ADEQ the TEG Dehydrator and the TEG Reboiler.ificant Activities list under Group A-I3 and Group A-I, Quantum Resources Management,

ADEQARK A N S A SDepartment of Environmental Quality

DEC 1..0 2007

Brad RogersQuantum Resources Management, LLC - Walker Creek Production Facility1775 Sherman Street, Suite 1200Denver, CO 80203

Dear Mr. Rogers:

The enclosed Permit No. 1126-AR-5 is your authority to construct, operate, and maintain theequipment and/or control apparatus as set forth in your application initially received on7/25/2007.

After considering the facts and requirements of A.C.A. §8-4-l0l et seq., and implementingregulations, I have determined that Permit No. 1126-AR-5 for the construction, operation andmaintenance of an air pollution control system for Quantum Resources Management, LLC Walker Creek Production Facility to be issued and effective on the date specified in the permit,unless a Commission review has been properly requested under §2.l.l4 of Regulation No.8,Arkansas Department of Pollution Control & Ecology Commission's Administrative Procedures,within thirty (30) days after service of this decision.

All persons submitting written comments during this thirty (30) day period, and all other personsentitled to do so, may request an adjudicatory hearing and Commission review on whether thedecision of the Director should be reversed or modified. Such a request shall be in the form andmanner required by §2.1.14 of Regulation No.8.

Sincerely,

) h-AI~}JJ~'"t---

Mike BatesChief, Air Division

ARKANSAS DEPARTMENT OF ENVIRONMENTAL QUALITY5301 NORTHSHORE DRIVE / NORTH UTILE ROCK / ARKANSAS 72118-5317/ TELEPHONE 501-682-0744/ FAX 501-682-0880

www.odeq.stote.or.us

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RESPONSE TO COMMENTS

Quantum Resources Management, LLCWalker Creek Production Facility

DRAFT PERMIT #1126-AR-5AFIN: 14-00175

On October 21,2007, the Director of the Arkansas Department of Environmental Qualitygave notice of a draft permitting decision for the above referenced facility. During thecomment period C-K Associates, LLC of Louisiana, on the behalf of Walker CreekProduction Facility, submitted comments, data, views or arguments on the draftpermitting decision. The Department's response to these issues follows.

Issue #1:

One commenter expressed concerns about Specific Conditions #12 and #17, pertaining tothe facility's requirement for monthly VOC monitoring as required by Standards forPerformance for New Stationary Sources Subpart KKK and requested these conditions beremoved from the permit.

Response #1:

The facility is a non-fractioning plant, but no longer has the design capacity to process 10MMSCFD. Routine monitoring requirements of §60.482-2(a)(l), §60.482-7(a), and§60.633(b)(l) are not required by facilities that do not have the design capacity to process10 MMSCFD. Therefore, Specific Conditions # 12 and #17 have been removed from thepermit.

Issue #2:

It was requested that the Amine Reboiler (SN-2I) be included III the InsignificantActivities list rather than included as a permitted source.

Response #2:

Based on the information provided in the application, the size of the Amine Reboiler, theestimated emissions generated by the reboiler, and the aggregate emissions of all unitsclassified as insignificant are below the requirements of Group A-I. Therefore, theAmine Reboiler has been added to the Insignificant Activities list under Group A-I andSN-2I has been removed from the permit.

m Facility

............................................... 3

............................................... 4

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.............................................. 16

.............................................. 17

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.............................................. 23

.ene Glycol (TEG) Dehydration Unit and a TEG Reboiler

'ovided, emissions from the TEG Dehydrator and thes classified as insignificant are below the requirements ofsize TEG Reboiler, the estimated emissions generated byemissions of all units classified as insignificant are belowI. Therefore, the TEG Dehydrator and the TEG Reboiler.ificant Activities list under Group A-I3 and Group A-I,

Quantum Resources Management, LLC - Walker Creek Production FacilityPermit # 1126-AR-5AFIN: 14-00175

Section I: FACILITY INFORMATION

PERMITTEE: Quantum Resources Management, LLCWalker Creek Production Facility

AFIN: 14-00175

PERMIT NUMBER: 1126-AR-5

FACILITY ADDRESS: State Highway 132Taylor, AR 71618

COUNTY: Columbia

CONTACT PERSON: Brad M. Rogers

CONTACT POSITION Environmental, Health & Safety Supervisor

TELEPHONE NUMBER: 303-815-1495

REVIEWING ENGINEER: Joseph Hurt

VTM North-South (Y): Zone 15, 3659905

VTM East-West (X): Zone 15,457013

3

Quantum Resources Management, LLC - Walker Creek Production FacilityPermit # I126-AR-5AFIN: 14-00175

Section II: INTRODUCTION

Summary

Quantum Resources Management, LLC (Quantum) owns and operates the Walker CreekProduction Facility, Crude Petroleum and Natural Gas Extraction (NAICS Code 211112 ),located off Arkansas State Highway 132 and 3.5 miles South of Taylor, Arkansas, inColumbia County. With this modification, Quantum would like to remove the 840 hpF3524GSI compressor engine (SN-15) from service and install one (I) Waukesha F3521Gcompressor engine (SN-20) rated at 445 hp and equipped with a catalytic converter.Additionally, Quantum submitted updated calculations for the 415 HP Caterpillar G370Engine (SN-16), which reduced the permitted Formaldehyde emissions from 0.41 Iblhr to0.07 lb/hr. Quantum would also like to add an amine reboiler, a Triethylene Glycol (TEG)dehydrator, and a TEG reboiler to the Insignificant Activities. With the modificationsproposed the total permitted emissions increases include 0.1 tpy of PM 10 and 0.1 tpy of S02,with permitted emission decreases of 0.8 tpy ofVOC, 15.8 tpy of CO, and 7.7 tpy of NO,.

Process Description

The low pressure liquids from the oil and gas wells are delivered to an inlet separator, then pipedthrough a 400 barrel intermediate Holding Tank and a 750 barrel Gunbarrel. The crude oil fromthe Gunbarrel is routed to one of the three 750 bbl storage tanks and pumped to the crude oilsales point. Produced water is routed to two 750 bbl storage tanks and then pumped intoinjection wells or trucked to an off-site disposal well. Vapors from the storage tanks arerecovered and routed back to the separator. The field gas is then compressed to a dischargepressure ranging from 600 to 950 psig by using the 840 HP Waukesha F3524 GSI compressor.

Compressed gas is passed through an H2S Treating Tower and then to the Gas Processing Unitwhere water and liquid hydrocarbons are removed. The liquid hydrocarbons are sent to aStabilizer Tower and then to a 30,000 gallon storage tank. Processed gas is metered and eithersold or re-injected into the Walker Creek Unit (WCU) formation.

The natural gas is then dehydrated by contact with Ethylene Glycol. The wet glycol solution isre-generated in a natural gas fired reboiler (SN-17-GD3) rated at 1.2 MMBTU/hr. Gases ventedfrom the Dehydrator Still Column vent, previously designated as SN-12, are estimated at 5.0 tpyof VOCs, including 1.0 tpy of BTEX HAPs, and this source is now designated as SN-18-GD4.

The refrigeration plant has a 415 HP Caterpillar G379 SI NA compressor engine with a catalyticconverter (SN-CE6) which follows H2S treating. Fugitive VOC emissions from the refrigerationunit (SN-19-F2) are estimated at 35 tpy.

4

Quantum Resources Management, LLC - Walker Creek Production FacilityPermit # 1126-AR-5AFTN: 14-00175

Regulations

The following table contains the regulations applicable to this permit.

Source No. Regulation Citations

FacilityArkansas Air Pollution Control Code, Regulation 18, effective FebruaryIS, 1999

FacilityRegulations of the Arkansas Plan ofImplementation for Air PollutionControl, Regulation 19, effective October IS, 2007

Facility & 40 CFR 60 Subpart KKK - Standards ofPerformance for Equipment LeaksSN-19 of VOCfrom Onshore Natural Gas Processing Plants

Facility & 40 CFR 60 Subpart VV - Standards ofPerformance for Equipment LeaksSN-19 of VOC in Synthetic Organic Chemicals Manufacturing Industry

Emissions

The following table is a summary of the facility's total emissions. The table, in itself is not anenforceable condition of the permit.

Table 1 - Total Allowable Emissions

Total Allowable EmissionsEmissions Rates

PollutantIb/hr tpy

PM 0.2 0.4PM\o 0.2 0.4

S0 2 0.2 0.2VOC 13.6 57.0CO 4.1 17.4NOx 4.0 17.2

Acetaldehyde* 0.02 0.08Acrolein* 0.02 0.05Benzene* 0.23 0.98

Formaldehyde" 0.12 0.49Methanol* 0.02 0.09Toluene* 0.01 0.01

*Hazardous AIr Pollutants (HAPs) are included 111 VOC totals.

5


Section III: PERMIT HISTORY

Permit # 1126-AR-A was issued to ARCO Oil and Gas on February 26, 1991 for theconstruction ofa central oil and gas producing plant located 3.5 miles South of Taylor,Columbia County, AR. The facility consisted of the following emission sources: three 1500 HPengines and compressors (SN-Ol through SN-03) equipped with catalytic converters, two 300HP internal combustion engines not equipped with a catalytic converter, one 1.2 M MBTU/hI'Triethylene Glycol (TEG) dehydrator, five 1000 barrel storage tanks, and a 1.2 MMBTU/hr TEGdehydrator equipped with an overhead vapor condenser-cooler.

Pel111it # 1126-AR-l was issued on March 10, 1993 following stack testing performed at the site,The facility consisted of the following emission sources: three 1500 HP engines andcompressors (SN-Ol through SN-03) equipped with catalytic converters, one 300 HP and one800 HP internal combustion engine not equipped with catalytic converters, one 1.2 MMBTU/hrTriethylene Glycol (TEG) dehydrator, six 1000 barrel storage tanks, and a 1.2 MMBTU/hr TEGdehydrator equipped with an overhead vapor condenser-cooler

Pellnit # 1126-AR-2 was issued on December 16,1994: This permit listed the followingsignificant sources: three 1500 HP engines and compressors (SN-Ol through SN-03) equippedwith catalytic converters, and a 300 HP engine with a catalytic converter. The addition of thecatalytic converter reduced the NOx emission rate from 202.3 tpy to below the threshold thatwould require a Title V application. Formaldehyde, a Hazardous Air Pollutant, is also producedin the combustion of natural gas in the compressor engines, and these estimates have been addedto the current revised emission estimates. Formaldehyde is emitted at less than 10 tpy,

Permit # 1126-AR-3 was issued on March 26, 1998 by the owner Vastar Resources, Inc. in orderto add a refrigeration plant and simultaneously eliminate one compressor (SN-4-CE-4), so thatNOx and CO emissions rates will be kept below the permitted levels at 96 tpy each. PermittedVOC emissions, however, increased from 33.2 tpy to 64.3 tpy. Four new sources of emissionswere added in the permit application: 1) a Caterpillar G370 natural gas engine to be used in therefrigeration plant; 2) an external combustion source for the ethylene glycol regenerator in therefrigerator plant; 3) fugitives from the refrigeration plant; and 4) emissions from the ethyleneglycol still column.

Interim authority to construct and operate a refrigeration plant was granted on April 14, 1998,after a teclmical review indicated that the changes proposed in the permit application met therequired criteria. The new refrigeration plant included a 415 HP Caterpillar G379 SI NAcompressor engine with a catalytic converter (SN-CE6) which follows H2S treating. Also 35tpy ofVOCs were identified as fugitives from the operation of the refrigeration unit (SN-F2).

Permit # 1126-AR-4 was issued on March 4, 2005. The modification resulted in a netreduction in facility wide permitted emission limits for NOx @ 70.4 tpy and CO @ 62.3 tpy.

Gruy removed the three (3) 1500 Hp compressor engines designated as SN-OI, 02 & 03, and

6

Quantum Resources Management, LLC - Walker Creek Production FacilityPermit # 1126-AR-5AFTN: 14-00175

installed one (1) 840 Hp Waukesha F3524GSI compressor engine SN-15. The facility stillconsists of the following: one (1) 415 Hp refrigeration compressor engine (SN-16-CE6), six (6)750 barrel stock tanks (SN-05 through SN-IO), one (1) 400 barrel holding tank (SN-14), one (1)ethylene glycol dehydrator reboiler (SN-17-GD3), ethylene glycol dehydrator reboiler vent (SN18-GD4), tank truck loading (SN-13, TL-I), and refrigeration plant fugitive emissions (SN-19F2).

7

Quantum Resources Management, LLC - Walker Creek Production FacilityPermit # I I26-AR-5AFIN: 14-00175

Section IV: EMISSION UNIT INFORMATION

Specific Conditions

I. The permittee will not exceed the emission rates set forth in the following table. Thepermittee will demonstrate compliance with this Specific Condition by using pipeline qualitynatural gas as a fuel for sources SN-16 and SN-17, and operating these sources at or lessthan capacity. Compliance with emission rates set forth in the following table for fugitivesource (SN-19) shall be demonstrated by compliance with Specific Conditions 10 through23. [§19.501 et seq. of the Regulations of the Arkansas Plan ofImplementation for AirPollution Control, effective October 15, 2007 (Regulation 19) and A.C.A. §8-4-203 asreferenced by §8-4-304 and §8-4-311]

Table 2 - Criteria Pollutants

SN Description Control Equipment Pollutant Ib/hr Tpy

01 Engine #I-Removed from Facility02 Engine #2-Removed from Facility03 Engine #3-Removed from Facility04 No longer in service05 Crude Oil Storage Tank #1 Vapor Recovery Unit VOC 0.1 0.406 Crude Oil Storage Tank #2 Vapor Recovery Unit VOC 0.1 0.407 Crude Oil Storage Tank #3 Vapor Recovery Unit VOC 0.1 0.408 Crude Oil Storage Tank #4 Vapor Recovery Unit VOC 0.1 0.4

09Crude Oil and Saltwater

Vapor Recovery Unit VOC 0.1 0.4Storage tank #5

10 Crude Oil Storage Tank #6 Vapor Recovery Unit VOC 0.1 0.411 Replaced with SN-GD3 (SN-17)12 Replaced with SN-GD4 (SN-18)13 Tank Truck Loading Vapor Recovery Unit VOC 0.1 0.114 400 barrel oil storage tank Vapor Recovery Unit VOC 0.1 0.115 Removed from service in 2007

PM 10 0.1 0.2

415 HP Caterpillar G370S02 0.1 0.1

16 Catalytic Converter VOC 0.2 0.5Engine

CO 2.0 8.6NOx 1.8 7.9

Ethylene Glycol Flue Gas Stack VOC 0.1 0.117 (1.2 MMBtu/hr Natural gas None CO 0.1 0.2

fired reboiler rated) NOx 0.2 0.7

18Ethylene Glycol Dehydrator

None VOC 1.2 5.1Still Column Vent

8

Quantum Resources Management, LLC - Walker Creek Production FacilityPe1111it # I I26-AR-5AFIN: 14-00175

SN Description Control Equipment Pollutant Ib/hr Tpy

19Facility (Fl) and Refrigeration

None VOC 11.0 47.8Plant (F2) Fugitives

PM 10 0.1 0.2

445 HP Waukesha F3521GS02 0.1 0.1

20Compressor Engine

Catalytic Converter VOC 0.3 0.9CO 2.0 8.6NOx 2.0 8.6

2. The permittee will not exceed the emission rates set forth in the following table. Thepermittee will demonstrate compliance with this condition by using pipeline quality naturalgas as a fuel for source SN-16 and operating the source at or less than capacity. [§18.801 ofthe Arkansas Air Pollution Control Code, effective February 15, 1999 (Regulation 18) andA.C.A. §8-4-203 as referenced by §8-4-304 and §8-4-311]

Table 3 - Non-Criteria Pollutants

SN Description Pollutant Ib/hr tpy

15 Removed from service in 2007PM 0.1 0.2

Acetaldehyde 0.01 0.04

415 HP CaterpillarAcrolein 0.01 0.04

16 Benzene 0.01 0.03G370 Engine

Formaldehyde 0.07 0.28Methanol am 0.05Toluene 0.01 0.01

Ethylene Glycol18 Dehydrator Still Benzene 0.21 0.93

Column VentPM 0.1 0.2

445 HP WaukeshaAcetaldehyde 0.01 0.04

Acrolein 0.01 0.0120 F3521G Compressor

Benzene 0.01 0.02Engine

Formaldehyde 0.05 0.21Methanol 0.01 0.04

9


3. The permittee shall only use pipeline quality natural gas to fire all combustion sources (SN16, SN-17, SN-18, & SN-20) located at this facility. Pipeline quality natural gas is definedas a natural gas which contains 0.5 grains or less of total sulfur per 100 standard cubic feet,and pipeline natural gas must either be composed of at least 70 percent methane by volumeor has a gross calorific value between 950 and 1100 Btu per standard cubic foot. Compliancewith this condition may be demonstrated by a valid gas tariff, purchase contract, fuelanalysis or other appropriate documentation. [A.CA. §8-4-203 as referenced by A.CA. §84-304 and §8-4-311, and 40 CFR 70.6 and 40 CFR 72.2].

4. Visible emissions will not exceed the limits specified in the following table of this permit asmeasured by EPA Reference Method 9. [A.CA. §8-4-203 as referenced by §8-4-304 and§8-4-311]

Table 4 - Visible Emissions

SN Limit Regulatory CitationPlant-wide 5% §18.501

5. The permittee will not cause or permit the emission of air contaminants, including odors orwater vapor and including an air contaminant whose emission is not otherwise prohibited byRegulation #18, if the emission of the air contaminant constitutes air pollution within themeaning of A.C.A. §8-4-303. [§18.801 of Regulation 18, and A.CA. §8-4-203 asreferenced by §8-4-304 and §8-4-31]

6. The permittee will not conduct operations in such a manner as to unnecessarily cause aircontaminants and other pollutants to become airborne. [§ 18.90 I 0 f Regulation 18, andA.CA. §8-4-203 as referenced by §8-4-304 and §8-4-311]

7. The permittee will maintain monthly records which demonstrate compliance with SpecificCondition #3. The permittee will update the records by the fifteenth day of the monthfollowing the month to which the records pertain. The permittee will maintain the recordsonsite, and make the records available to Department personnel upon request. [§ 19.705 ofRegulation 19 and A.C.A. §8-4-203 as referenced by §8-4-304 and §8-4-311]

8. The permittee shall conduct tests for CO and NOx on compressor engines SN-16 and SN-20in accordance with General Condition #7 and every five years thereafter. EPA ReferenceMethod 7E shall be used to determine NOx and EPA Reference Method 10 shall be used todetermine CO. The permittee shall test the engine within 90% of its rated capacity. If theengine is not tested within this range, the permittee shall be limited to operating within 10'%above the tested rate. The department reserves the right to select the engine to be tested.[Pursuant to §19.702 of Regulation 19 and 40 CFR Part 52, Subpart E]

10

Quantum Resources Management, LLC - Walker Creek Production FacilityPermit # 1126-AR-5AFIN: 14-001 75

9. The permittee shall document the elapsed time of any release (emergency or not; includingblowdowns) and the resulting amount ofVOCs that are released. [A.C.A.§8-4-203 asreferenced by §8-4-304, §8-4-311 and 40 CFR 70.6]

NSPS Requirements: Refrigeration Plant and Facility Fugitive Emissions (SN-19)

SN-19 is a compilation of fugitive emissions from the refrigeration plant and facility equipmentsuch as compressors, pumps, valves and connections.

10. The permittee shall demonstrate compliance with applicable standards for each pump,pressure relief device, sampling connection system, open-ended valve or line, valves ingas/vapor service and light liquid service, and flange or other connector in VOC service andany devices or systems required by Subpart VV §60.482-1 to §60.482-1 0 as required bySubpart KKK within 180 days of the initial startup of the equipment. Compliance with therequired standards shall be determined by a review of records and reports, review ofperformance test results, and inspection using the methods and procedures specified in§60.485. Refer to Appendix A and B. [40 CFR 60, Subpart VV §60.482-l as referenced bySubpart KKK]

11. Reciprocating compressors at this facility are exempt from the requirements of 40 CFR 60,Subpart VV §60.482-3. However, as specified by the recordkeeping requirements of§60.635(c), the facility shall record in a log that is kept readily accessible, information anddata used to demonstrate that a reciprocating compressor is in wet gas service and istherefore exempted from other requirements. [40 CFR 60, Subpart KKK §60.633(f)]

12. Pressure relief devices in gas/vapor service shall follow the operation and monitoringstandards of §60.482-4 with the exceptions of §60.633. [40 CFR 60, Subpart VV andSubpart KKK]

13. Sampling connection systems are exempt from the requirements of Subpart VV §60.482-5.[40 CFR 60, Subpart KKK §60.633]

14. Open-ended valves or lines shall be equipped and operated as required by §60.482-6. [40CFR 60, Subpart VV as referenced by Subpart KKK]

15. Pumps and valves in heavy liquid service, pressure relief devices in light liquid or heavyliquid service, and flanges and other connectors shall be monitored and repaired as requiredby §60.482-8. [40 CFR 60, Subpart VV as referenced by Subpart KKK]

11


16. Closed vent systems and control devices shall comply with the provisions of 40 CFR 60,Subpart VV §60.482-1O. The vapor recovery systems and combustion devices shall bedesigned to recover VOC's at :0:95% efficiency. These closed vent systems and controldevices shall be operated and maintained in accordance with design specifications and keptin good working order at all times. These systems and devices shall be operated at all timeswhen emissions may be vented to them. The facility shall also record and keep in a readilyaccessible location the information required in the reporting requirements of §60.486(d).[40 CFR 60, Subpart VV as referenced by Subpart KKK]

17. Closed vent systems shall be designed and operated with no detectable emissions. Within 60days of achieving the maximum production rate, but not later than 180 days of the startup ofthe affected equipment, the performance tests required in §60.l8 and §60.485 shall beconducted. This testing shall be repeated on an annual basis. [40 CFR 60, Subpart VV§60.482-l0 (f) as referenced by Subpart KKK]

18. All of the sources contained in the Production Facility as fugitive emissions (SN-19) aresubject to the recordkeeping requirements of §60.486. For each leak detected, the facilityshall perform the following: [40 CFR 60, Subpart VV as referenced by Subpart KKK]

a. Attach a readily visible, waterproof identification marked with the equipmentidentification number to the leaking equipment

b. Record the following information in a log to be kept for 2 years in a readily accessiblelocation:

I. The instrument and operator identification numbers and the equipmentidentification number.

11. The date the leak was detected and the dates of each attempt to repair the leak.

111. Repair methods applied in each attempt to repair the leak.

IV. "Above 10,000" if the maximum instrument reading measured by the methodsspecified in §60.485(a) after each repair attempt is equal to or greater than 10,000ppm.

v. "Repair delayed" and the reason for the delay if a leak is not repaired within 15calendar days after discovery of the leak.

VI. The signature of the owner or operator or designate whose decision it was that therepair could not be effected without a process shutdown.

VII. The expected date of successful repair of the leak if a leak is not repaired within15 days.

12

Quantum Resources Management, LLC - Walker Creek Production FacilityPermit # 1126-AR-5AFIN: 14-001 75

vui, Dates of process unit shutdowns that occur while the equipment is unrepaired.

IX. The date of successful repair of the leak

The facility shall also record and keep in a readily accessible location the informationrequired in the reporting requirements of§ 60.486(e).

19. In addition to the recordkeeping requirements of 40 CFR 60, Subpart VV §60.486 thefacility is subject to the recordkeeping requirements of §60.635. For all pressure reliefdevices subject to §60.633(b)(l), the following shall apply: [40 CFR 60, Subpart KKK]

a. When a leak is detected, a readily visible, weatherproof identification, marked with theequipment ill number shall be attached to the leaking equipment.

b. When each leak is detected, the following information shall be recorded in a log and keptfor 2 years in a readily accessible location:

I. The instrument and operator identification numbers and the equipmentidentification number.

11. The date the leak was detected and the dates of each attempt to repair the leak.

111. Repair methods applied in each attempt to repair the leak.

IV. "Above 10,000 ppm" if the maximum instrument reading measured after eachrepair attempt is 10,000 ppm or greater.

v. "Repair delayed" and the reason for the delay if a leak is not repaired within 15calendar days after the discovery of the leak.

VI. The signature of the owner or operator or designate whose decision it was thatrepair could not be effected without a process shutdown.

VII. The expected date of successful repair of the leak if a leak is not repaired within15 days.

Vlll. Dates of process unit shutdowns that occur while the equipment is unrepaired,

IX. The date of successful repair of the leak.

x. A list of identification numbers for equipment that are designated for nodetectable emissions. This designation shall be signed by the owner or operator.

13


20. Each owner or operator subject to the provisions of this subpart shall submit an initial reportand semiannual reports to the Department beginning six months after the initial startup date.[Recordkeeping requirements of 40 CFR 60, Subpart VV §60.487 as referenced by SubpartKKK]

The initial report shall include:

a. Process unit identification.

b. Number of valves subject to §60.482-7 including the valves exempted in §60.482-7(f).

c. Number of pumps subject to the requirements of§60.482-2.

d. Number of compressors subject to §60.482-3.

All semi-annual reports to the Department shall include the following information:

a. Process unit identification.

b. For each month during the semiannual period,

1. Number of valves for which leaks were detected.

11. Number of valves for which leaks were not repaired as required.

111. Number of pumps for which leaks were detected.

IV. Number of pumps for which leaks were not repaired as required.

v. Number of compressors for which leaks were detected.

VI. Number of compressors for which leaks were not repaired as required.

Vll. The facts that explain each delay of repair, and where appropriate, why a processunit shutdown was technically infeasible.

c. Dates of process unit shutdowns which occurred within the semiannual reporting period.

d. Revisions to items reported in the initial report if changes have occurred since the initialreport or subsequent revisions to the initial report.

14


21. In addition to the reporting requirements of 40 CFR 60, Subpart VV §60.487 the facility issubject to the reporting requirements of§60.636. An owner or operator shall include thefollowing information in the initial semiannual report: [Reporting requirements of 40 CFR60, Subpart KKK]

a. Number of pressure relief devices subject to the requirements of§60.633(b) except those exempted as described in §60.636(b).

In addition to the information required in §60.487(c)(2)(i) through (vi), the owner oroperator shall include, in all semiannual reports, in accordance with General Condition#6, the following information:

a. Number of pressure relief devices for which leaks were detected.

b. Number of pressure relief devices for which leaks were not repaired asrequired.

15

Quantum Resources Management, LLC - Walker Creek Production FacilityPermit # I126-AR-5AFIN: 14-00175

Section V: INSIGNIFICANT ACTIVITIES

The Department deems the following types of activities or emissions as insignificant on thebasis of size, emission rate, production rate, or activity in accordance with Group A of theInsignificant Activities list found in Regulation 18 and 19 Appendix A. Insignificant activityemission determinations rely upon the information submitted by the permittee in an applicationdated August J2, 2004, and electronic mail dated September 7, 2004, and based on commentssubmitted November J5, 2007.

Table 5 - Insignificant Activities

Description CategoryMethanol Tank, 500 gallons A-13

Triethylene Glycol Tank, 500 gallons A-3Glycol-amine Tank, 500 gallons A-3

Detergent Tank, 250 gallons A-2Triethylene Glycol (TEG) Dehydrator with a 4015 PV Kimray pump A-13

TEG Reboiler (0.1 MMBtulhr natural gas fired) A-IAmine Reboiler (1.0 MMBtulhr natural gas fired) A-I

16


Section VI: GENERAL CONDITIONS

I. Any terms or conditions included in this permit that specify and reference ArkansasPollution Control & Ecology Commission Regulation 18 or the Arkansas Water and AirPollution Control Act (AC.A §8-4-101 et seq.) as the sole origin of and authority for theterms or conditions are not required under the Clean Air Act or any of its applicablerequirements, and are not federally enforceable under the Clean Air Act. Arkansas PollutionControl & Ecology Commission Regulation 18 was adopted pursuant to the Arkansas Waterand Air Pollution Control Act (AC.A §8-4-101 et seq.). Any terms or conditions includedin this permit that specify and reference Arkansas Pollution Control & Ecology CommissionRegulation 18 or the Arkansas Water and Air Pollution Control Act (AC.A §8-4-101 etseq.) as the origin of and authority for the terms or conditions are enforceable under thisArkansas statute.

2. This permit does not relieve the owner or operator of the equipment and/or the facility fromcompliance with all applicable provisions of the Arkansas Water and Air Pollution ControlAct and the regulations promulgated under the Act. [AC.A §8-4-203 as referenced byAC.A. §8-4-304 and §8-4-311]

3. The permittee will notify the Department in writing within thirty (30) days aftercommencement of construction, completion of construction, first operation of equipmentand/or facility, and first attainment of the equipment and/or facility target production rate.[§19.704 of the Regulations of the Arkansas Plan of Implementation for Air PollutionControl (Regulation 19) and/or A.C.A. §8-4-203 as referenced by AC.A §8-4-304 and§8-4-311 ]

4. Construction or modification must commence within eighteen (18) months from the date ofpermit issuance. [§19.410(B) of Regulation 19 and/or §18.309(B) of the Arkansas AirPollution Control Code (Regulation 18) and AC.A §8-4-203 as referenced byA.C.A. §8-4-304 and §8-4-311]

5. The permittee must keep records for five years to enable the Department to determinecompliance with the terms of this permit; such as hours ofoperation, throughput, upsetconditions, and continuous monitoring data. The Department may use the records, at thediscretion of the Department, to determine compliance with the conditions of the permit.[§19.705 of Regulation 19 and/or §18.1004 of Regulation 18 and AC.A §8-4-203 asreferenced by A.C.A §8-4-304 and §8-4-311]

6. A responsible official must certify any reports required by any condition contained in thispermit and submit any reports to the Department at the address below. [§19.705 ofRegulation 19 and/or §18.1004 of Regulation 18 and A.C.A. §8-4-203 as referenced byA.C.A. §8-4-304 and §8-4-311]

17


Arkansas Department of Environmental QualityAir DivisionATTN: Compliance Inspector Supervisor5301 Northshore DriveNorth Little Rock, AR 72118

7. The permittee will test any equipment scheduled for testing, unless stated in the SpecificConditions of this permit or by any federally regulated requirements, within the followingtime frames: (1) newly constructed or modified equipment within sixty (60) days ofachieving the maximum production rate, but no later than 180 days after initial start-up ofthe permitted source or (2) existing equipment already operating according to the timeframes set forth by the Department. The permittee must notify the Department of thescheduled date of compliance testing at least fifteen (15) days in advance of such test. Thepermittee must submit compliance test results to the Department within thirty (30) days afterthe completion of testing. [§19.702 of Regulation 19 and/or §18.1002 of Regulation 18 andAC.A. §8-4-203 as referenced by A.CA. §8-4-304 and §8-4-311]

8. The permittee will provide: [§19.702 of Regulation 19 and/or §18.1002 of Regulation 18and A.CA §8-4-203 as referenced by A.CA. §8-4-304 and §8-4-3l1]

a. Sampling ports adequate for applicable test methods;

b. Safe sampling platforms;

c. Safe access to sampling platforms;

d. Utilities for sampling and testing equipment.

9. The permittee will operate equipment, control apparatus and emission monitoring equipmentwithin their design limitations. The permittee will maintain in good condition at all timesequipment, control apparatus and emission monitoring equipment. [§19.3030fRegulation19 and/or §18.1104 of Regulation 18 and A.CA §8-4-203 as referenced byACA. §8-4-304 and §8-4-311]

10. If the permittee exceeds an emission limit established by this permit, the permittee will bedeemed in violation of said permit and will be subject to enforcement action. TheDepartment may forego enforcement action for emissions exceeding any limits establishedby this permit provided the following requirements are met: [§19.601 of Regulation 19and/or §18.1101 of Regulation 18 and A.C.A. §8-4-203 as referenced by ACA. §8-4-304and §8-4-311]

a. The permittee demonstrates to the satisfaction of the Department that the emissionsresulted from an equipment malfunction or upset and are not the result of negligence orimproper maintenance, and the permittee took all reasonable measures to immediatelyminimize or eliminate the excess emissions.

18


b. The permittee reports the occurrence or upset or breakdown of equipment (by telephone,facsimile, or overnight delivery) to the Department by the end of the next business dayafter the occurrence or the discovery ofthe occurrence.

c. The permittee must submit to the Department, within five business days after theoccurrence or the discovery of the occurrence, a full, written report of such occurrence,including a statement of all known causes and of the scheduling and nature of the actionsto be taken to minimize or eliminate future occurrences, including, but not limited to,action to reduce the frequency of occurrence of such conditions, to minimize the amountby which said limits are exceeded, and to reduce the length of time for which said limitsare exceeded. If the information is included in the initial report, the information need notbe submitted again.

11. The permittee will allow representatives of the Department upon the presentation ofcredentials: [A.CA. §8-4-203 as referenced by A.c.A. §8-4-304 and §8-4-31I ]

a. To enter upon the permittee's premises, or other premises under the control of thepermittee, where an air pollutant source is located or in which any records are required tobe kept under the terms and conditions of this permit;

b. To have access to and copy any records required to be kept under the terms andconditions of this permit, or the Act;

c. To inspect any monitoring equipment or monitoring method required in this permit;

d. To sample any emission of pollutants; and

e. To perform an operation and maintenance inspection of the permitted source.

12. The Department issued this permit in reliance upon the statements and presentations made inthe permit application. The Department has no responsibility for the adequacy or properfunctioning of the equipment or control apparatus. [A.c.A. §8-4-203 as referenced byA.CA. §8-4-304 and §8-4-311]

13. The Department may revoke or modify this permit when, in the judgment of the Department,such revocation or modification is necessary to comply with the applicable provisions of theArkansas Water and Air Pollution Control Act and the regulations promulgated the ArkansasWater and Air Pollution Control Act. [§19.410(A) of Regulation 19 and/or §18.309(A) ofRegulation 18 and A.C.A. §8-4-203 as referenced by A.CA. §8-4-304 and §8-4-311]

14. This permit may be transferred. An applicant for a transfer must submit a written request fortransfer of the pennit on a form provided by the Department and submit the disclosurestatement required by Arkansas Code Annotated §8-1-1 06 at least thirty (30) days in advanceof the proposed transfer date. The permit will be automatically transferred to the newpermittee unless the Department denies the request to transfer within thirty (30) days of the

19


receipt of the disclosure statement. The Department may deny a transfer on the basis of theinformation revealed in the disclosure statement or other investigation or, deliberatefalsification or omission of relevant information. [§19.407(B) of Regulation 19 and/or§ 18.307(B) of Regulation 18 and ACA §8-4-203 as referenced by ACA §8-4-304 and§8-4-311 ]

15. This permit shall be available for inspection on the premises where the control apparatus islocated. [A.C.A. §8-4-203 as referenced by A.CA. §8-4-304 and §8-4-311]

16. This permit authorizes only those pollutant emitting activities addressed herein.[A.CA §8-4-203 as referenced by §8-4-304 and §8-4-311]

17. This permit supersedes and voids all previously issued air permits for this facility.[Regulation 18 and 19 and ACA §8-4-203 as referenced by §8-4-304 and §8-4-311]

18. The permittee must pay all permit fees in accordance with the procedures established inRegulation No.9. [A.C.A §8-1-105(c)]

19. Pursuant to §19.702 of Regulation 19 and/or §18.1002 of Regulation 18 and A.CA. §8 4203 as referenced by A.CA. §8-4-304 and §8-4-311, any equipment that is to be tested,unless stated in the Specific Conditions of this permit or by any federally regulatedrequirements, shall be tested with the following time frames: (1) Equipment to beconstructed or modified shall be tested within ninety (90) days of achieving the maximumproduction rate, but in no event later than 180 days after initial start up of the permittedsource or (2) equipment already operating shall be tested according to the time frames setforth by the Department or within 90 days of permit issuance if no date is specified. Thepermittee shall notify the Department of the scheduled date of compliance testing at leastfifteen (15) days in advance of such test. Compliance test results shall be submitted to theDepartment within thirty (30) days after the completed testing.

20. Pursuant to §19.7 of Regulation 19 and 40 CFR Part 52, Subpart E, the permittee shallsimultaneously conduct tests for CO and NOx on the compressor engine (SN-O1) inaccordance with plantwide condition SC # 7 and every five years thereafter. EPA ReferenceMethod 7E shall be used to determine NOx and EPA Reference Method 10 shall be used todetermine CO. The permittee shall test the engines within 90% of their rated capacity. If thetests are not performed within this range, the permittee shall be limited to operating within10% above the tested rate.

21. Pursuant to § 19.7 of Regulation 19,40 CFR Part 52, Subpart E, and A.CA. §8-4-203 asreferenced by §8-4-304 and §8-4-311, each emission point for which an emission testmethod is specified in this permit shall be tested in order to determine compliance with theemission limitations contained herein within sixty (60) days of achieving the maximumproduction rate, but in no event later than 180 days after initial start-up of the permittedsource. The permittee shall notify the Department of the scheduled date of compliancetesting at least fifteen (15) days in advance of such test. Compliance test results shall be

20


submitted to the Department within thirty (30) days after the completed testing. Thepermittee shall provide:

(1) Sampling ports adequate for applicable test methods(2) Safe sampling platforms(3) Safe access to sampling platforms(4) Utilities for sampling and testing equipment

21

APPENDIX A

40 CFR60 Subpart KKKStandards ofPerformance for Equipment Leaks of VOCfrom Onshore Natural Gas Processing

Plants

§60.630

SUbpart KKK-Standards of Performance for EquipmentLeaks of VOC From OnshoreNatural Gas ProcessingPlants.

SOURCE: 50 FR 26124, June 24. 1985. unlessotherwise noted.

§ 60.630 Applicability and designationof affected facility.

(a)(l) The provisions of this subpartapply to affected facilities in onshorenatural gas processing plants.

(2) A compressor in VOC service or inwet gas service is an affected facility.

(3) The group of all equipment exceptcompressors (definied in §60.631) withina process unit is an affected facility.

(b) Any affected facility under paragraph (a) of this section that commences construction. reconstruction,or modification after January 20, 1984,is subject to the requirements of thissubpart.

(c) Addition or replacement of equipment (defined in §60.63l) for the purpose of process improvement that is accomplished without a capital expenditure shall not by itself be considered amodification under this subpart.

(d) Facilities covered by subpart VVor subpart GGG of 40 CFR part 60 areexcluded from this subpart.

(e) A compressor station, dehydration unit, sweetening unit, underground storage tank, field gas gathering system, or liquefied natural gasunit is covered by this subpart if it islocated at an onshore natural gas processing plant. If the unit is not locatedat the plant site, then it is exemptfrom the provisions of this subpart.

§ 60.631 Definitions.As used in this subpart, all terms not

defined herein shall have the meaninggiven them in the Act, in subpart A orsubpart VV of part 60; and the following terms shall have the specificmeanings given them.

Alaskan North Slope means the approximately 69,000 square-miie area extending from the Brooks Range to theArctic Ocean.

Equipment means each pump. pressure relief device, open-ended valve orline, vaive, compressor, and flange or

40 CFR Ch. I (7-1-06 Edition)

other connector that is in VOC serviceor in wet gas service, and any device orsystem required by this subpart.

Field gas means feedstock gas entering the natural gas processing plant.

In light liquid service means that thepiece of equipment contains a liquidthat meets the conditions specified in§60.485(e) or §60.633(h)(2).

In wet gas service means that a pieceof equipment contains or contacts thefield gas before the extraction step inthe process.

Natural gas liquids means the hydrocarbons, such as ethane, propane, butane, and pentane, that are extractedfrom field gas.

Natural gas processing plant (gasplant) means any processing site engaged in the extraction of natural gasliquids from field gas, fractionation ofmixed natural gas liquids to naturalgas products, or both.

Non[ractionating plant means any gasplant that does not fractionate mixednatural gas liquids into natural gasproducts.

Onshore means all facilities exceptthose that are located in the territorialseas or on the outer continental shelf.

Process unit means equipment assembled for the extraction of natural gasliquids from field gas, the fractionationof the liquids into natural gas products, or other operations associatedwith the processing of natural gasproducts. A process unit can operateindependently if supplied with sufficient feed or raw materials and sufficient storage faclllties for the products.

Reciprocating compressor means apiece of equipment that increases thepressure of a process gas by positivedisplacement, employing linear movement of the driveshaft.

§ 60.632 Standards.(a) Each owner or operator subject to

the provisions of this subpart shallcomply with the requirements of§§60.482-l (a), (b), and (d) and 60.482-2through 60.482-10, excep';; as provided in§60.633, as soon as practicable, but nolater than 180 days after initial startup.

(b) An owner or operator may electto compiy with the requirements of§§ 60.483-1 and 60.483-2.

552

Environmental Protection Agency

(c) An owner or operator may applyto the Administrator for permission touse an alternative means of emissionlimitation that achieves a reduction inemissions of vae at least equivalent tothat achieved by the controls requiredin this subpart. In doing so, the owneror operator shall comply with requirements of §60.634 of this subpart.

(d) Each owner or operator subject tothe provisions of this subpart shallcomply with the provisions of §60.485except as provided in §60.633(f) of thissubpart.

(e) Each owner or operator subject tothe provisions of this subpart shallcomply with the provisions of §§60.486and 60.487 except as provided in§§60.633, 60.635, and 60.636 of this subpart.

(f) An owner or operator shall use thefollowing provision instead of§60.485(d)(1): Each piece of equipment ispresumed to be in vae service or inwet gas service unless an owner or operator demonstrates that the piece ofequipment is not in vae service or inwet gas service. For a piece of equipment to be considered not in vae service, it must be determined that thevae content can be reasonably expected never to exceed 10.0 percent byweight. For a piece of equipment to beconsidered in wet gas service, it mustbe determined that it contains or contacts the field gas before the extractionstep in the process. For purposes of determining the percent vae content ofthe process fluid that is contained in orcontacts a piece of equipment, procedures that conform to the methods described in ASTM E16!}-63, 77, or 93,E168-67, 77, or 92, or E26o--n, 91, or 96(incorporated by reference as specifiedin §60.l7) shall be used.

[50 FR 26124, June 24, 1985, as amended at 65FR 61773, Oct. 17, 2000]

§ 60.633 Exceptions.(a) Each owner or operator subject to

the provisions of this subpart maycomply with the following exceptionsto the provisions of subpart vv.

(b)(l) Each pressure relief device ingas/vapor service may be monitoredquarterly and within 5 days after eachpressure release to detect leaks by themethods specified in §60.485(b) exceptas provided in §60.632(c), paragraph

§60.633

(b)(4) of this section, and §60.482-4 (a)through (c) of subpart vv.

(2) If an instrument reading of 10,000ppm or greater is measured, a leak isdetected.

(3)(i) When a leak is detected, it shallbe repaired as soon as practicable, butno later than 15 calendar days after itis detected, except as provided in§60.482-9.

(Ii) A first attempt at repair shall bemade no later than 5 calendar daysafter each leak is detected.

(4)(i) Any pressure relief device thatis located in a nonfractionating plantthat is monitored only by nonplantpersonnel may be monitored after apressure release the next time themonitoring personnel are on site, instead of within 5 days as specified inparagraph (b)(l) of this section and§60.482-4(b)(1) of subpart vv.

(ii) No pressure relief device described in paragraph (b)(4)(i) of thissection shall be allowed to operate formore than 30 days after a pressure release without monitoring.

(c) Sampling connection systems areexempt from the requirements of§60.482-5.

(d) Pumps in light liquid service,valves in gas/vapor and light liquidservice, and pressure relief devices ingas/vapor service that are located at anonfractionating plant that does nothave the design capacity to process283,200 standard cubic meters per day(scmd) (10 million standard cubic feetper day) or more of field gas are exempt from the routine monitoring requirements of §§ 60.482-2(a)(1) and60.482-7(a), and paragraph (b)(1) of thissection.

(e) Pumps in light liquid service,valves in gas/vapor and light liquidservice, and pressure relief devices ingas/vapor service wi thin a process uni tthat is located in the Alaskan NorthSlope are exempt from the routinemonitoring requirements of §§60.4822(a)(1), 60.482-7(a), and paragraph (b)(1)of this section.

(f) Reciprocating compressors in wetgas service are exempt from the compressor control requirements of §60.4823.

(g) Flares used to comply wi th thissubpart shall comply with the requirements of §60.18.

553

§60.634

(h) An owner or operator may use thefollowing provisions instead of§60.485(e):

(1) Equipment is in heavy liquid service if the weight percent evaporated is10 percent or less at 150°C (302 OF) asdetermined by ASTM Method D86-78,82, 90, 95, or 96 (incorporated by reference as specified in §60.17).

(2) Equipment is in light liquid service if the weight percent evaporated isgreater than 10 percent at 150°C (302OF) as determined by ASTM MethodD86-78, 82, 90, 95, or 96 (incorporated byreference as specified in §60.17).

[50 FR 26124. June 24. 1985, as amended at 51FR 2702, Jan. 21, 1986; 65 FR 61773, Oct. 17,2000]

§ 60.634 Alternative means of emissionlimitation.

(a) If, in the Administrator's judgment, an alternative means of emissionlimitation will achieve a reduction invac emissions at least equivalent tothe reduction in vac .emissionsachieved under any design, equipment,work practice or operational standard,the Administrator will publish, in theFEDERAL REGISTER a notice permittingthe use of that aiternative means forthe purpose of compliance with thatstandard. The notice may conditionpermission on requirements related tothe operation and maintenance of thealternative means.

(b) Any notice under paragraph (a) ofthis section shall be published onlyafter notice and an opportunity for apublic hearing.

(c) The Administrator will considerapplications under this section from either owners or operators of affected facilities, or manufacturers of controlequipment.

(d) The Administrator will treat applications under this section accordingto the following criteria, except incases where he concludes that othercriteria are appropriate;

(1) The applicant must collect, verifyand submit test data, covering a periodof at least 12 months, necessary to support the finding in paragraph (a) of thissection.

(2) If the applicant is an owner or operator of an affected facility, he mustcommit in writing to operate andmaintain the alternative means so as


to achieve a reduction in vac emissions at least equivalent to the reduction in vac emissions achieved underthe design, equipment, work practiceor operational standard.

§ 60.635 Recordkeeping requirements.

(a) Each Owner or operator subject tothe provisions of this subpart shallcomply with the requirements of paragraphs (b) and (c) of this section in addition to the requirements of §60.486.

(b) The following recordkeeping requirements shall apply to pressure relief devices subject to the requirementsof §60.633(b)(1) of this subpart.

(1) When each leak is detected asspecified in §60.633(b)(2), a weatherproof and readily visible identification,marked with the equipment identification number. shall be attached to theleaking equipment. The identificationon the pressure relief device may be removed after it has been repaired.

(2) When each leak is detected asspecified in §60.633(b)(2). the followinginformation shall be recorded in a logand shall be kept for 2 years in a readily accessible location:

(i) The instrument and operator identification numbers and the equipmentidentification number.

(il) The date the leak was detectedand the dates of each attempt to repairthe leak.

(iil) Repair methods applied in eachattempt to repair the leak.

(iv) "Above 10,000 ppm" if the maximum instrument reading measured bythe methods specified in paragraph (a)of this section after each repair attempt is 10,000ppm or greater.

(v) "Repair delayed" and the reasonfor the delay if a leak is not repairedwithin 15 calendar days after discoveryof the leak.

(vi) The signature of the owner or operator (or designate) whose decision itwas that repair could not be effectedwithout a process shutdown.

(vll) The expected date of successfulrepair of the leak if a leak is not repaired within 15 days.

(viil) Dates of process unit shutdownsthat occur while the equipment isunrepaired.

(ix) The date of successful repair ofthe leak.

554


(x) A list of identification numbersfor equipment that are designated forno detectable emissions under the provisions of §60.482--4(a). The designationof equipment subject to the provisionsof §60.482--4(a) shall be signed by theowner or operator.

(c) An owner or operator shall comply with the following requirement inaddition to the requirement of§60.486(j): Information and data used todemonstrate that a reciprocating compressor is in wet gas service to applyfor the exemption in §60.633(f) shall berecorded in a log that is kept in a readily accessible location.

§ 60.636 Reporting requirements.(a) Each owner or operator subject to

the provisions of this subpart shallcomply with the requirements of paragraphs (b) and (c) of this section in addition to the requirements of §60.487.

(b) An owner or operator shall include the following information in theinitial semiannual report in addition tothe information required in §60.487(b)(1)-(4): Number of pressure relief devices subject to the requirements of§60.633(b) except for those pressure relief devices designated for no detectable emissions under the provisions of§60.482--4(a) and those pressure reliefdevices complying with §60.482--4(c).

(c) An owner or operator shall include the following information in allsemiannual reports in addition to theinformation required in §60.487(c)(2) (i)through (vi):

(1) Number of pressure relief devicesfor which leaks were detected as required in §60.633(b)(2) and

(2) Number of pressure relief devicesfor which leaks were not repaired as required in §60.633(b)(3).

Subpart LLL-Standards of Performance for Onshore NaturalGas Processing: S02 Emissions

SOURCE: 50 FR 40160, Oct. 1, 1985. unlessotherwise noted. .

§ 60.640 Applicability and designationof affected facilities.

(a) The provisions of this subpart areapplicable to the following affected fa-

§60.641

cilities that process natural gas: eachsweetening unit. and each sweeteningunit followed by a sulfur recovery unit.

(b) Facilities that have a design capactty less than 2 long tons per day(LTID) of hydrogen sulfide (H,S) in theacid gas (expressed as sulfur) are required to comply with §60.647(c) but arenot required to comply with §§ 60.642through 60.646.

(c) The provisions of this subpart areapplicable to faclllties located on landand include facilities located onshorewhich process natural gas producedfrom either onshore or offshore wells.

(d) The provisions of this subpartapply to each affected facility identified in paragraph (a) of this sectionwhich commences construction ormodification after January 20, 1984.

(e) The provisions of this subpart donot apply to sweetening facilities producing acid gas that is completely reinjected into oil-or-gas-bearing geologic strata or that is otherwise not released to the atmosphere.

§ 60.641 Definitions.All terms used in this subpart not de

fined below are given the meaning inthe Act and in subpart A of this part.

Acid gas means a gas stream of hydrogen sulfide (H,S) and carbon dioxide(CO,) that has been separated fromsour natural gas by a sweetening unit.

Natural gas means a naturally occurring mixture of hydrocarbon and nonhydrocarbon gases found in geologicformations beneath the earth's surface.The principal hydrocarbon constituentis methane.

Onshore means all facilities exceptthose that are located in the territorialseas or on the outercontinental shelf.

Reduced sulfur compounds means H,S,carbonyl sulfide (COS), and carbon disulfide (CS,).

Sulfur production rate means the rateof liquid sulfur accumulation from thesulfur recovery unit.

Sulfur recovery unit means a processdevice that recovers element sulfurfrom acid gas.

Sweetening unit means a process device that separates the H,S and CO2

contents from the sour natural gasstream.

Total SO, equivalents means the sumof volumetric or mass concentrations

555

APPENDIXB

40 CFR 60 Subpart VVStandards ofPerformance for Equipment Leaks of VOC in Synthetic Organic Chemicals

Manufacturing Industry

§60.480

where:P~asphalt charging rate to blowing still. Mg/

hr (ton/hr).V~volume of asphalt charged. m' (ft').dedensl ty of asphalt. kg/m? (lb/ft').K'<converston factor, 1000 kg/Mg (2000 Ib/

ton).8=duration of test fun, hr.

(i) The volume (V) of asphalt chargedshall be measured by any means accurate to within 10 percent.

(il) The density (d) of the asphaltshall be computed using the followingequation:

Where:d ~ Density of the asphalt, kg/m? Ob/ft')K, ~ 1056.1 kg/rn? (metric unIts)~ 64.70 lb/ft' (English Units)

K, ~ 0.6176 kg/(m' 'C) (metric units)~ 0.0694 Ib/(ft' 'F) (English UnIts)

T; ;:: temperature at the start of the blow, "O( OF)

(5) Method 9 and the procedures in§60.11 shall be used to determine opacity.

(d) The Administrator will determinecompliance with the standards in§60.472(a)(3) by using Method 22, modified so that readings are recorded every15 seconds for a period of consecutiveobservations during representativeconditions (in accordance with §60.8(c»totaling 60 minutes. A performancetest shall consist of one run.

(e) The owner or operator shall usethe monitoring device in §60.473 (a) or(b) to monitor and record continuouslythe temperature during the particulatematter run and shall report the resultsto the Administrator with the performance test results.

(f) If at a later date the owner or operator believes that the emission limits in §60.472(a) and (b) are being meteven though one of the conditions listed in this paragraph exisc, he may submit a written request to the Administrator to repeat the performance testand procedure outlined in paragraph (c)of this section.

(1) The temperature measured in accordance with §60.473(a) is exceedingthat measured during the performancetest.

(2) The temperature measured in accordance with §60.473(b) is lower than

40 CFRen. I (7-1-06 Edition)

that measured during the performancetest.

(g) If fuel oil is to be used to fire anafterburner used to control emissionsfrom a blowing still, the owner or operator may petition the Administrator inaccordance with §60.11(e) of the General Provisions to establish an opacitystandard for the blowing still that willbe the opacity standard when fuel oil isused to fire the afterburner. To obtainthis opacity standard, the owner or operator must request the Administratorto determine opacity during an initial,or subsequent, performance test whenfuel oil is used to fire the afterburner.Upon receipt of the results of the performance test, the Administrator willmake a finding concerning compliancewith the mass standard for the blowingstill. If the Administrator finds thatthe facility was in compliance with themass standard during the performancetest but failed to meet the zero opacitystandard, the Administrator will establish and promulgate in the FEDERALREGISTER an opacity standard for theblowing still that will be the opacitystandard when fuel oil is used to firethe afterburner. When the afterburneris fired with natural gas, the zero percent opacity remains the applicableopacity standard.

[54 FR 6677, Feb. 14, 1989, as amended 54 FR27016, June 27, 1989; 65 FR 61762, Oct. 17, 2000]

Subpart W-Standards of Performance for EquipmentLeaks of VOC in the SyntheticOrganic Chemicals Manufacturing Industry

SOURCE: 48 FR 48335, Oct. 18, 1983, unlessotherwise noted.


(a)(l) The provisions of this subpartapply to affected facilities in the synthetic organic chemicals manufacturing industry.

(2) The group of all equipment (defined in §60.481) within a process unit isan affected facility.

(b) Any affected facility under paragraph (a) of this section that commences construction or modification

436

Environmental Protection Agency §60,481

Closed vent system means a systemthat is not open to the atmosphere andthat Is composed of hard-piping, ductwork, connections, and, if necessary,flow-inducing devices that transportgas or vapor from a piece or pieces ofequipment to a control device or backto a process.

Connector means flanged, screwed,welded, or other joined fittings used to

65, subpart F, must comply with 40CFR part 65, subpart A.

(48 FR 48335, Oct. 18. 1983, as amended at 49FR 22607. May 30, 1984; 65 FR 61762. Oct. 17.2000; 65 FR 78276, Dec. 14, 2000]

§ 60,481 Definitions,

As used in this subpart, all terms notdefined herein shall have the meaninggiven them in the Act or in subpart Aof part 60, and the following termsshall have the specific meanings giventhem.

Capital expenditure means, in addi tionto the definition in 40 CFR 60.2, an expenditure for a physical or operationalchange to an existing facility that:

(a) Exceeds P, the product of the facility's replacement cost, R, and an adjusted annual asset guideline repair allowance, A, as reflected by the following equation: P = R x A, where

(1) The adjusted annual asset guideline repair allowance, A, is the productof the percent of the replacement cost,Y, and the applicable basic annualasset guideline repair allowance, B, divided by 100 as reflected by the following equation:

A = Y x (B + 100);

(2) The percent Y is determined fromthe following equation: Y = 1.0 - 0.575log X, where X is 1982 minus the year ofconstruction; and

(3) The applicable basic annual assetguideline repair allowance, B, is selected from the following table consistent with the applicable subpart:

TABLE FOR DETERMINING ApPLICABLE FOR B

after January 5, 1981, shall be subjectto the requirements of this subpart.

(c) Addition or replacement of equipment for the purpose of process improvement which is accomplished without a capital expenditure shall not byitself be considered a modificationunder this subpart.

(d)(l) If an owner or operator appliesfor one or more of the exemptions inthis paragraph, then the owner or operator shall maintain records as requiredin §60.486(i).

(2) Any affected facility that has thedesign capacity to produce less than1,000 Mg/yr (1,102 ton/yr) is exemptfrom §60.482.

(3) If an affected facility producesheavy liquid chemicals only fromheavy liquid feed or raw materials,then it is exempt from §60.482.

(4) Any affected facility that produces beverage alcohol is exempt from§60.482.

(5) Any affected facility that has noequipment in VOC service is exemptfrom §60.482.

(e) Alternative means o] compliance~(1)Option to comply with part 65. Owners oroperators may choose to comply withthe provisions of 40 CFR part 65, subpart F, to satisfy the requirements of§§ 60.482 through 60.487 for an affectedfacl1ity. When choosing to comply with40 CFR part 65, subpart F, the requirements of §60.485(d), (e), and (0, and§60.486(i) and (j) still apply. Other provisions applying to an owner or operator who chooses to comply with 40CFR part 65 are provided in 40 CFR 65.1.

(2) Part 60, subpart A. Owners or operators who choose to comply with 40CFR part 65, subpart F must also comply with §§60.1, 60.2, 60.5, 60.6, 60.7(a)(1)and (4), 60.14, 60.15, and 60.16 for thatequipment. All sections and paragraphsof subpart A of this part that are notmentioned in this paragraph (e)(2) donot apply to owners or operators ofequipment subject to this subpart complying with 40 CFR part 65, subpart F,except that provisions required to bemet prior to implementing 40 CFR part65 still apply. Owners and operatorswho choose to comply with 40 CFR part

WDOD.GGG.KKK ...

SUbpart applicable 10facilityValue of B10 be usedin equation

12.512.57.04.5

437

§60.481

connect two pipe lines or a pipe lineand a piece of process equipment.

Control device means an enclosedcombustion device, vapor recovery system, or flare.

Distance piece means an open or enclosed casing through which the pistonrod travels, separating the compressorcylinder from the crankcase.

Double block and bleed system meanstwo block valves connected In serieswith a bleed valve or line that can ventthe line between the two block valves.

Duct work means a conveyance system such as those commonly used forheating and ventilation systems. It isoften made of sheet metal and oftenhas sections connected by screws orcrimping. Hard-piping Is not ductwork.

Equipment means each pump, compressor, pressure relief device, sampling connection system, open-endedvalve or line, valve, and flange or otherconnector in VOO service and any devices or systems required by this subpart.

First attempt at repair means to takerapid action for the purpose of stoppingor reducing leakage of organic material to atmosphere using best practices.

Fuel gas means gases that are combusted to derive useful work or heat.

Fuel gas system means the offsite andonslte piping and flow and pressurecontrol system that gathers gaseousstream(s) generated by onsite operations, may blend them with othersources of gas, and transports the gaseous stream for use as fuel gas In combustion devices or in-process combustion equipment, such as furnaces andgas turbines, either singly or In combination.

Hard-piping means pipe or tubingthat Is manufactured and properly Installed using good engineering judgement and standards such as ASMEB31.3, Process Piping (available fromthe American Society of MechanicalEngineers, PO Box 2900, Fairfield, NJ07007-2900).

In gas/vapor service means that thepiece of equipment contains processfluid that Is In the gaseous state at operating conditions.

In heavy liquid service means that thepiece of equipment is not in gas/vaporservice or In light liquid service.


In light liquid service means that thepiece of equipment contains a liquidthat meets the conditions specified In§60.485(e).

In-situ sampling systems means nonextractive samplers or in-line samplers.

In vacuum service means that equipment is operating at an internal pressure which is at least 5 kllopascals(kPa)(0.7 psia) below ambient pressure.

In VOC service means that the pieceof equipment contains or contacts aprocess fluid that is at least 10 percentvao by weight. (The provisions of§60.485(d) specify how to determinethat a piece of equipment Is not in vaoservice.)

Liquids dripping means any visibleleakage from the seal including spraying, misting, clouding, and Ice formation.

Open-ended valve or line means anyvalve, except safety relief valves, having one side of the valve seat In contact with process fluid and one sideopen to the atmosphere, either directlyor through open piping.

Pressure release means the emission ofmaterials resulting from system pressure being greater than set pressure ofthe pressure relief device.

Process improvement means routinechanges made for safety and occupational health requirements, for energysavings, for better utility, for ease ofmaintenance and operation, for correction of design deficiencies, for bottleneck removal, for changing product requirements, or for environmental control.

Process unit means components assembled to produce, as intermediate orfinal products, one or more of thechemicals listed in §60.489 of this part.A process unit can operate independently If supplied with sufficient feed orraw materials and sufficient storage facilities for the product.

Process unit shutdown means a workpractice or operational procedure thatstops production from a process unit orpart of a process unit. An unscheduledwork practice or operational procedurethat stops production from a processunit or part of a process unit for lessthan 24 hours Is not a process unitshutdown. The use of spare equipmentand technically feasible bypassing of

438


equipment without stopping production are not process unit shutdowns.

Quarter means a 3-month period; thefirst quarter concludes on the last dayof the last full month during the 180days following initial startup.

Repaired means that equipment Is adjusted, or otherwise altered, in order toeliminate a leak as indicated by one ofthe following: an instrument reading of10,000 ppm or greater, indication of liquids dripping, or indication by a sensorthat a seal or barrier fluid system hasfailed.

Replacement cost means the capitalneeded to purchase all the depreciablecomponents in a facility.

Sampling connection system means anassembly of equipment within a process unit used during periods of representative operation to take samplesof the process fluid. Equipment used totake nonroutine grab samples is notconsidered a sampling connection system.

Sensor means a device that measuresa physical quantity or the change in aphysical quantity such as temperature,pressure, flow rate, pH, or liquid level.

Synthetic organic chemicals manufacturing industry means the Industry thatproduces, as intermediates or finalproducts, one or more of the chemicalslisted in §60.489.

Volatile organic compounds or vaemeans, for the purposes of this subpart,any reactive organic compounds as defined in §60.2 Definitions.

[48 FR 48335, Oct. 18, 1983, as amended at 49FR 22607, May 30, 1984: 49 FR 26738, June 29,1984; 60 FR 43258, Aug. 18, 1995; 65 FR 61762,Oct. 17, 2000; 65 FR 78276, Dec. 14, 2000]

§ 60.482-1 Standards: General.(a) Each owner or operator subject to

the provisions of this subpart shalldemonstrate compliance with the requirements of §§60.482-1 through 60.48210 or §60.480(e) for all equipment within180days of ini tial startup.

(b) Compliance with §§ 60.482-1 to60.482-10 will be determined by reviewof records and reports, review of performance test results, and inspectionusing the methods and procedures specified in §60.485.

(c)(l) An owner or operator may request a determination of equivalence ofa means of emission limitation to the

§60.482-2

requirements of §§60.482-2, 60.482-3,60.482-5, 60.482-6, 60.482-7, 60.482-8, and60.482-10 as provided in §60.484.

(2) If the Administrator makes a determination that a means of emissionlimitation is at least equivalent to therequirements of §§60.482-2, 60.482-3,60.482-5, 60.482-6, 60.482-7, 60.482-8, or60.482-10, an owner or operator shallcomply with the requirements of thatdetermination.

(d) Equipment that is in vacuumservice Is excluded from the requirements of §§60.482-2 to 60.482-10 if it isidentified as required in §60.486(e)(5l.

[48 FR 48335, Oct. 18, 1983, as amended at 49FR 22608, May 30, 1984; 65 FR 78276, Dec. 14,2000]

§ 60.482-2 Standards: Pumps in lightliquid service.

(a)(l) Each pump in light liquid service shall be monitored monthly to detect leaks by the methods specified in§60.485(b), except as provided in §60.482l(c) and paragraphs (d), (e), and (f) ofthis section.

(2) Each pump in light liquid serviceshall be checked by visual inspectioneach calendar week for indications ofliquids dripping from the pump seal.

(b)(l) If an instrument reading of10,000 ppm or greater is measured, aleak is detected.

(2) If there are indications of liquidsdripping from the pump seal. a leak isdetected.

(c)(l) When a leak is detected, it shallbe repaired as soon as practicable, butnot later than 15 calendar days after itis detected, except as provided in§60.482-9.

(2) A first attempt at repair shall bemade no later than 5 calendar daysafter each leak is detected.

(d) Each pump equipped with a dualmechanical seal system that includes abarrier fluid system is exempt from therequirements of paragraph (a), Providedthe following requirements are met:

(1) Each dual mechanical seal systemis-

(i) Operated with the barrier fluid ata pressure that is at all times greaterthan the pump stuffing box pressure; or

(iI) Equipment with a barrier fluiddegassing reservoir that is routed to aprocess or fuel gas system or connectedby a closed vent system to a control

439

§60.482-3

device that complies with the requirements of §60.482-10; or

(iil) Equipped with a system thatpurges the barrier fluid into a processstream with zero VOC emissions to theatmosphere.

(2) The barrier fluid system is inheavy liquid service or is not in VOCservice.

(3) Each barrier fluid system isequipped with a sensor that will detectfailure of the seai system, the barrierfluid system, or both.

(4) Each pump is checked by visualinspection, each calendar week, for indications of liquids dripping from thepump seals.

(5)(1) Each sensor as described inparagraph (d)(3) is checked daily or isequipped with an audible alarm, and

(ii) The owner or operator determines, based on design considerationsand operating experience, a criterionthat indicates failure of the seal system, the barrier fluid system, or both.

(6)(i) If there are indications of liquids dripping from the pump seal or thesensor indicates failure of the seal system, the barrier fluid system, or bothbased on the criterion determined inparagraph (d)(5)(il), a leak is detected.

(il) When a leak is detected, it shallbe repaired as soon as practicable, butnot later than 15 calendar days after itis detected, except as provided in§60.482-9.

(ili) A first attempt at repair shall bemade no later than 5 calendar daysafter each leak is detected.

(e) Any pump that is designated, asdescribed in §60.486(e)(1) and (2), for nodetectable emission, as indicated by aninstrument reading of less than 500ppm above background, is exempt fromthe requirements of paragraphs (a), (c),and (d) of this section if the pump:

(1) Has no externally actuated shaftpenetrating the pump housing,

(2) Is demonstrated to be operatingwith no detectable emissions as indicated by an instrument reading of lessthan 500 ppm above background asmeasured by the methods specified in§60.485(c), and

(3) Is tested for compliance withparagraph (e)(2) of this section initiallyupon designation, annually, and atother times requested by the Administrator.

40 CFRCh. I (7-1-06 Edition)

(f) If any pump is equipped with aclosed vent system capable of capturing and transporting any leakagefrom the seal or seals to a process or toa fuel gas system or to a control devicethat complies with the requirements of§60.482-lO, it is exempt from paragraphs(a) through (e) of this section.

(g) Any pump that is designated, asdescribed in §60.486(f)(1), as an unsafeto-monitor pump is exempt from themonitoring and inspection requirements of paragraphs (a) and (d)(4)through (6) of this section if:

(1) The owner or operator of thepump demonstrates that the pump isunsafe-to-monitor because monitoringpersonnel would be exposed to an immediate danger as a consequence ofcomplying with paragraph (a) of thissection; and

(2) The owner or operator of thepump has a written plan that requiresmonitoring of the pump as frequentlyas practicable during safe-to-monitortimes but not more frequently than theperiodic monitoring schedule otherwiseapplicable, and repair of the equipmentaccording to the procedures in paragraph (c) of this section if a leak is detected.

(h) Any pump that is located withinthe boundary of an unmanned plantsi te is exempt from the weekly visualinspection requirement of paragraphs(a)(2) and (d)(4) of this section, and thedaily requirements of paragraph (d)(5)of this section, provided that eachpump is visually inspected as often aspracticable and at least monthly.

[48 FR 48335, Oct. 18, 1983, as amended at 65FR 61762, Oct. 17, 2000; 65 FR 78276, Dec. 14,20001

§ 60.482-3 Standards: Compressors.

(a) Each compressor shall beequipped with a seal system that includes a barrier fluid system and thatprevents leakage of VOC to the atmosphere, except as provided in §60.482-l(c)and paragraph (h) and (i) of this section.

(b) Each compressor seal system asrequired in paragraph (a) shall be:

(1) Operated with the barrier fluid ata pressure that is greater than thecompressor stuffing box pressure; or

(2) Equipped with a barrier fluid system degassing reservoir that is routed

440


to a process or fuel gas system or connected by a closed vent system to acontrol device that complies with therequirements of §60.482-10; or

(3) Equipped with a system thatpurges the barrier fluid Into a processstream with zero vac emissions to theatmosphere.

(c) The barrier fluid system shall beIn heavy liquid service or shall not beIn vac service.

(d) Each barrier fluid system as described In paragraph (a) shall beequipped with a sensor that will detectfailure of the seal system, barrier fluidsystem, or both.

(e)(l) Each sensor as required In paragraph (d) shall be checked dally orshall be equipped with an audiblealarm.

(2) The owner or operator shall determine, based on design considerationsand operating experience, a criterionthat indicates failure of the seal system, the barrier fluid system, or both.

(f) If the sensor Indicates failure ofthe seal system, the barrier system, orboth based on the criterion determinedunder paragraph (e)(2), a leak Is detected.

(g)(l) When a leak Is detected, Itshall be repaired as soon as practicable,but not later than 15 calendar daysafter It Is detected, except as providedin §60.482-9.

(2) A first attempt at repair shall bemade no later than 5 calendar daysafter each leak Is detected.

(h) A compressor Is exempt from therequirements of paragraphs (a) and (b)of this section, If it is equipped with aclosed vent system to capture andtransport leakage from the compressordrive shaft back to a process or fuel gassystem or to a control device that complies with the requirements of §60.48210, except as provided In paragraph (I)of this section.

(I) Any compressor that Is desIgnated, as described In §60.486(e) (1)and (2), for no detectable emissions, asindicated by an Instrument reading ofless than 500 ppm above background, Isexempt from the requirements of paragraphs (a}-(h) If the compressor:

(1) Is demonstrated to be operatingwith no detectable emissions, as Indicated by an Instrument reading of lessthan 500 ppm above background, as

§60.482-4

measured by the methods specified in§60.485(c); and

(2) Is tested for compliance withparagraph (1)(1) of this section Initiallyupon designation, annually, and atother times requested by the Administrator.

(j) Any existing reciprocating compressor In a process unit which becomes an affected facility under provisions of §60.14 or §60.15 is exempt from§60.482(a), (b), (c), (d), (e), and (h), provided the owner or operator demonstrates that recasting the distancepiece or replacing the compressor arethe only options available to bring thecompressor Into compliance with theprovisions of paragraphs (a) through (e)and (h) of this section.

[48 FR 48335, Oct. 18, 1983, as amended at 65FR 61762, Oct. 17, 2000: 65 FR 78277, Dec. 14,2000]

§ 60.482-4 Standards: Pressure reliefdevices in gas/vapor service.

(a) Except during pressure releases,each pressure relief device in gas/vaporservice shall be operated with no detectable emissions, as Indicated by anInstrument reading of less than 500ppm above background, as determinedby the methods specified in §60.485(c),

(b)(l) After each pressure release, thepressure rellef device shall be returnedto a condition of no detectable emissions, as indicated by an instrumentreading of less than 500 ppm abovebackground, as soon as practicable, butno later than 5 calendar days after thepressure release, except as provided in§60.482-9.

(2) No later than 5 calendar daysafter the pressure release, the pressurerellef device shall be monitored to confirm the conditions of no detectableemissions, as indicated by an Instrument reading of less than 500 ppmabove background, by the methodsspecified In §60.485(c).

(c) Any pressure relief device that isrou ted to a process or fuel gas sys temor equipped with a closed vent systemcapable of capturing and transportingleakage through the pressure relief device to a control device as described In§60.482-10 is exempted from the requirements of paragraphs (a) and (b) of thissection.

441

Open-ended

§60.482-5

(d)(l) Any pressure relief device thatis equipped with a rupture disk unstream of the pressure relief device isexempt from the requirements of paragraphs (a) and (b) of this section, provided the owner or operator complieswi th the requirements in paragraph(d)(2) of this section.

(2) After each pressure release, a newrupture disk shall be installed upstream of the pressure relief device assoon as practicable, but no later than 5calendar days after each pressure release, except as provided in § 60.482-9.

[48 FR 48335, Oct. 18, 1983, as amended at 65FR 61762, Oct. 17, 2000; 65 FR 78277, Dec. 14,2000J

§ 60.482-5 Standards: Sampling connection systems.

(a) Each sampling connection systemshall be equipped with a closed-purged,closed-loop, or closed-vent system, except as provided in § 60.482-1(c), Gasesdisplaced during filling of the samplecontainer are not required to be collected or captured.

(b) Each closed-purge, closed-loop, orclosed-vent system as required in paragraph (a) of this section shall complywith the requirements specified inparagraphs (b)(l) through (4) of thissection:

(1) Return the purged process fluiddirectly to the process line; or

(2) Collect and recycle the purgedprocess fluid to a process; or

(3) Be designed and operated to capture and transport all the purged process fluid to a control device that complies with the requirements of §60.48210; or

(4) Collect, store, and transport thepurged process fluid to any of the following systems or facili ties;

(i) A waste management unit as defined in 40 CFR 63.111, if the wastemanagement unit is subject to, and operated in compliance with the provisions of 40 CFR part 63, subpart G, applicable to Group 1 wastewaterstreams;

(ii) A treatment, storage, or disposalfacili ty subject to regulation under 40CFR part 262, 264, 265, or 266; or

(iii) A facility permitted, licensed, orregistered by a State to manage municipal or industrial solid waste, if the


process fluids are not hazardous wasteas defined in 40 CFR part 261.

(c) In situ sampling systems and sampling systems without purges are exempt from the requirements of paragraphs (a) and (b) of this section.

[60 FR 43258, Aug. 18, 1995, as amended at 65FR 61762, Oct. 17, 2000; 65 FR 78277, Dec. 14,2000]

§ 60.482-6 Standards:valves or lines.

(a)(l) Each open-ended valve or lineshall be equipped with a cap, blindflange, plug, or a second valve, exceptas provided in §60.482-1(c).

(2) The cap, blind flange, plug, or second valve shall seal the open end at alltimes except during operations requiring process fluid flow through theopen-ended valve or line.

(b) Each open-ended valve or lineequipped with a second valve shall beoperated in a manner such that thevalve on the process fluid end is closedbefore the second valve is closed.

(c) When a double block-and-bleedsystem is being used, the bleed valve orline may remain open during operations that require venting the line between the block valves but shall comply with paragraph (a) at all othertimes.

(d) Open-ended valves or lines in anemergency shutdown system which aredesigned to open automatically in theevent of a process upset are exemptfrom the requirements of paragraphs(a), (b) and (c) of this section,

(e) Open-ended valves or lines containing materials which wouldautocatalytically polymerize or wouldpresent an explosion, serious overpressure, or other safety hazard ifcapped or equipped with a double blockand bleed system as specified in paragraphs (a) through (c) of this sectionare exempt from the requirements ofparagraphs (a) through (c) of this section.

[48 FR 48335, Oct. 18, 1983, as amended at 49FR 22607, May 30, 1984; 65 FR 78277, Dec. 14,2000]

442


§ 60,482-7 Standards: Valves in gas!vapor service and in light liquidservice.

(a) Each valve shall be monitoredmonthly to detect leaks by the methods specified in §60.485(b) and shallcomply with paragraphs (b) through(e), except as provided in paragraphs(f), (g), and (h), §60.483--1, 2, and §60.482l(c).

(b) If an instrument reading of 10,000ppm or greater is measured, a leak isdetected.

(c)(1) Any valve for which a leak isnot detected for 2 successive monthsmay be monitored the first month ofevery quarter, beginning wi th the nextquarter, until a leak is detected.

(2) If a leak is detected, the valveshall be monitored monthly until aleak is not detected for 2 successivemonths.

(d)(1) When a leak is detected, itshall be repaired as soon as practicable,but no later than 15 calendar days afterthe leak is detected, except as providedin §60.482-9.

(2) A first attempt at repair shall bemade no later than 5 calendar daysafter each leak is detected.

(e) First attempts at repair include,but are not limited to, the followingbest practices where practicable:

(1) Tightening of bonnet bolts;(2) Replacement of bonnet bolts;(3) Tightening of packing gland nuts;(4) Injection of lubricant into lubri-

cated packing.(f) Any valve that is designated, as

described in §60.486(e)(2), for no detectable emissions, as indicated by an instrument reading of less than 500 ppmabove background, is exempt from therequirements of paragraph (a) if thevalve:

(1) Has no external actuating mechanism in contact with the process fluid,

(2) Is operated with emissions lessthan 500 ppm above background as determined by the method specified in§60.485(c), and

(3) Is tested for compliance withparagraph (f)(2) of this section initiallyupon designation, annually, and atother times requested by the Administrator.

(g) Any valve that is designated, asdescribed in §60.486(f)(1), as an unsafe-

§60,482-8

to-monitor valve is exempt from therequirements of paragraph (a) if:

(1) The owner or operator of the valvedemonstrates that the valve is unsafeto monitor because monitoring personnel would be exposed to an immediate danger as a consequence of complying with paragraph (a), and

(2) The owner or operator of the valveadheres to a written plan that requiresmonitoring of the valve as frequentlyas practicable during safe-to-monitortimes.

(h) Any valve that is designated, asdescribed in §60.486(f)(2), as a difficultto-monitor valve is exempt from therequirements of paragraph (a) if;

(1) The owner or operator of the valvedemonstrates that the valve cannot bemonitored without elevating the monitoring personnel more than 2 metersabove a support surface.

(2) The process unit within which thevalve is located either becomes an affected facility through §60.14 or §60.15or the owner or operator designatesless than 3.0 percent of the total number of valves as difficult-to-monitor,and

(3) The owner or operator of the valvefollows a written plan that requiresmonitoring of the valve at least onceper calendar year.

[48 FR 48335, Oct. 18, 1983, as amended at 49FR 22608, May 30, 1984; 65 FR 61762, Oct. 17,2000J

§ 60.482-8 Standards: Pumps andvalves in heavy liquid service, pressure relief devices in light liquid orheavy liquid service, and cormectors.

(a) If evidence of a potential leak isfound by visual, audible, olfactory, orany other detection method at pumpsand valves in heavy liquid service,pressure relief devices in light liquid orheavy ltquid service, and connectors,the owner or operator shall follow either one of the following procedures:

(1) The owner or operator shall monitor the equipment within 5 days bythe method specified in §60.485(b) andshall comply with the requirements ofparagraphs (b) through (d) of this section.

(2) The owner or operator shall eliminate the visual, audible, olfactory, orother indication of a potential leak.

443

§60.482-9

(b) If an instrument reading of 10,000ppm or greater is measured, a leak isdetected.

(c)(1) When a leak is detected, it shallbe repaired as soon as practicable, butnot later than 15 calendar days after itis detected, except as provided in§60.482-9.

(2) The first attempt at repair shallbe made no later than 5 calendar daysafter each leak is detected.

(d) First attempts at repair include,but are not limited to, the best practices described under §60.482-7(e).

[48 CFR 48335, Oct. 18, 1983, as amended at 65FR 78277, Dec. 14, 20001

§ 60.482-9 Standards: Delay of repair.(a) Delay of repair of equipment for

which leaks have been detected will beallowed if repair within 15 days is technically infeasible without a processunit shutdown. Repair of this equipment shall occur before the end of thenext process unit shutdown.

(b) Delay of repair of equipment willbe allowed for equipment which is isolated from the process and which doesnot remain in VOC service.

(c) Delay of repair for valves will beallowed if:

(1) The owner or operator demonstrates that emissions of purged material resulting from immediate repairare greater than the fugitive emissionslikely to result from delay of repair,and

(2) When repair procedures are effected, the purged material is collectedand destroyed or recovered in a controldevice complying with §60.482-l0.

(d) Delay of repair for pumps will beallowed if:

(1) Repair requires the use of a dualmechanical seal system that includes abarrier fluid system, and

(2) Repair is completed as soon aspracticable, but not later than 6months after the leak was detected.

(e) Delay of repair beyond a processunit shutdown will be allowed for avalve, if valve assembly replacement isnecessary during the process unit shutdown, valve assembly supplies havebeen depleted, and valve assembly supplies had been sufficiently stocked before the supplies were depleted. Delayof repair beyond the next process unitshutdown will not be allowed unless

40 CFR Ch. I (7- l-{)6 Edition)

the next process unit shutdown occurssooner than 6 months after the firstprocess unit shutdown.

[48 FR 48335, Oct. 18, 1983. as amended at 65FR 78277, Dec. 14, 2000]

§ 60.482-10 Standards: Closed vent systems and control devices.

(a) Owners or operators of closed ventsystems and control devices used tocomply with provisions of this subpartshall comply with the provisions ofthis section.

(b) Vapor recovery systems (for example, condensers and absorbers) shallbe designed and operated to recover theVOC emissions vented to them with anefficiency of 95 percent or greater, or toan exit concentration of 20 parts permillion by volume, whichever is lessstringent.

(c) Enclosed combustion devices shallbe designed and operated to reduce theVOC emissions vented to them with anefficiency of 95 percent or greater, or toan exit concentration of 20 parts permillion by volume, on a dry basis, corrected to 3 percent oxygen, whicheveris less stringent or to provide a minimum residence time of 0.75 seconds ata minimum temperature of 816°C.

(d) Flares used to comply with thisSUbpart shall comply with the requirements of §60.18.

(e) Owners or operators of control devices used to comply with the provtsions of this subpart shall monitorthese control devices to ensure thatthey are operated and maintained inconformance with their designs.

(f) Except as provided in paragraphs(1) through (k) of this section, eachclosed vent system shall be inspectedaccording to the procedures and schedule specified in paragraphs (f)(l) and(f)(2) of this section.

(1) If the vapor collection system orclosed vent system is constructed ofhard-piping, the owner or operatorshall comply with the requirementsspecified in paragraphs (f)(l)(i) and(f)(l)(li) of this section:

(i) Conduct an initial inspection according to the procedures in §60.485(b);and

(li) Conduct annual visual inspections for visible, audible, or olfactoryindications of leaks.

444


(2) If the vapor collection system orciosed vent system is constructed ofductwork, the owner or operator shall:

(i) Conduct an initial inspection according to the procedures in §60.485(b);and

(il) Conduct annual inspections according to the procedures in §60.485(b).

(g) Leaks, as indicated by an instrument reading greater than 500parts permlllion by volume above backgroundor by visual inspections, shall be repaired as soon as practicable except asprovided in paragraph (h) of this section.

(1) A first attempt at repair shall bemade no later than 5 calendar daysafter the leak is detected.

(2) Repair shall be completed no laterthan 15 calendar days after the leak isdetected.

(h) Delay of repair of a closed ventsystem for which leaks have been detected is allowed if the repair is technically infeasible without a processunit shutdown or if the owner or operator determines that emissions resulting from immediate repair would begreater than the fugitive emissionslikely to result from delay of repair.Repair of such equipment shall be complete by the end of the next processunit shutdown.

(I) If a vapor collection system orclosed vent system is operated under avacuum, it is exempt from the inspection requirements of paragraphs(f)(I)(l) and (f)(2) of this section.

(j) Any parts of the closed vent system that are designated, as describedin paragraph (1)(1) of this section, asunsafe to inspect are exempt from theinspection requirements of paragraphs(f)(I)(i) and (f)(2) of this section if theycomply with the requirements specifiedin paragraphs (j)(1) and (j)(2) of thissection:

(1) The owner or operator determinesthat the equipment is unsafe to inspectbecause inspecting personnel would beexposed to an imminent or potentialdanger as a consequence of complyingwith paragraphs (f)(I)(l) or (f)(2) of thissection; and

(2) The owner or operator has a written plan that requires inspection of theequipment as frequently as practicableduring safe-to-inspect times.

§60.482-IO

(k) Any parts of the closed vent system that are designated, as describedin paragraph (1)(2) of this section, asdifficult to inspect are exempt fromthe inspection requirements of paragraphs (f)(I)(i) and (f)(2) of this sectionif they comply with the requirementsspecified in paragraphs (k)(1) through(k)(3) of this section:

(1) The owner or operator determinesthat the equipment cannot be inspected without elevating the inspecting personnel more than 2 metersabove a support surface; and

(2) The process unit wi thin which theclosed vent system is located becomesan affected faclllty through §§60.14 or60.15, or the owner or operator designates less than 3.0 percent of thetotal number of closed vent systemequipment as difficult to inspect; and

(3) The owner or operator has a wri tten plan that requires inspection of theequipment at least once every 5 years.A closed vent system is exempt frominspection if it is operated under a vacuum.

(1) The owner or operator shall recordthe information specified in paragraphs(1)(1) through (1)(5) of this section.

(1) Identification of all parts of theclosed vent system that are designatedas unsafe to inspect, an expianation ofwhy the equipment is unsafe to inspect, and the plan for inspecting theequipment.

(2) Identification of all parts of theclosed vent system that are designatedas difficult to inspect, an explanationof why the equipment is difficult to inspect, and the plan for inspecting theequipment.

(3) For each inspection during whicha leak is detected, a record of the information specified in §60.486(c).

(4) For each inspection conducted inaccordance with §60.485(b) duringwhich no leaks are detected, a recordthat the inspection was performed, thedate of the inspection, and a statementthat no leaks were detected.

(5) For each visual inspection conducted in accordance with paragraph(f)(l)(il) of this section during which noleaks are detected, a record that theinspection was performed, the date ofthe inspection, and a statement thatno leaks were detected.

445

§60.483-1

(m) Closed vent systems and controldevices used to comply with provisionsof this subpart shall be operated at alltimes when emissions may be vented tothem.

[48 FR 48335, Oct. 18, 1983, as amended at 51FR 2702, Jan. 21, 1986; 60 FR 43258, Aug. 18,1995; 61 FR 29878, June 12, 1996; 65 FR 78277,Dec. 14, 2000]

§ 60.483-1 Alternative standards forvalves-allowable percentage ofvalves leaking.

(a) An owner or operator may electto comply with an allowable percentage of valves leaking of equal to or lessthan 2.0 percent.

(b) The following requirements shallbe met if an owner or operator wishesto comply with an allowable percentage of valves leaking;

(1) An owner or operator must notifythe Administrator that the owner oroperator has elected to comply withthe allowable percentage of valvesleaking before Implementing this alternative standard, as specified In§60.487(d).

(2) A performance test as specified Inparagraph (c) of this section shall beconducted initially upon designation.annually, and at other times requestedby the Administrator,

(3) If a valve leak is detected, it shallbe repaired in accordance with §60.4827(d) and (e).

(c) Performance tests shall be conducted in the fo llowing manner:

(1) All valves in gas/vapor and lightliquid service within the affected Iactlity shall be moni tored wi thin 1 weekby the methods specified in §60.485(b).

(2) If an instrument reading of 10,000ppm or greater Is measured, a leak isdetected.

(3) The leak percentage shall be determined by dividing the number ofvalves for which leaks are detected bythe number of valves In gas/vapor andlight liquid service within the affectedfacili ty.

(d) Owners and operators who elect tocomply with this alternative standardshall not have an affected facility witha leak percentage greater than 2.0 percent.

[48 FR 48335, Oct. 18, 1983, as amended at 65FR 61762, Oct. 17, 2000; 65 FR 78278, Dec. 14,2000]


§ 60.483-2 Alternative standards forvalves-skip period leak detectionand repair.

(a)(l) An owner or operator may electto comply with one of the alternativework practices specified In paragraphs(b)(2) and (3) of this section.

(2) An owner or operator must notifythe Administrator before Implementing one of the alternative workpractices, as specified in §60.487(d).

(b)(l) An owner or operator shallcomply initially with the requirementsfor valves in gas/vapor service andvalves In light liquid service, as described in §60.482-7.

(2) After 2 consecutive quarterly leakdetection periods with the percent ofvalves leaking equal to or less than 2.0,an owner or operator may begin to skip1 of the quarterly leak detection periods for the valves In gas/vapor andlight liquid service.

(3) After 5 consecutive quarterly leakdetection periods with the percent ofvalves leaking equal to or less than 2.0,an owner or operator may begin to skip3 of the quarterly leak detection periods for the valves In gas/vapor andlight liquid service.

(4) If the percent of valves leaking Isgreater than 2.0, the owner or operatorshall comply with the requirements asdescribed In §60.482-7 but can againelect to use this section.

(5) The percent of valves leakingshall be determined by dividing thesum of valves found leaking during current monitoring and valves for whichrepair has been delayed by the totalnumber of valves subject to the requirements of this section.

(6) An owner or operator must keep arecord of the percent of valves foundleaking during each leak detection period.

[48 FR 48335, Oct. 18, 1983, as amended at 65FR 61762, Oct. 17, 2000; 65 FR 78278, Dec. 14,2000)

§ 60.484 Equivalence of means of emission limitation.

(a) Each owner or operator subject tothe provisions of this subpart mayapply to the Administrator for determination of equivalance for any meansof emission limitation that achieves areduction In emissions of VOC at least

446


equivalent to the reduction in emissions of VOC achieved by the controlsrequired in this subpart.

(b) Determination of equivalence tothe equipment, design, and operationalrequirements of this subpart will beevaluated by the following guidelines:

(I) Each owner or operator applyingfor an equivalence determination shallbe responsible for collecting andverifying test data to demonstrateequivalence of means of emission limitation.

(2) The Administrator will comparetest data for the means of emissionlimitation to test data for the equipment, design, and operational requirements.

(3) The Administrator may conditionthe approval of equivalence on requirements that may be necessary to assureoperation and maintenance to achievethe same emission reduction as theequipment, design, and operational requirements.

(c) Determination of equivalence tothe required work practices in this subpart will be evaluated by the followingguidelines:

(I) Each owner or operator applyingfor a determination of equivalenceshall be responsible for collecting andverifying test data to demonstrateequivalence of an equivalent means ofemission limitation.

(2) For each affected facility forwhich a determination of equivalenceis requested, the emission reductionachieved by the required work practiceshall be demonstrated.

(3) For each affected facility, forwhich a determination of equivalenceis requested, the emission reductionachieved by the equivalent means ofemission limitation shall be demonstrated.

(4) Each owner or operator applyingfor a determination of equivalenceshall commit in writing to work practice(s) that provide for emission reductions equal to or greater than the emission reductions achieved by the required work practice.

(5) The Administrator will comparethe demonstrated emission reductionfor the equivalent means of emissionlimitation to the demonstrated emission reduction for the required work

§60.485

practices and will consider the commitment in paragraph (c)(4).

(6) The Administrator may conditionthe approval of equivalence on requirements that may be necessary to assureoperation and maintenance to achievethe same emission reduction as the required work practice.

(d) An owner or operator may offer aunique approach to demonstrate theequivalence of any equivalent means ofemission limitation.

(e)(I) After a request for determination of equivalence is received, the Administrator will publish a notice in theFEDERAL REGISTER and provide the opportunity for public hearing if the Administrator judges that the requestmay be approved.

(2) After notice and opportunity forpublic hearing, the Administrator willdetermine the equivalence of a meansof emission limitation and will publishthe determination in the FEDERAL REGISTER.

(3) Any equivalent means of emissionlimi tations approved under this sectionshall constitute a required work practice, equipment, design, or operationalstandard within the meaning of section1l1(h)(I) of the Clean Air Act.

(f)(I) Manufacturers of equipmentused to control equipment leaks ofVOC may apply to the Administratorfor determination of equivalence forany equivalent means of emission limitation that achieves a reduction inemissions of VOC achieved by theequipment, design, and operational requirements of this subpart.

(2) The Administrator will make anequivalence determination accordingto the provisions of paragraphs (b), (c),(d), and (e) of this section.

[48 FR 48335, Oct. 18, 1983, as amended at 65FR 61762, Oct. 17, 2000]

§ 60.485 Test methods and procedures.

(a) In conducting the performancetests required in §60.8, the owner or operator shall use as reference methodsand procedures the test methods in appendix A of this part or other methodsand procedures as specified in this section, except as provided in §60.8(b).

(b) The owner or operator shall determine compliance with the standards in§§ 60.482, 60.483, and 60.484 as follows:

447

§60.485

(1) Method 21 shall be used to determine the presence of leaking sources.The instrument shall be calibrated before use each day of its use by the procedures specified in Method 21. The following calibration gases shall be used:

(I) Zero air (less than 10 ppm of hydrocarbon in air); and

(li) A mixture of methane or nhexane and air at a concentration ofabout, but less than, 10,000 ppm methane or n-hexane.

(c) The owner or operator shall determine compliance with the no detectable emission standards in §§60.482-2(e),60.482-3(1), 60.482-4, 60.482-7(f), and60.482-10(e) as follows:

(1) The requirements of paragraph (b)shall apply.

(2) Method 21 shall be used to determine the background level. All potential leak interfaces shall be traversedas close to the interface as possible.The arithmetic difference between themaximum concentration indicated bythe instrument and the backgroundlevel is compared with 500 ppm for determining compliance.

(d) The owner or operator shall testeach piece of equipment unless he demonstrates that a process unit is not inVOC service, i.e., that the VOC contentwould never be reasonably expected toexceed 10 percent by weight. For purposes of this demonstration, the following methods and procedures shall beused:

(1) Procedures that conform to thegeneral methods in ASTM E26Q-73, 91,or 96, E16li--67, 77, or 92, E169-63, 77, or 93(incorporated by reference-see §60.17)shall be used to determine the percentVOC content in the process fluid thatis contained in or contacts a piece ofequipment.

(2) Organic compounds that are considered by the Administrator to havenegligible photochemical reactivitymay be excluded from the total quantity of organic compounds in determining the VOC content of the processfluid.

(3) Engineering judgment may beused to estimate the VOC content, if apiece of equipment had not been shownpreviously to be in service. If the Administrator disagrees with the judgment, paragraphs (d) (1) and (2) of this

40 CFRCh. I (7-H)6 Edition)

section shall be used to resolve the disagreement.

(e) The owner or operator shall demonstrate that an equipment is in lightliquid service by showing that all thefollowing conditions apply:

(1) The vapor pressure of one or moreof the components is greater than 0.3kPa at 20°C (1.2 in. H20 at 68 OF).Standard reference texts or ASTMD287!f-83, 96, or 97 (incorporated by reference-see §60.17) shall be used to determine the vapor pressures.

(2) The total concentration of thepure components having a vapor pressure greater than 0.3 kPa at 20°C (1.2in. H20 at 68 OF) is equal to or greaterthan 20 percent by weight.

(3) The fluid is a liquid at operatingconditions.

(f) Samples used in conjunction withparagraphs (d), (e), and (g) of this section shall be representative of the process fluid that is contained in or contacts the equipment or the gas beingcombusted in the flare.

(g) The owner or operator shall determine compliance with the standards offlares as follows:

(1) Method 22 shall be used to determine visible emissions.

(2) A thermocouple or any otherequivalent device shall be used to monitor the presence of a pilot flame in theflare.

(3) The maximum permitted velocityfor air assisted flares shall be computed using the following equation:

Vmax =K J +K2HTWhere:Vma>t ;; Maximum permitted velocity. mlsec

(!tIsec)HT =Net heating value of the gas being com-

busted, MJ/scm (Btu/sci).K 1 = a.706 m1sec (metric uni ts)= 28.56 ft/sec (English units)K, = 0.7084 m'/(MJ-sec) (metric units)= 0.087 ft'/(Btu-sec) (English units)

(4) The net heating value (HT) of thegas being combusted in a flare shall becomputed using the following equation:

n

HT=KICjH j

i=!Where:K = Conversion constant, 1.740 x 107 (g

mole)(MJ)/ (ppm-scm-kcal) (metric units)

448


= 4.674 X 10' (g-mo1e)(Btu)/(ppm-scf-kcal)](English units)

C, ::; Concentration of sample component "1,"ppm

Hi = net heat of combustion of sample component "i" at 25 °C and 760 mm Hg (77 OFand 14.7 psi), kcallg-mo1e

(5) Method 18 and ASTM D2504-67, 77,or 88 (Reapproved 1993) (incorporatedby reference-see §60.17) shall be usedto determine the concentration of sample component "i."

(6) ASTM D2382-76 or 88 or D4809-95(incorporated by reference-see §60.17)shall be used to determine the net heatof combustion of component "i" if published values are not available or cannot be calculated.

(7) Method 2, 2A, 2C, or 2D, as appropriate, shall be used to determine theactual exit velocity of a flare. If needed, the unobstructed (free) cross-sectional area of the flare tip shall beused.

(54 FR 6678, Feb. 14, 1989, as amended at 54FR 27016, June 27, 1989; 65 FR 61763, Oct. 17,2000J

§ 60.486 Recordkeeping requirements.(a)(l) Each owner or operator subject

to the provisions of this subpart shallcomply with the recordkeeping requirements of this section.

(2) An owner or operator of morethan one affected facility subject tothe provisions of this subpart maycomply with the recordkeeping requirements for these facilities in onerecordkeeping system if the systemidentifies each record by each facility.

(b) When each leak is detected asspecified in §§60.482-2, 60.482-3, 60.482-7,60.482-8, and 60.483-2, the following requirements apply:

(1) A weatherproof and readily visibleidentification, marked with the equipment identification number, shall beattached to the leaking equipment.

(2) The identification on a valve maybe removed after it has been monitoredfor 2 successive months as specified in§60.482-7(c) and no leak has been detected during those 2 months.

(3) The identification on equipmentexcept on a valve, may be removedafter it has been repaired.

(c) When each leak is detected asspecified in §§ 60.482-2, 60.482-3, 60.482-7,60.482-8, and 60.483-2, the following in-

§60.486

formation shall be recorded in a logand shall be kept for 2 years in a readily accessible location:

(1) The instrument and operator identification numbers and the equipmentidentification number.

(2) The date the leak was detectedand the dates of each attempt to repairthe leak.

(3) Repair methods applied in eachattempt to repair the leak.

(4) "Above 10,000" if the maximum instrument reading measured by themethods specified in §60.485(a) aftereach repair attempt is equal to orgreater than 10,000 ppm.

(5) "Repair delayed" and the reasonfor the delay if a leak is not repairedwi thin 15 calendar days after discoveryof the leak.

(6) The signature of the owner or operator (or designate) whose decision itwas that repair could not be effectedwithout a process shutdown.

(7) The expected date of successful repair of the leak if a leak is not repairedwi thin 15 days.

(8) Dates of process unit shutdownsthat occur while the equipment isunrepaired.

(9) The date of successful repair ofthe leak.

(d) The following information pertaining to the design requirements forclosed vent systems and con troi devices described in §60.482-10 shall be recorded and kept in a readily accessiblelocation:

(1) Detailed schematics, design specifications, and piping and instrumentation diagrams.

(2) The dates and descriptions of anychanges in the design specifications.

(3) A description of the parameter orparameters monitored, as required in§60.482-1O(e), to ensure that control devices are operated and maintained inconformance with their design and anexplanation of why that parameter (orparameters) was selected for the monitoring.

(4) Periods when the closed vent systems and control devices required in§§60.482-2, 60.482-3, 60.482-4, and 60.482-5are not operated as designed, includingperiods when a flare pilot light doesnot have a flame.

(5) Dates of startups and shutdownsof the closed vent systems and control

449

§60.487

devices required in §§ 60.482-2, 60.482-3,60.482-4, and 60.482-5.

(e) The following information pertaining to all equipment subject to therequirements in §§60.482-1 to 60.482-10shall be recorded in a log that is keptin a readily accessibie location:

(1) A list of identification numbersfor equipment subject to the requirements of this subpart.

(2)(i) A list of identification numbersfor equipment that are designated forno detectable emissions under the provisions of §§ 60.482-2(e), 60.482-3(1) and60.482-7(f).

(il) The designation of equipment assubject to the requirements of §60.4822(e), §60.482-3(i), or §60.482-7(f) shall besigned by the owner or operator.

(3) A list of equipment identificationnumbers for pressure rellef devices required to comply with §60.482-4.

(4)(1) The dates of each compliancetest as required in §§60.482-2(e), 60.4823(i), 60.482-4, and 60.482-7(f).

(il) The background level measuredduring each compliance test.

(iil) The maximum instrument reading measured at the equipment duringeach compliance test.

(5) A list of identification numbersfor equipment in vacuum service.

(f) The following information pertaining to all valves subject to the requirements of §60.482-7(g) and (h) andto all pumps subject to the requirements of §60.482-2(g) shall be recordedin a log that is kept in a readily accessible location:

(I) A list of identification numbersfor valves and pumps that are designated as unsafe-to-monitor, an explanation for each valve or pump statingwhy the valve or pump is unsafe-tomonitor, and the plan for monitoringeach valve or pump.

(2) A list of identification numbersfor valves that are designated as difficult-to-monitor, an explanation foreach valve stating why the valve is difficult-to-monitor, and the schedule formonitoring each valve.

(g) The following information shallbe recorded for valves complying with§60.483-2:

(1) A schedule of monitoring.(2) The percent of valves found leak

ing during each monitoring period.


(h) The following information shallbe recorded in a log that is kept in areadily accessible location:

(1) Design criterion required in§§60.482-2(d)(5) and 60.482-3(e)(2) and explanation of the design criterion; and

(2) Any changes to this criterion andthe reasons for the changes.

(i) The following information shall berecorded in a log that is kept in a readily accessible location for use in determining exemptions as provided in§60.480(d):

(1) An analysis demonstrating the design capacity of the affected facility,

(2) A statement listing the feed orraw materials and products from theaffected facilities and an analysis demonstrating whether these chemicals areheavy liquids or beverage alcohol, and

(3) An analysis demonstrating thatequipment is not in vac service.

(j) Information and data used to demonstrate that a piece of equipment isnot in vac service shall be recorded ina log that is kept in a readily accessible location.

(k) The provisions of §60.7 (b) and (d)do not apply to affected facilities subject to this subpart.

[48 FR 48335, Oct. 18, 1983, as amended at 65FR 61763, Oct. 17, 2000; 65 FR 78278, Dec. 14,2000]

§ 60.487 Reporting requirements.(a) Each owner or operator subject to

the provisions of this subpart shall submi t semiannual reports to the Administrator beginning six months after theinitial startup date.

(b) The initial semiannual report tothe Administrator shall include the following information:

(1) Process unit identification.(2) Number of valves subject to the

requirements of §60.482-7, excludingthose valves designated for no detectable emissions under the provisions of§60.482-7(f).

(3) Number of pumps subject to therequirements of §60.482-2, excludingthose pumps designated for no detectable emissions under the provisions of§60.482-2(e) and those pumps complyingwith §60.482-2(f).

(4) Number of compressors subject tothe requirements of §60.482-3, excludingthose compressors designated for no detectable emissions under the provisions

450


of §60.482-3(i) and those compressorscomplying with §60.482-3(h).

(c) All semiannual reports to the Administrator shall include the followinginformation, summarized from the information in §60.486:

(1) Process unit identification.(2) For each month during the semi

annual reporting period,(I) Number of valves for which leaks

were detected as described in§60.482(7)(b) or §60.483-2,

(ll) Number of valves for which leakswere not repaired as required in§60.482-7(d)(I),

(iii) Number of pumps for which leakswere detected as described in §60.4822(b) and (d)(6)(i),

(iv) Number of pumps for which leakswere not repaired as required in§60.482-2(c)(I) and (d)(6)(ii),

(v) Number of compressors for whichleaks were detected as described in§60.482-3(f),

(vi) Number of compressors for whichleaks were not repaired as required in§60.482-3(g)(1), and

(vii) The facts that explain eachdelay of repair and, where appropriate,why a process unit shutdown was technically infeasible.

(3) Dates of process unit shutdownswhich occurred wi thin the semiannualreporting period.

(4) Revisions to items reported according to paragraph (b) if changeshave occurred since the initial reportor subsequent revisions to the initialreport.

(d) An owner or operator electing tocomply with the provisions of §§60.4831 or 60.483-2 shall notify the Administrator of the alternative standard selected 90 days before implementing either of the provisions.

(e) An owner or operator shall reportthe results of all performance tests inaccordance with §60.8 of the GeneralProvisions. The provisions of §60.8(d)do not apply to affected faclllties subject to the provisions of this subpartexcept that an owner or operator mustnotify the Administrator of the schedule for the initial performance tests atleast 30 days before the initial performance tests.

(0 The requirements of paragraphs(a) through (c) of this section remain inforce until and unless EPA, in dele-

§60.489

gating enforcement authority to aState under section lll(c) of the Act,approves reporting requirements or analternative means of compliance surveillance adopted by such State. Inthat event, affected sources within theState wlll be relieved of the obligationto comply with the requirements ofparagraphs (a) through (c) of this section, provided that they comply withthe requirements established by theState.

(48 FR 48335, Oct. 18, 1983, as amended at 49FR 22608, May 30. 1984; 65 FR 61763, Oct. 17.2000]

§ 60.488 Reconstruction.

For the purposes of this subpart:(a) The cost of the following fre

quently replaced components of the facility shall not be considered in calculating either the "fixed capital cost ofthe new components" or the "fixedcapital costs that would be required toconstruct a comparable new facility"under §60.15: pump seals, nuts andbolts, rupture disks, and packings.

(b) Under §60.15, the "fixed capitalcost of new components" includes thefixed capital cost of all depreciablecomponents (except components specified in §60.488 (a)) which are or will bereplaced pursuant to all continuousprograms of component replacementwhich are commenced within any 2year period following the applicabili tydate for the appropriate subpart. (Seethe "Applicability and designation ofaffected facility" section of the appropriate subpart.) For purposes of thisparagraph, "commenced" means thatan owner or operator has undertaken acontinuous program of component replacement or that an owner or operatorhas entered into a contractual obligation to undertake and complete, withina reasonable time, a continuous program of component replacement.

(49 FR 22608, May 30, 1984J

§ 60.489 List of chemicals produced byaffected facilities.

The following chemicals are produced, as intermediates or final products, by process units covered underthis subpart. The applicability date forprocess units producing one or more ofthese chemicals is January 5, 1981.

451

§60.489 40 CFRCh. I (7-1-06 Edition)

CAS No. Chemical CAS No. Chemical

105-57-7 . Acetal. 106-31-0 .. Butyric anhydride.75-Q7-D . Acetaldehyde. 109-74-0 .. Butyronltrile.107--89-1 . Acelaldol. 105-60-2. Caprolaetam.60-35-5 . Acetamide. 75-1-50. Carbon disulfide.103-84-4 . Acetanilide. 558-13-4," Carbon tetrabromide.64-19-7," Acetic acid. 5lH!:J.-{; . Carbon tetrachloride.108-24-7 .. Acetic anhydride. 9004-35-7 .. Cellulose acetate.67-64-1 Acetone. 79-11--8 . Chloroacetic acid.75-86-5 Acetone cyanohydrin. 108-42-9 .... m-cntoroanillne.75-05-8 . Acetonitrile. 95-51-2 .. o-ctucroaniline.98-86-2 Acetophenone. 106-47-8. p-cttlcroanmne.75-36-5 . Acetyl chloride. 3591:Hl9-8 . Chlorobenzaldehyde.74-86-2 . Acetylene. 108-90-7 . Chlorobenzene.107-02-8 . Acrolein. 118-91-2,535- Chlorobenzoicacid.79-06-1 . Acrylamide. 80-8, 74-11-79-10-7. Acrylic acid. 3'.107-13-1 . Acrylonitrile. 2136-81-4. Cnlorobenzotncntoride.124-04-9 . Adipic acid. 2136-89--2,111-69-3. Adiponitrile. 5216-25-1'.(") Alkyl naphthalenes. 1321-03-5. Chlorobenzoyl chloride.107-18-6. Allyl alcohol. 25497-29-4 ... Chlorodifluoromethane.107-05--1 . Allyl chloride. 75-45-6 . Chlorodifluoroethane.1321-11-5. Aminobenzoic acid. 67-66-3 .... Chloroform.111-41-1 . Aminoethylethanolamine. 25586-43-0 ... Chloronaphthalene.123-30-8. p-AminophenoL 88-73-3 ... o-cblorcnttrobenzene.62B-63~7, 123- Amyl acetates. 100-00--5 . p-chloronltrobenzene.

92-2. 25167-80-0 . Chlorophenols.71-41-0~ . Amyl alcohols. 126-99--8 . Chloroprene.110--58-7 . Amyl amine. 7790-94-5 . Ctuorosultonlc acid.543-59--9 .. Amyl chloride. 106-41-8. m-chlorotoluene.110-66-7~ . Amyl mercaptans. 95-49-8 . o-chlorotoluene.1322-06-1 . Amyl phenol. 106-43-4 . p-cnlorotoluene.62-53-3. Aniline. 75--72-9 . Chtorotnnuorometnane.142-04-1 . Aniline hydrochloride. 108-39-4. rn-cresol.29191-52-4 ... Anisidine. 95-48-7 .. o-cresol.100-66-3 . Anisole. 106-44-5. p-cresot.118-92-3 .. Anthranilic acid. 1319--77-3 ... Mixed crescts.64-65--1 . Anthraquinone. 1319--77-3. creevnc acid.100--52-7 Benzaldehyde. 4170-30-0. Crotonaldehyde.55--21-0 .. Benzamide. 3724-85-0 . Crotonic acid.71-43-2 . Benzene. 98-82-8. Cumene.98-48-6 . Benzeneoisultonlc acid. 80--15--9 Cumene hyoroperoxide.98-11-3 Benzenesutton!c acid. 372-09-8 . Cyanoacetic acid.134-81-6 . Benzil. 506--77-4 . Cyanogen chloride.76-93-7 . Benzilic acid. 108-80-5 . Cyanuric acid.65-85-0 Benzoic acid. 108-77--0. Cyanuric chloride.119--53-9 . Benzoin. 110-82-7. Cyclohexane.100-47-0 . Benzonltnte. 108-9:Hl . Cyclohexanol.119-61-9. Benzophenone. 108--94-1 . Oycronexanone.98-07-7 . Benzotnchtorlde. 110--83-8 . Cyclohexene.98-88-4 Benzoyl chloride. 108-91-8 .. Cyclohexylamine.10Q-51-6 Benzyl alcohol. 111-78-4 . Cyclooctadiene.100-46-9 . Benzylamine. 112-30--1 .. Decanol.120-51-4 .. Benzyl benzoate. 123-42-2 .. Diacetone alcohol.100-44-7 ... Benzyl chloride. 27576-04-1 . Diaminobenzoic acid.98-87-3. Benzyl dlcttlcrtde. 95-76-1,95-82- Dtchtcroaniline.92-52-4 Biphenyl. 9,554-00--7.80-05-7 . Bisphenol A. 608-27-5,10-86-1 . Bromobenzene. 608--31-1,27497-51-4 . Bromonaphthalene. 626-43-7,106-99--0 . Butadiene, 27134-27-6,106-98-9. 1-butene. 57311-92-9~.

123--86-4 . n-butyl acetate. 541-73-1 .... rn-dlcnlorobenzene.141-32-2. n-butyl acrylate. 95-50-1 . a-dichlorobenzene.71-36-3 . n-butyl alcohol. 106-46-7. p-dlchlcrcbenzene.78-92-2. s-butyl alcohol. 75-71-8 .. Dichlorodifluoromethane75-65-0 ... t-butyl alcohol. 111-44-4 Dichloroethyl ether.109--73-9 . n-butytamine. 107--06-2 .. t.z-oictaoroemane (EDC)13952-84-6. s-butylamine. 96-23-1 ... Dichlorohydrin.75--64-9 . t-butytamtne. 26952-23-8 . Dtchtoropropene.98-73-7 . p-tert-butyt benzoic acid. 101-83-7 .. Dicyclohexylamine.107-88-0 . t.a-ourvrene glycol. 109-89-7. Diethylamine.123-72-8 n-butyra'dehyde. 111-46-6 . Diethylene glycol.107~92-6 Butyric acid. 112-36-7 .. Diethylene glycol diethyl ether.

452

Environmental Protection Agency §60.489

CAS No. Chemical CAS No.> Chemical

111-96-6 ... Diethylene glycol dimethyl ether. 110-17-8. Fumaric acid.112-34-5. Diethylene glycol mono butyl ether. 9fHll-1 . Furfural.124-17-4. Diethylene glycol monobutyl ether ace- 56--81-5 . Glycerol.

tale. 26545-73-7 . Glycerol dichlorohydrin.111-90-0. Diethylene glycol monoethyl ether. 25791-95-2 Glycerol trtether.112-15-2. Diethylene glycol monoethyl ether ace- 56-4tH; . Glycine.

tate. 107-22-2. Glyoxal.111-77-3 . Diethylene glycol monomethyl ether. 118-74-1 . Hexachlorobenzene.64--67-5 . Diethyl sulfate. 67-72-1 . Hexachloroethane75-37-6 . Difluoroethane. 36653-82-4 . Hexadecyl alcohol.25167-7Q...8 . Dnsobvtylene. 124-09-4. Hexamethylenediamlne.26761-40-0 . Diisodecy! phthalate. 629-11-8 .. Hexamethylene glycol.27554-26-3 ... Diisooctyl phthalate. 100-97--0. Hexamethylenetetramine674-82-8 . Diketene. 74-90-8 . Hydrogen cyanide.124-40-3 . Dimethylamine. 123-31-9. Hydroquinone.121-69-7 . N,N-dimethylaniline. 99-96-7 . p-hydroxybenzoic acid.115-10-6 ... N,N-dimethyl ether. 26760-64-5 . lsoarnytene.68-12-2 . N,N-dimethyI1ormamide. 78-83-1 . Isobutanol.57-14-7 . Dimethylhydrazine. 110-19-0. Isobutyl acetate.77-78-1 . Dimethyl sulfate. 115-11-7. Isobutylene.75-18-3. Dimethyl sulfide. 78-84-2 . Isobutyraldehyde.67-68-5. Dimethyl sulfoxide. 79-31-2 ... Isobutyric acid.120-61-6. Dimethyl terephthatate. 25339-17-7. lsodecanor.99-34-3 .... a.s-omrtrobenaoic acid. 26952-21-6 . Isooctyl alcohol51-28-5. Dinitrophenol. 78-78-4 . Isopentane.25321-14-6 . Dmltrotonrene. 78-59-1 . Isophorone.123-91-1 . Dioxane. 121-91-5. lsophthalic acid.64lHl5-0 . Dioxilane. 78-79-5 .. Isoprene.122-39-4. Diphenylamine. 67-63-0 . Isopropanol.101-84-8 Diphenyl oxide. 108-21-4 . Isopropyl acetate.102--08-9 . Diphenyl thiourea. 75-31-0 . lsopropylamine.25265-71-8 . Dipropylene glycol. 75-29-6 . Isopropyl chloride.25378-22-7 . Dodecene. 25168-<J5-3 .. Isopropylphenol.28675-17-4 . Dodecylaniline. 463-51-4. Ketene.27193-86-8. Dodecylphenol. 1"1· Linear alkyl sulfonate.105-89-8 . Epichlorohydrin. 123-{)1-3. Linear alkylbenzene (linear64-17-5. Ethanol. dodecylbenzene).141-43-5~ . Ethanolamlnes. 110-16-7. Maleic acid.141-78-6 ... Ethyl acetate. 108-31-6. Maleic anhydride.141-97-9. Ethyl acetoacetate. 6915-15-7 . Malic acid.140-88-5. Ethyl acrylate. 141-79-7. Mesityl oxide.75-04-7 .. Ethylamine. 121-47-1 .. Metanilic acid.100-41-4 . Ethylbenzene. 79-41-4. Methacryllc acid.74-96-4. Ethyl bromide. 563-47-3. Methanyl chloride.9004-57-3. EthylceUulose. 67-56-1 . Methanol.75-00-3 Ethyl chloride. 79-20-9 . Methyl acetate.105-39-5. Ethyl cbroroacetate. 105-45-3 . Methyl acetoacetate.105-56-6. Ethylcyanoacetate. 74-89-5 . Methylamine.74-85-1 . Ethylene. 100-61-8 n-metnytanlune.96-49-1 ..... Ethylene carbonate. 74-83-9. Methyl bromide.107-07-3. Ethylene chlorohydrin. 37365-71-2. Methyl butyno1.107-15-3. Ethylenediamine. 74-87-3 . Methyl chloride.106-93-4. Ethylene dlbrcmtde. 108-87-2 .. Methylcyclohexane.107-21-1 . Ethylene glycol. 1331-22-2. Methylcyclohexanone111-55-7. Ethylene glycol dtacetate. 75-09-2 . Methylene chloride.110-71--4 ...... Ethylene glycol dimethyl ether. 101-77-9. Methylene crannlna.111-75-2. Ethylene glycol monobutyl ether. 101-68-8. Methylene diphenyl diisocyanate.112-Q7-2. Ethylene glycol monobutyl ether acetate. 78-93-3 . Methyl ethyl ketone.11o-ao-S Ethylene glycol monoethyl ether. 107-31-3. Methyl lormate.111-15--9 ... Ethylene glycol monethyl ether acetate. 108-11-2 .. Methyl Isobutyl carbinol.109-86-4 ... Ethylene glycol monomethyl ether. 108-10-1 . Methyl isobutyl ketone.110-49-6. Ethylene glycol monomethyl ether ace- 8tH;2-6 . Methyl methacrylate.

tate. 77-75-8 . Methylpentynol.122-99-6 . Ethylene glycol monophenyl ether. 98-83-9 . a-methylstyrene.2807-30-9. Ethylene glycol monopropyl ether. 110-91-8. Morpholine.75-21-8 .. Ethylene oxide. 85-47-2 ." a-naphthalene sulfonic acid.60-29-7 . Ethyl ether 120-18-3. b-napnthalene sullonic acid.104-75-7 . 2-ethylhexanol. 90-15-3 . a-naphthol.122-S1--o . Ethyl orthoformate. 135-19-3 b-naptnhot.95-92-1 . Ethyl oxalate. 75-98-9. Neopentanoic acid.41892-71-1 Ethyl sodium oxatacetate. 88-74-4 . o-nttroanlune.50-00-0. Formaldehyde. 100-01-6. p-nttroanlnne.75-12-7. Formamide. 91-23-6. o-nttroanrsote.64-18-<; . Formic acid. 100-17-4. p-nttroantsote.

453

§60.490 40 CFR Ch. I (7-1-06 Edition)

CAS No. ~ Chemical CAS No. Chemical

SOURCE: 48 FR 38737. Aug. 25. 1983, unlessotherwise noted.

[48 FR 48335. Oct. 18, 1983, as amended at 65FR 61763, Oct. 17, 2000]

Subpart WW-Standards of Performance for the BeverageCan Surface Coating Industry

-CAS numbers refer to the Chemical Abstracts Registrynumbers assigned to specific chemicals. isomers, or mixturesof chemicals. Some isomers or mixtures that are covered bythe standards do not have CAS numbers assigned to them.The standards apply to all of the chemicals listed, whetherCAS numbers have been assigned or not.

b No CAS number(s) have been assigned to this chemical,its isomers, or mixtures containing these chemicals.

<'CAS numbers for some of the isomers are listed; thestandards apply to art of the isomers and mixtures, even ifCAS numbers have not been assigned.

Toluenesulfonamide.Toluenesulfonic acids.Totuenesulfonyl chloride.Totuldinee.Tricntorobenzenes.

1,1, t-tncnloroethane.t.f.z-tnctuoroethane.Trichloroethylene.Trichlorofluoromethane.t.z.a-trctaoroo-opane.1,1,2-trichloro-l ,2,2-trifluoroethane.Triethylamine.Triethylene glycol.Triethylene glycol dimethyl ether.Triisobutylene.Trimethylamine.Urea.Vinyl acetate.Vinyl chlorideVinylidene chloride.Vinyl toluene.Xylenes (miXed).c-xylene.p-xylene.Xytencl.Xylidine.


(a) The provisions of this subpartapply to the foilowing affected facilities in beverage can surface coatinglines: each exterior base coat operation, each overvarnish coating operation, and each inside spray coatingoperation.

(b) The provisions of this subpartapply to each affected facility which isidentified in paragraph (a) of this section and commences construction,modification. or reconstruction afterNovember 26. 1980.

1333-07-9 .104-15-4 c .

98-59-9.26915-12-8 ..87-61-6,108-

70-3, 120--821".

71-55-6.79-00-5 .79-01-6.75-69-4.96--18-4.76--13-1 .121-44-8.112-27-6.112-49-2.7756-94-7 .75-50-3 .57-13-6.108--05-4 ..75-01-475-35-4 ..25013-15-4.1330--20--7 .95-47-6 .106-42-31300-71-6.1300-73--8 .

Phenyl anthranilic acidPhenylenediamine.Phosgene.Phthalic anhydride.Phthaumtdeb-picoline.PiperazinePolybutenes.

Polyethylene glycol.Polypropylene glycol.Propionatdehyde.Propionic acid.n-propyt alcohol.Propytamine.Propyl chloride.Propylene.Propylene chtoronydrin.Propylene dichloride.Propylene glycol.Propylene oxide.Pyridine.Quinone.Resorcinol.Resorcylic acid.Salicylic acid.Sodium acetate.Sodium benzoate.Sodium carboxymethyl cellulose.Sodium chtoroacetate.Sodium formate.Sodium phenate.Sorbic acid.Styrene.Succinic acid.Succinonitnle.Sulfanilic acid.Suttotane.Tannic acid.Terephtnalic acid.Tetractuoroetnanes.Tetrachlorophthatic anhydride.Tetraethyllead.Tetrahydrcnaphtnalene.Tetrahycrophmatlc anhydride.Tetramethyl lead.Tetramethylenediamine.Tetramethylethylenediamine.Toluene.Tcluene-2,4-diamine.Toluene-z,4-diisocyanate.Toluene dtisocyanates (mixture)

Nitrobenzene.Nitrobenzoic acid (o.m. and p).Nitroethane.Nitromethane.z-Nltrophenol,Nitropropane.Nitrotoluene.Nonene.NonylphenoLOctylphenol.Paraldehyde.Pentaerythtftol.n-pentane.t-pentenePercnloroetnytene.Perctuorcmethyt mercaptan.o-phenettoine.p-phenetidine.Phenol.Phenolsulfonic acids.

98-95-327178-83-2'79-24-3 .75-52-5 .88-75-5 ...25322-01-4 .1321-12-6 .27215-95-8 .25154-52-3 .27193-28-8 .123-63-7.115-77-5 ..109-66-{) .109-67-1127-18-4.594-42-3 .94-70-2 .156-43-4.108-95-2 .98-67-9,585-

38-6, 609-461,1333--39-7-'.

91-40-7 .("I·75-44-5 .85-44-9 .85-41--6.108-99--6 .110--85-0.9003-29-6,

25038-29-7'.25322-68-3 .25322-69-4 .123-38-8 ...79-09-4 .71-23-8.107-10-8.540-54-5.115-07-1 .127-00-4.78-87-5 .57-55-6.75-56-9110-85-1106-51-4.106-46-3 .27138-57-4 .69-72-7127-09-3 ...532~32-1 .9004-32-4 .3926-62-3.141-53-7 .139-02-6 ...110-44-1.100-42-5 ...110-15-6.110-61-2.121-57-3 .126-33--0 .1401-55-4 .100-21-6 ....79-34-5" .117-08-8.78-00-2119-64-2 ..85-43-8 .75-74-1 ..110--60-1 .110-18-9.108-88-3.95-80-7 .584-84-926471-62-5

454

CERTIFICATE OF SERVICE

I, Cynthia Hook, hereby certify that a copy of this permit has been mailed by first class mail to

Quantum Resources Management, LLC - Walker Creek Production Facility, 1775 Sherman

Cynthia Hook, AAII, Air Division

Documents

ADEQ the TEG Dehydrator and the TEG Reboiler.ificant Activities list under Group A-I3 and Group A-I, Quantum Resources Management,