AB2886 Implementation - California

SSSSWWWWRRRRCCCCBBBB

AB2886 ImplementationAB2886 ImplementationAB2886 ImplementationAB2886 Implementation

Stockton Training Stockton TrainingOctober 16, 2001October 16, 2001

Marilyn R. ArsenaultArsenaultLegg, Inc.

[email protected]

California California California California Underground Storage Underground Storage Underground Storage Underground Storage

Tank ProgramTank ProgramTank ProgramTank Program

SSSSWWWWRRRRCCCCBBBB AB2886 ImplementaionAB2886 ImplementaionAB2886 ImplementaionAB2886 Implementaion

• GeoTracker Data Flow Overview• Part 1- Implementation

– Electronic Data Formats for GeoTracker

– Data Requirements– Available Tools– Submitting Data to GeoTracker

• Part 2 - Format Details– Data Format Details– Advanced Format Content


SSSSWWWWRRRRCCCCBBBB Part 1 - ImplementationPart 1 - ImplementationPart 1 - ImplementationPart 1 - Implementation

• Formats

• Preparation

• Verification

• Uploading

SSSSWWWWRRRRCCCCBBBB Electronic FormatsElectronic FormatsElectronic FormatsElectronic Formats

• Standardized Data Format– Fields of information are listed in a

defined order

– Names of organizations, analytes, andmethods are generally given codes(valid values) for consistency

– Data delivery has a defined format(e.g., fixed length or comma/quotedelimited)

SSSSWWWWRRRRCCCCBBBB Delivery FormatDelivery FormatDelivery FormatDelivery Format

GLOBAL ID FIELD PT NAME PARAMETER RESULT UNITS

T0605902476 MW-1 BZ 25 UG/LT0605902476 MW-1 MTBE 33 UG/L

VALID VALUES

BZ = BenzeneMTBE = Methyl-tert-butyl etherUG/L = ug/L


GEO_XY GEO_Z GEO_WELL EDF 1.2i

SURVEY_XYZ

GeoTracker

SITE_MAP

SSSSWWWWRRRRCCCCBBBBLinking Data to GeoTrackerLinking Data to GeoTrackerLinking Data to GeoTrackerLinking Data to GeoTracker

• Global ID– An identifier created by the GeoTracker

System– Represents a site or facility identifier

• Field Point Name– The name assigned by the

Consultant/RP to a survey or samplecollection point

SSSSWWWWRRRRCCCCBBBB SURVEY_XYZSURVEY_XYZSURVEY_XYZSURVEY_XYZ


SURVEY_XYZ

GeoTracker

SITE_MAP

SSSSWWWWRRRRCCCCBBBB What is SURVEY_XYZ?What is SURVEY_XYZ?What is SURVEY_XYZ?What is SURVEY_XYZ?

• A format for electronic delivery ofwell location coordinates, elevationand groundwater measurement data

• Provides the geo-spatial coordinatesfor the GeoTracker System

SSSSWWWWRRRRCCCCBBBB Location InformationLocation InformationLocation InformationLocation Information

• One-time submittal

• Latitude/Longitude data only (indecimal degrees, to 7 decimal points)

• Measure 1 meter accuracy or better

• Submission will be based uponGlobal ID and Field Point Name

SURVEY_XYZ

GEO_XY

SSSSWWWWRRRRCCCCBBBB Elevation InformationElevation InformationElevation InformationElevation Information

• Periodic submittal

• From top of casing

• Measure to +/- 0.01 Foot Accuracy


SURVEY_XYZ

GEO_Z

SSSSWWWWRRRRCCCCBBBB Depth to GroundwaterDepth to GroundwaterDepth to GroundwaterDepth to Groundwater

• Submit each time a well is sampled

• From top of well casing:– Floating product surface– Groundwater surface

• Measure to +/-0.01 foot accuracy


SURVEY_XYZ

GEO_WELL

SSSSWWWWRRRRCCCCBBBB Site MapSite MapSite MapSite Map

• Periodic submittal

• Site Map

• File type– gif– tiff– jpeg– pdf

• Submission will be based uponGlobal ID

SITE_MAP

SURVEY_XYZ

SSSSWWWWRRRRCCCCBBBB SURVEY_XYZ BenefitsSURVEY_XYZ BenefitsSURVEY_XYZ BenefitsSURVEY_XYZ Benefits

• Geo-spatial data of known precisionand accuracy

• Data available for modelingconstituents

• Active archive for public use

SSSSWWWWRRRRCCCCBBBB EDF 1.2iEDF 1.2iEDF 1.2iEDF 1.2i


SURVEY_XYZ

GeoTracker

SITE_MAP

SSSSWWWWRRRRCCCCBBBB What is EDF?What is EDF?What is EDF?What is EDF?

• An electronic version of a laboratoryreport

• Data is formatted for ease of use bymultiple parties

• Provides a consistent level of quality

SSSSWWWWRRRRCCCCBBBB Chain-of-CustodyChain-of-CustodyChain-of-CustodyChain-of-Custody

• Global ID

• Field Point Names

• Sample IDs

• Collection Date/Time

• Preservation

EDF 1.2i

SSSSWWWWRRRRCCCCBBBB Analytical ResultsAnalytical ResultsAnalytical ResultsAnalytical Results

• Laboratory IDs

• Analyses Date

• Preparation Batch

• Results

EDF 1.2i

SSSSWWWWRRRRCCCCBBBB Data Quality ControlData Quality ControlData Quality ControlData Quality Control

• Control Limits• Surrogates• Blanks• Spikes

EDF 1.2i

SSSSWWWWRRRRCCCCBBBB How it WorksHow it WorksHow it WorksHow it Works

• Laboratory exports data from theirLaboratory Information ManagementSystem (LIMS)

• Data is converted into EDF 1.2i formatusing either tools developed by thelaboratory or tools provided by the EDFProgram

• Data is then transferred to the client withan associated hard copy report

SSSSWWWWRRRRCCCCBBBB Benefits of EDFBenefits of EDFBenefits of EDFBenefits of EDF

• Eliminates laborious reentry of hard copylaboratory data

• Hard copy reports from unrelatedlaboratories may have the same formatand appearance

• Nonconformance to standard analyticalmethods and procedures easily identified

• Conforms to SW-846 method requirements

• Provides a standard data format to beshared by multiple parties

SSSSWWWWRRRRCCCCBBBB Available ToolsAvailable ToolsAvailable ToolsAvailable Tools

• GeoTracker - Web-based Geo-spatialDatabase

• COELT - Corps of Engineers Loading Tool

• EDCC - Electronic DeliverableConsistency Checker

• DataStream Free - Data Verification andReporting Tool


COELT - Corp ofCOELT - Corp ofCOELT - Corp ofCOELT - Corp ofEngineers Loading ToolEngineers Loading ToolEngineers Loading ToolEngineers Loading Tool

• Laboratory software for preparation ofEDF deliverables

• Allows for link to Laboratory InformationManagement System and manual dataentry

• Electronic data consistency checkingensures format compliance

• Hard copy reports generated fromelectronic data - legally defensible

SSSSWWWWRRRRCCCCBBBB EDCC - ChecksEDCC - ChecksEDCC - ChecksEDCC - Checks

• Format Errors– Fields submitted in the incorrect order– Incorrect valid values

• Logic Errors– Analysis Date prior to Sample Date– Test without results

• Content Errors– Detection limits greater than reporting limits


EDCC - Electronic DataEDCC - Electronic DataEDCC - Electronic DataEDCC - Electronic DataConsistency CheckerConsistency CheckerConsistency CheckerConsistency Checker

• EDCC is available as software for aPC and is also accessible via theWeb at the GeoTracker site

• EDCC - PC version checks for alllaboratory generated content

• EDCC - Web version checks for alllaboratory generated content plusGlobal IDs and Field Point Names

SSSSWWWWRRRRCCCCBBBB DataStream FreeDataStream FreeDataStream FreeDataStream Free

• Reporting Tool

• Organizes Data

• Data Clean-Up

• QA/QC Reports

SSSSWWWWRRRRCCCCBBBB ImplementationImplementationImplementationImplementation

• Preparing for the sampling event

• Sample submission to the laboratory

• Laboratory analysis and reporting

• Data formats preparation

• Data format verification

• Uploading data into GeoTracker


GeoTracker Set-upGeoTracker Set-upGeoTracker Set-upGeoTracker Set-upTasksTasksTasksTasks

• Obtain Password

• Claim Facilities

• Establish Facility Security

• Obtain Global IDs

• Load Field Point Names


GeoTracker SecurityGeoTracker SecurityGeoTracker SecurityGeoTracker Security

AGENCY

CONSULT

LAB

Provides Access to facilities RPhas claimed

Provides Access to Consultant

Accesses Facility to Upload Data

May Access GeoTracker to CheckData

SSSSWWWWRRRRCCCCBBBB AuthorizationAuthorizationAuthorizationAuthorization

RP or authorized consultant

Site 1 Site 2 Site 3

• Consultant 1• Consultant 2• Consultant 3



Request Facilities

Obtains Password

Approves Facility Access

Agency

Web Request

Phone Approval

SSSSWWWWRRRRCCCCBBBB AuthorizationAuthorizationAuthorizationAuthorization

Consultant 1

Site 1 Site 2 Site 3

Request Facilities

Obtains Password

Approves Facility Access

Responsible Party

Web Request

Web Approval

SSSSWWWWRRRRCCCCBBBB GeoTracker PasswordGeoTracker PasswordGeoTracker PasswordGeoTracker PasswordSSSSWWWWRRRRCCCCBBBB

https://geotracker.swrcb.ca.gov/2886


Responsible PartyResponsible PartyResponsible PartyResponsible PartyGeoTracker Set-upTasksGeoTracker Set-upTasksGeoTracker Set-upTasksGeoTracker Set-upTasks

Go to GeoTracker and Submit aPassword

Claim Facility(s)

Agency Grants Access to Facility(s)

PASSWORD

FACILITY REQUEST

AGENCY


Consultant GeoTrackerConsultant GeoTrackerConsultant GeoTrackerConsultant GeoTrackerSet-upTasksSet-upTasksSet-upTasksSet-upTasks

Go to GeoTracker and Submit aPassword

Request Access to Facility(s)

Responsible Party Grants Access

Download Global IDsGLOBAL IDS

PASSWORD

FACILITY REQUEST

MONITORING REQUEST

CONSULT

CONSULT

CONSULT

DENY

LOGIN


Consultant GeoTrackerConsultant GeoTrackerConsultant GeoTrackerConsultant GeoTrackerSet-upTasks (cont.)Set-upTasks (cont.)Set-upTasks (cont.)Set-upTasks (cont.)

Assign Field Point Names toGlobal IDs

Upload Global IDs and Field PointNames into GeoTracker

ASSIGN FLD PT

UPLOAD FLD PT

CONSULT

CONSULT



Consultant AnalyticalConsultant AnalyticalConsultant AnalyticalConsultant AnalyticalData TasksData TasksData TasksData Tasks

EDCC

Submit Samples to Laboratory(Global IDs and Fld Pt Names)

Laboratory Sends ConsultantEDF1.2i

Electronic Data, Lab Report,EDCC Report

Consultant Reviews andGroups EDF1.2i for Site Report

EDCC

REPORT1

LAB

LAB

CONSULT

CONSULT

REP1 Global

REPORT2

APPEND


Consultant AnalyticalConsultant AnalyticalConsultant AnalyticalConsultant AnalyticalData Tasks (cont.)Data Tasks (cont.)Data Tasks (cont.)Data Tasks (cont.)

Consultant EDCC Web ChecksEDF1.2i

Consultant Uploads EDF1.2iTo GeoTracker Private

Lead Agency Worker Reviewsand Approves Electronic Data

Electronic Data is Moved toGeoTracker Public

EDF UPLOAD

REPORT SUBMITTAL

CONSULT

CONSULT

AGENCY

CONFIRMATION


Consultant SurveyConsultant SurveyConsultant SurveyConsultant SurveyTasksTasksTasksTasks

Survey Monitoring Wells

Create GEO_XY and GEO_Z

Web Check GEO_XY and GEO_Z

Upload into GeoTracker grouped inby Global ID(s)

CONSULT

CONSULT

CONSULT

CONSULT

CONSULT

CONSULT


Consultant Field DataConsultant Field DataConsultant Field DataConsultant Field DataTasksTasksTasksTasks

Collect Groundwater Measurementsfor each Well Sampled

Create GEO_WELL

Web Check GEO_WELL

Upload into GeoTracker grouped bySite Regulatory Report

CONSULT

CONSULT

CONSULT

CONSULT

SSSSWWWWRRRRCCCCBBBB Part 2 - The DetailsPart 2 - The DetailsPart 2 - The DetailsPart 2 - The Details

• SURVEY_XYZ format content

• EDF 1.2i format content

• Advanced format concepts



SURVEY_XYZ

GeoTracker

SITE_MAP


GEO_XY

Global ID T0627059321Field Point Name MW-1Field Point Class MW___XY Survey Date 01/09/2001Latitude 38.6481038Longitude -121.3949836XY Survey Meth SUBP___VExample Entry___VV Valid Value Example

V

SSSSWWWWRRRRCCCCBBBB Field Point ClassField Point ClassField Point ClassField Point Class

CODE DESCRIPTIONMW Remediation/Groundwater

Monitoring WellBH BoreholePUBW Public Drinking Water WellPRIW Domestic/Private Drinking

Water WellAGT Above Ground Tank

SSSSWWWWRRRRCCCCBBBB XY Survey MethodXY Survey MethodXY Survey MethodXY Survey Method

CODE DESCRIPTIONCONV Conventional survey technique.

(Third order – Class II) Minimumor 2 reference points: HPGN,HPGN-D, or 2 horizontal controlpoints derived from the HPGN orHPGN-D reference points.

RTK Real-Time Kinematic (RTK) GPSsurvey technique using a ….


GEO_XY

XY Datum ((((NAD83___XY Survey Org SURVEY-1GPS Equip Type (TXR___XY Survey DescXY Accuracy Val

V

V

SSSSWWWWRRRRCCCCBBBB XY_DATUMXY_DATUMXY_DATUMXY_DATUM

CODE DESCRIPTION

NAD83 NAD 83 HPGN Datum

SSSSWWWWRRRRCCCCBBBB GPS EQUIP TYPEGPS EQUIP TYPEGPS EQUIP TYPEGPS EQUIP TYPE

CODE DESCRIPTION

TXR Trimble PathfinderProXR <1m

TXRS Trimble PathfinderProXRS <1mTPOW Trimble PathfinderPower 1m

TPOC Trimble PathfinderPocket 2-5m

APRO Ashtech PromarkX < 2m

AZX Ashtech Z-Extreme < 1m

AZS Ashtech Z-Surveyor < 1m


GEO_Z

Global ID T0627059321Field Point Name MW-1Survey Date 01/09/2002Elevation 437.05Riser Height 2.88Elev Datum 29___Elev Survey Meth MEA___

V

V

SSSSWWWWRRRRCCCCBBBB Elevation DatumElevation DatumElevation DatumElevation Datum

CODE DESCRIPTION29 NDGV29(Mean Sea Level)88 NAVD88LOC Publically available local datum

from city, county or stateagency


Elev Survey MethodElev Survey MethodElev Survey MethodElev Survey Method

CODE DESCRIPTIONDIG Conventional differential leveling

(digital or non-digital)… Third OrderTRIG Trigonometric leveling using total

stations.CPGS Conventional elevation survey

technique (Third Order) based on aminimum of 2 GPS-derived controlpoints…


GEO_Z

Elev Accuracy ValElev Survey Org SURVEY-1Elev Survey Desc

SSSSWWWWRRRRCCCCBBBB Well InformationWell InformationWell InformationWell Information

GEO_WELL

Global ID T0627059321Field Point Name MW-1Measure Date 01/09/2002Grndwater Depth 140.05Riser Height 2.82Well Status ACT___Status Begin Date 01/09/2002

V

SSSSWWWWRRRRCCCCBBBB Well StatusWell StatusWell StatusWell Status

CODE DESCRIPTIONACT Groundwater well currently

used for remediation ormonitoring

INACT Groundwater well not includedin groundwater monitoringprogram

DRY Groundwater well is dry andcannot be sampled

SSSSWWWWRRRRCCCCBBBB Well InformationWell InformationWell InformationWell Information

GEO_WELL

Depth to ProductGrndwater DescDepth to Well

SSSSWWWWRRRRCCCCBBBB Site MapSite MapSite MapSite Map

• Site Map• Global ID

SITE_MAP



SURVEY_XYZ

GeoTracker

SITE_MAP



EDF 1.2i

Sample InformationSample InformationSample InformationSample InformationField Point Name MW-1Global ID T0627059321Collection Date 01/15/2002Collection Time 1256Field Organization FRM1___

Sample ID UST-1Matrix W___

V

V

SSSSWWWWRRRRCCCCBBBB Field OrganizationField OrganizationField OrganizationField Organization

TGGB TEG, Solana Beach, CARMTM RMT, Inc., Madison, WIMOOD Moodys of Dayton, Dayton, OHJFHM J.F. Hoffman, Merced, CAABRF ABR, Inc., Fairbanks, AKBBR Bill Belknap, Reedley, CABVEA Black &Veatch, Overland, KS

SSSSWWWWRRRRCCCCBBBB MatrixMatrixMatrixMatrix

CODE DESCRIPTIONSO Soil

W WaterGS Soil GasMH Hazardous Multi-Phase WasteTA Animal Tissue


EDF 1.2i

Sample InformationSample InformationSample InformationSample InformationProject Name UST PHASE 1Work Order #4352Laboratory LAB1___V

SSSSWWWWRRRRCCCCBBBB LaboratoryLaboratoryLaboratoryLaboratory

CODE DESCRIPTIONHPLE HP Labs, Escondido, CAKIFF KIFF Analytical LLC, Davis, CAEELR Excelchem Environmental Labs,

Roseville, CAMCAP McCampbell Analytical,

Pacheco, CAPIC Pace Analytical Services, Inc.,

Camarillo, CA

SSSSWWWWRRRRCCCCBBBB Test InformationTest InformationTest InformationTest Information

EDF 1.2i

Lab Sample ID LAB-4332-1

Lab Sample Type CS___

Analytical Method SW8260B___

Prep Method SW5030B___

Analysis Date 01/17/2002Prep Date 01/17/2002Prep Batch 5030-0117___

V

V

V

SSSSWWWWRRRRCCCCBBBB Lab Sample TypeLab Sample TypeLab Sample TypeLab Sample Type

CODE DESCRIPTIONLB1 Lab Blank #1LR1 Lab Replicate #1MS1 Lab Matrix Spike #1SD1 Lab Matrix Spike Duplicate #1BS1 Blank Spike #1BD1 Blank Spike Duplicate #1

SSSSWWWWRRRRCCCCBBBB MethodMethodMethodMethod

CODE DESCRIPTIONSW8260B Volatile Organic Compounds by GC/MSSW8270B Semivolatile Organic Compounds by

GC/MSSW8015B Non-Halogenated Organics Using

GC/FIDSW6010B Inductively Coupled Plasma-Atomic

Emission SpectroscopySW7421 Lead (AA, Furnace Technique)E160.1 Residue, Filterable (TDS)

SSSSWWWWRRRRCCCCBBBB Preparation MethodPreparation MethodPreparation MethodPreparation Method

CODE DESCRIPTIONSW3550B Ultrasonic ExtractionSW3580 Waste DilutionSW3580A Waste DilutionSW3810 HeadspaceSW5030B Purge-and-Trap for Aqueous

SamplesSW5035 Closed-System Purge-and-Trap


EDF 1.2i

Lab Report LAB-4332

Received Date 01/16/2002Chain-of-Custody UST-1

Basis N___

Mod Param List TLeach Method ___

Run Number 1

V

SSSSWWWWRRRRCCCCBBBB BasisBasisBasisBasis

CODE DESCRIPTIOND DryF Field FilteredL Lab FilteredN Not FilteredW WetC California Waste Extraction

Test


EDF 1.2i

Preservation P05___Sub Laboratory NA___Report Date 01/19/2002

Approved By TECH1

Test Notes ___

VV

V

SSSSWWWWRRRRCCCCBBBB PreservationPreservationPreservationPreservation

EDF 1.2i

CODE DESCRIPTIONP01 4 drops of 10% sodium

thiosulfate to 4 oz.P02 Adjust to pH 4-5P03 Add 3 mL 10% sodium

thiosulfate per 1 gal.P04 Adjust to pH < 2 with sulfuric

acid

SSSSWWWWRRRRCCCCBBBB Sub-Contract LaboratorySub-Contract LaboratorySub-Contract LaboratorySub-Contract Laboratory

CODE DESCRIPTIONHPLE HP Labs, Escondido, CAKIFF KIFF Analytical LLC, Davis, CAEELR Excelchem Environmental Labs,

Roseville, CAMCAP McCampbell Analytical,

Pacheco, CAPIC Pace Analytical Services, Inc.,

Camarillo, CA

SSSSWWWWRRRRCCCCBBBB Test NotesTest NotesTest NotesTest Notes

CODE DESCRIPTIONET Sample was extracted past end

of recommended max. holdingtime

CN Hydrocarbon response indiesel range but does notresemble diesel

CG Sample releases strong solventodor

AO Typical pattern for gasoline

SSSSWWWWRRRRCCCCBBBB Results InformationResults InformationResults InformationResults Information

EDF 1.2i

Parameter MTBE___Qualifier =___Value 45Units UG/L___Method Limit 0.5Reporting Limit 1.0Report Limit Qual MRL___

V

V

V

V

SSSSWWWWRRRRCCCCBBBB Parameter Parameter Parameter Parameter

CODE DESCRIPTIONMTBE Methyl-tert-butyl etherBZ BenzeneBZLCL ChlorotolueneBZME TolueneXYLENES XylenesPB Lead

SSSSWWWWRRRRCCCCBBBB QualifierQualifierQualifierQualifier

CODE DESCRIPTION< Less Than= Equal To> Greater ThanND Not Detected

SSSSWWWWRRRRCCCCBBBB Units Units Units Units

CODE DESCRIPTIONPPB Parts per billionPPM Parts per millionPPT Parts per trillionUG/G Micrograms per gramUG/KG Micrograms per kilogramUG/L Micrograms per literUG/ML Micrograms per milliliter

SSSSWWWWRRRRCCCCBBBB Detection QualifierDetection QualifierDetection QualifierDetection Qualifier

CODE DESCRIPTIONMDL Method Detection LimitPQL Practical Quantitation LimitMQL Method Quantitation LimitIDL Instrument Detection Limit

SSSSWWWWRRRRCCCCBBBB Results InformationResults InformationResults InformationResults Information

EDF 1.2i

Prim Value Type PR___UncertaintyDilution Factor 1Std Ref Material APG___Results Notes ___CL DateRetention Time

V

VV

SSSSWWWWRRRRCCCCBBBB Primary Value CodePrimary Value CodePrimary Value CodePrimary Value Code

CODE DESCRIPTIONPR Primary Result - The Primary Result for a

ParameterSR Semi-Quantitative ResultMS GC/MS Result - Value Confirmed Using GC/MSSR Semi-Quantitative ResultNR Not Reported - Data Not Reported1C First Column Result - The Value Obtained from the

First Column2C Second Column Result - The Value Obtained from

the Second Column

SSSSWWWWRRRRCCCCBBBB Standard Ref MaterialStandard Ref MaterialStandard Ref MaterialStandard Ref Material

CODE DESCRIPTIONABSSTD Absolute StandardsACCUSTD AccuStandardALDRICH Aldrich Chemical Co.APG Analytical Products

GroupBURJAC Burdick & JacksonCAMBRIDGE Cambridge Isotope Labs

SSSSWWWWRRRRCCCCBBBB Result NotesResult NotesResult NotesResult Notes

CODE DESCRIPTIONFX Analyte present in the instrument

blankGI Analyte confirmed by GC/MSFN Large closely eluting peak cannot

be separated from resultEW Surr. recovery outside of

acceptance limits, spike recov.accept.

SSSSWWWWRRRRCCCCBBBB Quality ControlQuality ControlQuality ControlQuality Control

EDF 1.2i

Laboratory LAB1___Prep Batch 5030-0117Analytical Method SW8260B___Parameter MTBE___Lab Sample Type MS1___Lab Sample ID LAB-4332-1-MSRef Lab ID LAB-4332-1

V

VVV

SSSSWWWWRRRRCCCCBBBB Quality ControlQuality ControlQuality ControlQuality Control

EDF 1.2i

Expected Value 95___Units UG/L___Matrix W___

VV

SSSSWWWWRRRRCCCCBBBB Control LimitsControl LimitsControl LimitsControl Limits

EDF 1.2i

Laboratory LAB1___Matrix W___Analytical Method SW8260B___Prep Method SW5030B___Parameter MTBE___CL Date 01/06/2001CL Type MEA___

VVV

V

V

V

SSSSWWWWRRRRCCCCBBBB Control Limit TypeControl Limit TypeControl Limit TypeControl Limit Type

CODE DESCRIPTIONMEA Method Established Accuracy

SSSSWWWWRRRRCCCCBBBB Control LimitsControl LimitsControl LimitsControl Limits

EDF 1.2i

Upper CL 120Lower CL 80

SSSSWWWWRRRRCCCCBBBB Data VerificationData VerificationData VerificationData Verification

• Blank hits

• Holding time

• Spikes outside of limits

SSSSWWWWRRRRCCCCBBBB Data Verification Cont.Data Verification Cont.Data Verification Cont.Data Verification Cont.

• Method sensitivity

• Preparation appropriate for analysis

• Method parameter list

• Proper preservation

SSSSWWWWRRRRCCCCBBBB Advanced ConceptsAdvanced ConceptsAdvanced ConceptsAdvanced Concepts

• Detection Limits

• Notes

Modified Parameter List

Expected Field

Batching

• Non-Client Samples

• Special QC Entry

Control Limits


Detection LimitsDetection LimitsDetection LimitsDetection Limits

Analyte Qual DataValue

MDL RDL GeoTrckValue

Benzene = 2 1 5 2

Benzene ND 2 1 5 ND

Benzene < 5 1 5 <5

SSSSWWWWRRRRCCCCBBBB Validation NotesValidation NotesValidation NotesValidation Notes

CODE DESCRIPTIONVR Val. Qual.: Rejected valueVQL Val. Qual.: QA/QC protocols not

met for lab control sampleVQM Val. Qual.: QA/QC protocols not

met for matrix spike/spike dup.VQS Val. Qual.: QA/QC protocols not

met for surrogate recovery

SSSSWWWWRRRRCCCCBBBB NotesNotesNotesNotes

TestNotes

ResultsNotes

ValidationNotes

Method Parameter Either

SW8260B Benzene Both

HoldingTime

BlankContamination

RejectedValue

H B VR

SSSSWWWWRRRRCCCCBBBB QA/QC SamplesQA/QC SamplesQA/QC SamplesQA/QC Samples

CollectDate

CollectTime

Sample Lab SampleType

01/17/2001 1200 MW-1 Client Sample

Lab Blank

Lab Control

SSSSWWWWRRRRCCCCBBBB Non-Client SamplesNon-Client SamplesNon-Client SamplesNon-Client Samples

• Samples analyzed for QA/QCpurposes that are not your samples

• Reported with a sample type of “NC”Non-Client samples

SSSSWWWWRRRRCCCCBBBB To Contact UsTo Contact UsTo Contact UsTo Contact Us

[email protected]

or

(800)-506-3887 (8am to 6pm PST)



Documents

AB2886 Implementation - California