88
Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8 8 1.9 69 2.1 9 2.6 71 0.21 Outlier 12 2.0 72 1.9 13 2.0 73 1.8 14 2.2 75 2.0 16 2.0 77 1.8 17 2.1 79 2.1 18 1.9 81 1.8 21 2.0 82 2.1 22 2.0 83 2.0 24 2.1 86 2.1 25 2.0 87 4.9 Outlier 26 2.0 89 1.8 27 2.2 90 2.4 28 2.1 92 2.0 29 2.2 94 1.8 30 1.7 95 42 Outlier 31 1.9 97 1.5 32 2.0 101 2.0 33 2.0 103 1.9 35 2.1 105 2.0 36 34 Outlier 106 1.9 38 2.3 107 1.9 39 2.0 111 2.0 40 1.9 112 2.1 41 2.1 115 2.0 42 2.0 117 2.0 44 2.1 45 2.0 46 1.9 Consensus median, pg/g 2.0 47 1.9 Median all values pg/g 2.0 48 2.0 Consensus mean, pg/g 2.0 49 8.0 Outlier Standard deviation, pg/g 0.16 50 2.0 Relative standard deviation, % 8.1 53 2.2 No. of values reported 78 54 2.0 No. of values removed 6 55 2.0 No. of reported non-detects 0 57 1.7 58 1.9 Analyte solution Congener: 2,3,7,8 TCDD Consenus statistics

 · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

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Page 1:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 20 Outlier 59 2.12 1.9 61 2.13 2.0 62 2.14 2.0 65 1.95 2.0 66 2.16 2.4 68 1.88 1.9 69 2.19 2.6 71 0.21 Outlier12 2.0 72 1.913 2.0 73 1.814 2.2 75 2.016 2.0 77 1.817 2.1 79 2.118 1.9 81 1.821 2.0 82 2.122 2.0 83 2.024 2.1 86 2.125 2.0 87 4.9 Outlier26 2.0 89 1.827 2.2 90 2.428 2.1 92 2.029 2.2 94 1.830 1.7 95 42 Outlier31 1.9 97 1.532 2.0 101 2.033 2.0 103 1.935 2.1 105 2.036 34 Outlier 106 1.938 2.3 107 1.939 2.0 111 2.040 1.9 112 2.141 2.1 115 2.042 2.0 117 2.044 2.145 2.046 1.9 Consensus median, pg/g 2.047 1.9 Median all values pg/g 2.048 2.0 Consensus mean, pg/g 2.049 8.0 Outlier Standard deviation, pg/g 0.1650 2.0 Relative standard deviation, % 8.153 2.2 No. of values reported 7854 2.0 No. of values removed 655 2.0 No. of reported non-detects 057 1.758 1.9

Analyte solutionCongener: 2,3,7,8 TCDD

Consenus statistics

Page 2:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.488

0.012

0.512

1.012

1.512

2.012

2.512

3.0121 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

2,3,7,8 TCDD

-5-4-3-2-1012345

71 97 30 57 94 68 81 77 73 89 65 103 40 8 2 46 106

107 31 18 72 58 47 111 13 50 39 92 16 12 5 55 42 22 45 105

117 25 115 54 101 32 4 33 75 48 21 26 83 3 17 61 112 41 79 35 82 24 44 59 62 69 86 28 66 27 53 14 29 38 90 6 9 87 49 1 36 95

Labcode

Z-score: 2,3,7,8 TCDD

Page 3:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 53 Outlier 59 5.12 4.9 61 5.23 5.0 62 5.14 4.5 65 2.0 Outlier5 4.9 66 5.36 5.6 68 5.08 4.7 69 5.19 6.7 71 1.1 Outlier12 5.2 72 4.913 4.7 73 4.814 5.2 75 5.016 5.0 77 4.717 4.9 79 4.918 5.2 81 4.521 4.8 82 5.022 5.0 83 4.924 5.1 86 5.025 4.9 87 4.926 4.5 89 4.827 5.0 90 6.128 4.8 92 4.429 4.5 94 4.530 4.1 95 108 Outlier31 4.8 97 4.532 5.0 101 4.933 5.1 103 4.735 5.4 105 4.936 86 Outlier 106 4.638 5.0 107 4.639 4.9 111 5.140 4.7 112 5.041 5.3 115 5.042 5.0 117 5.044 4.945 4.746 4.3 Consensus median, pg/g 4.947 4.9 Median all values pg/g 4.948 4.8 Consensus mean, pg/g 4.949 23 Outlier Standard deviation, pg/g 0.3950 4.7 Relative standard deviation, % 8.053 5.5 No. of values reported 7854 4.7 No. of values removed 655 5.0 No. of reported non-detects 057 3.858 4.9

Analyte solutionCongener: 1,2,3,7,8 PeCDD

Consenus statistics

Page 4:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.621

0.379

1.379

2.379

3.379

4.379

5.379

6.379

7.3791 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,7,8 PeCDD

-5-4-3-2-1012345

71 65 57 30 46 92 26 97 4 81 29 94 107

106 54 103 40 45 13 8 50 77 21 73 28 48 31 89 25 105 17 101 47 2 44 58 72 5 79 39 83 87 86 27 32 112 16 82 38 68 117 22 115 55 3 42 75 24 33 111 62 59 69 12 14 61 18 41 66 35 53 6 90 9 49 1 36 95

Labcode

Z-score: 1,2,3,7,8 PeCDD

Page 5:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 42 Outlier 59 5.12 5.0 61 4.93 5.0 62 5.14 4.6 65 5.35 4.7 66 4.76 5.1 68 4.68 4.8 69 5.29 5.5 71 1.0 Outlier12 5.4 72 5.013 4.7 73 4.814 5.2 75 5.416 5.0 77 5.017 5.1 79 5.018 5.1 81 4.621 4.8 82 4.822 4.6 83 4.924 5.2 86 5.025 4.8 87 4.926 4.7 89 4.627 5.7 90 5.028 4.8 92 4.529 4.7 94 4.630 4.1 95 102 Outlier31 4.8 97 4.932 4.9 101 4.833 5.3 103 4.635 5.2 105 5.036 82 Outlier 106 4.638 5.0 107 5.039 4.8 111 5.040 4.5 112 5.741 5.0 115 5.042 5.2 117 4.744 5.045 4.146 4.1 Consensus median, pg/g 4.947 5.2 Median all values pg/g 4.948 4.7 Consensus mean, pg/g 4.949 23 Outlier Standard deviation, pg/g 0.3450 4.4 Relative standard deviation, % 6.953 5.4 No. of values reported 7854 4.9 No. of values removed 555 5.0 No. of reported non-detects 057 3.958 4.9

Analyte solutionCongener: 1,2,3,4,7,8 HxCDD

Consenus statistics

Page 6:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.597

0.403

1.403

2.403

3.403

4.403

5.403

6.403

7.4031 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,4,7,8 HxCDD

-5-4-3-2-1012345

71 57 46 30 45 50 40 92 106 89 4 81 103 68 94 22 26 29 13 5

117 48 66 25 39 21 73 8

101 28 82 31 58 54 83 87 32 97 61 86 105 2

111 72 79 115 38 44 90 3 16 107 55 41 77 18 62 59 6 17 14 42 47 69 24 35 65 33 75 12 53 9

112 27 49 1 36 95

Labcode

Z-score: 1,2,3,4,7,8 HxCDD

Page 7:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 47 Outlier 59 5.32 5.0 61 5.03 5.0 62 5.14 4.5 65 4.95 4.5 66 4.76 5.1 68 4.38 4.4 69 5.19 5.5 71 1.2 Outlier12 5.1 72 5.013 4.3 73 4.014 5.0 75 5.116 5.0 77 5.117 4.5 79 4.618 5.3 81 4.721 4.8 82 5.422 4.6 83 4.924 5.0 86 4.925 5.0 87 5.026 5.2 89 4.527 5.8 90 5.028 4.7 92 4.229 4.6 94 4.130 4.0 95 95 Outlier31 5.0 97 5.332 5.2 101 4.833 5.0 103 3.835 4.9 105 4.936 76 Outlier 106 4.638 4.9 107 4.339 5.0 111 4.940 4.9 112 5.041 4.7 115 5.042 5.0 117 4.844 4.545 4.246 4.7 Consensus median, pg/g 4.947 5.0 Median all values pg/g 4.948 4.6 Consensus mean, pg/g 4.849 20 Outlier Standard deviation, pg/g 0.4050 5.3 Relative standard deviation, % 8.353 5.8 No. of values reported 7854 4.6 No. of values removed 555 5.0 No. of reported non-detects 057 3.758 4.8

Analyte solutionCongener: 1,2,3,6,7,8 HxCDD

Consenus statistics

Page 8:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.620

0.380

1.380

2.380

3.380

4.380

5.380

6.380

7.3801 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,6,7,8 HxCDD

-5-4-3-2-1012345

71 57 103 30 73 94 45 92 68 13 107 8 89 5 17 44 4 22 106 29 79 54 48 66 81 28 41 46 101 58 117 21 86 83 111 38 65 35 40 105 2 33 72 115 16 55 25 31 47 61 87 24 112 3 90 39 14 42 69 12 77 62 75 6 26 32 97 59 18 50 82 9 53 27 49 1 36 95

Labcode

Z-score: 1,2,3,6,7,8 HxCDD

Page 9:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 50 Outlier 59 5.12 5.1 61 4.93 5.1 62 5.14 4.8 65 4.85 4.8 66 5.56 5.9 68 5.68 5.2 69 5.19 5.7 71 1.1 Outlier12 5.5 72 5.113 4.7 73 4.314 5.3 75 5.416 5.0 77 5.617 5.0 79 4.818 5.2 81 5.121 4.9 82 4.722 5.0 83 5.024 5.1 86 5.125 4.8 87 4.826 4.9 89 4.527 6.4 90 5.428 4.8 92 4.929 5.0 94 4.230 4.6 95 104 Outlier31 5.0 97 5.632 5.3 101 4.833 5.5 103 4.135 5.6 105 5.136 89 Outlier 106 5.138 5.0 107 5.139 5.2 111 5.040 4.9 112 5.341 5.4 115 5.042 5.1 117 5.144 5.145 5.046 5.0 Consensus median, pg/g 5.147 6.4 Median all values pg/g 5.148 5.2 Consensus mean, pg/g 5.149 24 Outlier Standard deviation, pg/g 0.4050 4.7 Relative standard deviation, % 7.953 5.8 No. of values reported 7854 4.9 No. of values removed 555 5.1 No. of reported non-detects 057 4.458 5.2

Analyte solutionCongener: 1,2,3,7,8,9 HxCDD

Consenus statistics

Page 10:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.398

0.602

1.602

2.602

3.602

4.602

5.602

6.602

7.6021 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,7,8,9 HxCDD

-5-4-3-2-1012345

71 103 94 73 57 89 30 13 82 50 79 4 65 28 5 25 87 101 26 21 40 61 92 54 46 16 17 31 29 38 115 83 22 111 45 81 86 55 3

106 2 62 59 24 44 72 107

117 42 105 69 18 39 48 58 8 14 112 32 41 75 90 12 33 66 77 97 35 68 9 53 6 27 47 49 1 36 95

Labcode

Z-score: 1,2,3,7,8,9 HxCDD

Page 11:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 48 Outlier 59 5.22 4.9 61 5.13 5.0 62 5.34 4.8 65 5.05 4.8 66 5.16 5.0 68 4.58 5.0 69 5.09 7.3 71 1.1 Outlier12 5.5 72 5.013 4.9 73 4.614 5.1 75 5.316 5.0 77 4.917 4.9 79 5.018 5.3 81 4.821 4.9 82 5.822 5.0 83 5.024 5.1 86 5.025 4.8 87 5.226 4.9 89 4.427 5.3 90 6.428 4.7 92 4.829 4.7 94 5.730 4.6 95 97 Outlier31 5.0 97 5.432 5.1 101 5.133 4.7 103 4.935 5.8 105 4.836 88 Outlier 106 4.738 5.4 107 4.639 4.9 111 5.140 5.1 112 4.741 5.3 115 5.142 4.8 117 5.044 4.845 4.046 4.3 Consensus median, pg/g 5.047 5.2 Median all values pg/g 5.048 5.0 Consensus mean, pg/g 5.049 22 Outlier Standard deviation, pg/g 0.4650 4.4 Relative standard deviation, % 9.253 5.4 No. of values reported 7854 5.2 No. of values removed 555 5.0 No. of reported non-detects 057 4.158 5.0

Analyte solutionCongener: 1,2,3,4,6,7,8 HpCDD

Consenus statistics

Page 12:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.503

0.497

1.497

2.497

3.497

4.497

5.497

6.497

7.4971 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,4,6,7,8 HpCDD

-5-4-3-2-1012345

71 45 57 46 89 50 68 30 73 107 33 28 29 106

112 25 5 92 4 42 44 81 105 17 77 26 103 21 39 2 13 65 72 8 3 55 31 48 16 117 69 83 22 79 6 58 86 40 111 32 101 24 61 115 66 14 54 59 47 87 75 62 18 41 27 53 38 97 12 94 35 82 90 9 49 1 36 95

Labcode

Z-score: 1,2,3,4,6,7,8 HpCDD

Page 13:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 94 Outlier 59 112 10 61 9.93 10 62 104 9.6 65 9.95 9.5 66 9.56 11 68 9.18 9.6 69 109 14 71 2.2 Outlier12 11 72 1013 9.8 73 8.514 10 75 1016 9.8 77 9.817 9.7 79 1118 9.5 81 9.821 9.8 82 1222 9.6 83 9.924 10 86 9.225 9.8 87 1026 9.5 89 9.427 11 90 1228 9.2 92 9.029 8.8 94 9.130 8.2 95 205 Outlier31 9.8 97 1032 10 101 9.633 9.3 103 8.835 11 105 9.636 160 Outlier 106 8.938 11 107 9.239 9.7 111 1040 9.0 112 9.541 9.7 115 1042 9.8 117 9.844 9.845 8.246 8.8 Consensus median, pg/g 9.847 9.9 Median all values pg/g 9.848 9.6 Consensus mean, pg/g 9.949 47 Outlier Standard deviation, pg/g 0.8950 9.9 Relative standard deviation, % 9.053 10 No. of values reported 7854 12 No. of values removed 555 9.9 No. of reported non-detects 057 8.358 9.4

Analyte solutionCongener: OCDD

Consenus statistics

Page 14:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-1.282

0.718

2.718

4.718

6.718

8.718

10.718

12.718

14.7181 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

OCDD

-5-4-3-2-1012345

71 30 45 57 73 29 46 103

106 92 40 94 68 28 86 107 33 58 89 66 18 26 112 5 22 101 4 8 48 105 39 17 41 81 21 13 44 117 42 25 77 16 31 65 83 50 55 47 61 72 115 3 24 75 32 69 87 111 14 62 53 2 97 38 35 59 12 6 79 27 90 54 82 9 49 1 36 95

Labcode

Z-score: OCDD

Page 15:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 18 Outlier 59 2.02 1.9 61 2.03 2.0 62 2.14 1.9 65 1.85 1.9 66 2.16 2.1 68 2.08 1.8 69 2.09 2.5 71 0.20 Outlier12 1.9 72 2.013 2.0 73 1.914 2.0 75 2.116 1.9 77 2.117 2.1 79 2.118 1.9 81 2.021 2.0 82 2.022 1.9 83 2.024 1.9 86 2.025 2.0 87 1.926 1.9 89 1.827 2.2 90 2.228 1.9 92 1.829 1.8 94 2.130 1.7 95 41 Outlier31 1.9 97 2.332 2.0 101 2.033 1.8 103 2.135 2.2 105 2.036 33 Outlier 106 1.838 2.2 107 1.839 2.0 111 2.040 1.9 112 2.041 2.0 115 2.042 1.9 117 1.944 2.045 1.846 1.7 Consensus median, pg/g 2.047 2.1 Median all values pg/g 2.048 1.9 Consensus mean, pg/g 2.049 8.6 Outlier Standard deviation, pg/g 0.1450 1.9 Relative standard deviation, % 7.153 2.1 No. of values reported 7854 2.1 No. of values removed 555 2.0 No. of reported non-detects 057 1.658 2.1

Analyte solutionCongener: 2,3,7,8 TCDF

Consenus statistics

Page 16:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.045

0.455

0.955

1.455

1.955

2.455

2.9551 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

2,3,7,8 TCDF

-5-4-3-2-1012345

71 57 30 46 29 65 107 33 92 106 8 89 45 26 73 42 18 4 24 50 87 117 12 2 40 22 28 16 5 48 31 105 41 81 83 101 13 39 21 68 32 25 14 115

112 44 72 59 3 69 111 61 82 55 86 66 6 79 75 62 77 47 94 54 58 53 17 103 27 35 90 38 97 9 49 1 36 95

Labcode

Z-score: 2,3,7,8 TCDF

Page 17:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 45 Outlier 59 5.12 5.0 61 5.03 5.1 62 5.34 4.7 65 5.15 4.5 66 5.26 5.3 68 4.78 5.0 69 5.19 7.7 Outlier 71 1.1 Outlier12 5.2 72 5.013 4.8 73 4.914 5.3 75 5.016 5.0 77 5.217 5.0 79 5.118 4.7 81 5.021 5.0 82 5.022 5.0 83 5.024 4.8 86 5.225 4.8 87 5.026 5.0 89 4.727 5.6 90 6.028 4.8 92 4.829 4.7 94 4.530 4.5 95 111 Outlier31 4.8 97 5.632 5.3 101 4.833 5.2 103 4.535 5.8 105 5.336 90 Outlier 106 4.538 5.2 107 4.739 5.1 111 4.940 5.0 112 4.841 4.9 115 5.142 4.8 117 4.744 4.945 4.946 4.2 Consensus median, pg/g 5.047 5.1 Median all values pg/g 5.048 5.0 Consensus mean, pg/g 5.049 22 Outlier Standard deviation, pg/g 0.3450 4.9 Relative standard deviation, % 6.853 5.8 No. of values reported 7854 5.0 No. of values removed 655 4.9 No. of reported non-detects 057 3.958 4.8

Analyte solutionCongener: 1,2,3,7,8 PeCDF

Consenus statistics

Page 18:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.524

0.476

1.476

2.476

3.476

4.476

5.476

6.476

7.4761 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,7,8 PeCDF

-5-4-3-2-1012345

71 57 46 106 5

103 94 30 89 4 18 29 117

107 68 28 112 24 101 31 13 58 92 42 25 45 73 111 50 44 41 55 2 21 22 26 40 81 16 75 82 87 48 17 8 54 83 61 72 47 79 59 69 65 115 3 39 77 33 86 38 66 12 14 32 6 62 105 27 97 35 53 90 9 49 1 36 95

Labcode

Z-score: 1,2,3,7,8 PeCDF

Page 19:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 55 Outlier 59 5.22 4.8 61 5.03 5.1 62 5.14 4.5 65 5.05 4.6 66 5.16 5.4 68 4.58 4.7 69 5.19 8.3 Outlier 71 0.99 Outlier12 5.1 72 4.913 4.7 73 4.514 4.7 75 5.216 4.9 77 5.017 5.0 79 4.518 4.8 81 4.821 4.8 82 4.922 4.8 83 5.024 4.9 86 5.025 5.1 87 5.226 4.3 89 4.627 5.3 90 5.228 5.0 92 4.629 4.6 94 4.430 4.1 95 114 Outlier31 4.9 97 5.032 4.8 101 4.633 5.2 103 4.535 5.4 105 4.936 83 Outlier 106 4.338 4.6 107 4.439 4.8 111 5.040 4.7 112 4.641 4.8 115 5.142 4.8 117 5.044 4.445 4.546 4.0 Consensus median, pg/g 4.847 5.0 Median all values pg/g 4.948 4.7 Consensus mean, pg/g 4.849 20 Outlier Standard deviation, pg/g 0.3550 4.6 Relative standard deviation, % 7.253 5.9 No. of values reported 7854 4.9 No. of values removed 655 5.1 No. of reported non-detects 057 3.658 4.9

Analyte solutionCongener: 2,3,4,7,8 PeCDF

Consenus statistics

Page 20:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.688

0.313

1.313

2.313

3.313

4.313

5.313

6.313

7.3131 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

2,3,4,7,8 PeCDF

-5-4-3-2-1012345

71 57 46 30 106 26 107 44 94 73 45 103 68 4 79 50 29 5 38 89 112 92 101 14 40 13 8 48 18 22 32 41 42 2 21 39 81 31 82 58 24 54 72 105 16 111 83 77 17 61 47 65 117 86 28 97 66 25 55 12 115 3 69 62 87 75 59 33 90 27 35 6 53 9 49 1 36 95

Labcode

Z-score: 2,3,4,7,8 PeCDF

Page 21:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 50 Outlier 59 5.52 5.1 61 5.13 5.0 62 5.34 4.6 65 4.75 4.5 66 5.06 5.6 68 4.48 4.9 69 5.39 7.2 71 1.1 Outlier12 5.3 72 4.913 4.5 73 4.814 5.1 75 5.316 5.0 77 5.317 4.9 79 5.018 4.6 81 4.521 4.9 82 4.722 5.0 83 4.924 5.1 86 5.225 5.2 87 4.926 5.1 89 4.727 5.9 90 5.328 4.8 92 4.529 4.5 94 4.730 4.5 95 108 Outlier31 4.9 97 5.032 5.1 101 4.433 5.4 103 4.735 5.3 105 4.936 84 Outlier 106 4.338 5.7 107 4.739 5.0 111 5.040 4.7 112 4.941 5.1 115 5.042 5.0 117 4.944 4.945 4.346 4.2 Consensus median, pg/g 5.047 5.4 Median all values pg/g 5.048 5.1 Consensus mean, pg/g 5.049 23 Outlier Standard deviation, pg/g 0.4650 4.9 Relative standard deviation, % 9.153 5.7 No. of values reported 7854 5.2 No. of values removed 555 5.0 No. of reported non-detects 057 3.858 5.6

Analyte solutionCongener: 1,2,3,4,7,8 HxCDF

Consenus statistics

Page 22:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.508

0.492

1.492

2.492

3.492

4.492

5.492

6.492

7.4921 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,4,7,8 HxCDF

-5-4-3-2-1012345

71 57 46 106 45 101 68 5 30 81 29 92 13 4 18 107 94 65 103 89 82 40 73 28 21 50 87 31 44 112

117 8 72 17 83 105 42 16 66 55 22 79 111 3 97 39 115 2 61 41 14 48 24 26 32 54 86 25 62 75 77 12 69 90 35 47 33 59 6 58 38 53 27 9 49 1 36 95

Labcode

Z-score: 1,2,3,4,7,8 HxCDF

Page 23:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 54 Outlier 59 5.32 5.1 61 5.03 5.0 62 5.04 4.7 65 5.15 4.8 66 5.26 5.5 68 4.78 5.3 69 5.29 7.8 Outlier 71 1.1 Outlier12 5.2 72 4.913 4.7 73 4.714 5.3 75 4.916 5.0 77 5.217 5.3 79 5.218 5.2 81 4.921 4.8 82 4.922 5.0 83 5.124 5.0 86 5.225 5.1 87 4.626 4.7 89 4.627 5.7 90 5.228 4.9 92 4.729 4.8 94 4.830 4.5 95 114 Outlier31 4.9 97 5.632 5.1 101 4.833 4.8 103 4.935 5.5 105 4.936 88 Outlier 106 5.038 5.4 107 5.039 4.9 111 5.240 5.1 112 5.141 5.3 115 5.142 4.9 117 4.944 4.945 4.546 4.1 Consensus median, pg/g 5.047 5.4 Median all values pg/g 5.048 5.3 Consensus mean, pg/g 5.049 23 Outlier Standard deviation, pg/g 0.3150 4.9 Relative standard deviation, % 6.353 5.5 No. of values reported 7854 4.9 No. of values removed 655 5.0 No. of reported non-detects 057 3.958 5.6

Analyte solutionCongener: 1,2,3,6,7,8 HxCDF

Consenus statistics

Page 24:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.508

0.493

1.493

2.493

3.493

4.493

5.493

6.493

7.4931 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,6,7,8 HxCDF

-5-4-3-2-1012345

71 57 46 30 45 89 87 4 13 73 92 26 68 33 101 94 5 29 21 81 103

105 28 75 82 39 44 117 54 72 42 50 31 106 22 107 3 16 61 24 55 62 2 40 32 25 115 83 65 112 77 69 86 79 18 111 90 12 66 48 8 14 17 59 41 38 47 35 53 6 58 97 27 9 49 1 36 95

Labcode

Z-score: 1,2,3,6,7,8 HxCDF

Page 25:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 48 Outlier 59 5.82 4.9 61 5.03 5.0 62 5.14 4.5 65 5.25 4.6 66 5.16 5.1 68 4.68 4.8 69 5.19 8.4 Outlier 71 1.1 Outlier12 5.3 72 4.913 4.3 73 4.514 5.1 75 5.116 5.0 77 4.817 4.7 79 5.318 5.0 81 4.721 4.9 82 5.122 4.8 83 4.924 5.1 86 5.025 4.9 87 9.9 Outlier26 5.2 89 4.627 5.5 90 5.528 5.0 92 4.629 4.7 94 4.530 4.7 95 110 Outlier31 5.0 97 5.032 5.1 101 5.033 5.8 103 4.735 5.5 105 4.836 83 Outlier 106 4.738 5.0 107 4.639 5.2 111 5.040 4.5 112 5.241 5.4 115 5.042 5.0 117 4.844 4.845 4.346 4.3 Consensus median, pg/g 5.047 5.5 Median all values pg/g 5.048 5.0 Consensus mean, pg/g 5.049 22 Outlier Standard deviation, pg/g 0.3850 5.2 Relative standard deviation, % 7.653 5.8 No. of values reported 7854 5.4 No. of values removed 755 5.0 No. of reported non-detects 057 3.658 5.5

Analyte solutionCongener: 2,3,4,6,7,8 HxCDF

Consenus statistics

Page 26:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.500

0.500

1.500

2.500

3.500

4.500

5.500

6.500

7.5001 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

2,3,4,6,7,8 HxCDF

-5-4-3-2-1012345

71 57 13 45 46 40 94 73 4 5 68 89 92 107 81 106

103 29 17 30 77 8 44 117

105 22 21 83 2 25 72 31 16 97 55 115 61 111 18 38 101 3 86 48 42 28 14 82 62 24 32 6 66 75 69 50 39 65 26 112 79 12 54 41 27 90 58 47 35 33 59 53 9 87 49 1 36 95

Labcode

Z-score: 2,3,4,6,7,8 HxCDF

Page 27:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 51 Outlier 59 5.62 5.1 61 5.13 5.0 62 5.24 4.9 65 4.65 4.2 66 4.96 5.0 68 4.48 5.1 69 5.09 9.6 Outlier 71 1.0 Outlier12 5.3 72 5.013 4.9 73 4.614 4.9 75 5.416 5.0 77 5.017 5.1 79 4.618 4.6 81 4.421 5.0 82 5.422 5.0 83 4.924 5.2 86 5.025 5.1 87 4.926 5.0 89 4.827 5.6 90 4.828 4.9 92 4.429 4.7 94 5.330 4.3 95 105 Outlier31 4.7 97 5.132 4.9 101 4.933 5.3 103 5.335 5.3 105 5.136 85 Outlier 106 4.838 5.1 107 4.739 5.1 111 5.040 4.4 112 5.241 5.0 115 5.042 4.9 117 5.044 4.845 4.446 4.2 Consensus median, pg/g 5.047 5.2 Median all values pg/g 5.048 5.1 Consensus mean, pg/g 4.949 22 Outlier Standard deviation, pg/g 0.3650 5.8 Relative standard deviation, % 7.353 5.6 No. of values reported 7854 4.7 No. of values removed 655 5.0 No. of reported non-detects 057 3.958 5.7

Analyte solutionCongener: 1,2,3,7,8,9 HxCDF

Consenus statistics

Page 28:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.492

0.508

1.508

2.508

3.508

4.508

5.508

6.508

7.5081 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,7,8,9 HxCDF

-5-4-3-2-1012345

71 57 5 46 30 68 40 92 81 45 79 18 65 73 107 29 31 54 106 44 90 89 13 87 32 101 28 83 14 4 42 66 115

111 55 3 22 117 41 21 26 72 16 86 69 6 77 39 17 2 38 105 48 8 25 97 61 112 62 24 47 94 33 12 35 103 82 75 27 53 59 58 50 9 49 1 36 95

Labcode

Z-score: 1,2,3,7,8,9 HxCDF

Page 29:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 49 Outlier 59 5.82 4.9 61 5.13 5.0 62 5.24 4.7 65 5.05 4.9 66 4.96 5.1 68 4.78 5.0 69 5.19 7.1 71 1.1 Outlier12 5.9 72 5.013 4.8 73 4.514 5.2 75 5.316 4.9 77 5.217 5.0 79 4.718 5.1 81 4.921 5.0 82 6.122 4.9 83 5.024 5.2 86 5.025 5.2 87 2.0 Outlier26 5.2 89 4.727 6.6 90 5.128 4.7 92 4.529 4.5 94 4.930 4.3 95 111 Outlier31 4.8 97 5.932 5.2 101 4.633 4.8 103 4.935 5.4 105 5.136 86 Outlier 106 4.738 5.5 107 4.439 4.9 111 5.240 4.6 112 5.041 5.1 115 5.042 4.7 117 5.144 5.045 4.346 4.1 Consensus median, pg/g 5.047 5.4 Median all values pg/g 5.048 4.8 Consensus mean, pg/g 5.049 24 Outlier Standard deviation, pg/g 0.4950 5.0 Relative standard deviation, % 1053 5.3 No. of values reported 7854 5.1 No. of values removed 655 5.1 No. of reported non-detects 057 3.858 5.6

Analyte solutionCongener: 1,2,3,4,6,7,8 HpCDF

Consenus statistics

Page 30:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.499

0.501

1.501

2.501

3.501

4.501

5.501

6.501

7.5011 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,4,6,7,8 HpCDF

-5-4-3-2-1012345

71 87 57 46 45 30 107 73 92 29 40 101 68 42 89 4 28 106 79 33 48 13 31 22 103 94 5 66 81 2 16 39 21 112 17 72 83 50 44 3 8 86 115 65 55 61 105 6 41 90 18 117 69 54 77 62 25 32 24 14 26 111 75 53 47 35 38 58 59 12 97 82 27 9 49 1 36 95

Labcode

Z-score: 1,2,3,4,6,7,8 HpCDF

Page 31:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 49 Outlier 59 5.72 5.0 61 5.03 5.0 62 5.14 4.6 65 4.85 4.6 66 4.86 5.1 68 4.38 5.0 69 5.09 7.7 Outlier 71 1.0 Outlier12 5.6 72 5.013 5.2 73 4.714 5.5 75 5.516 5.0 77 5.017 5.1 79 5.218 4.9 81 4.821 4.8 82 4.822 5.0 83 5.024 5.1 86 5.125 5.2 87 5.026 4.9 89 4.727 5.7 90 4.928 4.7 92 4.429 4.9 94 4.930 4.4 95 113 Outlier31 5.0 97 6.432 5.1 101 4.833 5.6 103 4.535 5.4 105 4.936 88 Outlier 106 4.938 5.2 107 4.739 5.1 111 5.140 4.5 112 5.741 4.4 115 5.042 4.9 117 5.044 4.745 4.346 4.2 Consensus median, pg/g 5.047 5.4 Median all values pg/g 5.048 5.1 Consensus mean, pg/g 5.049 23 Outlier Standard deviation, pg/g 0.4050 5.1 Relative standard deviation, % 8.153 5.5 No. of values reported 7854 5.0 No. of values removed 655 5.0 No. of reported non-detects 057 3.958 5.8

Analyte solutionCongener: 1,2,3,4,7,8,9 HpCDF

Consenus statistics

Page 32:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-0.534

0.466

1.466

2.466

3.466

4.466

5.466

6.466

7.4661 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

1,2,3,4,7,8,9 HpCDF

-5-4-3-2-1012345

71 57 46 45 68 41 30 92 40 103 5 4 44 89 73 28 107

101 81 65 82 66 21 42 106 94 90 18 26 105 29 87 72 8 22 2 83 77 31 115 16 61 55 54 117 3 69 6

111 39 17 32 24 86 48 62 50 13 79 38 25 35 47 14 53 75 12 33 112 59 27 58 97 9 49 1 36 95

Labcode

Z-score: 1,2,3,4,7,8,9 HpCDF

Page 33:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 99 Outlier 59 112 9.6 61 113 10 62 114 10 65 9.95 9.3 66 8.56 11 68 9.88 9.3 69 109 12 71 2.3 Outlier12 11 72 9.913 9.5 73 8.214 9.3 75 1116 10 77 9.517 10 79 9.118 9.5 81 9.721 9.5 82 9.922 9.5 83 1024 10 86 9.525 10 87 5.126 9.3 89 1027 8.4 90 7.728 8.9 92 9.129 8.0 94 8.530 7.4 95 211 Outlier31 9.8 97 1032 10 101 8.933 11 103 8.135 11 105 9.736 178 Outlier 106 9.638 10 107 8.839 9.9 111 9.840 8.7 112 1041 9.2 115 1042 9.6 117 1044 9.145 8.046 7.7 Consensus median, pg/g 9.847 11 Median all values pg/g 9.848 10 Consensus mean, pg/g 9.649 45 Outlier Standard deviation, pg/g 1.150 10 Relative standard deviation, % 1153 11 No. of values reported 7854 11 No. of values removed 555 10 No. of reported non-detects 057 7.358 8.9

Analyte solutionCongener: OCDF

Consenus statistics

Page 34:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-1.251

0.750

2.750

4.750

6.750

8.750

10.750

12.750

14.7501 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 62 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

OCDF

-5-4-3-2-1012345

71 87 57 30 46 90 29 45 103 73 27 94 66 40 107 28 58 101 44 79 92 41 5 14 26 8 22 86 18 77 13 21 2 42 106

105 81 111 68 31 72 82 39 65 25 112 16 55 50 89 4 3 83 115

117 69 17 32 97 48 24 38 35 61 54 6 75 59 47 33 62 12 53 9 49 1 36 95

Labcode

Z-score: OCDF

Page 35:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 16 Outlier 59 102 10 61 123 10 65 104 10 66 9.95 9.6 68 9.26 2.7 Outlier 69 118 9.1 71 9.39 9.2 72 1012 11 73 1113 10 75 9.814 11 77 1016 10 79 9.317 10 81 10.018 11 82 9.821 9.8 83 9.922 9.8 86 1024 11 87 9.525 10 89 9.426 10 90 9.427 9.5 92 9.828 10 94 1129 9.1 95 9.630 10 97 1031 9.7 101 1132 9.7 103 1133 10.0 105 9.835 11 106 9.636 209 Outlier 107 9.738 11 111 9.939 10 112 1040 10 115 1041 11 117 9.742 1044 1045 1046 8.8 Consensus median, pg/g 1047 9.6 Median all values pg/g 1048 9.9 Consensus mean, pg/g 1049 9.9 Standard deviation, pg/g 0.6150 8.8 Relative standard deviation, % 6.053 11 No. of values reported 7754 9.4 No. of values removed 455 9.9 No. of reported non-detects 057 16 Outlier58 11

Analyte solutionCongener: PCB 77

Consenus statistics

Page 36:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-1.015

0.985

2.985

4.985

6.985

8.985

10.985

12.985

14.9851 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 77

-5-4-3-2-1012345

6 50 46 8 29 9 68 71 79 89 90 54 27 87 5 47 106 95 32 31 117

107 21 92 105 75 22 82 111 83 55 48 49 66 33 65 115 81 40 42 44 86 59 72 112 25 30 77 3 45 16 2 26 13 17 4 28 97 39 38 58 18 14 35 41 69 12 24 53 101 73 94 103 61 57 1 36

Labcode

Z-score: PCB 77

Page 37:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 18 Outlier 59 102 10 61 9.93 10 65 9.94 11 66 105 9.5 68 9.86 2.7 Outlier 69 108 8.7 71 9.79 9.3 72 1012 10 73 9.013 10 75 1014 10 77 9.616 9.8 79 8.917 9.6 81 1018 10 82 9.621 9.8 83 1022 9.9 86 9.824 10 87 9.625 10 89 9.926 11 90 8.727 9.4 92 9.728 10 94 9.829 8.8 95 1130 11 97 1031 9.6 101 1132 9.3 103 9.833 9.0 105 1035 9.5 106 1036 196 Outlier 107 9.238 11 111 1039 11 112 1140 9.1 115 1041 9.4 117 9.442 9.944 1045 9.546 9.1 Consensus median, pg/g 9.947 9.9 Median all values pg/g 9.948 11 Consensus mean, pg/g 9.949 10 Standard deviation, pg/g 0.5750 8.5 Relative standard deviation, % 5.753 9.9 No. of values reported 7754 9.9 No. of values removed 455 9.8 No. of reported non-detects 057 15 Outlier58 9.4

Analyte solutionCongener: PCB 126

Consenus statistics

Page 38:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-1.105

0.895

2.895

4.895

6.895

8.895

10.895

12.895

14.8951 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 126

-5-4-3-2-1012345

6 50 90 8 29 79 33 73 40 46 107 9 32 58 117 27 41 5 35 45 31 17 82 77 87 71 92 103 21 68 86 55 16 94 61 22 65 89 53 54 47 42 49 97 59 44 72 106 13 3 2

115 12 83 18 105 75 111 25 69 66 28 24 81 14 112 4 39 30 26 95 38 101 48 57 1 36

Labcode

Z-score: PCB 126

Page 39:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 16 Outlier 59 9.72 9.8 61 113 10 65 104 10 66 9.95 9.2 68 116 2.8 Outlier 69 108 9.2 71 119 9.7 72 1012 11 73 1413 10 75 9.914 11 77 9.516 9.9 79 8.717 9.4 81 1118 10 82 9.821 10 83 9.922 9.8 86 1024 10 87 9.625 9.6 89 9.626 10 90 9.527 9.2 92 9.528 8.9 94 8.829 9.0 95 1030 9.4 97 9.731 9.7 101 9.932 9.8 103 9.033 9.6 105 1035 10 106 9.236 217 Outlier 107 9.638 11 111 9.739 11 112 1140 9.1 115 1041 9.6 117 9.742 1044 9.845 9.646 8.9 Consensus median, pg/g 9.847 9.5 Median all values pg/g 9.848 11 Consensus mean, pg/g 9.949 9.8 Standard deviation, pg/g 0.8150 9.7 Relative standard deviation, % 853 11 No. of values reported 7754 9.0 No. of values removed 355 10 No. of reported non-detects 057 1258 8.7

Analyte solutionCongener: PCB 169

Consenus statistics

Page 40:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-1.264

0.736

2.736

4.736

6.736

8.736

10.736

12.736

14.7361 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 169

-5-4-3-2-1012345

6 58 79 94 46 28 54 29 103 40 5 27 8

106 30 17 47 90 92 77 87 25 45 107 33 89 41 111 31 59 117 97 9 50 82 44 2 49 22 32 75 16 101 66 83 21 55 72 35 3 86 65 13 42 115 26 95 4 69 18 24 105 81 48 38 53 112 61 39 68 14 12 71 57 73 1 36

Labcode

Z-score: PCB 169

Page 41:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 17 Outlier 59 112 10 61 103 10 65 104 10 66 105 9.3 68 9.96 2.8 Outlier 69 108 8.9 71 9.99 9.8 72 1012 11 73 1013 10 75 1014 10 77 9.816 9.9 79 9.617 9.8 81 9.918 11 82 1021 10 83 1022 10 86 1024 9.5 87 9.925 10 89 9.426 11 90 1027 9.9 92 1028 9.9 94 8.729 9.2 95 9.830 9.2 97 1231 9.8 101 1032 10 103 8.833 10 105 1035 11 106 9.836 207 Outlier 107 1038 11 111 9.639 11 112 9.340 9.2 115 9.941 10 117 9.942 1044 9.845 1046 9.1 Consensus median, pg/g 1047 9.7 Median all values pg/g 1048 11 Consensus mean, pg/g 1049 10 Standard deviation, pg/g 0.5850 9.0 Relative standard deviation, % 5.853 11 No. of values reported 7754 9.8 No. of values removed 455 10 No. of reported non-detects 057 16 Outlier58 10

Analyte solutionCongener: PCB 81

Consenus statistics

Page 42:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-1.000

1.000

3.000

5.000

7.000

9.000

11.000

13.000

15.0001 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 81

-5-4-3-2-1012345

6 94 103 8 50 46 30 29 40 112 5 89 24 111 79 47 77 31 54 9 44 95 106 17 68 71 28 81 117 87 115 16 27 2 72 92 58 65 86 90 101 3 55 25 41 73 105 66 22 32 75 42 13 107 49 83 61 69 45 14 21 82 4 33 35 26 59 18 39 12 38 48 53 97 57 1 36

Labcode

Z-score: PCB 81

Page 43:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 201 Outlier 59 992 102 61 983 100 65 1004 105 66 985 101 68 966 28 Outlier 69 1038 91 71 979 98 72 9812 96 73 9213 88 75 10414 110 77 9616 97 79 9017 95 81 9718 109 82 8821 100 83 9822 97 86 9324 100 87 9025 95 89 11026 107 90 9127 95 92 9228 109 94 9529 104 95 10430 92 97 10431 95 101 11032 92 103 9433 99 105 9735 100 106 9236 2100 Outlier 107 9338 101 111 9839 97 112 10240 101 115 10341 106 117 9642 9544 9545 9746 95 Consensus median, pg/g 9847 100 Median all values pg/g 9848 106 Consensus mean, pg/g 9849 108 Standard deviation, pg/g 6.250 94 Relative standard deviation, % 6.353 100 No. of values reported 7754 93 No. of values removed 455 99 No. of reported non-detects 057 151 Outlier58 73

Analyte solutionCongener: PCB 105

Consenus statistics

Page 44:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-13.315

6.685

26.685

46.685

66.685

86.685

106.685

126.685

146.6851 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 105

-5-4-3-2-1012345

6 58 82 13 79 87 90 8

106 30 92 73 32 54 107 86 103 50 17 42 27 46 31 44 94 25 12 68 117 77 39 71 22 16 81 45 105

111 61 66 72 83 9 59 33 55 3 53 65 21 24 35 47 38 40 5 2

112 69 115 95 29 97 75 4 41 48 26 49 18 28 89 101 14 57 1 36

Labcode

Z-score: PCB 105

Page 45:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 212 Outlier 59 982 102 61 883 100 65 994 109 66 955 99 68 996 25 Outlier 69 1018 90 71 1029 102 72 10112 96 73 8613 88 75 9514 109 77 9616 99 79 8817 98 81 10418 107 82 8121 97 83 9922 93 86 9624 97 87 9125 95 89 10826 103 90 9427 92 92 8828 107 94 9029 105 95 10230 92 97 10731 96 101 10032 100 103 8933 101 105 9635 103 106 9536 1980 Outlier 107 9638 103 111 10239 98 112 10340 93 115 10041 104 117 9542 9344 9945 9446 92 Consensus median, pg/g 9947 101 Median all values pg/g 9948 101 Consensus mean, pg/g 9849 114 Standard deviation, pg/g 6.150 92 Relative standard deviation, % 6.353 104 No. of values reported 7754 89 No. of values removed 455 100 No. of reported non-detects 057 171 Outlier58 102

Analyte solutionCongener: PCB 114

Consenus statistics

Page 46:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-12.100

7.900

27.900

47.900

67.900

87.900

107.900

127.900

147.9001 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 114

-5-4-3-2-1012345

6 82 73 92 13 79 61 54 103 94 8 87 27 46 30 50 40 42 22 90 45 75 25 117 66 106 77 12 107 31 86 105 21 24 17 39 59 65 68 5 44 16 83 55 101 3 32 115 33 69 47 72 48 58 2 95 9 71 111 26 35 38 112 53 81 41 29 97 28 18 89 4 14 49 57 1 36

Labcode

Z-score: PCB 114

Page 47:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 210 Outlier 59 992 101 61 923 100 65 1044 107 66 945 97 68 956 24 Outlier 69 1018 88 71 1009 100 72 10012 99 73 9113 99 75 9614 109 77 9916 99 79 9217 96 81 9718 107 82 9021 97 83 9822 97 86 9724 95 87 9125 93 89 11026 107 90 9227 96 92 9028 108 94 9429 102 95 10630 92 97 11831 95 101 11032 92 103 9333 108 105 9835 108 106 9236 2180 Outlier 107 9638 110 111 9839 98 112 10740 105 115 10041 106 117 10342 9544 9845 9946 91 Consensus median, pg/g 9947 100 Median all values pg/g 9948 102 Consensus mean, pg/g 10049 114 Standard deviation, pg/g 6.850 108 Relative standard deviation, % 6.853 109 No. of values reported 7754 96 No. of values removed 355 100 No. of reported non-detects 057 12158 106

Analyte solutionCongener: PCB 118

Consenus statistics

Page 48:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-11.787

8.213

28.213

48.213

68.213

88.213

108.213

128.213

148.2131 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 118

-5-4-3-2-1012345

6 8 92 82 87 46 73 79 90 61 106 32 30 103 25 66 94 24 42 68 31 17 27 107 75 54 22 21 86 81 5 39 105 44 83 111 16 45 77 59 12 13 55 115 9 71 3 47 72 69 2 48 29 117 65 40 41 95 58 4 26 112 18 33 35 50 28 14 53 38 101 89 49 97 57 1 36

Labcode

Z-score: PCB 118

Page 49:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 198 Outlier 59 932 101 61 973 100 65 1054 107 66 895 95 68 956 25 Outlier 69 1018 88 71 949 96 72 10212 98 73 9113 94 75 9614 112 77 9716 100 79 8817 101 81 9918 109 82 8821 100 83 10122 97 86 10024 100 87 5725 95 89 11526 106 90 10127 94 92 9328 108 94 7829 102 95 9030 93 97 10731 94 101 11032 104 103 7833 110 105 10435 104 106 10136 2090 Outlier 107 10038 108 111 10639 96 112 10740 106 115 10041 103 117 9842 9944 9445 10146 95 Consensus median, pg/g 10047 101 Median all values pg/g 10048 113 Consensus mean, pg/g 9949 117 Standard deviation, pg/g 9.250 93 Relative standard deviation, % 9.253 110 No. of values reported 7754 102 No. of values removed 355 100 No. of reported non-detects 057 11858 107

Analyte solutionCongener: PCB 123

Consenus statistics

Page 50:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-9.852

10.148

30.148

50.148

70.148

90.148

110.148

130.148

150.1481 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 123

-5-4-3-2-1012345

6 87 94 103 8 82 79 66 95 73 59 92 50 30 13 27 31 44 71 46 68 5 25 9 39 75 22 77 61 12 117 81 42 107 16 21 24 86 3

115 55 47 69 90 2

106 17 83 45 72 54 29 41 35 105 32 65 111 26 40 58 4 97 112 28 38 18 33 101 53 14 48 89 49 57 1 36

Labcode

Z-score: PCB 123

Page 51:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 206 Outlier 59 1032 105 61 1043 100 65 1024 102 66 865 113 68 1006 25 Outlier 69 1028 93 71 949 98 72 10112 95 73 12513 104 75 9314 110 77 10016 97 79 9117 102 81 9818 106 82 9321 97 83 10222 119 86 10424 95 87 9425 93 89 11426 108 90 9627 98 92 8628 105 94 10429 103 95 11430 87 97 11631 93 101 11032 103 103 10533 103 105 10135 102 106 9736 2100 Outlier 107 9538 105 111 9739 102 112 10940 95 115 10041 107 117 10042 9844 10045 9846 94 Consensus median, pg/g 10147 102 Median all values pg/g 10148 104 Consensus mean, pg/g 10249 108 Standard deviation, pg/g 8.350 96 Relative standard deviation, % 8.153 108 No. of values reported 7754 98 No. of values removed 355 99 No. of reported non-detects 057 13758 101

Analyte solutionCongener: PCB 156

Consenus statistics

Page 52:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-8.005

11.995

31.995

51.995

71.995

91.995

111.995

131.995

151.9951 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 156

-5-4-3-2-1012345

6 92 66 30 79 31 25 82 8 75 46 87 71 107 24 40 12 90 50 21 106 16 111 81 27 9 42 54 45 55 77 3

115 44 68 117 58 105 72 47 69 39 35 4 17 83 65 32 59 29 33 94 86 48 61 13 103 2 38 28 18 41 53 26 49 112

101 14 5 95 89 97 22 73 57 1 36

Labcode

Z-score: PCB 156

Page 53:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 204 Outlier 59 992 105 61 1013 100 65 1024 99 66 925 99 68 936 26 Outlier 69 1028 89 71 959 99 72 10112 96 73 13213 97 75 10114 108 77 9716 97 79 9217 94 81 10118 107 82 9621 96 83 9922 115 86 10324 95 87 10025 96 89 11026 105 90 9027 98 92 8028 102 94 10429 99 95 10830 86 97 10931 91 101 11032 94 103 10433 97 105 9935 101 106 9436 2140 Outlier 107 9538 98 111 10239 100 112 10540 95 115 10041 104 117 9842 8544 10045 9546 88 Consensus median, pg/g 9947 101 Median all values pg/g 9948 101 Consensus mean, pg/g 10049 116 Standard deviation, pg/g 8.650 98 Relative standard deviation, % 8.653 105 No. of values reported 7754 109 No. of values removed 355 100 No. of reported non-detects 057 13758 98

Analyte solutionCongener: PCB 157

Consenus statistics

Page 54:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-10.975

9.025

29.025

49.025

69.025

89.025

109.025

129.025

149.0251 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 157

-5-4-3-2-1012345

6 92 42 30 46 8 90 31 66 79 68 32 106 17 107 24 40 71 45 12 82 21 25 16 77 33 13 50 38 117 27 58 4

105 83 5 59 9 29 115 3 55 44 87 39 75 61 35 81 72 48 47 65 111 69 28 86 94 103 41 2 26 112 53 18 14 95 97 54 89 101 22 49 73 57 1 36

Labcode

Z-score: PCB 157

Page 55:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 223 Outlier 59 1052 103 61 943 100 65 1004 104 66 955 109 68 996 25 Outlier 69 1018 99 71 839 99 72 10112 96 73 13013 104 75 10114 113 77 9816 97 79 9917 94 81 10318 107 82 9821 98 83 9922 103 86 9924 95 87 9125 91 89 10826 106 90 9427 96 92 8728 107 94 8829 100 95 10630 88 97 10631 91 101 11032 97 103 8733 100 105 9635 101 106 9236 2200 Outlier 107 10338 103 111 10739 104 112 10540 99 115 10041 106 117 9642 9444 10045 9646 86 Consensus median, pg/g 10047 100 Median all values pg/g 10048 100 Consensus mean, pg/g 10049 215 Outlier Standard deviation, pg/g 8.450 95 Relative standard deviation, % 8.453 111 No. of values reported 7754 100 No. of values removed 455 100 No. of reported non-detects 057 13658 91

Analyte solutionCongener: PCB 167

Consenus statistics

Page 56:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-10.450

9.550

29.550

49.550

69.550

89.550

109.550

129.550

149.5501 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 167

-5-4-3-2-1012345

6 71 46 103 92 94 30 31 87 25 58 106 17 61 90 42 24 66 50 12 105

117 27 45 16 32 21 77 82 8 40 68 79 83 86 9 48 55 33 29 44 47 3 54 65 115 72 75 69 35 22 2 38 81 107 4 39 13 112 59 26 41 95 97 28 111 18 89 5

101 53 14 73 57 49 1 36

Labcode

Z-score: PCB 167

Page 57:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 206 Outlier 59 932 104 61 923 99 65 1014 101 66 885 103 68 956 26 Outlier 69 1028 95 71 979 99 72 10012 96 73 13613 95 75 10014 114 77 10316 97 79 9517 102 81 9818 107 82 10121 96 83 10122 99 86 10824 100 87 9325 92 89 11026 102 90 9827 98 92 9428 108 94 10129 97 95 11330 85 97 10331 93 101 11032 104 103 10233 104 105 9835 97 106 9636 2140 Outlier 107 10138 104 111 10039 109 112 10040 92 115 10041 110 117 10142 9044 9545 9346 97 Consensus median, pg/g 10047 100 Median all values pg/g 10048 107 Consensus mean, pg/g 10149 121 Standard deviation, pg/g 8.950 93 Relative standard deviation, % 8.853 103 No. of values reported 7754 92 No. of values removed 355 100 No. of reported non-detects 057 14258 102

Analyte solutionCongener: PCB 189

Consenus statistics

Page 58:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-10.000

10.000

30.000

50.000

70.000

90.000

110.000

130.000

150.0001 2 3 4 5 6 8 9 12 13 14 16 17 18 21 22 24 25 26 27 28 29 30 31 32 33 35 36 38 39 40 41 42 44 45 46 47 48 49 50 53 54 55 57 58 59 61 65 66 68 69 71 72 73 75 77 79 81 82 83 86 87 89 90 92 94 95 97 101

103

105

106

107

111

112

115

117

pg/g

fw

Labcode

PCB 189

-5-4-3-2-1012345

6 30 66 42 61 54 40 25 87 59 45 31 50 92 68 13 44 79 8 12 21 106 16 35 46 71 29 27 81 90 105 3 9 22 111 55 47 75 24 112

115 72 82 107

117 4 94 65 83 69 58 103 26 17 53 5 97 77 33 2 38 32 48 18 86 28 39 41 89 101 95 14 49 73 57 1 36

Labcode

Z-score: PCB 189

Page 59:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 217 Outlier 77 992 101 79 903 103 81 1014 89 82 875 93 83 996 64 86 1038 90 87 8912 102 90 10013 110 92 9716 98 94 8917 96 97 9718 99 101 10021 97 103 8922 105 105 9623 110 106 9624 97 107 9625 103 108 10526 91 112 9727 92 114 10228 103 115 10030 113 117 9533 9835 9736 2000 Outlier38 9539 10040 9841 41 Outlier42 9344 9746 9647 12348 10349 7553 10654 89 Consensus median, pg/g 9855 98 Median all values pg/g 9858 102 Consensus mean, pg/g 9861 96 Standard deviation, pg/g 8.265 104 Relative standard deviation, % 868 97 No. of values reported 6669 101 No. of values removed 371 103 No. of reported non-detects 073 10675 102

Analyte solutionCongener: PCB 28

Consenus statistics

Page 60:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-13.207

6.793

26.793

46.793

66.793

86.793

106.793

126.793

146.7931 2 3 4 5 6 8 12 13 16 17 18 21 22 23 24 25 26 27 28 30 33 35 36 38 39 40 41 42 44 46 47 48 49 53 54 55 58 61 65 68 69 71 73 75 77 79 81 82 83 86 87 90 92 94 97 101

103

105

106

107

108

112

114

115

117

pg/g

fw

Labcode

PCB 28

-5-4-3-2-1012345

41 6 49 82 94 4 87 103 54 79 8 26 27 42 5 38 117 61 106 17 105 46 107 21 24 35 44 68 112 97 92 40 33 55 16 83 18 77 115 90 101 39 2 81 69 75 58 114 12 25 71 28 86 3 48 65 22 108 53 73 13 23 30 47 1 36

Labcode

Z-score: PCB 28

Page 61:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 208 Outlier 77 1012 101 79 893 98 81 1014 112 82 935 82 83 996 64 86 1008 89 87 9112 98 90 9913 94 92 10216 96 94 10417 102 97 10518 97 101 9621 98 103 10522 105 105 9723 101 106 9724 103 107 10225 101 108 10126 95 112 10727 88 114 9828 103 115 9830 104 117 9233 10435 9836 2000 Outlier38 9739 10040 9041 7842 9644 9446 8647 11248 10949 9253 9554 96 Consensus median, pg/g 9955 99 Median all values pg/g 9958 99 Consensus mean, pg/g 9861 87 Standard deviation, pg/g 8.565 103 Relative standard deviation, % 968 95 No. of values reported 6669 100 No. of values removed 271 127 No. of reported non-detects 073 10675 100

Analyte solutionCongener: PCB 52

Consenus statistics

Page 62:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-11.684

8.316

28.316

48.316

68.316

88.316

108.316

128.316

148.3161 2 3 4 5 6 8 12 13 16 17 18 21 22 23 24 25 26 27 28 30 33 35 36 38 39 40 41 42 44 46 47 48 49 53 54 55 58 61 65 68 69 71 73 75 77 79 81 82 83 86 87 90 92 94 97 101

103

105

106

107

108

112

114

115

117

pg/g

fw

Labcode

PCB 52

-5-4-3-2-1012345

6 41 5 46 61 27 79 8 40 87 117 49 82 13 44 68 26 53 54 101 42 16 106 38 105 18 12 35 21 3

114

115 83 55 90 58 75 39 86 69 25 2 23 81 108 77 107 92 17 65 24 28 30 33 94 97 103 22 73 112 48 4 47 71 1 36

Labcode

Z-score: PCB 52

Page 63:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 188 Outlier 77 992 102 79 993 97 81 954 115 82 815 99 83 996 62 86 988 93 87 9112 96 90 10113 100 92 10016 97 94 9717 98 97 9018 99 101 9821 96 103 9922 106 105 9623 104 106 9424 98 107 9525 101 108 10226 90 112 10727 90 114 9828 104 115 10230 91 117 9533 10435 10336 1990 Outlier38 10239 10040 10341 7942 9644 9846 8547 11748 10649 11353 9754 94 Consensus median, pg/g 9855 99 Median all values pg/g 9958 101 Consensus mean, pg/g 9861 100 Standard deviation, pg/g 8.165 100 Relative standard deviation, % 868 97 No. of values reported 6669 100 No. of values removed 271 82 No. of reported non-detects 073 10375 98

Analyte solutionCongener: PCB 101

Consenus statistics

Page 64:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-12.126

7.875

27.875

47.875

67.875

87.875

107.875

127.875

147.8751 2 3 4 5 6 8 12 13 16 17 18 21 22 23 24 25 26 27 28 30 33 35 36 38 39 40 41 42 44 46 47 48 49 53 54 55 58 61 65 68 69 71 73 75 77 79 81 82 83 86 87 90 92 94 97 101

103

105

106

107

108

112

114

115

117

pg/g

fw

Labcode

PCB 101

-5-4-3-2-1012345

6 41 82 71 46 26 27 97 87 30 8 54 106 81 107

117 21 105 42 12 53 94 16 68 3 75 17 24 44 86 101

114

103 18 79 77 83 55 5 61 65 92 39 13 69 25 90 58 2 38 108

115 35 40 73 23 33 28 22 48 112 49 4 47 1 36

Labcode

Z-score: PCB 101

Page 65:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 239 Outlier 77 1012 100 79 1053 98 81 964 101 82 935 92 83 996 65 86 1028 89 87 9012 97 90 10413 92 92 9616 96 94 9517 97 97 9418 102 101 9721 98 103 9722 108 105 9723 111 106 10324 102 107 10725 103 108 11226 102 112 10327 98 114 9428 111 115 10030 99 117 10033 10535 10436 1970 Outlier38 10539 10240 9041 8142 10044 10046 9047 10548 10849 7353 9254 98 Consensus median, pg/g 9955 99 Median all values pg/g 9958 104 Consensus mean, pg/g 9961 116 Standard deviation, pg/g 8.265 98 Relative standard deviation, % 868 94 No. of values reported 6669 101 No. of values removed 271 93 No. of reported non-detects 073 10975 97

Analyte solutionCongener: PCB 138

Consenus statistics

Page 66:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-10.757

9.243

29.243

49.243

69.243

89.243

109.243

129.243

149.2431 2 3 4 5 6 8 12 13 16 17 18 21 22 23 24 25 26 27 28 30 33 35 36 38 39 40 41 42 44 46 47 48 49 53 54 55 58 61 65 68 69 71 73 75 77 79 81 82 83 86 87 90 92 94 97 101

103

105

106

107

108

112

114

115

117

pg/g

fw

Labcode

PCB 138

-5-4-3-2-1012345

6 49 41 8 40 46 87 5 13 53 71 82 68 97 114 94 92 81 16 101 75 103 12 17 105 21 54 3 27 65 30 83 55 42 2 44 117

115 77 4 69 18 39 24 26 86 25 106

112 35 90 58 33 38 47 79 107 22 48 73 23 28 108 61 1 36

Labcode

Z-score: PCB 138

Page 67:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 210 Outlier 77 992 106 79 1003 99 81 1044 101 82 875 93 83 996 65 86 1008 90 87 9412 98 90 12013 101 92 9716 100 94 9717 99 97 10018 105 101 9521 99 103 9822 100 105 9523 111 106 10124 103 107 10525 101 108 10726 98 112 10127 98 114 9828 107 115 9830 94 117 9433 10035 10436 2000 Outlier38 9839 10240 10141 8042 9644 9846 9247 10948 10949 10353 9254 98 Consensus median, pg/g 9955 99 Median all values pg/g 10058 102 Consensus mean, pg/g 9961 114 Standard deviation, pg/g 7.765 99 Relative standard deviation, % 868 92 No. of values reported 6669 102 No. of values removed 271 83 No. of reported non-detects 073 10475 103

Analyte solutionCongener: PCB 153

Consenus statistics

Page 68:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-10.732

9.268

29.268

49.268

69.268

89.268

109.268

129.268

149.2681 2 3 4 5 6 8 12 13 16 17 18 21 22 23 24 25 26 27 28 30 33 35 36 38 39 40 41 42 44 46 47 48 49 53 54 55 58 61 65 68 69 71 73 75 77 79 81 82 83 86 87 90 92 94 97 101

103

105

106

107

108

112

114

115

117

pg/g

fw

Labcode

PCB 153

-5-4-3-2-1012345

6 41 71 82 8 53 68 46 5

117 87 30 105

101 42 92 94 54 12 114 26 27 38 44 115

103 21 77 17 65 83 3 55 22 97 16 79 86 33 25 13 40 106

112 4 58 69 39 75 24 49 35 73 81 18 107 2 28 108 47 48 23 61 90 1 36

Labcode

Z-score: PCB 153

Page 69:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes1 238 Outlier 77 1012 101 79 1033 102 81 994 114 82 825 90 83 996 66 86 1038 89 87 9712 97 90 10913 110 92 11016 100 94 11017 99 97 7518 102 101 10021 96 103 11122 101 105 10023 109 106 10524 100 107 10725 100 108 11226 87 112 10327 100 114 9428 112 115 9930 91 117 10133 10835 9536 1980 Outlier38 10639 10840 9541 7842 9844 9946 9247 8848 10549 10953 9154 96 Consensus median, pg/g 10055 99 Median all values pg/g 10058 104 Consensus mean, pg/g 9961 106 Standard deviation, pg/g 9.065 101 Relative standard deviation, % 968 100 No. of values reported 6669 102 No. of values removed 271 95 No. of reported non-detects 073 10975 97

Analyte solutionCongener: PCB 180

Consenus statistics

Page 70:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-9.939

10.062

30.062

50.062

70.062

90.062

110.062

130.062

150.0621 2 3 4 5 6 8 12 13 16 17 18 21 22 23 24 25 26 27 28 30 33 35 36 38 39 40 41 42 44 46 47 48 49 53 54 55 58 61 65 68 69 71 73 75 77 79 81 82 83 86 87 90 92 94 97 101

103

105

106

107

108

112

114

115

117

pg/g

fw

Labcode

PCB 180

-5-4-3-2-1012345

6 97 41 82 26 47 8 5 30 53 46 114 35 40 71 21 54 87 75 12 42 83 17 44 81 115 55 105 16 24 27 68 101 25 65 2

117 22 77 69 3 18 79 86 112 58 106 48 38 61 107 39 33 23 49 73 90 94 13 92 103 28 108 4 1 36

Labcode

Z-score: PCB 180

Page 71:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes2 254 255 228 2318 2423 2424 1826 2628 2333 2635 2638 2340 2642 2544 2646 2248 2549 3053 2758 2259 2473 2675 2577 2587 2490 2592 2594 2697 26

103 26106 23107 25112 25117 27

Consensus median, pg/g 25Median all values pg/g 25Consensus mean, pg/g 25Standard deviation, pg/g 2.1Relative standard deviation, % 8No. of values reported 34No. of values removed 0No. of reported non-detects 0

Analyte solutionCongener: PBDE 28

Consenus statistics

Page 72:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-2.356

2.644

7.644

12.644

17.644

22.644

27.644

32.644

37.6442 4 5 8 18 23 24 26 28 33 35 38 40 42 44 46 48 49 53 58 59 73 75 77 87 90 92 94 97 103

106

107

112

117

pg/g

fw

Labcode

PBDE 28

-5-4-3-2-1012345

24 46 5 58 8 38 28 106 87 23 59 18 2 75 48 90 92 42 112 77 4

107 40 94 33 103 35 44 73 26 97 117 53 49

Labcode

Z-score: PBDE 28

Page 73:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes2 234 265 288 2318 2423 2524 2126 2428 2233 2335 2538 2240 2542 2544 2546 2448 2449 2653 2858 2459 2273 2575 2477 2487 2390 2392 2594 2397 24

103 23106 24107 25112 25117 23

Consensus median, pg/g 24Median all values pg/g 24Consensus mean, pg/g 24Standard deviation, pg/g 1.6Relative standard deviation, % 6No. of values reported 34No. of values removed 0No. of reported non-detects 0

Analyte solutionCongener: PBDE 47

Consenus statistics

Page 74:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-3.635

1.365

6.365

11.365

16.365

21.365

26.365

31.365

36.3652 4 5 8 18 23 24 26 28 33 35 38 40 42 44 46 48 49 53 58 59 73 75 77 87 90 92 94 97 103

106

107

112

117

pg/g

fw

Labcode

PBDE 47

-5-4-3-2-1012345

24 28 38 59 94 33 103 2 87 117 8 90 46 106 26 18 77 75 58 97 48 112 40 42 23 35 44 107 92 73 49 4 5 53

Labcode

Z-score: PBDE 47

Page 75:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes2 244 265 288 2118 2523 2424 2326 2528 2333 2635 2438 2440 2742 2544 2646 2348 2549 2653 2758 2459 2373 2675 2577 2487 2390 2392 2494 2597 24

103 25106 23107 24112 25117 21

Consensus median, pg/g 24Median all values pg/g 24Consensus mean, pg/g 24Standard deviation, pg/g 1.5Relative standard deviation, % 6No. of values reported 34No. of values removed 0No. of reported non-detects 0

Analyte solutionCongener: PBDE 99

Consenus statistics

Page 76:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-3.828

1.173

6.173

11.173

16.173

21.173

26.173

31.173

36.1732 4 5 8 18 23 24 26 28 33 35 38 40 42 44 46 48 49 53 58 59 73 75 77 87 90 92 94 97 103

106

107

112

117

pg/g

fw

Labcode

PBDE 99

-5-4-3-2-1012345

117 8 59 24 90 46 28 87 106 77 58 107 97 23 35 38 2 92 26 94 18 48 103 42 75 112 73 44 49 4 33 40 53 5

Labcode

Z-score: PBDE 99

Page 77:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes2 254 275 248 2318 2523 2424 2126 2328 2233 2435 2538 2540 2842 2644 2646 2148 2549 2653 2758 2459 2473 2775 2777 2587 2590 2592 2694 2597 22

103 25106 25107 26112 27117 24

Consensus median, pg/g 25Median all values pg/g 25Consensus mean, pg/g 25Standard deviation, pg/g 1.8Relative standard deviation, % 7No. of values reported 34No. of values removed 0No. of reported non-detects 0

Analyte solutionCongener: PBDE 100

Consenus statistics

Page 78:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-2.568

2.432

7.432

12.432

17.432

22.432

27.432

32.432

37.4322 4 5 8 18 23 24 26 28 33 35 38 40 42 44 46 48 49 53 58 59 73 75 77 87 90 92 94 97 103

106

107

112

117

pg/g

fw

Labcode

PBDE 100

-5-4-3-2-1012345

24 46 28 97 8 26 33 58 59 23 117 5 48 106 94 2 77 35 38 87 90 18 103 42 49 92 44 107 73 53 112 75 4 40

Labcode

Z-score: PBDE 100

Page 79:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes2 244 265 228 2318 2423 2224 2226 2328 2133 2335 2438 2340 2742 2544 2646 2248 2449 2453 2758 2259 2573 2575 2577 2487 2490 2492 2494 2497 24

103 25106 23107 23112 25117 25

Consensus median, pg/g 24Median all values pg/g 24Consensus mean, pg/g 24Standard deviation, pg/g 1.4Relative standard deviation, % 6No. of values reported 34No. of values removed 0No. of reported non-detects 0

Analyte solutionCongener: PBDE 153

Consenus statistics

Page 80:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-3.933

1.068

6.068

11.068

16.068

21.068

26.068

31.068

36.0682 4 5 8 18 23 24 26 28 33 35 38 40 42 44 46 48 49 53 58 59 73 75 77 87 90 92 94 97 103

106

107

112

117

pg/g

fw

Labcode

PBDE 153

-5-4-3-2-1012345

28 58 23 24 46 5

107

106 33 26 38 8 49 87 77 18 35 92 2 90 94 97 48 59 112 42 73 117

103 75 4 44 53 40

Labcode

Z-score: PBDE 153

Page 81:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes2 234 265 288 2318 2523 2224 2226 2328 2333 2635 2538 2340 2542 2144 2446 2448 2649 2553 2858 2459 2273 2475 2577 2587 2690 2292 2594 2397 25

103 23106 23107 24112 26117 25

Consensus median, pg/g 24Median all values pg/g 24Consensus mean, pg/g 24Standard deviation, pg/g 1.6Relative standard deviation, % 7No. of values reported 34No. of values removed 0No. of reported non-detects 0

Analyte solutionCongener: PBDE 154

Consenus statistics

Page 82:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-3.617

1.383

6.383

11.383

16.383

21.383

26.383

31.383

36.3832 4 5 8 18 23 24 26 28 33 35 38 40 42 44 46 48 49 53 58 59 73 75 77 87 90 92 94 97 103

106

107

112

117

pg/g

fw

Labcode

PBDE 154

-5-4-3-2-1012345

42 59 24 23 90 8

106 38 28 103 2 26 94 73 44 46 107 58 18 97 75 92 77 35 40 117 49 33 4 48 112 87 53 5

Labcode

Z-score: PBDE 154

Page 83:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes2 234 235 278 2018 2423 2224 1926 2728 2033 2235 2338 2240 2742 2444 2646 2148 2449 2453 2558 2259 2373 2475 2477 2587 2490 2392 2694 2597 24

103 25106 22107 24112 26117 22

Consensus median, pg/g 24Median all values pg/g 24Consensus mean, pg/g 24Standard deviation, pg/g 1.9Relative standard deviation, % 8No. of values reported 34No. of values removed 0No. of reported non-detects 0

Analyte solutionCongener: PBDE 183

Consenus statistics

Page 84:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-3.903

1.098

6.098

11.098

16.098

21.098

26.098

31.098

36.0982 4 5 8 18 23 24 26 28 33 35 38 40 42 44 46 48 49 53 58 59 73 75 77 87 90 92 94 97 103

106

107

112

117

pg/g

fw

Labcode

PBDE 183

-5-4-3-2-1012345

24 8 28 46 33 23 38 117 58 106 59 4 35 90 2 48 107 18 49 87 97 42 75 73 94 103 77 53 112 44 92 40 26 5

Labcode

Z-score: PBDE 183

Page 85:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes2 984 985 958 8618 9523 9024 9733 9435 8840 9042 8944 10048 9749 9758 10459 9477 10887 12690 10492 9994 11397 90

103 102106 91112 95

Consensus median, pg/g 97Median all values pg/g 97Consensus mean, pg/g 98Standard deviation, pg/g 8.7Relative standard deviation, % 9No. of values reported 25No. of values removed 0No. of reported non-detects 0

Analyte solutionCongener: PBDE 209

Consenus statistics

Page 86:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-15.100

4.900

24.900

44.900

64.900

84.900

104.900

124.900

144.9002 4 5 8 18 23 24 33 35 40 42 44 48 49 58 59 77 87 90 92 94 97 103

106

112

pg/g

fw

Labcode

PBDE 209

-5-4-3-2-1012345

8 35 42 40 23 97 106 59 33 18 112 5 24 48 49 4 2 92 44 103 58 90 77 94 87

Labcode

Z-score: PBDE 209

Page 87:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes5 52718 58424 50241 58642 48544 49048 50173 246 Outlier75 43887 50592 45594 45997 449

114 499

Consensus median, pg/g 499Median all values pg/g 494Consensus mean, pg/g 498Standard deviation, pg/g 46Relative standard deviation, % 9No. of values reported 14No. of values removed 1No. of reported non-detects 0

Analyte solutionCongener: α-HBCD

Consenus statistics

Page 88:  · Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes Lab code Conc. pg/g fw. Notes 1 20 Outlier 59 2.1 2 1.9 61 2.1 3 2.0 62 2.1 4 2.0 65 1.9 5 2.0 66 2.1 6 2.4 68 1.8

-58.500

41.500

141.500

241.500

341.500

441.500

541.500

641.500

741.5005 18 24 41 42 44 48 73 75 87 92 94 97 114

pg/g

fw

Labcode

α-HBCD

-5-4-3-2-1012345

73 75 97 92 94 42 44 114 48 24 87 5 18 41

Labcode

Z-score: α-HBCD