2009 Workshop Mix Design Procedures for Lime Stabilized Soil

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    Mixture Design Procedures

    for

    Lime Stabilized SoilODOT GCW 5/13/09

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    2

    Dolomitic Lime

    High Calcium Lime

    Hydrator

    Terminals

    CL&S Lime Plants and Terminals

    PLANTS

    1.....Blind River, Ontario

    2.....Dundas, Ontario

    3.....Beachville, Ontario

    4.....River Rouge, MI

    5.....Manitowoc, WI

    6.....South Chicago, IL

    7.....Gary, IN

    8.....Millersville, OH

    9.....Maple Grove, OH

    10...Grand River, OH

    11...Annville, PA

    12...Winchester, VA

    13...Strasburg, VA

    14...Black River, KY

    15...Maysville, KY

    16...Longview, AL

    17...Macon, GA

    TERMINALS

    A.....Baton Rouge, LA Terminal

    B....Tampa Terminal, Tampa, FL

    C.....Fort Lauderdale Terminal, FL

    D.....Sanford Terminal, FL

    E.....Jacksonville Terminal, FL

    F.....Brunswick Terminal, GA

    G....Raleigh Terminal, NC

    H.....Richmond Terminal, VA

    I......Hagerstown Terminal, MD

    J.....Detroit Terminal, MI

    1

    23

    4

    5

    67 8 9

    10 11

    12

    14

    13

    15

    16 17

    A

    B

    C

    D

    E

    F

    G

    H

    I

    J

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    CaCO3 + MgCO3 CaO + MgO + CO2

    CaO + MgO ---Quicklime

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    Lime Products for Treating Soil at the

    Construction Site

    Quicklime:

    Total Oxides 90%CaO/MgO

    Meets ASTM C977

    EnviroLime (Lime Kiln Dust)Total Oxides 18% - 30%

    Alumina & Silica Oxide 7% - 15%

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    Lime Treatment Options

    Drying up wet soil: Plasticity and swell reduction

    Modification:

    Plasticity and swell reduction Improved stability and compaction

    Solid working platform

    Stabilization:

    Permanent strength increase Long-term strength gains

    Less moisture absorption

    Freeze-thaw durability

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    Pozzolanic Reactions Using Lime

    (Clay Soil)

    On-going reaction with

    available silica and

    alumina in the soil forms

    complex cementitious

    materials (the

    POZZOLANIC effect.)

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    Lime-Soil Pozzolanic Action

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    STATE OF OHIO

    DEPARTMENT OF

    TRANSPORTATIONSUPPLEMENT 1120

    Mixture Design for Chemically

    Stabilized Soils

    July 20, 2007

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    Procedures developed by Dr. Dallas Little, Texas A&M University

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    1. Right Combination of Materials

    Requirements for Lime Stabilization

    3. Adequate Strength to Resist Freeze-Thaw

    2. Adequate Lime to Keep Pozzolanic Action Going

    4. Adequate Compaction and Moisture

    Clay contains silica and alumina

    Silt and sand

    Lime

    LKD

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    Lime Based Mix Designs for

    Different Soil Types

    AASHTOGroupClassification

    SoilType

    UnifiedGroup Symbol

    RecommendedAdditives

    GW GP GM GC SW SP SM SC ML CL OL MH CH OH PT

    A-1-a A-1-a A-1-b A-1-b A-1-bA-1-b

    orA-3

    A-2-4or

    A-2-5

    A-2-6or

    A-2-7A-4 A-6 A-4 A-5 A-7-6 A-7-5 A-8

    Poorlygra

    de

    dgrave

    lsan

    dgrave

    l

    san

    dm

    ixtures,

    littleorno

    fines

    LIM (Stabilization & Modification)

    LIME PLUS TYPE F Coal Fly sh (Stabilization)

    We

    llgra

    de

    dgrave

    lsand

    grave

    lsan

    d

    mixtures,

    littleorno

    fines

    Siltygrave

    ls,

    grave

    l-san

    d-s

    iltm

    ixtures

    Clayeygrave

    ls,

    grave

    l-san

    d-c

    laym

    ixtures

    We

    ll-gra

    de

    dsan

    dsandgrave

    llysan

    ds,

    littleorno

    fines

    Poorlygra

    de

    dsan

    dsand

    grave

    lly

    san

    ds,

    littleorno

    fines

    Siltysan

    ds,

    san

    d-s

    iltmix

    tures

    Clayey,

    san

    ds,

    san

    d-c

    laym

    ixtures

    Inorgan

    ics

    ilts,

    very

    finesan

    ds,

    roc

    k

    flour,s

    iltyorc

    layey

    finesan

    ds

    Inorgan

    icc

    layso

    flow

    to

    me

    dium

    plas

    tic

    ity,

    grave

    llyc

    lays,

    san

    dyc

    lays,

    siltyc

    lays,

    leanc

    lays

    Organ

    ics

    iltsan

    dorganic

    siltyc

    layso

    f

    lowp

    las

    tic

    ity

    Inorgan

    ics

    ilts,

    micaceou

    sor

    diatomaceous

    finesands

    ors

    ilts,

    elas

    tics

    ilts

    Inorgan

    icc

    layso

    fhighplas

    tic

    ity,

    fatc

    lays

    Organ

    icc

    layso

    fme

    dium

    tohighp

    las

    tic

    ity

    Pea

    t,muc

    k,

    an

    do

    therh

    ighlyorgan

    icso

    ils

    Lime stabilization should be considered when:

    - Soil PI > 10 and

    - % passing #200 > 25%

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    Requirements for Lime Stabilization

    Adequate Strength to Resist Freeze-Thaw

    Adequate Lime to Keep Pozzolanic Action Going

    Adequate Compaction and Moisture

    Right Combination of Materials

    Clay contains silica and alumina Lime

    Silt and sand LKD

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    Time

    Strengt

    h

    Autogenous Healing

    Strength Changes with Time and Temp

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    Laboratory Evaluations for Lime Stabilization

    1. pH Determination for Minimum Lime Content:

    ASTM D 6276 (Eads Grim Test)

    Min amount of lime to raise soil pH level to 12.4

    2. Optimum Moisture ContentASTM D 698 (Standard Proctor Density)

    Generally increases with lime or LFA

    3. Unconfined Compressive StrengthASTM D 5102

    Minimum of 100 psi

    Freeze-thaw durability

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    In place moisture content Particle size analysis

    Liquid limits, plastic limit, PI

    Soil classification

    Optimum moisture content

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    Laboratory Evaluations for Lime Stabilization

    1. pH Determination for Minimum Lime Content:- ASTM D 6276 (Eads Grim Test)

    Min amount of lime to raise soil pH level to 12.4

    2. Optimum Moisture ContentASTM D 698 (Standard Proctor Density)

    Generally increases with lime or LKD

    3. Unconfined Compressive StrengthASTM D 5102

    Minimum of 100 psi

    Freeze-thaw durability

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    Mix Design for Lime Stabilization

    pH Determination for Minimum Lime Content:

    ASTM D 6276 (Eads Grim Test)

    Min amount of lime to raise soil pH level to 12.4

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    ASTM D 6276 - Significance & Use

    The soil-lime pH test is performed as a test to indicate thesoil-lime proportion needed to maintain the elevated pH

    necessary for sustaining the reactions necessary to stabilizesoils (i.e., the min. % of lime required to raise thesoils pH to 12.4).

    What the test does:

    The test provides no reliable information relative to thepotential reactivity of a particular soil, nor will it provideinformation on the magnitude of increased strength realizedupon treatment of this soil with the indicated percentage oflime.

    What the test does not do:

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    Specifications: Memory function stores up to 50 sets of customizable pH, mV, or

    relative mV with the temperature at the time of the reading

    For more accurate results, pH calibration can be done using one,

    two or three-point, auto-buffer recognition or by choosing USA or

    NIST* buffer sets

    pH mode: 0.00 to 14.00pH; with a resolution of 0.01pH with

    accuracy of 0.01pH

    Temperature: 0.0 to 100.0C with a resolution of 0.1C and an

    accuracy of 0.3C

    Caution (pH meter):

    Not all pH meters are created equal!!! 1120.03 Sec A

    To ensure the best test results, look for the followingspecifications when selecting a pH meter to use for this test:

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    7

    8

    9

    10

    11

    12

    13

    0 2 4 6 8

    pH = 12.4

    % Lime 5% Lime

    Measured

    pH

    ASTM D 6276 (Eads Grim Test)

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    Laboratory Evaluations for Lime Stabilization

    1. pH Determination for Minimum Lime Content:- ASTM D 6276 (Eads Grim Test)

    Min amount of lime to raise soil pH level to 12.4

    2. Optimum Moisture ContentASTM D 698 (Standard Proctor Density)

    Generally increases with lime or LKD

    3. Unconfined Compressive StrengthASTM D 5102

    Minimum of 100 psi

    Freeze-thaw durability

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    92

    94

    96

    98

    100

    102

    104

    106

    108

    10 15 20 25 30

    No Lime

    5% Lime

    OMC = 17%

    DryDensity(PCF)

    Lime Changes Optimum Moisture Content

    OMC = 21%

    Moisture (%)

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    Laboratory Evaluations for Lime Stabilization

    1. pH Determination for Minimum Lime Content:- ASTM D 6276 (Eads Grim Test)

    Min amount of Lime to raise soil pH level to 12.4

    2. Optimum Moisture ContentASTM D 698 (Standard Proctor Density)

    Generally increases with lime or LKD

    3. Unconfined Compressive StrengthASTM D 5102

    Minimum of 100 psi

    Freeze-thaw durability

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    Mix soil, lime and water at OMC for UCCS specimens

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    Compacted at OMC for UCCS specimens

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    Expansion Testing (ODOT 1120.06)

    Measure the height and circumference of the UCSspecimens after curing (dry) and then measure

    again after 24 hour Capillary Soak Test.

    Report in percentage if the change of initial (dry)and soaked exceeds 1.5%

    This is NOT a NLA required test and typicallyshows NO real value to the mix design

    procedure.

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    Cure the UCCS Specimensfor 7 days @ 40 C

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    Strength Required for Durability (ODOT)

    Unconfined CompressiveStrength after 7 day cure at40 C and 24 hour CapillarySoak:

    50 psi greater thanUCS with no Lime

    Minimum 100 psi

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    Laboratory Evaluations for Lime Stabilization

    1. pH Determination for Minimum Lime Content:

    ASTM D 6276 (Eads Grim Test)

    Min amount of Lime to raise soil pH level to 12.4

    2. Optimum Moisture ContentASTM D 698 (Standard Proctor Density)

    Generally increases with lime or LFA

    3. Unconfined Compressive StrengthASTM D 5102

    Minimum of 100 psi before freezing

    Freeze-thaw durability

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    Differences When Testing LKD

    No 24 hour mellowing period Why? Increased strength requirements 150 psi vs. 100

    psi Why?

    Curing procedures remain the same.

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    Typical laboratory mistakes

    Compaction of OMC/MDD and UCS specimensprior to a 24 hour mellow period. Inadequatehydration of Lime can lead to poor OMC/MDDresults and poor UCS.

    pH meter not equipped to reach a reading higherthan 12.4. pH buffer solutions not up to 12.45 and may be

    expired.

    Mixing Lime, soil, and water by hand and not usinga mixer. Inadequate dispersion of Lime throughoutthe mix.

    Old Lime. Lime is a perishable and needs to befresh for mix design. 60 days typical.

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    Outside Comments

    Eads-Grim pH test is designated for Quicklime andHydrated Lime. Sometimes it is very difficult toachieve a pH of 12.4 when using LKD. Why?

    When bidding the testing, it seems to be difficult to

    get a grasp on how many actual test need to beperformed because we dont know how many soiltypes are on a given project. Bidding this item as aunit price would be much easier and competetive(Price per soil type).

    Time seems to be a very limiting factor to thespecification.

    We have never seen any results from the swelltest.

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    1. Right Combination of Materials

    For Lime, PI > 10 and % passing #200 > 25%

    Requirements for Lime Stabilization

    4. Adequate Strength to Resist Freeze-Thaw

    UCS > 100 psi (after 7 days @ 40 curing, 24-hr cap. soak)

    2. Adequate Lime to Keep Pozzolanic Action Going pH = 12.4 (per ASTM D 6276)

    3. Adequate Compaction and Moisture

    With Lime, the OMC increases, MDD decreases

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    Lime Treatment Options

    Drying up wet soil: Plasticity and swell reduction

    Modification: Plasticity and swell reduction

    Improved stability and compaction

    Solid working platform

    Stabilization:

    Permanent strength increase Long-term strength gains

    Less moisture absorption

    Freeze-thaw durability

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    Any Questions?