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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica St. Louis13715 Rider Trail NorthEarth City, MO 63045Tel: (314)298-8566
TestAmerica Job ID: 160-15789-1Client Project/Site: HDP
For:Perma-Fix Environmental Services Inc.2800 Solway RoadKnoxville, Tennessee 37931
Attn: Brian Miller
Authorized for release by:1/29/2016 2:39:03 PMRhonda Ridenhower, Manager of Project [email protected] forIvan Vania, Project Manager II(314)[email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of ContentsClient: Perma-Fix Environmental Services Inc.Project/Site: HDP
TestAmerica Job ID: 160-15789-1
Page 2 of 46TestAmerica St. Louis
1/29/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
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Case NarrativeClient: Perma-Fix Environmental Services Inc. TestAmerica Job ID: 160-15789-1Project/Site: HDP
Job ID: 160-15789-1
Laboratory: TestAmerica St. Louis
Narrative
CASE NARRATIVE
Client: Perma-Fix Environmental Services Inc.
Project: HDP
Report Number: 160-15789-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data
have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the
client.”
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT
The samples were received on 01/20/2016; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 18.9º C, 18.9º C, 18.9º C and 18.9º C.
TECHNETIUM-99 (ICPMS)Samples B02-01-01-P-S-S-00 (160-15789-1), B02-01-02-P-R-S-00 (160-15789-2), B02-01-03-P-E-S-00 (160-15789-3),
B02-01-04-P-S-S-00 (160-15789-4), B02-01-05-P-R-S-00 (160-15789-5), B02-01-06-P-E-S-00 (160-15789-6), B02-01-07-P-S-S-00 (160-15789-7), B02-01-08-P-R-S-00 (160-15789-8), B02-01-09-P-E-S-00 (160-15789-9), B02-01-10-P-S-S-00 (160-15789-10),
B02-01-11-P-R-S-00 (160-15789-11), B02-01-12-P-E-S-00 (160-15789-12), B02-01-13-P-S-S-00 (160-15789-13), B02-01-14-P-R-S-00
(160-15789-14), B02-01-15-P-E-S-00 (160-15789-15), B02-01-16-P-S-S-00 (160-15789-16), B02-01-17-P-R-S-00 (160-15789-17), B02-01-18-P-E-S-00 (160-15789-18), B02-01-19-P-S-S-00 (160-15789-19), B02-01-20-P-R-S-00 (160-15789-20), B02-01-21-P-E-S-00
(160-15789-21), B02-01-22-P-S-S-00 (160-15789-22), B02-01-23-P-R-S-00 (160-15789-23), B02-01-24-P-E-S-00 (160-15789-24), B02-01-02-P-R-Q-00 (160-15789-25) and B02-01-10-P-S-Q-00 (160-15789-26) were analyzed for Technetium-99 (ICPMS) in accordance
with EPA SW-846 Method 6020A. The samples were prepared on 01/20/2016 and analyzed on 01/28/2016.
TestAmerica St. LouisPage 3 of 46 1/29/2016
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Case NarrativeClient: Perma-Fix Environmental Services Inc. TestAmerica Job ID: 160-15789-1Project/Site: HDP
Job ID: 160-15789-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDSSamples B02-01-01-P-S-S-00 (160-15789-1), B02-01-02-P-R-S-00 (160-15789-2), B02-01-03-P-E-S-00 (160-15789-3),
B02-01-04-P-S-S-00 (160-15789-4), B02-01-05-P-R-S-00 (160-15789-5), B02-01-06-P-E-S-00 (160-15789-6), B02-01-07-P-S-S-00 (160-15789-7), B02-01-08-P-R-S-00 (160-15789-8), B02-01-09-P-E-S-00 (160-15789-9), B02-01-10-P-S-S-00 (160-15789-10),
B02-01-11-P-R-S-00 (160-15789-11), B02-01-12-P-E-S-00 (160-15789-12), B02-01-13-P-S-S-00 (160-15789-13), B02-01-14-P-R-S-00
(160-15789-14), B02-01-15-P-E-S-00 (160-15789-15), B02-01-16-P-S-S-00 (160-15789-16), B02-01-17-P-R-S-00 (160-15789-17), B02-01-18-P-E-S-00 (160-15789-18), B02-01-19-P-S-S-00 (160-15789-19), B02-01-20-P-R-S-00 (160-15789-20), B02-01-21-P-E-S-00
(160-15789-21), B02-01-22-P-S-S-00 (160-15789-22), B02-01-23-P-R-S-00 (160-15789-23), B02-01-24-P-E-S-00 (160-15789-24), B02-01-02-P-R-Q-00 (160-15789-25) and B02-01-10-P-S-Q-00 (160-15789-26) were analyzed for percent solids in accordance with EPA
Method 160.3 MOD. The samples were analyzed on 01/20/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)Samples B02-01-01-P-S-S-00 (160-15789-1), B02-01-02-P-R-S-00 (160-15789-2), B02-01-03-P-E-S-00 (160-15789-3), B02-01-04-P-S-S-00 (160-15789-4), B02-01-05-P-R-S-00 (160-15789-5), B02-01-06-P-E-S-00 (160-15789-6), B02-01-07-P-S-S-00 (160-15789-7), B02-01-08-P-R-S-00 (160-15789-8), B02-01-09-P-E-S-00 (160-15789-9), B02-01-10-P-S-S-00 (160-15789-10),
B02-01-11-P-R-S-00 (160-15789-11), B02-01-12-P-E-S-00 (160-15789-12), B02-01-13-P-S-S-00 (160-15789-13), B02-01-14-P-R-S-00 (160-15789-14), B02-01-15-P-E-S-00 (160-15789-15), B02-01-16-P-S-S-00 (160-15789-16), B02-01-17-P-R-S-00 (160-15789-17), B02-01-18-P-E-S-00 (160-15789-18), B02-01-19-P-S-S-00 (160-15789-19), B02-01-20-P-R-S-00 (160-15789-20), B02-01-21-P-E-S-00 (160-15789-21), B02-01-22-P-S-S-00 (160-15789-22), B02-01-23-P-R-S-00 (160-15789-23), B02-01-24-P-E-S-00 (160-15789-24), B02-01-02-P-R-Q-00 (160-15789-25) and B02-01-10-P-S-Q-00 (160-15789-26) were analyzed for Cesium-137 & Other Gamma Emitters
(GS) in accordance with DOE GA-01-R. The samples were dried on 01/20/2016, prepared on 01/22/2016 and analyzed on 01/24/2016.
Prep Batch 233605Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of bismuth-214. Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This
bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. B02-01-21-P-E-S-00 (160-15789-21), B02-01-22-P-S-S-00 (160-15789-22), B02-01-23-P-R-S-00 (160-15789-23), B02-01-24-P-E-S-00 (160-15789-24), B02-01-02-P-R-Q-00 (160-15789-25), B02-01-10-P-S-Q-00 (160-15789-26), (LCS 160-233605/2-A), (MB 160-233605/1-A) and (160-15789-A-21-D DU)
Prep Batch 233602Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of bismuth-214. Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This
bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. B02-01-01-P-S-S-00 (160-15789-1), B02-01-02-P-R-S-00 (160-15789-2),
B02-01-03-P-E-S-00 (160-15789-3), B02-01-04-P-S-S-00 (160-15789-4), B02-01-05-P-R-S-00 (160-15789-5), B02-01-06-P-E-S-00
(160-15789-6), B02-01-07-P-S-S-00 (160-15789-7), B02-01-08-P-R-S-00 (160-15789-8), B02-01-09-P-E-S-00 (160-15789-9), B02-01-10-P-S-S-00 (160-15789-10), B02-01-11-P-R-S-00 (160-15789-11), B02-01-12-P-E-S-00 (160-15789-12), B02-01-13-P-S-S-00
(160-15789-13), B02-01-14-P-R-S-00 (160-15789-14), B02-01-15-P-E-S-00 (160-15789-15), B02-01-16-P-S-S-00 (160-15789-16), B02-01-17-P-R-S-00 (160-15789-17), B02-01-18-P-E-S-00 (160-15789-18), B02-01-19-P-S-S-00 (160-15789-19), B02-01-20-P-R-S-00
(160-15789-20), (LCS 160-233602/2-A), (MB 160-233602/1-A) and (160-15789-A-1-F DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica St. LouisPage 4 of 46 1/29/2016
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TestAmerica St. Louis 13715 Rider Trail North
Earth City, MO 630l!5 phone 314.298.8566 fax
Clie'nt Contact Perrna-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Na1ne: Hematite Decommissioning Project Site: Westinghouse Hematite, MO p 0#832953
Sample Identification
B02-01-01-P-S-S-OO
802-01-02-P-R-S-DO
802-01-03.-P-E·S-OO
802-01-04-P-s-S-Oo
Chain of Custody Record
Regulatory· Program: Dow ONPDES
Projecti Manager: Brian Miller Tel/Fax: (314) srn-3333
Analysis Turnaround Time 0 CA!!ENDAR DAYS 0 WORKING DAYS
TAT if different from Below
0 2weeks
0 1 week
0 2 days
0 1 day -MU•f'•-
Tiype Sample I Sample I (<>Comp, #of
Date ' Tirrie G=GrabJ Matrix cont.
12131/15 1150 c Soil 1
1/4/16 0925 c Soil 1
1/4/16 0935 c Soil 1
12129/15 0925 c Soil 1
0RCRA 0 Other:
Site Contact: Ellen Jakub Lab Contact: Ivan Vania
~1 ...... ~ z ~ I -- .l!l e z > :;:: - ...... .. Cl
>- c E .5
"' ~ -0 ::c ,gi ~ "' Ci)
,, Q. .... <> ., . .,.. ~"' "':::i () ~ tt ... 0 "'::: VI ..c "' Q. 'O E .. Cl "' fl) Ii "' .. s .5 ..
~ ~· ~ s ti ..c ="' . ~ ;t ... 11. 11. < Q
N x x x N x x x N x x x N x x x
Date: 1/1912016 Carrier: Courier
I I
CJ)
~ U1 -..i 00 co 0 ::r Ill s· ~
Test America THE LEADER IN ENVIRON MENT AL TE:.STlNG
TestAmerica Laboratories, Inc. COC No: 011916-FSS1 __ 1_._ of_3_ COCs
Sampler: For Lab Use Onfy:
Walk-in Client I I Lab Sampling:
Job I SDG No.:
Sample $pecific Notes:
Mark Shaffer
Marl< Shaffer
Mark Shaffer
Mark Shatti:f
802-01-05-P-R-S-OO 12/29/15 1030 c Soil 1 N x x x .------ ··. - -~,: ."f. Mark sn'affer
802-01-06-P-E·S-OO 12/29/15 1035 c Soil 1 N x x x Jahmai Williamis
802-01-07 -P-8·S-OO 12/29/15 1100 c Soil 1 N x x x Jahmai WiUiam5
802-01-08-P-R-S-OO 12/29/15 1130 c Soil 1 N x x x Jahmai Williams
802-01-09-P-E-S-OO 12129/15 1135 c Soil 1 N x x x Jahmal Williams
802-01-10cP-S-8-00 12131/15 1045 c Soil 1 N x x x Brian Miller
802-01-11-P-R-S-OO 12/31/15 1115 c Soil 1 N x x x Chris Chandler
802-01-12-P-E-S-OO 12/31/15 1125 C Soil 1
'~~Ii:<f~~\~~lfgg¥'.~l~i:i;':W,g~~~q~j\;i~~,g~~~ii~qij~%i:>Ji't<%}fi;\t}#?W~~;.11~mlii-'. Possible Hazard Identification: Sample Disposal (A fee may be assessed if samples are retained longer thim 1 month) Are any samples frdm a listed EPA Hazardous' Waste? Please List any EPA Waste Codes for the sample in the Comments• Section if the lab is to dispose of the sample.
0 Non-Hazard O Flammable 0 Skin InitBnt 0 Poison B 0 Unknown 0 Return to Oient 0 Disposal by Lab 0 ArthiVe fa- Months
Special Instructions/QC Requirements & Comments: Potential for Radiologil::al Contamination
Custody Seals Intact: 0 Yes ....-.0 No
Re~~~~~(7,~M3 ~~ l~y:<-/
~ Cvrai~
Custody Seal No. :
c~_ pany: ~/I/&> f~q-i·r Company:
Uro-~::S Company:
(\ !Cooler Temp. (0 C): Obs'd:
D~~ITi!¥: t-;'>;;fReqe1Vj:ld·by: {) • /f20J/(tp l~~Ji r~
Corr'd: Thenn ID Nb.:
Company: Grc.~5 '1'6-6.6'.;7
DatelTime: f-2CJ-/(,p 8' :55
Company:
114- OlL-Cornpany:
Date/Time:
1-020. /b -efiY /~0 Date/Time: <p h;ZIJ·t~
[ Hematite !Jecommioomg Project I Pem1afix (mr W-estinghouse) f'.fon-Propne!:af\~ CJa$S 3 I Procedtlf'e:HDP-PR-OA-000, Chait< of Custody r R.e\llsioo: ~ I '""' I I II : '. 1--. __
Page 6 of 46
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TestAmerica St. Louis 13715 Rider Trail North
Earth City, MO 63045 phone 314.298.8566 fax
Client Contact Penna-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P0#832953
Sample Identification
802-01-13-P-S-S-OO
802-01-14-P-R-S-OO
802-01-15-P-E-S-OO
802-01-16-P-S-S-OO
802-01-17-P-R-S-OO
802-01-18-P-E-S-OO
802-01-19-P-S-S-OO
802-01-20-P-R-S-OO
802-01-21-P-E-S-OO
802-01-22"P-S-S-OO
802-01-23-P-R-S-OO
802-01-24-P-E-S-00
Possible Hazard Identification:
·-----_.
Chain of Custody Record Test America THE LEADER IN ENVIRONMENTAL TESTING
Regulatory Program: 0 DW 0 NPDES 0 RCRA 0 other: -- - - - TestAmerica Laboratories, Inc.
Project Manager: Brian Miller Site Contact:. Ellen Jakub Date: 1/19/2016 COC No: 011916-FSS1 Tel/Fax: (314) 810-3333 Lab Contact: Ivan Vania Carrier: Courier 2 of 3 CO Cs
Analysis Turnaround Time i::' Sampler:
0 CALENDAR DAYS 0 WORKINGDAYS e For Lab Use Only: - "" :;: I TAT if different from Below z ~ l Walk-in Client:
0 - .s e Lab Sampling; I 2Weeks z > "" .. "" 0 l week >- ~ .5 c » 0 2days .!!! (/) ::c .. Job/SDG No.: ::
"~ ! ... Cl. ...... D 1 day E (/) .. "' " ~ill "' :: c. 0 "' __ ,,,,..._ rn rn .c c.
Type "' e "' g> II> II> Ii Sample Sample !!! .g E ·- .. ~ (C=Comp, #of l! eij .c
Date Time G=Grab) Matrix Cont. :. (; 3: c.
Li: :;;: 0 Sample Specific Notes:
1/18/16 1005 c Soil 1 N x x x Mark Shaffer
1/18/16 1045 c Soil 1 N x x x Chris Chandler
1118116 1050 c Soil 1 N x x x Mark Shaffer
12129/16 1520 c Soil 1 N x x x Mark Shaffer
12131/15 1020 c Soil 1 N x x x Chris Chandler '
12131/15 1030 c Soil 1 N x x x Mark Shaffer
1/18!16 1105 c Soil 1 N x x x Mark Shaffer
1/18/16 1120 c Soil 1 N x x x Chris Chandler
1/18/16 1125 c Soil 1 N x x x Mark Shaffer
1/18/16 1315 c Soil 1 N v x x Mark Shaffer A
1/18/16 1340 c Soil 1 N x x x Chris Chandler
1/18/16 1345 c Soil 1 N x x x Mark Shaffer
>.,::' :'J•C ~~~ ··" ... ,,,.,,, ,:,; Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.
0 Non-Hazard 0Aammable D Skin Irritant 0 Poison B 0Unknown El Return to Client 0 Disposal by lab 0 Archive for Months
Special Instructions/QC Requirements & Comments: Potential tor Radiological Contamination
Custody Seals Intact: El Yes 0 No Custody Seal No.: Cooler Temp. (°C): Obs'd: Corr'd: Therm ID No.:
R,qzuished by: .~~v.D ~~ 0i/?O/l! ~~ Company: Datemme:
3';5;5 ,,,wefll(l. W<ub ¥1;£ (~'{Oqc)~ t~ltJ- /b
'~~:fj~\l'QJ1 ~ JJ ,,);?/~ Company: qi~rr~~:r&c!fJ '?Ji'@d by: ,d_ Company: Datemme:
~ ( -t_e /6 p; e_.~_,1 //tl-6/L- l.a2~·1&:i I~ ~elinquished by: I v Company: Oaternme: RE!ceived in Laboratory by: Company: Datemme:
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11·
TestAmerica St Louis 13715 Rider Trail North
Chain of Custody Record TestAmerica Earth City, MO 63045 phone 314.298.8566 fax
Client Contact Perma-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P0#832953
Sample Identification
802-01-02-P-R-Q-OO
802-01-10-P-S-Q-OO
r----_
------- --------
Regulatory Program: D DW 0 NPDES
Project Manager: Brian Miller Tel/Fax: (314) 810-3333
Analysis Turnaround Time 0 CALENDARDAYS 0 WORKING DAYS
TAT if different from Below
0 2 weeks
0 l Week
0 2 days
D lday -~ ........
Type Sample I Sample I (C--Comp, #of
Date Time G=Grab) Matrix Cont.
114116 I 925 I c Soil 1
1.2131/15 I 1045 I c Soil 1
---+-------
'THE LEADER IN ENVIRONMENTAL TS:ST1NG
QRCRA 0 01!1er: TestAmerica Laboratories, Inc. Site Contact: Ellen Jakub !Date: 1/19/2016 COC No: 011916-FSS1 uib Contact: Ivan Vania !Carrier: Courier __ 3_ of_3_ COCs
t- Sampler: f! - ... f z ::i -- s Z> ~ -- .. Cl
>c E .5
"' >--(/) :c .. .!! :;: .. ;;- ~~ ... _ ... "'
~ E (/) "'::J ... ~ ~:;: ... 0 .. (/).:: ... .., E .. Cl "' UJ ~! "' .. E .E "' ~ s .g E 10 .c .. .. ...
~~ = m 0 3: < !::! u.. Q..
For Lab Use Only: Walk-in Client I I Lab Sampling:
Job I SDG No.:
Sample Specific Notes:
N x x x Mark Shaffer
N x x x Brian Miller
~
-------_J_H-J-1-1
--r-J-~~~~~~~~~~~~~~~~~~~1--~~-t-~~-t-~~-': N ____... . ... , ... I
· -· -· ~ .. ··········-·-· "--rt= I I I I I I I I I I I I' ~ N--W_
--------- N-+-L
--------- ------~ ~ 1~~~m~z~~~Jj\~JJ~~~-~~·~~~~~m~~~~~rit~f:~-zP:~f?~J~~1-~.}f~1~··: r~~-~~t1l§ ;~r~ _:~11; ·~~k ~~-Possible Hazard Identification: Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month) Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.
0 Non-Hazard O Flammable 0 Skin Irritant 0 Poison B 0 Unknown 0 Return to Oient 0 Disposal by Lab 0 Archive fur Months
Special Instructions/QC Requirements & Comments: Potential for Radiological Contamination
Corr'd: Therm ID No.: Company: Datemme:
6~~5 CV'e55 .f'~P-t35 t -z.a- l<P Company: Datemme: 7-A sz_, 1-~,fb /030
Company:·· Date/Time:
I Hematite De-cammfoning; Praject I Permafi>; (for Westmgtm.ll!Se) Noo-Proprietaty ciass 3 I Procerlure:HD.0 -PR-OA-0(1'6, Chair. of Casiod!f I Re<.isron: 3
Login Sample Receipt Checklist
Client: Perma-Fix Environmental Services Inc. Job Number: 160-15789-1
Login Number: 15789
Question Answer Comment
Creator: Clarke, Jill C
List Source: TestAmerica St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or tampered with.
N/ASamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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Definitions/GlossaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Qualifiers
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Rad
Qualifier Description
U Result is less than the sample detection limit.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Method Method Description LaboratoryProtocol
SW8466020A Metals (ICP/MS), Tc-99 TAL SL
EPAMoisture Percent Moisture TAL SL
SW8466020A Metals (ICP/MS), Tc-99 in Activity TAL SL
DOEGA-01-R Cesium-137 & Other Gamma Emitters (GS) TAL SL
Protocol References:
DOE = U.S. Department of Energy
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566
TestAmerica St. Louis
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Sample SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
160-15789-1 B02-01-01-P-S-S-00 Solid 12/31/15 11:50 01/20/16 10:30
160-15789-2 B02-01-02-P-R-S-00 Solid 01/04/16 09:25 01/20/16 10:30
160-15789-3 B02-01-03-P-E-S-00 Solid 01/04/16 09:35 01/20/16 10:30
160-15789-4 B02-01-04-P-S-S-00 Solid 12/29/15 09:25 01/20/16 10:30
160-15789-5 B02-01-05-P-R-S-00 Solid 12/29/15 10:30 01/20/16 10:30
160-15789-6 B02-01-06-P-E-S-00 Solid 12/29/15 10:35 01/20/16 10:30
160-15789-7 B02-01-07-P-S-S-00 Solid 12/29/15 11:00 01/20/16 10:30
160-15789-8 B02-01-08-P-R-S-00 Solid 12/29/15 11:30 01/20/16 10:30
160-15789-9 B02-01-09-P-E-S-00 Solid 12/29/15 11:35 01/20/16 10:30
160-15789-10 B02-01-10-P-S-S-00 Solid 12/31/15 10:45 01/20/16 10:30
160-15789-11 B02-01-11-P-R-S-00 Solid 12/31/15 11:15 01/20/16 10:30
160-15789-12 B02-01-12-P-E-S-00 Solid 12/31/15 11:25 01/20/16 10:30
160-15789-13 B02-01-13-P-S-S-00 Solid 01/18/16 10:05 01/20/16 10:30
160-15789-14 B02-01-14-P-R-S-00 Solid 01/18/16 10:45 01/20/16 10:30
160-15789-15 B02-01-15-P-E-S-00 Solid 01/18/16 10:50 01/20/16 10:30
160-15789-16 B02-01-16-P-S-S-00 Solid 12/29/15 15:20 01/20/16 10:30
160-15789-17 B02-01-17-P-R-S-00 Solid 12/31/15 10:20 01/20/16 10:30
160-15789-18 B02-01-18-P-E-S-00 Solid 12/31/15 10:30 01/20/16 10:30
160-15789-19 B02-01-19-P-S-S-00 Solid 01/18/16 11:05 01/20/16 10:30
160-15789-20 B02-01-20-P-R-S-00 Solid 01/18/16 11:20 01/20/16 10:30
160-15789-21 B02-01-21-P-E-S-00 Solid 01/18/16 11:25 01/20/16 10:30
160-15789-22 B02-01-22-P-S-S-00 Solid 01/18/16 13:15 01/20/16 10:30
160-15789-23 B02-01-23-P-R-S-00 Solid 01/18/16 13:40 01/20/16 10:30
160-15789-24 B02-01-24-P-E-S-00 Solid 01/18/16 13:45 01/20/16 10:30
160-15789-25 B02-01-02-P-R-Q-00 Solid 01/04/16 09:25 01/20/16 10:30
160-15789-26 B02-01-10-P-S-Q-00 Solid 12/31/15 10:45 01/20/16 10:30
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-1Client Sample ID: B02-01-01-P-S-S-00Matrix: SolidDate Collected: 12/31/15 11:50
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.117
(2σ+/-)
0.0406
(2σ+/-)
101/24/16 17:2001/22/16 09:43pCi/g0.0239
RL MDC
0.0388
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 17:20 10.03120.01870.0186U0.0109Americium 241
pCi/g 01/22/16 09:43 01/24/16 17:20 10.1830.1080.108U0.0687Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 17:20 10.02040.03520.03100.159Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 17:20 10.02360.02630.02290.0998Lead 212
pCi/g 01/22/16 09:43 01/24/16 17:20 10.03320.03640.03200.168Lead 214
pCi/g 01/22/16 09:43 01/24/16 17:20 10.1780.4550.3742.53Potassium 40
pCi/g 01/22/16 09:43 01/24/16 17:20 11.180.7260.724U0.532Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 17:20 10.3270.1900.189U0.0877Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 17:20 10.02040.03520.03100.159Radium 226
pCi/g 01/22/16 09:43 01/24/16 17:20 10.3170.2510.2480.361Thorium 234
pCi/g 01/22/16 09:43 01/24/16 17:20 10.08240.04830.0483U0.0187Uranium 235
pCi/g 01/22/16 09:43 01/24/16 17:20 10.02390.04060.03880.117Thorium 232
Tl-208 0.0440 0.0137 0.0144 0.0117 pCi/g 01/22/16 09:43 01/24/16 17:20 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-1Client Sample ID: B02-01-01-P-S-S-00Matrix: SolidDate Collected: 12/31/15 11:50
Percent Solids: 90.9Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000054 0.000016 mg/Kg ☼ 01/20/16 16:10 01/28/16 21:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.0261 U
(2σ+/-)
0.00953
(2σ+/-)
101/28/16 21:1501/20/16 16:10pCi/g0.1841.07
RL MDC
0.00923
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 21:15 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
103
Lab Sample ID: 160-15789-2Client Sample ID: B02-01-02-P-R-S-00Matrix: SolidDate Collected: 01/04/16 09:25
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.09
(2σ+/-)
0.157
(2σ+/-)
101/24/16 17:2101/22/16 09:43pCi/g0.0862
RL MDC
0.113
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 17:21 10.09030.05390.0538U0.0155Americium 241
pCi/g 01/22/16 09:43 01/24/16 17:21 10.3210.3710.3521.16Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 17:21 10.06220.1220.08930.805Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 17:21 10.06240.1530.07341.04Lead 212
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-2Client Sample ID: B02-01-02-P-R-S-00Matrix: SolidDate Collected: 01/04/16 09:25
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte
Lead 214 0.989
(2σ+/-)
0.128
(2σ+/-)
101/24/16 17:2101/22/16 09:43pCi/g0.0567
RL MDC
0.0764
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 17:21 10.2342.191.0119.3Potassium 40
pCi/g 01/22/16 09:43 01/24/16 17:21 14.442.702.69U2.06Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 17:21 10.9740.3480.345U0.452Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 17:21 10.06220.1220.08930.805Radium 226
pCi/g 01/22/16 09:43 01/24/16 17:21 10.7280.5890.5751.24Thorium 234
pCi/g 01/22/16 09:43 01/24/16 17:21 10.2160.1360.135U0.116Uranium 235
pCi/g 01/22/16 09:43 01/24/16 17:21 10.08620.1570.1131.09Thorium 232
Tl-208 0.348 0.0428 0.0558 0.0303 pCi/g 01/22/16 09:43 01/24/16 17:21 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-2Client Sample ID: B02-01-02-P-R-S-00Matrix: SolidDate Collected: 01/04/16 09:25
Percent Solids: 82.1Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000061 0.000018 mg/Kg ☼ 01/20/16 16:10 01/28/16 21:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.111 U
(2σ+/-)
0.0747
(2σ+/-)
101/28/16 21:3801/20/16 16:10pCi/g0.2091.22
RL MDC
0.0740
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 21:38 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
100
Lab Sample ID: 160-15789-3Client Sample ID: B02-01-03-P-E-S-00Matrix: SolidDate Collected: 01/04/16 09:35
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.05
(2σ+/-)
0.158
(2σ+/-)
101/24/16 18:3501/22/16 09:43pCi/g0.110
RL MDC
0.116
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 18:35 10.09590.05670.0567U-0.00207Americium 241
pCi/g 01/22/16 09:43 01/24/16 18:35 10.4110.4580.4401.22Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 18:35 10.07630.1530.1121.00Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 18:35 10.06930.1650.08481.09Lead 212
pCi/g 01/22/16 09:43 01/24/16 18:35 10.07640.1330.08400.994Lead 214
pCi/g 01/22/16 09:43 01/24/16 18:35 10.3522.331.2419.2Potassium 40
pCi/g 01/22/16 09:43 01/24/16 18:35 15.773.303.30U0.763Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 18:35 11.170.3770.369U0.742Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 18:35 10.07630.1530.1121.00Radium 226
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-3Client Sample ID: B02-01-03-P-E-S-00Matrix: SolidDate Collected: 01/04/16 09:35
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte
Thorium 234 1.18
(2σ+/-)
0.528
(2σ+/-)
101/24/16 18:3501/22/16 09:43pCi/g0.809
RL MDC
0.514
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 18:35 10.2220.1470.146U0.154Uranium 235
pCi/g 01/22/16 09:43 01/24/16 18:35 10.1100.1580.1161.05Thorium 232
Tl-208 0.366 0.0500 0.0628 0.0372 pCi/g 01/22/16 09:43 01/24/16 18:35 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-3Client Sample ID: B02-01-03-P-E-S-00Matrix: SolidDate Collected: 01/04/16 09:35
Percent Solids: 81.8Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000061 0.000018 mg/Kg ☼ 01/20/16 16:10 01/28/16 21:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.00936 U
(2σ+/-)
0.0152
(2σ+/-)
101/28/16 21:4201/20/16 16:10pCi/g0.2081.22
RL MDC
0.0152
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 21:42 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
101
Lab Sample ID: 160-15789-4Client Sample ID: B02-01-04-P-S-S-00Matrix: SolidDate Collected: 12/29/15 09:25
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.0689
(2σ+/-)
0.0268
(2σ+/-)
101/24/16 18:3601/22/16 09:43pCi/g0.0597
RL MDC
0.0259
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 18:36 10.03160.2300.230U-0.00574Americium 241
pCi/g 01/22/16 09:43 01/24/16 18:36 10.1570.09370.0935U0.0612Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 18:36 10.02780.03110.02940.0995Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 18:36 10.02140.01850.01720.0521Lead 212
pCi/g 01/22/16 09:43 01/24/16 18:36 10.02610.03080.02780.127Lead 214
pCi/g 01/22/16 09:43 01/24/16 18:36 10.1780.3360.2801.85Potassium 40
pCi/g 01/22/16 09:43 01/24/16 18:36 12.060.3870.386U0.182Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 18:36 10.3530.08450.0843U0.0554Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 18:36 10.02780.03110.02940.0995Radium 226
pCi/g 01/22/16 09:43 01/24/16 18:36 10.2480.1670.166U0.161Thorium 234
pCi/g 01/22/16 09:43 01/24/16 18:36 10.07480.04500.0449U0.0323Uranium 235
pCi/g 01/22/16 09:43 01/24/16 18:36 10.05970.02680.02590.0689Thorium 232
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-4Client Sample ID: B02-01-04-P-S-S-00Matrix: SolidDate Collected: 12/29/15 09:25
Date Received: 01/20/16 10:30
Tl-208 0.0219 0.00902 0.00930 0.0109 pCi/g 01/22/16 09:43 01/24/16 18:36 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-4Client Sample ID: B02-01-04-P-S-S-00Matrix: SolidDate Collected: 12/29/15 09:25
Percent Solids: 96.8Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000050 0.000015 mg/Kg ☼ 01/20/16 16:10 01/28/16 21:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.0175 U
(2σ+/-)
0.0207
(2σ+/-)
101/28/16 21:4601/20/16 16:10pCi/g0.1700.993
RL MDC
0.0207
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 21:46 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
105
Lab Sample ID: 160-15789-5Client Sample ID: B02-01-05-P-R-S-00Matrix: SolidDate Collected: 12/29/15 10:30
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.658
(2σ+/-)
0.115
(2σ+/-)
101/24/16 18:3601/22/16 09:43pCi/g0.0756
RL MDC
0.0933
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 18:36 10.07620.04600.0459U-0.0263Americium 241
pCi/g 01/22/16 09:43 01/24/16 18:36 10.2690.3030.2910.813Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 18:36 10.04290.09210.06710.607Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 18:36 10.05130.1090.05900.710Lead 212
pCi/g 01/22/16 09:43 01/24/16 18:36 10.05220.09130.05800.679Lead 214
pCi/g 01/22/16 09:43 01/24/16 18:36 10.2181.570.80913.1Potassium 40
pCi/g 01/22/16 09:43 01/24/16 18:36 14.042.282.28U0.114Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 18:36 10.7980.2280.225U0.373Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 18:36 10.04290.09210.06710.607Radium 226
pCi/g 01/22/16 09:43 01/24/16 18:36 10.5630.2060.198U0.550Thorium 234
pCi/g 01/22/16 09:43 01/24/16 18:36 10.1660.1000.0996U0.0889Uranium 235
pCi/g 01/22/16 09:43 01/24/16 18:36 10.07560.1150.09330.658Thorium 232
Tl-208 0.222 0.0345 0.0415 0.0280 pCi/g 01/22/16 09:43 01/24/16 18:36 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-5Client Sample ID: B02-01-05-P-R-S-00Matrix: SolidDate Collected: 12/29/15 10:30
Percent Solids: 84.9Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000058 0.000017 mg/Kg ☼ 01/20/16 16:10 01/28/16 21:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0120 U
(2σ+/-)
0.0436
(2σ+/-)
101/28/16 21:5001/20/16 16:10pCi/g0.1971.15
RL MDC
0.0435
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 21:50 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
102
Lab Sample ID: 160-15789-6Client Sample ID: B02-01-06-P-E-S-00Matrix: SolidDate Collected: 12/29/15 10:35
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.16
(2σ+/-)
0.213
(2σ+/-)
101/24/16 18:3801/22/16 09:43pCi/g0.129
RL MDC
0.178
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 18:38 10.07770.05250.0523U0.0371Americium 241
pCi/g 01/22/16 09:43 01/24/16 18:38 10.4340.5240.5021.44Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 18:38 10.08180.1580.1240.941Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 18:38 10.08170.1600.09331.01Lead 212
pCi/g 01/22/16 09:43 01/24/16 18:38 10.07730.1430.1030.951Lead 214
pCi/g 01/22/16 09:43 01/24/16 18:38 10.2732.191.2817.3Potassium 40
pCi/g 01/22/16 09:43 01/24/16 18:38 16.833.723.72U-0.000967Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 18:38 11.190.4580.453U0.602Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 18:38 10.08180.1580.1240.941Radium 226
pCi/g 01/22/16 09:43 01/24/16 18:38 10.9130.3330.322U0.829Thorium 234
pCi/g 01/22/16 09:43 01/24/16 18:38 10.2020.1440.1410.264Uranium 235
pCi/g 01/22/16 09:43 01/24/16 18:38 10.1290.2130.1781.16Thorium 232
Tl-208 0.410 0.0544 0.0691 0.0362 pCi/g 01/22/16 09:43 01/24/16 18:38 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-6Client Sample ID: B02-01-06-P-E-S-00Matrix: SolidDate Collected: 12/29/15 10:35
Percent Solids: 79.4Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000062 0.000019 mg/Kg ☼ 01/20/16 16:10 01/28/16 21:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.0107 U
(2σ+/-)
0.0652
(2σ+/-)
101/28/16 21:5401/20/16 16:10pCi/g0.2131.25
RL MDC
0.0652
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-6Client Sample ID: B02-01-06-P-E-S-00Matrix: SolidDate Collected: 12/29/15 10:35
Percent Solids: 79.4Date Received: 01/20/16 10:30
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 21:54 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
101
Lab Sample ID: 160-15789-7Client Sample ID: B02-01-07-P-S-S-00Matrix: SolidDate Collected: 12/29/15 11:00
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.104
(2σ+/-)
0.0344
(2σ+/-)
101/24/16 19:1301/22/16 09:43pCi/g0.0277
RL MDC
0.0327
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:13 10.03360.01990.0199U-0.00799Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:13 10.1550.08880.0887U0.0400Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:13 10.02220.03300.02970.139Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:13 10.02230.02280.02000.0838Lead 212
pCi/g 01/22/16 09:43 01/24/16 19:13 10.03050.03340.02730.184Lead 214
pCi/g 01/22/16 09:43 01/24/16 19:13 10.1370.4620.3443.01Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:13 11.700.9770.971U1.06Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:13 10.3670.08810.0880U0.0463Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:13 10.02220.03300.02970.139Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:13 10.3370.09760.0968U0.121Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:13 10.07060.04310.0429U0.0375Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:13 10.02770.03440.03270.104Thorium 232
Tl-208 0.0303 0.0133 0.0137 0.0138 pCi/g 01/22/16 09:43 01/24/16 19:13 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-7Client Sample ID: B02-01-07-P-S-S-00Matrix: SolidDate Collected: 12/29/15 11:00
Percent Solids: 93.8Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000051 0.000015 mg/Kg ☼ 01/20/16 16:10 01/28/16 21:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0827 U
(2σ+/-)
0.0483
(2σ+/-)
101/28/16 21:5701/20/16 16:10pCi/g0.1751.02
RL MDC
0.0477
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 21:57 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
104
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-8Client Sample ID: B02-01-08-P-R-S-00Matrix: SolidDate Collected: 12/29/15 11:30
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.723
(2σ+/-)
0.121
(2σ+/-)
101/24/16 19:1601/22/16 09:43pCi/g0.105
RL MDC
0.0963
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:16 10.07260.04320.0432U0.0130Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:16 10.3390.3500.3380.867Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:16 10.05510.1090.08180.690Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:16 10.05290.1210.06450.791Lead 212
pCi/g 01/22/16 09:43 01/24/16 19:16 10.05350.09770.07040.651Lead 214
pCi/g 01/22/16 09:43 01/24/16 19:16 10.2151.750.96514.2Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:16 14.192.942.94U0.000Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:16 10.8720.3260.322U0.455Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:16 10.05510.1090.08180.690Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:16 10.6650.2380.229U0.636Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:16 10.1930.1120.111U0.108Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:16 10.1050.1210.09630.723Thorium 232
Tl-208 0.242 0.0417 0.0487 0.0345 pCi/g 01/22/16 09:43 01/24/16 19:16 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-8Client Sample ID: B02-01-08-P-R-S-00Matrix: SolidDate Collected: 12/29/15 11:30
Percent Solids: 81.9Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000061 0.000018 mg/Kg ☼ 01/20/16 16:10 01/28/16 22:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0497 U
(2σ+/-)
0.0240
(2σ+/-)
101/28/16 22:0101/20/16 16:10pCi/g0.2081.21
RL MDC
0.0236
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 22:01 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
100
Lab Sample ID: 160-15789-9Client Sample ID: B02-01-09-P-E-S-00Matrix: SolidDate Collected: 12/29/15 11:35
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.19
(2σ+/-)
0.175
(2σ+/-)
101/24/16 19:1501/22/16 09:43pCi/g0.104
RL MDC
0.128
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:15 10.1060.06260.0626U0.00334Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:15 10.4630.5680.5451.57Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:15 10.07570.1230.08640.849Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:15 10.07560.1720.08681.15Lead 212
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-9Client Sample ID: B02-01-09-P-E-S-00Matrix: SolidDate Collected: 12/29/15 11:35
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte
Lead 214 1.11
(2σ+/-)
0.147
(2σ+/-)
101/24/16 19:1501/22/16 09:43pCi/g0.0756
RL MDC
0.0904
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:15 10.2742.521.1722.2Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:15 14.983.073.05U2.74Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:15 11.200.7310.728U-0.558Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:15 10.07570.1230.08640.849Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:15 10.8310.3120.2960.915Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:15 10.2370.1300.130U0.115Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:15 10.1040.1750.1281.19Thorium 232
Tl-208 0.359 0.0493 0.0616 0.0406 pCi/g 01/22/16 09:43 01/24/16 19:15 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-9Client Sample ID: B02-01-09-P-E-S-00Matrix: SolidDate Collected: 12/29/15 11:35
Percent Solids: 81.6Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000061 0.000018 mg/Kg ☼ 01/20/16 16:10 01/28/16 22:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0613 U
(2σ+/-)
0.0149
(2σ+/-)
101/28/16 22:0501/20/16 16:10pCi/g0.2071.21
RL MDC
0.0138
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 22:05 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
101
Lab Sample ID: 160-15789-10Client Sample ID: B02-01-10-P-S-S-00Matrix: SolidDate Collected: 12/31/15 10:45
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.0576
(2σ+/-)
0.0268
(2σ+/-)
101/24/16 19:1401/22/16 09:43pCi/g0.0438
RL MDC
0.0262
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:14 10.02920.01720.0172U-0.00578Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:14 10.1970.1060.106U-0.0000829Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:14 10.02330.03370.03040.140Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:14 10.02310.02510.02270.0835Lead 212
pCi/g 01/22/16 09:43 01/24/16 19:14 10.02930.02920.02480.148Lead 214
pCi/g 01/22/16 09:43 01/24/16 19:14 10.1420.3910.3152.27Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:14 11.961.131.13U0.518Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:14 10.3490.05110.0509U0.0418Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:14 10.02330.03370.03040.140Radium 226
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-10Client Sample ID: B02-01-10-P-S-S-00Matrix: SolidDate Collected: 12/31/15 10:45
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte
Thorium 234 0.187 U
(2σ+/-)
0.113
(2σ+/-)
101/24/16 19:1401/22/16 09:43pCi/g0.305
RL MDC
0.111
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:14 10.05990.03850.0383U0.0376Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:14 10.04380.02680.02620.0576Thorium 232
Tl-208 0.0315 0.0110 0.0115 0.00903 pCi/g 01/22/16 09:43 01/24/16 19:14 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-10Client Sample ID: B02-01-10-P-S-S-00Matrix: SolidDate Collected: 12/31/15 10:45
Percent Solids: 92.2Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000052 0.000016 mg/Kg ☼ 01/20/16 16:10 01/28/16 22:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.0192 U
(2σ+/-)
0.0345
(2σ+/-)
101/28/16 22:0901/20/16 16:10pCi/g0.1791.05
RL MDC
0.0345
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 22:09 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
104
Lab Sample ID: 160-15789-11Client Sample ID: B02-01-11-P-R-S-00Matrix: SolidDate Collected: 12/31/15 11:15
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.861
(2σ+/-)
0.174
(2σ+/-)
101/24/16 19:1601/22/16 09:43pCi/g0.0721
RL MDC
0.150
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:16 10.1020.06140.0613U0.0265Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:16 10.4220.4220.4090.990Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:16 10.06350.1310.1010.798Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:16 10.06590.1430.08260.899Lead 212
pCi/g 01/22/16 09:43 01/24/16 19:16 10.06280.1230.09010.807Lead 214
pCi/g 01/22/16 09:43 01/24/16 19:16 10.3952.041.2415.8Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:16 15.833.273.26U2.05Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:16 11.200.3500.347U0.400Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:16 10.06350.1310.1010.798Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:16 10.7780.5300.5071.47Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:16 10.2430.1350.135U0.0887Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:16 10.07210.1740.1500.861Thorium 232
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-11Client Sample ID: B02-01-11-P-R-S-00Matrix: SolidDate Collected: 12/31/15 11:15
Date Received: 01/20/16 10:30
Tl-208 0.302 0.0500 0.0590 0.0362 pCi/g 01/22/16 09:43 01/24/16 19:16 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-11Client Sample ID: B02-01-11-P-R-S-00Matrix: SolidDate Collected: 12/31/15 11:15
Percent Solids: 85.5Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000058 0.000017 mg/Kg ☼ 01/20/16 16:10 01/28/16 22:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.000994 U
(2σ+/-)
0.00883
(2σ+/-)
101/28/16 22:1301/20/16 16:10pCi/g0.1991.16
RL MDC
0.00883
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 22:13 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
100
Lab Sample ID: 160-15789-12Client Sample ID: B02-01-12-P-E-S-00Matrix: SolidDate Collected: 12/31/15 11:25
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.08
(2σ+/-)
0.159
(2σ+/-)
101/24/16 19:4901/22/16 09:43pCi/g0.0901
RL MDC
0.114
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:49 10.09460.05650.0565U0.0156Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:49 10.3050.3340.3161.05Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:49 10.06700.1350.09720.899Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:49 10.06400.1510.07531.01Lead 212
pCi/g 01/22/16 09:43 01/24/16 19:49 10.06630.1320.07831.03Lead 214
pCi/g 01/22/16 09:43 01/24/16 19:49 10.3772.061.0517.3Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:49 14.022.392.38U1.36Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:49 11.090.6610.659U-0.522Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:49 10.06700.1350.09720.899Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:49 10.7740.3110.2990.814Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:49 10.2160.1340.133U0.136Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:49 10.09010.1590.1141.08Thorium 232
Tl-208 0.343 0.0496 0.0611 0.0369 pCi/g 01/22/16 09:43 01/24/16 19:49 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
TestAmerica St. Louis
Page 21 of 46 1/29/2016
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-12Client Sample ID: B02-01-12-P-E-S-00Matrix: SolidDate Collected: 12/31/15 11:25
Percent Solids: 81.1Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000062 0.000019 mg/Kg ☼ 01/20/16 16:10 01/28/16 22:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0494 U
(2σ+/-)
0.0315
(2σ+/-)
101/28/16 22:2801/20/16 16:10pCi/g0.2141.25
RL MDC
0.0312
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 22:28 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
99
Lab Sample ID: 160-15789-13Client Sample ID: B02-01-13-P-S-S-00Matrix: SolidDate Collected: 01/18/16 10:05
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.0969
(2σ+/-)
0.0352
(2σ+/-)
101/24/16 19:5001/22/16 09:43pCi/g0.0234
RL MDC
0.0337
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:50 10.02630.01560.0156U0.00804Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:50 10.1790.1150.114U0.112Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:50 10.02890.03720.03380.148Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:50 10.02200.02350.02090.0834Lead 212
pCi/g 01/22/16 09:43 01/24/16 19:50 10.02140.03160.02630.168Lead 214
pCi/g 01/22/16 09:43 01/24/16 19:50 10.2110.4050.3442.09Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:50 12.411.291.29U-0.117Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:50 10.3820.002370.00237U0.00101Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:50 10.02890.03720.03380.148Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:50 10.2640.1550.154U0.134Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:50 10.09120.03380.0337U0.0233Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:50 10.02340.03520.03370.0969Thorium 232
Tl-208 0.0346 0.0115 0.0120 0.0106 pCi/g 01/22/16 09:43 01/24/16 19:50 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-13Client Sample ID: B02-01-13-P-S-S-00Matrix: SolidDate Collected: 01/18/16 10:05
Percent Solids: 87.6Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000056 0.000017 mg/Kg ☼ 01/20/16 16:10 01/28/16 22:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.0154 U
(2σ+/-)
0.0248
(2σ+/-)
101/28/16 22:3201/20/16 16:10pCi/g0.1931.13
RL MDC
0.0248
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-13Client Sample ID: B02-01-13-P-S-S-00Matrix: SolidDate Collected: 01/18/16 10:05
Percent Solids: 87.6Date Received: 01/20/16 10:30
Re 30 - 110
Carrier
01/20/16 16:10 01/28/16 22:32 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
101
Lab Sample ID: 160-15789-14Client Sample ID: B02-01-14-P-R-S-00Matrix: SolidDate Collected: 01/18/16 10:45
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.03
(2σ+/-)
0.174
(2σ+/-)
101/24/16 19:5001/22/16 09:43pCi/g0.106
RL MDC
0.139
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:50 10.09000.05350.0535U0.0117Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:50 10.2600.3670.3331.51Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:50 10.06250.1190.08700.794Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:50 10.06810.1390.07800.886Lead 212
pCi/g 01/22/16 09:43 01/24/16 19:50 10.06880.1270.08110.941Lead 214
pCi/g 01/22/16 09:43 01/24/16 19:50 10.3342.161.0418.8Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:50 12.312.702.626.63Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:50 10.9700.1980.194U0.381Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:50 10.06250.1190.08700.794Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:50 10.7300.6090.5921.37Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:50 10.2220.1330.132U0.112Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:50 10.1060.1740.1391.03Thorium 232
Tl-208 0.302 0.0375 0.0487 0.0282 pCi/g 01/22/16 09:43 01/24/16 19:50 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-14Client Sample ID: B02-01-14-P-R-S-00Matrix: SolidDate Collected: 01/18/16 10:45
Percent Solids: 78.3Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000064 0.000019 mg/Kg ☼ 01/20/16 17:35 01/28/16 19:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0404 U
(2σ+/-)
0.0361
(2σ+/-)
101/28/16 19:5701/20/16 17:35pCi/g0.2181.28
RL MDC
0.0359
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 19:57 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
100
TestAmerica St. Louis
Page 23 of 46 1/29/2016
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-15Client Sample ID: B02-01-15-P-E-S-00Matrix: SolidDate Collected: 01/18/16 10:50
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.03
(2σ+/-)
0.162
(2σ+/-)
101/24/16 19:5201/22/16 09:43pCi/g0.0674
RL MDC
0.123
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:52 10.09280.05500.0550U-0.000866Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:52 10.3300.3990.3731.38Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:52 10.06090.1230.08840.825Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:52 10.05050.1460.06631.01Lead 212
pCi/g 01/22/16 09:43 01/24/16 19:52 10.06090.1260.07710.960Lead 214
pCi/g 01/22/16 09:43 01/24/16 19:52 10.3212.041.0217.3Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:52 14.052.462.46U1.93Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:52 10.9470.2340.227U0.534Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:52 10.06090.1230.08840.825Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:52 10.6670.2460.2350.709Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:52 10.2040.1200.120U0.0586Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:52 10.06740.1620.1231.03Thorium 232
Tl-208 0.335 0.0412 0.0539 0.0302 pCi/g 01/22/16 09:43 01/24/16 19:52 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-15Client Sample ID: B02-01-15-P-E-S-00Matrix: SolidDate Collected: 01/18/16 10:50
Percent Solids: 80.8Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000061 0.000018 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.00922 U
(2σ+/-)
0.0281
(2σ+/-)
101/28/16 20:0901/20/16 17:35pCi/g0.2101.22
RL MDC
0.0281
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:09 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
101
Lab Sample ID: 160-15789-16Client Sample ID: B02-01-16-P-S-S-00Matrix: SolidDate Collected: 12/29/15 15:20
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.0730 U
(2σ+/-)
0.0478
(2σ+/-)
101/24/16 19:5301/22/16 09:43pCi/g0.0860
RL MDC
0.0473
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:53 10.03940.02300.0230U-0.00551Americium 241
pCi/g 01/22/16 09:43 01/24/16 19:53 10.2820.1600.160U0.0606Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 19:53 10.02110.04200.03810.170Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 19:53 10.02790.03370.02920.130Lead 212
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-16Client Sample ID: B02-01-16-P-S-S-00Matrix: SolidDate Collected: 12/29/15 15:20
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte
Lead 214 0.206
(2σ+/-)
0.0422
(2σ+/-)
101/24/16 19:5301/22/16 09:43pCi/g0.0269
RL MDC
0.0364
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 19:53 10.2060.6390.5163.68Potassium 40
pCi/g 01/22/16 09:43 01/24/16 19:53 13.501.851.85U0.490Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 19:53 10.5110.006190.00617U0.00492Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 19:53 10.02110.04200.03810.170Radium 226
pCi/g 01/22/16 09:43 01/24/16 19:53 10.4000.1720.168U0.344Thorium 234
pCi/g 01/22/16 09:43 01/24/16 19:53 10.08010.02570.0257U0.00171Uranium 235
pCi/g 01/22/16 09:43 01/24/16 19:53 10.08600.04780.0473U0.0730Thorium 232
Tl-208 0.0403 0.0170 0.0175 0.0158 pCi/g 01/22/16 09:43 01/24/16 19:53 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-16Client Sample ID: B02-01-16-P-S-S-00Matrix: SolidDate Collected: 12/29/15 15:20
Percent Solids: 94.5Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000051 0.000015 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.0174 U
(2σ+/-)
0.0332
(2σ+/-)
101/28/16 20:1301/20/16 17:35pCi/g0.1761.03
RL MDC
0.0332
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:13 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
104
Lab Sample ID: 160-15789-17Client Sample ID: B02-01-17-P-R-S-00Matrix: SolidDate Collected: 12/31/15 10:20
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.550
(2σ+/-)
0.0980
(2σ+/-)
101/24/16 20:2501/22/16 09:43pCi/g0.0662
RL MDC
0.0803
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 20:25 10.06750.04020.0402U0.00945Americium 241
pCi/g 01/22/16 09:43 01/24/16 20:25 10.2360.2830.2700.834Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 20:25 10.04770.08120.06460.474Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 20:25 10.04480.08530.04990.534Lead 212
pCi/g 01/22/16 09:43 01/24/16 20:25 10.04280.08190.05690.567Lead 214
pCi/g 01/22/16 09:43 01/24/16 20:25 10.1681.190.6739.56Potassium 40
pCi/g 01/22/16 09:43 01/24/16 20:25 13.201.161.15U1.57Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 20:25 10.6830.2080.206U0.244Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 20:25 10.04770.08120.06460.474Radium 226
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-17Client Sample ID: B02-01-17-P-R-S-00Matrix: SolidDate Collected: 12/31/15 10:20
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte
Thorium 234 0.510 U
(2σ+/-)
0.339
(2σ+/-)
101/24/16 20:2501/22/16 09:43pCi/g0.545
RL MDC
0.335
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 20:25 10.1480.09620.0958U0.0852Uranium 235
pCi/g 01/22/16 09:43 01/24/16 20:25 10.06620.09800.08030.550Thorium 232
Tl-208 0.180 0.0313 0.0365 0.0259 pCi/g 01/22/16 09:43 01/24/16 20:25 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-17Client Sample ID: B02-01-17-P-R-S-00Matrix: SolidDate Collected: 12/31/15 10:20
Percent Solids: 92.5Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000052 0.000016 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.00233 U
(2σ+/-)
0.0385
(2σ+/-)
101/28/16 20:1701/20/16 17:35pCi/g0.1791.05
RL MDC
0.0385
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:17 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
103
Lab Sample ID: 160-15789-18Client Sample ID: B02-01-18-P-E-S-00Matrix: SolidDate Collected: 12/31/15 10:30
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.08
(2σ+/-)
0.170
(2σ+/-)
101/24/16 20:2601/22/16 09:43pCi/g0.0800
RL MDC
0.129
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 20:26 10.09160.05430.0543U0.00422Americium 241
pCi/g 01/22/16 09:43 01/24/16 20:26 10.3480.4430.4151.50Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 20:26 10.06250.1220.08920.807Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 20:26 10.06300.1500.07680.993Lead 212
pCi/g 01/22/16 09:43 01/24/16 20:26 10.07190.1380.09580.957Lead 214
pCi/g 01/22/16 09:43 01/24/16 20:26 10.2332.181.1418.2Potassium 40
pCi/g 01/22/16 09:43 01/24/16 20:26 15.012.122.10U2.57Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 20:26 11.050.3360.332U0.453Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 20:26 10.06250.1220.08920.807Radium 226
pCi/g 01/22/16 09:43 01/24/16 20:26 10.7080.2700.2580.754Thorium 234
pCi/g 01/22/16 09:43 01/24/16 20:26 10.1380.07980.0792U0.101Uranium 235
pCi/g 01/22/16 09:43 01/24/16 20:26 10.08000.1700.1291.08Thorium 232
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-18Client Sample ID: B02-01-18-P-E-S-00Matrix: SolidDate Collected: 12/31/15 10:30
Date Received: 01/20/16 10:30
Tl-208 0.375 0.0486 0.0623 0.0351 pCi/g 01/22/16 09:43 01/24/16 20:26 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-18Client Sample ID: B02-01-18-P-E-S-00Matrix: SolidDate Collected: 12/31/15 10:30
Percent Solids: 82.9Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000059 0.000018 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.00751 U
(2σ+/-)
0.00466
(2σ+/-)
101/28/16 20:2101/20/16 17:35pCi/g0.2031.19
RL MDC
0.00460
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:21 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
101
Lab Sample ID: 160-15789-19Client Sample ID: B02-01-19-P-S-S-00Matrix: SolidDate Collected: 01/18/16 11:05
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.0773
(2σ+/-)
0.0395
(2σ+/-)
101/24/16 20:2701/22/16 09:43pCi/g0.0623
RL MDC
0.0387
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 20:27 10.02850.01600.0160U0.00149Americium 241
pCi/g 01/22/16 09:43 01/24/16 20:27 10.2170.1200.120U0.00896Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 20:27 10.02380.03530.03100.164Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 20:27 10.02150.02470.02110.0987Lead 212
pCi/g 01/22/16 09:43 01/24/16 20:27 10.02920.03110.02740.141Lead 214
pCi/g 01/22/16 09:43 01/24/16 20:27 10.1830.4620.3552.95Potassium 40
pCi/g 01/22/16 09:43 01/24/16 20:27 11.881.121.12U0.758Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 20:27 10.3880.07110.0709U0.0514Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 20:27 10.02380.03530.03100.164Radium 226
pCi/g 01/22/16 09:43 01/24/16 20:27 10.2830.1000.0994U0.140Thorium 234
pCi/g 01/22/16 09:43 01/24/16 20:27 10.06910.03280.0327U0.0297Uranium 235
pCi/g 01/22/16 09:43 01/24/16 20:27 10.06230.03950.03870.0773Thorium 232
Tl-208 0.0302 0.0106 0.0110 0.0120 pCi/g 01/22/16 09:43 01/24/16 20:27 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
TestAmerica St. Louis
Page 27 of 46 1/29/2016
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-19Client Sample ID: B02-01-19-P-S-S-00Matrix: SolidDate Collected: 01/18/16 11:05
Percent Solids: 93.2Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000052 0.000016 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.00467 U
(2σ+/-)
0.0440
(2σ+/-)
101/28/16 20:2501/20/16 17:35pCi/g0.1801.05
RL MDC
0.0440
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:25 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
103
Lab Sample ID: 160-15789-20Client Sample ID: B02-01-20-P-R-S-00Matrix: SolidDate Collected: 01/18/16 11:20
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.780
(2σ+/-)
0.119
(2σ+/-)
101/24/16 20:2801/22/16 09:43pCi/g0.0658
RL MDC
0.0886
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 09:43 01/24/16 20:28 10.07930.04750.0474U-0.0165Americium 241
pCi/g 01/22/16 09:43 01/24/16 20:28 10.2980.3820.3581.31Bismuth 212
pCi/g 01/22/16 09:43 01/24/16 20:28 10.04900.09210.06950.582Bismuth 214
pCi/g 01/22/16 09:43 01/24/16 20:28 10.04860.1190.06090.791Lead 212
pCi/g 01/22/16 09:43 01/24/16 20:28 10.05210.1060.06630.790Lead 214
pCi/g 01/22/16 09:43 01/24/16 20:28 10.1781.700.87614.3Potassium 40
pCi/g 01/22/16 09:43 01/24/16 20:28 16.180.7720.772U0.000Protactinium 234m
pCi/g 01/22/16 09:43 01/24/16 20:28 10.8160.5060.502U-0.531Protactinium 231
pCi/g 01/22/16 09:43 01/24/16 20:28 10.04900.09210.06950.582Radium 226
pCi/g 01/22/16 09:43 01/24/16 20:28 10.6600.4250.4140.922Thorium 234
pCi/g 01/22/16 09:43 01/24/16 20:28 10.1820.1100.110U0.0613Uranium 235
pCi/g 01/22/16 09:43 01/24/16 20:28 10.06580.1190.08860.780Thorium 232
Tl-208 0.257 0.0356 0.0444 0.0248 pCi/g 01/22/16 09:43 01/24/16 20:28 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-20Client Sample ID: B02-01-20-P-R-S-00Matrix: SolidDate Collected: 01/18/16 11:20
Percent Solids: 85.4Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000059 0.000018 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0519 U
(2σ+/-)
0.0598
(2σ+/-)
101/28/16 20:2801/20/16 17:35pCi/g0.2011.17
RL MDC
0.0596
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-20Client Sample ID: B02-01-20-P-R-S-00Matrix: SolidDate Collected: 01/18/16 11:20
Percent Solids: 85.4Date Received: 01/20/16 10:30
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:28 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
100
Lab Sample ID: 160-15789-21Client Sample ID: B02-01-21-P-E-S-00Matrix: SolidDate Collected: 01/18/16 11:25
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.15
(2σ+/-)
0.214
(2σ+/-)
101/24/16 20:2901/22/16 10:00pCi/g0.128
RL MDC
0.179
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 10:00 01/24/16 20:29 10.1180.06980.0698U-0.00452Americium 241
pCi/g 01/22/16 10:00 01/24/16 20:29 10.4230.4100.3861.31Bismuth 212
pCi/g 01/22/16 10:00 01/24/16 20:29 10.08180.1740.1311.10Bismuth 214
pCi/g 01/22/16 10:00 01/24/16 20:29 10.08490.1670.09591.05Lead 212
pCi/g 01/22/16 10:00 01/24/16 20:29 10.08650.1580.1081.11Lead 214
pCi/g 01/22/16 10:00 01/24/16 20:29 10.4392.301.3917.9Potassium 40
pCi/g 01/22/16 10:00 01/24/16 20:29 17.4912.212.2U-1.61Protactinium 234m
pCi/g 01/22/16 10:00 01/24/16 20:29 11.380.3070.301U0.579Protactinium 231
pCi/g 01/22/16 10:00 01/24/16 20:29 10.08180.1740.1311.10Radium 226
pCi/g 01/22/16 10:00 01/24/16 20:29 10.9590.6210.6051.31Thorium 234
pCi/g 01/22/16 10:00 01/24/16 20:29 10.2450.1510.150U0.149Uranium 235
pCi/g 01/22/16 10:00 01/24/16 20:29 10.1280.2140.1791.15Thorium 232
Tl-208 0.428 0.0584 0.0734 0.0376 pCi/g 01/22/16 10:00 01/24/16 20:29 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-21Client Sample ID: B02-01-21-P-E-S-00Matrix: SolidDate Collected: 01/18/16 11:25
Percent Solids: 80.6Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000062 0.000019 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.0102 U
(2σ+/-)
0.0312
(2σ+/-)
101/28/16 20:3201/20/16 17:35pCi/g0.2131.24
RL MDC
0.0312
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:32 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
100
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-22Client Sample ID: B02-01-22-P-S-S-00Matrix: SolidDate Collected: 01/18/16 13:15
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.220
(2σ+/-)
0.0606
(2σ+/-)
101/24/16 21:0601/22/16 10:00pCi/g0.0609
RL MDC
0.0564
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 10:00 01/24/16 21:06 10.04750.4380.438U-0.00669Americium 241
pCi/g 01/22/16 10:00 01/24/16 21:06 10.2490.1600.159U0.196Bismuth 212
pCi/g 01/22/16 10:00 01/24/16 21:06 10.03510.05520.04620.294Bismuth 214
pCi/g 01/22/16 10:00 01/24/16 21:06 10.03170.04800.03360.264Lead 212
pCi/g 01/22/16 10:00 01/24/16 21:06 10.03640.05480.04320.323Lead 214
pCi/g 01/22/16 10:00 01/24/16 21:06 10.1830.7410.4845.58Potassium 40
pCi/g 01/22/16 10:00 01/24/16 21:06 12.451.501.49U1.21Protactinium 234m
pCi/g 01/22/16 10:00 01/24/16 21:06 10.4690.1530.152U0.131Protactinium 231
pCi/g 01/22/16 10:00 01/24/16 21:06 10.03510.05520.04620.294Radium 226
pCi/g 01/22/16 10:00 01/24/16 21:06 10.3590.1310.127U0.338Thorium 234
pCi/g 01/22/16 10:00 01/24/16 21:06 10.1230.07510.0746U0.0785Uranium 235
pCi/g 01/22/16 10:00 01/24/16 21:06 10.06090.06060.05640.220Thorium 232
Tl-208 0.0910 0.0195 0.0216 0.0166 pCi/g 01/22/16 10:00 01/24/16 21:06 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-22Client Sample ID: B02-01-22-P-S-S-00Matrix: SolidDate Collected: 01/18/16 13:15
Percent Solids: 92.4Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 0.000017 J 0.000053 0.000016 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.288
(2σ+/-)
0.0419
(2σ+/-)
101/28/16 20:4801/20/16 17:35pCi/g0.1821.06
RL MDC
0.0324
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:48 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
102
Lab Sample ID: 160-15789-23Client Sample ID: B02-01-23-P-R-S-00Matrix: SolidDate Collected: 01/18/16 13:40
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.894
(2σ+/-)
0.139
(2σ+/-)
101/24/16 21:0701/22/16 10:00pCi/g0.0970
RL MDC
0.104
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 10:00 01/24/16 21:07 10.08760.05300.0529U0.0336Americium 241
pCi/g 01/22/16 10:00 01/24/16 21:07 10.3120.3570.3381.11Bismuth 212
pCi/g 01/22/16 10:00 01/24/16 21:07 10.05880.1210.09000.783Bismuth 214
pCi/g 01/22/16 10:00 01/24/16 21:07 10.05410.1370.06750.918Lead 212
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-23Client Sample ID: B02-01-23-P-R-S-00Matrix: SolidDate Collected: 01/18/16 13:40
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte
Lead 214 0.835
(2σ+/-)
0.114
(2σ+/-)
101/24/16 21:0701/22/16 10:00pCi/g0.0548
RL MDC
0.0741
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 10:00 01/24/16 21:07 10.3841.891.0215.6Potassium 40
pCi/g 01/22/16 10:00 01/24/16 21:07 14.152.062.014.71Protactinium 234m
pCi/g 01/22/16 10:00 01/24/16 21:07 10.7640.2880.284U0.454Protactinium 231
pCi/g 01/22/16 10:00 01/24/16 21:07 10.05880.1210.09000.783Radium 226
pCi/g 01/22/16 10:00 01/24/16 21:07 10.6880.4700.4471.41Thorium 234
pCi/g 01/22/16 10:00 01/24/16 21:07 10.2010.1330.132U0.133Uranium 235
pCi/g 01/22/16 10:00 01/24/16 21:07 10.09700.1390.1040.894Thorium 232
Tl-208 0.319 0.0426 0.0540 0.0313 pCi/g 01/22/16 10:00 01/24/16 21:07 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-23Client Sample ID: B02-01-23-P-R-S-00Matrix: SolidDate Collected: 01/18/16 13:40
Percent Solids: 80.3Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 0.000027 J 0.000062 0.000019 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.464
(2σ+/-)
0.0477
(2σ+/-)
101/28/16 20:5201/20/16 17:35pCi/g0.2141.25
RL MDC
0.0212
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:52 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
100
Lab Sample ID: 160-15789-24Client Sample ID: B02-01-24-P-E-S-00Matrix: SolidDate Collected: 01/18/16 13:45
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 1.03
(2σ+/-)
0.151
(2σ+/-)
101/24/16 21:5501/22/16 10:00pCi/g0.110
RL MDC
0.108
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 10:00 01/24/16 21:55 10.09330.05570.0557U-0.0129Americium 241
pCi/g 01/22/16 10:00 01/24/16 21:55 10.3050.3620.3401.20Bismuth 212
pCi/g 01/22/16 10:00 01/24/16 21:55 10.05610.1200.08350.826Bismuth 214
pCi/g 01/22/16 10:00 01/24/16 21:55 10.05730.1490.07061.01Lead 212
pCi/g 01/22/16 10:00 01/24/16 21:55 10.05680.1190.07760.868Lead 214
pCi/g 01/22/16 10:00 01/24/16 21:55 10.3652.091.0417.7Potassium 40
pCi/g 01/22/16 10:00 01/24/16 21:55 14.352.662.65U2.16Protactinium 234m
pCi/g 01/22/16 10:00 01/24/16 21:55 10.6650.4040.403U0.306Protactinium 231
pCi/g 01/22/16 10:00 01/24/16 21:55 10.05610.1200.08350.826Radium 226
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-24Client Sample ID: B02-01-24-P-E-S-00Matrix: SolidDate Collected: 01/18/16 13:45
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte
Thorium 234 1.02
(2σ+/-)
0.285
(2σ+/-)
101/24/16 21:5501/22/16 10:00pCi/g0.716
RL MDC
0.265
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 10:00 01/24/16 21:55 10.2150.1210.121U0.131Uranium 235
pCi/g 01/22/16 10:00 01/24/16 21:55 10.1100.1510.1081.03Thorium 232
Tl-208 0.354 0.0454 0.0584 0.0336 pCi/g 01/22/16 10:00 01/24/16 21:55 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-24Client Sample ID: B02-01-24-P-E-S-00Matrix: SolidDate Collected: 01/18/16 13:45
Percent Solids: 80.5Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000062 0.000019 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0403 U
(2σ+/-)
0.0252
(2σ+/-)
101/28/16 20:5501/20/16 17:35pCi/g0.2121.24
RL MDC
0.0249
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:55 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
101
Lab Sample ID: 160-15789-25Client Sample ID: B02-01-02-P-R-Q-00Matrix: SolidDate Collected: 01/04/16 09:25
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.638
(2σ+/-)
0.119
(2σ+/-)
101/24/16 21:5601/22/16 10:00pCi/g0.0719
RL MDC
0.0993
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 10:00 01/24/16 21:56 10.07130.02310.0231U0.000Americium 241
pCi/g 01/22/16 10:00 01/24/16 21:56 10.2110.3130.2921.08Bismuth 212
pCi/g 01/22/16 10:00 01/24/16 21:56 10.05200.09370.07520.538Bismuth 214
pCi/g 01/22/16 10:00 01/24/16 21:56 10.04550.09700.05720.605Lead 212
pCi/g 01/22/16 10:00 01/24/16 21:56 10.06770.09750.07270.624Lead 214
pCi/g 01/22/16 10:00 01/24/16 21:56 10.3071.460.90911.1Potassium 40
pCi/g 01/22/16 10:00 01/24/16 21:56 13.902.172.17U0.453Protactinium 234m
pCi/g 01/22/16 10:00 01/24/16 21:56 10.7420.3150.313U0.365Protactinium 231
pCi/g 01/22/16 10:00 01/24/16 21:56 10.05200.09370.07520.538Radium 226
pCi/g 01/22/16 10:00 01/24/16 21:56 10.5900.3870.3770.832Thorium 234
pCi/g 01/22/16 10:00 01/24/16 21:56 10.1550.1170.1160.180Uranium 235
pCi/g 01/22/16 10:00 01/24/16 21:56 10.07190.1190.09930.638Thorium 232
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-25Client Sample ID: B02-01-02-P-R-Q-00Matrix: SolidDate Collected: 01/04/16 09:25
Date Received: 01/20/16 10:30
Tl-208 0.188 0.0323 0.0377 0.0239 pCi/g 01/22/16 10:00 01/24/16 21:56 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
Lab Sample ID: 160-15789-25Client Sample ID: B02-01-02-P-R-Q-00Matrix: SolidDate Collected: 01/04/16 09:25
Percent Solids: 83.9Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000059 0.000018 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 0.0145 U
(2σ+/-)
0.00323
(2σ+/-)
101/28/16 20:5901/20/16 17:35pCi/g0.2011.18
RL MDC
0.00294
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 20:59 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
101
Lab Sample ID: 160-15789-26Client Sample ID: B02-01-10-P-S-Q-00Matrix: SolidDate Collected: 12/31/15 10:45
Date Received: 01/20/16 10:30
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte
Actinium 228 0.156
(2σ+/-)
0.0485
(2σ+/-)
101/24/16 21:5701/22/16 10:00pCi/g0.0464
RL MDC
0.0459
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
pCi/g 01/22/16 10:00 01/24/16 21:57 10.03590.02940.0294U-0.00111Americium 241
pCi/g 01/22/16 10:00 01/24/16 21:57 10.1840.1040.104U0.0395Bismuth 212
pCi/g 01/22/16 10:00 01/24/16 21:57 10.02680.03690.03270.166Bismuth 214
pCi/g 01/22/16 10:00 01/24/16 21:57 10.02060.02680.02160.122Lead 212
pCi/g 01/22/16 10:00 01/24/16 21:57 10.03330.03430.02940.170Lead 214
pCi/g 01/22/16 10:00 01/24/16 21:57 10.2240.4790.3782.93Potassium 40
pCi/g 01/22/16 10:00 01/24/16 21:57 11.700.9790.978U0.505Protactinium 234m
pCi/g 01/22/16 10:00 01/24/16 21:57 10.3990.02160.0216U0.0145Protactinium 231
pCi/g 01/22/16 10:00 01/24/16 21:57 10.02680.03690.03270.166Radium 226
pCi/g 01/22/16 10:00 01/24/16 21:57 10.3130.2420.240U0.303Thorium 234
pCi/g 01/22/16 10:00 01/24/16 21:57 10.09550.04240.0423U0.0320Uranium 235
pCi/g 01/22/16 10:00 01/24/16 21:57 10.04640.04850.04590.156Thorium 232
Tl-208 0.0354 0.0117 0.0123 0.0128 pCi/g 01/22/16 10:00 01/24/16 21:57 1
(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Other Detected
Radionuclides
Uncert. Uncert.
TestAmerica St. Louis
Page 33 of 46 1/29/2016
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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Lab Sample ID: 160-15789-26Client Sample ID: B02-01-10-P-S-Q-00Matrix: SolidDate Collected: 12/31/15 10:45
Percent Solids: 89.2Date Received: 01/20/16 10:30
Method: 6020A - Metals (ICP/MS), Tc-99RL MDL
Technetium 99 ND 0.000056 0.000017 mg/Kg ☼ 01/20/16 17:35 01/28/16 21:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Analyte
Technetium 99 -0.0134 U
(2σ+/-)
0.00282
(2σ+/-)
101/28/16 21:0301/20/16 17:35pCi/g0.1921.12
RL MDC
0.00253
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
Re 30 - 110
Carrier
01/20/16 17:35 01/28/16 21:03 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
100
TestAmerica St. Louis
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QC Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Method: 6020A - Metals (ICP/MS), Tc-99
Client Sample ID: Method BlankLab Sample ID: MB 160-233463/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233463
RL MDL
Technetium 99 ND 0.000048 0.000014 mg/Kg 01/20/16 16:10 01/28/16 21:07 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-233463/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233463
Technetium 99 0.00123 0.00111 mg/Kg 90 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233463
Technetium 99 ND 0.00135 0.00121 mg/Kg 90 75 - 125☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233463
Technetium 99 ND 0.00135 0.00122 mg/Kg 91 75 - 125 1 30☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 160-233467/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233467
RL MDL
Technetium 99 ND 0.000048 0.000014 mg/Kg 01/20/16 17:35 01/28/16 19:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-233467/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233467
Technetium 99 0.00123 0.00113 mg/Kg 92 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: B02-01-14-P-R-S-00Lab Sample ID: 160-15789-14 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233467
Technetium 99 ND 0.00157 0.00144 mg/Kg 91 75 - 125☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: B02-01-14-P-R-S-00Lab Sample ID: 160-15789-14 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233467
Technetium 99 ND 0.00157 0.00142 mg/Kg 91 75 - 125 1 30☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica St. Louis
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QC Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity
Client Sample ID: Method BlankLab Sample ID: MB 160-233463/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233463
Technetium 99
Analyte
U 101/28/16 21:0701/20/16 16:10pCi/g0.164
MDC
0.959
RL
0.009060.00901
(2σ+/-) (2σ+/-)
MB
-0.009846
MB
Dil FacPrepared AnalyzedUnitResult Qualifier
Uncert.
Count
Uncert.
Total
Carrier
Re 30 - 110 01/20/16 16:10 01/28/16 21:07 1
Dil FacPrepared AnalyzedQualifier Limits%Yield
104
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-233463/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233463
Technetium 99
Analyte
120-809018.9421.0 1.92 0.955 0.164
RL MDC(2σ+/-)
LCS LCS
pCi/g
UnitResult Qual %RecAdded
Spike
Limits
%Rec.Uncert.
Total
Re
Carrier
30 - 110
LCS
Qualifier Limits%Yield
105
LCS
Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233463
Technetium 99
Analyte
125-759020.7823.1-0.0261 U 1.96 1.08 0.185
RL MDC(2σ+/-)
MS MS
pCi/g
UnitResult Qual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%Rec.Uncert.
Total
Re
Carrier
30 - 110
MS
Qualifier Limits%Yield
102
MS
Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233463
Technetium 99
Analyte
10.04125-759120.9523.1-0.0261 U 2.13 1.07 0.183
RL MDC(2σ+/-)
MSD MSD
pCi/g
UnitResult Qual %Rec LimitAdded
Spike
Result
Sample Sample
Qual Limits
%Rec.Uncert.
Total
RER
RER
Re
Carrier
30 - 110
MSD
Qualifier Limits%Yield
103
MSD
Client Sample ID: Method BlankLab Sample ID: MB 160-233467/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233467
Technetium 99
Analyte
U 101/28/16 19:3801/20/16 17:35pCi/g0.164
MDC
0.959
RL
0.004180.00259
(2σ+/-) (2σ+/-)
MB
-0.03562
MB
Dil FacPrepared AnalyzedUnitResult Qualifier
Uncert.
Count
Uncert.
Total
TestAmerica St. Louis
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QC Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-233467/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233467
Carrier
Re 30 - 110 01/20/16 17:35 01/28/16 19:38 1
Dil FacPrepared AnalyzedQualifier Limits%Yield
104
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-233467/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233467
Technetium 99
Analyte
120-809219.4321.0 1.88 0.965 0.165
RL MDC(2σ+/-)
LCS LCS
pCi/g
UnitResult Qual %RecAdded
Spike
Limits
%Rec.Uncert.
Total
Re
Carrier
30 - 110
LCS
Qualifier Limits%Yield
104
LCS
Client Sample ID: B02-01-14-P-R-S-00Lab Sample ID: 160-15789-14 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233467
Technetium 99
Analyte
125-759124.6026.90.0404 U 2.67 1.27 0.218
RL MDC(2σ+/-)
MS MS
pCi/g
UnitResult Qual %RecAdded
Spike
Result
Sample Sample
Qual Limits
%Rec.Uncert.
Total
Re
Carrier
30 - 110
MS
Qualifier Limits%Yield
101
MS
Client Sample ID: B02-01-14-P-R-S-00Lab Sample ID: 160-15789-14 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233467
Technetium 99
Analyte
10.06125-759124.3226.80.0404 U 2.31 1.28 0.219
RL MDC(2σ+/-)
MSD MSD
pCi/g
UnitResult Qual %Rec LimitAdded
Spike
Result
Sample Sample
Qual Limits
%Rec.Uncert.
Total
RER
RER
Re
Carrier
30 - 110
MSD
Qualifier Limits%Yield
99
MSD
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method BlankLab Sample ID: MB 160-233602/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233900 Prep Batch: 233602
Actinium 228
Analyte
U 101/24/16 17:5901/22/16 09:43pCi/g0.0535
MDCRL
0.03090.0309
(2σ+/-) (2σ+/-)
MB
0.01798
MB
Dil FacPrepared AnalyzedUnitResult Qualifier
Uncert.
Count
Uncert.
Total
101/24/16 17:5901/22/16 09:43pCi/g0.02440.01330.0133U-0.0001374Americium 241
101/24/16 17:5901/22/16 09:43pCi/g0.2160.05510.0551U0.0000Bismuth 212
101/24/16 17:5901/22/16 09:43pCi/g0.04200.006740.00674U-0.0007974Bismuth 214
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QC Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 160-233602/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233900 Prep Batch: 233602
Lead 212
Analyte
U 101/24/16 17:5901/22/16 09:43pCi/g0.0319
MDCRL
0.2940.294
(2σ+/-) (2σ+/-)
MB
-0.007355
MB
Dil FacPrepared AnalyzedUnitResult Qualifier
Uncert.
Count
Uncert.
Total
101/24/16 17:5901/22/16 09:43pCi/g0.03670.4880.488U-0.01219Lead 214
101/24/16 17:5901/22/16 09:43pCi/g0.2870.2090.209U-0.02888Potassium 40
101/24/16 17:5901/22/16 09:43pCi/g1.210.3300.330U0.0000Protactinium 234m
101/24/16 17:5901/22/16 09:43pCi/g0.3480.02040.0204U-0.008926Protactinium 231
101/24/16 17:5901/22/16 09:43pCi/g0.04200.006740.00674U-0.0007974Radium 226
101/24/16 17:5901/22/16 09:43pCi/g0.2370.02170.0217U0.007387Thorium 234
101/24/16 17:5901/22/16 09:43pCi/g0.06990.03910.0391U-0.007831Uranium 235
101/24/16 17:5901/22/16 09:43pCi/g0.05350.03090.0309U0.01798Thorium 232
Other Detected
Radionuclide
None
MB
(2σ+/-) (2σ+/-) MDCRL
pCi/g 01/22/16 09:43 01/24/16 17:59 1
MB
Dil FacPrepared AnalyzedUnitResult Qualifier
Uncert.
Count
Uncert.
Total
Radionuclides
Other Detected
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-233602/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233899 Prep Batch: 233602
Americium 241
Analyte
116-87106107.1101 11.2 0.529
RL MDC(2σ+/-)
LCS LCS
pCi/g
UnitResult Qual %RecAdded
Spike
Limits
%Rec.Uncert.
Total
Cesium 137 34.2 37.48 3.87 0.200 0.159 pCi/g 109 87 - 120
Cobalt 60 32.5 34.86 3.46 0.0940 pCi/g 107 87 - 115
Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233897 Prep Batch: 233602
Actinium 228
Analyte
10.660.067430.117 0.0338 0.0498
RL MDC(2σ+/-)
DU DU
pCi/g
UnitResult Qual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Americium 241 0.0109 U -0.00429
4
U 0.0213 0.0362 pCi/g 0.38 1
Bismuth 212 0.0687 U 0.02679 U 0.0980 0.175 pCi/g 0.20 1
Bismuth 214 0.159 0.1795 0.0365 0.0197 pCi/g 0.28 1
Lead 212 0.0998 0.08508 0.0300 0.0305 pCi/g 0.26 1
Lead 214 0.168 0.1697 0.0305 0.0234 pCi/g 0.03 1
Potassium 40 2.53 2.270 0.381 0.140 pCi/g 0.31 1
Protactinium
234m
0.532 U 0.7488 U 0.769 1.64 pCi/g 0.14 1
Protactinium 231 0.0877 U 0.08078 U 0.102 0.335 pCi/g 0.02 1
Radium 226 0.159 0.1795 0.0365 0.0197 pCi/g 0.28 1
Thorium 234 0.361 0.1348 U 0.112 0.331 pCi/g 0.62 1
Uranium 235 0.0187 U 0.04920 U 0.0439 0.0699 pCi/g 0.33 1
Thorium 232 0.117 0.06743 0.0338 0.0498 pCi/g 0.66 1
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QC Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Tl-208 10.990.018990.0440 0.0108 0.0149
RL MDC(2σ+/-)
DU DU
pCi/g
UnitResult Qual LimitResult
Sample Sample
Qual
Uncert.
RER
RER
Total
Other Detected
Radionuclides
Client Sample ID: Method BlankLab Sample ID: MB 160-233605/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233894 Prep Batch: 233605
Actinium 228
Analyte
U 101/24/16 21:0301/22/16 10:00pCi/g0.0923
MDCRL
0.04750.0475
(2σ+/-) (2σ+/-)
MB
0.002995
MB
Dil FacPrepared AnalyzedUnitResult Qualifier
Uncert.
Count
Uncert.
Total
101/24/16 21:0301/22/16 10:00pCi/g0.02360.01260.0126U0.0000561
2
Americium 241
101/24/16 21:0301/22/16 10:00pCi/g0.1420.06030.0603U-0.005028Bismuth 212
101/24/16 21:0301/22/16 10:00pCi/g0.03760.02080.0208U0.008034Bismuth 214
101/24/16 21:0301/22/16 10:00pCi/g0.02830.01810.0181U-0.001672Lead 212
101/24/16 21:0301/22/16 10:00pCi/g0.03110.01610.0161U0.001416Lead 214
101/24/16 21:0301/22/16 10:00pCi/g0.2743.453.45U-0.08620Potassium 40
101/24/16 21:0301/22/16 10:00pCi/g4.168.178.17U-1.227Protactinium 234m
101/24/16 21:0301/22/16 10:00pCi/g0.4350.2400.240U0.05978Protactinium 231
101/24/16 21:0301/22/16 10:00pCi/g0.03760.02080.0208U0.008034Radium 226
101/24/16 21:0301/22/16 10:00pCi/g0.3120.3610.361U-0.07351Thorium 234
101/24/16 21:0301/22/16 10:00pCi/g0.06000.01880.0188U0.006843Uranium 235
101/24/16 21:0301/22/16 10:00pCi/g0.09230.04750.0475U0.002995Thorium 232
Other Detected
Radionuclide
None
MB
(2σ+/-) (2σ+/-) MDCRL
pCi/g 01/22/16 10:00 01/24/16 21:03 1
MB
Dil FacPrepared AnalyzedUnitResult Qualifier
Uncert.
Count
Uncert.
Total
Radionuclides
Other Detected
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-233605/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233897 Prep Batch: 233605
Americium 241
Analyte
116-87100101.0101 10.5 0.493
RL MDC(2σ+/-)
LCS LCS
pCi/g
UnitResult Qual %RecAdded
Spike
Limits
%Rec.Uncert.
Total
Cesium 137 34.2 33.41 3.50 0.200 0.161 pCi/g 98 87 - 120
Cobalt 60 32.5 31.23 3.15 0.135 pCi/g 96 87 - 115
Client Sample ID: B02-01-21-P-E-S-00Lab Sample ID: 160-15789-21 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233900 Prep Batch: 233605
Actinium 228
Analyte
10.430.99331.15 0.160 0.101
RL MDC(2σ+/-)
DU DU
pCi/g
UnitResult Qual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Americium 241 -0.00452 U -0.00782
3
U 0.0568 0.0957 pCi/g 0.03 1
Bismuth 212 1.31 1.073 0.369 0.346 pCi/g 0.31 1
Bismuth 214 1.10 0.9712 0.148 0.0725 pCi/g 0.40 1
Lead 212 1.05 1.138 0.170 0.0680 pCi/g 0.25 1
Lead 214 1.11 1.058 0.149 0.0749 pCi/g 0.17 1
Potassium 40 17.9 18.42 2.27 0.434 pCi/g 0.12 1
Protactinium
234m
-1.61 U 3.044 U 2.29 7.62 pCi/g 0.32 1
Protactinium 231 0.579 U 0.2836 U 0.192 1.18 pCi/g 0.59 1
TestAmerica St. Louis
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QC Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: B02-01-21-P-E-S-00Lab Sample ID: 160-15789-21 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233900 Prep Batch: 233605
Radium 226
Analyte
10.400.97121.10 0.148 0.0725
RL MDC(2σ+/-)
DU DU
pCi/g
UnitResult Qual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
Thorium 234 1.31 1.079 0.689 0.908 pCi/g 0.18 1
Uranium 235 0.149 U 0.1499 U 0.127 0.169 pCi/g 0 1
Thorium 232 1.15 0.9933 0.160 0.101 pCi/g 0.43 1
Bi-210 10.451.1701.76 0.557 0.732
RL MDC(2σ+/-)
DU DU
pCi/g
UnitResult Qual LimitResult
Sample Sample
Qual
Uncert.
RER
RER
Total
Other Detected
Radionuclides
Eu-152 0.0375 U 0.1577 0.0903 0.103 pCi/g 0.71 1
Pb-210 1.76 1.170 0.557 0.732 pCi/g 0.45 1
Po-210 1.76 1.170 0.557 0.732 pCi/g 0.45
Ra-224 1.05 1.138 0.170 0.0680 pCi/g 0.25 1
Ra-228 1.15 0.9933 0.160 0.101 pCi/g 0.43 1
Sc-46 0.0673 0.07409 0.0230 0.0415 pCi/g 0.13 1
Sn-126 0.0458 U 0.4506 0.226 0.349 pCi/g 0.85 1
Ta-182 0.363 0.4135 0.128 0.149 pCi/g 0.18 1
Th-228 1.05 1.138 0.170 0.0680 pCi/g 0.25 1
Tl-208 0.428 0.3473 0.0660 0.0435 pCi/g 0.58 1
U-238 1.31 1.079 0.689 0.908 pCi/g 0.18 1
TestAmerica St. Louis
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QC Association SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Metals
Prep Batch: 233463
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid None160-15789-1 B02-01-01-P-S-S-00 Total/NA
Solid None160-15789-1 MS B02-01-01-P-S-S-00 Total/NA
Solid None160-15789-1 MSD B02-01-01-P-S-S-00 Total/NA
Solid None160-15789-2 B02-01-02-P-R-S-00 Total/NA
Solid None160-15789-3 B02-01-03-P-E-S-00 Total/NA
Solid None160-15789-4 B02-01-04-P-S-S-00 Total/NA
Solid None160-15789-5 B02-01-05-P-R-S-00 Total/NA
Solid None160-15789-6 B02-01-06-P-E-S-00 Total/NA
Solid None160-15789-7 B02-01-07-P-S-S-00 Total/NA
Solid None160-15789-8 B02-01-08-P-R-S-00 Total/NA
Solid None160-15789-9 B02-01-09-P-E-S-00 Total/NA
Solid None160-15789-10 B02-01-10-P-S-S-00 Total/NA
Solid None160-15789-11 B02-01-11-P-R-S-00 Total/NA
Solid None160-15789-12 B02-01-12-P-E-S-00 Total/NA
Solid None160-15789-13 B02-01-13-P-S-S-00 Total/NA
Solid NoneLCS 160-233463/2-A Lab Control Sample Total/NA
Solid NoneMB 160-233463/1-A Method Blank Total/NA
Prep Batch: 233467
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid None160-15789-14 B02-01-14-P-R-S-00 Total/NA
Solid None160-15789-14 MS B02-01-14-P-R-S-00 Total/NA
Solid None160-15789-14 MSD B02-01-14-P-R-S-00 Total/NA
Solid None160-15789-15 B02-01-15-P-E-S-00 Total/NA
Solid None160-15789-16 B02-01-16-P-S-S-00 Total/NA
Solid None160-15789-17 B02-01-17-P-R-S-00 Total/NA
Solid None160-15789-18 B02-01-18-P-E-S-00 Total/NA
Solid None160-15789-19 B02-01-19-P-S-S-00 Total/NA
Solid None160-15789-20 B02-01-20-P-R-S-00 Total/NA
Solid None160-15789-21 B02-01-21-P-E-S-00 Total/NA
Solid None160-15789-22 B02-01-22-P-S-S-00 Total/NA
Solid None160-15789-23 B02-01-23-P-R-S-00 Total/NA
Solid None160-15789-24 B02-01-24-P-E-S-00 Total/NA
Solid None160-15789-25 B02-01-02-P-R-Q-00 Total/NA
Solid None160-15789-26 B02-01-10-P-S-Q-00 Total/NA
Solid NoneLCS 160-233467/2-A Lab Control Sample Total/NA
Solid NoneMB 160-233467/1-A Method Blank Total/NA
Analysis Batch: 235007
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020A 233463160-15789-1 B02-01-01-P-S-S-00 Total/NA
Solid 6020A 233463160-15789-1 MS B02-01-01-P-S-S-00 Total/NA
Solid 6020A 233463160-15789-1 MSD B02-01-01-P-S-S-00 Total/NA
Solid 6020A 233463160-15789-2 B02-01-02-P-R-S-00 Total/NA
Solid 6020A 233463160-15789-3 B02-01-03-P-E-S-00 Total/NA
Solid 6020A 233463160-15789-4 B02-01-04-P-S-S-00 Total/NA
Solid 6020A 233463160-15789-5 B02-01-05-P-R-S-00 Total/NA
Solid 6020A 233463160-15789-6 B02-01-06-P-E-S-00 Total/NA
Solid 6020A 233463160-15789-7 B02-01-07-P-S-S-00 Total/NA
Solid 6020A 233463160-15789-8 B02-01-08-P-R-S-00 Total/NA
Solid 6020A 233463160-15789-9 B02-01-09-P-E-S-00 Total/NA
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QC Association SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Metals (Continued)
Analysis Batch: 235007 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020A 233463160-15789-10 B02-01-10-P-S-S-00 Total/NA
Solid 6020A 233463160-15789-11 B02-01-11-P-R-S-00 Total/NA
Solid 6020A 233463160-15789-12 B02-01-12-P-E-S-00 Total/NA
Solid 6020A 233463160-15789-13 B02-01-13-P-S-S-00 Total/NA
Solid 6020A 233467160-15789-14 B02-01-14-P-R-S-00 Total/NA
Solid 6020A 233467160-15789-14 MS B02-01-14-P-R-S-00 Total/NA
Solid 6020A 233467160-15789-14 MSD B02-01-14-P-R-S-00 Total/NA
Solid 6020A 233467160-15789-15 B02-01-15-P-E-S-00 Total/NA
Solid 6020A 233467160-15789-16 B02-01-16-P-S-S-00 Total/NA
Solid 6020A 233467160-15789-17 B02-01-17-P-R-S-00 Total/NA
Solid 6020A 233467160-15789-18 B02-01-18-P-E-S-00 Total/NA
Solid 6020A 233467160-15789-19 B02-01-19-P-S-S-00 Total/NA
Solid 6020A 233467160-15789-20 B02-01-20-P-R-S-00 Total/NA
Solid 6020A 233467160-15789-21 B02-01-21-P-E-S-00 Total/NA
Solid 6020A 233467160-15789-22 B02-01-22-P-S-S-00 Total/NA
Solid 6020A 233467160-15789-23 B02-01-23-P-R-S-00 Total/NA
Solid 6020A 233467160-15789-24 B02-01-24-P-E-S-00 Total/NA
Solid 6020A 233467160-15789-25 B02-01-02-P-R-Q-00 Total/NA
Solid 6020A 233467160-15789-26 B02-01-10-P-S-Q-00 Total/NA
Solid 6020A 233463LCS 160-233463/2-A Lab Control Sample Total/NA
Solid 6020A 233467LCS 160-233467/2-A Lab Control Sample Total/NA
Solid 6020A 233463MB 160-233463/1-A Method Blank Total/NA
Solid 6020A 233467MB 160-233467/1-A Method Blank Total/NA
General Chemistry
Analysis Batch: 233335
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture160-15789-1 B02-01-01-P-S-S-00 Total/NA
Solid Moisture160-15789-1 DU B02-01-01-P-S-S-00 Total/NA
Solid Moisture160-15789-2 B02-01-02-P-R-S-00 Total/NA
Solid Moisture160-15789-3 B02-01-03-P-E-S-00 Total/NA
Solid Moisture160-15789-4 B02-01-04-P-S-S-00 Total/NA
Solid Moisture160-15789-5 B02-01-05-P-R-S-00 Total/NA
Solid Moisture160-15789-6 B02-01-06-P-E-S-00 Total/NA
Solid Moisture160-15789-7 B02-01-07-P-S-S-00 Total/NA
Solid Moisture160-15789-8 B02-01-08-P-R-S-00 Total/NA
Solid Moisture160-15789-9 B02-01-09-P-E-S-00 Total/NA
Solid Moisture160-15789-10 B02-01-10-P-S-S-00 Total/NA
Solid Moisture160-15789-11 B02-01-11-P-R-S-00 Total/NA
Solid Moisture160-15789-12 B02-01-12-P-E-S-00 Total/NA
Solid Moisture160-15789-13 B02-01-13-P-S-S-00 Total/NA
Solid Moisture160-15789-14 B02-01-14-P-R-S-00 Total/NA
Solid Moisture160-15789-15 B02-01-15-P-E-S-00 Total/NA
Solid Moisture160-15789-16 B02-01-16-P-S-S-00 Total/NA
Solid Moisture160-15789-17 B02-01-17-P-R-S-00 Total/NA
Solid Moisture160-15789-18 B02-01-18-P-E-S-00 Total/NA
Solid Moisture160-15789-19 B02-01-19-P-S-S-00 Total/NA
Solid Moisture160-15789-20 B02-01-20-P-R-S-00 Total/NA
Solid Moisture160-15789-21 B02-01-21-P-E-S-00 Total/NA
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QC Association SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
General Chemistry (Continued)
Analysis Batch: 233335 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture160-15789-22 B02-01-22-P-S-S-00 Total/NA
Solid Moisture160-15789-23 B02-01-23-P-R-S-00 Total/NA
Solid Moisture160-15789-24 B02-01-24-P-E-S-00 Total/NA
Solid Moisture160-15789-25 B02-01-02-P-R-Q-00 Total/NA
Solid Moisture160-15789-26 B02-01-10-P-S-Q-00 Total/NA
Solid Moisture160-15789-26 DU B02-01-10-P-S-Q-00 Total/NA
Rad
Leach Batch: 233330
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Dry and Grind160-15789-1 B02-01-01-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-1 DU B02-01-01-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-2 B02-01-02-P-R-S-00 Total/NA
Solid Dry and Grind160-15789-3 B02-01-03-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-4 B02-01-04-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-5 B02-01-05-P-R-S-00 Total/NA
Solid Dry and Grind160-15789-6 B02-01-06-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-7 B02-01-07-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-8 B02-01-08-P-R-S-00 Total/NA
Solid Dry and Grind160-15789-9 B02-01-09-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-10 B02-01-10-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-11 B02-01-11-P-R-S-00 Total/NA
Solid Dry and Grind160-15789-12 B02-01-12-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-13 B02-01-13-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-14 B02-01-14-P-R-S-00 Total/NA
Solid Dry and Grind160-15789-15 B02-01-15-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-16 B02-01-16-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-17 B02-01-17-P-R-S-00 Total/NA
Solid Dry and Grind160-15789-18 B02-01-18-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-19 B02-01-19-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-20 B02-01-20-P-R-S-00 Total/NA
Solid Dry and Grind160-15789-21 B02-01-21-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-21 DU B02-01-21-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-22 B02-01-22-P-S-S-00 Total/NA
Solid Dry and Grind160-15789-23 B02-01-23-P-R-S-00 Total/NA
Solid Dry and Grind160-15789-24 B02-01-24-P-E-S-00 Total/NA
Solid Dry and Grind160-15789-25 B02-01-02-P-R-Q-00 Total/NA
Solid Dry and Grind160-15789-26 B02-01-10-P-S-Q-00 Total/NA
Prep Batch: 233463
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid None160-15789-1 B02-01-01-P-S-S-00 Total/NA
Solid None160-15789-1 MS B02-01-01-P-S-S-00 Total/NA
Solid None160-15789-1 MSD B02-01-01-P-S-S-00 Total/NA
Solid None160-15789-2 B02-01-02-P-R-S-00 Total/NA
Solid None160-15789-3 B02-01-03-P-E-S-00 Total/NA
Solid None160-15789-4 B02-01-04-P-S-S-00 Total/NA
Solid None160-15789-5 B02-01-05-P-R-S-00 Total/NA
Solid None160-15789-6 B02-01-06-P-E-S-00 Total/NA
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QC Association SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Rad (Continued)
Prep Batch: 233463 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid None160-15789-7 B02-01-07-P-S-S-00 Total/NA
Solid None160-15789-8 B02-01-08-P-R-S-00 Total/NA
Solid None160-15789-9 B02-01-09-P-E-S-00 Total/NA
Solid None160-15789-10 B02-01-10-P-S-S-00 Total/NA
Solid None160-15789-11 B02-01-11-P-R-S-00 Total/NA
Solid None160-15789-12 B02-01-12-P-E-S-00 Total/NA
Solid None160-15789-13 B02-01-13-P-S-S-00 Total/NA
Solid NoneLCS 160-233463/2-A Lab Control Sample Total/NA
Solid NoneMB 160-233463/1-A Method Blank Total/NA
Prep Batch: 233467
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid None160-15789-14 B02-01-14-P-R-S-00 Total/NA
Solid None160-15789-14 MS B02-01-14-P-R-S-00 Total/NA
Solid None160-15789-14 MSD B02-01-14-P-R-S-00 Total/NA
Solid None160-15789-15 B02-01-15-P-E-S-00 Total/NA
Solid None160-15789-16 B02-01-16-P-S-S-00 Total/NA
Solid None160-15789-17 B02-01-17-P-R-S-00 Total/NA
Solid None160-15789-18 B02-01-18-P-E-S-00 Total/NA
Solid None160-15789-19 B02-01-19-P-S-S-00 Total/NA
Solid None160-15789-20 B02-01-20-P-R-S-00 Total/NA
Solid None160-15789-21 B02-01-21-P-E-S-00 Total/NA
Solid None160-15789-22 B02-01-22-P-S-S-00 Total/NA
Solid None160-15789-23 B02-01-23-P-R-S-00 Total/NA
Solid None160-15789-24 B02-01-24-P-E-S-00 Total/NA
Solid None160-15789-25 B02-01-02-P-R-Q-00 Total/NA
Solid None160-15789-26 B02-01-10-P-S-Q-00 Total/NA
Solid NoneLCS 160-233467/2-A Lab Control Sample Total/NA
Solid NoneMB 160-233467/1-A Method Blank Total/NA
Prep Batch: 233602
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Fill_Geo-0 233330160-15789-1 B02-01-01-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-1 DU B02-01-01-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-2 B02-01-02-P-R-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-3 B02-01-03-P-E-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-4 B02-01-04-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-5 B02-01-05-P-R-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-6 B02-01-06-P-E-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-7 B02-01-07-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-8 B02-01-08-P-R-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-9 B02-01-09-P-E-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-10 B02-01-10-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-11 B02-01-11-P-R-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-12 B02-01-12-P-E-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-13 B02-01-13-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-14 B02-01-14-P-R-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-15 B02-01-15-P-E-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-16 B02-01-16-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-17 B02-01-17-P-R-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-18 B02-01-18-P-E-S-00 Total/NA
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QC Association SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Rad (Continued)
Prep Batch: 233602 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Fill_Geo-0 233330160-15789-19 B02-01-19-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-20 B02-01-20-P-R-S-00 Total/NA
Solid Fill_Geo-0LCS 160-233602/2-A Lab Control Sample Total/NA
Solid Fill_Geo-0MB 160-233602/1-A Method Blank Total/NA
Prep Batch: 233605
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Fill_Geo-0 233330160-15789-21 B02-01-21-P-E-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-21 DU B02-01-21-P-E-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-22 B02-01-22-P-S-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-23 B02-01-23-P-R-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-24 B02-01-24-P-E-S-00 Total/NA
Solid Fill_Geo-0 233330160-15789-25 B02-01-02-P-R-Q-00 Total/NA
Solid Fill_Geo-0 233330160-15789-26 B02-01-10-P-S-Q-00 Total/NA
Solid Fill_Geo-0LCS 160-233605/2-A Lab Control Sample Total/NA
Solid Fill_Geo-0MB 160-233605/1-A Method Blank Total/NA
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Tracer/Carrier SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP
Method: 6020A - Metals (ICP/MS), Tc-99 in ActivityPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-110)
Re
103160-15789-1
Percent Yield (Acceptance Limits)
B02-01-01-P-S-S-00
102160-15789-1 MS B02-01-01-P-S-S-00
103160-15789-1 MSD B02-01-01-P-S-S-00
100160-15789-2 B02-01-02-P-R-S-00
101160-15789-3 B02-01-03-P-E-S-00
105160-15789-4 B02-01-04-P-S-S-00
102160-15789-5 B02-01-05-P-R-S-00
101160-15789-6 B02-01-06-P-E-S-00
104160-15789-7 B02-01-07-P-S-S-00
100160-15789-8 B02-01-08-P-R-S-00
101160-15789-9 B02-01-09-P-E-S-00
104160-15789-10 B02-01-10-P-S-S-00
100160-15789-11 B02-01-11-P-R-S-00
99160-15789-12 B02-01-12-P-E-S-00
101160-15789-13 B02-01-13-P-S-S-00
100160-15789-14 B02-01-14-P-R-S-00
101160-15789-14 MS B02-01-14-P-R-S-00
99160-15789-14 MSD B02-01-14-P-R-S-00
101160-15789-15 B02-01-15-P-E-S-00
104160-15789-16 B02-01-16-P-S-S-00
103160-15789-17 B02-01-17-P-R-S-00
101160-15789-18 B02-01-18-P-E-S-00
103160-15789-19 B02-01-19-P-S-S-00
100160-15789-20 B02-01-20-P-R-S-00
100160-15789-21 B02-01-21-P-E-S-00
102160-15789-22 B02-01-22-P-S-S-00
100160-15789-23 B02-01-23-P-R-S-00
101160-15789-24 B02-01-24-P-E-S-00
101160-15789-25 B02-01-02-P-R-Q-00
100160-15789-26 B02-01-10-P-S-Q-00
105LCS 160-233463/2-A Lab Control Sample
104LCS 160-233467/2-A Lab Control Sample
104MB 160-233463/1-A Method Blank
104MB 160-233467/1-A Method Blank
Tracer/Carrier Legend
Re = Re
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