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178 IEEE TRANSACTIONS ON COMPONENTS, PACKAGING AND MANUFACTURING TECHNOLOGY, VOL. 7, NO. 2, FEBRUARY 2017 Experimental and Theoretical Assessment of Thin Glass Substrate for Low Warpage Scott McCann, Vanessa Smet, Venky Sundaram, Rao R. Tummala, and Suresh K. Sitaraman Abstract— This paper compares the warpage after lead- free solder assembly of ultrathin glass and organic substrates for microelectronic packages. Smart mobile devices demand packages to be thinner, which exacerbates warpage, which in turn affects interconnect pitch scaling and reliability. Although low-coefficient-of-thermal-expansion (CTE) organic laminates have been developed to reduce the warpage during assembly, glass substrates offer added benefits of much higher modulus and thermo-mechanical stability, with the potential to reduce warpage beyond low-CTE organic materials. The focus of this paper is on modeling and measurements to quantify the warpage of glass and organic laminates at 100-μm core thickness after thermo-compression bonding at 260 °C peak temperature. In the experiments, four-metal-layer glass substrates were fabri- cated at the panel level, diced into 18.4 × 18.4-mm 2 coupons, 10-mm× 10-mm × 630 - μm silicon dies were thermo- compression bonded, and the warpage of the assembled packages was measured using shadow moiré interferometry. In parallel to the experiments, numerical models that account for the viscoplastic behavior of the solder as well as the sequential build- up materials and processes have been developed. The predicted warpage from the models was compared to the experimental measurements. It was seen that the low-CTE glass had lower warpage than the organic core of equivalent CTE, while increas- ing the CTE of the glass increased the warpage. Also, the underfill fillet size was found to influence the warpage for thin substrate packages, and an optimal fillet size has been identified for minimizing warpage. B-staged and capillary underfill materials were compared and found to have similar warpage values. Index Terms—Die warpage, element birth and death, finite element simulation, substrate warpage, thin glass substrate. I. I NTRODUCTION D EVICE packaging today is commonly performed with organic substrate cores such as FR4 or BT on which dry film organic build-up layers are deposited to form wiring layers on both sides. However, organic packaging is limited for future mobile packaging and high performance needs due to the electrical and mechanical properties of the material. For exam- ple, the coefficient of thermal expansion (CTE) mismatch Manuscript received October 8, 2015; revised October 31, 2016 and December 13, 2016; accepted December 14, 2016. Date of publication Janu- ary 17, 2017; date of current version February 6, 2017. This work was sup- ported by the Low Cost Glass Interposers & Packages global industry consor- tium at Georgia Tech PRC. Recommended for publication by Associate Editor M. Ramkumar upon evaluation of reviewers’ comments. S. McCann and S. K. Sitaraman are with the Department of Mechanical Engineering, Georgia Institute of Technology, Atlanta, GA 30332 USA (e-mail: [email protected]; [email protected]). V. Smet is with the Packaging Research Center, Georgia Institute of Technology, Atlanta, GA 30332 USA (e-mail: [email protected]). V. Sundaram and R. R. Tummala are with the Department of Electrical and Computer Engineering, Georgia Institute of Technology, Atlanta, GA 30332 USA (e-mail: [email protected]; [email protected]). Color versions of one or more of the figures in this paper are available online at http://ieeexplore.ieee.org. Digital Object Identifier 10.1109/TCPMT.2016.2641164 between the organic substrate and silicon die creates warpage before and after lead-free solder assembly. The demand for thinner packages for mobile applications imposes strin- gent requirements for ultrathin substrates, which exacerbates warpage challenges. One of the single biggest barriers to ultrathin packages is the substrate warpage during chip assembly. The mismatch of CTE between the silicon ICs (3 ppm/°C) and typical organic laminate substrates (12–18 ppm/°C) not only causes warpage during assembly, but also induces stress in the interconnections leading to solder joint failures. Traditional organic laminates such as FR-4 or BT, with prepreg or build-up epoxy dielectric based redistribution layers (RDLs) are the main substrates used for fine-pitch ball grid array (BGA) packages [1], [2]. Such organic substrates are often thick with a core thickness ranging from 500 μm to 1 mm to allow for sufficient rigidity and low warpage to meet the JEDEC standard specifications [3]. Recently, ultralow CTE organic laminates with CTE in the range of 2–6 ppm/°C have been developed to address the warpage challenge, by increasing the filler loading and by changing the glass fabric reinforcement to lower CTE glasses. These low-CTE laminates have significantly improved the warpage control during IC assembly, with a 7.3 - mm × 7.3 - mm × 150-μm silicon chip on a 14 - mm × 14 - mm × 260- μm package substrate (core CTE of 1.8 ppm/°C), resulting in a warpage of about 70 μm at room temperature and about 35 μm at reflow temperature [4]. Although silicon or ceramic substrates can address the warpage with a combination of low CTE and high elastic modulus, high cost coming from small wafers or substrates has been a major impediment to adoption in smart mobile systems. Glass is an ideal candidate for next-generation packaging, combining the best electrical properties of ceramics, high dimensional stability of silicon, and large panel processing of organics for low cost [5]. The higher elastic modulus of glass should enable much thinner packages than organics for the same warpage specifications. The CTE of the glass can be tailored, allowing larger glass packages to be directly SMT attached to FR-4 boards with high reliability [6]. Glass is smooth and planar, and, therefore, amenable to fabricating ultraprecise fine lines and spaces [7]–[9]. However, glass does have challenges in handling, brittleness, and through via for- mation at high speed, although significant progress has already been demonstrated in addressing these challenges [10]–[12]. Although lower warpage is anticipated for glass than organics, given its much higher elastic modulus and low CTE, there has been no published literature quantifying the warpage of low CTE glass and organic substrates during IC assembly. 2156-3950 © 2017 IEEE. Personal use is permitted, but republication/redistribution requires IEEE permission. See http://www.ieee.org/publications_standards/publications/rights/index.html for more information.

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Page 1: 178 IEEE TRANSACTIONS ON COMPONENTS ... IEEE TRANSACTIONS ON COMPONENTS, PACKAGING AND MANUFACTURING TECHNOLOGY, VOL. 7, NO. 2, FEBRUARY 2017 Experimental and Theoretical Assessment

178 IEEE TRANSACTIONS ON COMPONENTS, PACKAGING AND MANUFACTURING TECHNOLOGY, VOL. 7, NO. 2, FEBRUARY 2017

Experimental and Theoretical Assessment ofThin Glass Substrate for Low Warpage

Scott McCann, Vanessa Smet, Venky Sundaram, Rao R. Tummala, and Suresh K. Sitaraman

Abstract— This paper compares the warpage after lead-free solder assembly of ultrathin glass and organic substratesfor microelectronic packages. Smart mobile devices demandpackages to be thinner, which exacerbates warpage, which inturn affects interconnect pitch scaling and reliability. Althoughlow-coefficient-of-thermal-expansion (CTE) organic laminateshave been developed to reduce the warpage during assembly,glass substrates offer added benefits of much higher modulusand thermo-mechanical stability, with the potential to reducewarpage beyond low-CTE organic materials. The focus of thispaper is on modeling and measurements to quantify the warpageof glass and organic laminates at 100-µm core thickness afterthermo-compression bonding at 260 °C peak temperature. Inthe experiments, four-metal-layer glass substrates were fabri-cated at the panel level, diced into 18.4 × 18.4-mm2 coupons,10-mm× 10-mm × 630 − µm silicon dies were thermo-compression bonded, and the warpage of the assembled packageswas measured using shadow moiré interferometry. In parallelto the experiments, numerical models that account for theviscoplastic behavior of the solder as well as the sequential build-up materials and processes have been developed. The predictedwarpage from the models was compared to the experimentalmeasurements. It was seen that the low-CTE glass had lowerwarpage than the organic core of equivalent CTE, while increas-ing the CTE of the glass increased the warpage. Also, the underfillfillet size was found to influence the warpage for thin substratepackages, and an optimal fillet size has been identified forminimizing warpage. B-staged and capillary underfill materialswere compared and found to have similar warpage values.

Index Terms— Die warpage, element birth and death, finiteelement simulation, substrate warpage, thin glass substrate.

I. INTRODUCTION

DEVICE packaging today is commonly performed withorganic substrate cores such as FR4 or BT on which dry

film organic build-up layers are deposited to form wiring layerson both sides. However, organic packaging is limited for futuremobile packaging and high performance needs due to theelectrical and mechanical properties of the material. For exam-ple, the coefficient of thermal expansion (CTE) mismatch

Manuscript received October 8, 2015; revised October 31, 2016 andDecember 13, 2016; accepted December 14, 2016. Date of publication Janu-ary 17, 2017; date of current version February 6, 2017. This work was sup-ported by the Low Cost Glass Interposers & Packages global industry consor-tium at Georgia Tech PRC. Recommended for publication by Associate EditorM. Ramkumar upon evaluation of reviewers’ comments.

S. McCann and S. K. Sitaraman are with the Department of MechanicalEngineering, Georgia Institute of Technology, Atlanta, GA 30332 USA(e-mail: [email protected]; [email protected]).

V. Smet is with the Packaging Research Center, Georgia Institute ofTechnology, Atlanta, GA 30332 USA (e-mail: [email protected]).

V. Sundaram and R. R. Tummala are with the Department of Electricaland Computer Engineering, Georgia Institute of Technology, Atlanta,GA 30332 USA (e-mail: [email protected]; [email protected]).

Color versions of one or more of the figures in this paper are availableonline at http://ieeexplore.ieee.org.

Digital Object Identifier 10.1109/TCPMT.2016.2641164

between the organic substrate and silicon die creates warpagebefore and after lead-free solder assembly. The demandfor thinner packages for mobile applications imposes strin-gent requirements for ultrathin substrates, which exacerbateswarpage challenges.

One of the single biggest barriers to ultrathin packages isthe substrate warpage during chip assembly. The mismatch ofCTE between the silicon ICs (3 ppm/°C) and typical organiclaminate substrates (12–18 ppm/°C) not only causes warpageduring assembly, but also induces stress in the interconnectionsleading to solder joint failures. Traditional organic laminatessuch as FR-4 or BT, with prepreg or build-up epoxy dielectricbased redistribution layers (RDLs) are the main substrates usedfor fine-pitch ball grid array (BGA) packages [1], [2]. Suchorganic substrates are often thick with a core thickness rangingfrom 500 µm to 1 mm to allow for sufficient rigidity andlow warpage to meet the JEDEC standard specifications [3].Recently, ultralow CTE organic laminates with CTE in therange of 2–6 ppm/°C have been developed to address thewarpage challenge, by increasing the filler loading and bychanging the glass fabric reinforcement to lower CTE glasses.These low-CTE laminates have significantly improved thewarpage control during IC assembly, with a 7.3−mm ×7.3−mm × 150-µm silicon chip on a 14 − mm × 14 − mm × 260-µm package substrate (core CTE of 1.8 ppm/°C), resulting ina warpage of about 70 µm at room temperature and about35 µm at reflow temperature [4]. Although silicon or ceramicsubstrates can address the warpage with a combination of lowCTE and high elastic modulus, high cost coming from smallwafers or substrates has been a major impediment to adoptionin smart mobile systems.

Glass is an ideal candidate for next-generation packaging,combining the best electrical properties of ceramics, highdimensional stability of silicon, and large panel processingof organics for low cost [5]. The higher elastic modulusof glass should enable much thinner packages than organicsfor the same warpage specifications. The CTE of the glasscan be tailored, allowing larger glass packages to be directlySMT attached to FR-4 boards with high reliability [6]. Glassis smooth and planar, and, therefore, amenable to fabricatingultraprecise fine lines and spaces [7]–[9]. However, glass doeshave challenges in handling, brittleness, and through via for-mation at high speed, although significant progress has alreadybeen demonstrated in addressing these challenges [10]–[12].Although lower warpage is anticipated for glass than organics,given its much higher elastic modulus and low CTE, there hasbeen no published literature quantifying the warpage of lowCTE glass and organic substrates during IC assembly.

2156-3950 © 2017 IEEE. Personal use is permitted, but republication/redistribution requires IEEE permission.See http://www.ieee.org/publications_standards/publications/rights/index.html for more information.

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McCANN et al.: EXPERIMENTAL AND THEORETICAL ASSESSMENT OF THIN GLASS SUBSTRATE FOR LOW WARPAGE 179

Fig. 1. Cross-sectional schematic of a glass BGA package for smart mobileapplication.

Fig. 2. Fabrication and assembly process for glass substrates. (a) Bareglass. (b) With polymer lamination. (c) With electroless seed layer. (d) Withpatterned photoresist. (e) After electrolytic copper. (f) After photoresist stripand copper etch. (g) With second polymer layer of build-up and SAP.(h) After die bonding and underfill.

The objective of this paper, therefore, is to model, design,fabricate, and measure the warpage of glass and organiclaminates at 100-µm core thickness after thermo-compressionbonding (TCB) at 260 °C peak temperature. A cross-sectionalschematic of the proposed glass BGA package for a smartmobile application is seen in Fig. 1. Using detailed finiteelement modeling (FEM) studies, this paper studies core CTE,core modulus, die and substrate thickness, underfill fillet size,and underfill type. This paper extends beyond the initial studiespreviously reported [13], which was limited to two metal-layersubstrates and simple test designs.

II. GLASS SUBSTRATE FABRICATION AND ASSEMBLY

This section outlines the fabrication process that was carriedout to create glass substrates starting with a bare thin glasspanel. The panel was a low-CTE EN-A1 glass from AsahiGlass Co. Ltd., measuring 150 mm × 150 mm × 100 µm, andwould produce a six-by-six array of 18.4 × 18.4 mm2 four-metal-layer substrates. Although the processing was carriedout on a panel, for the sake of clarity, the process steps aredescribed using one substrate, as illustrated in Fig. 2.

A. Glass Panel Fabrication

First, a bare glass panel was cleaned and dried, shown inFig. 2(a). A surface treatment was applied to both sides toenhance the adhesion between the glass and polymer. Then,17.5-µm polymer layer of ZEONIF ZS-100 was vacuumlaminated on both sides of the glass panel using a 60-s vacuumand 10-s pressure. The panel was hot pressed at 115 °C

for 90 s, and then the polymer was cured at a temperatureof 162 °C for 60 min [Fig. 2(b)].

The polymer-laminated panel was then cleaned using adesmear process. A copper seed layer was then depositedusing an electroless bath [Fig. 2(c)]. After the electro-less copper is deposited, a dry film photoresist was lami-nated. A developmental photoresist from Hitachi was exposedand developed [Fig. 2(d)]. Copper was then electroplatedto 10 µm thick, as seen in Fig. 2(e). The photoresist wasstripped, and the copper seed layer is etched, leaving onemetal layer on each side of the panel [Fig. 2(f)]. This methodof copper deposition and patterning is known as semiadditiveprocess (SAP). The above process steps [Fig. 2(b)–(f)] arerepeated to create the next metal layers [Fig. 2(g)].

After the final metal layers were fabricated, a dry-filmphotosensitive solder resist was laminated, cured, exposed,and developed to expose substrate copper pads for flip-chipassembly. An electroless nickel immersion gold surface finishwas used on the exposed copper pads.

Although metal layers were present on top and bottom ofthe glass substrate, no through-glass or polymer vias werefabricated in this paper because through vias are expected tohave little effect on warpage. Fabrication and reliability of viasthrough glass are being pursued by other researchers withinthe 3-D Packaging Research Center at Georgia Tech [14], [15].

B. Silicon on Glass Interconnect Assembly

Prior to assembly, the 150 − ×150 mm2 glass panel wasdiced at 1 mm/s into a six-by-six array of 18.4 × 18.4 mm2

using a Disco dicing tool with a blade intended for silicon.A 10 × 10-mm2 630-µm-thick silicon die was then assem-

bled to the glass substrate, as shown in Fig. 2(h). The silicondie, which was bumped with tin–silver solder, was assembledon the glass substrate by TCB, and the conditions variedbased on the type of underfill. For B-staged underfill, whichwas present during the assembly process, the peak tool headtemperature was 280 °C with 50-MPa pressure for 5 s withthe stage held at 70 °C. For capillary underfill, which wasnot present during the assembly process, the peak tool headtemperature was 260 °C with 1.5-MPa pressure for 5 s withthe stage held at 70 °C (Fig. 3). Additional details on theTCB can be found in [16].

Two different types of underfills with similar modulus andCTE, namely, capillary underfill and B-stage underfill, wereused for different test vehicles to investigate the effect ofunderfill timing on warpage. For the capillary underfill, theunderfill was dispensed in an L-shape along two edges of thedie, and the underfill flowed under the die through capillaryaction after TCB. Fillets were added for the remaining twoedges of the die after the capillary action, and the underfillwas cured at 165 °C for 90 min. For the B-stage underfill,the underfill was dispensed on the die and B-staged for 1 hat 70 °C prior to die assembly and the package was curedat 165 °C for 3 h after assembly. A silicon die assembled ona glass substrate with a B-staged underfill is shown in Fig. 4.

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Fig. 3. Tool head temperature and pressure profile used for TCB on capillaryunderfilled samples. The stage is held at 70 °C throughout the process.

Fig. 4. Silicon die assembled on a four-metal-layer glass substrate withB-staged underfill.

TABLE I

SAMPLES FABRICATED

III. DIE WARPAGE MEASUREMENTS

Shadow moiré measurements were done using akrometrix’sTherMoiré PS200S to determine the warpage of the die–substrate package. Details on shadow moiré can be foundin several publications [17]–[19]. The samples measured forwarpage are presented in Table I.

An example shadow moiré collected for the low-CTE glasssample at room temperature over the die region is shown inFig. 5. The die region measurements were taken from thedie side. The warpage values are computed by looking at themaximum and minimum out-of-plane displacements from theshadow moiré experiments. For example, as seen in Fig. 5,the die region has a positive displacement of 3 µm, whilethe substrate corners have a negative displacement of 5 µm,and thus, the overall warpage for this die–substrate packageis 8 µm. The warpage was dome shaped because the substratecontracted more than the die at room temperature.

Fig. 5. Low-CTE glass sample with B-staged underfill at room temperature(die region shadow moiré measurement from die side) showing 8-µm warpage.

Fig. 6. Die warpage comparison for low-CTE glass and low-CTE organicsamples as a function of temperature.

Die warpage was determined as the difference of the diecenter height and the average corner height, and thus, the datafor each sample at a given temperature are the average of fourmeasured values. Shadow moiré data were collected over atemperature range of 25 °C–260 °C, covering the range oftemperatures experiences in a 260 °C reflow cycle, which isnecessary to attach the package to a system board. The errormargin of the tool and grating used is ±1.5 µm.

It should be pointed out that at temperatures above 220 °C,the solder is likely to be in molten state and, thus, will providepractically no mechanical coupling between the die and thesubstrate. Therefore, at temperatures close to 220 °C andabove, the warpage will be minimal, as seen in Fig. 6.

Fig. 6 shows a comparison of the measured die warpageas a function of temperature for low-CTE glass and low-CTE organic samples. As seen, the die had a maximumwarpage at room temperature, and this warpage continued todecrease as the temperature was increased toward the stress-free temperature. The stress-free temperature for the dielectricpolymer on the glass substrate was 162 °C, for the solderassembly was 220 °C, and for the underfill cure was 160 °C.Therefore, in general, the die region had less warpage at highertemperature than at room temperature.

These samples had identical CTEs (3.3 ppm/°C). The glasshad a modulus of 77 GPa, and the organic had a modulusof 36 GPa. Comparing the low-CTE glass and the low-CTEorganic samples (Fig. 6), the higher modulus core of the glass

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McCANN et al.: EXPERIMENTAL AND THEORETICAL ASSESSMENT OF THIN GLASS SUBSTRATE FOR LOW WARPAGE 181

Fig. 7. Die warpage comparison for low-CTE glass and high-CTE glasssamples as a function of temperature.

samples provided greater rigidity to the package, which led tolower warpage.

Fig. 7 shows a comparison of the measured die warpage asa function of temperature for low-CTE glass and high-CTEglass samples. These samples had similar moduli (77 GPa forthe low-CTE glass and 74 GPa for the high-CTE glass), butthe high-CTE glass had a CTE of 9.8 ppm/°C, while the low-CTE glass had a CTE of 3.3 ppm/°C. Similar to the othersamples, high-CTE Glass showed maximum warpage at roomtemperature, decreasing warpage with increasing temperature,and minimal warpage above 160 °C. Comparing the low-CTEglass and the high-glass samples, low-CTE glass samples haveless warpage because there is less CTE mismatch between thesubstrate and silicon die.

IV. SIMULATION

In parallel to experiments, finite element models werecreated to understand the role of substrate properties andassembly processes on warpage. The modeling was done para-metrically in ANSYS 14.5, using plane-strain approximation.

A. Model Geometry and Mesh

Although 2.5-D or 3-D models are desirable to accountfor property and geometry variations in the third dimension,2-D models are appropriate for comparison between differentcases. Fig. 8 shows a schematic of the plane-strain model forthe low-CTE glass sample. The glass or organic substrate, thepolymer layers, copper RDLs, solder interconnects, underfill,and silicon die were included in the models. There were novias in the models, as in the experiments. The die–substrateassembly was cut along the diagonal with symmetry boundaryconditions on one side, as illustrated in Fig. 8. One node at theleft bottom was fixed in the y-direction to prevent rigid bodymotion. The fixed node was within the glass, as the glass ispresent from the beginning of fabrication, which is importantfor process modeling.

B. Material Properties

Table II shows the thermo-mechanical material proper-ties used in the models. Silicon’s modulus is directionally

Fig. 8. Example plane-strain model for the low-CTE glass sample.

TABLE II

MATERIAL PROPERTIES

dependent based on crystal orientation and standardprocessing, with the in-plane modulus being higher thanthe out-of-plane modulus or [100] direction [20]. Propertiesfor the polymer, ZEONIF ZS-100, were obtained from themanufacturer, Zeon Corporation. The low- and high-CTEglass represent the published properties for Asahi Glass Co.,Ltd.’s glass [21]. For the electroplated copper, temperature-dependent material properties were used [22]. An Anandviscoplastic model of solder was used to model the defor-mation of tin–silver solder [23], [24]. No surface finish wassimulated as surface finish thickness was several orders ofmagnitude less than the substrate thickness, and thus, thepresence of surface finish in the model was not likely toinfluence the predicted warpage results.

C. Process Modeling: Element Birth and Death

To mimic the actual fabrication process, element “birth” and“death” were used in the simulation model. At the beginning ofprocess simulation, only the glass core was present, as shownin Fig. 2(a). Therefore, the simulation started with “birthing”the glass panel, and “killing” all other layers or materials. Sucha “killing” or death means that such material elements werepresent in the model, however, with a modulus of elasticity thatis six orders of magnitude less than other “birthed” materials.

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182 IEEE TRANSACTIONS ON COMPONENTS, PACKAGING AND MANUFACTURING TECHNOLOGY, VOL. 7, NO. 2, FEBRUARY 2017

Fig. 9. Fabrication and assembly process temperature sequence used in birthand death modeling.

Material elements were “birthed” sequentially with their actualproperties at their stress-free temperature (Table II).

Fig. 9 illustrates the solution steps for a four-metal-layerpackage. As seen, starting from room temperature: 1) the glasscore was simulated to be heated to 160 °C, the temperatureat which the dielectric polymer was cured; 2) the glass coreand polymer were then simulated to be cooled to roomtemperature; 3) subsequently simulated to be heated to 40 °C;and 4) the temperature at which copper was electroplated.The process steps were repeated for the next two metallayers (5–9). These simulation steps completed the fabricationof the glass substrate with RDLs.

The next step was to simulate the flip-chip assemblyprocess. The substrate with build-up layers was then sim-ulated to be heated to 220 °C, the melting temperature oftin–silver solder, to mimic the reflow assembly process,where the chip, solder, and chip pads were “birthed” (10).The assembly was then uniformly cooled to the underfillcure temperature of 160 °C (11) and then further cooleddown to room temperature (12). This simulation mimics theB-staged underfill cure process. On the other hand, for acapillary underfill, the assembly is first cooled to room temper-ature from the reflow temperature, underfill is then dispensedat 90 °C on a hot plate, and then the underfill is cured ata temperature of about 160 °C. The current model does notinclude such cooling and reheating steps, as the results fromboth modeling approaches are nearly the same [26]. Also, thecurrent single-step cooling model from reflow temperature toroom temperature through underfill cure temperature is lesscomputationally expensive. Thus, the warpage of the assemblythrough the entire fabrication and assembly process simulationis captured.

D. Warpage Prediction and Validation

The warpage predicted by the finite element models wasvalidated against warpage measured using shadow moiré.An example of this validation is depicted in Fig. 10, whichshows the two experimental samples and simulated warpagedata as a function of temperature for the low-CTE glasssample. Both experimental and simulated results show the

Fig. 10. Predictive model validation for low-CTE glass sample.

maximum warpage at room temperature, and the magnitudepredicted by the simulations agrees with the experimental data.The model captures the decrease in warpage as the temperatureis increased.

Through vias were not included in the experimental samplesand the corresponding modeling because they were expectedto have relatively little effect. Models with fully filled throughvias were constructed to investigate the validity of this claim.Except for the presence of the vias, the models were otherwiseidentical to low-CTE glass samples in Table I. Assuming100-µm-diameter vias in an 18.4 × 18.4-mm2 substrate with400-µm board-level pitch on, the maximum necessary totalcopper volume is less than 5%. With this number of vias, thewarpage increases by 8.8% compared to the case without vias.However, the typical number of vias is often much lower, at1% or less. With this number of vias, the warpage increasesby 0.3% compared to the case without vias.

E. Effect of Die and Substrate Thickness

The warpage depends on both the die and substrate thick-ness as seen in Fig. 11, in which the predicted die warpagefor 100-, 200-, 400-, and 630-µm dies is plotted for 50-, 100-,200-, 300-, 400-, 500-, and 600-µm-thick glass substratesat 25 °C. The structures are otherwise assumed to be identicalto the low-CTE glass samples in Table I. From this plot,decreasing the die thickness increases the warpage. Also,decreasing the glass thickness increases the warpage. However,as long as the overall package is at 400-µm thick, the diewarpage is not predicted to exceed 10 µm. JEDEC requireswarpage to be less than 100 µm [3]. A package that is 400 µmthick, includes 70 µm of dielectric polymer, 40 µm of copper,and a 10 × 10-mm2 die, and exhibits less than 10 µm warpage(Fig. 11) shows glass is a strong candidate for low warpage.

V. UNDERFILL FILLET

Package-level warpage is important for board-level assem-bly, and thus, substrate warpage is modeled and experimentally

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McCANN et al.: EXPERIMENTAL AND THEORETICAL ASSESSMENT OF THIN GLASS SUBSTRATE FOR LOW WARPAGE 183

Fig. 11. Predicted die warpage (µm) as a function of glass thickness (µm)at 25 °C.

Fig. 12. Substrate region shadow moiré measurement from board side oflow-CTE glass sample at room temperature.

characterized. Fig. 12 shows an example shadow moiré mea-surement of the substrate at room temperature for a low-CTEglass sample. Substrate warpage measurements are taken fromthe non-die side due to the step height limitation of the shadowmoiré technique.

It was observed that the die and substrate warp in differentdirections below the stress-free temperature, as seen in Figs. 5and 12. This was because of the underfill fillet. As the underfillused in our study has a large CTE, it shrinks more than thesurrounding material, exerting a force that causes the substrateto bend. Thus, substrate warpage is influenced by the underfillfillet. Fig. 13 shows a cross-sectional schematic of this effectat room temperature. Near the stress-free temperature, thepackage is flat because the underfill fillet exerts no force onthe package.

With no underfill fillet or a very small fillet, the substratecontinues the dome shape of the die region below the stress-free temperature, as shown in Fig. 13(b). At the stress-freetemperature, the substrate is near flat. Varying the fillet sizebetween large [such as in Fig. 13(a)] and very small [such asin Fig. 13(b)] varies the amount of substrate warpage, and anintermediate size fillet is shown in Fig. 13(c).

Fig. 13. Warpage trend observed in thin glass substrate packages at roomtemperature for (a) large fillet, (b) no fillet, and (c) intermediate size fillet.

Fig. 14. Predictive model validation substrate warpage for the low-CTE glasssample.

A. Experimental Substrate Warpage

Shadow moiré measurements for substrate warpage, suchas in Fig. 12, were taken over a range of temperatures, andthe results are shown in Fig. 14 for low-CTE glass samples.Fig. 14 also includes the finite element model prediction.The finite element model used a fillet size of 240 µm totrack the experimental data. At 25 °C, the model predictsa shape that is dome-like where the die is and bowl-likebeyond the die region, similar to the W-shape in Fig. 13(a).As seen, the simulations show decreasing warpage withincreasing temperature. The warpage is minimum near theunderfill cure temperature. This is to be expected becausethe large structures in the assembly, namely, the die andthe substrate, are tightly bonded together by the underfillat the underfill cure glass transition temperature, and thus theunderfill cure temperature is near the stress-free temperaturefor the assembly.

B. Effect of Underfill Fillet on Substrate Warpage

The warpage is influenced significantly by underfill fillet,and along a die edge, there was a continuous fillet that

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Fig. 15. Warpage (µm) contour plot of low-CTE glass samples (Table I)with (a) full fillet, (b) half fillet, and (c) no fillet, at 25 °C.

influences the substrate warpage. This fillet can be adequatelycaptured through plane-strain approximation. On the otherhand, the corner warpage is influenced by the fillets onboth edges of the corner as well as the corner fillet itself,and therefore, it is difficult to capture through one cross-section model. The simulation result shown in Fig. 14 assumesa 240-µm fillet to match the experimental data. For a fillet thatis 630 µm tall (touches the top edge of the die) and 630 µmlong, the deformed assembly images are shown at 25 °C inFig. 15(a). This result is similar to the shape seen in Fig. 13(a).

To understand the role of the underfill fillet size, differentsizes of fillets were simulated. In all of the simulations, thestress-free temperatures, the geometry, and the mesh were keptidentical to be able to compare different cases. The warpedgeometry, as simulated, with a fillet that is 315 µm tall and315 µm long is shown in Fig. 15(b) at 25 °C. As seen,the substrate was less warped than the full fillet [Fig. 15(a)].The third case, which has no fillet, was also simulated, andthe results are shown in Fig. 15(c). The no fillet case is nearlyflat. In all cases, the die warpage is nearly identical, and this isbecause the fillet has minimal effect on the warpage of the die.

The substrate warpage is relevant in package to boardassembly, and the planarity of the package determines whetherassembly is feasible. As the substrate warpage is a functionof the fillet size, it is possible to optimize the fillet size for aminimum substrate warpage. For the low-CTE glass samples(Table I), the model predicted a minimum substrate warpagewith an 81-µm fillet. It should be noted that the optimalfillet size will change as a function of sample geometry,material CTE, and material modulus.

The degree to which the influence of the underfill filletis observed is enhanced by how thin the glass substrate isand how thick the silicon die is. The impact of underfill filletsize observed in glass should be true for other similarly thinsubstrates as well.

C. Capillary and B-Staged Underfill Comparison

Low-CTE glass samples with capillary underfill were fab-ricated in addition to low-CTE glass samples with B-stagedunderfill to compare underfill materials. Fig. 16 shows thecomparison of die warpage measured using shadow moiré.The die warpage results are similar between the two underfills,indicating that the two underfills couple the die and substrate

Fig. 16. Die warpage as a function of temperature for capillary and B-stagedunderfill.

together to a very similar degree. This is because the modulusof the two underfills is very close, at 2.9 GPa for the B-stagedunderfill and 3.0 GPa for the capillary underfill. Based on thesedata, the underfill type has little impact on the warpage andthe choice for underfill will be based on other considerations,such as desired bump pitch and assembly process conditions.

VI. CONCLUSION

The objective of this paper is to develop a flip-chip packagewith low warpage and understand the role of various parame-ters on warpage.

This paper has experimentally used thin glass panels asthe core material for microelectronic packaging and foundto have low warpage due to the high rigidity and siliconmatched CTE of glass. The fabrication process to depositbuild-up materials creates residual stresses due to the CTEmismatch between the core and build-up materials. This paperemployed similar structures on both sides of the glass panel,resulting in minimal warpage prior to assembly. The die isthermo-compression bonded and warpage is measured fromthe die and substrate sides. Low-CTE glass was demonstratedto have lower die warpage than low-CTE organic because ithas a higher modulus, providing greater structural rigidity.Low-CTE glass also had lower warpage than high-CTE glassbecause it has less CTE mismatch with the silicon die. Thesewarpage values are all lower than what is required by theJEDEC standard.

In conjunction with the experimental work, physics-basedfinite element models have been developed to mimic fabrica-tion and assembly processes. The model predictions agree wellwith the warpage values and trends seen from experiments.The underfill fillet greatly influences the shape of the substratewarpage after assembly at room temperature. Larger filletswarp the substrate upward around the die, while smaller filletshave less impact on the substrate warpage. It is possible tominimize substrate warpage through fillet size control, and anoptimal fillet size for minimum warpage was identified.

ACKNOWLEDGMENT

The authors would like to thank M. Kobayashi, A. Mieno,S. Raghavan, C. White, and J. Bishop.

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REFERENCES

[1] W. Lin, S. Wen, A. Yoshida, and J. Shin, “Evaluation of raw substratevariation from different suppliers and processes and their impact onpackage warpage,” IEEE Trans. Compon., Packag., Manuf. Technol.,accepted for publication.

[2] P. Lall, K. Patel, and V. Narayan, “Model for prediction of package-on-package warpage and the effect of process and material parameters,” inProc. ECTC, Las Vegas, NV, USA, 2013, pp. 608–622.

[3] Package Warpage Measurement of Surface-Mount Integrated Circuits atElevated Temperatures, document JESD22-B112A, JEDEC, 2009.

[4] T. Kotake, H. Murai, S. Takanezawa, M. Miyatake, M. Takekoshi, andM. Ose, “Ultra low CTE (1.8 ppm/°C) core material for next generationthin CSP,” in Proc. ECTC, Orlando, FL, USA, 2014, pp. 1407–1410.

[5] V. Sundaram et al., “First demonstration of a surface mountable, ultra-thin glass BGA package for smart mobile logic devices,” in Proc. ECTC,Orlando, FL, USA, 2014, pp. 365–370.

[6] X. Qin, N. Kumbhat, V. Sundaram, and R. Tummala, “Highly-reliablesilicon and glass interposers-to-printed wiring board SMT interconnec-tions: Modeling, design, fabrication and reliability,” in Proc. ECTC,2012, pp. 1738–1745.

[7] H. Lu et al., “Demonstration of 3–5 µm RDL line lithography on panel-based glass interposers,” presented at the ECTC, 2014.

[8] R. Furuya et al., “Demonstration of 2µm RDL wiring using dry filmphotoresists and 5µm RDL via by projection lithography for low-cost 2.5D panel-based glass and organic interposers,” in Proc. ECTC,San Diego, CA, USA, 2015, pp. 1488–1493.

[9] P. M. Raj et al., “‘Zero-undercut’ semi-additive copper patterning—A breakthrough for ultrafine-line RDL lithographic structures and preci-sion RF thinfilm passives,” in Proc. ECTC, San Diego, CA, USA, 2015,pp. 402–405.

[10] A. Shorey et al., “Advancements in fabrication of glass interposers,” inProc. ECTC, Orlando, FL, USA, 2014, pp. 20–25.

[11] A. B. Shorey, S. Kuramochi, and C. H. Yun, “Through glass via (TGV)technology for RF applications,” in Proc. IMAPS, Orlando, FL, USA,2015, pp. 386–389.

[12] S. McCann, Y. Sato, V. Sundaram, R. R. Tummala, and S. K. Sitaraman,“Prevention of cracking from RDL stress and dicing defects in glasssubstrates,” IEEE Trans. Device Mater. Rel., vol. 16, no. 1, pp. 43–49,Mar. 2016.

[13] S. R. McCann, V. Sundaram, R. R. Tummala, and S. K. Sitaraman,“Flip-chip on glass (FCOG) package for low warpage,” in Proc. ECTC,Orlando, FL, USA, 2014, pp. 2189–2193.

[14] K. Demir, A. Armutlulu, J. Tong, R. Pucha, V. Sundaram, andR. Tummala, “First demonstration of reliable copper-plated 30µmdiameter through-package-vias in ultra-thin bare glass interposers,” inProc. ECTC, Orlando, FL, USA, 2014, pp. 1098–1102.

[15] G. Kumar et al., “Coaxial through-package-vias (TPVs) for enhancingpower integrity in 3D double-side glass interposers,” in Proc. ECTC,Orlando, FL, USA, 2014, pp. 541–547.

[16] V. Smet, M. Kobayashi, T. Wang, P. M. Raj, and R. Tummala, “A newera in manufacturable, low-temperature and ultra-fine pitch Cu intercon-nections and assembly without solders,” in Proc. ECTC, Orlando, FL,USA, 2014, pp. 484–489.

[17] W. Tan and I. C. Ume, “Application of lamination theory to studywarpage across PWB and PWBA during convective reflow process,”IEEE Trans. Compon., Packag., Manuf. Technol., vol. 2, no. 2,pp. 217–223, Feb. 2012.

[18] P. S. Theocaris, “Moiré topography of curved surfaces,” Experim. Mech.,vol. 7, no. 7, pp. 289–296, 1967.

[19] H. Ding, R. E. Powell, C. R. Hanna, and I. C. Ume, “Warpagemeasurement comparison using shadow Moiré and projection Moirémethods,” IEEE Trans. Compon., Packag., Manuf. Technol., vol. 25,no. 4, pp. 714–721, Dec. 2002.

[20] M. A. Hopcroft, W. D. Nix, and T. W. Kenny, “What is the Young’smodulus of silicon?” J. Microelectromech. Syst., vol. 19, no. 2,pp. 229–238, 2010.

[21] L. Asahi Glass Co. (Nov. 2014). Alkali-Free Glass for Backside Grind-ing Process. [Online]. Available: http://www.agc.com/english/products/electronics/ena1.html

[22] R. S. Li and J. Jiao, “The effects of temperature and aging on Young’smoduli of polymeric based flexible substrates,” Int. J. MicrocircuitsElectron. Packag., vol. 23, no. 4, pp. 456–461, 2000.

[23] R. Darveaux, “Effect of simulation methodology on solder joint crackgrowth correlation,” in Proc. ECTC, 2000, pp. 1048–1058.

[24] N. Bai, X. Chen, and H. Gao, “Simulation of uniaxial tensile propertiesfor lead-free solders with modified Anand model,” Mater. Design,vol. 30, no. 1, pp. 122–128, 2009.

[25] Z. Corporation. (2011). ZEONIF: Insulation Materials for PrintedCircuit Boards. [Online]. Available: http://www.zeon.co.jp/business_e/enterprise/imagelec/zeonif.html

[26] M. Variyam, V. Sundararaman, S. K. Sitaraman, J. Wu, R. T. Pike, andC. P. Wong, “High-temperature, low-modulus adhesive attach for large-area thin-film processing on silicon and alumina tiles,” IEEE Trans.Electron. Packag. Manuf., vol. 22, no. 4, pp. 290–294, Oct. 1999.

Scott McCann, photograph and biography not available at the time ofpublication.

Vanessa Smet, photograph and biography not available at the time ofpublication.

Venky Sundaram, photograph and biography not available at the time ofpublication.

Rao R. Tummala, photograph and biography not available at the time ofpublication.

Suresh K. Sitaraman, photograph and biography not available at the timeof publication.