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Department of State Division of Publications 312 Rosa L. Parks, 8th Floor Snodgrass/TN Tower Nashville, TN 37243 Phone: 615.741.2650
For Department of State Use Only
Sequence Number: o o ·-\e. ~ \ S Notice ID(s): 2 ~ o"'\
Fax: 615.741.5133 , Email: [email protected]
File Date: .3 - \ (c ~ I 5
Notice of Rulemaking Hearing Hearings will be conducted in the manner prescribed by the Uniform Administrative Procedures Act, T. C.A. § 4-5-204. For questions and copies of the notice, contact the person listed below.
: Agency/Board/Commission: Environment and Conservation
Division: Solid Waste Management
Contact Person: David Moran William R. Snodgrass Tn Tower 312 Rosa L. Parks Avenue, 141
h Floor Address: Nashville, Tennessee 37243
Phone: (615) 532-0875
Email: [email protected]
Any Individuals with disabilities who wish to participate in these proceedings (to review these filings) and may require aid to facilitate such participation should contact the following at least 10 days prior to the hearing:
ADA Contact: ADA Coordinator William R. Snodgrass Tn Tower 312 Rosa L. Parks Avenue, 2nd Floor
Address: Nashville, Tennessee 37243 1-866-253-5827 (toll free) or (615) 532-0200
Phone: Hearing impaired callers may use the TN Relay Service at 1-800-848-0298.
Email: [email protected]
Hearing Location(s) (for additional locations, copy and paste table)
~---Address 1:--Conferenc~Roo_!!lM, 3rd Floor ----------------------
-----~-----------
Address 2: William R. Snodgrass Tenness ee Tower 312 Rosa L. Parks Avenue
Citl': Nashville, Tennessee ZiQ: I 37243
Hearing Date:] 05/19/15 Hearing Time: I 9:00 a.m. I X CST/CDT EST/EDT L_l ~----~---------
Additional Hearing Information:
This rulemaking is designed to: • Correct a typographical error to the process description to K1 07 • Add a common chemical name 1,1, 1-Trichloroethane to the U226 list of commercial chemical products.
This is not a new listing. • Update the regulatory language regarding the exclusion of comparable fuel and syngas fuel to be
equivalent with EPA's language. • Correct the introductory statements Rule 0400-12-01-.1 0(1 )(g)2(iv) so that it reads like the federal
language and to add a sentence to the certification statements to reference T.C.A. § 39-16-702(a)(4). • For the Waste code K161 of the Table 'Treatment Standards for Hazardous Wastes" in Rule 0400-12-01-
.10, delete the CAS number "137-30-4" in the third column to the right of "Dithiocarbamates (total) 10" and __________ _r~Qia_~i ng _ _!Lwith_'~~-~~-~-J_Ilat_Lt_l~_c;<:>_r1~i§i_tE3_rll_,._,itt1Jhe fed er_9!_!§ _ _rl_g__I,J_§_g_E3_.__ ___________________________________ _ SS-7037 (October 2011) RDA 1693
1
An initial set of draft rules has been prepared for public review and comment. Copies of these initial draft rules are available for review at the Tennessee Department of Environment and Conservation's (TDEC's) Environmental Field Offices located as follows:
Memphis Environmental Field Office 8383 Wolfe Lake Drive Bartlett, TN 38133 (901) 371-3000/ (901) 371-3170
Jackson Environmental Field Office 1625 Hollywood Drive Jackson, TN 38305 (731) 512-1300/1-888-891-8332
Columbia Environmental Field Office 1421 Hampshire Pike Columbia, TN 38401 (931) 380-3371/ 1-888-891-8332
Nashville Environmental Field Office 711 R. S. Gass Blvd. Nashville, TN 37216 (615) 687-7000/1-888-891-8332
Cookeville Environmental Field Office 1221 South Willow Avenue Cookeville, TN 38506 (931) 432-4015/1-888-891-8332
Chattanooga Environmental Field Office 1301 Riverfront Parkway Suite 206 Chattanooga,TN 37402 ( 423) 634-57 45/1-888-891-8332
Knoxville Environmental Field Office 3711 Middlebrook Pike Knoxville, TN 37921-5602 (865) 594-6035/1-888-891-8332
Johnson City Environmental Field Office 2305 Silverdale Road Johnson City, TN 37601-2162 ( 423) 854-5400/1-888-891-8332
The "DRAFT" rules may also be accessed for review using at http://tn.gov/environment/ppo/#swm.
Draft copies are also available for review at the Nashville Central Office (see address below).
Tennessee Department of Environment and Conservation Division of Solid Waste Management
William R. Snodgrass Tn Tower 312 Rosa L. Parks Avenue, 14th Floor
Nashville, Tennessee 37243 (615) 532-0780
Office hours are from 8:00AM to 4:30 PM, Monday through Friday (excluding holidays).
Oral or written comments are invited at the hearing. In addition, written comments may be submitted prior to or after the public hearing to: Tennessee Department of Environment and Conservation, Division of Solid Waste Management; Attention: David Moran, William R. Snodgrass Tn Tower, 312 Rosa L. Parks Avenue, 14th Floor, Nashville, Tennessee 37243; telephone 615-532-0875 or fax 615-532-0886. However, such written comments must be received by 4:30 PM CST, May 19, 2015, in order to assure consideration. For further information,
lease contact David Moran at the above address or telephone number orb~ ~-mail at [email protected].
Revision Type (check all that apply): X Amendment
New __ Repeal
SS-7037 (October 2011) RDA 1693 2
Rule(s) (ALL chapters and rules contained in filing must be listed. If needed, copy and paste additional tables to accommodate more than one chapter. Please enter only ONE Rule Number/Rule Title per row.)
_ Chapte!_~~!!'Jler ___ Cha_p.__t--,e~r~T~it:--cle-=--~c-::--0400-12-Qj______ Hazardous Waste Mana_gement Rule Number Rule Title
""-----t--:-=-:c~~'-------:-:-:-c~--~~-··- -:-:--- ""-~""--~----
04_0_0-_1~2~-~0_1-_:_02__ Identification and Listing of Hazardous Waste _ ~~~~~ 0400-12-01-.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste
-"-~- Treatment, Storage, and Disposal Fa~Bities ---~~~-----~~~-0400-12-01-.10 I Land Disposal Restrictions
---'-'~~-
SS-7037 (October 2011) RDA 1693 3
(Place substance of rules and other info here. Statutory authority must be given for each rule change. For information on formatting rules go to'-'-'-'-"-"-'-='-'-"-'-"-'-'-='-=="-'-"'"-="-'-'=.;"'-'-'~~"-'-'-'
Amendments
Chapter 0400-12-01 Hazardous Waste Management
Part 1 of subparagraph (c) of paragraph (4) of Rule 0400-12-01-.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following:
Industry and Hazardous
Waste Code
Wood preservation:
K001
Inorganic pigments:
K002
K003
K004
K005
K006
K007
K008
Organic chemicals:
K009
K010
K011
K013
K014
1. The following solid wastes are listed hazardous wastes from specific sources unless they are excluded under subparagraphs (a) and (c) of Rule 0400-12-01-.01 (3) and listed in paragraph (5) Appendix IX of this rule.
Hazardous Waste
Bottom sediment sludge from the treatment of wastewaters from wood preserving processes that use creosote and/or pentachlorophenol.
Wastewater treatment sludge from the production of chrome yellow and orange pigments.
Wastewater treatment sludge from the production of molybdate orange pigments.
Wastewater treatment sludge from the production of zinc yellow pigments.
Wastewater treatment sludge from the production of chrome green pigments.
Wastewater treatment sludge from the production of chrome oxide green pigments (anhydrous and hydrated).
Wastewater treatment sludge from the production of iron blue pigments.
Oven residue from the production of chrome oxide green pigments.
Distillation bottoms from the production of acetaldehyde from ethylene.
Distillation side cuts from the production of acetaldehyde from ethylene.
Bottom stream from the wastewater stripper in the production of acrylonitrile.
Bottom stream from the acetonitrile column in the production of acrylonitrile.
Bottoms from the acetonitrile purification column in the production of acrylonitrile.
Hazard Code
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(R, T)
(R, T)
(T)
SS-7037 (October 2011) 4
RDA 1693
K015
K016
K017
K018
K019
K020
K021
K022
K023
K024
K025
K026
K027
K028
K029
K030
K083
K085
K093
K094
K095
K096
K103
K104
K105
Still bottoms from the distillation of benzyl chloride.
Heavy ends or distillation residues from the production of carbon tetrachloride.
Heavy ends (still bottoms) from the purification column in the production of epichlorohydrin.
Heavy ends from the fractionation column in ethyl chloride production.
Heavy ends from the distillation of ethylene dichloride in ethylene dichloride production.
Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer production.
Aqueous spent antimony catalyst waste from fluoromethanes production.
Distillation bottom tars from the production of phenol/acetone from cumene.
Distillation light ends from the production of phthalic anhydride from naphthalene.
Distillation bottoms from the production of phthalic anhydride from naphthalene.
Distillation bottoms from the production of nitrobenzene by the nitration of benzene.
Stripping still tails from the production of methyl ethyl pyridines.
Centrifuge and distillation residues from toluene diisocyanate production.
Spent catalyst from the hydrochlorinator reactor in the production of 1,1, 1-trichloroethane.
Waste from the product steam stripper in the production of 1,1, 1-trichloroethane.
' Column bottoms or heavy ends from the combined production of trichloroethylene and perchloroethylene.
Distillation bottoms from aniline production.
Distillation or fractionation column bottoms from the production of chlorobenzenes.
Distillation light ends from the production of phthalic anhydride from ortho-xylene.
Distillation bottoms from the production of phthalic anhydride from ortho-xylene.
Distillation bottoms from the production of 1,1, 1-trichloroethane.
Heavy ends from the heavy ends column from the production of 1,1, 1-trichloroethane.
Process residues from aniline extraction from the production of aniline.
Combined wastewater streams generated from nitrobenzene/aniline production.
Separated aqueous stream from the reactor product washing step in the production of chlorobenzenes.
SS-7037 (October 2011) 5
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(R, T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
RDA 1693
K107
K108
K109
K110
K111
K112
K113
K114
K115
K116
K117
K118
K136
K149
K150
K151
K156
Column bottoms from product separation from the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.
Condensed column overheads from product separation and condensed reactor vent gases from the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.
Spent filter cartridges from product purification from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.
Condensed column overheads from intermediate separation from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.
Product washwaters from the production of dinitrotoluene via nitration of toluene.
Reaction by-product water from the drying column in the production of toluenediamine via hydrogenation of dinitrotoluene.
Condensed liquid light ends from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.
Vicinals from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.
Heavy ends from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.
Organic condensate from the solvent recovery column in the production of toluene diisocyanate via phosgenation of toluenediamine.
Wastewater from the reactor vent gas scrubber in the production of ethylene dibromide via bromination of ethene.
Spent adsorbent solids from purification of ethylene dibromide in the production of ethylene dibromide via bromination of ethene.
Still bottoms from the purification of ethylene dibromide in the production of ethylene dibromide via bromination of ethene.
Distillation bottoms from the production of alpha- (or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups, (This waste does not include still bottoms from the distillation of benzyl chloride.).
Organic residuals, excluding spent carbon adsorbent, from the spent chlorine gas and hydrochloric acid recovery processes associated with the production of alpha- (or methyl-) chlorinated toluenes, ringchlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups.
Wastewater treatment sludges, excluding neutralization and biological sludges, generated during the treatment of wastewaters from the production of alpha-(or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups.
Organic waste (including heavy ends, still bottoms, light ends, spent solvents, filtrates, and decantates) from the production of carbamates and carbamoyl oximes. (This listing does not apply to wastes generated 'from the manufacture of 3-iodo-2-propynyl n-butylcarbamate.)
SS-7037 (October2011) 6
(C,T)
(I,T)
(T)
(T)
(C,T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
RDA 1693
K157
K158
K159
K161
K174
K175
Wastewaters (including scrubber waters, condenser waters, washwaters, and separation waters) from the production of carbamates and carbamoyl bximes. (This listing does not apply to wastes generated from the manufacture of 3-iodo-2-propynyl nbutylcarbamate.)
Bag house dusts and filter/separation solids from the production of carbamates and carbamoyl oximes. (This listing does not apply to wastes generated from the manufacture of 3-iodo-2-propynyl nbutylcarbamate.).
Organics from the treatment of thiocarbamate wastes
Purification solids (including filtration, evaporation, and centrifugation solids), bag house dust and floor sweepings from the production of dithiocarbamate acids and their salts. (This listing does not include K125 or K126.)
Wastewater treatment sludges from the production of ethylene dichloride or vinyl chloride monomer (including sludges that result from commingled ethylene dichloride or vinyl chloride monomer wastewater and other wastewater), unless the sludges meet the following conditions: (i) they are disposed of in a Subtitle C or nonhazardous landfill licensed or permitted by the state or federal government; (ii) they are not otherwise placed on the land prior to final disposal; and (iii) the generator maintains documentation demonstrating that the waste was either disposed of in an on-site landfill or consigned to a transporter or disposal facility that provided a written commitment to dispose of the waste in an off-site landfill. Respondents in any action brought to enforce the requirements of Subtitle C must, upon a showing by the government that the respondent managed wastewater treatment sludges from the production of vinyl chloride monomer or ethylene dichloride, demonstrate that they meet the terms of the exclusion set forth above. In doing so, they must provide appropriate documentation (e.g., contracts between the generator and the landfill owner/operator, invoices documenting delivery of waste to landfill, etc.) that the terms of the exclusion were met.
Wastewater treatment sludges from the production of vinyl chloride monomer using mercuric chloride catalyst in an acetylene-based process.
SS-7037 (October 2011) 7
(T)
(T)
(T)
(R,T)
(T)
{T)
RDA 1693
K181
Inorganic chemicals:
K071
K073
K106
K176
K177
K178
Pesticides:
K031
K032
K033
K034
K035
Nonwastewaters from the production of dyes and/or pigments (including nonwastewaters commingled at the point of generation with nonwastewaters from other processes) that, at the point of generation, contain mass loadings of any of the constituents identified in part 3 of this subparagraph that are equal to or greater than the corresponding part 3 levels, as determined on a calendar year basis. These wastes will not be hazardous if the nonwastewaters are: (i) disposed in a Subtitle D landfill unit subject to the design criteria in 40 CFR 258.40, (ii) disposed in a Subtitle C landfill unit subject to either Rule 0400-12-01-.06(14)(b) or Rule 0400-12-01-.05(14)(b); (iii) disposed in other Subtitle D landfill units that meet the design criteria in 40 CFR 258.40, Rule 0400-12-01-.06(14)(b), or Rule 0400-12-01-.05(14)(b); or (iv) treated in a combustion unit that is permitted under Subtitle C, or an onsite combustion unit that is permitted under the Clean Air Act. For the purposes of this listing, dyes and/or pigments production is defined in subpart 2(i) of this subparagraph. Part 4 of this subparagraph describes the process for demonstrating that a facility's nonwastewaters are not K181. This listing does not apply to wastes that are otherwise identified as hazardous under subparagraphs (b) through (e) of paragraph (3) of this rule and subparagraphs (b) through (d) of paragraph (4) of this rule at the point of generation. Also, the listing does not apply to wastes generated before any annual mass loading limit is met.
Brine purification muds from the mercury cell process in chlorine production, where separately prepurified brine is not used.
Chlorinated hydrocarbon waste from the purification step of the diaphragm cell process using graphite anodes in chlorine production.
Wastewater treatment sludge from the mercury cell process in chlorine production.
Baghouse filters from the production of antimony oxide, including filters from the production of intermediates (e. g., antimony metal or crude antimony oxide).
Slag from the production of antimony oxide that is speculatively accumulated or disposed, including slag from the production of intermediates (e. g., antimony metal or crude antimony oxide).
Residues from manufacturing and manufacturing-site storage of ferric chloride from acids formed during the production of titanium dioxide using the chloride-ilmenite process.
By-product salts generated in the production of MSMA and cacodylic acid.
Wastewater treatment sludge from the production of chlordane.
Wastewater and scrub water from the chlorination of cyclopentadiene in the production of chlordane.
Filter solids from the filtration of hexachlorocyclopentadiene in the production of chlordane.
Wastewater treatment sludges generated in the production of creosote.
SS-7037 (October 2011) 8
(T)
(T)
(T)
(T)
(E)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
RDA 1693
K036
K037
K038
K039
K040
K041
K042
K043
K097
K098
K099
K123
K124
K125
K126
K131
K132
Explosives:
K044
K045
K046
K047
Petroleum refining:
K048
K049
KOSO
K051
K052
Still bottoms from toluene reclamation distillation in the production of disulfoton.
Wastewater treatment sludges from the production of disulfoton.
Wastewater from the washing and stripping of phorate production.
Filter cake from the filtration of diethylphosphorodithioic acid in the production of phorate.
Wastewater treatment sludge from the production of phorate.
Wastewater treatment sludge from the production of toxaphene.
Heavy ends or distillation residues from the distillation of tetrachlorobenzene in the production of 2,4,5-T.
2,6-Dichlorophenol waste from the production of 2,4-D.
Vacuum stripper discharge from the chlordane chlorinator in the production of chlordane.
Untreated process wastewater from the production of toxaphene.
Untreated wastewater from the production of 2,4-D.
Process wastewater (including supernates, filtrates, and washwaters) from the production of ethylenebisdithiocarbamic acid and its salt.
Reactor vent scrubber water from the production of ethylenebisdithiocarbamic acid and its salts.
Filtration, evaporation, and centrifugation solids from the production of ethylenebisdithiocarbamic acid and its salts.
Baghouse dust and floor sweepings in milling and packaging operations from the production or formulation of ethylenebisdithiocarbamic acid and its salts.
Wastewater from the reactor and spent sulfuric acid from the acid dryer from the production of methyl bromide.
Spent absorbent and wastewater separator solids from the production of methyl bromide.
Wastewater treatment sludges from the manufacturing and processing of explosives.
Spent carbon from the treatment of wastewater containing explosives.
Wastewater treatment sludges from the manufacturing, formulation and loading of lead-based initiating compounds.
Pink/red water from TNT operations.
Dissolved air flotation (OAF) float from the petroleum refining industry.
Slop oil emulsion solids from the petroleum refining industry.
Heat exchanger bundle cleaning sludge from the petroleum refining industry.
API separator sludge from the petroleum refining industry.
Tank bottoms (leaded) from the petroleum refining industry.
SS-7037 (October 2011) 9
(T)
(T}
(T}
(T}
(T}
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(C, T}
(T)
(T}
(C,T)
(T}
(R)
(R)
(T}
(R)
(T}
(T)
(T)
(T)
(T}
RDA 1693
K169
K170
K171
K172
Iron and steel:
K061
K062
Primary aluminum:
K088
Secondary lead:
K069
K100
Veterinary pharmaceuticals:
K084
K101
K102
Ink formulation:
K086
Crude oil storage tank sediment from petroleum refining operations.
Clarified slurry oil tank sediment and/or in-line filter/separation solids from petroleum refining operations.
Spent Hydrotreating catalyst from petroleum refining operations, including guard beds used to desulfurize feeds to other catalytic reactors (this listing does not include inert support media).
Spent Hydrorefining catalyst from petroleum refining operations, including guard beds used to desulfurize feeds to other catalytic reactors (this listing does not include inert support media).
Emission control dust/sludge from the primary production of steel in electric furnaces.
Spent pickle liquor generated by steel finishing operations of facilities within the iron and steel industry (SIC Codes 331 and 332).
Spent potliners from primary aluminum reduction.
Emission control dust/sludge from secondary lead smelting. (Note: This listing is stayed administratively for sludge generated from secondary acid scrubber systems. The stay will remain in effect until further administrative action is taken. If EPA takes further action effecting this stay, EPA will publish a notice of the action in the Federal Register).
Waste leaching solution from acid leaching of emission control dust/sludge from secondary lead smelting.
Wastewater treatment sludges generated during the production of veterinary pharmaceuticals from arsenic or organa-arsenic compounds.
Distillation tar residues from the distillation of aniline-based compounds in the production of veterinary pharmaceuticals from arsenic or organa-arsenic compounds.
Residue from the use of activated carbon for decolorization in the production of veterinary pharmaceuticals from arsenic or organaarsenic compounds.
Solvent washes and sludges, caustic washes and sludges, or water washes and sludges from cleaning tubs and equipment used in the formulation of ink from pigments, driers, soaps, and stabilizers containing chromium and lead.
SS-7037 (October 2011) 10
(T)
(T)
(I,T)
(I,T)
(T)
(C,T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
RDA 1693
Coking:
K060
K087
K141
K142
K143
K144
K145
K147
K148
Ammonia still lime sludge from coking operations.
Decanter tank tar sludge from coking operations.
Process residues from the recovery of coal tar, including, but not limited to, collecting sump residues from the production of coke from coal or the recovery of coke by-products produced from coal. This listing does not include K087 (decanter tank tar sludges from coking operations).
Tar storage tank residues from the production of coke from coal or from the recovery of coke by-products produced from coal.
Process residues from the recovery of light oil, including, but not limited to, those generated in stills, decanters, and wash oil recovery units from the recovery of coke by-products produced from coal.
Wastewater sump residues from light oil refining, including, but not limited to, intercepting or contamination sump sludges from the recovery of coke by-products produced from coal.
Residues from naphthalene collection and recovery operations from the recovery of coke by-products produced from coal.
Tar storage tank residues from coal tar refining.
Residues from coal tar distillation, including but not limited to, still bottoms.
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
(T)
Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq.
Part 6 of subparagraph (d) of paragraph (4) of Rule 0400-12-01-.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following:
Hazardous Waste No.
U394
U001
U034
U187
U005
U240
6. The commercial chemical products, manufacturing chemical intermediates, or offspecification commercial chemical products referred to in parts 1 through 4 of this subparagraph, are identified as toxic wastes (T), unless otherwise designated and are subject to the small quantity generator exclusion defined in parts (1)(e) 1 and 7 of this rule.
(Comment: For the convenience of the regulated community, the primary hazardous properties of these materials have been indicated by the letters T (Toxicity), R (Reactivity), I (lgnitability) and C (Corrosivity). Absence of a letter indicates that the compound is only listed for toxicity.)
These wastes and their corresponding Hazardous Waste Codes are:
Chemical Abstracts No.
30558-43-1
75-07-0
75-87-6
62-44-2
53-96-3
194-75-7
A2213.
Acetaldehyde (I)
Acetaldehyde, trichloro
Acetamide, N-(4-ethoxyphenyi)
Acetamide, N-9H-fluoren-2-yi-
Substance
Acetic acid, (2,4-dichlorophenoxy)-, salts & esters
SS-7037 (October 2011) 11
RDA 1693
U112 141-78-6 Acetic acid, ethyl ester (I)
U144 301-04-2 Acetic acid, lead{2+) salt
U214 563-68-8 Acetic acid, thallium{1 +)salt
see F027 93-76-5 Acetic acid, {2,4,5-trichlorophenoxy)-
U002 67-64-1 Acetone {I)
U003 75-05-8 Acetonitrile {I,T)
U004 98-86-2 Acetophenone
U005 53-96-3 2-Acetylaminofluorene
U006 75-36-5 Acetyl chloride (C,R,T)
U007 79-06-1 Acrylamide
U008 79-10-7 Acrylic acid {I)
U009 107-13-1 Acrylonitrile
U011 61-82-5 Amitrole
U012 62-53-3 Aniline {I,T)
U136 75-60-5 Arsinic acid, dimethyl-
U014 492-80-8 Auramine
U015 115-02-6 Azaserine
U010 50-07-7 Azirino[2',3':3,4]pyrrolo[1 ,2-a]indole-4,7-dione, 6-amino-8-([(aminocarbonyl)oxy]rnethyl]-1,1 a,2,8,8a,8b-hexahydro-8a-methoxy-5-methyl-, [1 aS-(1 aalpha, 8beta,8aalpha,8balpha)]-
U280 101-27-9 Barban.
U278 22781-23-3 Bendiocarb.
U364 22961-82-6 Bendiocarb phenol.
U271 17804-35-2 Benomyl.
U157 56-49-5 BenzU]aceanthrylene, 1 ,2-dihydro-3-methyl-
U016 225-51-4 Benz[c]acridine
U017 98-87-3 Benzal chloride
U192 23950-58-5 Benzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)-
U018 56-55-3 Benz[ a]anthracene
U094 57-97-6 Benz[a]anthracene, 7, 12-dimethyl-
U012 62-53-3 Benzenamine {I,T)
U014 492-80-8 Benzenamine, 4,4'-carbonimidoylbis[N,N-dimethyl-
U049 3165-93-3 Benzenamine, 4-chloro-2-methyl-, hydrochloride
U093 60-11-7 Benzenamine, N, N-dimethyl-4-(phenylazo )-
U328 95-53-4 Benzenamine, 2-methyl-
U353 106-49-0 Benzenamine, 4-methyl-
U158 101-14-4 Benzenamine, 4,4'-methylenebis[2-chloro-
U222 636-21-5 Benzenamine, 2-methyl-, hydrochloride
SS-7037 (October 2011) RDA 1693 12
U181 99-55-8
U019 71-43-2
U038 510-15-6
U030 101-55-3
U035 305-03-3
U037 108-90-7
U221 25376-45-8
U028 117-81-7
U069 84-74-2
U088 84-66-2
U102 131-11-3
U107 117-84-0
U070 95-50-1
U071 541-73-1
U072 106-46-7
U060 72-54-8
U017 98-87-3
U223 26471-62-5
U239 1330-20-7
U201 108-46-3
U127 118-74-1
U056 110-82-7
U220 108-88-3
U105 121-14-2
U106 606-20-2
U055 98-82-8
U169 98-95-3
U183 608-93-5
U185 82-68-8
U020 98-09-9
U020 98-09-9
U207 95-94-3
U061 50-29-3
U247 72-43-5
U023 98-07-7
U234 99-35-4
U021 92-87-5
U278 22781-23-3
SS-7037 (October 2011)
Benzenamine, 2-methyl-5-nitro
Benzene (I,T)
Benzeneacetic acid, 4-chloro-alpha-(4-chlorophenyl)-alpha-hydroxy-, ethyl ester
Benzene, 1-bromo-4-phenoxy-
Benzenebutanoic acid, 4-[bis(2-chloroethyl)amino]
Benzene, chloro-
Benzenediamine, ar-methyl-
1 ,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) ester
1 ,2-Benzenedicarboxylic acid, dibutyl ester
1 ,2-Benzenedicarboxylic acid, diethyl ester
1 ,2-Benzenedicarboxylic acid, dimethyl ester
1 ,2-Benzenedicarboxylic acid, dioctyl ester
Benzene, 1 ,2-dichloro-
Benzene, 1 ,3-dichloro-
Benzene, 1 A-dichloro-
Benzene, 1,1 '-(2,2-dichloroethylidene)bis[4-chloro
Benzene, (dichloromethyi)-
Benzene, 1 ,3-diisocyanatomethyl- (R,T)
Benzene, dimethyl- (I)
1 ,3-Benzenediol
Benzene, hexachloro-
Benzene, hexahydro- (I)
Benzene, methyl-
Benzene, 1-methyl-2,4-dinitro
Benzene, 2-methyl-1 ,3-dinitro
Benzene, (1-methylethyl)- (I)
Benzene, nitro-
Benzene, pentachloro-
Benzene, pentachloronitro
Benzenesulfonic acid chloride (C,R)
Benzenesulfonyl chloride (C,R)
Benzene, 1 ,2,4,5-tetrachloro-
Benzene, 1,1 '-(2,2,2-trichloroethylidene)bis[4-chloro
Benzene, 1,1 '-(2,2,2-trichloroethylidene)bis[4- methoxy
Benzene, (trichloromethyi)-
Benzene, 1 ,3,5-trinitro-
Benzidine
1 ,3-Benzodioxol-4-ol, 2,2-dimethyl-, methyl carbamate.
13 RDA 1693
U364 22961-82-6
U203 94-59-7
U141 120-58-1
U090 94-58-6
U367 1563-38-8
U064 189-55-9
U248 181-81-2
U022 50-32-8
U197 106-51-4
U023 98-07-7
U085 1464-53-5
U021 92-87-5
U073 91-94-1
U091 119-90-4
U095 119-93-7
U225 75-25-2
U030 101-55-3
U128 87-68-3
U172 924-16-3
U031 71-36-3
U159 78-93-3
U160 1338-23-4
U053 4170-30-3
U074 764-41-0
U143 303-34-4
U031 71-36-3
U136 75-60-5
U032 13765-19-0
U372 10605-21-7
U271 17804-35-2
U280 101-27-9
U238 51-79-6
U178 615-53-2
U373 122-42-9
U409 23564-05-8
U097 79-44-7
SS-7037 (October 2011)
1,3-Benzodioxol-4-ol, 2,2-dimethyl-,
1,3-Benzodioxole, 5-(2-propenyi)-
1,3-Benzodioxole, 5-(1-propenyi)-
1,3-Benzodioxole, 5-propyi-
7-Benzofuranol, 2,3-dihydro-2,2-dimethyi
Benzo[rst]pentaphene
2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-oxo-1-phenylbutyl)-, & salts, when present at concentrations of 0.3% or less
Benzo[a)pyrene
p-Benzoquinone
Benzotrichloride (C,R,T)
2,2'-Bioxirane
[1,1'-Biphenyl]-4,4'-diamine
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dichloro
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dimethoxy
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dimethyi
Bromoform
4-Bromophenyl phenyl ether
1,3-Butadiene, 1,1,2,3,4,4-hexachloro-
1-Butanamine, N-butyi-N-nitroso-
1-Butanol (I)
2-Butanone (I,T)
2-Butanone peroxide (R,T)
2-Butenal
2-Butene, 1 ,4-dichloro- (I,T)
2-Butenoic acid, 2-methyl-, 7 -[(2,3-dihydroxy- 2-( 1-methoxyethyl)-3-methyl-1-oxobutoxy]methyl)- 2,3,5,7a-tetrahydro-1 H-pyrrolizin-1-yl ester, [1 S-[1 alpha(Z),7(2S*,3R*),7aalpha))-
n-Butyl alcohol (I)
Cacodylic acid
Calcium chromate
Carbamic acid, 1 H-benzimidazol-2-yl, methyl ester.
Carbamic acid, [1-[(butylamino)carbonyl)-1 H-benzimidazol-2- yl)-, methyl ester.
Carbamic acid, (3-chlorophenyl)-, 4-chloro-2-butynyl ester.
Carbamic acid, ethyl ester
Carbamic acid, methylnitroso-, ethyl ester
Carbamic acid, phenyl-, 1-methylethyl ester.
Carbamic acid, [1,2-phenylenebis (iminocarbonothioyl)]bis-, dimethyl ester.
Carbamic chloride, dimethyl-
14 RDA 1693
U114 1111-54-6 Carbamodithioic acid, 1 ,2-ethanediylbis-, salts & esters
U062 2303-16-4 Carbamothioic acid, bis(1-methylethyl)-, S-(2,3-dichloro-2-propenyl) ester
U389 2303-17-5 Carbamothioic acid, bis(1-methylethyl)-, S-(2,3,3-trichloro-2-propenyl) ester.
U387 52888-80-9 Carbamothioic acid, dipropyl-, S-(phenylmethyl) ester.
U279 63-25-2 Carbaryl.
U372 10605-21-7 Carbendazim.
U367 1563-38-8 Carbofuran phenol.
U215 6533-73-9 Carbonic acid, dithallium(1+) salt
U033 353-50-4 Carbonic difluoride
U156 79-22-1 Carbonochloridic acid, methyl ester (I,T)
U033 353-50-4 Carbon oxyfluoride (R,T)
U211 56-23-5 Carbon tetrachloride
U034 75-87-6 Chloral
U035 305-03-3 Chlorambucil
U036 57-74-9 Chlordane, alpha & gamma isomers
U026 494-03-1 Chlornaphazin
U037 108-90-7 Chlorobenzene
U038 510-15-6 Chlorobenzilate
U039 59-50-7 p-Chloro-m-cresol
U042 110-75-8 2-Chloroethyl vinyl ether
U044 67-66-3 Chloroform
U046 107-30-2 Chloromethyl methyl ether
U047 91-58-7 beta-Chloronaphthalene
U048 95-57-8 a-Chlorophenol
U049 3165-93-3 4-Chloro-o-toluidine, hydrochloride
U032 13765-19-0 Chromic acid H2Cr04, calcium salt
U050 218-01-9 Chrysene
U051 Creosote
U052 1319-77-3 Cresol (Cresylic acid)
U053 4170-30-3 Crotonaldehyde
U055 98-82-8 Cumene (I)
U246 506-68-3 Cyanogen bromide (CN)Br
U197 106-51-4 2,5-Cyclohexadiene-1 ,4-dione
U056 110-82-7 Cyclohexane (I)
U129 58-89-9 Cyclohexane, 1 ,2,3,4,5,6-hexachloro-, (1 alpha,2alpha,3beta,4alpha,5alpha,6beta)-
U057 108-94-1 Cyclohexanone (I)
U130 77-47-4 1 ,3-Cyclopentadiene, 1 ,2,3,4,5,5-hexachloro-
U058 50-18-0 Cyclophosphamide
SS-7037 (October 2011) RDA 1693 15
U240 194-75-7 2,4-D, salts & esters
U059 20830-81-3 Daunomycin
U060 72-54-8 ODD
U061 50-29-3 DDT
U062 2303-16-4 Diallate
U063 53-70-3 Dibenz[a,h]anthracene
U064 189-55-9 Dibenzo[ a,i]pyrene
U066 96-12-8 1 ,2-Dibromo-3-chloropropane
U069 84-74-2 Dibutyl phthalate
U070 95-50-1 a-Dichlorobenzene
U071 541-73-1 m-Dichlorobenzene
U072 106-46-7 p-Dichlorobenzene
U073 91-94-1 3,3'-Dichlorobenzidine
U074 764-41-0 1 ,4-Dichloro-2-butene (I,T)
U075 75-71-8 Dichlorodifluoromethane
U078 75-35-4 1 , 1-Dichloroethylene
U079 156-60-5 1 ,2-Dichloroethylene
U025 111-44-4 Dichloroethyl ether
U027 108-60-1 Dichloroisopropyl ether
U024 111-91-1 Dichloromethoxy ethane
U081 120-83-2 2,4-Dichlorophenol
U082 87-65-0 2,6-Dichlorophenol
U084 542-75-6 1 ,3-Dichloropropene
U085 1464-53-5 1 ,2:3,4-Diepoxybutane (I,T)
U395 5952-26-1 Diethylene glycol, dicarbamate.
U108 123-91-1 1 ,4-Diethyleneoxide
U028 117-81-7 Diethylhexyl phthalate
U086 1615-80-1 N,N'-Diethylhydrazine
U087 3288-58-2 0,0-Diethyl S-methyl dithiophosphate
U088 84-66-2 Diethyl phthalate
U089 56-53-1 Diethylstilbesterol
U090 94-58-6 Dihydrosafrole
U091 119-90-4 3,3'-Dimethoxybenzidine
U092 124-40-3 Dimethylamine (I)
U093 60-11-7 p-Dimethylaminoazobenzene
U094 57-97-6 7, 12-Dimethylbenz[a]anthracene
U095 119-93-7 3,3'-Dimethylbenzidine
U096 80-15-9 alpha,alpha-Dimethylbenzylhydroperoxide (R)
SS-7037 (October 2011) RDA 1693 16
U097 79-44-7 Dimethylcarbamoyl chloride
U098 57-14-7 1, 1-Dimethylhydrazine
U099 540-73-8 1 ,2-Dimethylhydrazine
U101 105-67-9 2,4-Dimethylphenol
U102 131-11-3 Dimethyl phthalate
U103 77-78-1 Dimethyl sulfate
U105 121-14-2 2,4-Dinitrotoluene
U106 606-20-2 2,6-Dinitrotoluene
U107 117-84-0 Di-n-octyl phthalate
U108 123-91-1 1 ,4-Dioxane
U109 122-66-7 1 ,2-Diphenylhydrazine
U110 142-84-7 Dipropylamine (I)
U111 621-64-7 Di-n-propylnitrosamine
U041 106-89-8 Epichlorohydrin
U001 75-07-0 Ethanal (I)
U174 55-18-5 Ethanamine, N-ethyi-N-nitroso-
U404 121-44-8 Ethanamine, N,N-diethyl-
U155 91-80-5 1 ,2-Ethanediamine, N,N-dimethyi-N'-2-pyridinyi-N'-(2-thienylmethyl)-
U067 106-93-4 Ethane, 1 ,2-dibromo-
U076 75-34-3 Ethane, 1, 1-dichloro-
U077 107-06-2 Ethane, 1 ,2-dichloro-
U131 67-72-1 Ethane, hexachloro-
U024 111-91-1 Ethane, 1,1 '-[methylenebis(oxy)]bis[2-chloro-
U117 60-29-7 Ethane, 1,1 '-oxybis-(1)
U025 111-44-4 Ethane, 1,1 '-oxybis[2-chloro-
U184 76-01-7 Ethane, pentachloro-
U208 630-20-6 Ethane, 1,1, 1 ,2-tetrachloro-
U209 79-34-5 Ethane, 1,1 ,2,2-tetrachloro-
U218 62-55-5 Ethanethioamide
U226 71-55-6 Ethane, 1,1, 1-trichloro-
U227 79-00-5 Ethane, 1,1 ,2-trichloro-
U410 59669-26-0 Ethanimidothioic acid, N,N'- [thiobis[(methylimino)carbonyloxy]]bis-, dimethyl ester
U394 30558-43-1 Ethanimidothioic acid, 2-(dimethylamino)-N-hydroxy-2-oxo-, methyl ester.
U359 110-80-5 Ethanol, 2-ethoxy-
U173 1116-54-7 Ethanol, 2,2'-(nitrosoimino)bis-
U395 5952-26-1 Ethanol, 2,2'-oxybis-, dicarbamate.
U004 98-86-2 Ethanone, 1-phenyl-
U043 75-01-4 Ethene, chloro-
SS-7037 (October 2011) RDA 1693 17
U042 110-75-8 Ethene, (2-chloroethoxy)-
U078 75-35-4 Ethene, 1, 1-dichloro-
U079 156-60-5 Ethene, 1 ,2-dichloro-, (E)-
U210 127-18-4 Ethene, tetrachloro-
U228 79-01-6 Ethene, trichloro-
U112 141-78-6 Ethyl acetate (I)
U113 140-88-5 Ethyl acrylate (I)
U238 51-79-6 Ethyl carbamate (urethane)
U117 60-29-7 Ethyl ether (I)
U114 1111-54-6 Ethylenebisdithiocarbamic acid, salts & esters
U067 106-93-4 Ethylene dibromide
U077 107-06-2 Ethylene dichloride
U359 110-80-5 Ethylene glycol monoethyl ether
U115 75-21-8 Ethylene oxide (I,T)
U116 96-45-7 Ethylenethiourea
U076 75-34-3 Ethylidene dichloride
U118 97-63-2 Ethyl methacrylate
U119 62-50-0 Ethyl methanesulfonate
U120 206-44-0 Fluoranthene
U122 50-00-0 Formaldehyde
U123 64-18-6 Formic acid (C,T)
U124 110-00-9 Furan (I)
U125 98-01-1 2-Furancarboxaldehyde (I)
U147 108-31-6 2,5-Furandione
U213 109-99-9 Furan, tetrahydro-(1)
U125 98-01-1 Furfural (I)
U124 110-00-9 Furfuran (I)
U206 18883-66-4 Glucopyranose, 2-deoxy-2-(3-methyl-3-nitrosoureido )-, D-
U206 18883-66-4 D-Giucose, 2-deoxy-2-[[(methylnitrosoamino)- carbonyl]amino]-
U126 765-34-4 Glycidylaldehyde
U163 70-25-7 Guanidine, N-methyi-N'-nitro-N-nitroso-
U127 118-74-1 Hexachlorobenzene
U128 87-68-3 Hexachlorobutadiene
U130 77-47-4 Hexachlorocyclopentadiene
U131 67-72-1 Hexachloroethane
U132 70-30-4 Hexachlorophene
U243 1888-71-7 Hexachloropropene
U133 302-01-2 Hydrazine (R,T)
SS-7037 (October 2011) RDA 1693 18
U086 1615-80-1 Hydrazine, 1 ,2-diethyl-
U098 57-14-7 Hydrazine, 1, 1-dimethyl-
U099 540-73-8 Hydrazine, 1 ,2-dimethyl-
U109 122-66-7 Hydrazine, 1 ,2-diphenyl-
U134 7664-39-3 Hydrofluoric acid (C,T)
U134 7664-39-3 Hydrogen fluoride (C,T)
U135 7783-06-4 Hydrogen sulfide
U135 7783-06-4 Hydrogen sulfide H2S
U096 80-15-9 Hydroperoxide, 1-methyl-1-phenylethyl- (R)
U116 96-45-7 2-lmidazolidinethione
U137 193-39-5 lndeno[1 ,2,3-cd)pyrene
U190 85-44-9 1 ,3-lsobenzofurandione
U140 78-83-1 Isobutyl alcohol (I,T)
U141 120-58-1 lsosafrole
U142 143-50-0 Kepone
U143 303-34-4 Lasiocarpine
U144 301-04-2 Lead acetate
U146 1335-32-6 Lead, bis(acetato-O)tetrahydroxytri-
U145 7446-27-7 Lead phosphate
U146 1335-32-6 Lead subacetate
U129 58-89-9 Lindane
U163 70-25-7 MNNG
U147 108-31-6 Maleic anhydride
U148 123-33-1 Maleic hydrazide
U149 109-77-3 Malononitrile
U150 148-82-3 Melphalan
U151 7439-97-6 Mercury
U152 126-98-7 Methacrylonitrile (1, T)
U092 124-40-3 Methanamine, N-methyl- (I)
U029 74-83-9 Methane, bromo-
U045 74-87-3 Methane, chloro- (1, T)
U046 107-30-2 Methane, chloromethoxy-
U068 74-95-3 Methane, dibromo-
U080 75-09-2 Methane, dichloro-
U075 75-71-8 Methane, dichlorodifluoro-
U138 74-88-4 Methane, iodo-
U119 62-50-0 Methanesulfonic acid, ethyl ester
U211 56-23-5 Methane, tetrachloro-
SS-7037 (October 2011) RDA 1693 19
U153
U225
U044
U121
U036
U154
U155
U142
U247
U154
U029
U186
U045
U156
U226
U157
U158
U068
U080
U159
U160
U138
U161
U162
U161
U164
U010
U059
U167
U168
U026
U165
U047
U166
U236
U279
7 4-93-1 Methanethiol (I, T)
75-25-2 Methane, tribromo-
67-66-3 Methane, trichloro-
75-69-4 Methane, trichlorofluoro-
57-74-9 4,7-Methano-1 H-indene, 1 ,2,4,5,6,7 ,8,8-octachloro-2,3,3a,4,7,7a-hexahydro-
67 -56-1 Methanol (I)
91-80-5 Methapyrilene
143-50-0 1 ,3,4-Metheno-2H-cyclobuta[ cd]pentalen-2-one, 1,1 a,3,3a,4,5,5,5a,5b,6-decach lorooctahydro-
72-43-5 Methoxychlor
67-56-1 Methyl alcohol (I)
7 4-83-9 Methyl bromide
504-60-9 1-Methylbutadiene (I)
74-87-3 Methyl chloride (I,T)
79-22-1 Methyl chlorocarbonate (I,T)
71-55-6 Methyl chloroform
56-49-5 3-Methylcholanthrene
101-14-4 4,4'-Methylenebis(2-chloroanilin~)
7 4-95-3 Methylene bromide
75-09-2 Methylene chloride
78-93-3 Methyl ethyl ketone (MEK) (I,T)
1338-23-4 Methyl ethyl ketone peroxide (R,T)
7 4-88-4 Methyl iodide
108-10-1 Methyl isobutyl ketone (I)
80-62-6 Methyl methacrylate (I,T)
108-10-1 4-Methyl-2-pentanone (I)
56-04-2 Methylthiouracil
50-07-7 Mitomycin C
20830-81-3 5, 12-Naphthacenedione, 8-acetyl-1 0-[(3-amino-2,3,6-trideoxy)-alpha-L -lyxohexopyranosyl)oxy]-7,8,9, 1 0-tetrahydro-6,8, 11-trihydroxy-1-methoxy-, (88-cis)-
134-32-7 1-Naphthalenamine
91-59-8 2-Naphthalenamine
494-03-1 Naphthalenamine, N,N'-bis(2-chloroethyl)-
91-20-3 Naphthalene
91-58-7 Naphthalene, 2-chloro-
130-15-4 1 ,4-Naphthalenedione
72-57-1 2,7-Naphthalenedisulfonic acid, 3,3'-[(3,3'- dimethyl[1, 1 '-biphenyl]-4,4'-diyl)bis(azo)bis[5-amino-4-hydroxy]-, tetrasodium salt
63-25-2 1-Naphthalenol, methylcarbamate.
SS-7037 (October 2011) 20
RDA 1693
U166 130-15-4 1 A-Naphthoquinone
U167 134-32-7 alpha-Naphthylamine
U168 91-59-8 beta-Naphthylamine
U217 10102-45-1 Nitric acid, thallium(1+) salt
U169 98-95-3 Nitrobenzene (I,T)
U170 100-02-7 p-Nitrophenol
U171 79-46-9 2-Nitropropane (I,T)
U172 924-16-3 N-Nitrosodi-n-butylamine
U173 1116-54-7 N-Nitrosodiethanolamine
U174 55-18-5 N-Nitrosodiethylamine
U176 759-73-9 N-Nitroso-N-ethylurea
U177 684-93-5 N-Nitroso-N-methylurea
U178 615-53-2 N-Nitroso-N-methylurethane
U179 100-75-4 N-Nitrosopiperidine
U180 930-55-2 N-Nitrosopyrrolidine
U181 99-55-8 5-Nitro-o-toluidine
U193 1120-71-4 1 ,2-0xathiolane, 2,2-dioxide
U058 50-18-0 2H-1 ,3,2-0xazaphosphorin-2-amine, N,N-bis(2-chloroethyl)tetrahydro-, 2-oxide
U115 75-21-8 Oxirane (I,T)
U126 765-34-4 Oxiranecarboxyaldehyde
U041 106-89-8 Oxirane, (chloromethyl)-
U182 123-63-7 Paraldehyde
U183 608-93-5 Pentachlorobenzene
U184 76-01-7 Pentachloroethane
U185 82-68-8 Pentachloronitrobenzene (PCNB)
See F027 87-86-5 Pentachlorophenol
U161 108-10-1 Pentanol, 4-methyl-
U186 504-60-9 1 ,3-Pentadiene (I)
U187 62-44-2 Phenacetin
U188 108-95-2 Phenol
U048 95-57-8 Phenol, 2-chloro-
U039 59-50-7 Phenol, 4-chloro-3-methyl-
U081 120-83-2 Phenol, 2,4-dichloro-
U082 87-65-0 Phenol, 2,6-dichloro-
U089 56-53-1 Phenol, 4,4'-(1 ,2-diethyl-1 ,2-ethenediyl)bis-, (E)-
U101 105-67-9 Phenol, 2,4-dimethyl-
U052 1319-77-3 Phenol, methyl-
U132 70-30-4 Phenol, 2,2'-methylenebis[3,4,6-trichloro-
SS-7037 (October 2011) RDA 1693 21
U411 114-26-1 Phenol, 2-(1-methylethoxy)-, methylcarbamate.
U170 100-02-7 Phenol, 4-nitro-
See F027 87-86-5 Phenol, pentachloro-
See F027 58-90-2 Phenol, 2,3,4,6-tetrachloro-
See F027 95-95-4 Phenol, 2,4,5-trichloro-
See F027 88-06-2 Phenol, 2,4,6-trichloro-
U150 148-82-3 L -Phenylalanine, 4-[bis(2-chloroethyl)amino]-
U145 7446-27-7 Phosphoric acid, lead(2+) salt (2:3)
U087 3288-58-2 Phosphorodithioic acid, 0,0-diethyl S-methyl ester
U189 1314-80-3 Phosphorus sulfide (R)
U190 85-44-9 Phthalic anhydride
U191 109-06-8 2-Picoline
U179 100-75-4 Piperidine, 1-nitroso-
U192 23950-58-5 Pronamide
U194 107-10-8 1-Propanamine (I,T)
U111 621-64-7 1-Propanamine, N-nitroso-N-propyl-
U110 142-84-7 1-Propanamine, N-propyl- (I)
U066 96-12-8 Propane, 1 ,2-dibromo-3-chloro-
U083 78-87-5 Propane, 1 ,2-dichloro-
U149 109-77-3 Propanedinitrile
U171 79-46-9 Propane, 2-nitro- (I,T)
U027 108-60-1 Propane, 2,2'-oxybis[2-chloro-
U193 1120-71-4 1 ,3-Propane sultone
See F027 93-72-1 Propanoic acid, 2-(2,4,5-trichlorophenoxy)-
U235 126-72-7 1-Propanol, 2,3-dibromo-, phosphate (3:1)
U140 78-83-1 1-Propanol, 2-methyl- (I,T)
U002 67-64-1 2-Propanone (I)
U007 79-06-1 2-Propenamide
U084 542-75-6 1-Propene, 1 ,3-dichloro-
U243 1888-71-7 1-Propene, 1,1 ,2,3,3,3-hexachloro-
U009 107-13-1 2-Propenenitrile
U152 126-98-7 2-Propenenitrile, 2-methyl- (I,T)
U008 79-10-7 2-Propenoic acid (I)
U113 140-88-5 2-Propenoic acid, ethyl ester (I)
U118 97-63-2 2-Propenoic acid, 2-methyl-, ethyl ester
U162 80-62-6 2-Propenoic acid, 2-methyl-, methyl ester (I,T)
U373 122-42-9 Propham.
U411 114-26-1 Propoxur.
SS-7037 (October 2011) RDA 1693 22
U194 107-10-8 n-Propylamine (I,T)
U083 78-87-5 Propylene dichloride
U387 52888-80-9 Prosu lfocarb.
U148 123-33-1 3,6-Pyridazinedione, 1 ,2-dihydro-
U196 110-86-1 Pyridine
U191 109-06-8 Pyridine, 2-methyl-
U237 66-75-1 2,4-(1 H,3H)-Pyrimidinedione, 5-[bis(2- chloroethyl)amino]-
U164 56-04-2 4(1 H)-Pyrimidinone, 2,3-dihydro-6-methyl-2-thioxo-
U180 930-55-2 Pyrrolidine, 1-nitroso-
U200 50-55-5 Reserpine
U201 108-46-3 Resorcinol
U203 94-59-7 Safrole
U204 7783-00-8 Selenious acid
U204 7783-00-8 Selenium dioxide
U205 7488-56-4 Selenium sulfide
U205 7488-56-4 Selenium sulfide SeS2 (R,T)
U015 115-02-6 L-Serine, diazoacetate (ester)
See F027 93-72-1 Silvex (2,4,5-TP)
U206 18883-66-4 Streptozotocin
U103 77-78-1 Sulfuric acid, dimethyl ester
U189 1314-80-3 Sulfur phosphide (R)
See F027 93-76-5 2,4,5-T
U207 95-94-3 1 ,2,4,5-Tetrachlorobenzene
U208 630-20-6 1 , 1,1 ,2-Tetrachloroethane
U209 79-34-5 1,1 ,2,2-Tetrachloroethane
U210 127-18-4 Tetrachloroethylene
See F027 58-90-2 2,3,4,6-Tetrachlorophenol
U213 109-99-9 T etrahydrofuran (I)
U214 563-68-8 Thallium(!) acetate
U215 6533-73-9 Thallium(!) carbonate
U216 7791-12-0 Thallium(!) chloride
U216 7791-12-0 Thallium chloride TICI
U217 10102-45-1 Thallium(!) nitrate
U218 62-55-5 Thioacetamide
U410 59669-26-0 Thiodicarb.
U153 74-93-1 Thiomethanol (I,T)
U244 137-26-8 Thioperoxydicarbonic diamide [(H2N)C(S)]2S2, tetramethyl-
U409 23564-05-8 Th iophanate-methyl.
SS-7037 (October 2011) RDA 1693 23
U219 62-56-6 Thiourea
U244 137-26-8 Thiram
U220 108-88-3 Toluene
U221 25376-45-8 Toluenediamine
U223 26471-62-5 Toluene diisocyanate (R,T)
U328 95-53-4 o-Toluidine
U353 106-49-0 p-Toluidine
U222 636-21-5 a-Toluidine hydrochloride
U389 2303-17-5 Triallate.
U011 61-82-5 1 H-1 ,2,4-Triazol-3-amine
U226 71-55-6 1 , 1 , 1-Trichloroethane
U227 79-00-5 1,1 ,2-Trichloroethane
U228 79-01-6 Trichloroethylene
U121 75-69-4 Trichloromonofluoromethane
See F027 95-95-4 2,4,5-Trichlorophenol
See F027 88-06-2 2,4,6-Trichlorophenol
U404 121-44-8 Triethylamine.
U234 99-35-4 1 ,3,5-Trinitrobenzene (R,T}
U182 123-63-7 1 ,3,5-Trioxane, 2,4,6-trimethyl-
U235 126-72-7 Tris(2,3-dibromopropyl) phosphate
U236 72-57-1 Trypan blue
U237 66-75-1 Uracil mustard
U176 759-73-9 Urea, N-ethyi-N-nitroso-
U177 684-93-5 Urea, N-methyi-N-nitroso-
U043 75-01-4 Vinyl chloride
U248 181-81-2 Warfarin, & salts, when present at concentrations of 0.3% or less
U239 1330-20-7 Xylene (I)
U200 50-55-5 Yohimban-16-carboxylic acid, 11, 17-dimethoxy-18-[(3,4,5-trimethoxybenzoyl)oxy]-, methyl ester, (3beta, 16beta, 17alpha, 18beta,20alpha)-
U249 1314-84-7 Zinc phosphide Zn3P2, when present at concentrations of 10% or less
FOOTNOTE: 1CAS Number given for parent compound only.
Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq.
Subparagraph (a) of paragraph (6) of Rule 0400-12-01-.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following:
(a) Exclusion of comparable fuel and syngas fuel. [40 CFR 261.38]
1. Specifications for excluded fuels.
SS-7037 (October 2011) RDA 1693 24
SS-7037 (October 2011)
Wastes that meet the specifications for comparable fuel or syngas fuel under subpart (i) or (ii) of this part, respectively, and the other requirements of this subparagraph, are not solid wastes.
(i) Comparable fuel specifications.
(I) Physical specifications.
I. Heating value. The heating value must exceed 5,000 Btu/lbs. (11 ,500 J/g).
II. Viscosity. The viscosity must not exceed: 50 cS, as-fired.
(II) Constituent specifications. For compounds listed in Table 1 to this subparagraph, the specification levels and, where non-detect is the specification, minimum required detection limits are: (see Table 1 of this subparagraph).
(ii) Synthesis gas fuel specifications.
Synthesis gas fuel (i.e., syngas fuel) that is generated from hazardous waste must:
(I) Have a minimum Btu value of 100 Btu/Scf;
(II) Contain less than 1 ppmv of total halogen;
(Ill) Contain less than 300 ppmv of total nitrogen other than diatomic nitrogen (N2);
(IV) Contain less than 200 ppmv of hydrogen sulfide; and
(V) Contain less than 1 ppmv of each hazardous constituent in the target list of appendix VIII constituents in paragraph (5) of this rule.
(iii) Blending to meet the specifications.
(I) Hazardous waste shall not be blended to meet the comparable fuel specification under subpart (i) of this part, except as provided by item (II) of this subpart.
(II) Blending to meet the viscosity specification. A hazardous waste blended to meet the viscosity specification for comparable fuel shall:
I. As generated and prior to any blending, manipulation, or processing, meet the constituent and heating value specifications of subitem (i)(l)l and item (i)(ll) of this part;
II. Be blended at a facility that is subject to the applicable requirements of Rules 0400-12-01-.05 and .06, or subparagraph (4)(e) of Rule 0400-12-01-.03; and
Ill. Not violate the dilution prohibition of subpart (vi) of this part.
(iv) Treatment to meet the comparable fuel specifications.
(I) A hazardous waste may be treated to meet the specifications for comparable fuel set forth in subpart (i) of this part provided the treatment:
RDA 1693 25
I. Destroys or removes the constituents listed in the specification or raises the heating value by removing or destroying hazardous constituents or materials;
II. Is performed at a facility that is subject to the applicable requirements of Rules 0400-12-01-.05 and .06, or subparagraph (4)(e) of Rule 0400-12-01-.03; and
Ill. Does not violate the dilution prohibition of subpart (vi) of this part.
(II) Residuals resulting from the treatment of a hazardous waste listed in paragraph (4) of this rule to generate a comparable fuel remain a hazardous waste.
(v) Generation of a syngas fuel.
(I) A syngas fuel can be generated from the processing of hazardous wastes to meet the exclusion specifications of subpart (ii) of this part provided the processing:
I. Destroys or removes the constituents listed in the specification or raises the heating value by removing or destroying constituents or materials;
II. Is performed at a facility that is subject to the applicable requirements of Rules 0400-12-01-.05 and .06, or subparagraph (4)(e) of Rule 0400-12-01-.03 or is an exempt recycling unit pursuant to part ( 1 )(f)3 of this rule; and
Ill. Does not violate the dilution prohibition of subpart (vi) of this part.
(II) Residuals resulting from the treatment of a hazardous waste listed in paragraph (4) of this rule to generate a syngas fuel remain a hazardous waste.
(vi) Dilution prohibition.
No generator, transporter, handler, or owner or operator of a treatment, storage, or disposal facility shall in any way dilute a hazardous waste to meet the specifications of subitem (i)(l)l and item (i)(ll) of this part for comparable fuel, or subpart (ii) of this part for syngas.
2. Implementation.
SS-7037 (October2011)
(i) General.
(I) Wastes that meet the specifications provided by part 1 of this subparagraph for comparable fuel or syngas fuel are excluded from the definition of solid waste provided that the conditions under this subparagraph are met. For purposes of this subparagraph, such materials are called excluded fuel; the person claiming and qualifying for the exclusion is called the excluded fuel generator and the person burning the excluded fuel is called the excluded fuel burner.
(II) The person who generates the excluded fuel must claim the exclusion by complying with the conditions of this subparagraph and keeping records necessary to document compliance with those conditions.
(ii) Notices.
(I) Notices to the Commissioner.
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SS-7037 (October 2011)
I. The generator must submit a one-time notice, except as provided by subitem Ill of this item, to the Commissioner or to the Regional or State RCRA and CAA Directors, in whose jurisdiction the exclusion is being claimed and where the excluded fuel will be burned, certifying compliance with the conditions of the exclusion and providing the following documentation:
A. The name, address, and RCRA ID number of the person/facility claiming the exclusion;
B. The applicable EPA Hazardous Waste Code(s) that would otherwise apply to the excluded fuel;
C. The name and address of the units meeting the requirements of subpart (iii) of this part and part 3 of this subparagraph, that will burn the excluded fuel;
D. An estimate of the average and maximum monthly and annual quantity of material for which an exclusion would be claimed, except as provided by subitem Ill of this item; and
E. The following statement, which shall be signed and submitted by the person claiming the exclusion or his authorized representative:
"Under penalty of criminal and civil prosecution for making or submitting false statements, representations, or omissions, I certify that the requirements of subparagraph (6)(a) of Rule 0400-12-01-.02 have been met for all comparable fuels identified in this notification. Copies of the records and information required at subpart (6)(a)2(viii) of Rule 0400-12-01-.02 are available at the generator's facility. Based on my inquiry of the individuals immediately responsible for obtaining the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."
II. If there is a substantive change in the information provided in the notice required under this subpart, the generator must submit a revised notification.
Ill. Excluded fuel generators must include an estimate of the average and maximum monthly and annual quantity of material for which an exclusion would be claimed only in notices submitted after December 19, 2008 for newly excluded fuel or for revised notices as required by subitem II of this item.
(II) Public notice.
Prior to burning an excluded fuel, the burner must publish in a major newspaper of general circulation local to the site where the fuel will be burned, a notice entitled "Notification of Burning a Fuel Excluded Under
RDA 1693 27
SS-7037 (October 2011)
the Resource Conservation and Recovery Act" and containing the following information:
I. Name, address, and RCRA ID number of the generating facility(ies );
II. Name and address of the burner and identification of the unit(s) that will burn the excluded fuel;
Ill. A brief, general description of the manufacturing, treatment, or other process generating the excluded fuel;
IV. An estimate of the average and maximum monthly and annual quantity of the excluded fuel to be burned; and
V. Name and mailing address of the Commissioner or the Regional or State Directors to whom the generator submitted a claim for the exclusion.
(iii) Burning.
The exclusion applies only if the fuel is burned in the following units that also shall be subject to Federal/State/local air emission requirements, including all applicable requirements implementing section 112 of the Clean Air Act or the Tennessee Air Quality Act:
(I) Industrial furnaces as defined in subparagraph (2)(a) of Rule 0400-12-01-.01;
(II) Boilers, as defined in subparagraph (2)(a) of Rule 0400-12-01-.01, that are further defined as follows:
I. Industrial boilers located on the site of a facility engaged in a manufacturing process where substances are transformed into new products, including the component parts of products, by mechanical or chemical processes; or
II. Utility boilers used to produce electric power, steam, heated or cooled air, or other gases or fluids for sale;
(Ill) Hazardous waste incinerators subject to regulation under paragraph (15) of Rule 0400-12-01-.05 or Rule 0400-12-01-.06 and applicable CAA MACT standards or the comparable standard under the Tennessee Air Quality Act.
(IV) Gas turbines used to produce electric power, steam, heated or cooled air, or other gases or fluids for sale.
(iv) Fuel analysis plan for generators.
The generator of an excluded fuel shall develop and follow a written fuel analysis plan which describes the procedures for sampling and analysis of the material to be excluded. The plan shall be followed and retained at the site of the generator claiming the exclusion.
(I) At a minimum, the plan must specify:
I. The parameters for which each excluded fuel will be analyzed and the rationale for the selection of those parameters;
RDA 1693 28
SS-7037 (October 2011)
II. The test methods which will be used to test for these parameters;
Ill. The sampling method which will be used to obtain a representative sample of the excluded fuel to be analyzed;
IV. The frequency with which the initial analysis of the excluded fuel will be reviewed or repeated to ensure that the analysis is accurate and up to date; and
V. If process knowledge is used in the determination, any information prepared by the generator in making such determination.
(II} For each analysis, the generator shall document the following:
I. The dates and times that samples were obtained, and the dates the samples were analyzed;
II. The names and qualifications of the person(s) who obtained the samples;
Ill. A description of the temporal and spatial locations of the samples;
IV. The name and address of the laboratory facility at which analyses of the samples were performed;
V. A description of the analytical methods used, including any clean-up and sample preparation methods;
VI. All quantitation limits achieved and all other quality control results for the analysis (including method blanks, duplicate analyses, matrix spikes, etc.), laboratory quality assurance data, and the description of any deviations from analytical methods written in the plan or from any other activity written in the plan which occurred;
VII. All laboratory results demonstrating whether the exclusion specifications have been met; and
VIII. All laboratory documentation that support the analytical results, unless a contract between the claimant and the laboratory provides for the documentation to be maintained by the laboratory for the period specified in subpart (ix) of this part and also provides for the availability of the documentation to the claimant upon request.
(Ill) Syngas fuel generators shall submit for approval, prior to performing sampling, analysis, or any management of an excluded syngas fuel, a fuel analysis plan containing the elements of item (I) of this subpart to the Commissioner. The approval of fuel analysis plans must be stated in writing and received by the facility prior to sampling and analysis to demonstrate the exclusion of a syngas. The approval of the fuel analysis plan may contain such provisions and conditions as the Commissioner deems appropriate.
(v) Excluded fuel sampling and analysis.
(I) General.
RDA 1693 29
SS-7037 (October 2011)
For wastes for which an exclusion is claimed under the specifications provided by subpart 1 (i) or (ii) of this subparagraph, the generator of the waste must test for all the constituents in appendix VIII in paragraph (5) of this rule, except those that the generator determines, based on testing or knowledge, should not be present in the fuel. The generator is required to document the basis of each determination that a constituent with an applicable specification should not be present. The generator may not determine that any of the following categories of constituents with a specification in Table 1 to this subparagraph should not be present:
I. A constituent that triggered the toxicity characteristic for the constituents that were the basis for listing the hazardous secondary material as a hazardous waste, or constituents for which there is a treatment standard for the waste code in subparagraph (3)(a) of Rule 0400-12-01-.10;
II. A constituent detected in previous analysis of the waste;
Ill. Constituents introduced into the process that generates the waste; or
IV. Constituents that are byproducts or side reactions to the process that generates the waste.
(Note: Any claim under this subpart must be valid and accurate for all hazardous constituents; a determination not to test for a hazardous constituent will not shield a generator from liability should that constituent later be found in the excluded fuel above the exclusion specifications.)
(II) Use of process knowledge. For each waste for which the comparable fuel or syngas exclusion is claimed where the generator of the excluded fuel is not the original generator of the hazardous waste, the generator of the excluded fuel may not use process knowledge pursuant to item (I) of this subpart and must test to determine that all of the constituent specifications of subparts 1 (i) and (ii) of this subparagraph, as applicable, have been met.
(Ill) The excluded fuel generator may use any reliable analytical method to demonstrate that no constituent of concern is present at concentrations above the specification levels. It is the responsibility of the generator to ensure that the sampling and analysis are unbiased, precise, and representative of the excluded fuel. For the fuel to be eligible for exclusion, a generator must demonstrate that:
I. The 95% upper confidence limit of the mean concentration for each constituent of concern is not above the specification level; and
II. The analyses could have detected the presence of the constituent at or below the specification level.
(IV) Nothing in this subpart preempts, overrides or otherwise negates the provision in subparagraph (1)(b) of Rule 0400-12-01-.03, which requires any person who generates a solid waste to determine if that waste is a hazardous waste.
(V) In an enforcement action, the burden of proof to establish conformance with the exclusion specification shall be on the generator claiming the exclusion.
RDA 1693 30
SS-7037 (October 2011)
(VI) The generator must conduct sampling and analysis in accordance with the fuel analysis plan developed under subpart (iv) of this part.
(VII) Viscosity condition for comparable fuel.
I. Excluded comparable fuel that has not been blended to meet the kinematic viscosity specification shall be analyzed as-generated.
II. If hazardous waste is blended to meet the kinematic viscosity specification for comparable fuel, the generator shall:
A. Analyze the hazardous waste as-generated to ensure that it meets the constituent and heating value specifications of subpart 1 (i) of this subparagraph; and
B. After blending, analyze the fuel again to ensure that the blended fuel meets all comparable fuel specifications.
(VIII) Excluded fuel must be re-tested, at a minimum, annually and must be retested after a process change that could change its chemical or physical properties in a manner than may affect conformance with the specifications.
(vi) Reserved
(vii) Speculative accumulation.
Excluded fuel must not be accumulated speculatively, as defined in subpart (1)(b)3(viii) of this rule.
(viii) Operating record.
The generator must maintain an operating record on site containing the following information:
(I) All information required to be submitted to the implementing authority as part of the notification of the claim:
I. The owner/operator name, address, and the facility Installation ID number of the person claiming the exclusion;
II. For each excluded fuel, the hazardous waste codes that would be applicable if the material were discarded; and
Ill. The certification signed by the person claiming the exclusion or his authorized representative.
(II) A brief description of the process that generated the excluded fuel. If the comparable fuel generator is not the generator of the original hazardous waste, provide a brief description of the process that generated the hazardous waste;
(Ill) The monthly and annual quantities of each fuel claimed to be excluded;
(IV) Documentation for any claim that a constituent is not present in the excluded fuel as required under item (v)(l) of this part;
(V) The results of all analyses and all detection limits achieved as required under subpart (iv) of this part;
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SS-7037 (October 2011)
(VI) If the comparable fuel was generated through treatment or blending, documentation of compliance with the applicable provisions of subparts 1 (iii) and (iv) of this subparagraph;
(VII) If the excluded fuel is to be shipped off-site, a certification from the burner as required under subpart (x) of this part;
(VIII) The fuel analysis plan and documentation of all sampling and analysis results as required by subpart (iv) of this part; and
(IX) If the generator ships excluded fuel off-site for burning, the generator must retain for each shipment the following information on-site:
I. The name and address of the facility receiving the excluded fuel for burning;
II. The quantity of excluded fuel shipped and delivered;
Ill. The date of shipment or delivery;
IV. A cross-reference to the record of excluded fuel analysis or other information used to make the determination that the excluded fuel meets the specifications as required under subpart (iv) of this part; and
V. A one-time certification by the burner as required under subpart (x) of this part.
(ix) Records retention.
Records must be maintained for a period of three years.
(x) Burner certification to the generator.
Prior to submitting a notification to the Commissioner, a generator of excluded fuel who intends to ship the excluded fuel off-site for burning must obtain a onetime written, signed statement from the burner:
(I) Certifying that the excluded fuel will only be burned in an industrial furnace, industrial boiler, utility boiler, or hazardous waste incinerator, as required under subpart (iii) of this part;
(II) Identifying the name and address of the facility that will burn the excluded fuel; and
(Ill) Certifying that the State in which the burner is located is authorized to exclude wastes as excluded fuel under the provisions of this subparagraph.
(xi) Ineligible waste codes.
Wastes that are listed as hazardous waste because of the presence of dioxins or furans, as set out in appendix VII in paragraph (5) of this rule, are not eligible for these exclusions, and any fuel produced from or otherwise containing these wastes remains a hazardous waste subject to the full hazardous waste management requirements.
(xii) Regulatory status of boiler residues.
Burning excluded fuel that was otherwise a hazardous waste listed subparagraphs (4)(b) through (d) of this rule does not subject boiler residues,
RDA 1693 32
including bottom ash and emission control residues, to regulation as derived-from hazardous wastes.
(xiii) Residues in containers and tank systems upon cessation of operations.
(I) Liquid and accumulated solid residues that remain in a container or tank system for more than 90 days after the container or tank system ceases to be operated for storage or transport of excluded fuel product are subject to regulation under Rules 0400-12-01-.03 through 0400-12-01-.10.
(II) Liquid and accumulated solid residues that are removed from a container or tank system after the container or tank system ceases to be operated for storage or transport of excluded fuel product are solid wastes subject to regulation as hazardous waste if the waste exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (e) of this rule or if the fuel were otherwise a hazardous waste listed under subparagaphs (4)(b) through (d) of this rule when the exclusion was claimed.
(Ill) Liquid and accumulated solid residues that are removed from a container or tank system and which do not meet the specifications for exclusion under subpart 1 (i) or (ii) of this subparagraph are solid wastes subject to regulation as hazardous waste if:
I. The waste exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (d) of this rule; or
II. The fuel were otherwise a hazardous waste listed under subparagraphs (4)(b) through (d) of this rule. The hazardous waste code for the listed waste applies to these liquid and accumulated solid resides.
(xiv) Waiver of RCRA Closure Requirements.
Interim status and permitted storage and combustion units, and generator storage units exempt from the permit requirements under subparagraph (4)(e) of Rule 0400-12-01-.03, are not subject to the closure requirements of Rules 0400-12-01-.05 and 0400-12-01-.06 provided that the storage and combustion unit has been used to manage only hazardous waste that is subsequently excluded under the conditions of this subparagraph, and that afterward will be used only to manage fuel excluded under this subparagraph.
(xv) Spills and leaks.
(I) Excluded fuel that is spilled or leaked and that therefore no longer meets the conditions of the exclusion is discarded and must be managed as a hazardous waste if it exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (d) of this rule or if the fuel were otherwise a hazardous waste listed in subparagraphs (4)(b) through (d) of this rule.
(II) For excluded fuel that would have otherwise been a hazardous waste listed in subparagraphs (4)(b) through (d) of this rule and which is spilled or leaked, the hazardous waste code for the listed waste applies to the spilled or leaked material.
(xvi) Nothing in this part preempts, overrides, or otherwise negates the provisions in CERCLA Section 103, which establish reporting obligations for releases of hazardous substances, or the Department of Transportation requirements for hazardous materials in 49 CFR parts 171 through 180.
3. Failure to comply with the conditions of the exclusion.
SS-7037 (October 2011) RDA 1693 33
An excluded fuel loses its exclusion if any person managing the fuel fails to comply with the conditions of the exclusion under this subparagraph, and the material must be managed as hazardous waste from the point of generation. In such situations, EPA or the Commissioner may take enforcement action under RCRA section 3008(a), or the Commissioner may take enforcement action under T.C.A. §§ 68-212-101 et seq.
Table 1: Detection and Detection Limit Values for Comparable Fuel Specification
Total Nitrogen as N Total Halogens as Cl
Chemical Name
Total Organic Halogens as Cl Polychlorinated biphenyls total [Arocolors, total] Cyanide, total Metals: Antimony, total Arsenic, total Barium, total Beryllium, total Cadmium, total Chromium, total Cobalt Lead, total Manganese Mercury, total Nickel, total Selenium, total Silver, total Thallium, total
Hydrocarbons: Benzo[a]anthracene Benzene Benzo[b ]fluoranthene Benzo[k]fluoranthene Benzo[ a] pyrene Chrysene Dibenzo[a, h]anthracene 7, 12-Dimethylbenz[a]anthracene Fluoranthene lndeno(1, 2, 3-cd)pyrene 3-Methylcholanthrene Naphthalene Toluene
Oxygenates: Acetophenone Acrolein Allyl alcohol Bis(2-ethylhexl) phthalate [Di-2-ethylhexyl phthalate] Butyl benzyl phthalate o-Cresol [2-Methyl phenol] m-Cresol [3-Methyl phenol] p-Cresol [4-Methyl phenol] Di-n-butyl phthalate Diethyl phthalate 2, 4-Dimethylphenol
SS-7037 (October 2011) 34
CAS No.
NA NA NA 1336-36-3 57-12-5
7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7439-92-1 7439-96-5 7439-97-6 7440-02-0 7782-49-2 7440-22-4 7440-28-0
56-55-3 71-43-2 205-99-2 207-08·9 50-32-8 218-01·9 53-70-3 57-97-6 206-44-0 193-39-5 56-49-5 91-20-3 1 08-88·3
98-86-2 1 07-02·8 107-18·6 117-81-7 85-68-7 95-48-7 108-39·4 106-44-5 84-74-2 84-66-2 105-67-9
Concentration limit (mg/kg at 10,000 BTU/Ib)
4900 540 (1) ND NO
12 0.23 23 1.2
2.3 4.6 31 1.2 0.25 58 0.23 2.3 23
2400 4100 2400 2400 2400 2400 2400 2400 2400 2400 2400 3200 36000
2400 39 30 2400 2400 2400 2400 2400 2400 2400 2400
Minimum required
detection limit (mg/kg)
1.4 1
1.2
RDA 1693
Dimethyl phthalate 131-11-3 2400 Di-n-octyl phthalate 117-84-0 2400 Endothall 145-73-3 100 Ethyl methacrylate 97-63-2 39 2-Ethoxyethanol [Ethylene glycol monoethyl ether] 110-80-5 100 Isobutyl alcohol 78-83-1 39 lsosafrole 120-58-1 2400 Methyl ethyl ketone [2-Butanone] 78-93-3 39 Methyl methacrylate 80-62-6 39 1, 4-Naphthoquinone 130-15-4 2400 Phenol 108-95-2 2400 Propargyl alcohol [2-Propyn-1-ol] 107-19-7 30 Safrole 94-59-7 2400
Sulfonated Organics: Carbon disulfide 75-15-0 NO 39 Disulfoton 298-04-4 NO 2400 Ethyl methanesulfonate 62-50-0 NO 2400 Methyl methanesulfonate 66-27-3 NO 2400 Ph orate 298-02-2 NO 2400 1, 3-Propane sultone 1120-71-4 NO 100 T etraethyldithiopyrophosphate [Sulfotepp] 3689-24-5 NO 2400 Thiophenol [Benzenethiol] 108-98-5 NO 30 0, 0, 0-Triethyl phosphorothioate 126-68-1 NO 2400
Nitrogenated Organics: Acetonitrile [Methyl cyanide] 75-05-8 NO 39 2-Acetylaminofluorene [2-AAF] 53-96-3 NO 2400 Acrylonitrile 107-13-1 NO 39 4-Aminobiphenyl 92-67-1 NO 2400 4-Aminopyridine 504-24-5 NO 100 Aniline 62-53-3 NO 2400 Benzidine 92-87-5 NO 2400 Dibenz[a, j]acridine 224-42-0 NO 2400 0, 0-Diethyl 0-pyrazinyl Phosphorothioate [Thionazin] 297-97-2 NO 2400 Dimethoate 60-51-5 NO 2400 p-(Dimethylamino) azobenzene [4-dimethylaminoazobenzene] 3,3'-Dimethylbenzidine 60-11-7 NO 2400 a, a-Dimethylphenethylamine 119-93-7 NO 2400
122-09-8 NO 2400 3, 3'-Dimethoxybenzidine 119-90-4 NO 100 1, 3-Dinitrobenzene [m-Dinitrobenzene] 99-65-0 NO 2400 4, 6-Dinitro-o-cresol 534-52-1 NO 2400 2, 4-Dinitrophenol 51-28-5 NO 2400 2, 4-Dinitrotoluene 121-14-2 NO 2400 2, 6-Dinitrotoluene 606-20-2 NO 2400 Dinoseb [2-sec-Butyl-4, 6-dinitrophenol] 88-85-7 NO 2400 Diphenylamine 122-39-4 NO 2400 Ethyl carbamate [Urethane] 51-79-6 NO 100 Ethylenethiourea (2-lmidazolidinethione) 96-45-7 NO 110 Famphur 52-85-7 NO 2400 Methacrylonitrile 126-98-7 NO 39 Methapyrilene 91-80-5 NO 2400 Methomyl 16752-77-5 NO 57 2-Methyllactonitrile, [Acetone cyanohydrin] 75-86-5 NO 100 Methyl parathion 298-00-0 NO 2400 MNNG (N-Metyi-N-nitroso-N[prime]- nitroguanidine) 70-25-7 NO 110 1-Naphthylamine, [a-Naphthylamine] 134-32-7 NO 2400 2-Naphthylamine, [~-Naphthylamine] 91-59-8 NO 2400 Nicotine 54-11-5 NO 100 4-Nitroaniline, [p-Nitroaniline] 100-01-6 NO 2400
SS-7037 (October 2011) RDA 1693 35
Nitrobenzene 98-95-3 ND 2400 p-Nitrophenol, [p-Nitrophenol] 100-02-7 ND 2400 5-Nitro-o-toluidine 99-55-8 ND 2400 N-Nitrosodi-n-butylamine 924-16-3 ND 2400 N-Nitrosodiethylamine 55-18-5 ND 2400 N-Nitrosodiphenylamine, [Diphenylnitrosamine] 86-30-6 ND 2400 N-Nitroso-N-methylethylamine 10595-95-6 ND 2400 N-Nitrosomorpholine 59-89-2 ND 2400 N-Nitrosophiperidine 100-75-4 ND 2400 N-Nitrosopyrrolidine 930-55-2 ND 2400 2-Nitropropane 79-46-9 ND 30 Parathion 56-38-2 ND 2400 Phenacetin 62-44-2 ND 2400 1, 4-Phenylne diamine, [p-Phenylenediamine] 106-50-3 ND 2400 N-Phenylthiourea 103-85-5 ND 57 2-Picoline [alpha-Picoline] 109-06-8 ND 2400 Propylthioracil, [6-Propyl-2-thiouracil] 51-52-5 ND 100 Pyridine 110-86-1 ND 2400 Strychnine 57-24-9 ND 100 Thioacetamide 62-55-5 ND 57 Thiofanox 39196-18-4 ND 100 Thiourea 62-56-6 ND 57 T oluene-2,4-diamine [2,4-Diaminotoluene] 95-80-7 ND 57 Toluene-2, 6-diamine [2, 6-Diaminotoluene] 823-40-5 ND 57 a-Toluidine 95-53-4 ND 2400 p-Toluidine 106-49-0 ND 100 1, 3, 5-Trinitrobenzene, [sym-Trinitobenzene] 99-35-4 ND 2400
Halogenated Organics: Allyl chloride 107-05-1 ND 39 Aramite 140-57-8 ND 2400 Benzal chloride [Dichloromethyl benzene] 98-87-3 ND 100 Benzyl chloride 100-44-77 ND 100 bis(2-Chloroethyl)ether [Dichoroethyl ether] 111-44-4 ND 2400 Bromoform [Tribromomethane] 75-25-2 ND 39 Bromomethane [Methyl bromide] 74-83-9 ND 39 4-Bromophenyl phenyl ether [p-Bromo diphenyl ether] 101-55-3 ND 2400 Carbon tetrachloride 56-23-5 ND 39 Chlordane 57-74-9 ND 14 p-Chloroaniline 106-47-8 ND 2400 Chlorobenzene 108-90-7 ND 39 Chlorobenzilate 510-15-6 ND 2400 p-Chloro-m-cresol 59-50-7 ND 2400 2-Chloroethyl vinyl ether 110-75-8 ND 39 Chloroform 67-66-3 ND 39 Chloromethane [Methyl chloride] 74-87-3 ND 39 2-Chloronaphthalene [beta-Chloronaphthalene] 91-58-7 ND 2400 2-Chlorophenol [a-Chlorophenol] 95-57-8 ND 2400 Chloroprene [2-Chloro-1, 3-butadiene] 1126-99-8 ND 39 2, 4-D [2, 4-Dichlorophenoxyacetic acid] 94-75-7 ND 7 Diallate 2303-16-4 ND 2400 1, 2-Dibromo-3-chloropropane 96-12-8 ND 39 1, 2-Dichlorobenzene [a-Dichlorobenzene] 95-50-1 ND 2400 1, 3-Dichlorobenzene [m-Dichlorobenzene] 541-73-1 ND 2400 1, 4-Dichlorobenzene [p-Dichlorobenzene] 106-46-7 ND 2400 3, 3[prime]-Dichlorobenzidine 91-94-1 ND 2400 Dichlorodifluoromethane [CFC-12] 75-71-8 ND 39 1, 2-Dichloroethane [Ethylene dichloride] 107-06-2 ND 39 1, 1-Dichloroethylene [Vinylidene chloride] 75-35-4 ND 39 Dichloromethoxy ethane [Bis(2-chloroethoxy)methane] 111-91-1 ND 2400 2,4-Dichlorophenol 120-83·2 ND 2400
SS-7037 (October 2011) RDA 1693 36
2, 6-0ichlorophenol 1, 2-0ichloropropane [Propylene dichloride] cis-1, 3-0ichloropropylene trans-1, 3-0ichloropropylene 1 ,3-0ichloro-2propanol Endosulfan I Endosulfan II Endrin Endrin aldehyde Endrin Ketone Epichlorohydrin [1-Chloro-2, 3-epoxy propane] Ethylidene dichloride [1, 1-0ichloroethane] 2-Fiuoroacetamide Heptachlor Heptachlor epoxide Hexachlorobenzene Hexachloro-1, 3-butadiene [Hexachlorobutadiene] Hexachlorocyclopentadiene Hexachloroethane Hexachlorophene Hexachloropropene [Hexachloropropylene] lsodrin Kepone [Chlordecone] Lindane [gamma-BHC] [gammaHexachlorocyclohexane] Methylene chloride [Oichloromethane] 4, 4' -Methylene-bis(2-chloroaniline) Methyl iodide [lodomethane] Pentachlorobenzene Pentachloroethane Pentachloronitrobenzene [PCNB] [Quintobenzene] [Quintozene] Pentachlorophenol Pronamide Silvex [2, 4, 5-Trichlorophenoxypropionic acid] 2, 3, 7, 8-Tetrachlorodibenzo-p-dioxin [2, 3, 7, 8-TCOO] 1, 2, 4, 5-Tetrachlorobenzene 1, 1, 2, 2-Tetrachloroethane Tetrachloroethylene [Perchloroethylene] 2, 3, 4, 6-Tetrachlorophenol 1, 2, 4-Trichlorobenzene 1,1, 1-Trichloroethane [Methyl chloroform] 1,1 ,2-Trichloroethane [Vinyl trichloride]
Trichloroethylene Trichlorofluoromethane [Trichloromonofluoromethane] 2, 4, 5-Trichlorophenol 2, 4, 6-Trichlorophenol 1, 2, 3-Trichloropropane Vin I Chloride
Notes: NA -Not Applicable. ND -Nondetect. 125 or individual halogenated organics listed below.
Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq.
87-65-0 78-87-5 10061-01-5 10061-02-6 96-23-1 959-98-8 33213-65-9 72-20-8 7421-93-4 53494-70-5 106-89-8 75-34-3 640-19-7 76-44-8 1024-57-3 118-74-1 87-68-3 77-47-4 67-72-1 70-30-4 1888-71-7 465-73-6 143-50-0 58-89-9 75-09-2 101-14-4 74-88-4 608-93-5 76-01-7 82-68-8 87-86-5 23950-58-5 93-72-1 1746-01-6 95-94-3 79-34-5 127-18-4 58-90-2 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 95-95-4 88-06-2 96-18-4 75-01-4
NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO
2400 39 39 39 30 1.4 1.4 1.4 1.4 1.4 30 39 100 1.4 2.8 2400 2400 2400 2400 59000 2400 2400 4700 1.4 39 100 39 2400 39 2400 2400 2400 7.0 30 2400 39 39 2400 2400 39 39 39 39 2400 2400 39 39
Subparagraph (k) of paragraph (7) of Rule 0400-12-01-.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste Treatment, Storage, and Diposal Facilities is amended by deleting it in its entirety and substituting instead the following:
(k) Certification of Completion of Post-closure Care [40 CFR 265.120]
SS-7037 (October 2011) 37
RDA 1693
No later than 60 days after the completion of the established post-closure care period for each hazardous waste disposal unit, the owner or operator must submit to the Commissioner, by registered mail, a certification that the post-closure care period for the hazardous waste dispos,al unit was performed in accordance with the specifications in the approved post-closure plan. The certification must be signed by the owner or operator and a qualified Professional Engineer. Documentation supporting the qualified Professional Engineer's certification must be furnished to the Commissioner upon request until he releases the owner or operator from the financial assurance requirements for post-closure care under part (8)(f)3 of this rule.
Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq.
Part 2 of subparagraph (g) of paragraph (1) of Rule 0400-12-01-.10 Land Disposal Restrictions is amended by deleting subpart (iv) in its entirety and substituting instead the following:
SS-7037 (October 2011)
(iv) The treatment facility must submit a one-time certification signed by an authorized representative with the initial shipment of waste or treatment residue of a restricted waste to the land disposal facility. The certification must state:
"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification. Based on my inquiry of those individuals immediately responsible for obtaining this information, I believe that it has been maintained and operated properly so as to comply with the treatment standards specified in Rule 0400-12-001-.1 0(3)(a) without impermissible dilution of the prohibited waste. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."
A certification is also necessary for contaminated soil and it must state:
"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification and believe that it has been maintained and operated properly so as to comply with treatment standards specified in Rule 0400-12-01-.1 0(3)U) without impermissible dilution of the prohibited waste. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."
(I) A copy of the certification must be placed in the treatment facility's onsite files. If the waste or treatment residue changes, or the receiving facility changes, a new certification must be sent to the receiving facility, and a copy placed in the file.
(II) Debris excluded from the definition of hazardous waste under Rule 0400-12-01-.02(1)(c)6 (i.e., debris treated by an extraction or destruction technology provided by Table 1, subparagraph (3)(f) of this rule, and debris that the Commissioner has determined does not contain hazardous waste), however, is subject to the notification and certification requirements of part 4 of this subparagraph rather than the certification requirements of this subpart.
(Ill) For wastes with organic constituents having treatment standards expressed as concentration levels, if compliance with the treatment standards is based in whole or in part on the analytical detection limit alternative specified in part (3)(a)4 of this rule, the certification, signed by an authorized representative, must state the following:
RDA 1693 38
"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification. Based on my inquiry of those individuals immediately responsible for obtaining this information, I believe that the nonwastewater organic constituents have been treated by combustion units as specified in Rule 0400-12-01-.10(3)(c), Table 1. I have been unable to detect the nonwastewater organic constituents, despite having used best good-faith efforts to analyze for such constituents. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."
(IV) For characteristic wastes that are subject to the treatment standards in subparagraph (3)(a) of this rule (other than those expressed as a method of treatment) or subparagraph (3)U) of this rule and that contain underlying hazardous constituents as defined in part (b )1 0 of this paragraph; if these wastes are treated on-site to remove the hazardous characteristic; and are then sent off-site for treatment of underlying hazardous constituents, the certification must state the following:
"I certify under penalty of law that the waste has been treated in accordance with the requirements of Rule 0400-12-01-.10(3)(a) or Rule 0400-12-01-.10(3)U) to remove the hazardous characteristic. This decharacterized waste contains underlying hazardous constituents that require further treatment to meet treatment standards. I am aware that there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."
(V) For characteristic wastes that contain underlying hazardous constituents as defined in part (b )1 0 of this paragraph that are treated on-site to remove the hazardous characteristic and to treat underlying hazardous constituents to levels in subparagraph (3)(i) of this rule Universal Treatment Standards, the certification must state the following:
"I certify under penalty of law that the waste has been treated in accordance with the requirements of Rule 0400-12-01-.10(3)(a) to remove the hazardous characteristic, and that underlying hazardous constituents, as defined in Rule 0400-12-01-.1 0(1 )(b)1 0, have been treated on-site to meet the Rule 0400-12-01-.1 0(3)(i) Universal Treatment Standards. I am aware that there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."
Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq.
Waste code K161 of the Table 'Treatment Standards for Hazarous Wastes" following part 10 of subparagraph (a) of paragraph (3) of Rule 0400-12-01-.10 Land Disposal Restrictions is amended by deleting "137-30-4" in the third column to the right of "Dithiocarbamates (total) 1o" and replacing it with "NA" so that, as amended, the entry for K161 shall read as follows:
SS-7037 (October 2011) RDA 1693 39
K161 Purification solids (including Antimony 7440-36-0 1.9 1.15 mg/L TCLP filtration, evaporation, and centrifugation solids), baghouse dust and floor sweepings from the production of dithiocarbamate acids and their salts.
Arsenic 7440-38-2 1.4 5.0 mg/L TCLP
Carbon disulfide 75-15-0 3.8 4.8 mg/L TCLP
Dithiocarbamates NA 0.028; or 28; or CMBST (total) 10 CMBST,
CHOXD, BIODG orCARBN
Lead 7439-92-1 0.69 0.75 mg/L TCLP
Nickel 7440-02-0 3.98 11.0 mg/L TCLP
Selenium 7782-49-2 0.82 5. 7 mg/L TCLP
Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq.
SS-7037 (October 2011) 40
RDA 1693
I certify that the information included in this filing is an accurate and complete representation of the intent and scope of rulemaking proposed by the agency.
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Signature~.·. ~! ~ ... ;,(L ;f;:t ..,:;F.~tyc. ~/ I J
Name of Officer: Li a Hughey .. /
Title of Officer: Deputy Director, Division of Solid Waste Management
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SS-7037 (October 2011)
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41
Tre Hargett Secretary of State
RDA 1693
