•AR32I7D8- · united states environmenta- m'l protection agency v.,..,'« •» v 27 . o region m office of analytical services and quality assurance 201 defense highway suite 20o

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY v.,..,'« •»- M'v 27 . oREGION m

OFFICE OF ANALYTICAL SERVICES AND QUALITY ASSURANCE201 DEFENSE HIGHWAY

SUITE 20OANNAPOLIS, MARYLAND 21401

DATE : November 26, 1996

SUBJECT: Region III Data QA Review/)/?

FROM : Cynthia E. Caporale ( "&£?Region III ESATRPO (3EPfiO)

TO : Chris CorbettRegional Project Manager (3HW22)

Attached is the inorganic data validation report for the KeystoneSanitation Site (Case? 24906) completed by the Region IIIEnvironmental Services Assistance Team (ESAT) contractor under thedirection of Region III BSD. ,

- • : . . ' ' ' %

If you have any questions regarding this review, please call me at(410) 573-2732.

Attachment •

'cc: Russ Sloboda/Haliburton NUS

WA File: 0396004 TDF:1113

•AR32I7D8-Printed on Recycled Pap-.-r

USEPA REGION! III

MIC IE8IONAL ACCEPTANCE/REJECnON/REDUCEO VALUE RECOMMENDATION FORM

l*XTtlul«t NUMBER OF SAMPLES, i* i ««•«•••—.„„„....... ... .............————•"-————-————————— • tOO HAILDATE •

PARTI. DATA ACCEI ANCE OR REJECTION

INSTRUCTIONS, EPA REOZONS MUST ACCEFT OR iCJECT DATA WITHIN M DAYS. IF DATA ARC 8EZN6 REJECTED, THZS FORMMUST BE ACCOMPANIED BY I.I A SIGHED MEMO FROM THE REGIONAL OFFICIAL OESOtZBIMB THE CONTRACTUAL REASONS FORREJECTION. ATTACH ALL RELATED DOCUMENTS <OATA REVIEW,TELEPHONE tOCS, ETC.), t.J ALL KJECTED DATA.

A. FULL DATA ACCEPTANCE OR REJECTIONCHECK ONE OF THE FOLLOWING IF YOU FULLY ACCEPT OR FULLY REJECT ALL SAMPLES IN THIS S06.

* • ACCEPT ALL :;: '•' . REJECT ALL

B. REJECTION OF ALL SAMPLES FOR A PARTICULAR FRACTIONCHECK ONE OF THE FOLLOWING IF YOU FULLY RCJECT ALL SAMPLES IN A PARTICULAR FRACTION D4 THZS SD6.ALL FRACTIONS NOT MARKED AS REJECTED ARE ACCEPTED. ,

REJECT ALL, RTTALa CYAMBg

C. REJECTION AT THE SAMPLE AND FRACTIONAL LEVELCHECK THE FOLLOWING TO REJECT SAMPLES AT THE SAMPLE/FRACTIONAL LEVEL AMD COMPLETE THE REVERSE SIDEOF THZS FORM. •

___ PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE/FRACTION

PART II. REDUCED VALUE. • A. . .

INSTRUCTIONS! REGION RECOMMENDS REDUCED VALUE AND RETAINS THE DATA. FOR A REDUCED VALUE TO BE PROCESSED, THISFORM MUST BE ACCOMPANIED BY A SIGNED NEMO FROM THE RE6ZONAL OFFICIAL CZTZNB THE CONTRACTUAL NON-COHPLZANCE;THE DOLLAR AMOUNT FOR REDUCED VALUEJ AND A WRITTEN JUSTIFICATION (NARRATIVE} OF HOW SAMPLE WORTH WASDETERMINED FOR EACH AFFECTED SAMPLE. ATTACH ALL RELATED DOCUMENTS (DATA REVIEWS, TELEPHONE LOGS, ETC.!

CHECK ONE OF THE FOLLOWING:' ' . • ; ' • ' , . . ' . ' ' • ' • ' ' • • • • , ' ' . ' . - . . ' - . ' .NO REDUCED VALUE B»_» REDUCED VALUE (COMPLETE. REVERSE SIDE) :

IDENTIFY THE SAMPLES/FRACTIONS THAT ARC RECOMMENDED FOR REDUCED VALUE ON THE REVERSE SIDE OF THIS FORM.

••••••••••••••••••••M«WUHHM TKZS FORM CANNOT BE PROCEESSEO WITHOUT A SIGNATURE *••••••*»••••••••••••••«•••• . . . • ' . ' . y - ' . - - ' ' . • I - • . . ' . ; > ' •• • " • • ' ' ' • t i ' " •« NAME OF REGIONAL OFFICIAL, T &l\e VJilolrVC*_____________________________ •

&lfj*r a fj Aj2bi* SIGNATURE! C~\rPj+* a JA S A JefiOCOtV ___________ DATE! 7 * I I 1 tp_____ - •. •

« SEND THIS FORM TOt A BtfH ^ MMM| ^ ^ . •• . • . ' VRHR R R R R R R R R R R R R K ^ • «

«'

AR32I709•••••••••••••••••••••••••••••••••••••••M• SEE LIST OF SAMPLES ON REVERSE SIDE •••••••••••••••••••••••••••••••••••••••••I

I LAB CODE! CHEM . CASE MOli 2490C SDC NO., NCSHOS I

FART III. PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE ;

ENTER AN -X" IN THE BLOCK TO THE RIGHT OF THE "V-FOR THE FRACTION RECOMMENDED FOR REJECTIONENTER A -D" IN THE BLOCK TO THE RIGHT OF THE "Y" FOR THE FRACTION RECOMMENDED FOR REDUCED VALUE.ALL SAMPLES THAT ARE NOT MARKED WITH AN "JT OR A -0" AXE ACCEPTED. '

SAMPLE

LCSS

MCSMIS

HCSM11

HCSH12

HCSM17

HCSM19

HCSH25

HCSM25D

NCSH25S

HCSM26

HCSM28

HCSM3I

HCSH31

MCSM32

HCSM5S

HCSM34

11

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

FlHI

V

V

Y

Y

Y

Y

Y

V

V

Y

Y

Y

Y

Y

Y

V

IACTETAL

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

IONS 4S I

1

1

1

1

1

1

1

1

1

1

1

1

1

;iii

WALYZED 1CYANIDE

Y '

V 1

V 1

r'JY 1

V I

V 1

V 1

Y I

Y 1

Y r.VY I

Y '

Y 1

v 1

v «

1R32I7IO

USEPA REGION! HII • ' ' ' • " . * , ' ' - - '

' INORGANZC REOZONAL ACCEnANtt/REJeCTION/REOUCED VALUE RECOMKENDATZON FORM

.....-.——....._....*................__„_,_„ .

i LAB CODE, CKEM CASE NoT«m""" """""s"*""*;"I On NAME* KEYSTONE SANITATION NUMBER OF SAMPLES, 23 I •««««,..„.„•.....................................................—__m———M- • SOO HAILOATE

PART Z. DATA ACCEPTANCE OR REJECTION '

ZMSTRUCTIONSi EPA REGIONS MUST ACCEPT OR REJECT DATA WZTHZN SI DAYS, IF DATA ARE BEZNO REJECTED, THZS FORMMUST U ACCOMPANIED BY I.I A SIGNED NEMO FROM THi REGIONAL OFFZCIAL OESCRZBZN6 THE CONTRACTUAL, REASONS FORREJECTION. ATTACH ALL RELATED DOCUMENTS (DATA tEVZCWS,TCLEFHONE LOGS, ETC.}, t.) ALL REJECTED DATA.

A. FULL DATA ACCEPTANCE OR REJECTIONCHECK ONE OF THE FOLLOWING IF YOU FULLY ACCEPT OR FULLY REJECT ALL SAMPLES IN THIS SOG.

.£— ACCEPT ALL _____ REJECT ALL

B. REJECTION OF ALL SAMPLES FOR A PARTICULAR FRACTIONCHECK ONE OF THE FOLLOWING IF YOU FULLY REJECT ALL SAMPLES IN A PARTICULAR FRACTION IN THIS SOO.ALL FRACTIONS NOT MARKED AS REJECTED ARE ACCEPTED. /

* ' * . ' i ' • • ** - ' -

REJECT ALL, HfTUA : CYANIM '

C. REJECTION AT THE SAMPLE AND FRACTIONAL LEVEL ACHECK THE FOLLOWING TO REJECT SAMPLES AT THE SAMPLE/FRACTIONAL LEVEL AND COMPLETE THE REVERSE SIDE

;. OF THZS FORM. . ' ..• -.': • '- ;;'• • ' ' • . ' ; . ' • -

___. PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE/FRACTION

PART IX. REDUCED VALUE

INSTRUCTIONS, REGION RECOMMENDS REDUCED VALUE AND RETAINS THE DATA. FOR A REDUCED VALUE TO BE PROCESSED, THZSFORM MUST BE ACCOMPANIED BY A SIGNED NEMO FROM THE REGIONAL OFFICIAL CITING THE CONTRACTUAL NON-COMPLIANCE ITHE DOLLAR AMOUNT FOR REDUCED VALUE} AND A WRITTEN JUSTIFICATION (NARRATIVE) OF HOW SAMPLE WORTH WASDETERMINEDFOR EACH AFFECTED SAMPLE. ATTACH ALL RELATED DOCUMENTS (DATA REVIEWS, TELEPHONE LOGS, ETC.)

CHECK ONE OF THE FOLLOWING!

J NO REDUCED VALUE ;..'.. ': REDUCED VALUE (COMPLETE REVERSE SIDE)

IDENTIFY THE SAMPLES/FRACTIONS THAT ARE RECOMMENDED FOR REDUCED VALUE ON THE REVERSE SIDE OF THIS FORM.

, • ' I : . " ' " ' . ' • ' •

•••••••••••••••••••MHHMMH THZS FORM CANNOT BE FROCEESSEO WITHOUT A SIGNATURE ••••••••••••••••••••••••••••

NAME OF REGIONAL OFFICIAL!

SIGNATURE!

•••••••••••••••••••••••••••••••••••••••IK• SEE LIST OF SAMPLES ON REVERSE SIDE •

I Til

I LAB CODE, CHEM CASE NO. t 24916 S06 NO., HCSM80 |

FART IZZ. PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE

ENTER AM "X* IN THE BLOCK TO THE RIGHT OF THE -Y" FOR THE FRACTION RECOMMENDED FOR REJECTIONENTER A IT IN THE BLOCK TO .THE RIGHT OF THE -Y" FOR THE FRACTION RECOMMENDED FOR REDUCED VALUE;ALL SAMPLES.THAT ARE NOT MARKED WITH AN "X" OR A -0" ARE ACCEPTED.

SAMPLE

LCSW

HCSMII

HCSMI1

MCSMI2

HCSMM

HCSMI5

NOSH!*

MCSHI7

HCSMM

MCSMI9

HCSMII

Hcsms

HCSM14

MCSH15

HCSH1B

MCSM2I

HCSM21

HCSM24

HCSH24D

NCSM24S

MCSH27

MCSM29

HCSH3S

1 FRACTIONS ANALYZED1 METALS 1 CYANIDE

1 Y I 1 1

1 V 1 IV I

IV 1 1 1

1 V I 1 .Y 1

1 V 1 1 Y 1

1 V I 1 1

1 VI 1 1

1 VI 1 . 1

I v I 1 I

1 Y 1 IV I

1 V 1 1 1

1 V 1 1 V 1

1 V 1 1 1

1 Y 1 1 Y 1

IV 1 1 V 1

1 V 1 1 1

IV 1 1 V 1 V

1 V 1 1 Y 1

1 Y 1 1 V 1

1 Y 1 1 V 1

1 V I IV I

1 Y I I VI

1 V | | I

AR32I7I2

USEPA REGION, III

INORGANIC REGIONAL ACCEnANtt/REJECTION/REDUCEO VALUE RECOMMENDATION FORM

..____1________.__.....i__.__.__________ "»«"»•««»•»«•„•'

I LAB CODE, CKEM CASE«... """"~~~~~£ " "I

-• !.!.i.!!!!I.!!?!.... IMPBIOF t"IM>i * '—————————————.-..-————... ....——......... « SDO MAILDATE •

PARTI. DATA ACCEPTANCE OR REJECTION

INSTRUCTIONS, EPA REGIONS MUST ACCEPT OR REJECT DATA WITHIN SI DAYS. IF DATA ARE BEING REJECTED, THZS FORMMUST BE ACCOMPANIED BY I.) A SIGNED NEMO FROM THE REGIONAL OFFICIAL DESCRIBING THE CONTRACTUAL REASONS FORREJECTION. ATTACH ALL RELATED DOCUMENTS (DATA REVIEW, TELE PHONE LOGS, ETC.), C.) ALL 1CJECTEO DATA.

A. FULL DATA ACCEPTANCE OR REJECTIONCHECK ONE OF THE FOLLOWZNO IF YOU FULLY ACCEPT OR FULLY REJECT ALL SAMPLES IN THIS SOG.

_SL_ ACCEPT ALL ____ REJECT ALL ,

B. REJECTION OF ALL SAMPLES FOR A PARTICULAR FRACTIONCHECK ONE OF THE FOLLOWZNO ZF YOU FULLY REJECT ALL SAMPLES ZN A PARTICULAR FRACTION IN THIS SOG.ALL FRACTIONS NOT MARKED AS REJECTED ARC ACCEPTED.

REJECT ALL, METALS •_:.', CtUftOf

C. REJECTION AT THE SAMPLE AND FRACTIONAL LEVELCHECK THE FOLLOWING TO REJECT SAMPLES AT THE SAMPLE/FRACTIONAL LEVEL AND COMPLETE THE REVERSE SIDEOF THZS FORM. ;

___PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE/FRACTION• • " ' . " , ' * ' • ' . ' . " ' ' . -

PART II. REDUCED VALUE

INSTRUCTIONS: REGION RECOMMENDS REDUCED VALUE AND RETAINS THE DATA. FOR A REDUCED VALUE "TO, BE PROCESSED, THISFORM MUST BE ACCOMPANIED BY A SIGNED NEMO FROM THE REGIONAL OFFICIAL CZTZNG THE CONTRACTUAL NON-COMPLIANCE;THE DOLLAR AMOUNT FOR REDUCED VALUE) AND A WRITTEN JUSTIFICATION (NARRATIVE) OF HOW SAMPLE WORTH WASDETERMINED FOR EACH AFFECTED SAMPLE. ATTACH ALL RELATED DOCUMENTS (DATA REVIEWS, TELEPHONE LOGS, ETC.) .

CHECK ONE OF THE FOLLOWING,

. V NO REDUCED VALUE .___ REDUCED VALUE (COMPLETE REVERSE SZDE)

IDENTIFY THE SAMPLES/FRACTIONS THAT ARC RECOMMENDED FOR REDUCED VALUE ON THE REVERSE SZDE OF THIS FORM.

% - ' • - ; **' ' " "

••••••••••••••••••••••••••••M THIS FORM CANNOT BE PROCEESSEO WITHOUT A SIGNATURE ••••••••••••••••••••x»a*»M*N

• NAME OF REGIONAL OFFICIAL!•• SIGNATURE,

••••••••••••••••••••••••••••••••••••••••I• SEE LIST OF SAMPLES ON REVERSE SIDE « ,

A-R3.2 I 7 1

I LAB CODE, CHEM CASE NO;i 24906 SOG NO., HCSM16 I

PART HI. PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE

ENTER AN -X- IN THE BLOCK TO THE RIGHT OF THE *Y" FOR THE FRACTION RECOMMENDED FOR REJECTIONENTER A -0- IN THE BLOCK TO THE RIGHT OF THE *Y" FOR THE FRACTION RECOMMENDED FOR REDUCED VALUE.ALL SAMPLES THAT ARE NOT HARKED WITH AN>X" OR A "D" ARE ACCEPTED.

SAMPLE

LCSW

HCSHU

MCSMUO

MCSHltS

1 FRACT]1 METAL!

1 V 1

1 V 1

1 V 1

1 V I

EONSi 1

1

1

1

1

ANALYZEDCYANIDE

1

v I

v 1V 1

•{J/)R32I7I1»

LOCKHEED M A R T I N /

LOCKHEED MARTIS Region J, 1419 Forest Drive. Suite 104ENVIRONMENTAL SYSTEMS & TECH\OLOOIES Annapolis. Man-land 21403

Telephone <4 10) 268-7705: Fax 1 4 10) 268-8472

DATE! NOVEMBER 2 5 , 1996 • ' • • • _ .

SUBJECTS IKORGANIC DATA VALIDATION (ZK2 LEVEL)SITE: KEYSTONE SANITATION CASE 24906SDGS MCSMOO, MCSM03, MCSM16

' '.PROMl BAR! PRASADVV? MAHBOOBEH HECANIC __

DATA REVIEWER SENIOR OVERSIGHT CHEMIST

TOt CYNTHIA E. CAPORALEESAT REGIONAL PROJECT OFFICER,

THROUGH! DALE S. BOSHARTESAT TEAM MANAGER

•( j Case 24906 consisted of a total of thirty-four (34)x~— . samples in three Sample Delivery Groups (SDGs) analyzed

for metals and cyanide (CN) by the Chemtech ConsultingGroup (CHEM) . The samples were analyzed according to theContract Laboratory Program (CLP) Statement of Work (SOW)

. . ILH04.0, through the Routine Analytical Services (RAS)program. The specifics about the samples in this caseare listed below. ,SDG Matrix .- Sample (s)

HCSMOO Aqueous (unfiltered) 12

Aqueous (filtered) 8

HCSM03 ;4oli 13

MCSM16 Aqueous (unfiltered) 1

The sample set included one (1) each of the following:rinsate blank, unfiltered field blank, filtered fieldblank, unfiltered field duplicate pair, soil fieldduplicate; pair.

. . . - ' . ' , . ' i ' . . - ' ' • . - . ' • • ; 'SUMMARY

All analytes were successfully analyzed in all samples.. The. samples vere analyzed by the laboratory and validated

AR321715

Page 2 of 5

by the reviewer on an SDG basis. The results for therinsate blank were used for qualifying all samples*Areas of concern with respect to data usability arelisted below.MINOR ISSUES .

The continuing calibration (CCB), rinsata (RB) and field(FB) blanks had reported results greater than theInstrument Detection Limits. (IDLs) for the analyteslisted below. The reported results for these analytes inthe affected samples which are less than five times(< 5x) the blank concentrations may be biased high andhave been qualified "B".SDG Blank Type Analyta(3>MCSMOO CCB Magnesium (Mg)

RB Manganese (Mn), Zinc (Zn)FB (filtered) Mn, Zn

MCSM16 RB 2n

The percent difference (% D) for the ICP serial dilution ânalysis was outsida the control limit for the potassium(K) analyte in SDG MCSMO?. ' The'reported results for thisanalyte in the affected samples are estimated and havebeen qualified "Jn *

The initial and final Contract Required Detection Limit(CRDL) standard recoveries were mixed for the arsenic(As) and thallium (Td) analytes in SDG MCSMOO. Thequantitation limits for these analytes are estimated dueto opposing bias effects and have been qualified "UJW.The CRDL standard recovery was high for the chromium (Cr)analyte in SDG MCSMOO. The continuing calibration blankfor this analyte had a negative result with an absolutevalue > IDL. The reported results for the Cr analyte insamples MCSM20 and MCSM29, which are < 2x .CRDL and < 2xthe absolute value of the blank, ara estimated due toopposing bias effects and have been qualified "J".

The CRDL standard recovery was low for the As analyte inSDG MCSMOO. The quantitation limits for this analyte inthe affected samples may be biased low and have beenqualified "UL11.

The CRDL standard recoveries were high for the analytes j.listed below. The reported results for these analytas in "—-

AR32I7I6

. . - ' . : . Pages of 5the affected samples which are < 2x CRDL may be biasedhigh and have been qualified "Kn, unless superseded bythe "B«! qualifier.SDG Analytes

MCSMOO Cobalt (Co), Copper (Cu) ,, Lead (Pb) , Hn,Nickel (Ni), Zn

HCSM03 As, Cadmium (Cd) , Selenium (Se)

MCSM16 Co, Ni^

The preparation and continuing calibration blanks inSDG MCSMOO had negative results with absolute values> IDL for the analytes listed below. The reportedresults for these analytes in the affected samples,which are < 2x absolute value of the blank, and thequantitation limits may be biased low and have beenqualified "L" and "UL'Y respectively, unlesssuperseded by the "B" qualifier.

Blank Type Analvtes '

PB Aluminum (Al) , Calcium (Ca) , Cu,Iron (Fe) , Magnesium (Mg) , K,Sodium (Na) ,

NOTES ' '.';'•'. •'•;". .• • • . _• _ ' • . ••The As, Pb, Se and Tl analytes were analyzed using theICP method and had IDLs less than the CRDLs.

The sample shipment, designated for the CN analysis ofunfiltered sample MCSM01, was not received by the .laboratory. Hence, the CN analysis for sample MCSM01was not performed by the laboratory. See phone logby the laboratory dated 8/1/96 in Appendix B.The laboratory incorrectly reported on Form 2B ofSDG MCSMOO that tihe CRDL standard recovery for themercury (Hg) analyte was 0.0% instead of 99.0%. Thisdiscrepancy has been rectified during the validation.

The field duplicate results were outside the controllimits (20% RPD, ± CRDL) for several analytes in theaqueous sample pair MCSM27/MCSM29. The field duplicateresults were within the control limits (35% RPD,± 2x CRDL) for all analytes, except Zn, in the soilsample pair MCSM26/MCSM28. The concentrations for the

AR32I7I7

. Page 4 of 5outliers and their precision* estimates are reported inTable 4.The filtered aqueous sample MCSM08 had several analytesdetected at concentrations greater than those in itsunfiltered aliquot (sample MCSM02). The filtered aqueoussample MCSM20 had the Pb analyte detected at aconcentration greater than the CRDL while the Pb analytewas not detected in its unfiltered aliquot (sampleMCSM18). The concentrations for the outliers and theirprecision estimates are reported in Table 5. (Theprecision criteria for the laboratory duplicates havebeen applied to the field duplicates also.)Soil sample concentrations are calculated on the basis ofthe raw data values (in 0g/L), the gram weight of sampleused, the volume of the digestate/distillate, and the %solids according to the following equation:

mg/Kg = (raw value. uo/L)fdiaeatata volume. LV(weight,g)(% solids/100)

To obtain the quantitation limit, insert the IDL (Form X)for the raw value; refer to Forms XIII to obtain eachsample preparation weight and volume used. The •quantitation limits thus obtained are specific for eachsample and preparation method.The data were reviewed in accordance with the NationalFunctional Guidelines for Evaluating Inorganic Analyses,with modifications for use within Region III.

INFORMATION REGARDING REPORT CONTENT

Table 1A is a summary of qualifiers added to the results from thelaboratory during validation.ATTACHHBNTa

TABLE 1A SUMMARY OF QUALIFIERS ON DATA SUMMARY FORMAFTER DATA VALIDATION

TABLE IB CODES USED IN COMMENTS COLUMN

TABLE 2 GLOSSARY OF DATA QUALIFIER CODES

TABLE 3 DATA SUMMARY FO RMS < '

TABLE 4 SUMMARY OF FIELD DUPLICATE OUTLIERS

TABLE 5 SUMMARY OF UNFILTERED/FILTERED OUTLIERS

AR32I7I8

.11 nil .11 ...j I.

. . ' . . ' Page 5 of 5•' - ' ' V; *. . • - . - ; • •

ATTACHMENTS fContd.i ,

APPENDIX A RESULTS REPORTED BY LABORATORY FORM Is

APPENDIX B SUPPORT DOCUMENTATION

DCN: HP9611KEY.NAR

AR32I7I9

• ' . - • • • Page 1 of 3/

TABLE 1ASUMMARY OF QUALIFIERS ON DATA SUMMARY ,

FORM AFTER DATA VALIDATION

• ' . . ' - - . . ' ' ' . - . • ' ' NON- ' . • - . - . • ' „POSITIVE DETECTED

ANALYTB 8EK3 SAMPLES AFFECTED* VALUES VALUES BIAS COMMENTS*

Al MCSMOO 07,10,13-15,18,20, L UL Low PBN(-65.630g/L)21,24,27,35

As MCSMOO 14,20,21,27,29,35 UJ Low/ CRM(88.5%, .High 142.8%) •

00-02,04-07,09,10, UL Low CRL(83.5%) ,13,15,13

MCSM03 03,31,34 K High CRH( 123%) . . _ • • '

25 K High CRH(123%,117.8%) '

Cd MCSM03 03,11,12,19,33,34 K High CRH(111%).

Ca MCSMOO 13,15,21 L UL LoW

Cr MCSMOO 20,29 J High/ CBM(110.9%, .Low -1.2jug/L)

14,21,27,35 , UL, LOW CCN(-1.2/ig/L) '

Co MCSMOO 08 K High CRH(115.3%,' : 116.8%)

29,35 K High CRH(115.3%)

MCSM16 16 K High CRH(116.8%,' 111.9%)

Cu MCSMOO 00-02,04-07,09',10, K High CRH(117.1%,18 .. 115.8%)

08 K High CRH(121%,125.5%)

20,29 K High CRH(115.8%,•-.••••- :. '. ' ' ' ' / ..-121%)

13-15,21,24,27,35 UL Low PBN(-i.61jig/L) •

-«• All samples begin with the prefix "MCSM".* See explanation of Comments on table IB.

flR32l720

/ Y - • ' ' '- . ' - ".- :; • , ••'. ' "' , . ' • '• Page 2 of 3 ••^ TABLE 1A

SUMMARY OF QUALIFIERS ON DATA SUMMARYFORM AFTER DATA VALIDATION

' . ' ' • . ' • • • ' : • • • . . ' • : : • . ' - " • ; NON- .• .POSITIVE DETECTED

ANALYTB SDQ SAMPLES AFFECTED* VALUES VALUES BIAS COMMENTS*

Fe MCSMOO 06,10,13-15,21,27 L UL Low PBN(-53.78/jg/L)

Pb MCSMOO 01,02 K High CRH(126.8%,

08 K High CRH(130.7%) .

20,29 K High CRH(117.S%)

Mg MCSMOO 14 B . High CCB(20.8Mg/L) ', PBN(-66.64pg/L)

13,15,21 UL Low PBN(-66.64/ig/L)* ' " - • . • - . ' » • ' ' , , .

Mn MCSMOO 01,18 B High RB(2.10g/L)-CRH(114.9%)

05-07 B High FB(2.8/*g/L) ,CRH(114.9%)

00,02,04,10,15 K High CRH(114.9%)

14,20 K High CRH(113.1%).. ' ' ' , • • . . • ' ' . • ' . • - , '

,24 K High CRH(113.1%,* 115%)

Ni MCSMOO 02704,05,10 K High CRH( 114.6% )•' : ' • • ' • : - ' . . . ' • . ' - • I

29,35 K High CRH(114.7%) v-

MCSM16 16 K High CRH(117.5%,112.2%)

K MCSMOO 13-15,21 OL Low PBN(-79.44/ig/L)

MCSM03 All samples J . SD(17.2%) .

Se MCSM03 28 K High CRH(117.2%,. . , . : . ; - t . • • : • • > . . 135%) , • • • • • • • .

-H AH samples begin with the prefix "MCSM".* See explanation of Comments on Table IB. .

flR32!72l

Page 3 of 3 , iTABLB 1A

SUMMARY OF QUALIFIERS ON DATA SUMMARYFORM AFTER DATA VALIDATION

.•• ' • ' • ' •••-.- NON-. •' • •'• ' . -POSITIVE DETECTED

ANALYTB 3DQ SAMPLES Ag?ECTED+ VALUES VALUES BIAS COMMENTS*

Na MCSMOO 13,15,21 UL Low PBN(-74.66/ig/L) '

Tl MCSMOO 00-02,04-07,09,10, UJ High/ CRM(123.2%, -13,15,18 Low 75.4%)

14,20,21,27,29,35 UJ Low/ CRM(75.4%,High 147.4%)

Zn MCSMOO 00-02,04-07,09,10, B High RB(24.2pg/L)18 - CRH(115.4%)

20,27,29,35 B High RB(24.2pg/L)".-i CRH(112%)

• • , ' • • - . ' /

* 08 B High RB(24.2 g/L) .

1 4 , . • K High CRH(112%) • i J .

15 K High CRH(115.4%) •

MCSM16 16 B. High RB(24.2Mg/L)CRH(116.4%143.5%)

• ' I • ' • ' ' ' . • ' .

+ All samples begin with tha prefix "MCSM*1.* See explanation of Comments on Table IB.

AR32I722

' ' - . - ' . ; TABLE IB '.'.'• ' ..

CODES USED IN COMMENTS COLUMN

PBN . = The preparation blank had a negative result with absolutevalue > IDL (the blank result is in parenthesis). Thereported results which are < 2x the absolute value of theblank and the quantitation limits may be biased low.

CRN = The initial and final CRDL standard recoveries were mixed(> 110% or < 90%) [% recoveries are in parenthesis]. Thequantitation limits are estimated.

, . , . ' .,! * -.. ..... ^ , • - ^

CRL •* .The CRDL standard recovery .was low .(% recovery is inparenthesis). The quantitation limits may be biased low.

CRH « The CRDL standard recovery was high (% recovery is inparenthesis). The reported results which are < 2x CRDL maybe biased high. v

CBM «= The CRDL standard recovery was high and CCB had negativeresult with absolute value > IDL (recovery and blank valuesare in parenthesis)* The reported results, which are < 2x

' CRDL and < 2x absolute value of the blank, are estimated.CCN = The CCB had a negative result with absolute value > IDL

(the blank result is in parenthesis). The quantitationlimits may be biased low.

CCB •«= The continuing calibration blank had a result > IDL (theresult is in parenthesis). The reported results which are

: < 5x the blank concentration may be biased high.RB «= The rinsate blank had a result > IDL (the result is in

parenthesis). The reported results which are < 5x theblank concentration may be biased high.

FB «* The field blank had a result > IDL (the result is inparenthesis). The reported results which are < 5x theblank concentration may be biased high. .

SD «= The ICP serial dilution results were outside the controllimit (10% D) (% D is in parenthesis]. The reportedresults are estimated.

/5R32I723

' • ; • • . ' . . - ' -TABLE 2 • . ' • , - . - . ' • • ' i

' GLOSSARY 07 DATA QUALIFIER CODES (INORGANIC)

CODES RELATED TO IDENTIFICATION(confidence concerning presence or absence of analytes):

U = Not detected. The associated number indicatesapproximate sample concentration necessary to bedetected.

(NO CODE) =» confirmed identification.

B •> Not detected substantially above the level reportedin laboratory or field blanks.

' '. - , • .. . ' /

R =» Unusable result. Analyte may or may not be presentin the sample. Supporting data necessary toconfirm result.

CODES RELATED TO QUANTITATION(can be used for both positive results and sample quantitationl i m i t s ) : . . ' . ' '

J » Analyte Present. Reported value may not beaccurate or precise.

K 3 Analyte present. Reported valua may be biased v^Xhigh. Actual value is expected to be lower.

L =• Analyte present. Reported value may be biased low., Actual value is expected to be higher.

[] = Analyte present. As values approach the IDL thequantitation may not be accurate.

UJ = Not detected, quantitation limit may ba inaccurateor imprecise.

UL « Not detected, quantitation limit is probablyhigher. . ;

CODES

Q a No analytical result.

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( • ' ' ' ': - ' '. : , ' • ' ••,'•••'•,;• TABLE 4 '!' \'\ '. ' •

SUMMARY OP FIELD DUPLICATE OUTLIERS

SDG MCSMOO

Analvte HCSM27 MCSM29 Difference

Al ND 940 , 940

Fe 39.3 2260 2220.7

Pb ND 3.2 3.2

Mn 93.4 179 62. 8+

.'•/ SDG MCSM03

Analvte MCSM26 MCSM28 Rpp

Zn 213 83.8 87.1

ND B Not detected.+ «= RPD instead of difference.

ft'R 321-731

TABLB 5 ' .

SUMMARY OF UNPILTERED/ FILTERED OUTLIERS

Analvta HCSM02 MCSM03 Diffarenea

Al 177 553. 376

Cr 1,6 258 256.4

Fe 425 1330 905

Mn 19.2 39.2 20.0

Hi 11^0 193 182

Zn 22.8 49.1 -•- 26.3

Analvta MCSH18 MCSM2Q Diffarenea

Pb ND 3.1 3.1

ND. « Not detected.+ a RPD instead of difference.

AR32I732

APPENDIX A

RESULTS REPORTED BY LABORATORY

i J , ' ' \ ' • • / -' . . \v'.;>; FORM IS - -

BR32I733

8DO MCSMOO

i!R32l73lt

U.S. EPA - CLP •. . " " ' ' ' . ' ' ' • • ' ' l

EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET " '

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166MCSMOO

Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSMOO

Matrix (soil/water): WATER Lab Sample ID: 8739S

Level (low/med): LOW ; Date Received: 08/01/96

% Solids: 0.0 • ;.

Concentration Units (ug/L or mg/Kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39^37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron ,LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide ,• . f >

Concent rat ion

5759.0 ,9.0

22.81.0 '1.0

36200' 19.3

1.012.0

10303.0

289012.30.20

: 3.03120

' 5.02.0

231009.01.0

25.69.0

C

UUBUU

UB

UBBUUBUU

UU

U

Q

_

'.'

;

M

PPPPPPPPPPPPPPCVPPPPPPPPCA

Color Before:-BROWN Clarity Before: CLEAR Texture:

Color After: CLOUDY Clarity After: CLEAR Artifacts:

Comments: • ' ' " .

FORM I - IN 003 ILM04.0

AR32 I 735

U.S. EPA .- CLP ', .- 1- ' ... '. . ' ' .

• EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET ' •

Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166MCSM01

Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSMOO

Matrix (soil/water): WATER Lab Sample ID: 87473 .

Level (low/med): LOW . Date Received: 03/01/96* . - / - ' -

% Solids: 0.0 ' . .


CAS No.

7429-90-57440-36-07440-33-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration•

13909.09.016.11.01.0

331002.01.015.5139

• 4.62230

7.20.203.0

21905.02.0

10600 .9.01.017.1

C

UUBUU

au3

BBUUBUU

UUB

Q H

PPPPPPPPPPPPPPCVPPPPPPPPNR

Color Before: 'BROWN .( Clarity Before: CLEAR Texture:


Comments: .

FORM I - IN Minji ILM04.0004

AR32I736

U;S. EPA - CLP/;r •" 1- / . '

'' EPA SAMPLE NO.INORGANIC -ANALYSIS DATA SHEET

MCSM02Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No.i 24906 SAS No. : SDG No. :.MCSMOO


Level (low/med): LOW • Date Received: 08/01/96

% Solidst 0.0


CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-26-07440-62-27440-66-6

. ;

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmium /CalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium'ThalliumVanadiumZincCyanide

Concent rat ion

1779.09.016.4.1.0,1.0

326001..61,026:44253.3

236019.20.20

. 11,01640

5.0, • 2.0

71909.01.022.89.0

C

BUUBUU

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UU

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PPPPPPPPPPPPPPcvPPPPPPPPCA

Color Before: BROWN Clarity Before: CLEAR Texture:

Color After: CLOUDY • Clarity After: CLEAR Artifacts:

Comments: • v

FORM I - IN A-* ILM04.0005AR32I737

U.S.. EPA - CLP• r . ' ' - v • . •• ' •" * . •

EPA SAMPLEINORGANIC ANALYSIS DATA SHEET ..


Lab Code: CHEM Case No. : 24906 SAS No.: ., SDG No.: MCSMOO


Level (low/med): LOW Date Received: 08/01/96

% Solids: 0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43^97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-23-07440-62-27440-66-6

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc'Cyanide .

Concentration

2539.09.026.3

- . 1.01.0

256005.21.017.16523.0

452019.30.20'3.4

37305.02.0

100009.01.018.09.0

C

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Color Before: -BROWN

Color After : CLOUDY

Comments : . ' '

Clarity Before : CLEAR Texture :

Clarity After: CLEAR Artifacts:

- \ • • . ' . .

• • /' • . • . "• • • " • - - . « • .

' - • • . - • . • • . . • . • • . . - - • • ; . . . i

FORM I - IN ILMO.4.0OOG

AR32I738

U.S. EPA - CLP";..v. . •!•-• •. ': '• " . .. • /

- '"'. . • ' - ' -:i'' 'i '. " - - '

* " EPA SAMPLE NO.

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

INORGANIC ANALYSIS DATA SHEET • _____^___

MCSM09

Lab Code: CHEM Case No. :-24906 SAS No. : SDG No.: MCSMOO

Matrix (soil/water): WATER Lab Sample ID: 8740S .

Level (low/med):' LOW , Date Received: 08/01/96

% Solids: , 0.0


CAS No.

7429-90-57440-36-07440-36-27440-39-37440*41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmium -Calcium ;ChromiumCobaltCopper 'Iron, •.;••LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

3849.0

. 9.015.0•1.01.0

344001.71.0

13.44503.0

227041.20.203.0

2740• , 5.0

2.06050

."•.. 9.01.0

16.39.0

C

UUBUU

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UB

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UU•BU

Q M

P .PPPPPPPPPPPPPCVPPPPPPPPCA

Color Before: COLORLESS Clarity Before: CLEAR texture:

Color After': . CLOUDY - Clarity After: CLEAR Artifacts:'' _ • ' , * • : • ' • ' " ' • • • *

Comments: - ' ?•,

FORM I -. IN ILM04.0Oil

(5R32I739

U.S. EPA T CLP: ! . • . . _ . . . -' . 'V.'

EPA SAMPLEINORGANIC ANALYSIS DATA SHEET


Lab Code: CHEM Case No.: 24906 SAS No. : SDG No.: MCSMOO

Matrix {soil/water): WATER - Lab Sample ID: 3743S

Level (low/med) : LOW . Date Received; 08/01/96

* Solids: 0.0 - ' • '


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-4 '7440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

11.09.09.0

, . 1.01.0

. l.-Oi10.01.01 . 01.027.03.011.01.00.203.039.05.02.013.0

. < 9.01.02.09.0

C

Uuuuuuuuuuuuuuuuuuuuuuuu

Q M


Color Before:'BROWN Clarity Before: CLEAR • Texture:

Color After: COLORLESS Clarity After: CLEAR Artifacts:

Comments: ' . .FIELD QC SAMPLE

FORM I - IN ' ILM04.0013

U.S. EPA - CLP"-'-'.'"'.v ' ' ' ' i - ' ' ' • ' ,•

t .,".'" . : • > • ? ' •' . •.' • '

EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET .. . .


Lab Code.: CHEM Case No. : 24906 SAS No.: SDG No. : MCSMOO• ' • . . ' ' " . . . , . ' ""- . ' *


Level (low/med): LOW ; Date Received: 08/01/96

% Solids: 0.0

Concentration Units.(ug/L or mg/Kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-9S-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6 ,

•• •

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmium 'CalciumChromiumCobaltCopperIronLead 'MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concent rat ion

11.09.09.01.01.01.0

20.71.01.01.0

• 27.03.0

•11. 02.10.203.039.05.02.018.09.01.024.29.0

C

UuuuuuBUUUUUuBUUUUUUUuu

Q M

PPPPPPPPPPPPP.PcvPPPPPPPPCA

Color Before: -COLORLESS Clarity Before: CLEAR Texture:


Comments: .FIELD,QC SAMPLE .


015

,U.S... EPA - CLP

EPA SAMPLE N'INORGANIC ANALYSIS DATA SHEET ___ \


Lab Code: CHEM Case No. : 24906 SAS No. : SDG No. : MCSMOO

Matrix (soil/water): WATER ' Lab Sample ID: 8745S


% Solids: 0.0


CAS No.

7429-90-57440-36-07440-33-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

-

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinccyanide

Concentration

1269.09.011.71.01.0

244001.31.0

-' 13.42233.0

20703.10.203 . 0

2360; 5.0

2.07670

9.01.0

' 11.39.0

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Comments: ' , .

FORM I. - IN ILM04.0

016,rtR32l7l>2

U.S. EPA - CLP•.-''•'• 1 - , . -. . ' ' _ '

V' ' •' ' -• - , " " . . . '. ,V :v • ! ' ' ' " • ' -

EPA SAMPLE NO,INORGANIC ANALYSIS DATA SHEET

MCSM21Lab Name: CHEMTECH CONSULTING,GROUP Contract: 68-D5-0166



Level (low/med): LOW , Date Received: 08/09/96, • - * '

% Solids: 0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

' •'

AnalyteAluminumAntimonyArsenicBarium •BerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

11.09.0

- 9.01.0.1.01.010.01.01.01.0

27.03.0

11.01.00.203.0

39.0•" • 5.0

2.018.09.01.02.09.0

C

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Color After: COLORLESS

Comments :

: Clarity Before: CLEAR Texture:


'• i • .' • ~

. . • ' . - . - • . • • • «/ . . - . . -•- •; -'•••• • • ' • -

FORM I - IN ' nift ILM04.0

• A R 32 I 71* 3

U.S. EPA - CLP '. • , 1 . . . - . ' • '

EPA SAMPLE N(INORGANIC ANALYSIS DATA SHEET


Lab Co.de: CHEM Case NO.: 24906 -"SASNO.: SQG No. : MCSMOO


Level (low/med): LOW ' Date Received: 08/09/96

% Solids: 0.0


CAS No.

7429-90-57440-36-07440-33-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

30.49.0

- 9.010.21.01.0

123001.01.01.0

1533.0

348026.40.203.0

23105.0

, 2.02180

9.01.02.09.0

C

1UU3UU

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Color Before: COLORLESS Clarity Before: CLEAR Texture:

Color After: COLORLESS Clarity After: CLEAR Art if a*cts :>

Comments:

FORM I - IN . ILM04.0019

U.S. EPA- - CLP. . . , - . . 1 . • • ' ' • .

EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET




Level (low/med): LOW . ; Date Received: 08/09/96

\ Solids: 0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

;

Analyte


Concentration

11.0, • 9.0

9.0; 74.0. 1.0

1.018400

1.01.01.0

39.33.0

1190093.40.203.0

70005.02.0

93809.0; i.o6.19.0

C

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Color Before: COLORLESS Clarity Before: CLEAR Texture:


Comments: • ••. ; <

FORM I - IN ILM04.0020

A R 321?;!* 5-

U.S. EPA - CLP1 ' ' '



Lab Code: CHEM Case NO.: 24906 SAS No.: SDG No. : MCSMOO

Matrix (soil/water) : WATER , Lab Sample ID: 90043

Level (low/med): LOW Date Received: 03/09/96• * •

% Solids: 0 . 0 - . ' . , .

. Concentration Units (ug/L or mg/Kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-23-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLead .MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9409.09.0

93.41.01.0

231002.31.8

13.72260

3.214800179

0.20• • 6 . 8

83005.02.0

119009.01.0

23.8. 9.0

C

UU3UU

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Color Before: COLORLESS Clarity Before: CLEAR - Texture:

Color After: COLORLESS Clarity After: CLEAR • Artifacts:

Comments: '


iVR32l7t»6

U.S. EPA - CLP• : • : " • ' • ' 1





Level {low/med): LOW Date Received: 08/01/96

% Solids: 0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95 47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium -ThalliumVanadiumZincCyanide

Concent rat ion

1679.09.014.91.01.0

237005.31.07.4

1673.0

42308.10.20

. 9.13700

5.0• . 2.0

97309.01.0

34.7

C

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Color Before: .BROWN Clarity Before: CLEAR Texture:

Color After: CLOUDY .Clarity After: CLEAR Artifacts:. • - . ' , . - - ' ' - ' s

Comments:• ' • . -

FORM I - IN , j*nn ILM04.011137

A R 32 I 71* 7

U.S. EPA - CLP '• 1



Lab Code: CHEM Case No.: 24906 SAS No.: SDG No,: MCSMOO, ' • - . • • " • '

Matrix (soil/water): WATER •• . . Lab Sample ID: 8746S


% Solids: 0.0


CAS NO.

7429-90-57440-36-07440-33-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-3,7439-89-67439-92-17439-95-47439-96-57439-97-67440-02-0 '7440-09-77732-49-27440-22-47440-23-57440-28-07440-62-27440-65-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopper ,IronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium .VanadiumZincCyanide

Concentration

1499.09.018.91.0 '1.0

311002.71.0

. ' 3. 9 :. 73.5

3.02460

4.50.203.0

28005.02.0

205009.01.025.4

. . . •

C

3UUBUU

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Comments: - •

FORM I - IN ILM04.0008 v

U.S. EPA - CLP•' :. ...." 'I ' - • .. - ' . '• '

'EPA SAMPLE NO.INORGANIC ANALYSIS DATA . SHEET


Lab Code: CHEM Case No.: ,24906 SAS.No.: SDG No.: MCSMOO


Level (low/med): LOW I Date Received: 08/01/96

% Solids: 0.0 : -•.' ' • , ' • '''.' " ' " '' *


CAS No.

74 29 -SO -57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenic ,,BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMerCuryNickel .••••PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1239.0

• 9.013.81.01.0

.291001.0

: i, o11.81693.0

19204.70.203.0

20605.0

W 2.09800

• ' . ' , - 9 . 01.0

12.2

C

BUUBUU

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Color Before: BROWN

Color After: CLOUDY

Comments i . ' , . . . ' • .

; Clarity Before: CLEAR . Texture:

Clarity After: CLEAR ... Artifacts:

r . • - - • • - • ' • • - . , .

• • • ' •FORM I - IN An**' ILM04 . 0"09

AR32I7V9

U.S. EPA - CLP, ., ' 1 - _ .- .

: • . , EPA SAMPLEINORGANIC ANALYSIS DATA SHEET •'


Lab Code: CHEM Case No.: 24906 SAS No. : SDG No. : MCSMOO

Matrix (soil/water): WATER Lab Sample-ID: 8751S

Level (low/med): LOW , Date Received: 08/01/96

% Solids: 0.0

Concentration Units (ug/L;or mg/Kg dry weight): UG/Lf-

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-43-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

5539.09.018.51.01.0

31600 •2534.5

21.31330

4.42390

39.2. 0.20

193'1370

• 5.02.0

81009.01.0

-49.11

C

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Color Before: 'COLORLESS

Color After: COLORLESS-

Comments:

Clarity Before: CLEAR Texture:

Clarity After: CLEAR . Artifacts:

- • • • • • - ' « . - • .• • • • -

FORM I - IN _ ILM04.0010

4R32I750

U.S. EPA - CLP... : i

' ' * ' - ' • EPA SAMPLE NO./ . INORGANIC ANALYSIS DATA SHEET



Matrix (soil/water): WATER * Lab Sample ID: 8749S


% Solids: 0.0 ,


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

' 1279.09.011. L1.01.0

296006.1

- 1.09.973.43.0

188020.90.205.0

2480•' 5.0

2.05550

9.01.0

: 10.4

C

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Comments: -

FORM I - IN *? ' ' • ILM04.0

VR 32 I 75 I

U.S. EPA - CLP'1 ' ' '

• ; EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET '


Lab Code: CHEM Case No.: 24906 SAS No. : .; SDG No.: MCSMOO1 • ' '. . ' •

• ' - "

Matrix (soil/water): WATER Lab Sample ID: 8752S• r ' •


* Solids: 0.0 '

Concentration Units (ug/L or mg/Kg dry weight): UG/L ,

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-8 -7439-39-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77732-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

V

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel 'PotassiumSeleniumSilverSodiumThalliumVanadiumZiricCyanide

Concentration

11.09.29.01.01.01.0

3151.01.0

. ' 1.027.03.022.42.80.20

. 3.039*05.0

. 2.04939.0

"1.0.2.3

C

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Color Before: "COLORLESS Clarity Before: CLEAR Texture:


Comments: " . .FIELD QC SAMPLE

FORM I .- IN ILM04.0

0144R32I752

tf.S. EPA - CLP .•"•'••.• ; * ' • '•• - • •' '.

. - ' . ' ' " ' " - " • " * . • • '

' • EPA SAMPLE NO.'INORGANIC ANALYSIS DATASHEETo -. •• ..:..:


Lab Code: CHEM. Case No. : 24906 SAS No. : SDG No.:, MCSMOO" • • i ' . ' ' " . , - " " . • " ' •


Level (low/med): • LOW . Date Received: 08/01/96

t JSolids: 0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70 -27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28 07440-62-27440-66-6

Analyte /

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel ;.PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

84.89.09.0

• 12.41.01.0

222001.71.08.9

1283 . 1

2070 .15.50.203.0

2450•' ' 5.0

2.07990

9.01.08.1

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Color After: COLORLESS v Clarity After: CLEAR Artifacts:

Comments:

FORM I - IN ILM04.0

017AR32I753

• N ' U.S. EPA - CLP' . . 1 • ' • , . - • ' • . . . ' s

EPA SAMPLE NO ~• , INORGANIC ANALYSIS DATASHEET , ..'''________' )

I M C S M 3 5

Lab Code: CHEM Case No.: 24906 SAS No. : SDG No.: MCSMOO

Matrix (soil/water): WATER , Lab Sample ID: 9006S


% Solids: 0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-37439-39-67439-92-17439-95-47439-96r57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCoppeÎronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

11.09.09.0

60.31.01.0

5130I'.O1.21.0

4233 . 0

44102470.203.3

7545.02.0

59009.0l.'O

!'. 14 . 2

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Clarity Before: CLEAR Texture: .


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FORM I - IN ftnrt ILM04.0022

AR32l75l»-

' ••

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•IR 3217 55

U.S. EPA - CLP.'"•••• : i - ' '

- v '^ EPA SAMPLE NO.U ..-_•• INORGANIC ANALYSIS DATA SHEET''• ' -' . ' > '• .•'.•••••.• - , • • •' ~


Lab Code: CHEM Case No. : 24906 SAS No. : SDG No. : MCSM03

Matrix (soil/water): SOIL ' Lab Sample ID: 8991S

Level (Idw/medK: LOW Date Received: 08/09/96i • • ' ' ' . ' • ' • • ' . - • ' . ' ' ' - / - • •

* Solids: 52.2

Concentration Units (ug/L or mg/Kg dry weight): MG/KG

CAS No.

7429-9a-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-67439-89-67439-92-17439-95-47439-96-57439-97-r67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilver-SodiumThalliumVanadiumZincCyanide

Concentration21800

3.39.4

1060.650.48

194016720.229.6

3960054.9

3030936

0.1926.2801

f 1.80.74

157.3.3

25.7187 :

0.85

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Color Before:.BROWN. Clarity Before: , ; Texture: MEDIUM

Color After: YELLOW Clarity. After: Artifacts:

Comments: - '

FORM I - IN ILM04.0

AR32I756

U.S. EPA - CLP• . " 1 • • •• - '

EPA SAMPLEINORGANIC ANALYSIS DATA SHEET .


Lab Code: CHEM ' Case No. : 24906 SAS No. : SDG No. : MCSM03

Matrix (soil/water): SOIL Lab Sample ID: 89903

Level (low/med): LOW Date Received: 08/09/96% Solids: 66.8 ' ..

Concentration Units (ug/L or mg/Kg dry weight): MG/Kd

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-43-47440-5a-87439-39-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09*77732-49-27440-22-47440-23-57440-28-0,7440-62-27440-66-6

Analyte


Concentration20400

2.66,0

1580.650.29

130032.119.721.6

2320014.3

• 21604190.1522.4947

v 1.40.53

168, -. ' 2.6

22.335.9'0.65

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Comments: . " '

4R32I757

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Lab Code: CHEM Case No.; 24906 SAS No.: SDG No. : MCSM03

Matrix (soil/water): SOIL Lab Sample ID: 8989S


% Solids: 59.3


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440 -23- S7440-26-07440-62-27440-66-6

,

AnalyteAluminumAntimonyArsenicBarium'BerylliumCadmiumCalciumChromiumCobaltCopperIron'LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

196003.05.3

73.50.33.0.33

80230.114.518.4

3410011.2

35203000.1625.54791.70.66

1083.016.4

106 •'0.74

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Comments: .' .

FORM I - IN tfU'lOll ILM04.0

AR32I758

U.S. EPA - CLP• •• •' 1 • . '_ •' ' •...'-.. '.

EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET _


- . . • .Lab Code: CHEM Case No.: 24906 SAS No. : SDG No. : MCSM03


Level (low/med) : LOW Date Received: 08/09/96

% Solids: 33.1- • j • . • -

Concentration Units (ug/L or mg/Kg dry weight): MO/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440*70r27440-47-37440-43-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-29-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenic .BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilver .Sodium iThalliumVanadiumZincCyanide

Concentration13300

5.310.483.40.590.59

201034.616.058.2

2320034.0

1510371

0.2735.35103.01.2

148-.-• ' 5.3

17.9140 '.1.3

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FORM I - IN

AR32 I 759

U.S. EPA - CLP"•'. ' '. - '.:•<'.••:,••. 1 • - . • '. . ' : •

•- EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET


Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.': MCSM03


Level (low/med): , LOW Date Received: 08/09/96

* Solids: 59.7 ; •


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-4 ,'7440-23-57440-28-07440-62-27440-66-6

Analvte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopper'IronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration16700

3.0•7.696.20.680.33

145042.724.523.4

4050027.6

1780936

0.1718.8947

•*' 1.70.66

148: 3.0

27.8. 83.8 :

0.70

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Comments: . , .

FORM I -.IN ' ; lfl)l|Of/9 ILM04.0

AR321760

U.S. EPA - CLP ,. : • 1 ' - . ' • •

EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET

Lab Name:,CHEMTECH CONSULTING GROUP Contractt 68-D5-0166MCSM26

Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSM03



% Solids: 58.1.. . . • " - ' • . - - / •


CAS No.

7429-90--57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-23-07440-S2-2 .7440-66.-6

•

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration15900

3.0.: ) 7.6

89.70.610.34

1700-43.924.321.7

3610026.6

1670•• .* 895

0.1721.4366

* 1.7. 0.53IS!

-. 3.024.7213 :

0.77

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Color After: YELLOW Clarity After: ',' Artifacts:

Comments: . ' • .

FORM I -IN ' ILM04.0

AR32I76I

U.S. EPA - CLP -'•-"•' X ' ' •. ' : • • • • • ' •


MCSM25Lab Name:. CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM ' Case No.: 24906 SAS No.: SDG No.: MCSM03



% Solids: • , -. 45.6 :':••';/ ; . . • • . ' .. • .

Concentration Unite (ug/L or mg/Kg dry weight): MG/KG ,

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-7'7440-43-97440-70-27440-47-37440-48-47440-50-87439-69-67439-92-17439-95-47439-96-S7439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6••

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganese,MercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

170003.95.9

1240.500..43

120031.010.412.2

2150019.5

21102160.2215.7947

* 2.20.87

104: " • ' • • • 3 . 9

21.684. o:0.94

C

U

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Comments: • : ,

FORM I - IN - ILM04.0

AR32f762

U.S. EPA - CLP' • 1 , • .

EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET


Lab Code: CHEM Case No.: 24906. SAS No.: SDG No.: MCSM03' ' , ' ' ' '

Matrix (soil/water) : SOIL Lab Sample ID: 37333


% Solids: . 70.0

Concentration Units (ug/L or mg/Kg dry weight); MG/KG

CAS No. .

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-rl7439-95-47439-96-57439-97-67440-02-07440-09-77732-49-27440-22-4744 0-23'- 57440-28-07440-S2-27440-66-6

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercury.NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration14600

2.52.5

55.90.70'0.46

2050036.519.326.2

4010023.1.

9920584

0.1314 . 9727

.* 1.46.57

1622.5

22.4106 '•:

0.64

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Color After: YELLOW Clarity After: Artifacts: ;., •*, - i

Comments: .

FORM I - IN UDM006 ILM04-°

AR32I763

U.S. EPA - CLP'••' .': x ' -;' *'-' . • . ' .'.

EPA SAMPLE NO..INORGANIC ANALYSIS DATA SHEET


Lab Code: CHEM Case Nb.,:_ 24906 SAS No.: SDG No. : MCSM03



% Solids: ; • ' • • - . S4-.0: ,'/•/—..';"•,.:"• ' • ' . • • " ' • •


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-67439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

AnalyteAluminumAntimony :ArsenicBarium 'BerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

• ' • • ; • " : - . .

Concentration

161003.33.3

1270.770.36

84830.814.512.0

2650019.6

2050537

0.1717.8

. 952• .1.8

0.731183.3

26.9' 69.2*

0.79

C

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Color After: YELLOW • Clarity After: Artifacts:

Comments: ; . <

POEMI-™ ,,01,005

U.S. EPA -' CLP: ' X • . . " ' • . " .


MCSM12Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-P5-0166

Lab Code^ CHEM Case No.: 24906 , SAS Noi : SDG No.: MCSM03



% Solids: 61.8


CAS NO.

7429-90-57440-36-07440-38-2 ,7440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-37439-39-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron •LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration13000

2.92.9

36.30.320.39

120035.227.627.4

-. 4590017.3

16404900.1520.9537

• 1.60.63

1042,9

• . 13.197.6-0.66

C

UU.38BB

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U

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Color Before: BROWN Clarity Before: . Texture: MEDIUM

Color After: YELLOW Clarity Afteri Artifacts:

Comments: ' • ' - '

FORM I - IN IKM'004 ILM04.0

' i\R32l765

u.s. EPA - CLP • ?•• •I'/1.; 'i- :: •.' ''• • . "' ' . • - - '


MCSM11Lab Name: CHEMTECH CONSULTING GROUP • Contract: 68-D5-0166

Lab Code: CHEM -Case No. : 24906 SAS No.: SDG No.: MCSM03

Matrix (soil/water): SOIL ' Lab Sample ID: 8735S


% Solids: 63.0 ; '/.,


CAS No.

7429-90-57440-36-07440-38'-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-1-'.7439-95-47439-96-57439-97-67440-02 -0 .7440-09-77782-49-27440-22-47440-23 -S7440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalcium ;ChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

189002.82.881.20.720.48

286045.618.4

' 30.842600

33.513406650 . 1417.0

1030* ' • 1.6

0.63175

: 2.825.61360.67

C

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BB

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Color Before: .BROWN : Clarity Before: Texture: MEDIUM


Comments: . . '. c',: • • ' • .' . . • • • - . - . , . • " • - • •

- ' ' ' - * • : ' • • ' - . • . . ,

FORM I - IN ILM04.0

AR32I766

U.S. EPA - CLP' •• 1 ' . - . - ' • - ' ' ' . " • • "

: EPA SAMPLEINORGANIC ANALYSIS DATA SHEET

\JLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

MCSM03

Lab Code: CHEM Case No,: 24906 SAS No.: SDG No.: MCSM03

Matrix (soil/water) : SOIL ' Lab Sample ID: 373'6S

Level (low/med) : LOW Date Received: 08/01/96

* Solids: 49.3 - ,

Concentration-Units. (ug/L or mg/Kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-33-27440-39-37440-41-7.7440-43-97440-70-27440-47-37440-48-47440-50-37439-89-67439-92-17439-95-47439-96-57439-97-57440-02-07440-09-77782-49-27440-22-47440-23-57440-23-07440-62-27440-66-6

• _ m


Concentration19500

3.46.7

1070.910.53

361077.523.320.7

4730042.7

1300999

0.1920.1

1140.1.90.76

1873.4

31.3154 •

0.90

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Color Before: BROWN Clarity Before: Texturei MEDIUM

Color After: .YELLOW Clarity After: Artifacts:

Comments:

FORM I - IN tJl)'»002 ILM04

\R32I767

U.S. EPA - CLP: ' ' '•• 1 . •.. ' '' ' : ' , . ' ' •. •-



Lab Code: CHEM . Case No. : 24906 SAS No. : SDG No.: MCSM03


Level (low/med): LOW Date Received: 08/09/96* • ' ! . " ' • ' • • . ' •

* Solids: 81.9 , ^


CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96--S7439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6


Concentrationi . • ' ••

167002.14.886.20.710.37

425039.214.826.5

3990029.7

16207580.1218.2

1080' 1.2

0.47124

': 2.125.5100 '0.54

C

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Color After: YELLOW. Clarity After: Artifacts:

Comments: v ' ' •

FORM I - IN POH014 *I«M04.b

AR32 I 768

•

\ . * ' . ' 'v- '

•'/ '• 'V ' " '' ' , : ' •• '

". •'. • v

AR32I769 .

U.S. EPA - CLP•':.•'• ' a '.. ' .

EPA SAMPLE NO.INORGANIC .ANALYSIS DATA SHEET

MCSM16.Lab Name: CHEMTECH. CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No&. : 24906 SAS No. : . SDG No. : MCSM16

Matrix, (soil/water): WATER • Lab Sample ID: 9008S


% Solids: 0 . 0 . ' , ' • '

Concentration Units (ug/L;or mg/Kg dry weight): UG/L

.o-

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron <LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium 'ThalliumVanadiumZincCyanide

Concent rat ion

2149.09.0

53.71.01.0

43501.01.51.0

8463.0

34402380.209.4

21405.02.0

21000009.01.0

28.0-9.0

C

UuBUUBUBU

UB

UBBUU

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Color Before: COLORLESS Clarity Before: CLEAR Texture:"


Comments: . ' . - . • • ; . ' " . . ' • • ,

FORM I - IN 002 ILM04.0

AR32 1770

APPENDIX B' ; . - ' •

SUPPORT DOCUMENTATION

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AR32I78.I

U.S. EPA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 '

Lab Code: CHEM Case No. : 24906 ~ SAS No. : SDG No. : MCSMOO

SOW No.: ILM04.0 , .

- EPA SAMPLE NO. Lab Sample ID. ,MCSMOO 8739SMCSM01 8747S'MCSM02 8742SMCSM04 8741S ,MCSM05 8750S • .MCSM06 ' 8746SMCSM07 8748SMCSM08 '8751SMCSM09 8740S ' ' ' " f?MCSM10 8749SMCSM13 8743SMCSM14 8752SMCSM15 8744S.MCSM18 874SSMCSM20 8753S .MCSM21 9005SMCSM24 9000SMCSM24D 9001S2MCSM24S 9002DSMCSM27 9003S

Were ICP interelement corrections applied? Yes/No YESWere ICP background corrections applied? Yes/No YES

If yes-were raw data generated beforeapplication of background corrections? Yes/No NO

Comments; '* .

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee. a«--verified by the following signature.

Signature: \S=±J&P&F<K Name: PARVEEN HASAN, • • ' . — . t \ s T — : ———— ~ — ~ — ' . • ' . -Date: ______ tfff2/4t> _______ Title: QA/QC OFFICER

COVER PAGE - IN ILM04-°C\T\

AR32I782

U.S. EPA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-01S6

Lab Code: CHEM - Case No..: 24906 SAS No. : SDG No.: MCSMOO• •

SOW No.: ILM04.0

EPA SAMPLE NO. Lab Sample ID.MCSM29 9004S 'MCSM35 900SS -

Were ICP interelement corrections applied? Yes/No YESWere ICP background corrections applied? • Yes/No YES

If yes-were raw data generated beforeapplication of background corrections? ' Yes/No NO

Comments: ' ', • , '

• • • •I certify that this data package ia in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as_verified by the following signature. ,

Signature: *4- &W* -~_____ Name: PARVEEN HASAN

Date: ^r&ft&_______ Title: QA/QC OFFICER ••' . • . - • * , ' • • " .

COVER PAGE - IN . . ILM04.0£02

AR,32I783.

In Reference to Case Ncfc):

REGIONAL/LABORATORY COMMUNICATION SYSTEMTelephone Record Log

Date of Call:

Laboratory Name:Lab Contact: '

Region:Regional Contact:" - -' ''••/Call Initiated By: * Laboratory ___ Region

In reference to data for the following sample numbers):

Summary of Queations/bsues Discussed:

;s

Summary of Resolution:

: g,.Signature •. ••;••• ~ ~[ ' ; Date

» ; - ' , " * • • . . ' • . " ,

Distribution: (1) Lab Copy, (2) Region Copy, 0) ^ Copy R QM n J c r 7 8 M

U.S. EPA - CLP

.'•••• '. : " 2B 'CRDL STANDARD FOR AA AND ICP



AA CRDL Standard Source: INOR-VEN

ICP CRDL Standard Source: INOR-VEN '.

. Concentration'Units: ug/L

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium,VanadiumZinc

.

CRDL Standard for AA

True Found %R• <

f~ " .

0.2

-•- -

' .

- '.*

o.oo"Oil 8".•

'•.:•-'"."..

•e-re-«tc>,oflj-V\5PuVi pk

•• ' \ "'' •:'. l

CRDL Standard for ICPInitial Final

True Found VR Found .^ VR

120:020.0

10.010.0

20.0100.050.0

6.0

30.0

80.0• .•"• .

10.020.0

20.0100.040.0

'.' .

\130.6019.02

11.4011.52

21.92116.9858.54

7.61

34.48

91.66,x '

14.1821.31

25.64113.. 8646.18

108 . 895.1

114.0115.2

109.6117.0<£17.jr

ff26.§y

CT4T

T14.|/

141.8106.6

(£2B .2113 .5IS JU

129.04V 17.70

9.9710.74

21.29108.3757.90

7.05

32.50

84.47

14.2223.29

15.07109. OS41.37

1

i07.5(gtTTS99.7107.4

106.4108.4Q."S".j£__j.i7r|7108.3

105.6

142.2116.4

<g5 . JL

109.0103.4

'

,

Sft wrtU, fr t«4« ' KcSMco-oi. oH-°"T \O}

• ' : , : : . ' "028 ' / - :FORM II (PART 2) - IN ILM04.0

flR32(785

UvS. EPA - CLP

" : ' • ' " • • . ' . •' ' v 2B • ' •, '( . . . CRDL STANDARD FOR AA AND ICP

' • " . ' " ." *\ " ' " ~ " . " • ' ~


Lab Code: CHEM Case No. : 24906 SAS No.: SDG No. : MCSMOO

AA CRDL Standard Source: ' .

ICP CRDL Standard Source: INOR-VEN• ' • • ' • • •• • ' / ' . • • ' •' " •-

Concentration Units: ug/L

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmium -CalciumChromiumCobaltCopperIronLead ,MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

CRDL Standard f or AA

True Found %R

-. '.

-•

• • '>

' . . ' ' •

1 • ' /•

'' .

"

- —— rrr"


True Found %R Found . %R

1 120.020.0

10.010.0

20.0100. 050.0

6.0

; 30.0

eo:o.• •• •10.020.0

20.0100.040.0

.

128 . 0428.56

li.2211.18

• 22.18115.8360.48

6.32.33.94

91.74

9.2223.53

29.47113.5444.79

\

106.742. j««— ; — -^112.2111.8

'vSUl&15 .ITiii.65*v»_ — -**

105.3

( 13 . l]

fl4 .7*^ ^92.2117.6

J7 '."4"113.5112 .0

—\i/

, • : : i V : . 029 •'.- •-FORM II (PART 2) - IN ILM04.0

AR3J2I786

U.S. EPA- - CLP

' : ' 2BCRDL STANDARD FOR AA AND ICP


Lab Code: CHEM Case No. : 2490S SAS No. : SDG No. : MCSMOO

AA CRDL Standard Source: .

ICP CRDL Standard Source: INOR-VEN •I / • - • ' . " • .

Concentration Units: ug/L •

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc


True Found %R

/

1

•


True Found %R Found %R(*+)

•' 120.020.0

10 . 010 . 0

20:0100.050.0

6.0

30.0

80.0

10.020.0

20.0100.040.0

.

. •

131.3322.93

11.93-11.52

22.09' 116.75, 62 . 73

7.84

34.49

93.97

11.4523 . 34

19 . 93115.9346.56

\

109.5114.9

119.3115.2

llOi^*?gyg30.7]

liiTo8117 . 5

114 . 5116.7

99.5115.9116.4

>b

FORM II (PART 2) - IN 030 ILM04.0

AR32I787

1 ,'••'. U.S. EPA - CLP

, ' . ' , . ' ' '.. ;';"; :' '3: ' ' " - . • ' ' ' ' ' •

I i . . BLANKS

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166- - ' . " • • ' . ' ' * • "


Preparation Blank Matrix (soil/Water): WATER

Preparation Blank Concentration Units (ug/L or mg/kg): UG/L

•

1 Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium .VanadiumZincCyanide

InitialCalib.Blank(ug/L) C

• -82.99-.09.01.01.01.0

-60.6-1.11.0-2.0-46.33.0

-81.01.00.23.0

-75.55 .0-2.3

-78.59.0-1.02.09.0

BUUUUUBBUBBUBUUUBUBBUBUU

•

Continuing Calibration*Blank (ug/L) ,

1 C 2 C 3 C

. -54.39.09.01.01.01.0

-37.61.01.0-1.6-53.53.0

-59.81.00.23.0

-70.85.02.0

-71.59.01.02.09.0

BUUUUUBUUBBUBUUUBUUBUUUu-

-55.49.09.01.01.01.0

-48.21.01.0-1.1

, -53.03.0

-68.1..00.23.0

-64.65.0

•' v 2.0-62.5; 9.01.0

• 2.09.0

/

BUUUUUBUUBBUBUUUBUUBUUUU

-53.09.09.01 . 01.01.0

-47.71.01.0-1.3-44.33.0

-71.61.00.23.0

-77.15.02.0

-63.2^9.01.02.09.0

1V \^

BUUUUUBUUBBUBUUUBUUBUUUU—

Prepa-rationBlank c

665.6309.0009.0001.0001.000l.OQO

£r39 .31031.0001.000Q..61D1

(-53 .-78p3J . 000

C*66.640i.ooo"0.2003.000

,6"79 . 44S5.0002.000

74 . 66(£— 9". Oocf1.0002.000

' 9.000

BUUUUUBUUBBUBUUUBUUBUUUU

M

PPPP 'PPPPPPPPPPCVPPPPPPPPCA

FORM III - IN ILM04.0

033AR32I788

U.S. EPA - CLP :. • . • ' • . ' . • i - >. . • • •• /. , -: . . / , • -S ' . . . . • .

. ' .. '•' BLANKS '. .-.: •" '~ " ' ' , " . " ' • • ' • " •


Lab Code: CHEM Case No. : 24906 SAS No.: SDG No. : MCSMOO

Preparation Blank Matrix (soil/water):/ . . . . . - • _ ' . . . . .

Preparation Blank Concentration Units (ug/L or mg/kg):

Analyte

AluminumAntimonyArsenicBarium.BerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide.


•1 V .

• ' .^

• •

Continuing CalibrationBlank (ug/L)

4. _ C 2. C 3. r-»C(& >& >.V

-52.99.09.01.21.01 .0

-45.2<3l£TTtT

. -29^03,0

-75.61.00.23.0

-33.45.02.0

-63.59.01.02.09.0

V

.-. V

BUUBUUBBU>B3UBUUUBUUBUUUU—

13.09.09.01.01.01.0

25.01.01.01.027.03.0

<rgcL-y1.00.23.039.05.02.018.09.01.02.0

——— I ———— —— _

3UUUuu3Uuuuu3Uuuuuuuuuu

11.09.09.01.01.0,1.010.01.01.01.027.03.011.01.0

3.039.05.02.018.09.01.02.0

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FORM III - IN ' > . , ILM04.0

/1R32I789

U*S. EPA - CLP

•' '/'/''';- 5A '••.';' " • -: • ' . " rEPA SAMPLE NO.

SPIKE SAMPLE RECOVERY

_ MCSM24SLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.: MCSMOO/ ' • . ' • ; , . ' ' , ' ' "

Matrix (soil/water); WATER Level (low/med): LOW1 " • " , " ' • • • ' - ' ,-'• •

V Solids for Sample: 0.0 .

Concentration Units (ug/L or mg/kg dry weight): UG/L

. •

u

Analyte


ControlLimitVR

75-12575-12575-12575-12575-12575-125

75-12575-12575-12575-12575-125

75-12575-12575-125

- /

75-12575-125

75-12575-12575-12575-125

Spiked SampleResult (SSR) C

2124.7800501.180041.5700

1989.260049.200049.7400

200.5500503.4400237.70001239.710021.4000

529.06000.9360

500.6200

9.420044.1800

56.5800500.4600512.4400100.3000

: '

T..

•

1 •

SampleResult (SR) C

80.35009.00009.000010.19001.00001.0000

1.00001.00001.0000

153.00003.0000

•

26.40000.20003.0000

' • , • ' •' 5. 00002.0000

9.00001.00002.00009.0000

BUUBUU

UUU

u

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•

SpikeAdded (SA)

2000.00500.0040.00

2000.0050.0050.00

200.00500.00250.001000.0020.00

500.001.00

500.00

10.0050.00

50 . 00, 500.00500.00100.00

%R

102.2100.2103.999.098.499.5

100.3100.7

. 95 . 1108.7107.0

100.593.6100.1

94.288.4

113 .2100.1102.5100.3

Q""M

PPPPPPNRPPPPPNRPCVPNRPPNRPPPCA

Comments:

FORM V (Part 1) - IN ILM04.0

AR32 I 790

U.S. EPA - CLP

. . ..EPA SAMPLE W

DUPLICATES > • • \

MCSM24DLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166


Matrix (soil/water) t WATER , ' Level (low/med) :* LOW

% Solids for Sample: 0.0 . % solids for Duplicate: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

I s.

Analyte

AluminumAntimony (ArsenicBariumBerylliumCadmiumCalciumChromium 'CobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

ControlLimit

,

5000.0

100.0

15.0

^ - • .

Sample (S) C

80.3500. 9.00009.000010.19001.00001.0000

12273.57001.00001.00001.0000

153.00003.0000

3476.060026.40000.20003.0000

2311.20005.00002.0000

2180.76009.00001.00002.00009.0000

3UU3UU

uuuu3

Uu3UU3UUUu

Duplicate (D) C

77.42009,00009.000010.23001.00001.0000

12353.90001.00001.00001.0000

." 152.14003.0000

3505.730026.54000.20003.0000

2330.80005.00002,0000

2194.67009.00001.00002.0000.9.0000

BUU3UU

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0.7

0.6

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FORM'vi-- IN ; 040 ILM04-°

SR32I79I

U.S. EPA - CLP

. ; ' $ • y • .. . • . . - •, ' ' EPA SAMPLE NO.

ICP SERIAL DILUTIONS

MCSM24LLab Name: CHEMTECH CONSULTING GROUP, Contract: 68-D5-0166

Lab Code: CHEM Case No.: 24906 SAS No;: SDG No.: MCSMOO

Matrix (soil/water):^WATER Level (low/med): LOW" ' - • • . ' ' ' . . ' • • • • • • . . ' ' - ; • , ' *

, Concentration Units: ug/L

\j

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilver vSodiumThalliumVanadiumZinc

":••• - ' .'"•

Initial SampleResult (I) C

80.359.009.0010.191.001.00

12273.571.001.001.00

153.003.00

3476.0626.40

3.002311.20

5.002.00

2180.769.001.002.00

IUUBUU

UuU

uB

UBUUBUUU

SerialDilutionResult (S) C

79.5045.0045.0012 . 005.005.00

12463.60.: 5.00

5.005.00

135.0015.00

3532.7526.90

15.002141.5025.0010.00

2026.4045.00

. 5.0010.00

BUUBUUBUUUUUBB

UBUUBUUU

VDiffer-ence

1.1

17.8

1..5

100.0

1.61.9

7.3

7.1

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PPPPPPPPPPPPPPNRPPPPPP-PP

, . . . .FORM IX - IN 043 ILM04-°

- - ' * ' , . . ' . ' * " •

/1R32I792

U.S. 'EPA' - CLP ' . - : • • •

' • . - - • . .-10 • . • • • - . • • • • 'INSTRUMENT DETECTION LIMITS (QUARTERLY) .

- . • • ; ->.' • . ' - • • • • • - : " • • . . ' • ' . ' • ' 'Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

- • * • , • . .

Lab Code: CHEM , Case No.: 24906 SAS No.: SDG No.: MCSMOO- • • • ' . ) • • • - • • •

ICP ID Number: Date: 07/15/96 .

Flame AA ID Number: CN- ' . . X .

Furnace AA ID Number: ' -

Analyte


Wave-length(nm)

578 . 00

Back-ground

.

.

.

•*

CRDL(ug/L)

200501020055

50001050251003

5000150.240

5000510

500010502010

IDL(ug/L)

1

• • •

9.0

M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRCA

Comments: • "CN: SP-E LAMBDA-1.(UV/VIS) SPECTROMETER

044FORM X - IN. ILM04.0

AR321793

\ U.S. EPA - CLP

;•••' ^ - .- • • '< : ' 10 -i • ••". •' .•"INSTRUMENT DETECTION LIMITS (QUARTERLY)

Lab Name: CHEMTECH "CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM . Case No.: 24906 SAS No.: SDG No..: MCSMOO

ICP ID Number: PO ; Date: 07/15/96 •

Flame AA ID Number: ' ' '. ,

Furnace AA ID Number:


Wave-length(nm)

306.20206.80189.00493.40313.00226 . 50317.90267.70228.60324.70271.40220.40279.00257.60

231.60766.50

, 196.00328.00588.90190.90292.40206 .20

'• " ... • ;' .'/-

Back-ground

.

..

V

. ' ' •

CRDL(ug/L)

200601020055

50001050251003

5000150.240

5000510

500010502010

IDL(ug/L)

11.09.09.01.01.01.010.01.01.01.027.03.011.01.0

3.039.05.02.018.09.01.02.0

M

PPPPPPPPPPPPPPNRPPPPPPPPNR

Comments: •PO: ICP 6lfe TRACE ANALYZER

FORM X - IN 046 , ILM04.0

AR32I791*

U.S. EPA - CLP

10 '•• . • -' • • ' ' ' 'INSTRUMENT DETECTION LIMITS (QUARTERLY)

Lab Name: CHEMTECH "CONSULTING GROUP Contract: 58-D5-0166 - ^

Lab Code: CHEM Case No.: 24906 SAS No.; SDG No..: MCSMOO

ICP, ID Number: Date; 07/15/96

Flame AA ID Number: CV

?urnace AA ID Number:


Wave-,length(nm)

.-

253.70

." • ,

Back-ground m

' '

- \ : - .

•*

' •

-

CRDL'(ug/D

200601020055

50001050251003

5000150.240

5000510

500010502010

IDL(ug/L)

0.2

M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRCVNRNRNRNRNRNRNRNRNR

C o m m e n t s : ' • - . . 'CV: SPECTRO-PRODUCTS MERCURY ANALYZER

FORM X - IN ' ' ILM04.0045

AR32I795

: • ' '/ U.S. EPA - CLP • '' '"','' • " ' • • • - ' • • . • |

. • • ' . ; . . '-:•"•" 13. • ' f ' • • . - " ••PREPARATION LOG : , i

Lab Name: CHEMTECH-CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No, : 24906 SAS No.: SDG No. : MCSMOO

Method: CA ' -'•';• ; , ; ' • , •

EPASample No.

MCSMOOMCSM02MCSM04MCSM09MCSM13MCSM15MCSM18 ;MCSM21MCSM24MCSM24DMCSM24SMCSM27MCSM29PBW

^

• S "

PreparationDate

08/09/9608/09/96

. 08/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/96

. " . • • •

. • ' • , v •' . •

.'.:'.

' ' . ' • • . . •' :

.'

Weight(gram)

.

•

.• • .

--

Volume(mL>

5050505050505050505050505050

,• *

FORM XIII - IN ,. ILM04.0053

AR32I796:

.••.-.'. • . ' ';•- ' u-s. EPA,'- CLP ;.'•. i • - . ' ' - '

' ' ' - . • . 13 . , ,PREPARATION LOG

Lab Name: CHEMTECH'CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.: MCSMOO

Method: CV . '

EPASample No.

MCSMOO '..MCSM01MCSM02MCSM04MCSM05MCSM06MCSM07MCSM03MCSM09MCSM10MCSM13MCSM14MCSM15' MCSM18MCSM20MCSM21MCSM24MCSM24DMCSM24SMCSM27MCSM29MCSM35PBW

-

. .

PreparationDate08/14/9608/14/9608/14/9608/14/9603/14/9608/14/9603/14/9608/14/9608/14/9608/14/9608/14/9608/14/9603/14/9608/14/9603/14/9608/14/9608/14/9608/14/9608/14/9608/14/9608/14/9608/14/9608/14/96

• - *•

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. Weight(gram)

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.

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100100100100100100100100100100100100100100100100100100100100100100100

T'

FORM XI11 - IN ' ' "54 ILMQ4.0

AR32I797

U.S.' EPA - CLP .

' • -'• ' . " ' . ' . ' " • - ^ '13 : . :j- •' - ' . ' . ' • " • • •

• - PREPARATION LOG•* • ' ' '- ^ ' ' • { : • ' ' ' ' • ' ' ' .

ab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No. : 24906 SAS No. : ' SDG No. : MCSMOO

Method: P .

u

EPASample No .

LCSWMCSMOOMCSM01MCSM02MCSM04MCSM05MCSM06MCSM07MCSM08MCSM09MCSM10MCSM13MCSM14MCSM1SMCSM18MCSM20MCSM21MCSM24MCSM24DMCSM24SMCSM27MCSM29MCSM35PBW

. PreparationDate08/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/96OB/16/9608/16/9608/16/96OB/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/96

- ' - • !

:-.',."•

Weight(gram)

•

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• •.

. - . :

•

Volume(mL)

100100100100100100100100100100100100100100100100100100100100100100100100

*.

-055FORM XIII - IN ILM04.0

AR32I798

U.S. EPA - CLP

- • ' - ' '.' . ' "'' " "- 14' •• ' " • • , ' "ANALYSIS RUN LOG , ' .

Lab. Name: CHEMTECH "CONSULTING GROUP Contract: 63-D5-0166 .

Lab Code: CHEM Case No.: 24906 SAS No. : . SDG No. : MCSMOO* • - • "

Instrument ID Number: PO Method: P . >

Start date: 09/01/96 . End date: 09/01/96 ,

EPASampleNo.

SOSSSSICVICVICVICVICBCRI-\ICSAICSABccvCCB:— IPBWZZZZZZLCSWZZZZZZMCSMOOMCSM09MCSM04MCSM02MCSM13MCSM15CCVCCB— 2-^MCSM18MCSM06MCSM01MCSM07MCSM10

D/F

1.001.001.001.001.001.001.001.00liOO1.001.001.001.001.001.001.001.00

,•• i.oo1.001.001.001.001.001.001.001.001.00

» 1.001.001.001.001.00

Time

09030919092109230926092709340940094409430954100310061009101210161022102510301035103910431046104910531056105911031106110911131116

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FORM XIV - IN V ILM04/

' 060

ft R 3-21.7 9 9

IT

U.S. EPA - CLP , .

. ' '.X--' 14 : |fANALYSIS RUN LOG


Lab Code: CHEM Case No. : 24906 SAS No.: "\ SDG No.;. MCSMOO

Instrument ID Number: PO- Method: P .

Start date: 09/01/96 v End date: 09/01/96

EPASampleNo.

MCSM05CRI— 7-ICSAICSABCCVCCB -3MCSM27MCSM29MCSM21MCSM35ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB-M-ZZZZZZZZZZZZMCSM14MCSM20CRI— 3ICSAICSABCCVCCB— fMCSM24MCSM24DMCSM24SMCSM24LZZZZZZ

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001 .001.001.001.001.001.001.001.001.001.001.001.001.001 . 001.00.1.0.0-1 . 005.001.00

Time

11191124112711301133113611391144114711511211121512181223122812351238124112441253131713231327133513401343134613501353135914031415

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. U . S . EPA - CLP

. ' .' • ' ' 14 . ' • . ' . '• ' • , . . '. • '. ".ANALYSIS RUN LOG



Instrument ID Number: PO Method: P

Start date: 09/01/96 . End date: 09/01/96

EPASampleNo.

ZZZZZZZZZZZZZZZZZZMCSM08ZZZZZZCCVCCB— feZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCRI— U'ICSAICSABccv-CCB-''ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB -? •ZZZZZZ

D/F

1.001.005.001.001.001.001.001.001.001.005.001.001.001.001.00

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10.00- 1.001.001.00

Time

14181421142314321439144214451452145514591504151015141517152115321544154715501602160516031614162216251630163616451657170017031709

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FORM XIV - IN . I-LM04

062

AR32I80I

U.S. EPA - CLP

• . . . • ' ' ' • - ' " ' ; • • • - ' ' • ' ' ' • • ' • ' 1 4 - 'il' ' • ' 'ANALYSIS RUN LOG ?

Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No. : 24906 SAS No. : SDG No.: MCSMOO/ . - • - - • .

- ' ' ' • • , ' ' • • . ' , ! ' . .

Instrument ID Number:- CN Method: CA

Start date: 08/09/96 • End date: 08/09/96

EPASampleNo.

SOS10.0S100.0S500.0S1000.0ICVICBCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZ -ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZMCSMOOPBWMCSM09MCSM04MCSM02MCSM13MCSM15MCSM18CCV

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00•1.001.001.001.001 . 001.001.001.001.00.1.001.001.00

Time

20002002200420062008201020122014201620182020202220242026202820302032203420362038204020422044204620482050205220542056205821002102

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FORM XIV - IN • . ILM04.0

05H

AR32I802"

U.S. EPA - CLP

' • • • ' ' " ' . " . • • '' ' ' ' ' . 14- .'••'• • '• 'ANALYSIS RUN LOG '• - . , - • • • • • . - . - • , • •



Instrument ID Number: CN Method: CA1 • • ,' •

Start date: 03/09/96 End date: 03/09/96

EPASampleNo.

CCBMCSM24MCSM24DMCSM24SMCSM27MCSM29MCSM21CCVCCB

. .

D/F

1.001.001.0.01.001.001.001.001.001.00

.

.. .

Time

210421062103211021122114211621132120

% R ALS3AS

•

'<

BA

*

BECD

•

CACRCO

/

Cu

•

inS

FE

»ll

P3

rte

MG

(3

MNHGNIK SEAG

.

NATLV

V

zN

f

->

CN

XXXXXXXXX

J

—

FORM XIV » IN ' '* ILM04

, OS?

'rtR'321803

'•', r . • . u,s. EPA - CLP.' '• -. ,'..; • ' .• • ' '':":•>• -r": •' •'•./'.-..; 14 . . .•.'.'j . : -• , ". .

ANALYSIS RUN LOG

Lab Name; CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No. : 24906 SAS No.: ' SDG No.: MCSMOO

Instrument ID Number: CV Method: CV


EPASampleNo.

SOSO. 2SO. 5Sl.OS5.0S10.0ICVICBCCVCCBCRAPBWMCSMOOMCSM09MCSM04MCSM02MCSM13MCSM15MCSM18MCSM06CCVCCBMCSM01MCSM07MCSM10MCSM05MCSM08MCSM14MCSM20MCSM24MCSM24DMCSM24S

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001 . 0.01.001.00•1.001.001.001.00•1.001.001.00i

Time

15071509151115131515151715191521152315251527152915311533153515371539154115431545154715491551155315551557155916011603160516071609

% R

•

•

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't .• - . • ,

AL

i.

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•

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FORM XIV - IN « ILM04.0

058

AR32f80l*

U.S. EPA - CLP .

. . •' . • 14ANALYSIS ;RDN LOG • .


Lab Code: CHEM Case No. : 24906 SAS No. : SDG No.': MCSMOO



EPASampleNo.

CCVCCBMCSM27MCSM29MCSM21MCSM35ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.00

,1.00i.oo1.001.001.001.001.001.00

f

.

Time

161116131615161716191621162316251627162916311633163516371639164116431645164716491651

%'R

/ . •

,

Analytes •:

ALS3AS

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FORM-XIV - IN . , • ILM04

059

AR32I805

MERCURYX .. ColdVaporAAicremiECH^ ™ ^ — — . — - _ — _^ ****** mm, «ktf*6S3UP. WC.

b: o.

Std. Name .

•

mLused

\

. .. .

Std. Ret £ From Logbook

- , . •' :'•''

• ' - • ' 1

Chemical Used j Lotfc

£,C/, 1 <fc3*r-Na.a.-Hit*y*il r fleJfct .

v 1• . • • • • 1 . v ,

I

Lib SampleKb.

CSeatSaapbNo.

MatrixW/S

fBozSop.

fBozS-Bfic

ot Hj100 eL 1000 oL

DE.Tut

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Time sn»TV

AO [tf'\ 1

£•10 'f'l*Sr.o af-o

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eaf T.OPPB<o-02

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r*Corre!anon Coefficient yHOi.

Rev.12/95 AR32I806''t

Page f efJL-

P ^_ -L——v— ;.... —-F=--1i : j -

.... .—••• •- ;.:. : :i.~-~ '-—T:._..., ..... -j .. :.. .....:_.......—„,.....——.————rj——— ~.i • —— rTTTtti——*S. . ......' ;•::-.. ...;: • :• Ij.;!..-..

r——

•1R32I807

8DO MCSM03

U.S. EPA - CLP' . ' " / • _ ' ' -

• • •' •*

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE| ,


Lab Code: CHEM Case No.: 24906 SAS No.: .SDG No.: MCSM03

SOW NO.: ILM04.0

EPA SAMPLE NO. Lab Sample ID.MCSM03 8736SMCSM11 8735S .MCSMl'2 8737S xMCSM17 8986S .MCSM19 8738SMCSM25 ' 8983SMCSM25D - 8984S2MCSM25S 8985DSMCSM26 8993S -MCSM28 8987SMCSM30. 8988S ,MCSM31 ,•: 8989SMCSM32 8990S •MCSM33 ' 8991SMCSM34 8992S

UWere ICP interelement corrections applied? Yes/No YESWere ICP background corrections applied? Yes/No YES


Comments: '"The "E" qualifier on Form I and IX for the Potassium indicates

a chemical or a physical interference, which was suspected during thePotassium analysis only. •. -

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee*—ae yerified by the following signature.

Signature: ' ~t*S;r . Name: PARVEEN HASAN

Date: ______<H*2>foc, Title: QA/QC OFFICER

COVER PAGE - IN -- * ILM04.0

AR32I809

U.S. EPA * CLP'

• • 23CRDL STANDARD FOR AA AND ICP


Lab Code: CHEM Case No.: 24906 SAS No.: • SDG No.: MCSM039 ' . ' •


ICP CRDL Standard Source: INOR-VEN

Concentration Units: ug/L •

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopper'IronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilver .SodiumThalliumVanadiumZinc


True Found *R

0.2 0.22 110.0


True Found , %R Found J^R

120.020.0

10.010.0

20.0100.050.0

6.0

30.0

30.0*

10.020.0

20.0100.040.0

131.44,20.73

10.3511.10

21.32103.0351.99

6.40

32.12

86.72

11.7222.23

25.97105 . 2044.30

109.5103.6

103.5

106.6103.1104 . 0

106.7

107.1

108.4

111.4

129.3106.2110.3

123.4024.59

10.3410.63

19.95100.3043.33

4.90

30.23

31.44

13.50C20.52

23.9699.4243.30

1

102.3£237$103.4106.3

100W97.3

31.7

lOO. 9

101.8

3:35. 3103.1

119.899.4103.2

/ 1

FORM II (PART 2) - IN UO'tOlS ILM04.0

AR32I8IQ "'.

, U.S. EPA - CLP'

• • ' • ' - ' • ' ' ' - • ' • . • ' ' • • • . • " ' V ' . ' 2 B ' . . • • .I j : CRDL STANDARD FOR AA AND ICP

' " ' < - ' •


Lab Code: CHEM Case No. : 24906 SAS No. : SDG No. : MCSM03

AA CRDL Standard Source: • , .



Analyte


CRDL Standard for AA• • . • • . :. . i

True Found AR

-

*

%

^

. •• ./ . ;. •


True Found %R Found >$£•'• ' - ' . ' ^ y120.020.0

/'•.'•10.010.0

20.0100.050.0

•6.0

30.0

80.0*

:10.020 . 0

.- .20.0

100.040.0

' v

.

*

-

129.0423.56

11.0011.19

19.94102.4449.32

7.47•31.14

62.92

10.0020.23

' ,21 . 07101.6647.06

107.5tfi7~a— —110.0111.9

99.7102.498.6

124.5

103.8

103.6

100.0101.2

105.4101.7117.6

4y

FORM II (PART 2) - IN 'V |,tj| |A<f« ILM04.0

; A R 3 2 I 8 I I

'. . • • ; •••••' ' t U.S. EPA.- CLP. .'. • . • - ' . .

.••'.' '' . 23 ' -. • . _•CRDL STANDARD FOR AA AND ICP

•-• •-• ' ;. • •••- ' •• • ' • ' ^ . - •: ' ...." • . - . \JLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No. : 249.06 SAS No.: SDG No.: MCSM03

AA CRDL Standard Source:

ICP CRDL Standard Source: INOR-VENv . •, . ' '. . ' • •


Analyte



True Found %R

'•

•

x

CRDL Standard, for ICPInitial Final

True Found %R Found . _%Rtfft

120.020*. 0

10.010.0

20.0100.050.0

6.0

30.0

30.0**,

10 . 020.0

. • r

20.0100.040.0

'

125.4321.52

9.3410.82

19.30102.3650.46

7.22

30.79

32.21

111 1520 . 19

19.72101.4742.44

104.5107.6

93.4108.2

99102x 4100.9

120.3

102.5

102.3

111.5101.0

98.6101.5106.1

FORM II (PART 2) - IN

AR32I8I2

UiS. EPA - CLP: • - . . - ' • • ' ' ' ( • ' '• • - ' . . - . . . ' • • • ; • , ' • ' • . • ? 3 • ' ' . - . - • ; ;

' . . -. ' : '. •••'.; ;.:';'BLANKS' ••'" •' '• ••' • : •-', .: '.. '..-Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

. . " • - ' - . : " ' > - • ' ' • •

Lab Code: CHEM Case No.;:. 24906 SAS No.: SDG No.: MCSM03

Preparation Blank Matrix (soil/water): SOIL

Preparation Blank Concentration Units (ug/L or mg/kg): MG/KG

t

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium ,ThalliumVanadiumZincCyanide


11 . 09.09.01.01.01.010. 01.01.01.0

27.03.0

ll.O1.00.23.0

39.05.02.0

18.09.01.02.09.0

UUUUUUUUUUUUUUUUUUUUuuuu


1 , C 2 C 3 C

11.09.09.01.01.01.010.0

- 1.01.01.0

27.03.011 . 01.00.23.0

39.05.02.0

18.09.01.02.09.0

UUUUUUUUDU0uuuuuuuu.uuuuu

11.09.09.01.01.01.0

10.01.01.01.0

27.03.0

11.01.00.23.0

39.05,0

' ? •• 2.018.09.0

:•' 1.02.09.0

1

UUuuuuuuuuuuuuuuuuuuuuuu

11.09.09.01.01.01.010 . 01.01.01.0

27.03.0

11.01.00.23.0

39.05.02.0

18.09.01.02.09.0

UUUUUUUUUUUUUUUUUUUUuuuu

Prepa-rationBlank C

-2.7621.8001.8000.2000.2000.2002.0000.2000.2000.2005.4000.600-2.3860.2000.1000.6007.8001.0000.4003.6001.8000.2000.4000.450

BUUUuuuuuuuuBUuuuuuuuuuu

MppppppppppppppCVppppppppCA

( £f $*~-$*. e fe J'.McSMO-S IMi.

FORM III - IN ILM04.0

: AR32I8I3

O.S. EPA - CLP

' -'. • "; - ' ' . . • -'3 •'. • ' . ' ' - '

• ' • • ' . : . • ' . . • ' BLANKS .. . • - - • ' • . „ . • . • • • • • • • • - . . ' ' - - • ' 'Lab Name: CHEMTECH CONSULTING GROUP Contract:.68-05-0166

Lab Code: CHEM . Case, No. : -24906 SAS No.: SDG No.: MCSM03

Preparation Blank Matrix (soil/water):• ' • . ' ' '


Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLead ;.MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Initial .Calib.Blank(ug/L) C

•. • • • ' • _

' *

_

. • • • • .- • ' •' i • .Continuing Calibration

Blank (ug/L)M^_ . ' ''tt , . ^ 'V '*m+L f** ^ > *N ^ j* jW J . C *\ V*

11.09.09.01.01.01.045.31.0vl.O

1.034.33;0

11.01.00.23.0

39.05.04.413.09.01.02.09.0

UUUUUUBUUU3Uu0UUUU30Uu00_

12.59.09.01.01.01.010.01.01.01.0

27. Of3.011.01.00.23.0

39.0S.O

•; 2.0•' 13.0

9.0, : 1.0

2.09;0

300000000000000000300000_

11.09.09.01*01.01.0

-10.61.01.01.727.03.0

-13.51.00.23.0

39.05.02.0

13.09.01.02.0

/1 "

00000030B30030000000000

-mm

. -

Prepa.-r at ionBlank C

-

.

^

M

PPP .PPPPP••• .

V

>*pppCVPPPPPPPPCA

. . . .FORM III - IN ''U'1022 ILM04.0

AR32I8U

0.S. EPA - CLP

' : ; . ' ' • 9 ' • : ; : . - • ' ' •SAMPLE NO.ICP SERIAL DIL0TIONS

MCSM25LLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No.: 24906 SAS No. : SDG No.: MCSM03

Matrix (soil/water): SOIL Level (low/med): LOW


• ' 'Analyte

AluminumAntimonyArsenic.BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Initial SampleResult (I) C• 39122.06

9.0013.69285.58• 1.161.00

2755.6071.4723.6427,98

49592.60' 44.84

. 4853.26497.69

36.172181.28

5.002.00

239,239.0649.64±93.40

U

BUB

B

B

B800B0B

SerialDilutionResult (S) C

38731.7045.0045.00295.805.005.00

2729.0072.9527.5030.45

51191.2049.70

4946. OS518.75

37.501805.8025.0010.00167.4545.0052.60207.80

00B00B

BB

B

BB0UBUB

%Differ-ence

1.0

100.03.6

100.0

1.02.115.48.83.210.81.94.2

3.717.2

30.0

6.07.4

, .

Q**

,

E

M

PPPPPPPPPPPPPPNRPPPPPPPP

FORM IX - IN 'w.-wfcu ILM04.0

-•'i'R 3 2-1-815

U.S. EPA - CLP

' - ..-'..'...- 13 • • . '• ' ' . • '.•—- .PREPARATION LOG j

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68TD5-0166

Lab Code:-CHEM Case No. : 24906 SAS No. : . SDG No. : MCSM03• ' ' ' .' ' - ; '

Method: CA , . ' ' .

EPASample No.

LCSSMCSM03MCSM11MCSM12MCSM17MCSM19MCSM25MCSM25D ,MCSM25SMCSM25MCSM23MCSM30MCSM31MCSM32MCSM33MCSM34PBS '

PreparationDate

08/12/9603/12/96OB/12/9608/12/9603/12/9603/12/9608/12/9608/12/9608/12/9608/12/9608/12/9608/12/9603/12/9608/12/9608/12/9608/12/9608/12/96

'

ii

-

Weight(gram)

1.001.001.061.101.061.011.051.051.051.001.08

; - 1.031.021.041.021.011.00

. '/ , •

' *

Volume(raL)

5050505050505050505050505050505050

*

--

FORM XIII - IN. UU''039 ILM04.0

AR32I8I6

; U.S. EPA - CLP' • '

- ' ' • ".••••.•••'•'•'•„•.r 13 ! v . . '• . •• ' .PREPARATION LOG


Lab.Code: CHEM Case No:: 24906 SAS No.: SDG No.:.MCSM03

Method: CV ••; ;

EPASample No.

LCSSMCSM03MCSM11MCSM12 -MCSM17MCSM19MCSM25MCSM25DMCSM25SMCSM26 •MCSM28MCSM30MCSM31MCSM32MCSM33MCSM34PBS

PreparationDate

08/19/9608/19/9608/19/9608/19/9608/19/9608/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96

V ' • t-

• '•'.•'• ' . . ' .\

' > > . ' -

. Weight' (gram)

0.200.210.220.210.220.220.200.200.200.200.200.220.210.200.200.200.20

1 • ' . -

- . • ,

Volume(mL)

100100100100100100100100100100100100100100100100100

UUH040FORM XII1 - IN ILM04.0

AR32I8I7

U.S. EPA - CLP

. 13 .PREPARATION LOG

' • ."•• • ' , ' • . . • > > ' : • • • • ' • ' • • 'Lab Name: CHEMTECH CONSULTING GROUP •' Contract: 68-D5-0166

Lab Code: CHEM Case No.: 24906 SAS No.: . SDG No.: MCSM03

Method: ? . . ' • . . : - ' ' -

EPA"Sample No.

LCSSMCSM03MCSM11MCSM12MCSM17MCSM19MCSM25MCSM25DMCSM25SMCSM26MCSM23MCSM30MCSM31MCSM32MCSM33MCSM34P3S

•'. • ' . . .

PreparationDate

08/14/9603/14/9608/14/9608/14/9603/14/9608/14/9608/14/9608/14/9603/14/9608/14/9603/14/9603/14/9608/14/9608/14/9603/14/9603/14/9603/14/96

.

i

Weight(gram)

1.001.051.011.021.021.011.01

• '1--031.041.021.021.021.021:041.041.051.00

•

Volume(mL)

200200200200200200200200200200200200200

' 200• 200200200

FORM XII! - IN , | !U,04.0

/1R32I8I8

U.S. EPA - CLP

' • ••[•••* ' ' • ' 1 4 ' • ; • ' • • ' ' ' . - . ' • •ANALYSIS RUN LOG


Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSM03

Instrument ID Number: PO . Method: P

Start date: 08/20/96 . End date: 08/20/96

EPASampleNo.

SOSS ,ssICVICVICVICVICBCRI— \ICSAICSABCCVCCB-\PBSZZZZZZLCSSZZZZZZMCSM11MCSM03MCSM12MCSM19MCSM17MCSM28CCVCCB -'Z.MCSM30MCSM31MCSM32MCSM33MCSM34

•

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

09560959100110031005100710101022102610311035104110481051105410581101110611121116111911231126113011371140114311471151115511561201

V R

....

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FORM XIV - IN ' • ILM04.0

iiOM'046• ' " • • . . * ' > t

AR32I8I9

U.S. EPA - CLP

• , ' • • ' . 1 4 . • ' •. ' • ANALYSIS RUN LOG

Lab Name: CHEMTECH" CONSULTING GRO0P Contract: 68-D5-0166

Lab Code: CHEM . Case No.: 24906 SAS No.: SDG No. : MCSM03

Instrument ID Number: PO, . Method: P


EPASampleNo.

MCSM26ZZZZZZCRI— T-ICSAICSA3CCVCCB— 3MCSM25MCSM25DMCSM25SMCSM25LZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB— 4-ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCRI— 3ICSA .•ICSABCCVCCB-*5ZZZZZZZZZZZZ

D/F

1.001.001.001.001.001.001.001.001.001.005.001.001.001*005.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

12051210121712231236123912421253130213121316132013251331134113451353135613591404140714111417142314271430144514521455145815041507

% R AL

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FORM XIV - IN „ ILMOT

;[R32I820

U.S. EPA - CLP

' • • • ' • . . ,•:. -;. - ;—":''''. ' : '14' ' ;:-:5i;- \: -,. • •• ... , • /. . ANALYSIS RUN LOG

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 ,

Lab Code: CHEM Case No. : 24906 SAS No.: SDG No. : MCSM03

Instrument -ID'Number: PO Method: P x


o

EPASampleNo.

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f 1

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1.005.001.001.001.001.001.001.001.00

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FORM XIV - IN - ILM04.0

AR32I82I

U.S. EPA - CLP

• • " • - - • ; 14 * • ": - .!ANALYSIS RUN LOG

' -.•' ' - - - ••• .-:' - . •: . - •' "• -:.Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No.: 24906 SAS No. : SDG No. : MCSM03

Instrument ID Number: CN .< Method: CA

Start date: 08/12/96 End date: 08/12/96 ,

EPA •SampleNo.

SOS10.0S100.0S500.0S1000.0ICVICBCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCV

D/F

1.001.001.001.001.001.001.001.0011.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

• 1.001.001.001.00

Time

21002102210421062103211021122114211621132120212221242126212321302132213421362133214021422144214621482150215221542156215322002202

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UUM042.AR32I822

:•• . • U.S. EPA - CLP ;

' •"' ' ' ' ' ,=;-;\ 14 ' -' ."- •- ' --, .. ::ANALYSIS RUN LOG

b Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

,ab Code: CHEM . Case No.: 24906 SAS No. :> SDG No.: MCSM03

Instrument ID Number: CN , . Method: CA

jtart date: 08/12/96 End date: 08/12/96

i EPA; Sample: NO.

CCBZZZZZZZZZZZZZZZZZZ .PBSLCSS'MCSMllMCSM03MCSM12MCSM19MCSM25CCVCCBMCSM25DMCSM25SMCSM17MCSM28MCSM30MCSM31MCSM32MCSM33MCSM34MCSM26CCVCCB

•

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1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

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00*1043

AR32I823

1 . U.S.; EPA - CLP

• • • ' • • ' • • . . - ' 1 4 - ' • • • ' . -ANALYSIS RUN LOG . ">

Lab Name: CHEMTECH CONSULTING GROUP , Contract: 68-D5-0166

Lab Code: CHEM Case* No.: 24906 SAS No.: SDG No. : MCSM03


Start date: 08/19/96 , End date: OB/19/96

EPASampleNo .

SOSO. 2SO. 5Sl.'OS5.0S10.0ICVICBCCVCCBCRAP3SLCSS ,MCSM11MCSM03MCSM12MCSM19MCSM25MCSM25DMCSM25SCCVccaMCSM17MCSM23MCSM3 0MCSM31MCSM32MCSM33MCSM34MCSM26ZZZZZZZZZZZZ

• ' • ' •D/F

1.001.001.001.001.001.001.001.001.001.001.001.0010VOO1.001.001.001.001.001.001.001.001.001.001.001.001 . 00.1.001.001%001.001.0010.00

Time

175717591301130313051807180913111313131518171319182113231325132713291331133313351837133913411343184518471349IS?!1353135513571359

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W)M044

/JR32I821*

U.S. EPA -'CLP

' - . ' • ' ' • ' . • : - • •' .".'14' •'ANALYSIS RUN LOG


Lab Code: CHEM Case No.: 24906 SAS No. : SDG No. : MCSM03

Instrument ID Number: CV Method: CV. ;,


f

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EPASampleNo.

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Time

19011903190519071909191119131915191719191921192319251927192919,3119331935193"7193919411943194519471949195119531955195719592001

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FORM XIV - IN „ ILM04.0

nO'1045

AR32I825

SDO MCSM16

/5R32I826

o.1 U.S. EPA - CLP

COVER PAGE - /INORGANIC ANALYSES DATA PACKAGE •

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166\ " , ' • ' : • '

Lab Code: CHEM Case No. : 24906 SAS No.: SDG No. : MCSM16

SOW No.: ILM04.0 _ ,'•

EPA SAMPLE NO. Lab Sample ID.•MCSM16 9008SMCSM16D 9009S2MCSM16S 9010DS

Were ICP interelement corrections applied? ' Yes/No YESWere ICP background corrections applied? Yes/No YES


Comments: ' • ."E" qualifiers on Form I and IX for the Barium and the Potassium

indicate a chemical or a physical interferences, which were suspectedduring the Barium and the Potassium analysis only.

I certify that this data package is in compliance with the terms andconditions of the contract, both .technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or the -Manager's desigriee --ets verified by the following signature.

Signature: (tm/J T ^ .Name: PARVEEN HASAN

Date:. _____0?f/$/f£ ,Title: QA/QC OFFICER

COVER PAGE - IN - - ILM04.0001

AR32I827

U.S. EPA - CLP

' 2 3 - . . - • " .CRDL STANDARD FOR AA AND ICP

Lab Name: CHEMTECH CONSULTING. GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No.: 24906 . SAS No.: SDG No. : MCSM16




AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc


True Found %R

.

0.2 0.21•

105.0

: CRDL Standard for ICPInitial Final

True Found %R Found %RO ro120.020.0

'10 . 0. . 10.0

20.0100.050.0

6 . 0

30.0

80.0

10,020.0

20.0100.040.0

130.6019.02

11.4011.52

,

21.92116.93

. 53.54

7.61

34.43

91.66

14.1321.31

25.64113.8645.13

108.395.1

114.0115.2

,'109.6117.0117.1

126 .3

114 . 9

114 . 6

141.3106.6

128.2113.9115.4

129.0417.70

9.9710.74

§

21.29108.3757.90

7.05

32.50

84.47

14.2223.29

15.07109.0541.37

107.5-.83 . S

99.7107-"

, ,10o -/108.4115.3

117.5

103.3* •

105 . 6

142.2116.4

75.4109.0103.4

FORM II (PART 2) - IN 008 ILM04.0

AR32I828

U.S. EPA - CLP

, . . • . • • • . : - . • . - . .V J • ' . ' ; • CRDL 'STANDARD FOR AA AND ICP

Lab Name: CHEMTECH .CONSULTING GROUP Contract: 68-D5-0166

Lab Code': CHEM Case No. : 24906 SAS No.: SDG No..: MCSM16

,AA CRDL Standard Source: ;


• • " Concentration Units: ug/L

Analyte


CRDL Standard for AA- • ,-"" '

True Found %R

,

. ' .

• ".

~~~ • '

'

• '-•

•'. --.

^ ,' '

• /

.'.

:' ' ..'••.•.-

CRDL Standard for ICP .Initial Final

True Found VR Found iR

120.020.0

10.010.0

20.0100 . 050.0

- 6.0

30.0

80.0

10.020.0

20 . 0100.040.0

. •• .

. '

- 128.0428.56

. 11.2211 . 18

22.18115.8360.46

. %6.32

33.94

91.74

9.2223.53

29.47113.5444.79

^mmmmm ,

106.7142.8

112.2111.8

110.9115.8121.0 *105 . 3

113.1

114.7.

92.2117,6

147.4113.5112.0

. .FORM II (PART 2) - IN . 009 ILM04.0

AR32I829

U.S,' EPA - CLP

23' x . CRDL STANDARD FOR AA AND ICP


Lab Code: CHEM . Case No. : 24906 SAS No. : SDG No. : MCSM16

AA CRDL Standard Source: .



.Analyte



True Found %R" . ' ' !

_ . •

CRDL Standard for ICPInitial ;. Final

True Found %R Found, s-S*-

120 . 020.0

10.010.0

20.0100.050.0

6.0

30.0

30.0

10.020,0

20.0100.040.0

•

.

.• -

131.33• 22.98

,11.9311 . 52

22.03116.7562.73

7.84

34.49

93.97^

11.4523.34

19.93115.9346.56

109.5114.9

119.3115 -1

llVjGTSTj)125.5

130.7^

115.0•(£i7TT114.5116.7

99.6115.9€23

- 010FORM II (PART 2) - IN ' ILM04.0

AR32I830

U.S. EPA - CLP

, .' • • ' . , .. 2B • . •• •• -.CRDL STANDARD FOR AA AND ICP


Lab Code: CHEM Case No. :y 24906 SAS No.: SDG No. : MCSM16

AA CRDL Standard Source: ! ,


Concentration Units: ug/L ' .

1

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperironLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc


True Found %R

,

,

- " .

•"• :

'.' i

. x' v :'.. .

• .'. . ' • - ' • _ . . '

1 '",-'• •


True Found VR Found %R

120.020.0

10.010.0

20.0100.050.0

6.0

30.0

80.0

10.020.0

•. . .

20.0100.040.0

,- "

.,V

- • ;

•

'

128.2820.58

,

11.9310.78

22.38111.93'59.69

9.60

33.45

89.76*

10.8024.00

- .27.10112.7157.40

4 ———————

MS m

106.9102.9

119.3107.8

111 .9JL11.9;119.4.160.0

111.5••12 ."J?—

108.0120.0

135.5112 . 7ss

M cSf\ i1

FORM II (PART 2) - IN . ' Oil ILM04.0

AR32I83I

U^S. EPA - CLP

' ' .. < '•••'. . ' BLANKS. . -.-. _ ' - . ;

Lab Name: CHEMTECH CONSULTING GROUP Contract: 63 -D5- 0166

Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.: MCSM16

Preparation Blank Matrix (soil/water) : WATER

Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium .ThalliumVanadiumZincCyanide


-82.99.09.01 . 01.01.0

-60.6-1.11.0-2.0

-46.33.0

' -31.01.00.23.0

-75.55.0-2.350.49.0-1.02.09.0

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1 C 2 C 3 C

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-37.61.01.0-1.6

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-70.85.02.0

46.09.01.02.09.0

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-55.49.09.01.01.01.0

-48.21.01.0

-1.1-53.03.0

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-64.6. 5.0

2.046.09.01.02.09.0

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-53.09.0

. 9.01.01.0

, 1.0-47.71.01.0-1.3

-44.33.0

-71.81.00.23.0

-77.15.02.0

46.09 . 01.02.0

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AR32I832

U.S. EPA - CLP

- ', BLANKS

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 •

Lab Code: CHEM Case No. : 24906 SAS No.: , SDG No. : MCSM16

Preparation Blank Matrix (soil/water):


Analyte


InitialCalib.'Blank(ug/L) C

•

-

, , /.

.


*v 0>c *• .'d> - <£> c-52.99.09.01.21.01.0

-45.2-1.21.0

-2.1-29.03.0

-75.61.00.23 .0

-88 4'5.02.0

• 46.09.01.02.0

B00B00BB0BB0BUUUBUUUU0U

13.09.09.01.01.01.0

26.01.01.01.0

27.03.0

20.81.0

3.039.05.0

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9.01.02.0

BUUUUUBUUUUUBU

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11.09.09.01.01.01.010.01.01.01.0

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FORM III - IN . ' 013 ILM04.0

IVR32I833

. U.S. EPA - CLP

- ' ' .•', ' ' ' • ' . . . - . ' 3 ' . . - . - • • • • :"" ' ' • - - ' . • . . • • . ' " ~x ,

. . • • • - • • v • BLANKS • ' ' - . . : . ' ; /'. ' '. • • - . ' . ' - ' • **^

Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 -

Lab Code:' CHEM 'Case No.: 24906 SAS No.: SDG No.: MCSM16

Preparation Blank. Matrix (soil/water):


Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium .ThalliumVanadiumZincCyanide

InitialCalib.Blank(ugVD C

•

•

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Blank (ug/L)*• s-~ »C * *e£ '*/T*\ C(3) <£> (&)

15.99.09.01.01.01.024.71.01.01.027.03.022.21.0

3.039.05.02.0

9.01.02.0

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AR32l83lf

U.S. EPA - CLP

• • " . ' . . .'-.:•;• 13 ' . . ' • jr ' / • ' " '• . - '" •'• ''PREPARATION LOG


Lab Code: CHEM Case No..;: 24906. SAS No.: SDG No.: MCSM16

Method: CA ' "-. v.y.

EPASample No.

MCSM16MCSM16DMCSM16SPBW

• •• •

PreparationDate

08/14/9608/14/9608/14/9608/14/96

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FORM XIII - IN VT«*w ILM04.0D-4Q

AR32I835

• U.S. EPA - CLP

. • ' ' ; .' ... 13 • . ' '' • • . • • : . - • PREPARATION LOG,



Method: C V . . ' • " . ' . ,

EPASample No.

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PreparationDate

08/26/9608/26/9603/26/9603/26/96

•

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AR32I836

0.S. EPA - CLP

• - ' ' : •' • • : : . '13; r .'.••' • • • . - -.'•,. PREPARATION LOG .

LabName: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.: MCSM16

Method: P .' •.-•.•:••':••••• ' ' '

EPASample No .

LCSWMCSM16MCSM16DMCSM16SPBW

- • : '•-

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PreparationDate

08/23/9608/23/9608/23/96OB/23/96OB/23/96

• • /. ,• .. • ••

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10Q100100100100

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FORM XIII - IN ftJIO 'ILM°4-°

AR32I837

a ^ u.s. EPA - .CLP v• . ' , : . . ' . • • ' - ' • 1 4 • " . '

. ANALYSIS RUN LOG

Lab Name: CHEMTECli CONSULTING GROUP Contract: 68-D5-0166


Instrument ID Number: PO Method: P

Start date: 09/01/96 Erid date: 09/01/96

EPASampleNo.

SOSSSsICVICVICVICVIC3 :CRI— \ICSAICSABCCVCCB-rNZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB— 2ZZZZZZZZZZZZZZZZZZZZZZZZ .ZZZZZZ

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D/F

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, 1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

• i.oo1.001.00

Time

09030919092109230926092709340940094409430954100310061009101210161022102510301035103910431046104910531056105911031106110911131116

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FORM XIV - IN

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AR32I838

' U.S. EPA - CLP . .

• V :'^V " . • ' • ; - . - > ' • "-i4 '.al>'"' - . - ' . . ' . ' . - • > - .ANALYSIS RUN LOG

Lab Name: CHEMTECH CONSULTING/GROUP Contract: 68-D5-0166•- , N ' - ' -

Lab Code: CHEM Case No.: 24906 . SAS No.: SDG No.: MCSM16

Instrument ID Number: PO • Method: P

Start date: 09/01/96 ; End date: 09/01/96

EPASampleNo.

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11191124112711301133113611391144114711511211121512161223122812351238124112441253131713231327133513401343134613501353135914031415

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FORM XIV - IN . ILM04.0

047

AR32I839

U.S. EPA - CLP

. .•' •' ' ' '. 14 ' . ' ,V ANALYSIS RUN LOG


Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSM16

Instrument ID'Number: PO Method: P

Start date: 09/01/96 '• . ' End date: 09/01/96

EPASampleNo.

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D/F

1.001.005.001.001.00

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Time

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FORM XIV - IN " ILMOX J

flR32l8itO

: , , ,;. _ U.S. :EPA - CLP ? ' . . ; ; ,

•'-. - ••• . •'-:-•" 14 . • ' •'" • vANALYSIS RUN LOG

Lab Name: CHEMTECH" CONSULTING GROUP Contract: 68-D5-0166

Lab Code: CHEM Case No i: 24906 SAS No.: SDG No.: MCSM16

Instrument ID Number: CN > . Method: CA . .

Start date: 08/14/96 ' End date: 08/14/96

EPASampleNo.

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FORM XIV - IN . ILM04.0

1R32/81H

, U.S. EPA - CLP

' . " • ' 14 : ' , •ANALYSIS RUN LOG' • • . • ' • ; • - , . ' . - : . , . • • • . \ J -

Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166 •——'

Lab Code: CHEM Case No. :. 24 906 SAS NO.: SDG No. : MCSM16


Start date: 08/26/96 End date: OB/26/96

EPASampleNo.

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Time

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FORM XIV - IN „ ' • ILM04

044

„ U.S. EPA - CLP

'• '' - ' • ' ".-'N '" 14' ' ' ' . : ' , - ' ' 'ANALYSIS RUN LOG

Name: CHEMTECH CONSULTING GROUP .'•'•' \ Contract: 68-D5-0166

Lab Code: CHEM . . Case No.: 24906 SAS No.: SDG No.t MCSM16

Instrument ID Number: CV - Method: CV


EPASampleNo.

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FORM XIV - IN ILM04.0

' 045

'!R32I8I*3

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