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IS

a 419 - 1967

Superseding IS I 420 - 1953 )

Indian StaPzdard

SPECIFICATION FOR

PUTTY, FOR USE ON WINDOW FRAMES

First Revision )

Fifth Reprint NOVEMBER 1991

( Incorporating Amendment No. I )

UDC 691

.X35

@ coPrr;ght197 1

BUREAU OF INDIAN STANDARDS

MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG

NEW DELHI llOflO2

Sept ember 1967

( Reaffirmed 2002 )

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( SuperoedingS t420 1953

I ndian St andard

SPECIFICATION .FOR

PUTTY, FOR USE ON WINDOW FRAMES

Fi rst Rev i si on

Paints ad Allied Products Sectional Committee, CM2 8

Chairman

h~ W. E. i%RRlS

Vice-Chairttratr

SURL S. S. N YUDU

Members

Repesenlitrg

Gvotllass Nerolac Paints Private Ltd, Bombay

So l u r laiut & ~aruisb ManulLlcturing

CillCUllil

SHIU

H. N.

~

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IS :

419 - 1967

SIIRI

M. JJ.

SATYANAILAYAN,~ (

Allemzlr?)

Smr P. G. V. RAXIANAN Indian Aluminiunl Co J.ltl.

~~alcr~tc;t

SHW H. S.

CHAWLA ( dlerunle)

SUXI M. N. R.zo

Indian Paint Association. (:alcutla

SIral 13. V. D.\I.AL Alternate)

SHltI

R. I(. J

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IS :

419 1967

I ndian St andard

SPECIFICATION FOR

PUTTY, FOR USE ON WINDOW FRAMES

Fi rst Rev i si on

0. FOREWORD

This Indian Standard ( First Revision ) was adopted by the Indian.

Institution on 30 June 1967, after the draft finalized by the Paints

Allied Products Sectional Committee had been approved hy the Chemical

is standard \vas first published in 1953 when it covered putty for use

wooden frames.

At the time of revision of this standard, the concerned

Committee decided to enlarge its scope to cover putty for USC (HI

also, which was covered by IS : 420-1953*. Consequently,

standard supcrscdcs IS : 4.20-1953* which has since been withdrawn.

In drawing up the alnalgamated revision,

adequate consideration has

given to stipulate various reyuiremcnts independent of approved sample.

the formulation of a specification for whitine for putty ( SEC S

:

2468-

) reference to this standard has been given m the composition of thct

Performance test for consistency has, been improved by making it

objective. At1 other changes found necessary as a result of cxpcricancc

through the use of the standard have also been effected.

.

0.3.1 Full aliquucnt of JSS 3070

Specification

for putty

issurtl by 1l1(*

of Standardization, Ministry of Defence,

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IS : 419 - 1967

8.6 For the purpose of deciding whether a ,particular requirement of this

standard is complied with, the final value, observed or calculated, expressing

the result uf a test or au+&, sh;dl be rounded oil iu accordance with

1s

:

2-19(i0*. The number ol significant places retained in the muuded OK

value should be the same a~ that of the specified value in this standard..

I.. SCOPE

,

1.1 This standard prescribes the requirements and the method5 of sampling

and test for putty for use in fixing glass panes on wood and metal hames and

for filling splits, cracks and holes in wood nr metal.

2.

TERMINOLOGY

2.1

For the purpose of this standard, the definitions given under 2 of

IS

:

85l XOt, in IS

:

1303-I 9G3$ and the following shall apply:

Scl l i t y l i ruc -

Ihc

time taken fnr the putty to ronvert itself into

cohesive mass which dncs not yield to specified pressure applied nlier

a specified drying timr.

3. REQUIREMENTS

3.1 Form and Condition

- The material shall bc hnmngenenus paste and

shall be free from grit and other visible impurities.

3.2 Composition -

The matcriid sMl consist nnl\, of whiting ( conhlniny

t ~ IS :

24(i8-1 K3 ),

linseed nil, raw ( cothmhg to IS :

75-l J5O(l

i :wcl

suitaljle varnish medium in surh prnpnrtinus as to forIn n p:~qtcwhic.lr shnll

comply with the requirements of this standard.

3 3 Consistency-

The material, after thnrnllgh working in Ilands, sh:lll

~avc good plastic quality without sliminess or stickiness thnt wi)lIId ret&r it

iificult to handle and apply.

3.3.1. In addition, it shall work readily and smnnthly under a palettc

kllifc

>ltlout crumbling or cracking and, after bring moulded in place, it sh;~ll

i -:-et-t itself into a cohesive mass which dnes not yield to spcrilictl prrssllrth

;r

*?ied after 72 hours ils prcscsil)ed iii hppcndix A.

3.4 Ihe material shall also comply will1 tllc requirements given in Table 1.

*R&s for rountlillg dtm~mrriral values ( re:iwd .

-Methods of test for oil pss~es for paints.

Glossarv of terms relating to paints ( rr~i.wcl ).

:q

d p&f&ion for whiting for putty.

,~bpecification for linseed oil, raw, for paints.

( Since revised

),

4

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IS : 419 - 1967

TABLE 1 REQ

UILIEMENTS FOR PUTTY, FOR USE ON WINDOW FRAMES

i Cluuhe 3.4 )

sr.

CHAR ACTERIRTIC REQI~IREMIZNT Xhrmm OBTEST

, Nu.

(REFTO CL No.xn

IS : 8S- i954P )

(1)

(2)

(3)

4)

i) Residue on sieve, percent by

5.0

9

weight

Max

ii) Water content, percent hy

1.0

10

weight, Max

iii) Keeping properties

Not less than

13

G months

*Methods of test for oil pastes for paints.

4. PACKING AND MARKING

4.1 Packing

- Thr maierial slxdl lw snitd~ly pnrlwd ns np=rcl to lw~um=n

the purchaser and the supplier.

4.2

Marking -

The containers shall be marked with the name of the

material; manufacturers name and trade-mark, if any; w&lit of tile material:

and month and year of manufacture.

4.2.1 The containers may also be marked \ vith tlw TST C ~Mkuticm

hlark.

NOTF:-T~IP use of the IS1 Ckr~ifiration Mark is gmwhcl by 111r proviriona nf

the Indian Standards Ins1iluliou ( (:rrtific.ation Marks ) ACI ad chr Ruler and

Regulations made thereunclrr.

111~IS1 Mark on products c~~vrrrd by an Indian

Standard conveys the assurance that they have been l~r~~duc~4 IO comply with 111~

requirements of that sfandard, under a well-defined system of inspection,

tesrin aucl

quality control which is devised and supervised by IS1 and operated by the pro durcr.

IS1 marked products are also continuously checked by IS1 for ronformity to the

standard as a further safeguard. Details of cnnditions under which a licrncr for the

use of the ISI Certification Mark may be granted to manufacturers or processors,

may he obtained from the Indian Standards Institution.

5. SAMPLING

5.1 Representative samples of the material shall be drawn as prescribed in

3

of IS

: ,s-

1950

*

*Methods of test for oil pastes for paints,

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IS : 419 - 967

6. TEST METHODS

6.1 Tests shall be conducted as prescribed in Appendix A and IS : 85-1950*.

References to Appendix A and IS

:

85-1950* are given in 3.3.1 and co1 4 of

Table 1 respectively.

6.2

Quality bf Reagents -

Unless specified otherwise, pure chemicals and

distilled water ( see IS

:

1070-l 96Ot ) shall be employed in the test.

NQTE

Pure chemicals shall mean chemicals that do not contain impurities

which affect the results of analysis.

APPENDIX A

( Clause

3.3.1 )

DETERMINATION OF SETTING TIME

A-O. GENERAL

A-O.1

Outline of the Method

-

The putty applied to a specified thickness

over a metal panel is subjected to pressure test after stipulated period and

layers examined for deformity.

A-l. APPARATUS

A-l.1 Apparatus for Setting Time Test - as shown in Fig. 1.

A-2. PROCEDURE

A-2.1

Apply the material on two clean metal panels of 60

x 60

mm size tc

give a thickness of 5 mm. Allow the putty to dry for

72

hours. At the end 01

this period, superimpose the two panels, so that the putty layers are under

contact and place-on table A. Lower the steel ball

B

and plunger C to the

centre of the metal panels and place a weight of 500 g on top of the plunger

.Maintain the pressure on the plunger for 5 minutes. At the end of the

t

minutes period, separate the panels and examine for deformation.

A-2.1.1 The material shall be deemed to have passed the test if putt

layers do not get deformed under this load.

*Methods of test for oil pastes for paints.

$Specificatioti for water, distilled quality ( revised).

6

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1 :4i9-1967

I

I

I

1

I 1

90

56

All dimensious in millimetres.

Fm. 1 APPARATUS FOR SETTING TIME TEST

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IS : 4i9 - 1967

Subcommittee for Revision of Indian Standards on

Finished Products, CDC 8 : 13

Hel,resenling

Kational Iksl HULIYC, hlcutta

SHNI I. K. ADHIKARI

D E P u T Y DIREUTON

RESEARCH

( GHEivf 1

S&I 0. L. GIJPTA

?iHBI s. s. MAYUUIJ

SHBI M. K. RAO

Indian Pain1 Association, Calcutta

Railway Board ( Ministry of Railways )

Ministry of Defence ( DGI )

Solar Paint & Varnish Mauufacturincr Co.

Calcutta

Indian Paint Association, Calcutta

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BUREAU OF INDIAN STANDARDS

Headquarters:

Manak Bhavan, 9 Bahadur Shah Zafar Marg, NEW DELHI 110002

Telephones: 331 01 31, 331 13 75

Telegrams: Manaksanstha

( Common to all Offices)

Regional Offices: Telephone

Central Manak Bhavan, 9 Bahadur Shah Zafar Marg.

331 01 31

NEW DELHI 110002 331 1375

*Eastern

: l/14 C. I. T. Scheme VII M, V. I. P. Road,

36 24 99

Maniktola, CALCUTTA 700054

Northern : SC0 445-446, Sector 35-C,

CHANDIGARH 160036

I

I

21843

3 1641

r41 24 42

Southern : C. I. T. Campus, MADRAS 600113

twestern

:

Manakalaya. E9 MIDC, Marol, Andheri

(

East ), 6 32 92 95

BOMBAY 400093

Branch Off ices:

*Pushpak. Nurmohamed Shaikh Marg, Khanpur,

I

2 63 48

AHMADABAD 380001

2 63 49

SPeenya Industrial Area 1 st Stage, Bangalore Tumkur Road

38 49 55

BANGALORE 560058

I

38 49 56

Ganaotri Complex, 5th Floor, Bhadbhada Road, T. T. Nagar,

667 16

BIHOPAL 462003

Plot No. 82/83. Lewis Road. BHUBANESHWAR 751002

53j5. Ward No. 29, R.G. Barua Road, 5th Byelane,

GUWAMATI 781003

5 36 27

3 31 77

5-8-56C L. N. Gupta Marg ( Nampally Station Road ),

HYDERABAD 500001

23 1083

R14 Yudhister Marg. C Scheme, JAIPUR 302005

1171418 B Sarvodaya Nagar, KANPUR 208005

Patliputra Industrial Estate, PATNA 800013

T.C. No. 14/1421. Universitv P.O.. Palayam

TRIVANDRUM 695035

(

63471

6 98 32

{

21 68 76

21 82 92

6 23 05

16

21

04

16 21 17

fnspect ion Off ices

With Sale Point ):

Pushpanjali. First Floor, 205-A West High Court Road,

Shankar Nagar Square, NAGPUR 440010

2 51 71

._

Institution of Engineers ( India ) Building, 1332 Shivaji Nagar,

5 24 35

PUNE 411005

*Sales Office in Calcutta is at 5 Chowringhee Approach, P. 0. Printer, 27 68 00

Street. Calcutta 700072

tSales Office in Bombav is at Noveltv Chambers. Grant Road. 89 66 28

Born 400007

fSales Office in Bangalore is at Unity Building, Narasimharaja

Square, 22

36 71

Bangalore 5600@2

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AblENDhIENT NO. 2 SEPTEhIBER 1989

10

IS : 419 - 1967 SPECIFICATION FOR PUTTY, FOR

.

USE ON WINDOW FRAMES

Fi rst Revi si on )

Pqge 4, clause 3.2 ) -

lnsert the following after 3.2:

3.2.1 The calcium c:rrbon;lte content of cxtrncted pigment, from putty,

shall be not less than 80 percent.

Reprography Unit,

BIS, New Delhi, India

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AMENDMENT NO.3 OCTOBER 1992

TO

IS 419 : 1967 SPECIFICATION FOR PUTTY FOR USE

ON WINDOW FRAMES

First Revision)

Page 5, Table 1, SINo. 2, coZ3 ) - Substitute 1.5' for 1.0.

(CHDO20)

ReprographyUnit, BIS, New Delhi. India

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AMENDMENT NO. 4 OCTOBER 1997

TO

IS 419 : 1967 SPECIFICATION FOR PUTTY FOR USE

ON WINDOW FRAMES

First Revision)

Page 4, clause 3.2 ) -

Substitute the following for the existing clause:

3.2 Composition - The material shall consist of mainly whiting and linseed

if necessary, varnish and suitable additives may be added in the formulation

putty. The material shall be mixed in such proportions as to form a paste

with the requirements of this standard.

(

Amendment No. 2, clause 3.2.1 ) -

Insert at the end when tested as per

( Page 4, clnltse 3.3.1, li ne 4 ) - Substitute the words Appendix B for

Appendix A.

Page6, Appendix

A) -Substitute the words

Appendix

Bfor

Appendix

A and renumber the subsequent clauses.

(

Page

6,

clause

6.2 ) - Insert the following appendix after Note under

APPENDIX A

Clause 3.2.1)

OF CALCIUM CARBONATE CONTENT

General - The calcium carbonate content is determined volumetrically,

standard potassium permanganate solution.

Standard Potassium Permanganate Solu tion 0.1 N) - Dissolve 3.2 g

potassium permanganate in 1000 ml of water and allow it to stand for 8 to 14

days.

Siphon off the clear supematant solution into dark-coloured glass

stoppered bottle. Weigh accurately about 3.3 g of sodium oxalate, previously

for a few hours at 100 2 2C and cooled over fused calcium chloride in a

desiccator. Dissolve it in water and make up the solution to exactly 500 ml.

Transfer 25 ml of sodium oxalate solution to a conical flask, add 50 ml of water

and 10 ml of dilute sulphuric acid (1:l by volume). Heat the solution to about

60C and titrate with potassium permanganate solution.

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Amend No. 4 to IS 419 : 1967

Strength of permanganate solution = 0.373 x -+

where

M = mass in g of sodium oxalate in 100 ml of solution, and

V =

volume in ml of potassium permanganate required for titration

against 25 ml of sodium oxalate solution.

A-1.1.2

Bromine Water

A-1.1.3 Ammonium Oxalate Solution -

saturated.

A-1.1.4 Dilute Hydrochloric Acid - Add one volume of concentrated

hydrochloric acid [ see IS 265

:

1993 Hydrochloric acid - Specification

fourth revision ) ] to four volumes of water.

A-l.2 Procedure - Transfer about 0.2 g of accurately weighed whiting, dried

as described in 7 of IS 33 : 1976 Inorganic pigments and extenders for paints

- Methods of sampling and test (

third revision )

to a beaker. Dissolve the

whiting in about 20 ml of dilute hydrochloric acid. Digest for 10 minutes on a

steam bath, dilute to 1.50 ml, filter and wash the residue with water. Add a few

miililitres of bromine water, heat to boiling and make the boiling solution

ammoniacal. Filter off the residue, wash it thoroughly and reduce the filtrate by

evaporation to 200 ml. To the slightly ammoniacal solution, heated to boiling,

add an excess of hot ammonium oxalate solution. Continue boiling till the

precipitate becomes granular. Allow to stand for one hour, filter and wash with

hot water. Pierce the apex of the filter paper with a stirring rod and wash the

precipitate into beaker with hot water. Pour warm dilute sulphuric acid through

the paper and wash it a few times with warm acid. Add about 30 ml of dilute

sulphuric acid, dilute to about 250 ml, heat to 60C and titrate with -standard

potassium pemlanganate solution.

A-l.3 Calculation

Calcium carbonate, percent by mass =

0.500 4 v

M

where

V = volume in ml of 0.1 N potassium permanganate solution used for

titration, and

M = mass in g of the material taken for test.

2

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Anlend No. 4 to IS 419 : 1967

A-l.4

The carbon dioxide content shall also be estimated by a suitable method.

This shall not be less than the equivalent value for calcium carbonate (CaCO3)

content. )

( CHD 020 )

Reprography Unit, BIS, New Delhi, India

3

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AMENDMENT NO 5 MAY 2004

rO

IS 419:1967 SPECIFICATION FOR PUTTY FOR

USE ON WINDOW FRAMES

First Revision

[ P{z~e 5, Table 1 see also Amendment No. 3 ]

Substitute the following

for the existing:

Table 1 Requirements for Putty For Use on Window Frames

Clause 3.4

S1

No.

Characteristic Requirement

Method ofT*

Refto

1

2

3 4

1

Residue on sieve, percent by

5.0 IS 101 Part tJ/Sec 1 : 19891

weight, Mar

ii

Water content, percent by

I .5 1S 101 Patt2/Sec 1 : 19882

weight, Mar

ii]

Keeping properties

Not less than 6

IS 101 Part 6/See 2 : 19893

months

Method of sampling and test for paints, varnishes and related products : Part 8 Tests for

pigments and other solids, Section 1 Residue on sieve third

revkion .

~Method of sampling and test for paints, varnishes and related products : Part 2 Tests on

liquid paints chemical examination , Section 1 Water content

third revision .

3 Method of sampling and test for paints, varnishes and related products : Part 6 Durability

tests on p~int films, Section 2 Keeping properties

third revision .

C HD 20

..

Reprography Unit, BIS, New Delhi, India