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page 1 Precision Back Pressure Regulators Research Series Low ow / Laboratory scale Gas, Liquid & Mixed Phase Service

Research Precision Back Pressure Regulators

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Back pressure regulators for use in maintaining upstream constant pressure.

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  • page 1

    Precision Back Pressure Regulators

    Research Series Low fl ow / Laboratory scaleGas, Liquid & Mixed Phase Service

  • page 2

    Research SeriesLow fl ow / Laboratory scaleGas, Liquid & Mixed Phase Service

    Precision: within 0.5%Pressure: 0.02 to 5000 psigTemperature: to 327C (620F )Flow: 0 to 20,000 ml/min

    Chemically Compatibile Materials:

    Unique Diaphragm Regulator Technology:Dome-loaded design is 5X more precise than traditional spring loaded regulators

    Elegant friction-less diaphragm is the only moving part

    Suitable for ultra-pure and aggressive chemicals

    Two modes of operation:

    Key Applications: Catalyst research

    Reservoir core analysis

    1/8 HP1 - SS316LAvailable to 5000 psig

    Precision Back Pressure Regulators

    ZF1 with HPLC (Valco-Style) fi ttingsSS316L body, SS316L Diaphragm,

    Kalrez FFKM o-ring

    In Stock!Most common confi gurations are in stock for shipment in 2-5 days

    e

    Material Body Diaphram O-ring

    SS316L x x

    Hastelloy C x x

    Zirconium x

    PTFE x x

    Polymide x

    PEEK x

    FKM (Viton) x x

    FFKM (Kalrez) x

    Manual adjustment by mechanical pilot regulator

    Computer automation by electronic pressure regulator

    Kalrez and Viton are registered trademarks of DuPont Performance Elastomers

  • page 3

    The Equilibar back pressure regulator is an exciting breakthrough in precision pressure control. Designed for critical and demanding processes, the patented Equilibar o ers unmatched precision across a wide range of pressures and fl ow rates.

    Traditional back pressure regulators use springs to gradually open up as the overpressure is used to compress the spring.

    The Equilibar back pressure regulator uses only a frictionless fl exible diaphragm to modulate the pressure. It fully opens in less than 1% overpressure in most applications. Our multiple orifi ces allow us to control over incredibly wide fl ow rate ratios - over 1000:1 ratios in most applications - and handle two phase fl ows.

    Equilibar back pressure technology is protected by US and foreign patents. Learn more about our precision back pressure technology on our website.

    Unmatched Precision...

    Sensitivity and Precision - Our Key Performance Advantage

    Inlet Outlet

    Pilot(Reference)Diaphragm

    E/P

    Electro-PneumaticRegulator

    ManualPressureRegulator

    - OR -

    2 Set-Point Options

    1/4 GS4 SS16 back pressure regulatorwith manual set-point regulator

    How the Equilibar Back Pressure Regulator Works

    The Equilibar Precision Back Pressure Regulator works like a fl uid transistor by forming a unique force balance on a fl exible diaphragm between three separate pressures.

    The fl uid inlet pressure and the downstream outlet pressure exist on the wetted side of the diaphragm. The pilot set-point applies pressure on the non-wetted side.

    The lower pressure of the outlet tries to hold the diaphragm in a leak-tight seal with the orifi ces. However, any slight excess between the fl uid inlet pressure and the pilot set-point pressure quickly overwhelms these seating forces and pulls the diaphragm away from the orifi ces.

    The pilot set-point pressure acts in a 1:1 ratio to set the pressure to be controlled on the inlet port. As shown at right, this pilot pressure can be supplied by either an electro-pneumatic regulator or a manual regulator.

  • page 4

    Material General Operating Pressures

    Polyimide (also PEEK, PVDF, PCTFE) 5 psig to max. body pressure

    SS316, Hastelloy C276 50 psig to max. body pressure

    PTFE/Glass, PTFE 0.2 psig to max. body pressure

    PolyEthylene 0.02 psig to 20 psig

    Research Series Models

    Standard Research Models

    Model Part #Inlet /Outlet

    Port

    Reference Port

    BodyMaterials Dim A Dim B

    Max StdPressure

    Max Custom

    Pressure

    Cv Range(precision)

    Available EndFittings

    NPT (std) (inch) (psig) Min2 Max Std Available

    Low FlowLF1 1/8

    1/8 NPT1/4 NPT

    (PTFE)

    SS316L (std)

    Hastelloy CPTFE

    2.5 1.3 1000 2000

    1E-7 0.07NPT

    1/16 HPLC

    1/8 W125

    Autoclave

    BSP, VCO-style, VCR- style,

    SAE, 1/8 HPLC

    (Valco Style)

    LF2 1/4

    High FlowHF1 1/8

    1E-4 0.6HF2 1/4

    High Pressure

    HP1 1/8

    1/8 NPTSS316L

    (std) Hastelloy C

    2.5

    1.45 5000 N/A

    1E-6 0.07HP2 1/4 2.75

    High Pressure &

    Flow

    HPF1 1/8 2.51E-4 0.5

    HPF2 1/4 2.75

    For gas, liquid and mixed phase processesRugged Bar Stock DesignUltra Low Pressure and Flow RangesHigh Precision

    Available Diaphragms

    Wetted components: Body, diaphragm, o-ring 1 - Minimum Cv dependant on diaphragm and set-point pressure and set-point pressure

    Dimensions and Cv values subject to change

    3.00

    1.50

    2.00

    P.21

    OutletInlet

    1/8" NPT Reference Port(All models)

    B

    A

    NL1 mounting bracket fi ts all Research Series Regulators *Also fi ts GS2, GS3, NL2, NL3 standard models

    Material Notes

    Viton Standard, temp. to 200C

    FFKM (Kalrez) Chemical compatibility, temp. to 327C

    Available O-Rings (wetted)

    Model Part #Inlet /Outlet

    Port

    Reference Port

    BodyMaterials Dim A Dim B

    Max StdPressure

    Max Custom

    Pressure

    Cv Range(precision)

    Available EndFittings

    (inch) (psig) Min1 Max Std Available

    Ultra Low Flow

    ULF1 1/8

    1/8

    SS316L (std)

    Hastelloy CPTFE

    2.5

    1.45

    3000 5000

    ~1E-7 (@ 100 psig)

    0.05

    NPT

    1/16 HPLC

    1/8W125

    Autoclave

    BSP, VCO-style, VCR- style,

    1/8HPLC (Valco Style)

    ULF2 1/4 2.75 ~1E-8 (@1000 psig)

    Zero Flow ZF1 1/8 2.5 1000 3000

  • page 5

    Selecting the right Series

    * Custom Solution Models are not included in the standard Equilibar patents.

    The ZF Series BPR extends Equilibars low fl ow performance down to e ective zero fl ow while maintaining a very stable inlet pressure. The patent pending design uses a soft o-ring to improve fl ow shut-o . This is useful for reservoir core analysis and other lab reactor applications with microscopic or intermittent fl ow rates.

    The ZF Series is not suitable for all applications and has a narrower pressure and fl ow operating range. In order to maintain reasonable elastomeric seal life, fl ow rates less than 2 standard liter/minute and set-point pressures below 1500 psig are recommended.

    LF Series (Low Flow)The LF Series BPR is capable of low fl ow operation down to about 10 cc/min of gas. Pressure rating to 1000 psig.

    HF Series (High Flow)The HF Series BPR is similar to the LF Series, but with higher fl ow capacity.

    HP Series (High Pressure)The HP Series BPR has the same performance and design as the LF but with a more robust body rated to 5000 psig.

    The ULF Series BPR functions similar to Equilibars LF and HP Series. In some applications, however, the ULF is able to extend low fl ow performance down to 0.01 to 0.1 ml/min (gas). Equilibar application engineers will provide guidance when the advantages of the ULF design outweigh any potential disadvantages.

    ULF Series (Ultra Low Flow)

    ZF Series (Zero Flow Capability)

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    Res

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    Mod

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    Mod

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    Mod

    els

    Each of these standard Research Series models is based on our patented Equilibar precision back pressure regulator (BPR) technology. These models are capable of greater than 1000:1 fl ow rate turn-down ratios in most applications. They can also be used with 100:1 turn-down ratio in set-point pressure.

  • page 6

    Pressure Stability That Sets A New Industry Standard...Research Series StabilityThese charts below represent data of the LF1 BPRs pressure stability through an amazing 6 orders of fl ow rates and Cv magnitudes! The inlet pressure of most back pressure regulators varies signifi cantly with changes in process fl ow.

    Gas analysis applications such as Petrochemical and Catalyst Research can take real advantage of the unmatched low fl ow capability of these regulators. Equilibar regulators can achieve as high as 10,000:1 fl ow turn down ratios.

    High Pressure StabilityEquilibar regulators are able to handle the most extreme pressure requirements with our Research Series regula-tors. The HP1 can reach up to 5,000 psig for high pres-sure applications. Using PTFE/Glass reinforced compos-ites and Stainless Steel 316 diaphragms we are able to meet the pressure and low fl ow requirements of todays most demanding analysis instruments.

    0

    1000

    2000

    3000

    4000

    5000

    6000

    7000

    8000

    0

    200

    400

    600

    800

    1000

    1200

    1E-9 1E-7 1E-5 1E-3 1E-1

    Inle

    t Pre

    ssur

    e, k

    pag

    Inle

    t Pre

    ssur

    e, p

    sig

    Cv

    High Pressure Performance

    Set Point: 1000 psig, 6895 kpag

    Set Point: 300 psig, 2068 kpag

    4E-6 4E-5 4E-4 4E-3 4E-2 4E-1 4E+0

    1

    6

    60

    600

    0.01

    0.1

    1

    10

    100

    0.1 1 10 100 1000 10000 100000

    Air Flow, SCFM

    Inle

    t Pre

    ssur

    e, k

    pag

    Inle

    t Pre

    ssur

    e, p

    sig

    Air Flow, ml/min

    Ultra Wide Flow Range PerformanceEB1LF Air Trials

    Various Set Points: .04, 0.2, 1, 6, and 30 psig0.06

    0.6

    6

    60

    600

    0.01

    0.1

    1

    10

    100

    1E-8 1E-7 1E-6 1E-5 1E-4 1E-3 1E-2 1E-1 1E+0

    Inle

    t Pre

    ssur

    e, k

    pag

    Inle

    t Pre

    ssur

    e, p

    si g

    Cv

    Exponential Cv PerformanceEB1LF Air Trials

    Various Set Points: .04, 0.2, 1, 6, and 30 psigVarious Set Points: .04, 0.2, 1, 6, and 30 psig

    High Temperature ApplicationsHigh Temperature Seals: Equilibar has developed high temperature (to 327C or 620F ) versions of the Research Series Back Pressure Regulators for use in research reactors and other high temperature processes. These units use DuPont Kalrez O-rings to seal metallic diaphragms. The seals are selected based on your maximum expected temperature, with many available in stock for quick delivery. Each unit is built to order to precisely fi t your application.

    Remote Set-Point Controller: Equilibar Back Pressure Regulators are dome loaded with a 1:1 pressure ratio and require a set point pressure reducing regulator which can be remotely located outside of the hot zone. The dome loading consumes no fl uid, so that your temperature control is not infl uenced by fl ow to the reference side of the diaphragm. The set point controller can be manual or electro-pneumatic. See pages 8 & 9 for options.

    Research Series

  • page 7

    Applications

    Closed Loop ControlFuel Cell TestingThe Equilibar back pressure regulator excels at the de-manding requirements of Fuel Cell test systems. In fact, several of our products were specifi cally designed to meet their requirements of 1000:1 fl ow rate and 100:1 pressure turn-down ratios.

    The schematic at right shows how a closed loop control system can be used to provide extremely tight control, even across widely varying process conditions.

    Our Research Series are used for the small scale fuel cell test systems, while medium and large systems use our GS and NLB Series respectively.

    There are hundreds of potential applications for the unique capabilities of the Equilibar. The Research Series is specifi cally designed for a variety of gas, liquid, and mixed phase applications where precision is a must.

    Applications span from ultra low fl ow rates to extreme high pressures. By using unique combinations of diaphragms and o-ring materials, Equilibar regulators are able to perform in the harshest environments that include high temperature and aggressive chemicals.

    Catalyst Research ReactorsMany catalyst research applications rely on high performance back pressure regulators to maintain stable pressure at elevated temperatures and down to nano fl ow rates. Because of the Equilibars unique ability to handle two-phase fl ow, it is possible to substitute a low pressure liquid/gas separator for the high-pressure separator.

    Reactant #1Set-PointPressure

    Two-phaseDome-loaded

    Back Pressure Regulator

    MFC

    MFC

    Reactant #2CatalystResearchReactor

    PG

    Separator

    Liquid reactant #3

    Sample

    MFC

    TemperatureControl

    ConfiningPressure

    Two-phaseDome-loaded

    Back Pressure Regulator

    Set-PointPressure

    LiquidGas

    Collector

    CO2,gas

    Brine

    Oil

    FM

    Reservoir Core AnalysisThere are many types of petroleum upstream core analy-sis applications that depend on back pressure regulators to maintain the pressure downstream of the sample. Core fl ooding (as shown at right), PVT analysis, pyrolysis, slim tube analysis can all benefi t from the ultra-low flow capability of Equilibars Research Series. The ZF (Zero Flow) Series in particular was developed to address the demanding requirements of this industry.

  • page 8

    Application Supply Pressure Ports

    Equilibar Part Number

    Outlet Pressure Range

    Repeatability & Sensitivity

    Suggested Pressure Gauge

    High Pressure

    High Pressure Regulators

    Max 6000 psig

    1/4 Inlet

    Outlet Gauge

    HPR-500-B 0-500 psig

    Sensitive through a wide range of

    pressures

    600p-2.5b-2L

    HPR-1500-B 0-1500 psig 1500p-2.5b-2L

    HPR-2500-B 0-2500 psig 3000p-2.5b-2L

    HPR-4000-B 0-4000 psig 500p-2.5b-2L

    HPR-6000-B 0-6000 psig 6000p-2.5b-2L

    High Precision

    Bellofram Type 10

    (2-stage)

    Max 50 psig

    1/4 Inlet

    Outlet Gauge

    T10LR-25 0.5 to 25 psig

    Highly sensitive and stable

    Varies 0.005 psi with 25 psi supply

    variation

    25p-2.5b-2c

    Max 150 psig

    T10-25 2 to 25 psig 25p-2.5b-2c

    T10-60 2 to 60 psig 60p-2.5b-2c

    T10-120 2 to 120 psig 160p-2.5b-2c

    Compact Economical

    BelloframType 41

    (1-stage)

    Max 250 psig

    1/4Inlet

    OutletGauge

    T41-2 0-10 psig

    Highly sensitive

    Varies 0.35 psig with 25 psi supply

    variation

    5p-2.5b-1c

    T41-10 0-10 psig 10p-2.5b-1c

    T41-30 0-30 psig 30p-2.5b-1c

    T41-60 0-60 psig 60p-2.5b-1c

    T41-100 0-100 psig 100p-2.5b-1c

    Ultra Low Pressure

    LPR2 Ultra Low Pressure

    Regulator

    5 - 30 psig (Stable

    Regulated)

    1/4 Inlet

    Outlet (No Gauge)

    LPR2-B (Bleed)

    &LPR2-NB

    (Non-Bleed)

    .25-7 inWC(0.01 to 0.25 psig) Sensitivity: 0.02

    inWC

    Stability: 0.06 inWC

    0-10 WC0-30 WC1-10 inWC

    1-28 inWC

    Vacuum

    Vacuum Regulators

    30hg (Vac)

    1/8"Inlet

    Outlet (no gauge)

    VPR-30 0.4 to 30 inHg

    Sensitivity0.1 inHg

    20-turn knob

    30h-2.5b-2VPR-10 0.4 to 10 inHg

    Panel Mount Only

    VPR-3 0-3 inHg Consult factory

    Manual ControlEquilibar Precision Back Pressure Regulators get their pilot control signal using a fl uid set-point pressure (also called reference or pilot pressure) on their top port.

    You can supply your own fl uid set point signal or choose one of the popular pilot set point regulators below.

    Set-Point Kits

  • page 9

    Process AutomationAutomating your process pressure is easily accomplished by using an electronic pressure regulator to provide the pilot set-point pressure to the Equilibar dome-loaded back pressure regulator.

    Equilibar is proud to represent precision electronic regulators from Propor-tion-Air. These devices are custom tuned on the bench to work perfectly with the Equilibar precision back pressure regulators or vacuum regulators.

    Contact Equilibar or visit our website for additional details about the many possible confi guration of these products.

    Set-Point Controllers

    Regulator Description Key Features

    Low Pressure - Ultra Precision Regulator (150 psi max)

    QPV Series

    Aluminum IP65 enclosure

    Optional digital display

    4-20 mA or 0-10 VDC

    * Min range: 0-0.3 psig, vacuum * Max range: 0-150 psig * Available in gauge, absolute, vacuum and vacuum- positive ranges * Superior proportional valve action * Accuracy: 0.1% - 0.5% FS * Resolution: 0.005% - 0.2% FS * Tuned ready for set-point service * Optional DeviceNet / Serial communication * Factory set for your pressure

    Medium Pressure - Precision Regulator (500 psi max)

    QB Series

    Aluminum IP65 enclosure

    Optional digital display

    4-20 mA or 0-10 VDC

    * Min range: vacuum; 0-1 psig * Max range: , 0 -500 psig * Available in gauge, absolute, vacuum and vacuum- positive ranges * 0.2 to 0.5% FS accuracy * Tuned ready for set-point service * Good for most applications * Factory set for your pressure

    High Pressure - Precision Regulator (1000 psi max)

    GP Series

    Aluminum IP65 enclosure

    4-20 mA or 0-10

    VDC

    * Min range: Vacuum or 0-500 * Max range: , 0 -1000 psig * Available in gauge, absolute, vacuum and vacuum- positive ranges * 0.5% FS accuracy * Factory set for your pressure

  • page 10

    Available Options and Accessories

    Equilibar Research Series Back Pressure Regulators are now available in stackable designs to minimize space requirements in parallel analysis systems

    Equilibar Research Series ULF unit shown with integrated 1000 psi Proportion-Air GP1 electronic pressure regulator. In this application, the inert process gas was used as the supply source for the GP1.

    Equilibar is expanding to higher pressures. This custom EHP1 is rated for 7000 psig.

    Equilibar Research Series back pressure regulator shown with integrated HPR 6000 psig manual set-point regulator. Inert gas bottles are often used as the supply gas for these applications.

  • page 11

    Other products from Equilibar

    GS Series Back Pressure RegulatorsThis series is ideal for gas and mixed phase applications due to the 2-piece body design.

    EVR Series Vacuum RegulatorsThe EVR Series uses the GS Series BPR, but adds a manual set-point kit to make vacuum control of processes easy and simple.

    NL Series Back Pressure RegulatorsThe NL Series has the same exact performance as the GS Series BPRs, plus an additional water hammer suppression feature, making them ideal for most liquid applications.

    Contact our EngineersAt Equilibar, your applications unique requirements will be carefully addressed by one of our trained application engineers. Please contact us if you have any questions or special requirements.

    Web: www.equilibar.com

    Email: [email protected]

    Telephone: (828)650-6590

    Fax: (801)504-4439

    Address: Equilibar, LLC 320 Rutledge Road Fletcher, NC 28732

    Application Engineering . . .How we are di erentUnlike mass-market regulator distributors, everything about Equilibar is focused on you, the scientist or engineer with a unique pressure control challenge.

    We assign an Application Engineer to you, typically within moments of your call. We work with you closely to identify the optimum model, trim, and diaphragm to best meet your challenge. You can stay in touch with your Application Engineer by email, telephone, mobile phone, or fax.

    After installation, if there are any unexpected issues, your Application Engineer is still available to support you with start-up information or (if needed) expedited replacement parts.

    About EquilibarEquilibar, LLC manufactures and markets our specialized products worldwide. Equilibar branded products are made in the USA, and protected by US and foreign patents.

    All of our products are assembled, inspected and tested by trained technicians in Fletcher, NC.

  • page 12 pppppagppppppppaaaaaapagpagpagpagpagpagpagpagppppppagpagpppaaapapppagppagppapappppagpppagppppagppagpagpagapp ggge 1e 1e 1e 1e 1e 11111111111e 1ee 1111e 1111122222222222222222222222 22222 22222 222 Copyright 2013 Equilibar LLC

    320 Rutledge Rd. Fletcher, NC 28732Tel: (828)650-6590 Fax: (801)504-4439www.equilibar.com [email protected]