: 11141621201A Sample number(s): 6288929-6288930,6288932-6288934,6288936-6288941 UNSPK: 6288929BKG: 6288929

7a Perchlorate EPA 314.0 89 80-120 9.0 U 9.0 U 0 (1) 15

Batch number: 11141621202B Sample number(s): 6288929-6288930,6288932-6288934,6288936-6288941 UNSPK: 6288929BKG: 6288929

11a Anions by 300.0 - Fluoride 34* 80-120 0.80 U 0.80 U 0 (1) 2011a Anions by 300.0 - Nitrate 112 80-120 2.3 2.3 2 (1) 20

Batch number: 11144102201A Sample number(s): 6288934,6288938-6288941 UNSPK: P286418 BKG: P28641817a Cyanide by 9012B 98 75-125 0.18 U 0.17 U 0 (1) 20

Batch number: 11139039402A Sample number(s): 6288929,6288932-6288934,6288936-6288937 BKG: 628892918a pH by 9045C 6.53 6.48 1 3

Batch number: 11139039402B Sample number(s): 6288938-6288941 BKG: 628894118a pH by 9045C 7.97 8.08 1 3

Batch number: 11139182102A Sample number(s): 6288929,6288932-6288934,6288936-6288937 BKG: 628892932a OR Potential 389 400 3 6

Batch number: 11139182102B Sample number(s): 6288938-6288941 BKG: 628894132a OR Potential 369 372 1 6

Batch number: 11144162401A Sample number(s): 6288929-6288933,6288936-6288937 BKG: 628892928a Moisture Content by 160.3 12.2 12.0 1 20Moisture Content by 160.3 12.2 12.0 1 20Moisture Content by 160.3 12.2 12.0 1 20

Batch number: 11158162401B Sample number(s): 6288938 BKG: P300341Moisture Content by 160.3 15.9 15.4 3 20

Batch number: 11160162401A Sample number(s): 6288934,6288939-6288941 BKG: 6288941Moisture Content by 160.3 11.8 12.4 4 20

Surrogate Quality ControlSurrogate recoveries which are outside of the QC window are confirmedunless attributed to dilution or otherwise noted on the Analysis Report.

Analysis Name: 1a Volatile Organics EPA 8260BBatch number: B111401AA

Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene________________________________________________________________________________________________________________6288929 105 107 102 94

Page 19 of 24




Surrogate Quality Control6288930 102 104 105 966288931 102 103 104 966288933 104 108 98 926288934 104 103 100 946288936 105 109 98 926288938 105 103 103 866288939 105 105 103 906288940 103 102 102 876288941 104 103 101 90Blank 103 103 100 91LCS 104 109 103 98MS 102 104 105 96MSD 102 103 104 96________________________________________________________________________________________________________________Limits: 80-120 80-120 81-117 74-121

Analysis Name: 14b 1,4-Dioxane by 8260B SIMBatch number: E111371AA

Toluene-d8________________________________________________________________________________________________________________6288935 1006288942 100Blank 100LCS 100LCSD 100________________________________________________________________________________________________________________Limits: 80-120

Analysis Name: 14a 1,4-Dioxane by 8260B SIMBatch number: E111381AA

Toluene-d8________________________________________________________________________________________________________________6288929 986288930 996288931 986288933 996288934 996288936 986288938 986288939 986288940 986288941 98Blank 99LCS 99LCSD 99MS 99MSD 98________________________________________________________________________________________________________________Limits: 70-130

Analysis Name: 1b Volatile Organics EPA8260Batch number: L111372AA

Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene________________________________________________________________________________________________________________6288935 100 102 101 986288942 100 100 99 98Blank 99 101 101 99

Page 20 of 24




Surrogate Quality ControlLCS 102 99 102 101LCSD 103 100 102 101________________________________________________________________________________________________________________Limits: 86-118 80-120 88-110 86-115

Analysis Name: 5b Semivolatiles by EPA 8270CBatch number: 11138WAD026

2-Fluorophenol Phenol-d6 2,4,6-Tribromophenol Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-d14________________________________________________________________________________________________________________6288935 55 33 107 85 84 74Blank 54 32 105 86 86 73LCS 47 29 99 81 81 73LCSD 56 36 103 83 84 76________________________________________________________________________________________________________________Limits: 20-130 20-120 30-130 40-130 45-130 45-135

Analysis Name: 4b Select SVOC EPA 8270SIMBatch number: 11138WAG026

Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-d14________________________________________________________________________________________________________________6288935 96 101 110Blank 106 114 122LCS 109 104 109LCSD 105 101 105________________________________________________________________________________________________________________Limits: 40-130 45-130 45-135

Analysis Name: 4a Select SVOC EPA 8270SIMBatch number: 11139SLG026

Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-d14________________________________________________________________________________________________________________6288929 106 99 1036288930 110 95 1006288931 103 95 1066288933 105 98 1036288934 104 98 1016288936 102 98 1076288937 95 92 1006288938 111 100 1066288939 105 96 976288941 107 98 95Blank 101 103 106LCS 121 104 105MS 110 95 100MSD 103 95 106________________________________________________________________________________________________________________Limits: 40-130 45-130 45-135

Analysis Name: 5a Semivolatiles by EPA 8270CBatch number: 11139SLH026

Phenol-d6 2-Fluorophenol 2,4,6-Tribromophenol Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-d14________________________________________________________________________________________________________________6288929 75 77 73 75 77 766288930 96 96 88 89 91 896288931 96 96 91 88 93 946288933 86 89 80 83 83 856288934 89 92 80 84 86 86

Page 21 of 24




Surrogate Quality Control6288936 90 91 77 84 87 906288937 89 90 79 83 84 906288938 88 90 76 83 83 856288939 88 88 75 79 84 906288940 88 89 71 81 82 886288941 90 88 67 81 85 89Blank 86 91 81 84 87 80LCS 95 95 84 89 90 89MS 96 96 88 89 91 89MSD 96 96 91 88 93 94________________________________________________________________________________________________________________Limits: 25-120 25-130 35-130 40-130 45-130 45-135

Analysis Name: 4a Select SVOC EPA 8270SIMBatch number: 11143SLE026

Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-d14________________________________________________________________________________________________________________6288940 106 93 88Blank 121 106 112LCS 104 96 98MS 107 90 95MSD 102 95 91________________________________________________________________________________________________________________Limits: 40-130 45-130 45-135

Analysis Name: 15a NDMA by 1625CBatch number: 11146SLE026

N-Nitrosodimethylamine-d6

________________________________________________________________________________________________________________6288934 796288938 1046288939 936288940 936288941 86Blank 91LCS 104MS 164*MSD 143________________________________________________________________________________________________________________Limits: 50-150

Analysis Name: 9a TPH by EPA 8015B Gas C5-C12Batch number: 11139A34A

Trifluorotoluene-F________________________________________________________________________________________________________________6288934 806288938 766288939 776288940 686288941 72Blank 81LCS 88LCSD 86________________________________________________________________________________________________________________Limits: 61-122

Page 22 of 24




Surrogate Quality ControlAnalysis Name: 9b TPH by EPA 8015B Gas C5-C12Batch number: 11143A20A

Trifluorotoluene-F________________________________________________________________________________________________________________6288942 72Blank 72LCS 119LCSD 113________________________________________________________________________________________________________________Limits: 63-135

Analysis Name: 8b PCBs/PCTs by 8082Batch number: 111380016A

Tetrachloro-m-xylene Decachlorobiphenyl________________________________________________________________________________________________________________6288935 121 96Blank 118 64LCS 89 57LCSD 113 81________________________________________________________________________________________________________________Limits: 30-150 45-120

Analysis Name: 8a PCBs/PCTs by 8082Batch number: 111380023A

Tetrachloro-m-xylene Decachlorobiphenyl________________________________________________________________________________________________________________6288929 99 976288930 99 1076288931 103 1056288933 130 128*6288934 132 1136288936 119 1186288937 113 1116288938 104 1136288939 108 1036288940 117 1126288941 98 96Blank 118 118LCS 120 115LCSD 112 117MS 99 107MSD 103 105________________________________________________________________________________________________________________Limits: 53-139 45-120

Analysis Name: 25a Formaldehyde 8315ABatch number: 111400002A

Butyraldehyde________________________________________________________________________________________________________________6288934 1266288938 1226288939 1256288940 129*6288941 126Blank 125LCS 119MS 112

Page 23 of 24




Surrogate Quality ControlMSD 116________________________________________________________________________________________________________________Limits: 64-126

Analysis Name: 16a Energetics by 8330ABatch number: 111430006A

2-Nitro-m-xylene________________________________________________________________________________________________________________6288938 122Blank 114LCS 121LCSD 114MS 101MSD 99________________________________________________________________________________________________________________Limits: 80-146

Analysis Name: 16a Energetics by 8330ABatch number: 111450004A

2-Nitro-m-xylene________________________________________________________________________________________________________________6288934 1276288939 1236288940 1216288941 131Blank 136LCS 123LCSD 32*MS 115MSD 116________________________________________________________________________________________________________________Limits: 80-146

Analysis Name: 21a Glycols by 8015BBatch number: 111370018A

Tetramethylene glycol________________________________________________________________________________________________________________6288934 886288938 896288939 906288940 886288941 89Blank 90LCS 99MS 91MSD 93________________________________________________________________________________________________________________Limits: 29-137

Analysis Name: 9a TPH by EPA 8015B Oil/DieselBatch number: 111380034A

Chlorobenzene Orthoterphenyl________________________________________________________________________________________________________________6288934 69 796288938 67 756288939 59 646288940 70 76

Page 24 of 24




Surrogate Quality Control6288941 67 77Blank 73 78LCS 81 83MS 66 75MSD 67 76________________________________________________________________________________________________________________Limits: 37-125 47-145

Analysis Name: 20a Terphenyls by 8015BBatch number: 111390019A

n-Triacontane-d62________________________________________________________________________________________________________________6288934 926288939 866288940 906288941 85Blank 90LCS 90MS 84MSD 93________________________________________________________________________________________________________________Limits: 50-150

Analysis Name: 19a Alcohols by 8015BBatch number: 111390030A

Acetone________________________________________________________________________________________________________________6288934 746288938 696288939 736288940 696288941 71Blank 84LCS 83MS 77MSD 77________________________________________________________________________________________________________________Limits: 42-138

Analysis Name: 20a Terphenyls by 8015BBatch number: 111460029A

n-Triacontane-d62________________________________________________________________________________________________________________6288938 91Blank 88LCS 86MS 92MSD 98________________________________________________________________________________________________________________Limits: 50-150

Explanation of Symbols and AbbreviationsThe following defines common symbols and abbreviations used in reporting technical data:

RL Reporting Limit BMQL Below Minimum Quantitation LevelN.D. none detected MPN Most Probable Number

TNTC Too Numerous To Count CP Units cobalt-chloroplatinate unitsIU International Units NTU nephelometric turbidity units

umhos/cm micromhos/cm ng nanogram(s)C degrees Celsius F degrees Fahrenheit

meq milliequivalents lb. pound(s)g gram(s) kg kilogram(s)

ug microgram(s) mg milligram(s)ml milliliter(s) l liter(s)

m3 cubic meter(s) ul microliter(s)

< less than - The number following the sign is the limit of quantitation, the smallest amount of analyte which can bereliably determined using this specific test.

> greater than

J estimated value – The result is ≥ the Method Detection Limit (MDL) and < the Limit of Quantitation (LOQ).

ppm parts per million - One ppm is equivalent to one milligram per kilogram (mg/kg), or one gram per million grams. Foraqueous liquids, ppm is usually taken to be equivalent to milligrams per liter (mg/l), because one liter of water has aweight very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter of gas per liter of gas.

ppb parts per billion

Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weightbasis concentration to approximate the value present in a similar sample without moisture. All other results are reported

on an as-received basis.

U.S. EPA CLP Data Qualifiers: Organic Qualifiers Inorganic Qualifiers

A TIC is a possible aldol-condensation product B Value is <CRDL, but ≥IDLB Analyte was also detected in the blank E Estimated due to interferenceC Pesticide result confirmed by GC/MS M Duplicate injection precision not metD Compound quantitated on a diluted sample N Spike sample not within control limitsE Concentration exceeds the calibration range of S Method of standard additions (MSA) used

the instrument for calculationN Presumptive evidence of a compound (TICs only) U Compound was not detectedP Concentration difference between primary and W Post digestion spike out of control limits

confirmation columns >25% * Duplicate analysis not within control limitsU Compound was not detected + Correlation coefficient for MSA <0.995

X,Y,Z Defined in case narrative

Analytical test results meet all requirements of NELAC unless otherwise noted under the individual analysis.

Measurement uncertainty values, as applicable, are available upon request.

Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiologicalanalysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, thetest results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contactus. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of ourstaff. This report shall not be reproduced except in full, without the written approval of the laboratory.

WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted.THE FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED ORIMPLIED. WE DISCLAIM ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FORPARTICULAR PURPOSE AND WARRANTY OF MERCHANTABILITY. IN NO EVENT SHALL LANCASTER LABORATORIES BE LIABLEFOR INDIRECT, SPECIAL, CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSSOF PROFIT OR GOODWILL REGARDLESS OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF LANCASTERLABORATORIES AND (B) WHETHER LANCASTER LABORATORIES HAS BEEN INFORMED OF THE POSSIBILITY OF SUCHDAMAGES. We accept no legal responsibility for the purposes for which the client uses the test results. No purchase order or other order forwork shall be accepted by Lancaster Laboratories which includes any conditions that vary from the Standard Terms and Conditions, andLancaster hereby objects to any conflicting terms contained in any acceptance or order submitted by client.

Documents

· ANALYTICAL RESULTS Prepared by: Lancaster Laboratories 2425 New Holland Pike Lancaster, PA 17605-2425 Prepared for: CDM Federal Programs Corp. 14420 Albemarle Point Place Suite