Preparedby:JD · BH112-013 Analyte Group Primary ID Duplicate ID Analyte Group Primary ID Triplicate ID Analyte Group Analyte(s) Note: Data validation assesses each analyte in terms

Duplicate Analysis RPDs Sample ID CPT139-001 QC142 QC143Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1425693 & 119818 Date Sampled 17/11/2014 17/11/2014 17/11/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 <25 ND NDTRH C10 - C14 Fraction mg/kg 50 <50 <50 <50 ND NDTRH C15 - C28 Fraction mg/kg 100 <100 <100 <100 ND NDTRH C29 - C36 Fraction mg/kg 100 <100 <100 <100 ND NDTRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 <25 ND NDTRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 <25 ND NDTRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 <50 ND NDTRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 <50 ND NDTRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 <100 ND NDTRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 <100 ND NDBenzene mg/kg 0.2 <0.2 <0.2 <0.2 ND NDToluene mg/kg 0.5 <0.5 <0.5 <0.5 ND NDEthylbenzene mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (m & p) mg/kg 0.5 <0.5 <0.5 <2 ND NDXylene (o) mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAcenaphthylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAnthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenz(a)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(a)pyrene mg/kg 0.05 <0.5 <0.5 0.1 ND NDBenzo(a)pyrene (TEQs) mg/kg 0.5 - - <0.5 - -Benzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND -Benzo(a)pyrene TEQ (medium bound)* mg/kg 0.5 0.6 0.6 - 0.00% -Benzo(a)pyrene TEQ (upper bound)* mg/kg 0.5 1.2 1.2 - 0.00% -Benzo(b)&(k)fluoranthene mg/kg 0.2 - - <0.2 - NDBenzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Chrysene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDDibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluoranthene mg/kg 0.1 <0.5 <0.5 0.2 ND NDFluorene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDIndeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDNaphthalene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPhenanthrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPyrene mg/kg 0.1 <0.5 <0.5 0.2 ND NDPAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 0.55 ND NDArsenic mg/kg 4 <5 <5 <4 ND NDCadmium mg/kg 0.4 <1 <1 <0.4 ND NDChromium mg/kg 1 3 <2 2 ND 40.00%Copper mg/kg 1 <5 <5 3 ND NDLead mg/kg 1 17 6 12 95.65% 34.48%Mercury mg/kg 0.1 <0.1 <0.1 <0.1 ND NDNickel mg/kg 1 <2 <2 1 ND NDZinc mg/kg 1 20 6 13 107.69% 42.42%

LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated

Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR

Project: MIC - MIT Site Investigation

RPDs

Golder Associates Pty Ltd 2 of 3

Prepared by: JDChecked by: MB

Duplicate Analysis RPDs Sample ID MIP109-001 QC105_MIP QC106_MIPProject No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1425693 & 119818 Date Sampled 17/11/2014 17/11/2014 17/11/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 <25 ND NDTRH C10 - C14 Fraction mg/kg 50 <50 <50 <50 ND NDTRH C15 - C28 Fraction mg/kg 100 <100 <100 <100 ND NDTRH C29 - C36 Fraction mg/kg 100 <100 <100 <100 ND NDTRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 <25 ND NDTRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 <25 ND NDTRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 <50 ND NDTRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 <50 ND NDTRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 <100 ND NDTRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 <100 ND NDBenzene mg/kg 0.2 <0.2 <0.2 <0.2 ND NDToluene mg/kg 0.5 <0.5 <0.5 <0.5 ND NDEthylbenzene mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (m & p) mg/kg 0.5 <0.5 <0.5 <2 ND NDXylene (o) mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAcenaphthylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAnthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenz(a)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(a)pyrene mg/kg 0.05 <0.5 <0.5 0.05 ND NDBenzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 <0.5 ND NDBenzo(b)&(k)fluoranthene mg/kg 0.2 - - <0.2 - -Benzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND NDChrysene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDDibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluoranthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluorene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDIndeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDNaphthalene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPhenanthrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPyrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 0.05 ND NDArsenic mg/kg 5 6 <5 5 18.18% 18.18%Cadmium mg/kg 0.4 <1 <1 <0.4 ND NDChromium mg/kg 1 13 9 12 36.36% 8.00%Copper mg/kg 1 15 8 13 60.87% 14.29%Lead mg/kg 1 34 36 34 5.71% 0.00%Mercury mg/kg 0.1 <0.1 <0.1 <0.1 ND NDNickel mg/kg 1 7 4 6 54.55% 15.38%Zinc mg/kg 1 48 32 40 40.00% 18.18%




RPDs



Number of Primary Samples: Number of Triplicate Samples:Number of Duplicate Samples: Number of Other QAQC Samples:

Type

Sample IDBH112-013

Analyte Group Primary ID Duplicate ID

Analyte Group Primary ID Triplicate ID

Analyte Group Analyte(s)

Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form.

*When concentrations are less than the LOR for both primary and duplicate/triplicate results, no RPDs are calculated

Performed By: James Dudley Checked By Mitch BlencoweDate: 16/01/2015 Date: 28/01/2015

QAQC Sample Information (Method Blank - MB, Rinsate Blank - RB, Field Blank - FB, Trip Blank - TB)

Y

Date Sampled: 10/11/2014, 11/11/2014 & 13/11/2014 Sample Medium: Soil

Y ASS screening. Re-batch of ES1425177

YAre there non-NATA accredited methods used? N

Project Number: 147623070Primary Laboratory: ALS Workorder Number: ES1425827Secondary Laboratory: - Workorder Number: -

This batch has been validated and is considered suitable for environmental interpretive use.

No Trip Spike was prepared in this batch.

Laboratory reports signed by authorised personnel? Y All.

MS recoveries were not required for this batch

Trip Spike Information

Analyte Spike Concentrations Recovery Concentration % Recovery

Matrix Spike (MS) AnalysesAnalyte Group Comments

Laboratory Control Spike (LCS) Analyses

CommentsALS: Laboratory Duplicate analyses were within the laboratory based quality objectives.

DATA VALIDATION SUMMARY SHEET (Sydney)

0 0Documentation and Sample Handling Information

Sample Information3 0

Chromatograms supplied as appropriate? N/A

Y/N Comments

Samples received intact and chilled? Y Ice present - 19'C, security seal intactSamples analysed within appropriate holding times?

Signed by field staff and laboratory personnel.

Sample volumes sufficient for QC analysis?

Y

All requested analysis completed?

Project Name: MIC - MIT Site Investigation

Sample IDBlanks were not required for this batch

Comments

Comments

Analyte Group Comments

ASS Field Screening

COC completed properly?

Comments

Surrogate recoveries were not required for this batch

Overall Comments

Field triplicates were not collected in this batch.

CommentsField duplicates were not collected in this batch.

Field Triplicates (FT) AnalysesComments

Surrogate Compound Monitoring Analyses

LCS recoveries were not required for this batch

Laboratory Duplicates (LD) Analyses

Field Duplicates (FD) Analyses

Analyte Group

Golder Associates Pty Ltd. 1 of 1


TypeMB

Sample ID







Are there non-NATA accredited methods used? N

NAnalysis of pH (5 weeks), CEC (2 weeks), Mercury (2 weeks), PCBs (4 weeks),Pesticides (4 weeks), TRH (4 weeks), PAHs (4 weeks), and BTEX (4 weeks) wereout of holding times.

Date Sampled: 22/12/2014 Sample Medium: Vapour

Y Metals, TRH, BTEX, PAHs, OCPs, OPPs, Asbestos, pH and CEC.

Y




Due to an processing error at the primary laboratory, the analysis of samples in this batch was delayed by up to 6 weeks. The delayed analysis means several tests were completed out-side of the recommended holdingtime. Analysis outside of the recommended holding time means a potential under-reporting of the results. This is of most concern for the volatile organic compounds which may have degraded during the extended holdingtime. This is not expected to affect the outcomes of the investigation based on the following:- While being held by the laboratory, all the samples were refrigerated to 4 degrees and therefore any degradation or volatile loss would have been minimal.- The majority of the samples reported concentrations of volatile compounds below the laboratory limits of reporting, and the limits of reporting are significantly lower than the adopted assessment criteria. Hence, any loss ordegradation is unlikely to have impacted on the interpretation of the analytical results; and- Based on the field observations it is unlikely that the samples initially contained gross concentrations of volatile contaminants.





All other LCS recoveries conducted by ALS were within the laboratory based data quality objectivesMatrix Spike (MS) Analyses



QAQC Sample Information (Method Blank - MB, Rinsate Blank - RB, Field Blank - FB, Trip Blank - TB)Sample ID

ALS: Matrix Spike recoveries were within the laboratory based data quality objectives





Y/N Comments

Samples received intact and chilled? Y Yes - samples received intact, with ice at a temperature of 3.8'c

Samples analysed within appropriate holding times?



YAll requested analysis completed?


LCS recovery of Copper was less than the lower control limit. This is not expected to affect the outcomes of the investigation as exceedances was relatively minor and reported concentrations of Copper were considerablylower than the assessment criteria.

Comments

No surrogate outliers were observed in this batch.

Overall Comments

Field triplicates were not scheduled for analysis in this batch.

CommentsField duplicates were not scheduled for analysis in this batch.



Total Metals LCS recovery of Copper (92.5%) was less that the lower control limit of 93%.

Laboratory Duplicates (LD) AnalysesComments

ALS: Laboratory Duplicate analyses were within the laboratory based quality objectives.Field Duplicates (FD) Analyses

Analyte Group

ALS: All results were less than the LOR

Comments

CommentsMethod Blank




TypeMBRBRBTB

Benzene 17 85%Toluene 16 80%

Ethlybenzene 16 80%meta- & para-Xylene 16 80%

ortho-Xylene 17 85%Naphthalene 17 85%

Sample IDPB_MW06, BHB8, BHB14 and

Anonymous

Analyte Group Primary ID Duplicate IDBHA-1_10/12/14 QC100_10/12/14

PB_MW16_10/12/14 QC102_10/12/14BHB2_10/12/14 QC103_10/12/14BHB3_10/12/14 QC105_10/12/14

Analyte Group Primary ID Triplicate IDBHA-1_10/12/14 QC101_10/12/14BHB2_10/12/14 QC104_10/12/14


PAHs 4-Terphenyl-d14





Y

Date Sampled: 10/12/2014 - 11/12/2014 Sample Medium: Soil

Y Metals, TPH, BTEXN, PAHs, PCBs, sVOCs, VOCs and PFOS/PFOA

Y

Project Number: 147623070Primary Laboratory: ALS Workorder Number: ES1427638Secondary Laboratory: Envirolab (ELS) Workorder Number: 120886


Recovery of 4-Terphenyl-d14 (31.9%) in sample QC103 was below the lower data quality objective.

Laboratory control spike recoveries were reported outside of the control limit for Benzo(g.h.i)perylene, 2-Methylphenol, Nitrobenzene and Azobenzene. This is not expected to affect the integrity of the batch as all results forthese analytes were reported as below the LOR.The matrix spike for 2.4-Dinitrotoluene (54.0%) was less than the lower control limit of 60%. This is not expected to affect the integrity of the batch as results for this analyte were reported as below the LOR for all samples.


Nitroaromatics and Ketones ALS: Matrix Spike recovery of 2.4-Dinitrotoluene (54.0%) was less than the lower control limit of 60%.



All

ELS: All LCS recoveries from ELS were within the data quality objectives.Matrix Spike (MS) Analyses




All results were less than the LOR

ELS: Matrix Spike recoveries were not conducted by ELS

Comments





Y/N Comments

Samples received intact and chilled? Y ALS: Ice present, 3.2'C, security seal intactELS: Ice present, 3.9'C








TRIP BLANK All results were less than the LOR

QC106_10/12/14 All results were less than the LORQC107_11/12/14 All results were less than the LOR

SAMPLE ID: TRIP SPIKE

20 Recovery within the acceptable control limits (70 - 130%)

20 Recovery within the acceptable control limits (70 - 130%)20 Recovery within the acceptable control limits (70 - 130%)20 Recovery within the acceptable control limits (70 - 130%)20 Recovery within the acceptable control limits (70 - 130%)20 Recovery within the acceptable control limits (70 - 130%)

All


Comments

No other surrogate outliers were observed in this batch.

Overall Comments

All calculated RPDs achieved the acceptable controlAll calculated RPDs achieved the acceptable control

CommentsAll calculated RPDs achieved the acceptable control



PAHs ALS: Recovery of Benzo(g.h.i)perylene (120%) was greater than the upper control limit of 118%.


ALS: Laboratory Duplicate analyses were within the laboratory based quality objectives.

ELS: Laboratory Duplicate analyses were not conducted by ELSField Duplicates (FD) Analyses

Analyte Group

Sample ID

All calculated RPDs achieved the acceptable controlAll calculated RPDs achieved the acceptable control

All calculated RPDs achieved the acceptable control

Nitroaromatics and Ketones ALS: Recovery of Azobenzene (64.9%) was less than the lower control limit of 66%.

Phenols ALS: Recovery of 2-Methylphenol (52.3%) was less than the lower control limit of 55.6%.Nitroaromatics and Ketones ALS: Recovery of Nitrobenzene (67.5%) was less than the lower control limit of 68.3%.

All ALS: All other LCS recoveries from ALS were within the data quality objectives.

ALS: All other MS recoveries from ALS were within the data quality objectives.


Duplicate Analysis RPDs Sample ID BHA-1_10/12/14 QC100_10/12/14 QC101_10/12/14Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1427638 & 120886 Date Sampled 10/12/2014 10/12/2014 10/12/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateArsenic (Filtered) mg/L 0.001 <0.001 <0.001 <0.001 ND NDCadmium (Filtered) mg/L 0.0001 0.0004 0.0005 0.0005 22.22% 22.22%Chromium (Filtered) mg/L 0.001 <0.001 <0.001 <0.001 ND NDCopper (Filtered) mg/L 0.001 0.006 0.004 0.003 40.00% 66.67%Lead (Filtered) mg/L 0.001 <0.001 <0.001 <0.001 ND NDMercury (Filtered) mg/L 0.00005 <0.0001 <0.0001 <0.00005 ND NDNickel (Filtered) mg/L 0.001 0.041 0.04 0.042 2.47% 2.41%Zinc (Filtered) mg/L 0.001 1.31 1.31 1.1 0.00% 17.43%1,2,4-trimethylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,3,5-Trimethylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDBenzene mg/L 0.001 <0.001 <0.001 <0.001 ND NDToluene mg/L 0.001 <0.002 <0.002 <0.001 ND NDIsopropylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDn-Butylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDn-Propylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDp-Isopropyltoluene mg/L 0.001 <0.005 <0.005 <0.001 ND NDsec-Butylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDStyrene mg/L 0.001 <0.005 <0.005 <0.001 ND NDtert-Butylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDEthylbenzene mg/L 0.001 <0.002 <0.002 <0.001 ND NDXylenes (m & p) mg/L 0.002 <0.002 <0.002 <0.002 ND NDXylene (o) mg/L 0.001 <0.002 <0.002 <0.001 ND NDXylenes (Sum of total) (Lab Reported) mg/L 0.002 <0.002 <0.002 - ND -Total BTEX mg/L 0.001 <0.001 <0.001 - ND -Acenaphthene mg/L 0.001 <0.001 <0.001 <0.001 ND NDAcenaphthylene mg/L 0.001 <0.001 <0.001 <0.001 ND NDAnthracene mg/L 0.001 <0.001 <0.001 <0.001 ND NDBenz(a)anthracene mg/L 0.001 <0.001 <0.001 <0.001 ND NDBenzo(a)pyrene mg/L 0.0005 <0.0005 <0.0005 <0.001 ND NDBenzo(a)pyrene (TEQs) mg/L 0.0005 <0.0005 <0.0005 <0.005 ND NDBenzo(b)&(k)fluoranthene mg/L 0.002 - - <0.002 - -Benzo(b)&(j)fluoranthene mg/L 0.001 <0.001 <0.001 - ND -Benzo(g,h,i)perylene mg/L 0.001 <0.001 <0.001 <0.001 ND NDBenzo(k)fluoranthene mg/L 0.001 <0.001 <0.001 <0.02 ND NDChrysene mg/L 0.001 <0.001 <0.001 <0.001 ND NDDibenz(a,h)anthracene mg/L 0.001 <0.001 <0.001 <0.001 ND NDFluoranthene mg/L 0.001 <0.001 <0.001 <0.001 ND NDFluorene mg/L 0.001 <0.001 <0.001 <0.001 ND NDIndeno(1,2,3-c,d)pyrene mg/L 0.001 <0.001 <0.001 <0.001 ND NDNaphthalene mg/L 0.001 <0.001 <0.001 <0.001 ND NDPhenanthrene mg/L 0.001 <0.001 <0.001 <0.001 ND NDPyrene mg/L 0.001 <0.001 <0.001 <0.001 ND NDPAH (Sum of Common 16 PAHs - Lab Reported) mg/L 0.0005 <0.0005 <0.0005 0 ND ND2-Chloronaphthalene mg/L 0.002 <0.002 <0.002 <0.004 ND ND2-Methylnaphthalene mg/L 0.002 <0.002 <0.002 <0.004 ND ND3-Methylcholanthrene mg/L 0.002 <0.002 <0.002 <0.004 ND ND7,12-Dimethylbenz(a)anthracene mg/L 0.002 <0.002 <0.002 <0.004 ND NDTRH C6 - C9 Fraction mg/L 0.01 <0.02 <0.02 <0.01 ND NDTRH C10 - C14 Fraction mg/L 0.05 <0.05 <0.05 <0.05 ND NDTRH C15 - C28 Fraction mg/L 0.1 <0.1 <0.1 <0.1 ND NDTRH C29 - C36 Fraction mg/L 0.05 <0.05 <0.05 <0.1 ND NDTRH+C10 - C36 (Sum of total) (Lab Reported) mg/L 0.05 <0.05 <0.05 - ND -TRH+C10 - C40 (Sum of total) (Lab Reported) mg/L 0.1 <0.1 <0.1 - ND -TRH C6 - C10 Fraction F1 mg/L 0.01 <0.02 <0.02 <0.01 ND NDTRH C6 - C10 Fraction Less BTEX F1 mg/L 0.01 <0.02 <0.02 <0.01 ND NDTRH >C10 - C16 Fraction F2 mg/L 0.05 <0.1 <0.1 <0.05 ND NDTRH >C10 - C16 Fraction Less Naphthalene F2 mg/L 0.05 <0.1 <0.1 <0.05 ND NDTRH >C16 - C34 Fraction F3 mg/L 0.1 <0.1 <0.1 <0.1 ND NDTRH >C34 - C40 Fraction F4 mg/L 0.1 <0.1 <0.1 <0.1 ND ND2-(Acetylamino) fluorene mg/L 0.002 <0.002 <0.002 <0.004 ND ND2-Picoline mg/L 0.002 <0.002 <0.002 - ND -3,3-Dichlorobenzidine mg/L 0.002 <0.002 <0.002 - ND -4-(Dimethylamino) azobenzene mg/L 0.002 <0.002 <0.002 <0.01 ND ND4-Aminobiphenyl mg/L 0.002 <0.002 <0.002 - ND -4-Bromophenyl phenyl ether mg/L 0.002 <0.002 <0.002 <0.01 ND ND4-Chlorophenyl phenyl ether mg/L 0.002 <0.002 <0.002 <0.01 ND ND4-Nitroquinoline-n-oxide mg/L 0.002 <0.002 <0.002 - ND -Acetophenone mg/L 0.002 <0.002 <0.002 <0.01 ND NDAzobenzene mg/L 0.002 <0.002 <0.002 <0.01 ND NDBis(2-chloroethoxy) methane mg/L 0.002 <0.002 <0.002 <0.01 ND NDBis(2-chloroethyl) ether mg/L 0.002 <0.002 <0.002 <0.01 ND NDDibenzofuran mg/L 0.002 <0.002 <0.002 <0.01 ND NDHexachlorocyclopentadiene mg/L 0.005 <0.01 <0.01 <0.01 ND NDHexachloropropene mg/L 0.002 <0.002 <0.002 <0.004 ND NDMethapyrilene mg/L 0.002 <0.002 <0.002 <0.02 ND NDn-Nitrosomorpholine mg/L 0.002 <0.002 <0.002 <0.01 ND NDN-Nitrosopiperidine mg/L 0.002 <0.002 <0.002 <0.01 ND NDn-Nitrosopyrrolidine mg/L 0.004 <0.004 <0.004 - ND -Phenacetin mg/L 0.002 <0.002 <0.002 <0.01 ND ND1,1,1,2-Tetrachloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1,2,2-Tetrachloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1,1-Trichloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1,2-Trichloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2,3-Trichloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2-Dibromo-3-chloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2-Dibromoethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1-Dichloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2-Dichloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1-Dichloroethene mg/L 0.001 <0.005 <0.005 <0.001 ND NDcis-1,2-Dichloroethene mg/L 0.001 <0.005 <0.005 <0.001 ND NDtrans-1,2-dichloroethene mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2-Dichloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,3-Dichloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND2,2-Dichloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1-Dichloropropene mg/L 0.001 <0.005 <0.005 <0.001 ND NDcis-1,3-Dichloropropene mg/L 0.001 <0.005 <0.005 <0.001 ND NDtrans-1,3-dichloropropene mg/L 0.001 <0.005 <0.005 <0.001 ND NDcis-1,4-Dichloro-2-butene mg/L 0.005 <0.005 <0.005 - ND -trans-1,4-Dichloro-2-butene mg/L 0.005 <0.005 <0.005 - ND -Bromodichloromethane mg/L 0.001 <0.005 <0.005 <0.001 ND NDBromoform ug/L 1 <5 <5 <1 ND NDBromomethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDCarbon disulfide mg/L 0.005 <0.005 <0.005 - ND -Carbon tetrachloride mg/L 0.001 <0.005 <0.005 <0.001 ND NDChlorodibromomethane mg/L 0.001 <0.005 <0.005 <0.001 ND NDChloroethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDChloroform mg/L 0.001 <0.005 <0.005 <0.001 ND NDChloromethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDDibromomethane ug/L 1 <5 <5 <1 ND NDDichlorodifluoromethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDHexachlorobutadiene mg/L 0.001 <0.002 <0.002 <0.001 ND NDHexachloroethane mg/L 0.002 <0.002 <0.002 <0.004 ND NDIodomethane mg/L 0.005 <0.005 <0.005 - ND -Pentachloroethane mg/L 0.002 <0.005 <0.005 <0.004 ND NDTrichloroethene mg/L 0.001 <0.005 <0.005 <0.001 ND NDTetrachloroethene mg/L 0.001 <0.005 <0.005 0.003 ND NDTrichlorofluoromethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDVinyl chloride mg/L 0.01 <0.05 <0.05 <0.01 ND NDn-Nitrosodiethylamine mg/L 0.002 <0.002 <0.002 - ND -N-Nitrosodi-n-butylamine mg/L 0.002 <0.002 <0.002 <0.01 ND NDN-Nitrosodi-n-propylamine mg/L 0.002 <0.002 <0.002 <0.01 ND NDn-Nitrosomethylethylamine mg/L 0.002 <0.002 <0.002 - ND -1-Naphthylamine mg/L 0.002 <0.002 <0.002 <0.01 ND NDn-Nitrosodiphenylamine & Diphenylamine mg/L 0.004 <0.004 <0.004 - ND -2-Nitroaniline mg/L 0.004 <0.004 <0.004 <0.01 ND ND3-Nitroaniline mg/L 0.004 <0.004 <0.004 <0.01 ND ND4-Chloroaniline mg/L 0.002 <0.002 <0.002 <0.01 ND ND4-Nitroaniline mg/L 0.002 <0.002 <0.002 <0.01 ND ND2-methyl-5-nitroaniline mg/L 0.002 <0.002 <0.002 <0.01 ND NDAniline mg/L 0.002 <0.002 <0.002 <0.01 ND NDNitrobenzene mg/L 0.002 <0.002 <0.002 <0.01 ND NDPentachloronitrobenzene mg/L 0.002 <0.002 <0.002 <0.01 ND ND


RPDs


Prepared by: JDChecked by:MB

1,3,5-Trinitrobenzene mg/L 0.002 <0.002 <0.002 - ND -2,4-Dinitrotoluene mg/L 0.004 <0.004 <0.004 - ND -2,6-Dinitrotoluene mg/L 0.004 <0.004 <0.004 <0.01 ND ND1,2,3-Trichlorobenzene mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2,4-Trichlorobenzene mg/L 0.001 <0.002 <0.002 <0.001 ND ND1,2-Dichlorobenzene mg/L 0.001 <0.002 <0.002 <0.001 ND ND1,3-Dichlorobenzene mg/L 0.001 <0.002 <0.002 <0.001 ND ND1,4-Dichlorobenzene mg/L 0.001 <0.002 <0.002 <0.001 ND ND2-Chlorotoluene mg/L 0.001 <0.005 <0.005 <0.001 ND ND4-Chlorotoluene mg/L 0.001 <0.005 <0.005 <0.001 ND NDBromobenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDChlorobenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDHexachlorobenzene mg/L 0.002 <0.004 <0.004 <0.004 ND NDPentachlorobenzene mg/L 0.002 <0.002 <0.002 <0.004 ND NDPronamide mg/L 0.002 <0.002 <0.002 - ND -a-BHC mg/L 0.002 <0.002 <0.002 <0.004 ND NDAldrin mg/L 0.002 <0.002 <0.002 <0.004 ND NDAldrin & Dieldrin (Sum of total) (Lab Reported) mg/L 0.004 <0.004 <0.004 - ND -b-BHC mg/L 0.002 <0.002 <0.002 <0.004 ND NDd-BHC mg/L 0.002 <0.002 <0.002 <0.004 ND NDDDD mg/L 0.002 <0.002 <0.002 <0.004 ND NDDDE mg/L 0.002 <0.002 <0.002 <0.004 ND NDDDT mg/L 0.002 <0.004 <0.004 <0.004 ND NDDDT+DDE+DDD (Sum of total) (Lab Reported) mg/L 0.004 <0.004 <0.004 - ND -Dieldrin mg/L 0.002 <0.002 <0.002 <0.004 ND NDEndosulfan I mg/L 0.002 <0.002 <0.002 <0.004 ND NDEndosulfan II mg/L 0.002 <0.002 <0.002 <0.004 ND NDEndosulfan sulphate mg/L 0.002 <0.002 <0.002 <0.004 ND NDEndrin mg/L 0.002 <0.002 <0.002 <0.004 ND NDg-BHC mg/L 0.002 <0.002 <0.002 <0.004 ND NDHeptachlor mg/L 0.002 <0.002 <0.002 <0.004 ND NDHeptachlor & heptachlor epoxide (Sum Lab Reported) mg/l 0.002 <0.002 <0.002 - ND -Heptachlor epoxide mg/L 0.002 <0.002 <0.002 <0.004 ND NDChlorfenvinphos mg/L 0.002 <0.002 <0.002 - ND -Chlorpyriphos mg/L 0.002 <0.002 <0.002 - ND -Chlorpyriphos-methyl mg/L 0.002 <0.002 <0.002 - ND -Diazinon mg/L 0.002 <0.002 <0.002 - ND -Dichlorvos mg/L 0.002 <0.002 <0.002 - ND -Dimethoate mg/L 0.002 <0.002 <0.002 - ND -Ethion mg/L 0.002 <0.002 <0.002 - ND -Fenthion mg/L 0.002 <0.002 <0.002 - ND -Malathion mg/L 0.002 <0.002 <0.002 - ND -Pirimphos-ethyl mg/L 0.002 <0.002 <0.002 - ND -Prothiofos mg/L 0.002 <0.002 <0.002 - ND -6:2 Fluorotelomer Sulfonate (6:2 FtS) mg/L 0.0001 <0.0001 <0.0001 - ND -Perfluorooctanoate mg/L 0.00002 0.00036 0.00031 - 14.93% -PFOA mg/L 0.00002 0.00036 0.00031 - 14.93% -PFOS mg/L 0.00002 0.00134 0.00132 - 1.50% -Carbazole mg/L 0.002 <0.002 <0.002 <0.01 ND NDChlorobenzilate mg/L 0.002 <0.002 <0.002 - ND -2,4-Dimethylphenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND2-Methylphenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND2-Nitrophenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND3- & 4- Methylphenol mg/L 0.004 <0.004 <0.004 - ND -Phenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND2,4,5-Trichlorophenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND2,4,6-Trichlorophenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND2,4-Dichlorophenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND2,6-Dichlorophenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND2-Chlorophenol mg/L 0.002 <0.002 <0.002 <0.004 ND ND4-Chloro-3-methylphenol mg/L 0.002 <0.002 <0.002 - ND -Pentachlorophenol mg/L 0.004 <0.004 <0.004 <0.02 ND NDBis(2-ethylhexyl) phthalate mg/L 0.01 <0.01 <0.01 <0.02 ND NDButylbenzyl phthalate mg/L 0.002 <0.002 <0.002 <0.02 ND NDDiethyl phthalate mg/L 0.002 <0.002 <0.002 <0.02 ND NDDimethyl phthalate mg/L 0.002 <0.002 <0.002 <0.02 ND NDDi-n-butyl phthalate mg/L 0.002 <0.002 <0.002 <0.02 ND NDDi-n-octyl phthalate mg/L 0.002 <0.002 <0.002 <0.02 ND NDMethyl Ethyl Ketone mg/L 0.05 <0.05 <0.05 - ND -2-Hexanone mg/L 0.05 <0.05 <0.05 - ND -Methyl iso-butyl ketone mg/L 0.05 <0.05 <0.05 - ND -Isophorone mg/L 0.002 <0.002 <0.002 <0.01 ND NDVinyl acetate mg/L 0.05 <0.05 <0.05 - ND -





Duplicate Analysis RPDs Sample ID PB_MW16_10/12/14 QC102_10/12/14 -Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1427638 & 120886 Date Sampled 10/12/2014 10/12/2014 -

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateArsenic (Filtered) mg/L 0.001 <0.001 <0.001 - ND -Cadmium (Filtered) mg/L 0.0001 0.0001 <0.0001 - 0.00% -Chromium (Filtered) mg/L 0.001 <0.001 <0.001 - ND -Copper (Filtered) mg/L 0.001 0.004 0.004 - 0.00% -Lead (Filtered) mg/L 0.001 0.001 0.001 - 0.00% -Mercury (Filtered) mg/L 0.00005 <0.0001 <0.0001 - ND -Nickel (Filtered) mg/L 0.001 0.015 0.017 - 12.50% -Zinc (Filtered) mg/L 0.001 0.454 0.429 - 5.66% -Benzene mg/L 0.001 <0.001 <0.001 - ND -Toluene mg/L 0.001 <0.002 <0.002 - ND -Ethylbenzene mg/L 0.001 <0.002 <0.002 - ND -Xylenes (m & p) mg/L 0.002 <0.002 <0.002 - ND -Xylene (o) mg/L 0.001 <0.002 <0.002 - ND -Xylenes (Sum of total) (Lab Reported) mg/L 0.002 <0.002 <0.002 - ND -Total BTEX mg/L 0.001 <0.001 <0.001 - ND -Acenaphthene mg/L 0.001 <0.001 <0.001 - ND -Acenaphthylene mg/L 0.001 <0.001 <0.001 - ND -Anthracene mg/L 0.001 <0.001 <0.001 - ND -Benz(a)anthracene mg/L 0.001 <0.001 <0.001 - ND -Benzo(a)pyrene mg/L 0.0005 <0.0005 <0.0005 - ND -Benzo(a)pyrene (TEQs) mg/L 0.0005 <0.0005 <0.0005 - ND -Benzo(b)&(j)fluoranthene mg/L 0.001 <0.001 <0.001 - ND -Benzo(g,h,i)perylene mg/L 0.001 <0.001 <0.001 - ND -Benzo(k)fluoranthene mg/L 0.001 <0.001 <0.001 - ND -Chrysene mg/L 0.001 <0.001 <0.001 - ND -Dibenz(a,h)anthracene mg/L 0.001 <0.001 <0.001 - ND -Fluoranthene mg/L 0.001 <0.001 <0.001 - ND -Fluorene mg/L 0.001 <0.001 <0.001 - ND -Indeno(1,2,3-c,d)pyrene mg/L 0.001 <0.001 <0.001 - ND -Naphthalene mg/L 0.001 <0.001 <0.001 - ND -Phenanthrene mg/L 0.001 <0.001 <0.001 - ND -Pyrene mg/L 0.001 <0.001 <0.001 - ND -PAH (Sum of Common 16 PAHs - Lab Reported) mg/L 0.0005 <0.0005 <0.0005 - ND -TRH C6 - C9 Fraction mg/L 0.01 <0.02 <0.02 - ND -TRH C10 - C14 Fraction mg/L 0.05 <0.05 <0.05 - ND -TRH C15 - C28 Fraction mg/L 0.1 <0.1 <0.1 - ND -TRH C29 - C36 Fraction mg/L 0.05 <0.05 <0.05 - ND -TRH+C10 - C40 (Sum of total) (Lab Reported) mg/L 0.1 <0.1 <0.1 - ND -TRH C6 - C10 Fraction F1 mg/L 0.01 <0.02 <0.02 - ND -TRH C6 - C10 Fraction Less BTEX F1 mg/L 0.01 <0.02 <0.02 - ND -TRH >C10 - C16 Fraction F2 mg/L 0.05 <0.1 <0.1 - ND -TRH >C10 - C16 Fraction Less Naphthalene F2 mg/L 0.05 <0.1 <0.1 - ND -TRH >C16 - C34 Fraction F3 mg/L 0.1 <0.1 <0.1 - ND -TRH >C34 - C40 Fraction F4 mg/L 0.1 <0.1 <0.1 - ND -




RPDs



Duplicate Analysis RPDs Sample ID BHB2_10/12/14 QC103_10/12/14 QC104_10/12/14Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1427638 & 120886 Date Sampled 10/12/2014 10/12/2014 10/12/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter Duplicate1,2,4-trimethylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,3,5-Trimethylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDBenzene mg/L 0.001 <0.001 <0.001 <0.001 ND NDToluene mg/L 0.001 <0.002 <0.002 <0.001 ND NDIsopropylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDn-Butylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDn-Propylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDp-Isopropyltoluene mg/L 0.001 <0.005 <0.005 <0.001 ND NDsec-Butylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDStyrene mg/L 0.001 <0.005 <0.005 <0.001 ND NDtert-Butylbenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDEthylbenzene mg/L 0.001 <0.002 <0.002 <0.001 ND NDXylenes (m & p) mg/L 0.002 <0.002 <0.002 <0.002 ND NDXylene (o) mg/L 0.001 <0.002 <0.002 <0.001 ND NDXylenes (Sum of total) (Lab Reported) mg/L 0.002 <0.002 <0.002 - ND -Total BTEX mg/L 0.001 <0.001 <0.001 - ND -Acenaphthene mg/L 0.001 <0.001 <0.001 <0.001 ND NDAcenaphthylene mg/L 0.001 <0.001 <0.001 <0.001 ND NDAnthracene mg/L 0.001 <0.001 <0.001 <0.001 ND NDBenz(a)anthracene mg/L 0.001 <0.001 <0.001 <0.001 ND NDBenzo(a)pyrene mg/L 0.0005 <0.0005 <0.0005 <0.001 ND NDBenzo(a)pyrene (TEQs) mg/L 0.0005 <0.0005 <0.0005 <0.005 ND NDBenzo(b)&(k)fluoranthene mg/L 0.002 - - <0.002 - -Benzo(b)&(j)fluoranthene mg/L 0.001 <0.001 <0.001 - ND -Benzo(b)fluoranthene mg/L 0.01 - - <0.01 - -Benzo(g,h,i)perylene mg/L 0.001 <0.001 <0.001 <0.001 ND NDBenzo(k)fluoranthene mg/L 0.001 <0.001 <0.001 <0.01 ND NDChrysene mg/L 0.001 <0.001 <0.001 <0.001 ND NDDibenz(a,h)anthracene mg/L 0.001 <0.001 <0.001 <0.001 ND NDFluoranthene mg/L 0.001 <0.001 <0.001 <0.001 ND NDFluorene mg/L 0.001 <0.001 <0.001 <0.001 ND NDIndeno(1,2,3-c,d)pyrene mg/L 0.001 <0.001 <0.001 <0.001 ND NDNaphthalene mg/L 0.001 <0.001 <0.001 <0.001 ND NDPhenanthrene mg/L 0.001 <0.001 <0.001 <0.001 ND NDPyrene mg/L 0.001 <0.001 <0.001 <0.001 ND NDPAH (Sum of Common 16 PAHs - Lab Reported) mg/L 0.0005 <0.0005 <0.0005 0 ND ND2-Chloronaphthalene mg/L 0.002 <0.002 <0.002 <0.002 ND ND2-Methylnaphthalene mg/L 0.002 <0.002 <0.002 <0.002 ND ND3-Methylcholanthrene mg/L 0.002 <0.002 <0.002 <0.002 ND ND7,12-Dimethylbenz(a)anthracene mg/L 0.002 <0.002 <0.002 <0.002 ND NDTRH C6 - C9 Fraction mg/L 0.01 0.13 0.13 0.11 0.00% 16.67%TRH C10 - C14 Fraction mg/L 0.05 <0.05 <0.05 <0.05 ND NDTRH C15 - C28 Fraction mg/L 0.1 <0.1 <0.1 <0.1 ND NDTRH C29 - C36 Fraction mg/L 0.05 <0.05 <0.05 <0.1 ND NDTRH+C10 - C36 (Sum of total) (Calculated) mg/L <0.2 <0.2 <0.25 ND NDTRH+C10 - C40 (Sum of total) (Lab Reported) mg/L 0.1 <0.1 <0.1 - ND -TRH C6 - C10 Fraction F1 mg/L 0.01 0.13 0.13 0.11 0.00% 16.67%TRH C6 - C10 Fraction Less BTEX F1 mg/L 0.01 0.13 0.13 0.11 0.00% 16.67%TRH >C10 - C16 Fraction F2 mg/L 0.05 <0.1 <0.1 <0.05 ND NDTRH >C10 - C16 Fraction Less Naphthalene F2 mg/L 0.05 <0.1 <0.1 <0.05 ND NDTRH >C16 - C34 Fraction F3 mg/L 0.1 <0.1 <0.1 <0.1 ND NDTRH >C34 - C40 Fraction F4 mg/L 0.1 <0.1 <0.1 <0.1 ND ND2-(Acetylamino) fluorene mg/L 0.002 <0.002 <0.002 <0.002 ND ND2-Picoline mg/L 0.002 <0.002 <0.002 - ND -3,3-Dichlorobenzidine mg/L 0.002 <0.002 <0.002 - ND -4-(Dimethylamino) azobenzene mg/L 0.002 <0.002 <0.002 <0.005 ND ND4-Aminobiphenyl mg/L 0.002 <0.002 <0.002 - ND -4-Bromophenyl phenyl ether mg/L 0.002 <0.002 <0.002 <0.005 ND ND4-Chlorophenyl phenyl ether mg/L 0.002 <0.002 <0.002 <0.005 ND ND4-Nitroquinoline-n-oxide mg/L 0.002 <0.002 <0.002 - ND -Acetophenone mg/L 0.002 <0.002 <0.002 <0.005 ND NDAzobenzene mg/L 0.002 <0.002 <0.002 <0.005 ND NDBenzyl alcohol mg/L 0.005 - - <0.005 ND NDBis(2-chloroethoxy) methane mg/L 0.002 <0.002 <0.002 <0.005 ND NDBis(2-chloroethyl) ether mg/L 0.002 <0.002 <0.002 <0.005 ND NDBis(2-chloroisopropyl) ether mg/L 0.005 - - <0.005 ND NDDibenzofuran mg/L 0.002 <0.002 <0.002 <0.005 ND NDEthylmethanesulfonate mg/L 0.005 - - <0.005 ND NDHexachlorocyclopentadiene mg/L 0.005 <0.01 <0.01 <0.005 ND NDHexachloropropene mg/L 0.002 <0.002 <0.002 <0.002 ND NDtrans-Isosafrole mg/L 0.01 - - <0.01 ND NDMethapyrilene mg/L 0.002 <0.002 <0.002 <0.01 ND NDn-Nitrosomorpholine mg/L 0.002 <0.002 <0.002 <0.005 ND NDN-Nitrosopiperidine mg/L 0.002 <0.002 <0.002 <0.005 ND NDn-Nitrosopyrrolidine mg/L 0.004 <0.004 <0.004 - ND -Phenacetin mg/L 0.002 <0.002 <0.002 <0.005 ND NDSafrole mg/L 0.005 - - <0.005 ND ND1,1,1,2-Tetrachloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1,2,2-Tetrachloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1,1-Trichloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1,2-Trichloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2,3-Trichloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2-Dibromo-3-chloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2-Dibromoethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1-Dichloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2-Dichloroethane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1-Dichloroethene mg/L 0.001 <0.005 <0.005 <0.001 ND NDcis-1,2-Dichloroethene mg/L 0.001 0.008 0.009 0.01 11.76% 22.22%trans-1,2-dichloroethene mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2-Dichloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,3-Dichloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND2,2-Dichloropropane mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,1-Dichloropropene mg/L 0.001 <0.005 <0.005 <0.001 ND NDcis-1,3-Dichloropropene mg/L 0.001 <0.005 <0.005 <0.001 ND NDtrans-1,3-dichloropropene mg/L 0.001 <0.005 <0.005 <0.001 ND NDcis-1,4-Dichloro-2-butene mg/L 0.005 <0.005 <0.005 - ND -trans-1,4-Dichloro-2-butene mg/L 0.005 <0.005 <0.005 - ND -Bromochloromethane mg/L 0.001 - - <0.001 ND NDBromodichloromethane mg/L 0.001 <0.005 <0.005 <0.001 ND NDBromoform ug/L 1 <5 <5 <1 ND NDBromomethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDCarbon disulfide mg/L 0.005 <0.005 <0.005 - ND -Carbon tetrachloride mg/L 0.001 <0.005 <0.005 <0.001 ND NDChlorodibromomethane mg/L 0.001 <0.005 <0.005 <0.001 ND NDChloroethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDChloroform mg/L 0.001 <0.005 <0.005 <0.001 ND NDChloromethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDDibromomethane ug/L 1 <5 <5 <1 ND NDDichlorodifluoromethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDHexachlorobutadiene mg/L 0.001 <0.002 <0.002 <0.001 ND NDHexachloroethane mg/L 0.002 <0.002 <0.002 <0.002 ND NDIodomethane mg/L 0.005 <0.005 <0.005 - ND -Pentachloroethane mg/L 0.002 <0.005 <0.005 <0.002 ND NDTrichloroethene mg/L 0.001 0.145 0.154 0.17 6.02% 15.87%Tetrachloroethene mg/L 0.001 <0.005 <0.005 0.004 ND NDTrichlorofluoromethane mg/L 0.01 <0.05 <0.05 <0.01 ND NDVinyl chloride mg/L 0.01 <0.05 <0.05 <0.01 ND NDn-Nitrosodiethylamine mg/L 0.002 <0.002 <0.002 - ND -N-Nitrosodi-n-butylamine mg/L 0.002 <0.002 <0.002 <0.005 ND NDN-Nitrosodi-n-propylamine mg/L 0.002 <0.002 <0.002 <0.005 ND NDn-Nitrosomethylethylamine mg/L 0.002 <0.002 <0.002 - ND -1-Naphthylamine mg/L 0.002 <0.002 <0.002 <0.005 ND ND2-Naphthylamine mg/L 0.005 - - <0.005 - -Diphenylamine mg/L 0.005 - - <0.005 - -n-Nitrosodiphenylamine & Diphenylamine mg/L 0.004 <0.004 <0.004 - ND -2-Nitroaniline mg/L 0.004 <0.004 <0.004 <0.005 ND ND3-Nitroaniline mg/L 0.004 <0.004 <0.004 <0.005 ND ND4-Chloroaniline mg/L 0.002 <0.002 <0.002 <0.005 ND ND4-Nitroaniline mg/L 0.002 <0.002 <0.002 <0.005 ND ND2-methyl-5-nitroaniline mg/L 0.002 <0.002 <0.002 <0.005 ND NDAniline mg/L 0.002 <0.002 <0.002 <0.005 ND NDNitrobenzene mg/L 0.002 <0.002 <0.002 <0.005 ND ND


RPDs



Pentachloronitrobenzene mg/L 0.002 <0.002 <0.002 <0.005 ND ND1,3,5-Trinitrobenzene mg/L 0.002 <0.002 <0.002 - ND -1,3-Dinitrobenzene mg/L 0.005 - - <0.005 - -2,4-Dinitrotoluene mg/L 0.004 <0.004 <0.004 - ND -2,6-Dinitrotoluene mg/L 0.004 <0.004 <0.004 <0.005 ND ND1,2,3-Trichlorobenzene mg/L 0.001 <0.005 <0.005 <0.001 ND ND1,2,4,5-Tetrachlorobenzene mg/L 0.002 - - <0.002 - -1,2,4-Trichlorobenzene mg/L 0.001 <0.002 <0.002 <0.001 ND ND1,2-Dichlorobenzene mg/L 0.001 <0.002 <0.002 <0.001 ND ND1,3-Dichlorobenzene mg/L 0.001 <0.002 <0.002 <0.001 ND ND1,4-Dichlorobenzene mg/L 0.001 <0.002 <0.002 <0.001 ND ND2-Chlorotoluene mg/L 0.001 <0.005 <0.005 <0.001 ND ND4-Chlorotoluene mg/L 0.001 <0.005 <0.005 <0.001 ND NDBromobenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDChlorobenzene mg/L 0.001 <0.005 <0.005 <0.001 ND NDHexachlorobenzene mg/L 0.002 <0.004 <0.004 <0.002 ND NDPentachlorobenzene mg/L 0.002 <0.002 <0.002 <0.002 ND NDDinoseb mg/L 0.02 - - <0.02 - -Pronamide mg/L 0.002 <0.002 <0.002 - ND -a-BHC mg/L 0.002 <0.002 <0.002 <0.002 ND NDAldrin mg/L 0.002 <0.002 <0.002 <0.002 ND NDAldrin & Dieldrin (Sum of total) (Lab Reported) mg/L 0.004 <0.004 <0.004 - ND -b-BHC mg/L 0.002 <0.002 <0.002 <0.002 ND NDcis-Chlordane mg/L 0.002 - - <0.002 - -trans-Chlordane mg/L 0.002 - - <0.002 - -d-BHC mg/L 0.002 <0.002 <0.002 <0.002 ND NDDDD mg/L 0.002 <0.002 <0.002 <0.002 ND NDDDE mg/L 0.002 <0.002 <0.002 <0.002 ND NDDDT mg/L 0.002 <0.004 <0.004 <0.002 ND NDDDT+DDE+DDD (Sum of total) (Lab Reported) mg/L 0.004 <0.004 <0.004 - ND -Dieldrin mg/L 0.002 <0.002 <0.002 <0.002 ND NDEndosulfan I mg/L 0.002 <0.002 <0.002 <0.002 ND NDEndosulfan II mg/L 0.002 <0.002 <0.002 <0.002 ND NDEndosulfan sulphate mg/L 0.002 <0.002 <0.002 <0.002 ND NDEndrin mg/L 0.002 <0.002 <0.002 <0.002 ND NDEndrin aldehyde mg/L 0.002 - - <0.002 - -g-BHC mg/L 0.002 <0.002 <0.002 <0.002 ND NDHeptachlor mg/L 0.002 <0.002 <0.002 <0.002 ND NDHeptachlor & heptachlor epoxide (Sum Lab Reported) mg/l 0.002 <0.002 <0.002 - ND -Heptachlor epoxide mg/L 0.002 <0.002 <0.002 <0.002 ND NDChlorfenvinphos mg/L 0.002 <0.002 <0.002 - ND -Chlorpyriphos mg/L 0.002 <0.002 <0.002 - ND -Chlorpyriphos-methyl mg/L 0.002 <0.002 <0.002 - ND -Diazinon mg/L 0.002 <0.002 <0.002 - ND -Dichlorvos mg/L 0.002 <0.002 <0.002 - ND -Dimethoate mg/L 0.002 <0.002 <0.002 - ND -Ethion mg/L 0.002 <0.002 <0.002 - ND -Fenthion mg/L 0.002 <0.002 <0.002 - ND -Malathion mg/L 0.002 <0.002 <0.002 - ND -Pirimphos-ethyl mg/L 0.002 <0.002 <0.002 - ND -Prothiofos mg/L 0.002 <0.002 <0.002 - ND -Carbazole mg/L 0.002 <0.002 <0.002 <0.005 ND NDChlorobenzilate mg/L 0.002 <0.002 <0.002 - ND -2,4-Dimethylphenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND2,4-Dinitrophenol mg/L 0.02 - - <0.02 - -2-Methylphenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND2-Nitrophenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND3- & 4- Methylphenol mg/L 0.004 <0.004 <0.004 - ND -4,6-Dinitro-2-methylphenol mg/L 0.02 - - <0.02 - -4-Methylphenol mg/L 0.004 - - <0.004 - -4-Nitrophenol mg/L 0.02 - - <0.02 - -Phenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND2,3,4,6-Tetrachlorophenol mg/L 0.002 - - <0.002 - -2,4,5-Trichlorophenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND2,4,6-Trichlorophenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND2,4-Dichlorophenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND2,6-Dichlorophenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND2-Chlorophenol mg/L 0.002 <0.002 <0.002 <0.002 ND ND4-Chloro-3-methylphenol mg/L 0.002 <0.002 <0.002 - ND -Pentachlorophenol mg/L 0.004 <0.004 <0.004 <0.01 ND NDBis(2-ethylhexyl) phthalate mg/L 0.01 <0.01 <0.01 <0.01 ND NDButylbenzyl phthalate mg/L 0.002 <0.002 <0.002 <0.01 ND NDDiethyl phthalate mg/L 0.002 <0.002 <0.002 <0.01 ND NDDimethyl phthalate mg/L 0.002 <0.002 <0.002 <0.01 ND NDDi-n-butyl phthalate mg/L 0.002 <0.002 <0.002 <0.01 ND NDDi-n-octyl phthalate mg/L 0.002 <0.002 <0.002 <0.01 ND NDAroclor 1016 mg/L 0.002 - - <0.002 - -Aroclor 1232 mg/L 0.002 - - <0.002 - -Aroclor 1242 mg/L 0.002 - - <0.002 - -Aroclor 1248 mg/L 0.002 - - <0.002 - -Aroclor 1254 mg/L 0.002 - - <0.002 - -Aroclor 1260 mg/L 0.002 - - <0.002 - -Aroclor 1221 mg/L 0.002 - - <0.002 - -PCB (Sum of Total-Lab Reported) mg/L 0.001 <0.001 <0.001 ND ND NDMethyl Ethyl Ketone mg/L 0.05 <0.05 <0.05 - ND -2-Hexanone mg/L 0.05 <0.05 <0.05 - ND -Methyl iso-butyl ketone mg/L 0.05 <0.05 <0.05 - ND -Cyclohexane mg/L 0.001 - - <0.001 - -Isophorone mg/L 0.002 <0.002 <0.002 <0.005 ND NDVinyl acetate mg/L 0.05 <0.05 <0.05 - ND -





Duplicate Analysis RPDs Sample ID BHB3_10/12/14 QC105_10/12/14 -Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1427638 & 120886 Date Sampled 10/12/2014 10/12/2014 -

Analyte Units LOR Primary vs Duplicate Primary vs Inter Duplicate1,2,4-trimethylbenzene mg/L 0.001 <0.005 <0.005 - ND -1,3,5-Trimethylbenzene mg/L 0.001 <0.005 <0.005 - ND -Benzene mg/L 0.001 <0.001 <0.001 - ND -Toluene mg/L 0.001 <0.002 <0.002 - ND -Isopropylbenzene mg/L 0.001 <0.005 <0.005 - ND -n-Butylbenzene mg/L 0.001 <0.005 <0.005 - ND -n-Propylbenzene mg/L 0.001 <0.005 <0.005 - ND -p-Isopropyltoluene mg/L 0.001 <0.005 <0.005 - ND -sec-Butylbenzene mg/L 0.001 <0.005 <0.005 - ND -Styrene mg/L 0.001 <0.005 <0.005 - ND -tert-Butylbenzene mg/L 0.001 <0.005 <0.005 - ND -Ethylbenzene mg/L 0.001 <0.002 <0.002 - ND -Xylenes (m & p) mg/L 0.002 <0.002 <0.002 - ND -Xylene (o) mg/L 0.001 <0.002 <0.002 - ND -Xylenes (Sum of total) (Lab Reported) mg/L 0.002 <0.002 <0.002 - ND -Total BTEX mg/L 0.001 <0.001 <0.001 - ND -Acenaphthene mg/L 0.001 <0.001 <0.001 - ND -Acenaphthylene mg/L 0.001 <0.001 <0.001 - ND -Anthracene mg/L 0.001 <0.001 <0.001 - ND -Benz(a)anthracene mg/L 0.001 <0.001 <0.001 - ND -Benzo(a)pyrene mg/L 0.0005 <0.0005 <0.0005 - ND -Benzo(a)pyrene (TEQs) mg/L 0.0005 <0.0005 <0.0005 - ND -Benzo(b)&(j)fluoranthene mg/L 0.001 <0.001 <0.001 - ND -Benzo(g,h,i)perylene mg/L 0.001 <0.001 <0.001 - ND -Benzo(k)fluoranthene mg/L 0.001 <0.001 <0.001 - ND -Chrysene mg/L 0.001 <0.001 <0.001 - ND -Dibenz(a,h)anthracene mg/L 0.001 <0.001 <0.001 - ND -Fluoranthene mg/L 0.001 <0.001 <0.001 - ND -Fluorene mg/L 0.001 <0.001 <0.001 - ND -Indeno(1,2,3-c,d)pyrene mg/L 0.001 <0.001 <0.001 - ND -Naphthalene mg/L 0.001 <0.001 <0.001 - ND -Phenanthrene mg/L 0.001 <0.001 <0.001 - ND -Pyrene mg/L 0.001 <0.001 <0.001 - ND -PAH (Sum of Common 16 PAHs - Lab Reported) mg/L 0.0005 <0.0005 <0.0005 - ND -2-Chloronaphthalene mg/L 0.002 <0.002 <0.002 - ND -2-Methylnaphthalene mg/L 0.002 <0.002 <0.002 - ND -3-Methylcholanthrene mg/L 0.002 <0.002 <0.002 - ND -7,12-Dimethylbenz(a)anthracene mg/L 0.002 <0.002 <0.002 - ND -TRH C6 - C9 Fraction mg/L 0.01 0.24 0.25 - 4.08% -TRH C10 - C14 Fraction mg/L 0.05 <0.05 <0.05 - ND -TRH C15 - C28 Fraction mg/L 0.1 <0.1 <0.1 - ND -TRH C29 - C36 Fraction mg/L 0.05 <0.05 <0.05 - ND -TRH+C10 - C40 (Sum of total) (Lab Reported) mg/L 0.1 <0.1 <0.1 - ND -TRH C6 - C10 Fraction F1 mg/L 0.01 0.24 0.25 - 4.08% -TRH C6 - C10 Fraction Less BTEX F1 mg/L 0.01 0.24 0.25 - 4.08% -TRH >C10 - C16 Fraction F2 mg/L 0.05 <0.1 <0.1 - ND -TRH >C10 - C16 Fraction Less Naphthalene F2 mg/L 0.05 <0.1 <0.1 - ND -TRH >C16 - C34 Fraction F3 mg/L 0.1 <0.1 <0.1 - ND -TRH >C34 - C40 Fraction F4 mg/L 0.1 <0.1 <0.1 - ND -2-(Acetylamino) fluorene mg/L 0.002 <0.002 <0.002 - ND -2-Picoline mg/L 0.002 <0.002 <0.002 - ND -3,3-Dichlorobenzidine mg/L 0.002 <0.002 <0.002 - ND -4-(Dimethylamino) azobenzene mg/L 0.002 <0.002 <0.002 - ND -4-Aminobiphenyl mg/L 0.002 <0.002 <0.002 - ND -4-Bromophenyl phenyl ether mg/L 0.002 <0.002 <0.002 - ND -4-Chlorophenyl phenyl ether mg/L 0.002 <0.002 <0.002 - ND -4-Nitroquinoline-n-oxide mg/L 0.002 <0.002 <0.002 - ND -Acetophenone mg/L 0.002 <0.002 <0.002 - ND -Azobenzene mg/L 0.002 <0.002 <0.002 - ND -Bis(2-chloroethoxy) methane mg/L 0.002 <0.002 <0.002 - ND -Bis(2-chloroethyl) ether mg/L 0.002 <0.002 <0.002 - ND -Dibenzofuran mg/L 0.002 <0.002 <0.002 - ND -Hexachlorocyclopentadiene mg/L 0.005 <0.01 <0.01 - ND -Hexachloropropene mg/L 0.002 <0.002 <0.002 - ND -Methapyrilene mg/L 0.002 <0.002 <0.002 - ND -n-Nitrosomorpholine mg/L 0.002 <0.002 <0.002 - ND -N-Nitrosopiperidine mg/L 0.002 <0.002 <0.002 - ND -n-Nitrosopyrrolidine mg/L 0.004 <0.004 <0.004 - ND -Phenacetin mg/L 0.002 <0.002 <0.002 - ND -1,1,1,2-Tetrachloroethane mg/L 0.001 <0.005 <0.005 - ND -1,1,2,2-Tetrachloroethane mg/L 0.001 <0.005 <0.005 - ND -1,1,1-Trichloroethane mg/L 0.001 <0.005 <0.005 - ND -1,1,2-Trichloroethane mg/L 0.001 <0.005 <0.005 - ND -1,2,3-Trichloropropane mg/L 0.001 <0.005 <0.005 - ND -1,2-Dibromo-3-chloropropane mg/L 0.001 <0.005 <0.005 - ND -1,2-Dibromoethane mg/L 0.001 <0.005 <0.005 - ND -1,1-Dichloroethane mg/L 0.001 <0.005 <0.005 - ND -1,2-Dichloroethane mg/L 0.001 <0.005 <0.005 - ND -1,1-Dichloroethene mg/L 0.001 <0.005 <0.005 - ND -cis-1,2-Dichloroethene mg/L 0.001 0.02 0.022 - 9.52% -trans-1,2-dichloroethene mg/L 0.001 <0.005 <0.005 - ND -1,2-Dichloropropane mg/L 0.001 <0.005 <0.005 - ND -1,3-Dichloropropane mg/L 0.001 <0.005 <0.005 - ND -2,2-Dichloropropane mg/L 0.001 <0.005 <0.005 - ND -1,1-Dichloropropene mg/L 0.001 <0.005 <0.005 - ND -cis-1,3-Dichloropropene mg/L 0.001 <0.005 <0.005 - ND -trans-1,3-dichloropropene mg/L 0.001 <0.005 <0.005 - ND -cis-1,4-Dichloro-2-butene mg/L 0.005 <0.005 <0.005 - ND -trans-1,4-Dichloro-2-butene mg/L 0.005 <0.005 <0.005 - ND -Bromodichloromethane mg/L 0.001 <0.005 <0.005 - ND -Bromoform ug/L 1 <5 <5 - ND -Bromomethane mg/L 0.01 <0.05 <0.05 - ND -Carbon disulfide mg/L 0.005 <0.005 <0.005 - ND -Carbon tetrachloride mg/L 0.001 <0.005 <0.005 - ND -Chlorodibromomethane mg/L 0.001 <0.005 <0.005 - ND -Chloroethane mg/L 0.01 <0.05 <0.05 - ND -Chloroform mg/L 0.001 <0.005 <0.005 - ND -Chloromethane mg/L 0.01 <0.05 <0.05 - ND -Dibromomethane ug/L 1 <5 <5 - ND -Dichlorodifluoromethane mg/L 0.01 <0.05 <0.05 - ND -Hexachlorobutadiene mg/L 0.001 <0.002 <0.002 - ND -Hexachloroethane mg/L 0.002 <0.002 <0.002 - ND -Iodomethane mg/L 0.005 <0.005 <0.005 - ND -Pentachloroethane mg/L 0.002 <0.005 <0.005 - ND -Trichloroethene mg/L 0.001 0.303 0.307 - 1.31% -Tetrachloroethene mg/L 0.001 <0.005 <0.005 - ND -Trichlorofluoromethane mg/L 0.01 <0.05 <0.05 - ND -Vinyl chloride mg/L 0.01 <0.05 <0.05 - ND -n-Nitrosodiethylamine mg/L 0.002 <0.002 <0.002 - ND -N-Nitrosodi-n-butylamine mg/L 0.002 <0.002 <0.002 - ND -N-Nitrosodi-n-propylamine mg/L 0.002 <0.002 <0.002 - ND -n-Nitrosomethylethylamine mg/L 0.002 <0.002 <0.002 - ND -


RPDs



1-Naphthylamine mg/L 0.002 <0.002 <0.002 - ND -n-Nitrosodiphenylamine & Diphenylamine mg/L 0.004 <0.004 <0.004 - ND -2-Nitroaniline mg/L 0.004 <0.004 <0.004 - ND -3-Nitroaniline mg/L 0.004 <0.004 <0.004 - ND -4-Chloroaniline mg/L 0.002 <0.002 <0.002 - ND -4-Nitroaniline mg/L 0.002 <0.002 <0.002 - ND -2-methyl-5-nitroaniline mg/L 0.002 <0.002 <0.002 - ND -Aniline mg/L 0.002 <0.002 <0.002 - ND -Nitrobenzene mg/L 0.002 <0.002 <0.002 - ND -Pentachloronitrobenzene mg/L 0.002 <0.002 <0.002 - ND -1,3,5-Trinitrobenzene mg/L 0.002 <0.002 <0.002 - ND -2,4-Dinitrotoluene mg/L 0.004 <0.004 <0.004 - ND -2,6-Dinitrotoluene mg/L 0.004 <0.004 <0.004 - ND -1,2,3-Trichlorobenzene mg/L 0.001 <0.005 <0.005 - ND -1,2,4-Trichlorobenzene mg/L 0.001 <0.002 <0.002 - ND -1,2-Dichlorobenzene mg/L 0.001 <0.002 <0.002 - ND -1,3-Dichlorobenzene mg/L 0.001 <0.002 <0.002 - ND -1,4-Dichlorobenzene mg/L 0.001 <0.002 <0.002 - ND -2-Chlorotoluene mg/L 0.001 <0.005 <0.005 - ND -4-Chlorotoluene mg/L 0.001 <0.005 <0.005 - ND -Bromobenzene mg/L 0.001 <0.005 <0.005 - ND -Chlorobenzene mg/L 0.001 <0.005 <0.005 - ND -Hexachlorobenzene mg/L 0.002 <0.004 <0.004 - ND -Pentachlorobenzene mg/L 0.002 <0.002 <0.002 - ND -Pronamide mg/L 0.002 <0.002 <0.002 - ND -a-BHC mg/L 0.002 <0.002 <0.002 - ND -Aldrin mg/L 0.002 <0.002 <0.002 - ND -Aldrin & Dieldrin (Sum of total) (Lab Reported) mg/L 0.004 <0.004 <0.004 - ND -b-BHC mg/L 0.002 <0.002 <0.002 - ND -d-BHC mg/L 0.002 <0.002 <0.002 - ND -DDD mg/L 0.002 <0.002 <0.002 - ND -DDE mg/L 0.002 <0.002 <0.002 - ND -DDT mg/L 0.002 <0.004 <0.004 - ND -DDT+DDE+DDD (Sum of total) (Lab Reported) mg/L 0.004 <0.004 <0.004 - ND -Dieldrin mg/L 0.002 <0.002 <0.002 - ND -Endosulfan I mg/L 0.002 <0.002 <0.002 - ND -Endosulfan II mg/L 0.002 <0.002 <0.002 - ND -Endosulfan sulphate mg/L 0.002 <0.002 <0.002 - ND -Endrin mg/L 0.002 <0.002 <0.002 - ND -g-BHC mg/L 0.002 <0.002 <0.002 - ND -Heptachlor mg/L 0.002 <0.002 <0.002 - ND -Heptachlor & heptachlor epoxide (Sum Lab Reported) mg/l 0.002 <0.002 <0.002 - ND -Heptachlor epoxide mg/L 0.002 <0.002 <0.002 - ND -Chlorfenvinphos mg/L 0.002 <0.002 <0.002 - ND -Chlorpyriphos mg/L 0.002 <0.002 <0.002 - ND -Chlorpyriphos-methyl mg/L 0.002 <0.002 <0.002 - ND -Diazinon mg/L 0.002 <0.002 <0.002 - ND -Dichlorvos mg/L 0.002 <0.002 <0.002 - ND -Dimethoate mg/L 0.002 <0.002 <0.002 - ND -Ethion mg/L 0.002 <0.002 <0.002 - ND -Fenthion mg/L 0.002 <0.002 <0.002 - ND -Malathion mg/L 0.002 <0.002 <0.002 - ND -Pirimphos-ethyl mg/L 0.002 <0.002 <0.002 - ND -Prothiofos mg/L 0.002 <0.002 <0.002 - ND -Carbazole mg/L 0.002 <0.002 <0.002 - ND -Chlorobenzilate mg/L 0.002 <0.002 <0.002 - ND -2,4-Dimethylphenol mg/L 0.002 <0.002 <0.002 - ND -2-Methylphenol mg/L 0.002 <0.002 <0.002 - ND -2-Nitrophenol mg/L 0.002 <0.002 <0.002 - ND -3- & 4- Methylphenol mg/L 0.004 <0.004 <0.004 - ND -Phenol mg/L 0.002 <0.002 <0.002 - ND -2,4,5-Trichlorophenol mg/L 0.002 <0.002 <0.002 - ND -2,4,6-Trichlorophenol mg/L 0.002 <0.002 <0.002 - ND -2,4-Dichlorophenol mg/L 0.002 <0.002 <0.002 - ND -2,6-Dichlorophenol mg/L 0.002 <0.002 <0.002 - ND -2-Chlorophenol mg/L 0.002 <0.002 <0.002 - ND -4-Chloro-3-methylphenol mg/L 0.002 <0.002 <0.002 - ND -Pentachlorophenol mg/L 0.004 <0.004 <0.004 - ND -Bis(2-ethylhexyl) phthalate mg/L 0.01 <0.01 <0.01 - ND -Butylbenzyl phthalate mg/L 0.002 <0.002 <0.002 - ND -Diethyl phthalate mg/L 0.002 <0.002 <0.002 - ND -Dimethyl phthalate mg/L 0.002 <0.002 <0.002 - ND -Di-n-butyl phthalate mg/L 0.002 <0.002 <0.002 - ND -Di-n-octyl phthalate mg/L 0.002 <0.002 <0.002 - ND -PCB (Sum of Total-Lab Reported) mg/L 0.001 <0.001 <0.001 - ND -Methyl Ethyl Ketone mg/L 0.05 <0.05 <0.05 - ND -2-Hexanone mg/L 0.05 <0.05 <0.05 - ND -Methyl iso-butyl ketone mg/L 0.05 <0.05 <0.05 - ND -Isophorone mg/L 0.002 <0.002 <0.002 - ND -Vinyl acetate mg/L 0.05 <0.05 <0.05 - ND -






TypeMBRBRBTB

Sample ID







Matrix spikes were not conducted for PFOS and 6:2 Fluorotelomer sulfonate (6:2 FtS). This is not expected to affect the outcomes of the investigation as the spike was scheduled for an anonymous sample not pertinent tothis investigation.

Metals bottles were not received by ALS for several samples in this batch. This will not affect the outcomes of the investigation as metals bottles were not collected at these locations as metals was not a contaminant ofconcern. Metals analysis was checked on the COC by field personnel as it formed a part of a financially preferable ALS combination (Metals/TRH/BTEX/PAHs).

LCS recovery of Methapyrilene was greater than the upper control limit and may indicate an over-reporting of this analyte in this batch. However, this is not expected to affect the integrity of the data as all concentrations ofMethapyrilene were below the LOR.


Comments

Overall Comments

Field triplicates were not scheduled for analysis in this batch.

CommentsField duplicates were not scheduled for analysis in this batch.



Nitrosamines ALS: Recovery of Methapyrilene (97.3%) was greater than the upper control limit of 94%.


ALS: Laboratory Duplicate analyses were within the laboratory based quality objectives.


Analyte Group

Sample IDAll results were less than the LOR

Comments



TB_11/12/14 All results were less than the LOR

QC108_12/12/14 All results were less than the LORQC109_15/12/14 All results were less than the LOR





Y/N Comments

Samples received intact and chilled? N ALS: Ice present, 5.6'C, security seal not intact.Samples analysed within appropriate holding times?



Y





Several bottles received by ALS were broken on receipt. Consequently, several analyses for PB_MW12 were not conducted by ALS. This will not affect the overall outcomes of the investigation as the well was resampledand submitted to ALS for analysis in batch ES1428622.



Perfluorinated Compounds ALS: Matrix Spike recoveries conducted for PFOS and 6:2 Fluorotelomer sulfonate (6:2 FtS) were not conducted.



All other LCS recoveries from ALS were within the data quality objectives.Matrix Spike (MS) Analyses






Y

Date Sampled: 10/11/2014 - 19/11/2014 Sample Medium: Water

Y

Metals, TPH, BTEXN, PAHs, sVOCs, VOCs and PFOS/PFOAALS received broken bottles for PB_MW12. Only TPH C6-C9/BTEX analysed.Metals not received on several samples. Metals analysis not conducted where bottleswere not available.

Y



TypeMBMBRBRBTB

Benzene 0.2 100%Toluene 14 51%

Ethylbenzene 2 45%meta- & para-Xylene 11.7 44%

ortho-Xylene 4.6 48%Naphthalene 16.3 45%

Sample ID

Analyte Group Primary ID Duplicate IDSS02_0.0 - 0.1 QC100_16/12/14

TP124_001_0.0 - 0.1 QC103_18/12/14TP109_001_0.0 - 0.1 QC106_18/12/14

Heavy Metals TP118_001_0.0 - 0.1 QC108_18/12/14


Heavy Metals TP113b_002_0.8 - 0.9 QC110_19/12/14


TP115_001_0.0-0.1 QC105_18/12/14

Heavy Metals TP212-001_0 - 0.1 QC166

Analyte Group Primary ID Triplicate IDTP124_001_0.0 - 0.1 QC104_18/12/14TP109_001_0.0 - 0.1 QC107_18/12/14TP113b_002_0.8 - 0.9 QC111_19/12/14

TP212-001_0 - 0.1 QC167


TPH/BTEX Toluene-D8

TPH/BTEX 4-Bromofluorobenzene




Metals bottles were not received by ALS for one sample in this batch. This will not affect the outcomes of the investigation as metals was not a contaminant of concern at this location. Metals analysis was checked on the COC by field personnel asit formed a part of a financially preferable ALS combination (Metals/TRH/BTEX/PAHs).

Due to laboratory capacity constraints over the christmas break, extraction and analysis of the samples was delayed by up to one week. The delayed analysis caused several tests to be completed out-side of the recommended holding time. Theanalysis outside of the recommended holding time may have resulted in potential under-reporting of results. This is of most concern for the volatile organic compounds which may have degraded during the extended holding time. This is notexpected to affect the outcomes of the investigation based on the following:This is not expected to affect the outcomes of the investigation based on the following:- While being held by the laboratory, all the samples were refrigerated to 4 degrees and therefore any degradation or volatile loss would have been minimal.- The majority of the samples reported concentrations of volatile compounds below the laboratory limits of reporting, and the limits of reporting are significantly lower than the adopted assessment criteria. Hence, any loss or degradation is unlikely tohave impacted on the interpretation of the analytical results; and- Based on the field observations it is unlikely that the samples initially contained gross concentrations of volatile contaminants.


Comments

No other surrogate outliers were observed in this batch.

Overall Comments

All calculated RPDs achieved the data quality objectives.

CommentsAll calculated RPDs achieved the data quality objectives.

RPD for Chromium (30.77%) does not achieve the data quality objectives.All other RPDs were within the acceptable limits.Field Triplicates (FT) Analyses

Comments

RPD for Lead (33.33%) does not achieve the data quality objectives.All other RPDs were within the acceptable limits.


ALS: All LCS recoveries from ALS were within the data quality objectives.


Recovery of 4-Bromofluorobenzene (71.5%) in sample TP113C_001_0.0-0.1 was less that the lower data quality objective.


N Several samples were analysed outside their appropriate holding times by approximately one week


The surrogate recovery 4-Bromofluorobenzene in sample TP113C_001_0.0-0.1 returned a result less than the data quality objectives. This is not expected to affect the integrity of the data as surrogate recoveries for the other TPH/BTEX surrogates(Toluene-D8 & 1.2-Dichloroethane-D4) achieved the data quality objectives.

Several RPDs calculated for heavy metals on field duplicates (TP118_001, TP118_002, TP113b_002, TP110_001 and TP212_001) did not achieve the data quality objectives. This is likely a result of heterogeneity within the sample matrix. In allcases, the highest result will be adopted for assessment.

The surrogate recovery Toluene-D8 in sample TP113C_002_0.9-1.0 returned a result less than the data quality objectives. This is not expected to affect the integrity of the data as surrogate recoveries for the other TPH/BTEX surrogates (4-Bromofluorobenzene & 1.2-Dichloroethane-D4) achieved the data quality objectives.

Recovered concentrations from the trip spike sample indicate a loss of volatile compounds and a potential under-reporting of the results may have occurred for these volatile compounds. Based on the following, the exceedence is not considered tohave had a material impact on the data:- All samples collected in this batch remained in cooler boxes chilled with ice for the entirety of the sampling program and throughout transit to the laboratory;- All samples in this batch reported concentrations of volatile compounds below the laboratory limits of reporting, and the limits of reporting are significantly lower than the adopted assessment criteria. Hence, any loss or degradation is unlikely tohave impacted on the interpretation of the analytical results; and- Based on the field observations it is unlikely that the samples initially contained gross concentrations of volatile contaminants.

7.3 Recovery below the acceptable control limit of 70%

CommentsALS: Laboratory Duplicate analyses were within the laboratory based quality objectives.ELS: Laboratory Duplicate analyses were not conducted by ELSField Duplicates (FD) Analyses

Analyte Group

Sample ID

ELS: MS recoveries were not conducted by ELS


Comments



TRIP BLANK All results were less than the LOR

Method Blank ELS: All results were less than the LOR

QC102_17/12/14 All results were less than the LORQC101_16/12/14

Recovery below the acceptable control limit of 70%








Y/N Comments

Samples received intact and chilled? Y ALS: Ice present, 9.3'CELS: Ice present, 5.2'C




Y


Project Name: MIC - MIT Site Investigation Project Number: 147623070Primary Laboratory: ALS Workorder Number: ES1428622Secondary Laboratory: Envirolab (ELS) Workorder Number: 121411


Recovery of Toluene-D8 (72.2%) in sample TP113C_002_0.9-1.0 was less that the lower data quality objective.

As stated by ALS "The TRIP SPIKE and TRIP SPIKE CONTROL have been analysed for volatile TPH and BTEX only. The TRIP SPIKE and TRIP SPIKE CONTROL were prepared in the lab using reagent grade sand spiked with petrol. The TRIPSPIKE was dispatched from the lab and the TRIP SPIKE CONTROL retained. The spike samples were extracted and analysed concurrently with samples reported in this batch."

2.2 Recovery below the acceptable control limit of 70%


ALS: All MS recoveries from ALS were within the data quality objectives.


Analyte Control SpikeConcentrations Trip Spike Concentration % Recovery

ELS: All LCS recoveries from ELS were within the data quality objectives.Matrix Spike (MS) Analyses




0.9 Recovery below the acceptable control limit of 70%5.1 Recovery below the acceptable control limit of 70%

<0.2 Recovery within the acceptable control limits (70 - 130%)7.2

Date Sampled: 11/12/2014 - 19/12/14 Sample Medium: Soil/Water

Y pH, CEC, Metals, TPH, BTEXN, PAHs, Phenols, OCPs, OPPs, PCBs, sVOCs, VOCs and AsbestosMetals not received for sample PB_MW12 Metals analysis not conducted.

YAre there non-NATA accredited methods used? Y Asbestos weights and percentages are not covered by NATA

Sample ID: TRIP SPIKE

RPD for Mercury (85.71%) does not achieve the data quality objectives.All other RPDs were within the acceptable limits.

RPD for Zinc (66.67%) does not achieve the data quality objectives.All other RPDs were within the acceptable limits.

All calculated RPDs achieved the data quality objectives.All calculated RPDs achieved the data quality objectives.RPD for Lead (88.52%) does not achieve the data quality objectives.All other RPDs were within the acceptable limits.

Golder Associates Pty Ltd.

Duplicate Analysis RPDs Sample ID SS02_0.0 - 0.1 QC100_16/12/14 -Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1428622 & 121411 Date Sampled 16/12/2014 16/12/2014 -

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 - ND -TRH C10 - C14 Fraction mg/kg 50 <50 <50 - ND -TRH C15 - C28 Fraction mg/kg 100 <100 <100 - ND -TRH C29 - C36 Fraction mg/kg 100 <100 <100 - ND -TRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 - ND -TRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 - ND -TRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 - ND -TRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 - ND -TRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 - ND -TRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 - ND -Benzene mg/kg 0.2 <0.2 <0.2 - ND -Toluene mg/kg 0.5 <0.5 <0.5 - ND -Ethylbenzene mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (m & p) mg/kg 0.5 <0.5 <0.5 - ND -Xylene (o) mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 - ND -Acenaphthylene mg/kg 0.1 <0.5 <0.5 - ND -Anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benz(a)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(a)pyrene mg/kg 0.05 <0.5 <0.5 - ND -Benzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND -Benzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Chrysene mg/kg 0.1 <0.5 <0.5 - ND -Dibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Fluoranthene mg/kg 0.1 <0.5 <0.5 - ND -Fluorene mg/kg 0.1 <0.5 <0.5 - ND -Indeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 - ND -Naphthalene mg/kg 0.1 <0.5 <0.5 - ND -Phenanthrene mg/kg 0.1 <0.5 <0.5 - ND -Pyrene mg/kg 0.1 <0.5 <0.5 - ND -PAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 - ND -Arsenic mg/kg 4 71 67 - 5.80% -Cadmium mg/kg 0.4 4 4 - 0.00% -Chromium mg/kg 1 206 214 - 3.81% -Copper mg/kg 1 6550 6970 - 6.21% -Lead mg/kg 1 3390 3200 - 5.77% -Mercury mg/kg 0.1 <0.1 <0.1 - ND -Nickel mg/kg 1 76 75 - 1.32% -Zinc mg/kg 1 16,500 16,300 - 1.22% -




RPDs



Duplicate Analysis RPDs Sample ID TP124_001_0.0 - 0.1 QC103_18/12/14 QC104_18/12/14Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1428622 & 121411 Date Sampled 18/12/2014 18/12/2014 18/12/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 <25 ND NDTRH C10 - C14 Fraction mg/kg 50 <50 <50 <50 ND NDTRH C15 - C28 Fraction mg/kg 100 <100 <100 <100 ND NDTRH C29 - C36 Fraction mg/kg 100 <100 <100 <100 ND NDTRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 <25 ND NDTRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 <25 ND NDTRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 <50 ND NDTRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 <50 ND NDTRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 <100 ND NDTRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 <100 ND NDBenzene mg/kg 0.2 <0.2 <0.2 <0.2 ND NDToluene mg/kg 0.5 <0.5 <0.5 <0.5 ND NDEthylbenzene mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (m & p) mg/kg 0.5 <0.5 <0.5 <2 ND NDXylene (o) mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAcenaphthylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAnthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenz(a)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(a)pyrene mg/kg 0.05 <0.5 <0.5 <0.05 ND NDBenzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 <0.5 ND NDBenzo(b)&(k)fluoranthene mg/kg 0.2 - - <0.2 - -Benzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Chrysene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDDibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluoranthene mg/kg 0.1 <0.5 0.9 <0.1 57.14% NDFluorene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDIndeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDNaphthalene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPhenanthrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPyrene mg/kg 0.1 <0.5 1 <0.1 66.67% NDArsenic mg/kg 4 <5 <5 <4 ND NDCadmium mg/kg 0.4 <1 <1 <0.4 ND NDChromium mg/kg 1 6 6 8 0.00% 28.57%Copper mg/kg 1 <5 <5 5 ND 0.00%Lead mg/kg 1 11 12 14 8.70% 24.00%Mercury mg/kg 0.1 <0.1 <0.1 <0.1 ND NDNickel mg/kg 1 2 2 4 0.00% 66.67%Zinc mg/kg 1 12 14 18 15.38% 40.00%Hexachlorobenzene mg/kg 0.05 <0.05 <0.05 - ND -a-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDAldrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDAldrin & Dieldrin (Sum of total) mg/kg 0.05 <0.05 <0.05 <0.2 ND NDb-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDChlordane (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND NDcis-Chlordane mg/kg 0.05 <0.05 <0.05 <0.1 ND NDtrans-Chlordane mg/kg 0.05 <0.05 <0.05 <0.1 ND NDd-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDD mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDE mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDT mg/kg 0.1 <0.2 <0.2 <0.1 ND NDDDT+DDE+DDD (Sum of total) mg/kg 0.05 <0.05 <0.05 <0.3 ND NDDieldrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan mg/kg 0.05 <0.05 <0.05 - ND NDEndosulfan I mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan II mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan sulphate mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin aldehyde mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin ketone mg/kg 0.05 <0.05 <0.05 - ND NDg-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDHeptachlor mg/kg 0.05 <0.05 <0.05 <0.1 ND NDHeptachlor & heptachlor epoxide mg/kg 0.05 - - <0.2 ND NDHeptachlor epoxide mg/kg 0.05 <0.05 <0.05 <0.1 ND NDMethoxychlor mg/kg 0.1 <0.2 <0.2 <0.1 ND NDAzinphos-methyl mg/kg 0.05 <0.05 <0.05 - ND NDBromophos-ethyl mg/kg 0.05 <0.05 <0.05 <0.1 ND NDCarbophenothion mg/kg 0.05 <0.05 <0.05 - ND NDChlorfenvinphos mg/kg 0.05 <0.05 <0.05 - ND NDChlorpyriphos mg/kg 0.05 <0.05 <0.05 <0.1 ND NDChlorpyriphos-methyl mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDiazinon mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDichlorvos mg/kg 0.05 <0.05 <0.05 - ND NDDimethoate mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEthion mg/kg 0.05 <0.05 <0.05 <0.1 ND NDFenamiphos mg/kg 0.05 <0.05 <0.05 - ND NDFenitrothion mg/kg 0.1 - - <0.1 ND NDFenthion mg/kg 0.05 <0.05 <0.05 - ND NDMalathion mg/kg 0.05 <0.05 <0.05 - ND NDParathion-methyl mg/kg 0.2 <0.2 <0.2 - ND NDMonocrotophos mg/kg 0.2 <0.2 <0.2 - ND NDParathion mg/kg 0.2 <0.2 <0.2 - ND NDPirimphos-ethyl mg/kg 0.05 <0.05 <0.05 - ND NDProthiofos mg/kg 0.05 <0.05 <0.05 - ND NDRonnel mg/kg 0.1 - - <0.1 ND NDCarbazole mg/kg 0.5 - - - ND -Chlorobenzilate mg/kg 0.5 - - - ND -Demeton-s-methyl mg/kg 0.05 <0.05 <0.05 - ND -


Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LOR

RPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR


RPDs



Duplicate Analysis RPDs Sample ID TP109_001_0.0 - 0.1 QC106_18/12/14 QC107_18/12/14Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1428622 & 121411 Date Sampled 18/12/2014 18/12/2014 18/12/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 <25 ND NDTRH C10 - C14 Fraction mg/kg 50 <50 <50 <50 ND NDTRH C15 - C28 Fraction mg/kg 100 <100 <100 <100 ND NDTRH C29 - C36 Fraction mg/kg 100 <100 <100 <100 ND NDTRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 <25 ND NDTRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 <25 ND NDTRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 <50 ND NDTRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 <50 ND NDTRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 <100 ND NDTRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 <100 ND NDBenzene mg/kg 0.2 <0.2 <0.2 <0.2 ND NDToluene mg/kg 0.5 <0.5 <0.5 <0.5 ND NDEthylbenzene mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (m & p) mg/kg 0.5 <0.5 <0.5 <2 ND NDXylene (o) mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND NDTotal BTEX mg/kg 0.2 <0.2 <0.2 - ND NDAcenaphthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAcenaphthylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAnthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenz(a)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(a)pyrene mg/kg 0.05 <0.5 <0.5 <0.05 ND NDBenzo(a)pyrene (TEQs) mg/kg 0.5 - - <0.5 ND NDBenzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND NDBenzo(b)&(k)fluoranthene mg/kg 0.2 - - <0.2 ND NDBenzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND NDBenzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND NDChrysene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDDibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluoranthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluorene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDIndeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDNaphthalene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPhenanthrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPyrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 0 ND NDArsenic mg/kg 4 10 10 12 0.00% 18.18%Cadmium mg/kg 0.4 <1 <1 <0.4 ND NDChromium mg/kg 1 19 21 23 10.00% 19.05%Copper mg/kg 1 <5 <5 2 ND NDLead mg/kg 1 13 11 16 16.67% 20.69%Mercury mg/kg 0.1 <0.1 <0.1 <0.1 ND NDNickel mg/kg 1 <2 <2 3 ND 40.00%Zinc mg/kg 1 <5 <5 7 ND 33.33%Hexachlorobenzene mg/kg 0.05 <0.05 <0.05 <0.1 ND NDa-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDAldrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDAldrin & Dieldrin (Sum of total) mg/kg 0.05 <0.05 <0.05 <0.2 ND NDb-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDChlordane (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND NDcis-Chlordane mg/kg 0.05 <0.05 <0.05 <0.1 ND NDtrans-Chlordane mg/kg 0.05 <0.05 <0.05 <0.1 ND NDd-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDD mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDE mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDT mg/kg 0.1 <0.2 <0.2 <0.1 ND NDDDT+DDE+DDD (Sum of total) mg/kg 0.05 <0.05 <0.05 <0.3 ND NDDieldrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan mg/kg 0.05 <0.05 <0.05 - ND NDEndosulfan I mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan II mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan sulphate mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin aldehyde mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin ketone mg/kg 0.05 <0.05 <0.05 - ND NDg-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDHeptachlor mg/kg 0.05 <0.05 <0.05 <0.1 ND NDHeptachlor & heptachlor epoxide mg/kg 0.05 - - <0.2 ND NDHeptachlor epoxide mg/kg 0.05 <0.05 <0.05 <0.1 ND NDMethoxychlor mg/kg 0.1 <0.2 <0.2 <0.1 ND NDAzinphos-methyl mg/kg 0.05 <0.05 <0.05 - ND NDBromophos-ethyl mg/kg 0.05 <0.05 <0.05 <0.1 ND NDCarbophenothion mg/kg 0.05 <0.05 <0.05 - ND NDChlorfenvinphos mg/kg 0.05 <0.05 <0.05 - ND NDChlorpyriphos mg/kg 0.05 <0.05 <0.05 <0.1 ND NDChlorpyriphos-methyl mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDiazinon mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDichlorvos mg/kg 0.05 <0.05 <0.05 - ND NDDimethoate mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEthion mg/kg 0.05 <0.05 <0.05 <0.1 ND NDFenamiphos mg/kg 0.05 <0.05 <0.05 - ND NDFenitrothion mg/kg 0.1 - - <0.1 ND NDFenthion mg/kg 0.05 <0.05 <0.05 - ND NDMalathion mg/kg 0.05 <0.05 <0.05 - ND NDParathion-methyl mg/kg 0.2 <0.2 <0.2 - ND NDMonocrotophos mg/kg 0.2 <0.2 <0.2 - ND NDParathion mg/kg 0.2 <0.2 <0.2 - ND NDPirimphos-ethyl mg/kg 0.05 <0.05 <0.05 - ND NDProthiofos mg/kg 0.05 <0.05 <0.05 - ND NDRonnel mg/kg 0.1 - - <0.1 ND NDDemeton-s-methyl mg/kg 0.05 <0.05 <0.05 - ND -PCB mg/kg 0.1 <0.1 <0.1 <0.1 ND ND




RPDs



Duplicate Analysis RPDs Sample ID TP118_001_0.0 - 0.1 QC108_18/12/14 -Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1428622 & 121411 Date Sampled 18/12/2014 18/12/2014 -

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 - ND -TRH C10 - C14 Fraction mg/kg 50 <50 <50 - ND -TRH C15 - C28 Fraction mg/kg 100 <100 <100 - ND -TRH C29 - C36 Fraction mg/kg 100 <100 <100 - ND -TRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 - ND -TRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 - ND -TRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 - ND -TRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 - ND -TRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 - ND -TRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 - ND -Benzene mg/kg 0.2 <0.2 <0.2 - ND -Toluene mg/kg 0.5 <0.5 <0.5 - ND -Ethylbenzene mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (m & p) mg/kg 0.5 <0.5 <0.5 - ND -Xylene (o) mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 - ND -Acenaphthylene mg/kg 0.1 <0.5 <0.5 - ND -Anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benz(a)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(a)pyrene mg/kg 0.05 <0.5 <0.5 - ND -Benzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND -Benzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Chrysene mg/kg 0.1 <0.5 <0.5 - ND -Dibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Fluoranthene mg/kg 0.1 <0.5 <0.5 - ND -Fluorene mg/kg 0.1 <0.5 <0.5 - ND -Indeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 - ND -Naphthalene mg/kg 0.1 <0.5 <0.5 - ND -Phenanthrene mg/kg 0.1 <0.5 <0.5 - ND -Pyrene mg/kg 0.1 <0.5 <0.5 - ND -PAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 - ND -Arsenic mg/kg 4 <5 <5 - ND -Cadmium mg/kg 0.4 <1 <1 - ND -Chromium mg/kg 1 <2 <2 - ND -Copper mg/kg 1 <5 <5 - ND -Lead mg/kg 1 17 44 - 88.52% -Mercury mg/kg 0.1 <0.1 <0.1 - ND -Nickel mg/kg 1 <2 <2 - ND -Zinc mg/kg 1 6 6 - 0.00% -Hexachlorobenzene mg/kg 0.05 <0.05 <0.05 - ND -a-BHC mg/kg 0.05 <0.05 <0.05 - ND -Aldrin mg/kg 0.05 <0.05 <0.05 - ND -Aldrin & Dieldrin (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND -b-BHC mg/kg 0.05 <0.05 <0.05 - ND -Chlordane (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND -cis-Chlordane mg/kg 0.05 <0.05 <0.05 - ND -trans-Chlordane mg/kg 0.05 <0.05 <0.05 - ND -d-BHC mg/kg 0.05 <0.05 <0.05 - ND -DDD mg/kg 0.05 <0.05 <0.05 - ND -DDE mg/kg 0.05 <0.05 <0.05 - ND -DDT mg/kg 0.1 <0.2 <0.2 - ND -DDT+DDE+DDD (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND -Dieldrin mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan I mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan II mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan sulphate mg/kg 0.05 <0.05 <0.05 - ND -Endrin mg/kg 0.05 <0.05 <0.05 - ND -Endrin aldehyde mg/kg 0.05 <0.05 <0.05 - ND -Endrin ketone mg/kg 0.05 <0.05 <0.05 - ND -g-BHC mg/kg 0.05 <0.05 <0.05 - ND -Heptachlor mg/kg 0.05 <0.05 <0.05 - ND -Heptachlor epoxide mg/kg 0.05 <0.05 <0.05 - ND -Methoxychlor mg/kg 0.1 <0.2 <0.2 - ND -Azinphos-methyl mg/kg 0.05 <0.05 <0.05 - ND -Bromophos-ethyl mg/kg 0.05 <0.05 <0.05 - ND -Carbophenothion mg/kg 0.05 <0.05 <0.05 - ND -Chlorfenvinphos mg/kg 0.05 <0.05 <0.05 - ND -Chlorpyriphos mg/kg 0.05 <0.05 <0.05 - ND -Chlorpyriphos-methyl mg/kg 0.05 <0.05 <0.05 - ND -Diazinon mg/kg 0.05 <0.05 <0.05 - ND -Dichlorvos mg/kg 0.05 <0.05 <0.05 - ND -Dimethoate mg/kg 0.05 <0.05 <0.05 - ND -Ethion mg/kg 0.05 <0.05 <0.05 - ND -Fenamiphos mg/kg 0.05 <0.05 <0.05 - ND -Fenthion mg/kg 0.05 <0.05 <0.05 - ND -Malathion mg/kg 0.05 <0.05 <0.05 - ND -Parathion-methyl mg/kg 0.2 <0.2 <0.2 - ND -Monocrotophos mg/kg 0.2 <0.2 <0.2 - ND -Parathion mg/kg 0.2 <0.2 <0.2 - ND -Pirimphos-ethyl mg/kg 0.05 <0.05 <0.05 - ND -Prothiofos mg/kg 0.05 <0.05 <0.05 - ND -Demeton-s-methyl mg/kg 0.05 <0.05 <0.05 - ND -





RPDs




Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 - ND -TRH C10 - C14 Fraction mg/kg 50 <50 <50 - ND -TRH C15 - C28 Fraction mg/kg 100 <100 <100 - ND -TRH C29 - C36 Fraction mg/kg 100 <100 <100 - ND -TRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 110 <50 - 75.00% -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 - ND -TRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 - ND -TRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 - ND -TRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 - ND -TRH >C16 - C34 Fraction F3 mg/kg 100 110 <100 - 9.52% -TRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 - ND -Benzene mg/kg 0.2 <0.2 <0.2 - ND -Toluene mg/kg 0.5 <0.5 <0.5 - ND -Ethylbenzene mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (m & p) mg/kg 0.5 <0.5 <0.5 - ND -Xylene (o) mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 - ND -Acenaphthylene mg/kg 0.1 <0.5 <0.5 - ND -Anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benz(a)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(a)pyrene mg/kg 0.05 <0.5 <0.5 - ND -Benzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND -Benzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Chrysene mg/kg 0.1 <0.5 <0.5 - ND -Dibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Fluoranthene mg/kg 0.1 <0.5 <0.5 - ND -Fluorene mg/kg 0.1 <0.5 <0.5 - ND -Indeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 - ND -Naphthalene mg/kg 0.1 <0.5 <0.5 - ND -Phenanthrene mg/kg 0.1 <0.5 <0.5 - ND -Pyrene mg/kg 0.1 <0.5 <0.5 - ND -PAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 - ND -Arsenic mg/kg 4 <5 <5 - ND -Cadmium mg/kg 0.4 <1 <1 - ND -Chromium mg/kg 1 4 3 - 28.57% -Copper mg/kg 1 8 6 - 28.57% -Lead mg/kg 1 16 11 - 37.04% -Mercury mg/kg 0.1 <0.1 <0.1 - ND -Nickel mg/kg 1 <2 <2 - ND -Zinc mg/kg 1 18 9 - 66.67% -Hexachlorobenzene mg/kg 0.05 <0.05 <0.05 - ND -a-BHC mg/kg 0.05 <0.05 <0.05 - ND -Aldrin mg/kg 0.05 <0.05 <0.05 - ND -Aldrin & Dieldrin (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND -b-BHC mg/kg 0.05 <0.05 <0.05 - ND -Chlordane (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND -cis-Chlordane mg/kg 0.05 <0.05 <0.05 - ND -trans-Chlordane mg/kg 0.05 <0.05 <0.05 - ND -d-BHC mg/kg 0.05 <0.05 <0.05 - ND -DDD mg/kg 0.05 <0.05 <0.05 - ND -DDE mg/kg 0.05 <0.05 <0.05 - ND -DDT mg/kg 0.1 <0.2 <0.2 - ND -DDT+DDE+DDD (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND -Dieldrin mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan I mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan II mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan sulphate mg/kg 0.05 <0.05 <0.05 - ND -Endrin mg/kg 0.05 <0.05 <0.05 - ND -Endrin aldehyde mg/kg 0.05 <0.05 <0.05 - ND -Endrin ketone mg/kg 0.05 <0.05 <0.05 - ND -g-BHC mg/kg 0.05 <0.05 <0.05 - ND -Heptachlor mg/kg 0.05 <0.05 <0.05 - ND -Heptachlor epoxide mg/kg 0.05 <0.05 <0.05 - ND -Methoxychlor mg/kg 0.1 <0.2 <0.2 - ND -Azinphos-methyl mg/kg 0.05 <0.05 <0.05 - ND -Bromophos-ethyl mg/kg 0.05 <0.05 <0.05 - ND -Carbophenothion mg/kg 0.05 <0.05 <0.05 - ND -Chlorfenvinphos mg/kg 0.05 <0.05 <0.05 - ND -Chlorpyriphos mg/kg 0.05 <0.05 <0.05 - ND -Chlorpyriphos-methyl mg/kg 0.05 <0.05 <0.05 - ND -Diazinon mg/kg 0.05 <0.05 <0.05 - ND -Dichlorvos mg/kg 0.05 <0.05 <0.05 - ND -Dimethoate mg/kg 0.05 <0.05 <0.05 - ND -Ethion mg/kg 0.05 <0.05 <0.05 - ND -Fenamiphos mg/kg 0.05 <0.05 <0.05 - ND -Fenthion mg/kg 0.05 <0.05 <0.05 - ND -Malathion mg/kg 0.05 <0.05 <0.05 - ND -Parathion-methyl mg/kg 0.2 <0.2 <0.2 - ND -Monocrotophos mg/kg 0.2 <0.2 <0.2 - ND -Parathion mg/kg 0.2 <0.2 <0.2 - ND -Pirimphos-ethyl mg/kg 0.05 <0.05 <0.05 - ND -Prothiofos mg/kg 0.05 <0.05 <0.05 - ND -Demeton-s-methyl mg/kg 0.05 <0.05 <0.05 - ND -





RPDs



Duplicate Analysis RPDs Sample ID TP113b_002_0.8 - 0.9 QC110_19/12/14 QC111_19/12/14Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1428622 & 121411 Date Sampled 19/12/2014 19/12/2014 19/12/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 <25 ND NDTRH C10 - C14 Fraction mg/kg 50 <50 <50 <50 ND NDTRH C15 - C28 Fraction mg/kg 100 <100 <100 <100 ND NDTRH C29 - C36 Fraction mg/kg 100 <100 <100 <100 ND NDTRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 <25 ND NDTRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 <25 ND NDTRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 <50 ND NDTRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 <50 ND NDTRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 <100 ND NDTRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 <100 ND NDBenzene mg/kg 0.2 <0.2 <0.2 <0.2 ND NDToluene mg/kg 0.5 <0.5 <0.5 <0.5 ND NDEthylbenzene mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (m & p) mg/kg 0.5 <0.5 <0.5 <2 ND NDXylene (o) mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAcenaphthylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAnthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenz(a)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(a)pyrene mg/kg 0.05 <0.5 <0.5 <0.05 ND NDBenzo(a)pyrene (TEQs) mg/kg 0.5 - - <0.5 ND NDBenzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND -Benzo(b)&(k)fluoranthene mg/kg 0.2 - - <0.2 ND NDBenzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Chrysene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDDibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluoranthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluorene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDIndeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDNaphthalene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPhenanthrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPyrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 0 ND ND2-Chloronaphthalene mg/kg 0.5 <0.5 <0.5 - ND -2-Methylnaphthalene mg/kg 0.5 <0.5 <0.5 - ND -3-Methylcholanthrene mg/kg 0.5 <0.5 <0.5 - ND -7,12-Dimethylbenz(a)anthracene mg/kg 0.5 <0.5 <0.5 - ND -Arsenic mg/kg 4 <5 <5 <4 ND NDCadmium mg/kg 0.4 <1 <1 <0.4 ND NDChromium mg/kg 1 <2 2 9 ND NDCopper mg/kg 1 <5 <5 4 ND NDLead mg/kg 1 6 8 10 28.57% 50.00%Mercury mg/kg 0.1 1.2 3 0.9 85.71% 28.57%Nickel mg/kg 1 <2 <2 1 ND 66.67%Zinc mg/kg 1 <5 5 10 0.00% 66.67%n-Nitrosodiethylamine mg/kg 0.5 <0.5 <0.5 - ND -N-Nitrosodi-n-butylamine mg/kg 0.5 <0.5 <0.5 - ND -N-Nitrosodi-n-propylamine mg/kg 0.5 <0.5 <0.5 - ND -n-Nitrosomethylethylamine mg/kg 0.5 <0.5 <0.5 - ND -1-Naphthylamine mg/kg 0.5 <0.5 <0.5 - ND -n-Nitrosodiphenylamine & Diphenylamine mg/kg 1 <1 <1 - ND -2-Nitroaniline mg/kg 1 <1 <1 - ND -3-Nitroaniline mg/kg 1 <1 <1 - ND -4-Chloroaniline mg/kg 0.5 <0.5 <0.5 - ND -4-Nitroaniline mg/kg 0.5 <0.5 <0.5 - ND -2-methyl-5-nitroaniline mg/kg 0.5 <0.5 <0.5 - ND -Aniline mg/kg 0.5 <0.5 <0.5 - ND -Nitrobenzene mg/kg 0.5 <0.5 <0.5 - ND -Pentachloronitrobenzene mg/kg 0.5 <0.5 <0.5 - ND -1,3,5-Trinitrobenzene mg/kg 0.5 <0.5 <0.5 - ND -2,4-Dinitrotoluene mg/kg 1 <1 <1 - ND -2,6-Dinitrotoluene mg/kg 1 <1 <1 - ND -1,2,3-Trichlorobenzene mg/kg 0.5 <0.5 <0.5 - ND -1,2,4-Trichlorobenzene mg/kg 0.5 <0.5 <0.5 - ND -1,2-Dichlorobenzene mg/kg 0.5 <0.5 <0.5 - ND -1,3-Dichlorobenzene mg/kg 0.5 <0.5 <0.5 - ND -1,4-Dichlorobenzene mg/kg 0.5 <0.5 <0.5 - ND -2-Chlorotoluene mg/kg 0.5 <0.5 <0.5 - ND -4-Chlorotoluene mg/kg 0.5 <0.5 <0.5 - ND -Bromobenzene mg/kg 0.5 <0.5 <0.5 - ND -Chlorobenzene mg/kg 0.5 <0.5 <0.5 - ND -Hexachlorobenzene mg/kg 0.05 <0.05 <0.05 <0.1 ND NDPentachlorobenzene mg/kg 0.5 <0.5 <0.5 - ND -Pronamide mg/kg 0.5 <0.5 <0.5 - ND -1,2,4-trimethylbenzene mg/kg 0.5 <0.5 <0.5 - ND -1,3,5-Trimethylbenzene mg/kg 0.5 <0.5 <0.5 - ND -Isopropylbenzene mg/kg 0.5 <0.5 <0.5 - ND -n-Butylbenzene mg/kg 0.5 <0.5 <0.5 - ND -n-Propylbenzene mg/kg 0.5 <0.5 <0.5 - ND -p-Isopropyltoluene mg/kg 0.5 <0.5 <0.5 - ND -sec-Butylbenzene mg/kg 0.5 <0.5 <0.5 - ND -Styrene mg/kg 0.5 <0.5 <0.5 - ND -tert-Butylbenzene mg/kg 0.5 <0.5 <0.5 - ND -a-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDAldrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDAldrin & Dieldrin (Sum of total) mg/kg 0.05 <0.05 <0.05 <0.2 ND NDb-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDChlordane (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND NDcis-Chlordane mg/kg 0.05 <0.05 <0.05 <0.1 ND NDtrans-Chlordane mg/kg 0.05 <0.05 <0.05 <0.1 ND NDd-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDD mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDE mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDT mg/kg 0.1 <0.2 <0.2 <0.1 ND NDDDT+DDE+DDD (Sum of total) mg/kg 0.05 <0.05 <0.05 <0.3 ND NDDieldrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan I mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan II mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan sulphate mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin aldehyde mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin ketone mg/kg 0.05 <0.05 <0.05 - ND -g-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDHeptachlor mg/kg 0.05 <0.05 <0.05 <0.1 ND NDHeptachlor & heptachlor epoxide mg/kg 0.05 - - <0.2 ND NDHeptachlor epoxide mg/kg 0.05 <0.05 <0.05 <0.1 ND NDMethoxychlor mg/kg 0.1 <0.2 <0.2 <0.1 ND NDAzinphos-methyl mg/kg 0.05 <0.05 <0.05 - ND -Bromophos-ethyl mg/kg 0.05 <0.05 <0.05 <0.1 ND NDCarbophenothion mg/kg 0.05 <0.05 <0.05 - ND -Chlorfenvinphos mg/kg 0.05 <0.05 <0.05 - ND -Chlorpyriphos mg/kg 0.05 <0.05 <0.05 <0.1 ND NDChlorpyriphos-methyl mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDiazinon mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDichlorvos mg/kg 0.05 <0.05 <0.05 - ND -Dimethoate mg/kg 0.05 <0.05 <0.05 <0.1 ND ND


RPDs



Duplicate Analysis RPDs Sample ID TP113b_002_0.8 - 0.9 QC110_19/12/14 QC111_19/12/14Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1428622 & 121411 Date Sampled 19/12/2014 19/12/2014 19/12/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter Duplicate


RPDs

Ethion mg/kg 0.05 <0.05 <0.05 <0.1 ND NDFenamiphos mg/kg 0.05 <0.05 <0.05 - ND -Fenitrothion mg/kg 0.1 - - <0.1 ND NDFenthion mg/kg 0.05 <0.05 <0.05 - ND -Malathion mg/kg 0.05 <0.05 <0.05 - ND -Parathion-methyl mg/kg 0.2 <0.2 <0.2 - ND -Monocrotophos mg/kg 0.2 <0.2 <0.2 - ND -Parathion mg/kg 0.2 <0.2 <0.2 - ND -Pirimphos-ethyl mg/kg 0.05 <0.05 <0.05 - ND -Prothiofos mg/kg 0.05 <0.05 <0.05 - ND -Ronnel mg/kg 0.1 - - <0.1 ND NDCarbazole mg/kg 0.5 <0.5 <0.5 - ND -Chlorobenzilate mg/kg 0.5 <0.5 <0.5 - ND -Demeton-s-methyl mg/kg 0.05 <0.05 <0.05 - ND -2,4-Dimethylphenol mg/kg 0.5 <0.5 <0.5 - ND -2-Methylphenol mg/kg 0.5 <0.5 <0.5 - ND -2-Nitrophenol mg/kg 0.5 <0.5 <0.5 - ND -3- & 4- Methylphenol mg/kg 0.5 <0.5 <0.5 - ND -Phenol mg/kg 0.5 <0.5 <0.5 - ND -2,4,5-Trichlorophenol mg/kg 0.5 <0.5 <0.5 - ND -2,4,6-Trichlorophenol mg/kg 0.5 <0.5 <0.5 - ND -2,4-Dichlorophenol mg/kg 0.5 <0.5 <0.5 - ND -2,6-Dichlorophenol mg/kg 0.5 <0.5 <0.5 - ND -2-Chlorophenol mg/kg 0.5 <0.5 <0.5 - ND -4-Chloro-3-methylphenol mg/kg 0.5 <0.5 <0.5 - ND -Pentachlorophenol mg/kg 1 <1 <1 - ND -Bis(2-ethylhexyl) phthalate mg/kg 5 <5 <5 - ND -Butylbenzyl phthalate mg/kg 0.5 <0.5 <0.5 - ND -Diethyl phthalate mg/kg 0.5 <0.5 <0.5 - ND -Dimethyl phthalate mg/kg 0.5 <0.5 <0.5 - ND -Di-n-butyl phthalate mg/kg 0.5 <0.5 <0.5 - ND -Di-n-octyl phthalate mg/kg 0.5 <0.5 <0.5 - ND -Methyl Ethyl Ketone mg/kg 5 <5 <5 - ND -2-Hexanone mg/kg 5 <5 <5 - ND -Methyl iso-butyl ketone mg/kg 5 <5 <5 - ND -Isophorone mg/kg 0.5 <0.5 <0.5 - ND -Vinyl acetate mg/kg 5 <5 <5 - ND -2-(Acetylamino) fluorene mg/kg 0.5 <0.5 <0.5 - ND -2-Picoline mg/kg 0.5 <0.5 <0.5 - ND -3,3-Dichlorobenzidine mg/kg 0.5 <0.5 <0.5 - ND -4-(Dimethylamino) azobenzene mg/kg 0.5 <0.5 <0.5 - ND -4-Aminobiphenyl mg/kg 0.5 <0.5 <0.5 - ND -4-Bromophenyl phenyl ether mg/kg 0.5 <0.5 <0.5 - ND -4-Chlorophenyl phenyl ether mg/kg 0.5 <0.5 <0.5 - ND -4-Nitroquinoline-n-oxide mg/kg 0.5 <0.5 <0.5 - ND -Acetophenone mg/kg 0.5 <0.5 <0.5 - ND -Azobenzene mg/kg 1 <1 <1 - ND -Bis(2-chloroethoxy) methane mg/kg 0.5 <0.5 <0.5 - ND -Bis(2-chloroethyl) ether mg/kg 0.5 <0.5 <0.5 - ND -Dibenzofuran mg/kg 0.5 <0.5 <0.5 - ND -Hexachlorocyclopentadiene mg/kg 2.5 <2.5 <2.5 - ND -Hexachloropropene mg/kg 0.5 <0.5 <0.5 - ND -Methapyrilene mg/kg 0.5 <0.5 <0.5 - ND -n-Nitrosomorpholine mg/kg 0.5 <0.5 <0.5 - ND -N-Nitrosopiperidine mg/kg 0.5 <0.5 <0.5 - ND -n-Nitrosopyrrolidine mg/kg 1 <1 <1 - ND -Phenacetin mg/kg 0.5 <0.5 <0.5 - ND -1,1,1,2-Tetrachloroethane mg/kg 0.5 <0.5 <0.5 - ND -1,1,2,2-Tetrachloroethane mg/kg 0.5 <0.5 <0.5 - ND -1,1,1-Trichloroethane mg/kg 0.5 <0.5 <0.5 - ND -1,1,2-Trichloroethane mg/kg 0.5 <0.5 <0.5 - ND -1,2,3-Trichloropropane mg/kg 0.5 <0.5 <0.5 - ND -1,2-Dibromo-3-chloropropane mg/kg 0.5 <0.5 <0.5 - ND -1,2-Dibromoethane mg/kg 0.5 <0.5 <0.5 - ND -1,1-Dichloroethane mg/kg 0.5 <0.5 <0.5 - ND -1,2-Dichloroethane mg/kg 0.5 <0.5 <0.5 - ND -1,1-Dichloroethene mg/kg 0.5 <0.5 <0.5 - ND -cis-1,2-Dichloroethene mg/kg 0.5 <0.5 <0.5 - ND -trans-1,2-dichloroethene mg/kg 0.5 <0.5 <0.5 - ND -1,2-Dichloropropane mg/kg 0.5 <0.5 <0.5 - ND -1,3-Dichloropropane mg/kg 0.5 <0.5 <0.5 - ND -2,2-Dichloropropane mg/kg 0.5 <0.5 <0.5 - ND -1,1-Dichloropropene mg/kg 0.5 <0.5 <0.5 - ND -cis-1,3-Dichloropropene mg/kg 0.5 <0.5 <0.5 - ND -trans-1,3-dichloropropene mg/kg 0.5 <0.5 <0.5 - ND -cis-1,4-Dichloro-2-butene mg/kg 0.5 <0.5 <0.5 - ND -trans-1,4-Dichloro-2-butene mg/kg 0.5 <0.5 <0.5 - ND -Bromodichloromethane mg/kg 0.5 <0.5 <0.5 - ND -Bromoform mg/kg 0.5 <0.5 <0.5 - ND -Bromomethane mg/kg 5 <5 <5 - ND -Carbon disulfide mg/kg 0.5 <0.5 <0.5 - ND -Carbon tetrachloride mg/kg 0.5 <0.5 <0.5 - ND -Chlorodibromomethane mg/kg 0.5 <0.5 <0.5 - ND -Chloroethane mg/kg 5 <5 <5 - ND -Chloroform mg/kg 0.5 <0.5 <0.5 - ND -Chloromethane mg/kg 5 <5 <5 - ND -Dibromomethane mg/kg 0.5 <0.5 <0.5 - ND -Dichlorodifluoromethane mg/kg 5 <5 <5 - ND -Hexachlorobutadiene mg/kg 0.5 <0.5 <0.5 - ND -Hexachloroethane mg/kg 0.5 <0.5 <0.5 - ND -Iodomethane mg/kg 0.5 <0.5 <0.5 - ND -Pentachloroethane mg/kg 0.5 <0.5 <0.5 - ND -Trichloroethene mg/kg 0.5 <0.5 <0.5 - ND -Tetrachloroethene mg/kg 0.5 <0.5 <0.5 - ND -Trichlorofluoromethane mg/kg 5 <5 <5 - ND -Vinyl chloride mg/kg 5 <5 <5 - ND -







Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 - ND -TRH C10 - C14 Fraction mg/kg 50 <50 <50 - ND -TRH C15 - C28 Fraction mg/kg 100 <100 <100 - ND -TRH C29 - C36 Fraction mg/kg 100 140 <100 - 33.33% -TRH+C10 - C36 (Sum of total) mg/kg 50 140 <50 - 94.74% -TRH+C10 - C40 (Sum of total) mg/kg 50 290 <50 - 141.18% -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 - ND -TRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 - ND -TRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 - ND -TRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 - ND -TRH >C16 - C34 Fraction F3 mg/kg 100 180 <100 - 57.14% -TRH >C34 - C40 Fraction F4 mg/kg 100 110 <100 - 9.52% -Benzene mg/kg 0.2 <0.2 <0.2 - ND -Toluene mg/kg 0.5 <0.5 <0.5 - ND -Ethylbenzene mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (m & p) mg/kg 0.5 <0.5 <0.5 - ND -Xylene (o) mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 - ND -Acenaphthylene mg/kg 0.1 <0.5 <0.5 - ND -Anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benz(a)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(a)pyrene mg/kg 0.05 <0.5 <0.5 - ND -Benzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND -Benzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Chrysene mg/kg 0.1 <0.5 <0.5 - ND -Dibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Fluoranthene mg/kg 0.1 <0.5 <0.5 - ND -Fluorene mg/kg 0.1 <0.5 <0.5 - ND -Indeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 - ND -Naphthalene mg/kg 0.1 <0.5 <0.5 - ND -Phenanthrene mg/kg 0.1 <0.5 <0.5 - ND -Pyrene mg/kg 0.1 <0.5 <0.5 - ND -PAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 - ND -Arsenic mg/kg 4 <5 <5 - ND -Cadmium mg/kg 0.4 <1 <1 - ND -Chromium mg/kg 1 10 10 - 0.00% -Copper mg/kg 1 11 14 - 24.00% -Lead mg/kg 1 42 30 - 33.33% -Mercury mg/kg 0.1 <0.1 <0.1 - ND -Nickel mg/kg 1 6 8 - 28.57% -Zinc mg/kg 1 58 52 - 10.91% -





RPDs



Duplicate Analysis RPDs Sample ID TP115_001_0.0-0.1 QC105_18/12/14 -Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1428622 & 121411 Date Sampled 18/12/2014 18/12/2014 -

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 - ND -TRH C10 - C14 Fraction mg/kg 50 <50 <50 - ND -TRH C15 - C28 Fraction mg/kg 100 <100 <100 - ND -TRH C29 - C36 Fraction mg/kg 100 <100 <100 - ND -TRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND -TRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 - ND -TRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 - ND -TRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 - ND -TRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 - ND -TRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 - ND -TRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 - ND -Benzene mg/kg 0.2 <0.2 <0.2 - ND -Toluene mg/kg 0.5 <0.5 <0.5 - ND -Ethylbenzene mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (m & p) mg/kg 0.5 <0.5 <0.5 - ND -Xylene (o) mg/kg 0.5 <0.5 <0.5 - ND -Xylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 - ND -Acenaphthylene mg/kg 0.1 <0.5 <0.5 - ND -Anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benz(a)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(a)pyrene mg/kg 0.05 <0.5 <0.5 - ND -Benzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND -Benzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Benzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 - ND -Benzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND -Chrysene mg/kg 0.1 <0.5 <0.5 - ND -Dibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 - ND -Fluoranthene mg/kg 0.1 <0.5 <0.5 - ND -Fluorene mg/kg 0.1 <0.5 <0.5 - ND -Indeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 - ND -Naphthalene mg/kg 0.1 <0.5 <0.5 - ND -Phenanthrene mg/kg 0.1 <0.5 <0.5 - ND -Pyrene mg/kg 0.1 <0.5 <0.5 - ND -PAH (Sum of Common 16 PAHs) mg/kg 0.5 <0.5 <0.5 - ND -Arsenic mg/kg 4 <5 <5 - ND -Cadmium mg/kg 0.4 <1 <1 - ND -Chromium mg/kg 1 4 3 - 28.57% -Copper mg/kg 1 18 15 - 18.18% -Lead mg/kg 1 18 22 - 20.00% -Mercury mg/kg 0.1 <0.1 <0.1 - ND -Nickel mg/kg 1 5 4 - 22.22% -Zinc mg/kg 1 60 68 - 12.50% -





RPDs



Duplicate Analysis RPDs Sample ID TP212-001_0 - 0.1 QC166 QC167Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1428622 & 121411 Date Sampled 11/12/2014 11/12/2014 11/12/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicateTRH C6 - C9 Fraction mg/kg 10 <10 <10 <25 ND NDTRH C10 - C14 Fraction mg/kg 50 <50 <50 <50 ND NDTRH C15 - C28 Fraction mg/kg 100 <100 <100 <100 ND NDTRH C29 - C36 Fraction mg/kg 100 <100 <100 <100 ND NDTRH+C10 - C36 (Sum of total) mg/kg 50 <50 <50 - ND -TRH+C10 - C40 (Sum of total) mg/kg 50 <50 <50 - ND NDTRH C6 - C10 Fraction F1 mg/kg 10 <10 <10 <25 ND NDTRH C6 - C10 Fraction Less BTEX F1 mg/kg 10 <10 <10 <25 ND NDTRH >C10 - C16 Fraction F2 mg/kg 50 <50 <50 <50 ND NDTRH >C10 - C16 Fraction Less Naphthalene F2 mg/kg 50 <50 <50 <50 ND NDTRH >C16 - C34 Fraction F3 mg/kg 100 <100 <100 <100 ND NDTRH >C34 - C40 Fraction F4 mg/kg 100 <100 <100 <100 ND NDBenzene mg/kg 0.2 <0.2 <0.2 <0.2 ND NDToluene mg/kg 0.5 <0.5 <0.5 <0.5 ND NDEthylbenzene mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (m & p) mg/kg 0.5 <0.5 <0.5 <2 ND NDXylene (o) mg/kg 0.5 <0.5 <0.5 <1 ND NDXylenes (Sum of total) mg/kg 0.5 <0.5 <0.5 - ND -Total BTEX mg/kg 0.2 <0.2 <0.2 - ND -Acenaphthene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAcenaphthylene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDAnthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDBenz(a)anthracene mg/kg 0.1 <0.5 <0.5 0.1 ND 133.33%Benzo(a)pyrene mg/kg 0.05 <0.5 <0.5 0.1 ND 133.33%Benzo(a)pyrene (TEQs) mg/kg 0.5 - - <0.5 ND NDBenzo(a)pyrene TEQ (lower bound)* mg/kg 0.5 <0.5 <0.5 - ND -Benzo(b)&(k)fluoranthene mg/kg 0.2 - - 0.2 ND NDBenzo(b)&(j)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND NDBenzo(g,h,i)perylene mg/kg 0.1 <0.5 <0.5 0.1 ND 133.33%Benzo(k)fluoranthene mg/kg 0.5 <0.5 <0.5 - ND NDChrysene mg/kg 0.1 <0.5 <0.5 0.1 ND 133.33%Dibenz(a,h)anthracene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDFluoranthene mg/kg 0.1 <0.5 0.6 0.3 18.18% 50.00%Fluorene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDIndeno(1,2,3-c,d)pyrene mg/kg 0.1 <0.5 <0.5 0.1 ND 133.33%Naphthalene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPhenanthrene mg/kg 0.1 <0.5 <0.5 <0.1 ND NDPyrene mg/kg 0.1 <0.5 0.6 0.3 18.18% 50.00%Arsenic mg/kg 4 5 6 10 18.18% 66.67%Cadmium mg/kg 0.4 <1 <1 0.4 ND 85.71%Chromium mg/kg 1 30 22 29 30.77% 3.39%Copper mg/kg 1 13 13 11 0.00% 16.67%Lead mg/kg 1 31 34 37 9.23% 17.65%Mercury mg/kg 0.1 <0.1 <0.1 <0.1 ND NDNickel mg/kg 1 5 7 7 33.33% 33.33%Zinc mg/kg 1 43 58 48 29.70% 10.99%Hexachlorobenzene mg/kg 0.05 <0.05 <0.05 <0.1 ND NDa-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDAldrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDAldrin & Dieldrin (Sum of total) mg/kg 0.05 <0.05 <0.05 <0.2 ND NDb-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDChlordane (Sum of total) mg/kg 0.05 <0.05 <0.05 - ND -cis-Chlordane mg/kg 0.05 <0.05 <0.05 <0.1 ND NDtrans-Chlordane mg/kg 0.05 <0.05 <0.05 <0.1 ND NDd-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDD mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDE mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDDT mg/kg 0.1 <0.2 <0.2 <0.1 ND NDDDT+DDE+DDD (Sum of total) mg/kg 0.05 <0.05 <0.05 <0.3 ND NDDieldrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan mg/kg 0.05 <0.05 <0.05 - ND -Endosulfan I mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan II mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndosulfan sulphate mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin aldehyde mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEndrin ketone mg/kg 0.05 <0.05 <0.05 - ND -g-BHC mg/kg 0.05 <0.05 <0.05 <0.1 ND NDHeptachlor mg/kg 0.05 <0.05 <0.05 <0.1 ND NDHeptachlor & heptachlor epoxide mg/kg 0.05 - - <0.2 ND NDHeptachlor epoxide mg/kg 0.05 <0.05 <0.05 <0.1 ND NDMethoxychlor mg/kg 0.1 <0.2 <0.2 <0.1 ND NDAzinphos-methyl mg/kg 0.05 <0.05 <0.05 - ND -Bromophos-ethyl mg/kg 0.05 <0.05 <0.05 <0.1 ND NDCarbophenothion mg/kg 0.05 <0.05 <0.05 - ND -Chlorfenvinphos mg/kg 0.05 <0.05 <0.05 - ND -Chlorpyriphos mg/kg 0.05 <0.05 <0.05 <0.1 ND NDChlorpyriphos-methyl mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDiazinon mg/kg 0.05 <0.05 <0.05 <0.1 ND NDDichlorvos mg/kg 0.05 <0.05 <0.05 - ND -Dimethoate mg/kg 0.05 <0.05 <0.05 <0.1 ND NDEthion mg/kg 0.05 <0.05 <0.05 <0.1 ND NDFenamiphos mg/kg 0.05 <0.05 <0.05 - ND -Fenitrothion mg/kg 0.1 - - <0.1 ND NDFenthion mg/kg 0.05 <0.05 <0.05 - ND -Malathion mg/kg 0.05 <0.05 <0.05 - ND -Parathion-methyl mg/kg 0.2 <0.2 <0.2 - ND -Monocrotophos mg/kg 0.2 <0.2 <0.2 - ND -Parathion mg/kg 0.2 <0.2 <0.2 - ND -Pirimphos-ethyl mg/kg 0.05 <0.05 <0.05 - ND -Prothiofos mg/kg 0.05 <0.05 <0.05 - ND -Ronnel mg/kg 0.1 - - <0.1 ND NDCarbazole mg/kg 0.5 - - - ND -Chlorobenzilate mg/kg 0.5 - - - ND -Demeton-s-methyl mg/kg 0.05 <0.05 <0.05 - ND -





RPDs




TypeMB

Sample ID








Y

Date Sampled: 16/12/2014 Sample Medium: Soil

Y TCLP Metals

Y


Project Number: 147623070

Primary Laboratory: ALS Workorder Number: ES1501124(rebatch of ES1428622)

Secondary Laboratory: - Workorder Number: -


Surrogate recoveries were not conducted in this batch.



Matrix Spike recoveries were within the laboratory based quality objectives.



Matrix Spike (MS) AnalysesAnalyte Group Comments


QAQC Sample Information (Method Blank - MB, Rinsate Blank - RB, Field Blank - FB, Trip Blank - TB)Sample ID





Y/N Comments

Samples received intact and chilled? Y Rebatch from ES1428622. Samples stored in an appropriate environment in the interim.Samples analysed within appropriate holding times?







Comments

Overall Comments

Field triplicates were not scheduled for analysis in this rebatch.

CommentsTCLP analysis not scheduled on duplicate samples in this rebatch



All LCS recoveries from ALS were within the data quality objectives.


Laboratory Duplicate analyses were within the laboratory based quality objectives.


Analyte Group


Comments



TypeMBMB

Sample ID

Analyte Group Primary ID Duplicate IDAll SV01 QC100


SV02 QC101






Y

Date Sampled: 22/12/2014 Sample Medium: Vapour

Y All.

YAre there non-NATA accredited methods used? N

Project Number: 147623070Primary Laboratory: Envirolab (ELS) Workorder Number: 121502Secondary Laboratory: ALS Workorder Number: EN1411040


Several field triplicate outliers were observed in this batch. This is not expected to affect the outcomes of the investigation as the concentrations reported by both ALS and ELS were in the same order of magnitude.Furthermore, the highest reported concentration will be adopted for assessment.



ELS: Matrix Spike recoveries were not conducted by Envirolab



ALS: All LCS recovereis were within the data quality objectives.Matrix Spike (MS) Analyses



Comments





Y/N Comments

Samples received intact and chilled? Y Suma canisters delivered in appropriate conditionSamples analysed within appropriate holding times?





Sample ID

ALS: Matrix Spike recoveries were not conducted by ALS

ELS: All results were less than the LOR

Comments





Method Blank

Comments


Overall Comments

RPDs calculated for cis-1,2-Dichloroethene (46.15%), Benzene (80.37%), Toluene (33.33%) andTetrachloroethene(70.1%) did not meet the acceptable control limits.All other RPDs calculated achieved the data quality objectives.

CommentsAll calculated RPDs achieved the data quality objectives.



ELS: All LCS recovereis were within the data quality objectives.


ELS: Laboratory Duplicate analyses were within the laboratory based quality objectives.ALS: Laboratory Duplicate analyses were within the laboratory based quality objectives.


Analyte Group


Duplicate Analysis RPDs Sample ID SV01 QC100 -Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: 121502 & EN1411040 Date Sampled 22/12/2014 22/12/2014 -

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePropylene µg/m3 0.9 <24 <24 - ND -Dichlorodifluoromethane µg/m3 2.5 <69 <69 - ND -Chloromethane µg/m3 1.0 <29 <29 - ND -1,2-Dichlorotetrafluoroethane µg/m3 2.5 <69 <69 - ND -Vinyl chloride µg/m3 1.3 <36 <36 - ND -1,3-Butadiene µg/m3 1.1 <31 <31 - ND -Bromomethane µg/m3 1.9 <53 <53 - ND -Chloroethane µg/m3 1.3 <37 <37 - ND -Ethanol µg/m3 0.9 <26 <26 - ND -Acrolein µg/m3 1.1 <32 <32 - ND -Trichlorofluoromethane µg/m3 2.8 <79 <79 - ND -Isopropyl Alcohol µg/m3 1.2 <34 <34 - ND -1,1-Dichloroethene µg/m3 2.0 <56 <56 - ND -1,1,2-Trichlorotrifluoroethane µg/m3 3.8 <107 <107 - ND -Carbon Disulfide µg/m3 1.6 <44 <44 - ND -trans-1,2-dichloroethene µg/m3 2.0 120 120 - 0.00% -MTBE µg/m3 1.8 <50 <50 - ND -1,1- Dichloroethane µg/m3 2.0 <57 <57 - ND -Vinyl Acetate µg/m3 1.8 <49 <49 - ND -MEK µg/m3 1.5 <41 <41 - ND -Hexane µg/m3 1.8 <49 <49 - ND -

-1,2-Dichloroethene µg/m3 2.0 2900 2800 - 3.51% -Ethyl Acetate µg/m3 1.8 <50 <50 - ND -Chloroform µg/m3 2.4 120 120 - 0.00% -Tetrahydrofuran µg/m3 1.5 <41 <41 - ND -1,1,1-Trichloroethane µg/m3 2.7 <76 <76 - ND -1,2-Dichloroethane µg/m3 2.0 <57 <57 - ND -Benzene µg/m3 1.6 <45 <45 - ND -Carbon tetrachloride µg/m3 3.1 <88 <88 - ND -Cyclohexane µg/m3 1.7 <48 <48 - ND -Heptane µg/m3 2.0 <57 <57 - ND -Trichloroethene µg/m3 2.7 280000 260000 - 7.41% -1,2-Dichloropropane µg/m3 2.3 <65 <65 - ND -1,4-Dioxane µg/m3 1.8 <50 <50 - ND -Bromodichloromethane µg/m3 3.4 <94 <94 - ND -Methyl Methacrylate µg/m3 2.0 <57 <57 - ND -MIBK µg/m3 2.0 <57 <57 - ND -

-1,3-Dichloropropene µg/m3 2.3 <64 <64 - ND --1,3-Dichloropropene µg/m3 2.3 <64 <64 - ND -

Toluene µg/m3 1.9 <53 <53 - ND -1,1,2-Trichloroethane µg/m3 2.7 <76 <76 - ND -Methyl Butyl Ketone µg/m3 2.0 <57 <57 - ND -Dibromochloromethane µg/m3 1.6 <46 <46 - ND -Tetrachloroethene µg/m3 3.4 400 440 - 9.52% -1,2-Dibromoethane µg/m3 3.8 <108 <108 - ND -Chlorobenzene µg/m3 2.3 <64 <64 - ND -Ethylbenzene µg/m3 2.2 <61 <61 - ND -

-& -Xylene µg/m3 4.3 <122 <122 - ND -Styrene µg/m3 2.1 <60 <60 - ND -

-Xylene µg/m3 2.2 <61 <61 - ND -Bromoform µg/m3 5.2 <145 <145 - ND -1,1,2,2-Tetrachloroethane µg/m3 3.4 <96 <96 - ND -4-ethyl toluene µg/m3 2.5 <69 <69 - ND -1,3,5-Trimethylbenzene µg/m3 2.5 <69 <69 - ND -1,2,4-Trimethylbenzene µg/m3 2.5 <69 <69 - ND -1,3-Dichlorobenzene µg/m3 3.0 <84 <84 - ND -Benzyl chloride µg/m3 2.6 <72 <72 - ND -1,4-Dichlorobenzene µg/m3 3.0 <84 <84 - ND -1,2-Dichlorobenzene µg/m3 3.0 <84 <84 - ND -1,2,4-Trichlorobenzene µg/m3 3.7 <104 <104 - ND -Naphthalene µg/m3 2.6 <73 <73 - ND -Hexachloro- µg/m3 5.3 <149 <149 - ND -TPH C5 - C8 Aliphatic µg/m3 200 100000 97000 - 3.05% -TPH C9 - C12 Aliphatic µg/m3 50 <1400 <1400 - ND -TPH C9 - C10 Aromatic µg/m3 100 <2800 <2800 - ND -TPH C6 - C10 - BTEX (F1) µg/m3 200 110000 110000 - 0.00% -TPH >C10 - C12 - µg/m3 40 <1120 <1120 - ND -LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated



RPDs



Duplicate Analysis RPDs Sample ID SV02 - QC100Project No. : 147623070 Sample Type Primary Field Duplicate Field TriplicateBatch/es: 121502 & EN1411040 Date Sampled 22/12/2014 - 22/12/2014

Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePropylene µg/m3 0.9 <24 - - - -Dichlorodifluoromethane µg/m3 2.5 <69 - - - -Chloromethane µg/m3 1.0 <29 - - - -1,2-Dichlorotetrafluoroethane µg/m3 2.5 <69 - - - -Vinyl chloride µg/m3 1.3 <36 - <13 - ND1,3-Butadiene µg/m3 1.1 <31 - - - -Bromomethane µg/m3 1.9 <53 - - - -Chloroethane µg/m3 1.3 <37 - - - -Ethanol µg/m3 0.9 <26 - - - -Acrolein µg/m3 1.1 <32 - - - -Trichlorofluoromethane µg/m3 2.8 <79 - - - -Isopropyl Alcohol µg/m3 1.2 <34 - - - -1,1-Dichloroethene µg/m3 2.0 <56 - - - -1,1,2-Trichlorotrifluoroethane µg/m3 3.8 <107 - - - -Carbon Disulfide µg/m3 1.6 <44 - - - -trans-1,2-dichloroethene µg/m3 2.0 <56 - - - -MTBE µg/m3 1.8 <50 - - - -1,1- Dichloroethane µg/m3 2.0 <57 - - - -Vinyl Acetate µg/m3 1.8 <49 - - - -MEK µg/m3 1.5 <41 - - - -Hexane µg/m3 1.8 <49 - - - -

-1,2-Dichloroethene µg/m3 2.0 1300 - 2080 - 46.15%Ethyl Acetate µg/m3 1.8 <50 - - - -Chloroform µg/m3 2.4 <68 - - - -Tetrahydrofuran µg/m3 1.5 <41 - - - -1,1,1-Trichloroethane µg/m3 2.7 <76 - <27 - ND1,2-Dichloroethane µg/m3 2.0 <57 - - - -Benzene µg/m3 1.6 <45 - 19.2 - 80.37%Carbon tetrachloride µg/m3 3.1 <88 - - - -Cyclohexane µg/m3 1.7 <48 - - - -Heptane µg/m3 2.0 <57 - - - -Trichloroethene µg/m3 2.7 75000 - 72000 - 4.08%1,2-Dichloropropane µg/m3 2.3 <65 - - - -1,4-Dioxane µg/m3 1.8 <50 - - - -Bromodichloromethane µg/m3 3.4 <94 - - - -Methyl Methacrylate µg/m3 2.0 <57 - - - -MIBK µg/m3 2.0 <57 - - - -

-1,3-Dichloropropene µg/m3 2.3 <64 - - - --1,3-Dichloropropene µg/m3 2.3 <64 - - - -

Toluene µg/m3 1.9 <53 - 74.2 - 33.33%1,1,2-Trichloroethane µg/m3 2.7 <76 - - - -Methyl Butyl Ketone µg/m3 2.0 <57 - - - -Dibromochloromethane µg/m3 1.6 <46 - - - -Tetrachloroethene µg/m3 3.4 110 - 52.9 - 70.10%1,2-Dibromoethane µg/m3 3.8 <108 - - - -Chlorobenzene µg/m3 2.3 <64 - - - -Ethylbenzene µg/m3 2.2 <61 - <22 - ND

-& -Xylene µg/m3 4.3 <122 - <43 - NDStyrene µg/m3 2.1 <60 - - - -

-Xylene µg/m3 2.2 <61 - <22 - NDBromoform µg/m3 5.2 <145 - - - -1,1,2,2-Tetrachloroethane µg/m3 3.4 <96 - - - -4-ethyl toluene µg/m3 2.5 <69 - - - -1,3,5-Trimethylbenzene µg/m3 2.5 <69 - - - -1,2,4-Trimethylbenzene µg/m3 2.5 <69 - - - -1,3-Dichlorobenzene µg/m3 3.0 <84 - - - -Benzyl chloride µg/m3 2.6 <72 - - - -1,4-Dichlorobenzene µg/m3 3.0 <84 - - - -1,2-Dichlorobenzene µg/m3 3.0 <84 - - - -1,2,4-Trichlorobenzene µg/m3 3.7 <104 - - - -Naphthalene µg/m3 2.6 <73 - <26 - NDHexachloro- µg/m3 5.3 <149 - - - -TPH C5 - C8 Aliphatic µg/m3 200 27000 - - - -TPH C9 - C12 Aliphatic µg/m3 50 <1400 - - - -TPH C9 - C10 Aromatic µg/m3 100 <2800 - - - -TPH C6 - C10 - BTEX (F1) µg/m3 200 30000 - 38100 - 23.79%TPH >C10 - C12 (F2) µg/m3 40 <1120 - <4000 - ND




RPDs



PP2 ESA - MOOREBANK INTERMODAL TERMINAL

21 July 2015Report No. 147623070-019-R-Rev0

APPENDIX HCalibration Certificates



APPENDIX IMIP Charts

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12MIP 101

EC (mS/m x10)

PID Max (uV x 100,000)

FID Max (uV x 100,000)

XSD Max (uV x 100,000)

SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 102

EC (mS/m x10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 103

EC (mS/m x10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 104

EC (mS/m x10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 105

EC (mS/m x10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 106

EC (mS/m x10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 107

EC (mS/m x10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 108

EC (mS/m x 10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 110

EC (mS/m x 10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 111

EC (mS/m x 10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 112

EC (mS/m x 10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

0 1 2 3 4 5 6 7 8 9 10 11 12

MIP 113

EC (mS/m x 10)




SWL (mBGL)

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

1 2 3 4 5 6 7 8 9 10 11 12

MIP 114a

EC (mS/m x 10)




SWL (mBGL)



APPENDIX JUST GPR Investigation Report, ETS January 2015



APPENDIX KHistoric Aerial Photographs

1965

Aer

ialP

hoto

grap

h

2Tren

ch

Form

erPR

AYa

rd

Form

erD

ryG

ap

1970

Aer

ialP

hoto

grap

h

3

Re-

alig

ned

Tren

ch

Dry

Gap

Part

lyFi

lled

1978

Aer

ialP

hoto

grap

h

4

Form

erD

ryG

ap

Form

erD

ryG

ap–

now

part

lyfil

l

Form

erPR

AYa

rd



APPENDIX LLaboratory Certificates

Documents

Preparedby:JD · BH112-013 Analyte Group Primary ID Duplicate ID Analyte Group Primary ID Triplicate ID Analyte Group Analyte(s) Note: Data validation assesses each analyte in terms