Alpine Analytical Laboratory

Alpine Analytical Laboratory

Price List

&

Reference Guide

1315 Cherry Ave. Helena, Montana 59601

www.alpineanalytical.com

(406) 449-6282

Fax (406) 449-1390

Alpine Analytical Laboratory March 2019

Alpine Analytical, Laboratory is an independent analytical laboratory located in beautiful Helena, MT.

Founded in 1994 and continually growing and updating our facilities, instrumentation and procedures

to stay in tune with the latest regulations and technologies. Through this growth we have remained committed

to providing documented high quality analytical data with rapid turnaround while maintaining personalized customer

service.

We are open to receive samples 8 am through 5 pm Monday through Friday, except holidays. If necessary other times

can be arranged by appointment.

Alpine Analytical Laboratory has a comprehensive, written QA/QC program designed to insure consistent

high quality analytical data that meets or exceeds criteria established by the USEPA and state agencies. Quality

control samples consisting of blanks, duplicates, spikes, and known samples, as applicable, are analyzed as an

integral part of every analysis batch. Results of these analyses are routinely reported at no additional cost

as part of our comprehensive data package. Our goal is to provide data that is technically sound and legally defensable.

Excellent customer service consists not only of generating quality data suitable for the customers need but also

providing the data to the customer as close as possible to when the customer would like the results, if not before.

Turnaround time can be very critical. Rapid turnaround of sample results can save you time and money. In some

instances it can even help to minimize your liability. We routinely report results within one week of sample receipt

by our laboratory. When you have a problem and need results right away, we understand. We can provide rush

analyses for most parameters in a matter of hours at an additional cost.

Upon receipt of a sample we will commit in writing to an analysis completion date and time upon request..

General Information:

Hours of Operation

Quality Data

Rapid Turnaround


We have designed our reports to be complete and easily understood. Each report includes date of analysis

and reference to method used. Batch specific quality control data is generated for every sample and can be included

in reports at no additional charge. The report can be custom designed to meet your specific needs, both in

hard copy and electronic format.

Results of analyses performed are confidential information and will be provided only to you and anyone else

whom you have approved.

Alpine Analytical Laboratory provides at no charge to its customers, properly prepared sample containers,

preservatives and chain of custody forms. We will also provide sampling instructions upon request, or assist you in

locating someone to collect your samples.

Please see the miscellaneous section of this Price List and Reference guide for recommended containers,

preservatives, and holding times.

Samples will be held for at least 30 days after the report is generated. Longer archiving can be arranged if necessary.

Samples that are not-hazardous will be disposed at no cost. Disposal of samples determined to be hazardous will

be the responsibility of the person or organization submitting the sample.

We require chain of custody forms for all samples submitted for analysis. It provides evidence of sample handling,

which is important in cases involving litigation. It also expedites the measurement process and adds confidence

to the results.

Sample Disposal

Chain of Custody

Reporting

Sample Containers


Analytical data, to be valuable, must accurately describe the characteristics and/or concentrations of the

constituents of the material being sampled and be appropriate for its intended purpose. If requested our qualified

staff can assist you in selecting the proper sampling, preservation and analysis methods to meet this purpose.

Use of the proper methods and appropriate holding times is vitally important to obtaining useful analytical data.

Alpine Analytical Laboratory uses methodology accepted and set forth by US EPA,

American Public Health Association (APHA), the American Society for Testing and Materials (ASTM), the

Association of Official Analytical Chemists (AOAC), the National Institute for Occupational Safety and Health (NIOSH),

the Soil Science Society of America (SSSA), and various other state and federal agencies.

The prices listed on the following pages are for single parameter analysis in small quantities. Suite prices

and volume discounts are available. The methods and detection limits listed are those routinely used by our

laboratory. Many additional parameters, methods, and detection limits are available. We will, upon request,

provide a price quotation based upon your analytical needs.

In the event that you need results right away, we can perform most analyses within a matter of minutes or hours.

The cost for this service is usually double the normal cost, but depends upon the situation. Samples that are

submitted such that we need to work weekends or holidays are also charged a rush charge.

Our normal terms are net 30 days. After 30 days, interest charges may be added.

Methodology

Prices and Discounts

Rush Charges

Terms


Reporting

Parameter Limit Units Method Description Price

Alkalinity, Total as CaCO3 1 mg/L SM 2320 B Titrimetric $15.00

Ammonia as N 0.08 mg/L SM 4500 NH3 B Ion Specific Electrode $15.00

Biochemical Oxygen Demand (BOD) 1 mg/L SM 5210 B 5 Day, Ion Specific Electrode $45.00

Bicarbonate as HCO3 1 mg/L SM 2320 B Titrimetric $15.00

Carbonaceous BOD (CBOD) 1 mg/L SM5210 B 5 Day, Ion Specific Electrode $45.00

Carbonate as CO3 1 mg/L SM 2320 B Titrimetric $15.00

Carbon Dioxide as CO2 1 mg/L SM 2320 B Titrimetric $15.00

Chemical Oxygen Demand (COD) 1 mg/L EPA 410.4 Spectrophotometric $30.00

Chloride 0.1 mg/L EPA 300.0 Ion Chromatographic $15.00

Chlorine Residual 0.1 mg/L SM 4500 Cl G Spectrophotometric $10.00

Color 0 color units SM 2120 B Comparison $20.00

Conductance, Specific 1 mmho/cm EPA 120.1 Electrode $10.00

Cyanide, WAD 0.05 mg/L SM 4500CN I Micro-Dist $55.00

Cyanide, Free 0.05 mg/L SM 4500CN F Ion Specific Electrode $40.00

Cyanide, Total 0.05 mg/L SM 4500CN C Micro-Dist $55.00

Fluoride 0.1 mg/L SM 4500 F Ion Specific Electrode $15.00

Formaldehyde 0.1 mg/L NCASI Colorimetric $30.00

Hardness, Total as CaCO3 1 mg/L SM 2340 B ICP $24.00

Kjeldahl Nitrogen as N, Total 0.2 mg/L SM 4500 Norg Ion Specific Electrode $30.00

MBAS (Surfactants) 1 mg/L SM 5540 C Spectrophotometric $15.00

WATER - NONMETALS


Reporting


WATER - NONMETALS

Methane 1 mg/L EPA 8015M GC-FID, Headspace $50.00

Methane 1 mg/L EPA 3810 GC-FID, Headspace $50.00

Nitrate as N 0.01 mg/L EPA 300.0 Ion Chromatographic $15.00

Nitrite as N 0.01 mg/L EPA 300.0 Ion Chromatographic $15.00

Nitrate + Nitrite as N 0.01 mg/L EPA 300.0 Ion Chromatographic $15.00

Nitrogen, Total 0.1 mg/L SM 4500 N C Persulfate $40.00

Nitrogen, Total 0.2 mg/L Calculated Calculated from TKN and Nitrate N/C

Oil & Grease, Gravimetric (Hexane) 1 mg/L EPA 1664 Gravimetric $60.00

Organic Carbon, Total (TOC) 1 mg/L SM 5310 B Combustion $35.00

Organic Carbon, Dissolved (DOC) 1 mg/L SM 5310 B Combustion $35.00

Oxygen, Dissolved 1 mg/L SM 4500 O Electrode $10.00

pH 0.1 s.u. SM 4500 H+

Electrode $10.00

Phenols, Total 0.01 mg/L EPA 420.1 Spectrophotometric $30.00

Phosphorus, Ortho 0.01 mg/L EPA 300.0 Ion Chromatographic $15.00

Phosphorus, Ortho 0.01 mg/L EPA 365.2 Spectrophotometric $15.00

Phosphorus, Ortho, low level 0.005 mg/L EPA 365.2 Spectrophotometric $25.00

Phosphorous, Hydrolyzable 0.01 mg/L EPA 365.2 Spectrophotometric $15.00

Phosphorus, Total 0.01 mg/L EPA 200.7 ICP $20.00

Phosphorous, Total 0.01 mg/L SM 4500 P E Spectrophotometric $20.00

Phosphorus, Total, low level 0.005 mg/L SM 4500 P E Spectrophotometric $25.00


Reporting


WATER - NONMETALS

Residue, Filterable (TDS) 5 mg/L SM 2540 C Gravimetric $15.00

Residue, Non-filterable (TSS) 1 mg/L SM 2540 D Gravimetric $15.00

Residue, Total 10 mg/L SM 2540 B Gravimetric $10.00

Residue, Volatile (VSS) 10 mg/L SM 2540 E Gravimetric - Combustion $25.00

Settleable Matter 0.5 ml/L SM 2540 F Imhoff Cone $10.00

Specific Gravity --- --- SM 2710 F Hydrometer $10.00

Sulfate 0.5 mg/L EPA 300.0 Ion Chromatographic $15.00

Sulfide 1 mg/L SM 4500 S2 F Iodometric titration $45.00

Thiosulfate 1 mg/L EPA 300.0 Ion Chromatographic $25.00

Turbidity 0.01 NTU EPA 180.1 Nephelometric $10.00


Reporting


Aluminum 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Aluminum, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Antimony 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Antimony, low level 0.0005 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Arsenic 1 mg/L EPA 200.7 / 6010 ICP $12.00

Arsenic, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Arsenic Speciation (+3, +5) 0.005 mg/L EPA 206.3 ICP-MS $34.00

Barium 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Barium, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Beryllium 1.0 mg/L EPA 200.7 / 6010 ICP $12.00

Beryllium, low level 0.0008 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Bismuth 2.0 mg/L EPA 200.7 / 6010 ICP $14.00

Bismuth 0.002 mg/L EPA 200.8 / 6020 ICP-MS $50.00

Boron 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Cadmium 0.0005 EPA 200.8 / 6020 ICP-MS $22.00

Cadmium, low level 0.00003 mg/L EPA 200.8 / 6020 ICP-MS $44.00

Calcium 1 mg/L EPA 200.7 ICP $12.00

WATER - METALS


Reporting


WATER - METALS

Chromium 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Chromium, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Chromium, Hexavalent 0.01 mg/L SM 3500 Cr B Spectrophotometric $35.00

Cobalt 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Cobalt, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Copper 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Copper, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Gold 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Gold, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Iron 0.02 mg/L EPA 200.7 / 6010 ICP $12.00

Lead 0.5 mg/L EPA 200.7 / 6010 ICP $12.00

Lead, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Lead, ultra low level 0.0003 mg/L EPA 200.8 / 6020 ICP-MS $30.00

Lithium 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Magnesium 1 mg/L EPA 200.7 / 6010 ICP $12.00

Manganese 0.05 mg/L EPA 200.7 / 6010 ICP $12.00

Manganese, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Mercury, low level 0.0006 mg/L EPA 200.8 / 6020 ICP-MS $27.00

Mercury,ultra low level 0.00001 mg/L EPA 200.8 / 6020 ICP-MS $54.00


Reporting


WATER - METALS

Molybdenum 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Molybdenum, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Nickel 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Nickel, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Potassium 1 mg/L SM 3500 K B Flame Photometric $12.00

Potassium 10 mg/L EPA 200.7 / 6010 ICP $12.00

Selenium 1 mg/L EPA 200.7 / 6010 ICP $12.00

Selenium, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Silicon 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Silver 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Silver, low level 0.0002 mg/L EPA 200.8 / 6020 ICP-MS $30.00

Sodium 1 mg/L SM 3500 Na B Flame Photometric $12.00

Sodium 1 mg/L EPA 200.7 / 6010 ICP $12.00

Strontium 0.5 mg/L EPA 200.7 / 6010 ICP $12.00

Thallium 0.1 mg/L EPA 200.7 / 6010 ICP $12.00

Thallium, low level 0.0002 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Tin 0.1 mg/L EPA 200.7 / 6010 ICP $112.00

Uranium 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Uranium, low level 0.0002 mg/L EPA 200.8 / 6020 ICP-MS $30.00


Reporting


WATER - METALS

Vanadium 0.5 mg/L EPA 200.7 / 6010 ICP $12.00

Vanadium, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Zinc 0.05 mg/L EPA 200.7 / 6010 ICP $12.00

Zinc, low level 0.001 mg/L EPA 200.8 / 6020 ICP-MS $22.00

Filtering sample for metals $10.00

Digestion for total metals $20.00


Reporting


Total Coliform + E. Coli 1 colonies/100 mL SM 9223 B Quantitray $22.00

Total Coliform + E. Coli P/A presence/absence SM 9223 B Enzyme Substrate $22.00

Total Coliform 1 colonies/100 mL SM 9223 B Quantitray $22.00

Heterotrophic Plate Count 1 colonies/100 mL Quantitray Call

Slime Producing Bacteria P/A presence/absence BART SLYM BART $35.00

Iron-Related Bacteria P/A presence/absence BART IRB BART $35.00

Sulfate-Reducing Bacteria P/A presence/absence BART SRB BART $35.00

MICROBIOLOGICAL


Price

pH Magnesium Alkalinity

Specific Conductance Hardness Chloride $100.00

Total Dissolved Solids Sodium Nitrate+Nitrite

Calcium Potassium Sulfate

Aluminum Chromium Molybdenum

Antimony Cobalt Nickel

Arsenic Copper Selenium $65.00

Barium Iron Silver

Beryllium Lead Thallium

Boron Magnesium Vanadium

Cadmium Manganese Zinc

Calcium

WATER - SUITES

Parameters

CATION-ANION BALANCE

METAL SCAN - HIGH LEVEL (>1.0 mg/L)Analysis by ICP for the following elements:


Price

WATER - SUITES

Parameters

Aluminum Chromium Molybdenum

Antimony Cobalt Nickel

Arsenic Copper Selenium $125.00

Barium Iron Silver

Beryllium Lead Thallium

Boron Magnesium Uranium

Cadmium Manganese Vanadium

Calcium Zinc

METAL SCAN - LOW LEVEL Analysis by ICP or ICP-MS for the following elements:


Price

WATER - SUITES

Parameters

pH Fluoride Chromium

Specific Conductance Nitrate + Nitrite Iron $101.00

Total Dissolved Solids Sulfate Manganese

Calcium Total Coliform Lead

Magnesium Arsenic Selenium

Hardness Cadmium Uranium

Drinking Water 101


Price

WATER - SUITES

Parameters

pH Alkalinity Chromium

Specific Conductance Chloride Iron $151.00

Total Dissolved Solids Fluoride Lead

Calcium Nitrate + Nitrite Manganese

Magnesium Sulfate Selenium

Hardness Total Coliform Uranium

Sodium Arsenic Arsenic III & V

Potassium Cadmium

Drinking Water 151


Price

WATER - SUITES

Parameters

pH Magnesium Alkalinity

Specific Conductance Hardness Chloride

Total Dissolved Solids Sodium Nitrate+Nitrite

Calcium Potassium Sulfate

Total Coliform Fluoride

$201.00

Aluminum Cobalt Silver

Antimony Copper Thallium

Arsenic Iron Uranium

Barium Lead Vanadium

Beryllium Magnesium Zinc

Boron Manganese

Cadmium Molybdenum

Calcium Nickel

Chromium Selenium

Drinking Water 201

Analysis by ICP or ICP-MS for the following elements:


Parameter

Reporting

Limit Matrix Method Description Price

VPH See Soil MADEP VPH GC-FID/PID, Purge & Trap $130.00

(Volatile Petroleum Hydrocarbons ) Table Water MADEP VPH GC-FID/PID, Purge & Trap $120.00

Below Air MADEP VPH GC-FID/PID, Purge & Trap $120.00

BTEX See Soil EPA 8021 GC-PID, Purge & Trap $75.00

(Benzene, Toluene, Ethylbenzene, & Xylenes ) Table Water EPA 8021 GC-PID, Purge & Trap $75.00

Below Air EPA 8021 GC-PID, Purge & Trap $75.00

MBTEXN See Soil EPA 8021 GC-PID, Purge & Trap $90.00

(BTEX plus MTBE and Naphthalene ) Table Water EPA 8021 GC-PID, Purge & Trap $90.00

Below Air EPA 8021 GC-PID, Purge & Trap $90.00

MBTEX + GRO See Soil GRO GC-FID, Purge & Trap $120.00

(MBTEX plus Gasoline Range Organics ) Table Water GRO GC-FID, Purge & Trap $120.00

Below Air GRO GC-FID, Purge & Trap $120.00

VPH is a method employed to separate the aliphatic and aromatic fractions in the sample. Through the use of two different detectors on the gas

chromatograph it is possible to separate the sample into aliphatic and aromatic fractions. The specificity of the photoionization detector allows the

aromatics to be measured separately from the aliphatics. Whereas the flame ionization detector responds to both aromatics and aliphatics, but

cannot distinguish between them. The presence of MTBE and/or Naphthalene are confirmed by GC-MS.

The parameters measured by the VPH method and the associated reporting limits are listed below.

Parameter Water Air

MTBE (Methyltertbutyl ether) 2 mg/L 3 mg/M3

Benzene 0.5 mg/L 1 mg/M3

Toluene 0.5 mg/L 1 mg/M3

Ethylbenzene 0.5 mg/L 1 mg/M3

Xylenes (o, m, p) 0.5 mg/L 1 mg/M3

Naphthalene 1 mg/L 2 mg/M3

C5-C8 Aliphatics 20 mg/L 30 mg/M3

C9-C12 Aliphatics 20 mg/L 30 mg/M3

C9-C10 Aromatics 20 mg/L 30 mg/M3

TPH (Total Purgeable Hydrocarbons) 20 mg/L 30 mg/M3

2 mg/g

0.05 mg/g

0.15 mg/g

0.1mg/g

2 mg/g

2 mg/g

2 mg/g

ORGANICS

Reporting Limits

Soil

0.1 mg/g

0.05 mg/g

0.05 mg/g


Parameter

Reporting

Limit Matrix Method Description Price

EPH Screen See Soil MADEP EPH (modified) GC-FID $85.00

(Extractable Petroleum Hydrocarbons ) Table Water MADEP EPH (modified) GC-FID $75.00

EPH Screen plus aliphatic/aromatic separation See Soil MADEP EPH (modified) GC-FID $225.00

Table Water MADEP EPH (modified) GC-FID $215.00

EPH Screen plus aliphatic/aromatic separation See Soil MADEP EPH (modified) GC-FID $310.00

also include polynuclear aromatic hydrocarbons Table Water MADEP EPH (modified) GC-FID / GC-MS $400.00

PAH's See Soil EPA 8270 GC-MS $200.00

(Polynuclear Aromatic Hydrocarbons ) Table Water EPA 8270 GC-MS $200.00

Carbon Scan 0.10% all GC-FID GC-FID $110.00

A screening limit of 200 mg/g for soil and 1000 mg/L for water has been established by MTDEQ. Samples with TEH (Total Extractable Hydrocarbons)

concentrations do not need further analysis unless specifically requested by MTDEQ. For soil samples exceeding the screening limits,

the separation into aliphatic and aromatic fractions plus MBTEXN analysis is required (in most cases). The need for PAH analysis is determined

on a case by case basis by MTDEQ, as is the need for aromatic/aliphatic separation on water samples. The table below lists the parameters

measured plus their reporting limits.

Parameter Water

C9-C18 Aliphatics 300 mg/L

C19-C36 Aliphatics 300 mg/L

C11-C22 Aromatics 300 mg/L

TEH (Total Extractable Hydrocarbons ) 300 mg/L

Acenaphthene 10 ug/L

Anthracene 10 mg/L

Benzo(a)anthracene 10 mg/L

Benzo(a)pyrene 10 mg/L

Benzo(b,k)fluoranthene 10 mg/L

Chrysene 10 mg/L

Dibenzo(a,h)anthracene 10 mg/L

Fluoranthene 10 mg/L

Fluorene 10 mg/L

Indeno(1,2,3-cd)pyrene 10 mg/L

Naphthalene 10 mg/L

2-Methylnaphthalene 10 mg/L

Pyrene 10 mg/L

0.33 mg/g

0.33 mg/g

0.33 mg/g

0.66 mg/g

0.33 mg/g

0.33 mg/g

0.66 mg/g

0.33 mg/g

20 mg/g

0.33 mg/g

0.33 mg/g

0.33 mg/g

0.33 mg/g

0.66 mg/g

ORGANICS

Reporting Limits

Soil

20 mg/g

20 mg/g

20 mg/g


Parameter

Reporting

Limit Matrix Method Description PriceVOC's see Water EPA 8260 GC-MS, Purge & Trap $210.00

(long list ) table Soil EPA 8260 GC-MS, Purge & Trap $210.00

Reporting Limit Reporting Limit

Parameter Water (mg/L) Soil (mg/g) Parameter Water (mg/L) Soil (mg/g)

Acetone 50 10 2,2-Dichloropropane 1.0 0.20

Benzene 1.0 0.20 1,1-Dichloropropene 1.0 0.20

Bromobenzene 1.0 0.20 cis-1,3-Dichloropropene 1.0 0.20

Bromochloromethane 1.0 0.20 trans -1,3-Dichloropropene 1.0 0.20

Bromodichloromethane 1.0 0.20 Ethylbenzene 1.0 0.20

Bromoform 1.0 0.20 Hexachlorobutadiene 1.0 0.20

Bromomethane 1.0 0.20 2-Hexanone 20 4.0

n -Butylbenzene 1.0 0.20 Iodomethane 1.0 0.20

sec -Butylbenzene 1.0 0.20 Isopropylbenzene 1.0 0.20

tert -Butylbenzene 1.0 0.20 p-Isopropyltoluene 1.0 0.20

Carbon Disulfide 1.0 0.20 Methyl t-butyl Ether (MTBE) 1.0 0.20

Carbon Tetrachloride 1.0 0.20 Methyl Ethyl Ketone 20 4.0

Chlorobenzene 1.0 0.20 Methyl Isobutyl Ketone 20 4.0

Chloroethane 1.0 0.20 Methylene Chloride 1.0 0.20

2-Chloroethyl Vinyl Ether 1.0 0.20 Naphthalene 1.0 0.20

Chloroform 1.0 0.20 n -Propylbenzene 1.0 0.20

Chloromethane 1.0 0.20 Styrene 1.0 0.20

2-Chlorotoluene 1.0 0.20 1,1,1,2-Tetrachloroethane 1.0 0.20

4-Chlorotoluene 1.0 0.20 1,1,2,2-Tetrachloroethane 1.0 0.20

1,2-Dibromo-3-chloropropane 1.0 0.20 Tetrachloroethene (PCE) 1.0 0.20

1,2-Dibromoethane (EDB) 1.0 0.20 Toluene 1.0 0.20

Dibromomethane 1.0 0.20 1,2,3-Trichlorobenzene 1.0 0.20

1,2-Dichlorobenzene 1.0 0.20 1,2,4-Trichlorobenzene 1.0 0.20

1,3-Dichlorobenzene 1.0 0.20 1,1,1-Trichloroethane 1.0 0.20

1,4-Dichlorobenzene 1.0 0.20 1,1,2-Trichloroethane 1.0 0.20

Dichlorodifluoromethane 1.0 0.20 Trichloroethene (TCE) 1.0 0.20

1,1-Dichloroethane 1.0 0.20 Trichlorofluoromethane 1.0 0.20

1,2-Dichloroethane 1.0 0.20 1,2,3-Trichloropropane 1.0 0.20

1,1-Dichloroethene 1.0 0.20 1,2,4-Trimethylbenzene 1.0 0.20

cis -1,2-Dichloroethene 1.0 0.20 1,3,5-Trimethylbenzene 1.0 0.20

trans -1,2-Dichloroethene 1.0 0.20 Vinyl Acetate 1.0 0.20

1,2-Dichloropropane 1.0 0.20 Vinyl Chloride 1.0 0.20

1,3-Dichloropropane 1.0 0.20 0-Xylene 1.0 0.20

m,p-Xylene 1.0 0.20

ORGANICS


Parameter

Reporting

Limit Matrix Method Description PriceVOC's see Water EPA 524.2 GC-MS, Purge & Trap $125.00

(Volatile Organic Compounds ) table Water EPA 624/8260 GC-MS, Purge & Trap $125.00(short list ) Soil EPA 8260 GC-MS, Purge & Trap $125.00

0.001 mg/g Soil EPA 3810 GC-FID, Headspace $50.00Methane 0.001 mg/L Water EPA 3810 GC-FID, Headspace $50.00

0.007 mg/L Air EPA 3810 GC-FID, Headspace $50.00



Benzene 1.0 0.20 2,2-Dichloropropane 1.0 0.20

Bromobenzene 1.0 0.20 1,1-Dichloropropene 1.0 0.20

Bromochloromethane 1.0 0.20 cis-1,3-Dichloropropene 1.0 0.20

Bromodichloromethane 1.0 0.20 trans -1,3-Dichloropropene 1.0 0.20

Bromoform 1.0 0.20 Ethylbenzene 1.0 0.20

Bromomethane 1.0 0.20 Methyl t-butyl Ether (MTBE) 1.0 0.20

Carbon Tetrachloride 1.0 0.20 Methylene Chloride 1.0 0.20

Chlorobenzene 1.0 0.20 Methyl Ethyl Ketone 1.0 0.20

Chloroethane 1.0 0.20 Styrene 1.0 0.20

2-Chloroethyl Vinyl Ether 1.0 0.20 1,1,1,2-Tetrachloroethane 1.0 0.20

Chloroform 1.0 0.20 1,1,2,2-Tetrachloroethane 1.0 0.20

Chloromethane 1.0 0.20 Tetrachloroethene (PCE) 1.0 0.20

2-Chlorotoluene 1.0 0.20 Toluene 1.0 0.20

4-Chlorotoluene 1.0 0.20 1,1,1-Trichloroethane 1.0 0.20

Dibromochloromethane 1.0 0.20 1,1,2-Trichloroethane 1.0 0.20

1,2-Dibromoethane 1.0 0.20 Trichloroethene (TCE) 1.0 0.20

Dibromomethane 1.0 0.20 Trichlorofluoromethane 1.0 0.20

1,2-Dichlorobenzene 1.0 0.20 1,2,3-Trichloropropane 1.0 0.20

1,3-Dichlorobenzene 1.0 0.20 Vinyl Chloride 1.0 0.20

1,4-Dichlorobenzene 1.0 0.20 0-Xylene 1.0 0.20

Dichlorodifluoromethane 1.0 0.20 m,p-Xylene 1.0 0.20

1,1-Dichloroethane 1.0 0.20

1,2-Dichloroethane 1.0 0.20

1,1-Dichloroethene 1.0 0.20

cis -1,2-Dichloroethene 1.0 0.20

trans -1,2-Dichloroethene 1.0 0.20

1,2-Dichloropropane 1.0 0.20

1,3-Dichloropropane 1.0 0.20

ORGANICS


Parameter

Reporting

Limit Method Description Price

SVOC's see EPA 8270 GC-MS $350.00

(Semi-Volatile Organic Compounds ) table EPA 8270 GC-MS $350.00



Phenols

4-Chloro-3-methylphenol 10 0.33 Bis(2-ethylhexyl phthalate 10 0.33

2-Chlorophenol 10 0.33 Butyl benzyl phthalate 10 0.33

4-Chlorophenol 10 0.33 Di-n-butyl phthalate 10 0.33

2-Methylphenol 10 0.33 Di-n-octyl phthalate 10 0.33

3-Methylphenol 10 0.33 Diethyl phthalate 10 0.33

4-Methylphenol 10 0.33 Dimethyl phthalate 10 0.33

2,4-Dichlorophenol 10 0.33

2,4-Dimethylphenol 10 0.33

4,6-Dinitro-2-methylphenol 50 1.65 N-nitrosodi-n-propylamine 10 0.33

2,4-Dinitrophenol 50 1.65 N-Nitrosodimethylamine 10 0.33

2-Nitrophenol 10 0.33 N-Nitrosodiphenylamine 10 0.33

4-Nitrophenol 50 1.65

Pentachlorophenol 50 1.65

Phenol 10 0.33

2,4,5-Trichlorophenol 10 0.33 2,4-Dinitrotoluene 10 0.33

2,4,6-Trichlorophenol 10 0.33 2,6-Dinitrotoluene 10 0.33

Polynuclear Aromatic Hydrocarbons Nitrobenzene 10 0.33

Acenaphthene 10 0.33 Isophorone 10 0.33

Acenaphthalene 10 0.33

Anthracene 10 0.33

Benzo(a)anthracene 10 0.33 Bis(2-chloroethyl ether 10 0.33

Benzo(b)fluoranthene 10 0.33 Bis(2-chloroethoxy) methane 10 0.33

Benzo(k)fluoranthene 10 0.33 Bis(2-chloroisopropyl) ether 10 0.33

Benzo(g,h,I)perylene 10 0.33 4-Bromophenyl phenyl ether 10 0.33

Benzo(a) pyrene 10 0.33 4-Chlorophenyl phenyl ether 10 0.33

Chrysene 10 0.33

Dibenzo(a,h)anthracene 10 0.33

Fluoranthene 10 0.33 2-Chloronaphthalene 10 0.33

Fluorene 10 0.33 1,2-Dichlorobenzene 10 0.33

Indeno(1,2,3-cd)pyrene 10 0.33 1,3-Dichlorobenzene 10 0.33

Naphthalene 10 0.33 1,4-Dichlorobenzene 10 0.33

Phenanthrene 10 0.33 Hexachlorobenzene 10 0.33

Pyrene 10 0.33 Hexachlorobutadiene 10 0.33

Hexachlorocyclopentadiene 10 0.33

Benzidine 20 0.66 Hexachloroethane 10 0.33

Pyridine 20 0.66 1,2,4-Trichlorobenzene 10 0.33

3,3'-Dichlorobenzidine 20 0.66

Nitroaromatics and Isophorone

Haloethers

Chlorinated Hydrocarbons

Benzidenes

ORGANICS

Matrix

Water

Soil

Phthalate Esters

Nitrosamines


Parameter

Reporting

Limit Method Description Price

Phenols see EPA 8270 GC-MS $160.00

(Acid Extractables ) table EPA 8270 GC-MS $160.00

Phthalate Esters see EPA 8270 GC-MS $180.00

table EPA 8270 GC-MS $180.00

PAH's see EPA 8270 GC-MS $200.00

(Polynuclear Aromatic Compounds ) table EPA 8270 GC-MS $200.00



Phenols

4-Chloro-3-methylphenol 10 0.33 Bis(2-ethylhexyl phthalate 10 0.33

2-Chlorophenol 10 0.33 Butyl benzyl phthalate 10 0.33

4-Chlorophenol 10 0.33 Di-n-butyl phthalate 10 0.33

2-Methylphenol 10 0.33 Di-n-octyl phthalate 10 0.33

3-Methylphenol 10 0.33 Diethyl phthalate 10 0.33

4-Methylphenol 10 0.33 Dimethyl phthalate 10 0.33

2,4-Dichlorophenol 10 0.33

2,4-Dimethylphenol 10 0.33

4,6-Dinitro-2-methylphenol 50 1.65

2,4-Dinitrophenol 50 1.65



Pentachlorophenol 50 1.65

Phenol 10 0.33

2,4,5-Trichlorophenol 10 0.33

2,4,6-Trichlorophenol 10 0.33

Polynuclear Aromatic Hydrocarbons

Acenaphthene 10 0.33

Acenaphthalene 10 0.33

Anthracene 10 0.33

Benzo(a)anthracene 10 0.33

Benzo(b)fluoranthene 10 0.33

Benzo(k)fluoranthene 10 0.33

Benzo(g,h,I)perylene 10 0.33

Benzo(a) pyrene 10 0.33

Chrysene 10 0.33

Dibenzo(a,h)anthracene 10 0.33

Fluoranthene 10 0.33

Fluorene 10 0.33

Indeno(1,2,3-cd)pyrene 10 0.33

Naphthalene 10 0.33

Phenanthrene 10 0.33

Pyrene 10 0.33

Water

Soil

Phthalate Esters

ORGANICS

Matrix

Water

Soil

Water

Soil


Parameter Method Description

Reporting

Limit mg/L

Regulatory

Limit mg/L Price

TCLP Extraction (metals, base-neutrals, acid

extractables, pesticides, & herbicides) EPA 1311 20 hour --- --- $50.00

TCLP ZHE (Zero Headspace Extraction ) for volatiles EPA 1311 20 hour, ZHE --- --- $100.00

Arsenic (As) EPA 6020 ICP/MS 0.5 5.0 $22.00

Barium (Ba) EPA 6010 ICP 10 100 $12.00

Cadmium (Cd) EPA 6010 ICP 0.1 1.0 $12.00

Chromium (Cr) EPA 6010 ICP 0.5 5.0 $12.00

Lead (Pb) EPA 6010 ICP 0.5 5.0 $12.00

Mercury (Hg) EPA 6020 ICP/MS 0.02 0.2 $27.00

Selenium (Se) EPA 6020 ICP/MS 0.1 1.0 $22.00

Silver (Ag) EPA 6010 ICP 0.5 5.0 $12.00

2,4-Dinitrotoluene EPA 8270 GC-MS 0.05 0.13 $300.00

Hexachloro-1,3-butadiene EPA 8270 GC-MS 0.05 0.50

Hexachlorobenzene EPA 8270 GC-MS 0.05 0.13

Hexachloroethane EPA 8270 GC-MS 0.05 3.0

Nitrobenzene EPA 8270 GC-MS 0.05 2.0

Pyridine EPA 8270 GC-MS 0.10 5.0

o,m,p Cresol EPA 8270 GC-MS 0.15 200 $250.00

Pentachlorophenol EPA 8270 GC-MS 0.25 100

2,4,5-Trichlorophenol EPA 8270 GC-MS 0.05 400

2,4,6-Trichlorophenol EPA 8270 GC-MS 0.05 2

Waste - TCLP (Toxicity Characteristic Leaching Procedure )

Extraction

Metals (requires TCLP extraction )

Base-Neutral Extractables (requires TCLP extraction )

Acid Extractables (requires TCLP extraction )



Reporting

Limit Price

Digestion for total metals EPA 3050 acid digestion --- $20.00

Arsenic (As) EPA 6020 ICP-MS 5.0 mg/Kg $22.00

Barium (Ba) EPA 6010 ICP 100 mg/Kg $12.00

Cadmium (Cd) EPA 6010 ICP 1.0 mg/Kg $12.00

Chromium (Cr) EPA 6010 ICP 5.0 mg/Kg $12.00

Copper (Cu) EPA 6010 ICP 5.0 mg/Kg $12.00

Lead (Pb) EPA 6010 ICP 5.0 mg/Kg $12.00

Mercury (Hg) EPA 6020 ICP-MS 1.0 mg/Kg $27.00

Nickel (Ni) EPA 6010 ICP 5.0 mg/Kg $12.00

Molybdenum (Mo) EPA 6010 ICP 5.0 mg/Kg $12.00

Selenium (Se) EPA 6020 ICP-MS 5.0 mg/Kg $22.00

Silver (Ag) EPA 6010 ICP 5.0 mg/Kg $12.00

Zinc (Zn) EPA 6010 ICP 5.0 mg/Kg $12.00

Flashpoint EPA 1010 Pensky-Martins --- $40.00

Loss on ignition Ignition at 600oC Ignition at 600

oC --- $20.00

Moisture Dry at 105oC Dry at 105

oC --- $10.00

Paint Filter Test EPA 9095 filter --- $10.00

pH EPA 9040/9045 electrode --- $10.00

Solids Dry at 105oC Dry at 105

oC --- $10.00

Total Kjeldahl Nitrogen (TKN ) EPA 351.4 digestion/electrode 0.5 mg/Kg $35.00

Inquire for pricing on all other parameters

Waste

Metals Digestion

Total Metals (requires digestion )

Miscellaneous


Parameter Method

Reporting

Limit Price

Digestion EPA 3050

Arsenic (As) EPA 6020 5.0 mg/Kg

Barium (Ba) EPA 6010 100 mg/Kg

Cadmium (Cd) EPA 6010 1.0 mg/Kg

Chromium (Cr) EPA 6010 5.0 mg/Kg $151.00

Lead (Pb) EPA 6010 5.0 mg/Kg

Mercury (Hg) EPA 6020 1.0 mg/Kg

Selenium (Se) EPA 6020 5.0 mg/Kg

Silver (Ag) EPA 6010 5.0 mg/Kg

RCRA Metals

Total RCRA Metals



Reporting

Limit mg/L

Regulatory

Limit mg/L Price

Benzene EPA 8260 GC-MS, purge & trap 0.01 0.5 $150.00

Carbon Tetrachloride EPA 8260 GC-MS, purge & trap 0.01 0.5

Chlorobenzene EPA 8260 GC-MS, purge & trap 0.01 100

Chloroform EPA 8260 GC-MS, purge & trap 0.01 6.0

1,4-Dichlorobenzene EPA 8260 GC-MS, purge & trap 0.01 7.5

1,2-Dichloroethane EPA 8260 GC-MS, purge & trap 0.01 0.5

1,1-Dichloroethylene EPA 8260 GC-MS, purge & trap 0.01 0.7

Methyl ethyl ketone (MEK ) EPA 8260 GC-MS, purge & trap 0.25 200

Tetrachloroethylene (PCE ) EPA 8260 GC-MS, purge & trap 0.01 0.5

Trichloroethylene (TCE ) EPA 8260 GC-MS, purge & trap 0.01 0.7

Vinyl Chloride EPA 8260 GC-MS, purge & trap 0.01 0.2


Reporting

Limit mg/L

Regulatory

Limit mg/L Price

SPLP Extraction (metals, base-neutrals, acid

extractables, pesticides, & herbicides)EPA 1312 20 hour --- --- $50.00

SPLP ZHE (Zero Headspace Extraction ) for volatiles EPA 1312 20 hour, ZHE --- --- $100.00

All other SPLP analyses and price are the same as for TCLP.

Waste - TCLP (Toxicity Characteristic Leaching Procedure )

Volatiles (requires TCLP ZHE extraction )

SPLP (Synthetic Precipitation Leaching Procedure )

Extraction


Parameter Reporting Limit Units Price

Sample preparation --- --- InquireAcid-Base Potential 1 T CaCO3/1000T $25.00

Acid Potential 1 T CaCO3/1000T $15.00

Alkalinity, saturated paste 0.01 meq/L $20.00

Ammonia as N 1 mg/g $15.00

Cation Exchange Capacity (CEC) 1 meq/100g $25.00

Chloride 1 mg/g $15.00

Conductivity, saturated paste 0.01 mmho/cm $15.00

Moisture 0.1 % $10.00

Neutralization Potential 1 TCaCO3/1000T $15.00

Nitrate as N 1 mg/g $15.00

Organic Matter 0.1 % $20.00

pH, marble --- s.u. $30.00

pH, saturated paste --- s.u. $15.00

Phosphorus, NaHCO3 1 mg/g $20.00

Particle Size, sieve analysis 0.1 % $10.00/sieve

Particle Size, sand,silt clay 1 % $20.00

Potassium 1 mg/g $10.00

Saturation Percentage 0.1 % $10.00

Sodium Adsorption Ratio (includes Na, Ca, Mg) 0.01 --- $30.00

Sodium, available 0.01 meq/100g $20.00

Sodium, exchangable 0.01 meq/100g $20.00

Sulfate 0.1 mg/g $15.00

Total Nitrogen as N 1 mg/g $40.00

Total Kjeldahl Nitrogen as N 1 mg/g $45.00

Sample preparation charge applies to all analyses except: Conductivity, moisture, Organic matter, pH, particle size, and saturation percentage.

SOIL


Parameter Reporting Limit Units Price

SOIL

Digestion for metals --- --- $20.00

AquaRegia Digestion for metals $30.00

HydreoFluoric Acid Digestion for metals $30.00

Bomb Digestion for metals --- --- $40.00

Arsenic 0.02 mg/g $22.00

Barium 0.1 mg/g $12.00

Boron 0.1 mg/g $12.00

Cadmium 0.1 mg/g $12.00

Calcium 1 mg/g $12.00

Chromium 0.1 mg/g $12.00

Copper 0.1 mg/g $12.00

Lead 1 mg/g $12.00

Magnesium 1 mg/g $12.00

Manganese 0.1 mg/g $12.00

Mercury 0.1 mg/g $27.00

Molybdenum 0.1 mg/g $12.00

Nickel 0.1 mg/g $12.00

Selenium 0.01 mg/g $22.00

Zinc 0.1 mg/g $12.00

Digestion method: EPA 3050, SW846.

Analysis method: USEPA 6010/6020, SW846.


Documents

Alpine Analytical Laboratory