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LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt , K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational Wave Detection LIGO Science Collaboration (LSC) Meeting Joint Meeting of Optics and Suspension Working Groups LIGO Hanford Observatory, March 22, 2006 Ke-Xun Sun, Patrick Lu, and Robert Byer Stanford University

LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

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Page 1: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

1LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Progress in Grating Optical Sensorsfor Gravitational Wave Detection

LIGO Science Collaboration (LSC) MeetingJoint Meeting of Optics and Suspension Working Groups

LIGO Hanford Observatory, March 22, 2006

Ke-Xun Sun, Patrick Lu, and Robert Byer Stanford University

Page 2: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

2LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Grating Angular Sensor

GratingQuad

Detector

No Transmissive Optics Components: Enhanced Thermal Stability No Additional Optics: Enhanced Signal Integrity

•Grating angular sensor

– Grating can magnify the angle without using a telescope

– Grating can compress the beam cross section without using a focusing lens

– Simultaneously extract pure rotational and displacement signal

– Compact size with short working distance (5cm in lab test)

– No optics between the reflection surface and the quad photodiode

•More stable?5 cm

5-port Grating Configuration

Page 3: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

3LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Possible LIGO Installations Options

Intermediate test mass

Or suspension point interferometer

Back of the high reflectors

Main test massTilted Illumination

Page 4: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

4LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Grating Based Angular SensorDiffractive Angular Interferometry

)1(out )1(

out

Laser Beam

)1(out

)1(out

in

md inm sinsin

Page 5: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

5LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Overall Enhancement of Angular Sensitivity

0 10 20 30 40 50 60 70 80 90100

101

102

103

Diffraction Angle of +1 Order [degree]

Enh

ance

men

t of

A

ngul

ar S

ensi

tivity

• Grating angle amplification

2cos( )

'cos( )

inm in

m

P K P

• Beam cross section compression

K. Sun, S. Buchman, and R. L. Byer, “Grating Angle Magnification Enhanced Angular and Integrated Sensors for LISA Applications,” accepted for publication at J. Phys. C. Special issue of Almadi 6 Conference on Gravitational Waves

Page 6: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

6LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Grating Design Configuration

• Normal incidence

• TM mode (E-vector perpendicular to grove directions

• Density 933~935 lines/mm

• Wavelength 1064 nm

Page 7: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

7LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Grating Profile and Diffraction Efficiency

• Holographic grating• Sinusoidal profile• Density 933~935 lines/mm• Wavelength 1064 nm

Order # Eff. Eff.(TM) Phase TM, degAmpl.TM Diffr. angle, degAz. angle, degPolariz. angle, deg1 0.29809 0.29809 96.26951 1.722202 84.23187 0 900 0.365359 0.365359 128.0311 0.604449 0 0 90

-1 0.29809 0.29809 31.32713 1.722202 -84.2319 0 90

Effi ci ency of P20- 08 wi th AOI , 935l i nes/ mm, wave: 1. 064um

0. 00000. 20000. 40000. 6000

0 20 40 60 80 100

AOI ( degrees)

Effici

ency

- 1 TM- 1 TE

Page 8: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

8LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Experimental Setup

Page 9: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

9LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Recent Grating Angular Sensing Experiment with Two Detectors

Custom Grating 935 lines/mm

NPRO

Quad Det.

Scope

S.A.

N-1 ~ -840

6 cm

Quad Det.

• Simple construction

• No extra optics

• No other uncertainty and noise

Page 10: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

10LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Angular Motion Control

PZTs

Excursion: ~0.5 m/100V

Page 11: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

11LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Signal Spectrum for 10 nm, 0.5 rad Angular Drive

• Differential drive of two PZTs with oscillatory voltages of opposite phase (~2V)

• PZT displacement 10 nm

• Grating rotation 0.5 rad

• SNR ~42 dB

• Noise floor level ~4 nrad

• Estimate of 3 dB SNR sensitivity: 8 nrad/Hz1/2

Page 12: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

12LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Grating Fabrication Approaches

• Electron-beam lithographic techniques for dielectric gratings

• Trans-Imprinting for metallic gratings– Transference of pattern from dielectric to gold coatings

via imprinting

• Focused Ion Beam– Using Ga+ ions to mill gold or dielectric directly

• Ion etcher (Collaboration with LLNL)• Laser machining

Page 13: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

13LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Dielectric grating fabrication (initial attempt)

• Similar to recipe on last slide, except that chrome is patterned with lift-off.

• Poor adhesion between resist and quartz lead to inaccurate liftoff

• Surface roughness from non-optimized gas concentrations

Page 14: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

14LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Dielectric grating fabrication

• Approach: fabricate gratings in dielectrics first, then transfer them to the proof mass materials.

• Use e-beam litho because of its flexibility compared to other methods

– Flexibility needed when making 2d patterns

Quartz wafer

Cr evap

ZEP spin

Pattern ZEP

RIE Cr

RIE quartz

Page 15: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

15LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Dielectric Grating Fabrication - improved results -

• High quality dielectric grating fabricated with proper height (as confirmed by AFM and SEM inspection).

• Cross-sectional view confirms rectangular profile. SEM cross-section

AFM Measurement

E-beam resist, exposed and developed

Page 16: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

16LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Trans-Imprinting Trial Successful

• Initial trial succeeded in making a grating pattern in gold.

• Performed at 1 GPa • Using cited numbers of

250 MPa yield stress, required force for 2mmx2mm grating is 113 lbs.

• SEM shows the grain boundaries of the gold.

• Still remains to be determined how much force proof mass can sustain.

Page 17: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

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Focused Ion Beam

• As proof of principle, milled 1μm lines with Ga+

ions

• Used FEI Strata 235DB dual-beam FIB/SEM

• 3000pA and 20,000pA apertures used.

• Smaller current produced more accurate lines

• An estimated 5.6 hours for 1mmx1mm grating

• Improvements in the future:– Dose optimization for

depth control– Finer steering of ion beam

3000 pA, punched completely through gold layer

20,000 pA, jagged edges

Page 18: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

18LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Focused Ion Beam Etching Getting Real

• Optimizations in – Beam current

– Pixel size

– Etching time

• Has a hope to be a viable way of grating fabrication for sensor applications

Page 19: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

19LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Grating by Trans-Imprinting

• Grating on Au can be directly imprinted using quartz dielectric grating

• Grating on Au coated W substrate (may have LISA applications)

Page 20: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

20LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Collaboration on Diffractive Optics with Lawrence Livermore National Laboratory

Collaborative Research Highlight • LLNL is the primary center of design

and fabrication of high quality dielectric gratings due to NIF application

• The Stanford/LLNL collaboration strongly favors Stanford research– LLNL will supply high quality

dielectric gratings to Stanford LIGO and LISA programs

– LLNL sponsors a Stanford graduate student

– Stanford will characterize gratings for LLNL, LIGO and LISA applications, and provide data to LLNL

Page 21: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

21LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

JPL DRDF ProgramSponsored Research Highlight

– Grating angular sensor is the subject, supporting a full time grad student– Program execution

• Majority of the deliverables made within only six months • Spending rate is on target

– Excellent progresses in achieving deliverables• Diffraction orders at large diffraction angle demonstrated• Specialty 935 lines/mm gratings design verified• Angular sensitivity reaches 4 nrad/Hz1/2, far better than requirement of 100

nrad/Hz1/2

• Dielectric grating fabrication succeeded• Feasibility of grating marks on Au surface demonstrated with a variety of

methods

– Publications• First paper accepted for publication at JPCS

– “Grating angle magnification enhanced angular sensor”

• Submissions scheduled for LISA 6th Symposium

Page 22: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

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Conclusion

• Compact angular sensors for possible LIGO interferometer control applications

• Two-sided detection scheme will provide pure rotation measurement

• Lithographic Techniques for dielectric gratings– High quality dielectric gratings fabricated

• Imprinting– Demonstrated viable grating transfer process

• Focused Ion Beam– Proved feasibility of patterning grating on gold surface

Page 23: LSC Meeting LIGO Hanford March 19-23, 2006 1 LIGO_LSC_Sun_Grating_060322v2.ppt, K. Sun LIGO-G050142-00-Z Progress in Grating Optical Sensors for Gravitational

LSC Meeting LIGO Hanford March 19-23, 2006

23LIGO_LSC_Sun_Grating_060322v2.ppt, K. SunLIGO-G050142-00-Z

Acknowledgements

• Support for this project comes from – NSF LIGO for gravitational wave detection

– JPL DRDF for precision angular sensing