Upload
voanh
View
213
Download
0
Embed Size (px)
Citation preview
Analytical Report 482073for
Terranext
Project Manager: Chuck Gordon
WVBA
15-APR-14
3154-25
3725 E. Atlanta Ave, Phoenix, AZ 85040Ph: (602) 437-0330
Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Collected By: Client
Page 1 of 112 Final 1.000
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Project Manager: Chuck Gordon Terranext4050 E. Cotton Center Blvd.Phoenix, AZ 85040 Reference: TWA Report No(s): 482073 WVBA Project Address:
Chuck Gordon:
We are reporting to you the results of the analyses performed on the samples received under the project namereferenced above and identified with the TWA Report Number(s) 482073. All results being reported underthis Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.Subcontracted analyses are identified in this report with either the NELAC certification number of thesubcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance withNELAC standards. The uncertainty of measurement associated with the results of analysis reported is availableupon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC MatrixDuplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reported using allother available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter andreproduced in full, unless written approval is granted by TransWest Analytical. This report will be filed for atleast 5 years in our archives after which time it will be destroyed without further notice, unless otherwisearranged with you. The samples received, and described as recorded in Report No. 482073 will be filed for 60days, and after that time they will be properly disposed without further notice, unless otherwise arranged withyou. We reserve the right to return to you any unused samples, extracts or solutions related to them if weconsider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standardpractices, controlled substances under regulated protocols, etc).
We thank you for selecting TransWest Analytical to serve your analytical needs. If you have any questionsconcerning this report, please feel free to contact us at any time.
Respectfully,
15-APR-14
Project ManagerSkip Harden
Page 2 of 112 Final 1.000
CASE NARRATIVE
482073Work Order Number(s):15-APR-14Report Date: 3154-25Project ID:
Project Name: WVBA
Date Received:
Client Name: Terranext
03/27/2014
None
None
Sample receipt non conformances and comments:
Sample receipt non conformances and comments per sample:
Page 3 of 112 Final 1.000
Flagging Criteria
R5
All method blanks, laboratory spikes, and/or matrix spikes met quality control objectives for the parametersassociated with this Work Order except as detailed below or on the Data Qualifier page of this report. DataQualifiers used in this report are in accordance with ADEQ Arizona Data Qualifiers, Revision 3.0 9/20/2007.Data qualifiers (flags) contained within this analytical report have been issued to explain a quality controldeficiency, and do not affect the quality (validity) of the data unless noted otherwise in the case narrative.
MS/MSD RPD exceeded the laboratory acceptance limit. Recovery met acceptance criteria.
Arizona Flags
Page 4 of 112 Final 1.000
Sample Cross Reference 482073
Terranext, Phoenix, AZWVBA
Sample Id
43A Canal67A Canal83A CanalSalt CanalRID-105RID-106RID-107RID-96RID-108RID-109RID-110EQBRID-111RRID-113RID-114RID-104RID-102RID-103RID-101RID-100RID-99RID-97RID-95RID-94RID-93RID-91RID-92RID-90RID-89RID-88Trip Blank
03-27-14 07:2703-27-14 08:1503-27-14 08:4203-27-14 09:0403-27-14 09:2503-27-14 09:3903-27-14 09:5203-27-14 10:0003-27-14 10:0803-27-14 10:2103-27-14 10:3703-27-14 10:4303-27-14 10:3503-27-14 11:4603-27-14 11:5803-27-14 12:1503-27-14 12:3903-27-14 12:5603-27-14 13:1303-27-14 13:3203-27-14 13:4803-27-14 13:5603-27-14 14:0803-27-14 14:0003-27-14 14:3803-27-14 14:5103-27-14 15:0503-27-14 15:1803-27-14 15:3603-27-14 15:5003-27-14 07:27
Date Collected Lab Sample Id
482073-001482073-002482073-003482073-004482073-005482073-006482073-007482073-008482073-009482073-010482073-011482073-012482073-013482073-014482073-015482073-016482073-017482073-018482073-019482073-020482073-021482073-022482073-023482073-024482073-025482073-026482073-027482073-028482073-029482073-030482073-031
Sample DepthMatrix
WWWWWWWWWWWWWWWWWWWWWWWWWWWWWWW
Page 5 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 07.27 Date Collected:482073-001Lab Sample Id:WaterMatrix: 43A CanalSample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 11.26
04.11.14 05.01
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 6 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 07.27 Date Collected:482073-001Lab Sample Id:WaterMatrix: 43A CanalSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500
4.64 <1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.006.56
<5.00<1.50<2.00<1.501.91
<2.00<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.5000.610 0.580
<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09
Analysis Date
% Moisture:
Page 7 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 07.27 Date Collected:482073-001Lab Sample Id:WaterMatrix: 43A CanalSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
1.27 <2.00<5.00<5.00
<0.500<0.500
3.87 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
100104
9995
04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 8 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 08.15 Date Collected:482073-002Lab Sample Id:WaterMatrix: 67A CanalSample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 11.59
04.11.14 05.33
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 9 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 08.15 Date Collected:482073-002Lab Sample Id:WaterMatrix: 67A CanalSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500
3.74 <1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.005.82
<5.00<1.50<2.00<1.501.52
<2.00<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35
Analysis Date
% Moisture:
Page 10 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 08.15 Date Collected:482073-002Lab Sample Id:WaterMatrix: 67A CanalSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
1.17 <2.00<5.00<5.00
<0.500<0.500
3.56 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
100106101
95
04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 11 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 08.42 Date Collected:482073-003Lab Sample Id:WaterMatrix: 83A CanalSample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 12.18
04.11.14 05.39
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 12 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 08.42 Date Collected:482073-003Lab Sample Id:WaterMatrix: 83A CanalSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500
2.43 <1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.004.25
<5.00<1.50<2.00<1.501.05
<2.00<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01
Analysis Date
% Moisture:
Page 13 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 08.42 Date Collected:482073-003Lab Sample Id:WaterMatrix: 83A CanalSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
1.16 <2.00<5.00<5.00
<0.500<0.500
3.29 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
96104100
96
04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 14 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.04 Date Collected:482073-004Lab Sample Id:WaterMatrix: Salt CanalSample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
0.00600
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 12.25
04.11.14 05.59
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 15 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.04 Date Collected:482073-004Lab Sample Id:WaterMatrix: Salt CanalSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.002.04
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.5000.960 0.970
<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19
Analysis Date
% Moisture:
Page 16 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.04 Date Collected:482073-004Lab Sample Id:WaterMatrix: Salt CanalSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
4.32 <2.00<5.00<5.00
<0.500<0.500
7.01 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
98101
9996
04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 17 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.25 Date Collected:482073-005Lab Sample Id:WaterMatrix: RID-105Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
0.0130
0.0134
0.0120
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 12.32
04.11.14 06.05
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 18 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.25 Date Collected:482073-005Lab Sample Id:WaterMatrix: RID-105Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45
Analysis Date
% Moisture:
Page 19 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.25 Date Collected:482073-005Lab Sample Id:WaterMatrix: RID-105Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
2.39 <2.00<5.00<5.00
<0.500<0.5000.590 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
113113107100
04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 20 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.39 Date Collected:482073-006Lab Sample Id:WaterMatrix: RID-106Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
0.00700
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 12.38
04.11.14 06.12
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 21 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.39 Date Collected:482073-006Lab Sample Id:WaterMatrix: RID-106Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.001.69
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500
4.66 0.960
<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11
Analysis Date
% Moisture:
Page 22 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.39 Date Collected:482073-006Lab Sample Id:WaterMatrix: RID-106Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
21.5 <2.00<5.00<5.00
<0.500<0.500
8.06 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
96102101
94
04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 23 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.52 Date Collected:482073-007Lab Sample Id:WaterMatrix: RID-107Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
0.00600
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 12.45
04.11.14 06.18
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 24 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.52 Date Collected:482073-007Lab Sample Id:WaterMatrix: RID-107Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.001.11
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500
2.38 <0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37
Analysis Date
% Moisture:
Page 25 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 09.52 Date Collected:482073-007Lab Sample Id:WaterMatrix: RID-107Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
5.95 <2.00<5.00<5.00
<0.500<0.500
8.11 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
98102101
97
04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 26 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.00 Date Collected:482073-008Lab Sample Id:WaterMatrix: RID-96Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
0.00800
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 12.51
04.11.14 06.25
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 27 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.00 Date Collected:482073-008Lab Sample Id:WaterMatrix: RID-96Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.000.650 <5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.5000.600
<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03
Analysis Date
% Moisture:
Page 28 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.00 Date Collected:482073-008Lab Sample Id:WaterMatrix: RID-96Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
5.19 <2.00<5.00<5.00
<0.500<0.500
2.85 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
97103102
97
04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 29 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.08 Date Collected:482073-009Lab Sample Id:WaterMatrix: RID-108Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
0.00900
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 12.58
04.11.14 06.31
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 30 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.08 Date Collected:482073-009Lab Sample Id:WaterMatrix: RID-108Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.000.620 <5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29
Analysis Date
% Moisture:
Page 31 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.08 Date Collected:482073-009Lab Sample Id:WaterMatrix: RID-108Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
4.90 <2.00<5.00<5.00
<0.500<0.500
2.69 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
98104100
96
04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 32 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.21 Date Collected:482073-010Lab Sample Id:WaterMatrix: RID-109Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
0.00900
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 13.04
04.11.14 06.38
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 33 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.21 Date Collected:482073-010Lab Sample Id:WaterMatrix: RID-109Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.002.26
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500
2.60 <0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55
Analysis Date
% Moisture:
Page 34 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.21 Date Collected:482073-010Lab Sample Id:WaterMatrix: RID-109Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
10.6 <2.00<5.00<5.00
<0.500<0.500
7.15 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
97102
9995
04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 35 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.37 Date Collected:482073-011Lab Sample Id:WaterMatrix: RID-110Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 13.11
04.11.14 06.44
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 36 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.37 Date Collected:482073-011Lab Sample Id:WaterMatrix: RID-110Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.003.32
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21
Analysis Date
% Moisture:
Page 37 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.37 Date Collected:482073-011Lab Sample Id:WaterMatrix: RID-110Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
8.16 <2.00<5.00<5.00
<0.500<0.500
1.53 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
97103
9994
04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 38 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.43 Date Collected:482073-012Lab Sample Id:WaterMatrix: EQBSample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 13.17
04.11.14 06.51
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 39 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.43 Date Collected:482073-012Lab Sample Id:WaterMatrix: EQBSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47
Analysis Date
% Moisture:
Page 40 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.43 Date Collected:482073-012Lab Sample Id:WaterMatrix: EQBSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500<0.500
<2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
95104
9893
04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 41 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.35 Date Collected:482073-013Lab Sample Id:WaterMatrix: RID-111RSample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 13.37
04.11.14 06.57
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 42 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.35 Date Collected:482073-013Lab Sample Id:WaterMatrix: RID-111RSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.004.10
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13
Analysis Date
% Moisture:
Page 43 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 10.35 Date Collected:482073-013Lab Sample Id:WaterMatrix: RID-111RSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
1.53 <2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
99105100
95
04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 44 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 11.46 Date Collected:482073-014Lab Sample Id:WaterMatrix: RID-113Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 13.43
04.11.14 07.17
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 45 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 11.46 Date Collected:482073-014Lab Sample Id:WaterMatrix: RID-113Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.003.44
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.5000.520
1.14 <0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40
Analysis Date
% Moisture:
Page 46 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 11.46 Date Collected:482073-014Lab Sample Id:WaterMatrix: RID-113Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
3.03 <2.00<5.00<5.00
<0.500<0.500
8.24 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
99104
9995
04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 47 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 11.58 Date Collected:482073-015Lab Sample Id:WaterMatrix: RID-114Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 13.50
04.11.14 07.23
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 48 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 11.58 Date Collected:482073-015Lab Sample Id:WaterMatrix: RID-114Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.002.39
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.002.12
<0.5003.01 7.48
<0.500<0.500
<1.00<0.500
<1.00<1.00
937532Seq Number:
RL
04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06
Analysis Date
% Moisture:
Page 49 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 11.58 Date Collected:482073-015Lab Sample Id:WaterMatrix: RID-114Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
03.31.14 21.52 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
2.86 <2.00<5.00<5.00
<0.500<0.500
45.6 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937532Seq Number:
RL
04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
99107
9794
04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 50 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.15 Date Collected:482073-016Lab Sample Id:WaterMatrix: RID-104Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 13.56
04.11.14 07.30
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 51 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.15 Date Collected:482073-016Lab Sample Id:WaterMatrix: RID-104Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09
Analysis Date
% Moisture:
Page 52 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.15 Date Collected:482073-016Lab Sample Id:WaterMatrix: RID-104Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
3.38 <2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
95959792
04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 53 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.39 Date Collected:482073-017Lab Sample Id:WaterMatrix: RID-102Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
0.0161
0.0157
0.0130
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 14.03
04.11.14 07.36
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 54 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.39 Date Collected:482073-017Lab Sample Id:WaterMatrix: RID-102Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28
Analysis Date
% Moisture:
Page 55 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.39 Date Collected:482073-017Lab Sample Id:WaterMatrix: RID-102Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
3.86 <2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
97999992
04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 56 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.56 Date Collected:482073-018Lab Sample Id:WaterMatrix: RID-103Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.00
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938352
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 14.09
04.11.14 07.43
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 57 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.56 Date Collected:482073-018Lab Sample Id:WaterMatrix: RID-103Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54
Analysis Date
% Moisture:
Page 58 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 12.56 Date Collected:482073-018Lab Sample Id:WaterMatrix: RID-103Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500<0.500
<2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
97969893
04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 59 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.13 Date Collected:482073-019Lab Sample Id:WaterMatrix: RID-101Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938492
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 14.16
04.13.14 18.45
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 60 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.13 Date Collected:482073-019Lab Sample Id:WaterMatrix: RID-101Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500
1.14 <0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20
Analysis Date
% Moisture:
Page 61 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.13 Date Collected:482073-019Lab Sample Id:WaterMatrix: RID-101Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500<0.500
<2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
99999994
04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 62 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.32 Date Collected:482073-020Lab Sample Id:WaterMatrix: RID-100Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.03.14 10.10
04.07.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938379
938492
937261
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.11.14 14.23
04.13.14 18.52
03.28.14 07.09
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 63 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.32 Date Collected:482073-020Lab Sample Id:WaterMatrix: RID-100Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.001.45
<0.5002.51 2.29
<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46
Analysis Date
% Moisture:
Page 64 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.32 Date Collected:482073-020Lab Sample Id:WaterMatrix: RID-100Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
3.25 <2.00<5.00<5.00
<0.500<0.500
8.97 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
97969892
04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 65 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.48 Date Collected:482073-021Lab Sample Id:WaterMatrix: RID-99Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
0.0481
0.0144
0.0430
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 17.01
04.14.14 13.20
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 66 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.48 Date Collected:482073-021Lab Sample Id:WaterMatrix: RID-99Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.5000.500
<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11
Analysis Date
% Moisture:
Page 67 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.48 Date Collected:482073-021Lab Sample Id:WaterMatrix: RID-99Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
8.31 <2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
97969893
04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 68 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.56 Date Collected:482073-022Lab Sample Id:WaterMatrix: RID-97Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
0.0483
0.0125
0.0430
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 17.33
04.14.14 13.39
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 69 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.56 Date Collected:482073-022Lab Sample Id:WaterMatrix: RID-97Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.5000.600
<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37
Analysis Date
% Moisture:
Page 70 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 13.56 Date Collected:482073-022Lab Sample Id:WaterMatrix: RID-97Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
8.01 <2.00<5.00<5.00
<0.500<0.5000.630 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
9699
10093
04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 71 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.08 Date Collected:482073-023Lab Sample Id:WaterMatrix: RID-95Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
0.00600
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 17.40
04.14.14 13.46
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 72 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.08 Date Collected:482073-023Lab Sample Id:WaterMatrix: RID-95Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.003.48
<0.5006.18 7.86
<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03
Analysis Date
% Moisture:
Page 73 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.08 Date Collected:482073-023Lab Sample Id:WaterMatrix: RID-95Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
2.99 <2.00<5.00<5.00
<0.500<0.500
44.0 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
98979893
04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 74 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.00 Date Collected:482073-024Lab Sample Id:WaterMatrix: RID-94Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 17.59
04.14.14 13.52
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 75 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.00 Date Collected:482073-024Lab Sample Id:WaterMatrix: RID-94Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500
1.03 <0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29
Analysis Date
% Moisture:
Page 76 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.00 Date Collected:482073-024Lab Sample Id:WaterMatrix: RID-94Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
1.34 <2.00<5.00<5.00
<0.500<0.5000.650 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
95949693
04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 77 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.38 Date Collected:482073-025Lab Sample Id:WaterMatrix: RID-93Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 18.06
04.14.14 13.59
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 78 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.38 Date Collected:482073-025Lab Sample Id:WaterMatrix: RID-93Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55
Analysis Date
% Moisture:
Page 79 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.38 Date Collected:482073-025Lab Sample Id:WaterMatrix: RID-93Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.5000.630 <2.00<5.00<5.00
<0.500<0.500
1.05 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
98989891
04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 80 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.51 Date Collected:482073-026Lab Sample Id:WaterMatrix: RID-91Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 18.13
04.14.14 14.21
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 81 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.51 Date Collected:482073-026Lab Sample Id:WaterMatrix: RID-91Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21
Analysis Date
% Moisture:
Page 82 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 14.51 Date Collected:482073-026Lab Sample Id:WaterMatrix: RID-91Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500<0.500
<2.00<5.00<5.00
<0.500<0.500
1.11 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
96959894
04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 83 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.05 Date Collected:482073-027Lab Sample Id:WaterMatrix: RID-92Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 18.19
04.14.14 14.27
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 84 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.05 Date Collected:482073-027Lab Sample Id:WaterMatrix: RID-92Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.003.07
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.001.92
<0.5004.84 7.77
<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48
Analysis Date
% Moisture:
Page 85 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.05 Date Collected:482073-027Lab Sample Id:WaterMatrix: RID-92Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
13.5 <2.00<5.00<5.00
<0.500<0.500
76.2 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
96969992
04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 86 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.18 Date Collected:482073-028Lab Sample Id:WaterMatrix: RID-90Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 18.26
04.14.14 14.34
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 87 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.18 Date Collected:482073-028Lab Sample Id:WaterMatrix: RID-90Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14
Analysis Date
% Moisture:
Page 88 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.18 Date Collected:482073-028Lab Sample Id:WaterMatrix: RID-90Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500<0.500
<2.00<5.00<5.00
<0.500<0.5000.630 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
98959793
04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 89 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.36 Date Collected:482073-029Lab Sample Id:WaterMatrix: RID-89Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 18.32
04.14.14 14.40
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 90 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.36 Date Collected:482073-029Lab Sample Id:WaterMatrix: RID-89Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.003.53
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.001.09
<0.5002.84 3.06
<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40
Analysis Date
% Moisture:
Page 91 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.36 Date Collected:482073-029Lab Sample Id:WaterMatrix: RID-89Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
10.3 <2.00<5.00<5.00
<0.500<0.500
35.5 <2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
100989893
04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 92 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.50 Date Collected:482073-030Lab Sample Id:WaterMatrix: RID-88Sample Id:
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
MKO
MKO
TNL
Analyst:
Analyst:
Analyst:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14 11.10
04.09.14 11.10
Date Prep:
Date Prep:
MLI
MLI
RYR
Tech:
Tech:
Tech:
Chromium
Chromium
Chromium, Hexavalent
Parameter
Parameter
Parameter
Result
Result
Result
0.0100
0.0100
0.00500
Flag
Flag
Flag
mg/L
mg/L
mg/L
Units
Units
Units
1
1
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
7440-47-3
7440-47-3
18540-29-9
<0.0100
<0.0100
<0.00500
938492
938532
937325
Seq Number:
Seq Number:
Seq Number:
SUB: AZ0765
SUB: AZ0765
RL
RL
RL
04.13.14 18.39
04.14.14 14.47
03.28.14 07.48
Analysis Date
Analysis Date
Analysis Date
% Moisture:
% Moisture:
% Moisture:
Page 93 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.50 Date Collected:482073-030Lab Sample Id:WaterMatrix: RID-88Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06
Analysis Date
% Moisture:
Page 94 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 15.50 Date Collected:482073-030Lab Sample Id:WaterMatrix: RID-88Sample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500<0.500
<2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
97969792
04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 95 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 07.27 Date Collected:482073-031Lab Sample Id:WaterMatrix: Trip BlankSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene
Parameter Result
20.0 0.500
1.50 0.500 0.500
1.00 5.00 5.00 2.00 2.50 1.50 2.50
0.500 0.500 0.500
4.00 0.500
5.00 1.50 2.00 1.50
0.500 2.00
0.500 0.500
1.50 1.50 1.50 2.00
0.500 0.500 0.500 0.500 0.500 0.500
1.00 0.500
1.00 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
937846Seq Number:
RL
04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32
Analysis Date
% Moisture:
Page 96 of 112 Final 1.000
Certificate of Analytical Results 482073
Terranext, Phoenix, AZWVBA
03.27.14 16.40 Date Received:03.27.14 07.27 Date Collected:482073-031Lab Sample Id:WaterMatrix: Trip BlankSample Id:
VOCs by EPA 8260B Analytical Method:
OEMAnalyst:
SW5030CPrep Method:
04.04.14 00.34 Date Prep:
OEMTech:
trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes
Parameter Result
0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00
0.500 0.500 0.500
2.00 5.00 5.00
0.500 0.500 0.500
2.00 1.00 2.00 1.50 1.00 2.00 5.00
0.500 1.00
Flag
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
Units
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
DilCas Number
10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500<0.500
<2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500<1.00
937846Seq Number:
RL
04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32
Analysis Date
Surrogate
69-13366-13970-13070-135
%Recovery Flag
%%%%
94949791
04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32
Cas Number
1868-53-717060-07-02037-26-5460-00-4
Units Analysis Date
Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
Limits
% Moisture:
Page 97 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
653451-1-BLK
653576-1-BLK
482073-001
482073-021
653575-1-BLK
653697-1-BLK
MB Sample Id:
MB Sample Id:
Parent Sample Id:
Parent Sample Id:
MB Sample Id:
MB Sample Id:
Water
Water
Water
Water
Water
Water
Matrix:
Matrix:
Matrix:
Matrix:
Matrix:
Matrix:
Total Metals by EPA 6010B
Total Metals by EPA 6010B
Total Metals by EPA 6010B
Total Metals by EPA 6010B
Metals, Dissolved, by EPA 6010B
Metals, Dissolved, by EPA 6010B
Analytical Method:
Analytical Method:
Analytical Method:
Analytical Method:
Analytical Method:
Analytical Method:
SW3010A
SW3010A
SW3010A
SW3010A
SW3010A
SW3010A
Prep Method:
Prep Method:
Prep Method:
Prep Method:
Prep Method:
Prep Method:
04.03.14
04.07.14
04.03.14
04.07.14
04.07.14
04.09.14
Date Prep:
Date Prep:
Date Prep:
Date Prep:
Date Prep:
Date Prep:
Chromium
Chromium
Chromium
Chromium
Chromium
Chromium
Parameter
Parameter
Parameter
Parameter
Parameter
Parameter
%RPD
%RPD
%RPD
%RPD
%RPD
%RPD
Flag
Flag
Flag
Flag
Flag
Flag
20
20
20
20
20
20
RPDLimit
RPDLimit
RPDLimit
RPDLimit
RPDLimit
RPDLimit
1
4
1
2
1
2
938379
938492
938379
938492
938352
938532
Seq Number:
Seq Number:
Seq Number:
Seq Number:
Seq Number:
Seq Number:
04.11.14 11:13
04.13.14 16:48
04.11.14 11:33
04.13.14 17:08
04.11.14 04:44
04.14.14 13:07
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Limits
Limits
Limits
Limits
Limits
Limits
80-120
80-120
75-125
75-125
80-120
80-120
LCSD %Rec
LCSD %Rec
MSD %Rec
MSD %Rec
LCSD %Rec
LCSD %Rec
108
106
108
107
106
104
LCSD Result
LCSD Result
MSD Result
MSD Result
LCSD Result
LCSD Result
1.08
1.06
1.08
1.12
1.06
1.04
LCS %Rec
LCS %Rec
MS %Rec
MS %Rec
LCS %Rec
LCS %Rec
109
110
107
105
107
102
1.09
1.10
1.07
1.10
1.07
1.02
Spike Amount
Spike Amount
Spike Amount
Spike Amount
Spike Amount
Spike Amount
1.00
1.00
1.00
1.00
1.00
1.00
MB Result
MB Result
Parent Result
Parent Result
MB Result
MB Result
<0.0100
<0.0100
<0.0100
0.0481
<0.0100
<0.0100
653451-1-BKS
653576-1-BKS
482073-001 S
482073-021 S
653575-1-BKS
653697-1-BKS
LCS Sample Id:
LCS Sample Id:
MS Sample Id:
MS Sample Id:
LCS Sample Id:
LCS Sample Id:
653451-1-BSD
653576-1-BSD
482073-001 SD
482073-021 SD
653575-1-BSD
653697-1-BSD
LCSD Sample Id:
LCSD Sample Id:
MSD Sample Id:
MSD Sample Id:
LCSD Sample Id:
LCSD Sample Id:
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
Units
Units
Units
Units
LCS Result
LCS Result
MS Result
MS Result
LCS Result
LCS Result
Page 98 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
482073-001
482073-021
937261-1-BLK
937325-1-BLK
482073-001
482073-020
Parent Sample Id:
Parent Sample Id:
MB Sample Id:
MB Sample Id:
Parent Sample Id:
Parent Sample Id:
Water
Water
Water
Water
Water
Water
Matrix:
Matrix:
Matrix:
Matrix:
Matrix:
Matrix:
Metals, Dissolved, by EPA 6010B
Metals, Dissolved, by EPA 6010B
Chromium Hexavalent by SM 3500 Cr-D
Chromium Hexavalent by SM 3500 Cr-D
Chromium Hexavalent by SM 3500 Cr-D
Chromium Hexavalent by SM 3500 Cr-D
Analytical Method:
Analytical Method:
Analytical Method:
Analytical Method:
Analytical Method:
Analytical Method:
SW3010A
SW3010A
Prep Method:
Prep Method:
04.07.14
04.09.14
Date Prep:
Date Prep:
Chromium
Chromium
Chromium, Hexavalent
Chromium, Hexavalent
Chromium, Hexavalent
Chromium, Hexavalent
Parameter
Parameter
Parameter
Parameter
Parameter
Parameter
%RPD
%RPD
%RPD
%RPD
%RPD
%RPD
Flag
Flag
Flag
Flag
Flag
Flag
20
20
20
20
20
20
RPDLimit
RPDLimit
RPDLimit
RPDLimit
RPDLimit
RPDLimit
0
3
1
2
0
0
938352
938532
937261
937325
937261
937261
Seq Number:
Seq Number:
Seq Number:
Seq Number:
Seq Number:
Seq Number:
04.11.14 05:07
04.14.14 13:27
03.28.14 07:09
03.28.14 07:48
03.28.14 07:09
03.28.14 07:09
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Analysis Date
Limits
Limits
Limits
Limits
Limits
Limits
75-125
75-125
81-119
81-119
36-153
36-153
MSD %Rec
MSD %Rec
LCSD %Rec
LCSD %Rec
MSD %Rec
MSD %Rec
106
107
99
98
97
96
MSD Result
MSD Result
LCSD Result
LCSD Result
MSD Result
MSD Result
1.06
1.08
0.0990
0.0980
0.102
0.0960
MS %Rec
MS %Rec
LCS %Rec
LCS %Rec
MS %Rec
MS %Rec
106
104
100
96
97
96
1.06
1.05
0.100
0.0960
0.102
0.0960
Spike Amount
Spike Amount
Spike Amount
Spike Amount
Spike Amount
Spike Amount
1.00
1.00
0.100
0.100
0.100
0.100
Parent Result
Parent Result
MB Result
MB Result
Parent Result
Parent Result
<0.0100
0.0144
<0.00500
<0.00500
0.00500
<0.00500
482073-001 S
482073-021 S
937261-1-BKS
937325-1-BKS
482073-001 S
482073-020 S
MS Sample Id:
MS Sample Id:
LCS Sample Id:
LCS Sample Id:
MS Sample Id:
MS Sample Id:
482073-001 SD
482073-021 SD
937261-1-BSD
937325-1-BSD
482073-001 SD
482073-020 SD
MSD Sample Id:
MSD Sample Id:
LCSD Sample Id:
LCSD Sample Id:
MSD Sample Id:
MSD Sample Id:
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
Units
Units
Units
Units
MS Result
MS Result
LCS Result
LCS Result
MS Result
MS Result
Page 99 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
482073-022Parent Sample Id:WaterMatrix:
Chromium Hexavalent by SM 3500 Cr-DAnalytical Method:
Chromium, Hexavalent
Parameter %RPD Flag
20
RPDLimit
1
937325Seq Number:
03.28.14 07:48
Analysis Date
Limits
36-153
MSD %Rec
98
MSD Result
0.141
MS %Rec
990.142
Spike Amount
0.100
Parent Result
0.0430
482073-022 SMS Sample Id: 482073-022 SDMSD Sample Id:
mg/L
UnitsMS Result
Page 100 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
653270-1-BLKMB Sample Id:WaterMatrix:
VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 03.31.14Date Prep:
AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethane2-ButanoneMTBEn-ButylbenzeneSec-Butylbenzenetert-ButylbenzeneCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformChloromethane2-Chlorotoluene4-Chlorotoluenep-Cymene (p-Isopropyltoluene)Dibromochloromethane1,2-Dibromo-3-Chloropropane1,2-DibromoethaneDibromomethane1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-dichloroethene1,2-Dichloropropane1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenecis-1,3-Dichloropropenetrans-1,3-dichloropropeneEthylbenzeneHexachlorobutadiene2-HexanoneisopropylbenzeneMethylene ChlorideIodomethane (Methyl Iodide)4-Methyl-2-PentanoneNaphthalenen-PropylbenzeneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachloroethane
Parameter %RPD Flag
28202024202025272120202022212024242620282020212023202020272020212421202024202020202220202022212720202020
RPDLimit
8020102173210121141303101001035103051380231106020562012
937532Seq Number:
03.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
Analysis Date
Limits
55-16570-13070-13067-12570-13069-13058-13858-14670-13058-12861-13365-12859-13857-14070-13060-14666-12847-14470-13070-13067-13570-13060-12870-13070-13070-13070-13070-1309-13466-13270-13058-14467-12963-13770-13070-13060-14164-13570-13070-13070-13054-14565-12970-13061-12768-12867-13164-13365-12870-13070-13070-130
LCSD %Rec
123108
99106109104
91118115105101
98108106102
99108
98102101101105109107107105102107106107108110109109107100105110107105109
99116106105104119112104105100116
LCSD Result
49.121.519.721.121.820.718.247.222.920.920.219.621.621.120.319.721.519.520.320.220.221.021.821.321.420.920.321.321.121.321.621.921.821.821.419.920.922.021.421.021.719.746.521.121.020.847.522.420.720.920.023.1
LCS %Rec
11310897
10511110411311011110310098
11010810011310910010198
10010699
10710910510510210710711111010411011110810511211110710899
110105103104113106102105102114
45.121.619.421.022.120.722.543.922.220.519.919.621.921.520.022.621.820.020.219.619.921.119.821.321.721.021.020.321.321.322.221.920.722.022.121.520.922.422.121.321.519.743.921.020.520.745.021.120.321.020.322.7
Spike Amount
40.020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.040.020.020.020.040.020.020.020.020.020.0
MB Result
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
653270-1-BKSLCS Sample Id: 653270-1-BSDLCSD Sample Id:
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
UnitsLCS Result
Page 101 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
653270-1-BLKMB Sample Id:WaterMatrix:
VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 03.31.14Date Prep:
TetrachloroethyleneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-Trichloropropane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzeneo-Xylenem,p-XylenesVinyl AcetateVinyl Chloride
Parameter %RPD Flag
202027202020202220202020202225
RPDLimit
509500196130037
937532Seq Number:
03.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
Analysis Date
Limits
63-12770-13066-13169-12762-13370-13070-13045-15170-13070-13070-13070-13070-13052-14243-120
LCSD %Rec
110105100102107105105106108100102105105120
94
LCSD Result
21.920.920.020.421.421.020.921.221.620.020.420.941.823.918.7
LCS %Rec
1051049197
10710510397
1029999
105104116101
20.920.818.219.421.421.020.619.420.419.819.721.041.723.220.1
Spike Amount
20.020.020.020.020.020.020.020.020.020.020.020.040.020.020.0
MB Result
<0.500<2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500
653270-1-BKSLCS Sample Id: 653270-1-BSDLCSD Sample Id:
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
UnitsLCS Result
Dibromofluoromethane1,2-Dichloroethane-D4Toluene-D84-Bromofluorobenzene
Surrogate LCSD Flag
03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09
Analysis Date
Limits
69-13366-13970-13070-135
LCSD %Rec
9810199103
LCS %Rec
100105101103
MB %Rec
9810310397
%%%%
UnitsLCSFlag
MBFlag
Page 102 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
653524-1-BLKMB Sample Id:WaterMatrix:
VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 04.04.14Date Prep:
AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethane2-ButanoneMTBEn-ButylbenzeneSec-Butylbenzenetert-ButylbenzeneCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformChloromethane2-Chlorotoluene4-Chlorotoluenep-Cymene (p-Isopropyltoluene)Dibromochloromethane1,2-Dibromo-3-Chloropropane1,2-DibromoethaneDibromomethane1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-dichloroethene1,2-Dichloropropane1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenecis-1,3-Dichloropropenetrans-1,3-dichloropropeneEthylbenzeneHexachlorobutadiene2-HexanoneisopropylbenzeneMethylene ChlorideIodomethane (Methyl Iodide)4-Methyl-2-PentanoneNaphthalenen-PropylbenzeneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachloroethane
Parameter %RPD Flag
28202024202025272120202022212024242620282020212023202020272020212421202024202020202220202022212720202020
RPDLimit
15022148211212012182312530112111212141133211131492227
937846Seq Number:
04.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
Analysis Date
Limits
55-16570-13070-13067-12570-13069-13058-13858-14670-13058-12861-13365-12859-13857-14070-13060-14666-12847-14470-13070-13067-13570-13060-12870-13070-13070-13070-13070-1309-13466-13270-13058-14467-12963-13770-13070-13060-14164-13570-13070-13070-13054-14565-12970-13061-12768-12867-13164-13365-12870-13070-13070-130
LCSD %Rec
1019498969797
1089995
10096
10195
1029595
100969895
1009694949499
101101
9495969599979696989796
100989897
101999299
10196
104103102
LCSD Result
40.218.819.619.219.319.421.539.618.919.919.220.119.020.319.018.919.919.219.519.020.019.218.718.818.819.820.220.218.818.919.119.019.819.419.119.219.519.419.120.019.619.538.620.219.818.339.420.119.120.820.620.3
LCS %Rec
8794
100989693
10097949998
10294
1029496
100899698
10295899294
1001009995959597
10096979299979398979996
1009791949297
10210195
34.718.820.019.519.218.619.938.818.719.819.520.318.720.418.819.220.017.819.219.520.318.917.818.318.819.919.919.819.019.019.019.319.919.119.318.419.719.318.619.519.319.738.320.019.318.137.718.419.420.420.218.9
Spike Amount
40.020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.040.020.020.020.040.020.020.020.020.020.0
MB Result
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
653524-1-BKSLCS Sample Id: 653524-1-BSDLCSD Sample Id:
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
UnitsLCS Result
Page 103 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
653524-1-BLKMB Sample Id:WaterMatrix:
VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 04.04.14Date Prep:
TetrachloroethyleneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-Trichloropropane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzeneo-Xylenem,p-XylenesVinyl AcetateVinyl Chloride
Parameter %RPD Flag
202027202020202220202020202225
RPDLimit
416323204113311
937846Seq Number:
04.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
Analysis Date
Limits
63-12770-13066-13169-12762-13370-13070-13045-15170-13070-13070-13070-13070-13052-14243-120
LCSD %Rec
9598
101100
95101
97101
97100100105105
9591
LCSD Result
19.019.520.220.018.920.119.420.219.420.019.920.942.119.018.2
LCS %Rec
92979697939899
10294
1011011011029491
18.319.419.119.418.619.519.820.318.720.220.120.240.718.818.1
Spike Amount
20.020.020.020.020.020.020.020.020.020.020.020.040.020.020.0
MB Result
<0.500<2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500
653524-1-BKSLCS Sample Id: 653524-1-BSDLCSD Sample Id:
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
UnitsLCS Result
Dibromofluoromethane1,2-Dichloroethane-D4Toluene-D84-Bromofluorobenzene
Surrogate LCSD Flag
04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52
Analysis Date
Limits
69-13366-13970-13070-135
LCSD %Rec
979897100
LCS %Rec
96999998
MB %Rec
97979892
%%%%
UnitsLCSFlag
MBFlag
Page 104 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
482071-008Parent Sample Id:WaterMatrix:
VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 03.31.14Date Prep:
AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethane2-ButanoneMTBEn-ButylbenzeneSec-Butylbenzenetert-ButylbenzeneCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformChloromethane2-Chlorotoluene4-Chlorotoluenep-Cymene (p-Isopropyltoluene)Dibromochloromethane1,2-Dibromo-3-Chloropropane1,2-DibromoethaneDibromomethane1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-dichloroethene1,2-Dichloropropane1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenecis-1,3-Dichloropropenetrans-1,3-dichloropropeneEthylbenzeneHexachlorobutadiene2-HexanoneisopropylbenzeneMethylene ChlorideIodomethane (Methyl Iodide)4-Methyl-2-PentanoneNaphthalenen-PropylbenzeneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachloroethane
Parameter %RPD Flag
20202022202022222020202028202020222220202020222020202020332020202020202020202020202033202020202620372020
RPDLimit
33200042131203032621011111420100211112011120101071102
937532Seq Number:
04.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
Analysis Date
Limits
35-16069-13070-13063-11970-13057-12153-14146-13665-12765-12770-13070-13058-14560-15270-13059-15365-12347-14870-13070-13070-13070-13050-11767-11766-11570-13070-13070-13016-15166-12964-12665-15266-12666-13570-13067-11562-14572-14067-12270-13070-13068-14352-12270-13059-12166-12753-12554-12969-12649-14270-13064-122
MSD %Rec
116110100107113106104115114106102100108111102105108
98105102101108109107111107106105112105110110109110108108106113110107109
97116106103108118108106
98103118
MSD Result
46.221.920.021.322.621.120.746.022.821.120.320.021.522.120.421.022.619.521.020.420.121.521.821.422.121.421.220.922.421.822.023.024.521.921.621.621.122.522.021.421.819.446.521.120.621.547.021.521.119.520.523.6
MS %Rec
11910799
10711410510011711310310199
10710710310811010410310110110710810811010610210711210711110910710811011010511011110911110911610710310711811610597
103116
47.721.319.721.422.721.019.946.722.620.520.119.721.421.420.521.623.120.720.520.220.121.321.521.621.921.220.321.322.422.122.122.924.121.621.921.920.922.022.121.722.121.846.421.320.521.347.223.120.919.320.623.1
Spike Amount
40.020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.040.020.020.020.040.020.020.020.020.020.0
Parent Result
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.001.04
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.000.730
<0.5001.072.66
<0.500<0.500
<1.00<0.500
<1.00<1.00
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
482071-008 SMS Sample Id: 482071-008 SDMSD Sample Id:
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
UnitsMS Result
Page 105 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
482071-008Parent Sample Id:WaterMatrix:
VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 03.31.14Date Prep:
TetrachloroethyleneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-Trichloropropane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzeneo-Xylenem,p-XylenesVinyl AcetateVinyl Chloride
Parameter %RPD Flag
202024202020202020222020202321
RPDLimit
1062002114202137
937532Seq Number:
04.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
Analysis Date
Limits
69-13070-13061-12664-12368-13665-11270-13053-17158-11667-12870-13070-13070-13043-13346-132
MSD %Rec
105106
95102109105109107110102103107106101
97
MSD Result
27.221.218.920.421.821.027.721.322.020.320.521.442.220.219.3
MS %Rec
10610610110510910610696
10699
103105104104104
27.421.220.120.921.821.127.119.121.219.820.521.041.720.820.8
Spike Amount
20.020.020.020.020.020.020.020.020.020.020.020.040.020.020.0
Parent Result
6.26<2.00<5.00<5.00
<0.500<0.500
5.99<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500
482071-008 SMS Sample Id: 482071-008 SDMSD Sample Id:
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
UnitsMS Result
Dibromofluoromethane1,2-Dichloroethane-D4Toluene-D84-Bromofluorobenzene
Surrogate MSD Flag
04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27
Analysis Date
Limits
69-13366-13970-13070-135
MSD %Rec
98103100102
MS %Rec
98103101100
%%%%
UnitsMSFlag
Page 106 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
482073-016Parent Sample Id:WaterMatrix:
VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 04.04.14Date Prep:
AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethane2-ButanoneMTBEn-ButylbenzeneSec-Butylbenzenetert-ButylbenzeneCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformChloromethane2-Chlorotoluene4-Chlorotoluenep-Cymene (p-Isopropyltoluene)Dibromochloromethane1,2-Dibromo-3-Chloropropane1,2-DibromoethaneDibromomethane1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-dichloroethene1,2-Dichloropropane1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenecis-1,3-Dichloropropenetrans-1,3-dichloropropeneEthylbenzeneHexachlorobutadiene2-HexanoneisopropylbenzeneMethylene ChlorideIodomethane (Methyl Iodide)4-Methyl-2-PentanoneNaphthalenen-PropylbenzeneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachloroethane
Parameter %RPD
R5
Flag
20202022202022222020202028202020222220202020222020202020332020202020202020202020202033202020202620372020
RPDLimit
33215241110521120252512225310151313213321141814043781003
937846Seq Number:
04.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
Analysis Date
Limits
35-16069-13070-13063-11970-13057-12153-14146-13665-12765-12770-13070-13058-14560-15270-13059-15365-12347-14870-13070-13070-13070-13050-11767-11766-11570-13070-13070-13016-15166-12964-12665-15266-12666-13570-13067-11562-14572-14067-12270-13070-13068-14352-12270-13059-12166-12753-12554-12969-12649-14270-13064-122
MSD %Rec
11594
100101
9496
103107
989995
10094
1019796
1059898959897989795
101100104
96979697
102979597969594
1009995
103101101
93101107
9798
104103
MSD Result
45.918.819.920.218.719.220.642.619.519.819.019.918.820.219.319.221.019.519.518.919.619.419.519.318.920.220.020.819.219.419.119.420.419.319.019.319.218.918.720.019.718.941.320.220.118.640.321.319.319.520.720.6
MS %Rec
8396
101969592
1159693
10196
10092
1019591
1031039797
10095939496
1011029996949594
1009698949496959798
10390
101979194999898
103100
33.019.120.219.219.018.422.938.518.620.119.220.018.420.118.918.220.620.619.419.320.019.018.518.719.120.220.319.819.118.819.018.820.019.219.518.718.819.118.919.319.620.536.020.219.318.137.619.719.519.520.619.9
Spike Amount
40.020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.040.020.020.020.040.020.020.020.020.020.0
Parent Result
<20.0<0.500
<1.50<0.500<0.500
<1.00<5.00<5.00<2.00<2.50<1.50<2.50
<0.500<0.500<0.500
<4.00<0.500
<5.00<1.50<2.00<1.50
<0.500<2.00
<0.500<0.500
<1.50<1.50<1.50<2.00
<0.500<0.500<0.500<0.500<0.500<0.500
<1.00<0.500
<1.00<1.00
<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00
<0.500<0.500
482073-016 SMS Sample Id: 482073-016 SDMSD Sample Id:
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
UnitsMS Result
Page 107 of 112 Final 1.000
QC Summary 482073
TerranextWVBA
482073-016Parent Sample Id:WaterMatrix:
VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 04.04.14Date Prep:
TetrachloroethyleneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-Trichloropropane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzeneo-Xylenem,p-XylenesVinyl AcetateVinyl Chloride
Parameter %RPD
R5
Flag
202024202020202020222020202321
RPDLimit
13302302810011151
937846Seq Number:
04.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
Analysis Date
Limits
69-13070-13061-12664-12368-13665-11270-13053-17158-11667-12870-13070-13070-13043-13346-132
MSD %Rec
94100104100
94103
9798
104101
99104104
8796
MSD Result
22.219.920.720.018.820.619.419.620.720.119.820.841.517.419.2
MS %Rec
9397
10110093
100977494
1011001031038397
22.019.420.120.018.519.919.414.818.820.119.920.641.016.619.3
Spike Amount
20.020.020.020.020.020.020.020.020.020.020.020.040.020.020.0
Parent Result
3.38<2.00<5.00<5.00
<0.500<0.500<0.500
<2.00<1.00<2.00<1.50<1.00<2.00<5.00
<0.500
482073-016 SMS Sample Id: 482073-016 SDMSD Sample Id:
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
UnitsMS Result
Dibromofluoromethane1,2-Dichloroethane-D4Toluene-D84-Bromofluorobenzene
Surrogate MSD Flag
04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35
Analysis Date
Limits
69-13366-13970-13070-135
MSD %Rec
98989899
MS %Rec
97979698
%%%%
UnitsMSFlag
Page 108 of 112 Final 1.000