APPENDIX A – EXPENDITURES BY LICENSE · 2 ! Table&of&Contents& 1.#INTRODUCTION

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003D/05/0053

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Assessment'Report'on'Prospecting'and'Channel'Sampling'

Conducted'from'December'2013'to'December'2014'on'75'claims'of'the'Long'Point'Property'

Located'at:'St.'Lewis,'Labrador''

License'19576M,'17332M,'&'22073M'

'NTS:'03D/05'

Newfoundland'and'Labrador''

Submitted'by:'Suzanne'Butler'B.Sc.''

Date:'February'9,'2015'Work'year:'2014'Total'Claims:'75'

Program'Expenditures:'$52,262.28

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Table&of&Contents&

1.#INTRODUCTION....................................................................................................................................................3!1.1! Property#Location#and#Access ...............................................................................................................................3!1.2! Physiography ..............................................................................................................................................................4!1.3#Claim#Status.....................................................................................................................................................................4!

2.#PREVIOUS#WORK.................................................................................................................................................5!3.#GEOLOGY ................................................................................................................................................................6!3.1#Regional#Geology...........................................................................................................................................................6!3.2#Property#Geology#and#Mineralization....................................................................................................................7!

4.#2014#EXPLORATION#PROGRAM......................................................................................................................8!5.#CONCLUSION#AND#RECOMMENDATIONS.................................................................................................. 12!6.#REFERENCES....................................................................................................................................................... 13!#APPENDIX A - Expenditures By License APPENDIX B - Channel Samples with Descriptions and Assay Data APPENDIX C - Assay Certificates APPENDIX D - Company Personnel and Contractors

List of Figures Figure 1: Search Minerals Property, St. Lewis, Labrador. ............................................................................... 3!Figure 2: Claim Location, Licenses 19576M, 17332M, and 22073M. ............................................................ 5!Figure 3: Regional Geology Map of License 19576M, 17332M, and 22073M. .............................................. 7!Figure 4: Licenses 19576M, and 17332M Channel Locations ....................................................................... 11!Figure 5: License 22073M Channel Locations............................................................................................... 12! List&of&Tables&Table 1 – Claim Status...................................................................................................................................... 4!Table 2 – Licenses 19576M, 17332M, and 22073M Channel Sample Summary ............................................ 9!&# # #

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1.&INTRODUCTION&

Search Minerals Inc., by way of its wholly owned subsidiary Alterra Resources Inc., owns 75 claims on licenses 19576M, 17332M, and 22073M. These licenses are located near St. Lewis, approximately 30 kilometres southeast of Port Hope Simpson and were staked by Alterra Resources Inc. for Rare Earth Element (REE) exploration. This report documents the work conducted on licenses 19576M, 17332M, and 22073M in the 2014 exploration season.

1.1 Property&Location&and&Access&

Licenses 19576M, 17332M, and 22073M are located on a peninsula, between Mary’s Harbour and St. Lewis, and are accessible by boat and helicopter. Figure 1 shows the location of Search Minerals’ property.

Figure&1:&Search&Minerals&Property,&St.&Lewis,&Labrador.&

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1.2 Physiography&

Licenses 19576M, 17332M, and 22073M are located within the coastal barrens ecoregion and are comprised primarily of exposed headlands with topography ranging from 0-130 m above sea level. Vegetation is reduced by frequent forest fires and contains exposed bedrock with mosses and lichens, alder, dwarf birch, Labrador tea, and bogs. Bedrock exposure ranges from less than 5% in heavily wooded areas of the license to greater or equal to 75% on exposed headland areas.

1.3&Claim&Status&

Licenses 19576M, 17332M, and 22073M are comprised of 75 claims. A summary of the claim status is shown in Table 1, and claim locations in Figure 2. A list of company personnel and contractors is shown in Appendix D.

Expenditures by license are shown in Appendix A.

Table&1&–&Claim&Status&

Claim # Year # of Claims Issued Work Date Req’d

Expenditures Actual

Expenditures 19576M 3 33 12/12/2011 12/12/2014 $7,721.17 $18,687.60 17332M 4 12 22/02/2010 22/02/2015 $4,252.60 $14,925.43 22073M 5 30 22/12/2009 22/12/2014 $9,978.62 $18,649.26

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Figure&2:&Claim&Location,&Licenses&19576M,&17332M,&and&22073M.&

2.&PREVIOUS&WORK&

There has been no previous work by other companies on this license. Search Minerals Inc. has conducted exploration on license 22073M, and 17332M, since 2010, and on license 19576M since 2011.

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3.&GEOLOGY&

Labrador geology is comprised of five Precambrian provinces: the Archean Nain and Superior Provinces, the Paleoproterozoic Churchill and Makkovik Provinces, and the Mesoproterozoic to Neoproterozoic Grenville Province (Wardle et al., 1997 and references therein). The provinces are divided on the basis of structural trends, metamorphic criteria, and geochronological data (Gower et al., 1980 and references therein).

3.1&Regional&Geology&& The Grenville Province underlies a major portion of Labrador, stretching from the southern

coast and extending northwards past Groswater Bay, where the Grenville front truncates the other provinces and marks the northern limit of Grenvillian deformation (Gower, 1996; Greene, 1974). The Port Hope Simpson-Mary’s Harbour area occupies a geologically complex position within the Grenville Province, with associations linked to three lithotectonic blocks: from north to south, the Lake Melville, Mealy Mountains, and Pinware terranes (Gower, 1996, 2005). Differing geology, structural history, and levels of metamorphism distinguish the terranes. Each terrane is separated from another by a major fault zone (Gower et al., 1987, 1988).

The Lake Melville terrane is up to 60 km wide, but as one moves SE, towards the claim area, it

becomes much narrower and more strongly deformed (Gower, 1996). The most characteristic lithology in the Lake Melville terrane is K-feldspar megacrystic granitoids associated with metasedimentary gneisses; also present are granitoid gneisses and layered mafic to anorthositic rocks (Gower, 1996; Gower et al., 1987, 1988, 1994). The boundary between the Lake Melville terrane and the southern-lying Mealy Mountains terrane is quite sharp, and is termed the Fox Harbour fault zone (Gower, 2005). This fault zone is marked by abundant high-grade mylonites, changes in lineations north and south of the fault, and a contrast in garnet abundances of rocks of similar composition north and south of the fault (Gower, 1996, 2005).

Rock types within the Mealy Mountains terrane consist mainly of anorthosite, lecuogabbro,

leucotroctolite, pelitic gneisses, and granitoids (Gower, 1996; Gower et al., 1987, 1988). Further south in the Pinware terrane, there exist supracrustal quartzofeldspathic rocks, foliated to gneissic granitoids, layered mafic intrusions, and mafic dykes (Gower, 1996). The quartzofeldspathic rocks are interpreted to be of a felsic volcanic origin, based on an inhomogeneous texture that likely indicates pyroclastic origin (Gower, 1996). The boundary between the Mealy Mountains and southern-lying Pinware terrane is marked by gneissic rocks and mylonites of the Long Harbour fault zone, a structural feature that strikes primarily beneath the waters of St. Lewis Inlet (Gower, 1996, 2005). Farther west, near the area where the St. Lewis River empties into St. Lewis Inlet, several thrusts are interpreted to mark the surface along which the Mealy Mountains terrane overthrust the Pinware terrane in a southeasterly direction (Gower, 2005). Regional geology is shown in Figure 3.

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Figure&3:&Regional&Geology&Map&of&License&19576M,&17332M,&and&22073M.&

3.2&Property&Geology&and&Mineralization&

Due to the preliminary nature of exploration work on the property, license 19576M was not mapped in any detail. Most work involved prospecting, lithogeochemical sampling, and utilizing a spectrometer to highlight areas of anomalous radioactivity.

An east-west quartzite-sediment unit was observed in the northern portion of the peninsula,

and several felsic units to the south. Small Mafic units were observed throughout the area, and are conformable with the structure. Pegmatites are seen confirmable with the structure, and also cross-cutting, and are sometimes mineralized. ''

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4.&2014&EXPLORATION&PROGRAM&

&The first year exploration program on licenses 19576M, 17332M, and 22073M consisted of

prospecting and channel sampling. Prospecting on licenses 19576M, 17332M, and 22073M was conducted in the 2014 field

season. Numerous traverses were run on foot, using a boat to access different portions of the peninsula. Channel sampling focused on mineralized outcrops that were found using visual inspection as well as the use of hand-held spectrometers. A hand-held GPS unit was used for precise location control. Channel samples, 10cm deep and 8cm wide, were cut by gas-powered diamond saw from cleaned outcrops to provide samples for assay and logging/reference. Each channel was cut into two vertical sections, similar to drill core, with a 6 cm thick section (weathering removed) being sent out for assay to Activation Laboratories Ltd.. A 2 cm thick section was stored in channel boxes for reference and to provide due diligence/verification samples. The channels were cut perpendicular to strike, pieced together, logged and photographed to produce geological and geochemical sections. These channel samples, or horizontal drill holes, produce the same data as vertical diamond drill holes, except the data is from horizontal geological sections and the collected sample is 6 to 8 times bigger than NQ drill core. Additional 8 cm wide cuts from a channel interval make excellent preliminary metallurgical samples (1m of channel yields about 30kg of sample). Samples were then transported and delivered by Alterra Resources personnel to Activation Laboratories Ltd., located in Goose Bay, Labrador, where they were crushed to 80% - mesh and riffled to produce a representative sample. The samples were then pulverized to 95% - 200 mesh with the pulverizing mills being cleaned after every sample with cleaning sand. Next, samples were transported by means of courier to the ActLabs analytical facility in Ancaster, Ontario where they were analysed for REE, major elements, and an extensive suite of trace elements. A representative sample was treated by a lithium metaborate/tetraborate fusion and then analyzed by ICP and ICP/MS techniques. Mass balance is required as an additional quality control technique and elemental totals of the oxides should be between 98% and 101%. For QA/QC purposes Alterra requires duplicates every 25 samples and two Alterra reproducibility standards every 25 samples. ActLabs analyses duplicates and splits approximately every 15 samples and also analyses 29 measured standards for QA/QC.

License 19576M

Sixteen channels, totaling 15.48 m, and containing 52 samples (507210-507237, 507244-507260, and 507262-507268), were collected from license 19576M in the 2014 field season. Of these sixteen channels, several were mineralized. LPC-14-01 contained a 0.64 m (507211-507212) section that resulted in 2.6% Zr, and 2854 ppm Dy, LPC-14-07 contained a 0.48 m (507244) section that contained 7.9% Zr, and 5000 ppm Dy, and LPC-14-09 contained a 1.30 m section that contained 1890 ppm Zr, and 308 ppm Dy.

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License 17332M

Two channels, totaling 1.26 m, and containing seven samples (507238-507243, and 507261), were collected on license 17332M in the 2014 field season. Of these channels, one was mineralized. LPC-14-06 contained a 0.67 m (507238-507240) section that resulted in 1960 ppm Zr, and 75.1 ppm Dy. License 22073M

Seven channels, totaling 8.53 m, and containing 35 samples (507269-507303), were collected on license 22073M in the 2014 field season. Of these channels, two were mineralized. LPC-14-22A contained a 0.65 m (507286-507289) section that resulted in 1.2% Zr, and 295 ppm Dy, and LPC-14-22B contained a 0.43 m (507296-507298) section that resulted in 5785 ppm Zr, and 943 ppm Dy, and LPC-14-23 contained a 0.36 m (507302) section that resulted in 1.7 % Zr, and 991 ppm Dy.

Channel samples on licenses 19576M, 17332M are shown in Figure 4, and channel samples located on license 22073M is shown in Figure 5, with their associated channel numbers. A summary of the channels is shown in Table 2, and the assay data with descriptions for each channel sample are listed in Appendix B, and assay certificates in Appendix C.

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Table&2&–&Licenses&19576M,&17332M,&and&22073M&Channel&Sample&Summary&

Channel ID License Easting

(NAD 83) Northing (NAD 83)

AZ (°)

Length (m) Date Cut Assay # Work Order

LPC-14-01 19576M 579563 5800211 194 1.13 29-Sep-14 507210-507213 A14-08533 LPC-14-02 19576M 582584 5799689 202 2.8 30-Sep-14 507214-507222 A14-08532 LPC-14-03 19576M 582578 5799704 202 0.68 30-Sep-14 507223-507226 A14-08528 LPC-14-04 19576M 582783 5799684 180 0.92 30-Sep-14 507227-507230 A14-08527 LPC-14-05 19576M 582359 5799682 190 1.8 01-Oct-14 507231-507237 A14-08525 LPC-14-06 17332M 582324 5799722 150 0.97 01-Oct-14 507238-507243 A14-08524 LPC-14-07 19576M 582709 5799660 160 0.48 01-Oct-14 507244 A14-08523 LPC-14-08 19576M 582709 5799663 160 0.4 01-Oct-14 507245 A14-08522 LPC-14-09 19576M 579808 5800771 200 1.76 03-Oct-14 507246-507250 A14-08521 LPC-14-10 19576M 579792 5800741 204 1.9 03-Oct-14 507251-507255 A14-08519 LPC-14-11 19576M 577184 5800953 190 0.36 05-Oct-14 507256 A14-08518 LPC-14-12 19576M 576814 5800848 202 0.3 05-Oct-14 507257 A14-08512 LPC-14-13 19576M 576812 5800845 202 0.32 05-Oct-14 507258 A14-08511 LPC-14-14 19576M 576813 5800846 202 0.45 05-Oct-14 507259-507260 A14-08510 LPC-14-15 17332M 580757 5800533 200 0.29 05-Oct-14 507261 A14-08509 LPC-14-16 19576M 579780 5801035 200 0.3 05-Oct-14 507262 A14-08508 LPC-14-17 19576M 579297 5800860 136 1.88 03-Oct-14 507263-507268 A14-08507 LPC-14-18 22073M 575767 5801447 202 1.92 11-Oct-14 507269-507275 A14-08506 LPC-14-19 22073M 575831 5801508 202 0.34 11-Oct-14 507276-507278 A14-08505 LPC-14-20 22073M 575831 5801504 200 0.35 11-Oct-14 507279 A14-08503 LPC-14-21 22073M 572850 5802859 198 1.12 24-Oct-14 507281-507283 A14-08566 LPC-14-22A 22073M 572894 5802807 210 2.83 24-Oct-14 507284-507295 A14-08568 LPC-14-22B 22073M 572894 5802807 210 0.43 24-Oct-14 507296-507298 A14-08565 LPC-14-23 22073M 572070 5802942 205 1.54 24-Oct-14 507299-507303 A14-08564

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Figure&4:&Licenses&19576M,&and&17332M&Channel&Locations&

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Figure&5:&License&22073M&Channel&Locations&

5.&CONCLUSION&AND&RECOMMENDATIONS&

Exploration on licenses 19576M, 17332M, and 22073M was successful in finding potential REE mineralization. Further work should be completed on the western portion of 22073M, and if possible, these three licenses should be merged into one license.

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6.&REFERENCES& !Beaven, A.P. 1958: The Labrador Uranium Area. Proceedings of the Geological Association of Canada, December, 1958, Vol. 10, pp.137-145. Christie, A.M. 1951: Geology of the southern coast of Labrador, from Forteau Bay to Cape Porcupine, Newfoundland. Geological Survey of Canada, Paper, No. 51‐13. Daly, R.A. 1902: The geology of the northeast coast of Labrador. Museum of Comparative Zoology, Bulletin, Vol. 38, No. 5, pages 205‐270. Eade, K.E. 1962: Geology, Battle Harbour ‐ Cartwright, Coast Of Labrador, Newfoundland. Geological Survey of Canada, Preliminary Map, No. 22‐1962. Gower, C.F., Ryan, B.A., Bailey, D.G., and Thomas, A. 1980: The position of the Grenville Front in eastern and central Labrador. Canadian Journal of Earth Sciences, 17: 784-788. Gower, C.F., Neuland, S., Newman, M., Smyth, J. 1987: Geology of the Port Hop Simpson map region, Grenville province, eastern Labrador, Current Research (1987) Newfoundland Department of Mines and Energy, Mineral Development Division, Report 87:1, p.183-199. Gower, C.F., Van Nostrand, T., Smyth, J. 1988: Geology of the St. Lewis River map region, Grenville province, eastern Labrador, Current Research (1988) Newfoundland Department of Mines, Mineral Development Division, Report 88:1, p. 59-73. Gower, C.F., van Nostrand, T., and Evans-Lamswood, D. 1994. Geology of the Pinware River Region, Southeast Labrador. Current Research, Newfoundland Department of Mines and Energy, Geological Survey Branch, Report 94-1, pages 347-369. Gower, C.F. 1996. The evolution of the Grenville Province in eastern Labrador, Canada. Geological Society, London, Special Publications. V. 112, p197-218. Gower, C.F. 2005. Kinematic evidence for terrane displacements in the Grenville Province in eastern Labrador. Current Research, Newfoundland and Labrador Department of Natural Resources, Geological Survey, Report 05-1, pages 73-92. Gower, C.F., Neuland, S., Newman, M., Smyth, J. 1987: Geology of the Port Hope Simpson map region, Grenville province, eastern Labrador, Current Research (1987) Newfoundland Department of Mines and Energy, Mineral Development Division, Report 87‐1, p. 183‐199. Gower, C.F., Van Nostrand, T., Smyth, J. 1988: Geology of the St. Lewis River map region, Grenville province, eastern Labrador, Current Research (1988) Newfoundland Department of Mines, Mineral

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Development Division, Report 88‐1, p. 59‐73. Greene, B.A., 1974. An Outline of the Geology of Labrador. Journal of the Geological Association of Canada, Volume 1, Number 3. Lieber, O.M. 1860: Notes on the geology of the cost of Labrador. Report of the United States Coast Survey for 1860, pages 402‐408. Tucker, R.D., and Gower, C.F. 1994: A U-Pb geochronological framework for the Pinware Terre, Grenville Province, Southeast Labrador. The Journal of Geology, v:102, p.67-78. Van Nostrand, T. and Gower, C.F., 2010: Geology of the Alexis River area (NTS sheets 13A/11, 12, 13 and 14), southeastern Labrador. Geological Survey, Mines Branch, Department of Natural Resources, Government of Newfoundland and Labrador, Map 2010-19, Open File 013A/0081. Wardle, R.J., Gower, C.F., Ryan, B., James, D., Nolan, L., Nunn, G.A.G., and Kerr, A. 1997: A new geological map of Labrador. Report of Activities, Newfoundland Geological Survey, p.61-62. ''

APPENDIX A – EXPENDITURES BY LICENSE

Alterra Resources Inc.Assessment reportWork Year: 2014License(s) 019576M, 022073M, & 017332M

Exploration Costs 019576M 022073M 017332MSalaries and wages $6,139.40 $7,200.81 $6,341.52EI Expense $67.77 $98.12 $65.07CPP Expense $120.14 $173.06 $115.33Assay $4,042.87 $2,764.85 $576.81Camp costs $3,905.24 $3,905.24 $3,905.24Field supplies $110.56 $110.56 $110.56Field travel $250.77 $250.77 $250.77NCC Payment $1,413.33 $1,413.33 $1,413.33Boat Rental $200.00 $300.00 $200.00Total $16,250.09 $16,216.74 $12,978.63

Total $16,250.09 $16,216.74 $12,978.6315% Admin fee $2,437.51 $2,432.51 $1,946.80Grand Total $18,687.60 $18,649.26 $14,925.43

APPENDIX B – CHANNEL SAMPLE DESCRIPTIONS AND ASSAY DATA

Channel_ID Lic_Num Easting Northing Chem_Num From_m To_m Length P ROCK TYPE Rock Type 2 RT 2 Perc Grain Size Fabric Mt Perc Pyx Perc Bt Perc Amph Perc L Perc Ti PercLPC-14-01 19576M 579563 5800211 507210 0 0.13 0.13 felsic f fol <1 — 5-7 — — <1LPC-14-01 19576M 579563 5800211 507211 0.13 0.22 0.09 pegmatite f-m peg 1 — 1 2-5 — 1LPC-14-01 19576M 579563 5800211 507212 0.22 0.77 0.55 pegmatite c peg 1-3 5-10 — 5-10 — 3-7LPC-14-01 19576M 579563 5800211 507213 0.77 1.13 0.36 pegmatite f-vc peg — — <1 — — —LPC-14-02 19576M 582584 5799689 507214 0 0.6 0.6 sediment f-m fol — — 5-10 60-70 — —LPC-14-02 19576M 582584 5799689 507215 0.6 0.72 0.12 sediment f-m fol — — 10 20 — —LPC-14-02 19576M 582584 5799689 507216 0.72 0.92 0.2 pegmatite f-c peg — — — — — 1-2LPC-14-02 19576M 582584 5799689 507217 0.92 1.02 0.1 sediment vf fol — — 3-5 — — —LPC-14-02 19576M 582584 5799689 507218 1.02 1.07 0.05 pegmatite f-m vein — — 5 10-15 — 1-2LPC-14-02 19576M 582584 5799689 507219 1.07 1.34 0.27 pegmatite mafic 5 f-vc peg — — — — — <1LPC-14-02 19576M 582584 5799689 507220 1.34 1.76 0.42 sediment vf-f peg — — 1-2 30 — 1-3LPC-14-02 19576M 582584 5799689 507221 1.76 2.16 0.4 sediment vf-f peg/fol — — 1-3 20 — 1-3LPC-14-02 19576M 582584 5799689 507222 2.16 2.8 0.64 sediment vf-f peg/fol — — 1-3 20 — 1-3LPC-14-03 19576M 582578 5799704 507223 0 0.2 0.2 sediment f fol — — <1 — — —LPC-14-03 19576M 582578 5799704 507224 0.2 0.36 0.16 pegmatite m prg — — <1 — — —LPC-14-03 19576M 582578 5799704 507225 0.36 0.45 0.09 pegmatite m peg — — 1 — tr 1LPC-14-03 19576M 582578 5799704 507226 0.45 0.68 0.23 sediment f fol — — <1 — — —LPC-14-04 19576M 582783 5799684 507227 0 0.06 0.06 mafic f — — 20 15 — 1-3LPC-14-04 19576M 582783 5799684 507228 0.06 0.34 0.28 pegmatite f-m peg 1? — <1 10 — 1-2LPC-14-04 19576M 582783 5799684 507229 0.34 0.47 0.13 pegmatite pegmatite 20 f peg 1-3 — 15 5 — 3-5LPC-14-04 19576M 582783 5799684 507230 0.47 0.92 0.45 sediment pegmatite 15 vf fol tr — 1 1-2 — 1-2LPC-14-05 19576M 582359 5799682 507231 0 0.13 0.13 sediment vf-f fol — — <1 <1 — —LPC-14-05 19576M 582359 5799682 507232 0.13 0.34 0.21 pegmatite f-c peg tr — — — ? 1-2LPC-14-05 19576M 582359 5799682 507233 0.34 0.67 0.33 pegmatite f-c peg — — — — — <1LPC-14-05 19576M 582359 5799682 507234 0.67 0.92 0.25 pegmatite f-m peg tr — — — — <1LPC-14-05 19576M 582359 5799682 507235 0.92 1.24 0.32 pegmatite f-m peg tr — — — — <1LPC-14-05 19576M 582359 5799682 507236 1.24 1.44 0.2 pegmatite f-c peg — — — — — <1LPC-14-05 19576M 582359 5799682 507237 1.44 1.8 0.36 sediment vf-f fol — — <1 — — —LPC-14-06 17332M 582324 5799722 507238 0 0.25 0.25 pegmatite m peg — — — — — <1LPC-14-06 17332M 582324 5799722 507239 0.25 0.51 0.26 pegmatite m peg — — — — — <1LPC-14-06 17332M 582324 5799722 507240 0.51 0.67 0.16 pegmatite m peg — — — — — <1LPC-14-06 17332M 582324 5799722 507241 0.67 0.76 0.09 mafic f — — 20 20 — —LPC-14-06 17332M 582324 5799722 507242 0.76 0.85 0.09 pegmatite m peg — — — — — <1LPC-14-06 17332M 582324 5799722 507243 0.85 0.97 0.12 mafic f — — 20 20 — —LPC-14-07 19576M 582709 5799660 507244 0 0.48 0.48 pegmatite 10 — — — — 10LPC-14-08 19576M 582709 5799663 507245 0 0.4 0.4 felsic tr — <1 — — —LPC-14-09 19576M 579808 5800771 507246 0 0.46 0.46 sediment vf fol — — <1 — — —LPC-14-09 19576M 579808 5800771 507247 0.46 0.79 0.33 pegmatite peg — — — — — 1?LPC-14-09 19576M 579808 5800771 507248 0.79 1.16 0.37 pegmatite peg — — — — — 1-2LPC-14-09 19576M 579808 5800771 507249 1.16 1.56 0.4 pegmatite sediment 30 vf-m peg — — — — — 1-2?LPC-14-09 19576M 579808 5800771 507250 1.56 1.76 0.2 sediment vf fol — — <1 — — —LPC-14-10 19576M 579792 5800741 507251 0 0.28 0.28 sediment vf fol — — <1 — — —LPC-14-10 19576M 579792 5800741 507252 0.28 0.76 0.48 pegmatite m-c peg 1-2LPC-14-10 19576M 579792 5800741 507253 0.76 1.05 0.29 pegmatite m-c peg 1-2LPC-14-10 19576M 579792 5800741 507254 1.05 1.58 0.53 pegmatite m-c peg 1-2LPC-14-10 19576M 579792 5800741 507255 1.58 1.9 0.32 sediment vf fol — — <1 — — —LPC-14-11 19576M 577184 5800953 507256 0 0.36 0.36 sediment f-m folLPC-14-12 19576M 576814 5800848 507257 0 0.3 0.3 mafic f — — 20 30 — —LPC-14-13 19576M 576812 5800845 507258 0 0.32 0.32 felsic f fol 1-2 — 1 — —LPC-14-14 19576M 576813 5800846 507259 0 0.27 0.27 felsic vf fol 1 — 1 — — —LPC-14-14 19576M 576813 5800846 507260 0.27 0.45 0.18 felsic f fol 1-2 — 1-2 — — —LPC-14-15 17332M 580757 5800533 507261 0 0.29 0.29 felsic vf-f fol tr — 1 — — 1-2LPC-14-16 19576M 579780 5801035 507262 0 0.3 0.3 mafic f — — 15 35 — —LPC-14-17 19576M 579297 5800860 507263 0 0.21 0.21 sediment vf fol — — <1 — — —LPC-14-17 19576M 579297 5800860 507264 0.21 0.44 0.23 pegmatite peg — — — — — —LPC-14-17 19576M 579297 5800860 507265 0.44 0.83 0.39 pegmatite peg — — — — — —LPC-14-17 19576M 579297 5800860 507266 0.83 1.11 0.28 pegmatite peg — — — — — —LPC-14-17 19576M 579297 5800860 507267 1.11 1.58 0.47 pegmatite peg — — — — — —LPC-14-17 19576M 579297 5800860 507268 1.58 1.88 0.3 sediment vf fol — — <1 — — —LPC-14-18 22073M 575767 5801447 507269 0 0.38 0.38 felsic vf fol <1 — 1-2 — — —LPC-14-18 22073M 575767 5801447 507270 0.38 0.71 0.33 felsic vf fol <1 — 1-2 — — —LPC-14-18 22073M 575767 5801447 507271 0.71 0.96 0.25 felsic vf fol <1 — 1-2 — — —LPC-14-18 22073M 575767 5801447 507272 0.96 1.22 0.26 felsic vf fol <1 — 1-2 — — —LPC-14-18 22073M 575767 5801447 507273 1.22 1.49 0.27 felsic vf fol <1 — 1 — — —LPC-14-18 22073M 575767 5801447 507274 1.49 1.65 0.16 pegmatite f-vc peg <1 — — — — —

Channel_ID Lic_Num Easting Northing Chem_Num From_m To_m LengthLPC-14-01 19576M 579563 5800211 507210 0 0.13 0.13LPC-14-01 19576M 579563 5800211 507211 0.13 0.22 0.09LPC-14-01 19576M 579563 5800211 507212 0.22 0.77 0.55LPC-14-01 19576M 579563 5800211 507213 0.77 1.13 0.36LPC-14-02 19576M 582584 5799689 507214 0 0.6 0.6LPC-14-02 19576M 582584 5799689 507215 0.6 0.72 0.12LPC-14-02 19576M 582584 5799689 507216 0.72 0.92 0.2LPC-14-02 19576M 582584 5799689 507217 0.92 1.02 0.1LPC-14-02 19576M 582584 5799689 507218 1.02 1.07 0.05LPC-14-02 19576M 582584 5799689 507219 1.07 1.34 0.27LPC-14-02 19576M 582584 5799689 507220 1.34 1.76 0.42LPC-14-02 19576M 582584 5799689 507221 1.76 2.16 0.4LPC-14-02 19576M 582584 5799689 507222 2.16 2.8 0.64LPC-14-03 19576M 582578 5799704 507223 0 0.2 0.2LPC-14-03 19576M 582578 5799704 507224 0.2 0.36 0.16LPC-14-03 19576M 582578 5799704 507225 0.36 0.45 0.09LPC-14-03 19576M 582578 5799704 507226 0.45 0.68 0.23LPC-14-04 19576M 582783 5799684 507227 0 0.06 0.06LPC-14-04 19576M 582783 5799684 507228 0.06 0.34 0.28LPC-14-04 19576M 582783 5799684 507229 0.34 0.47 0.13LPC-14-04 19576M 582783 5799684 507230 0.47 0.92 0.45LPC-14-05 19576M 582359 5799682 507231 0 0.13 0.13LPC-14-05 19576M 582359 5799682 507232 0.13 0.34 0.21LPC-14-05 19576M 582359 5799682 507233 0.34 0.67 0.33LPC-14-05 19576M 582359 5799682 507234 0.67 0.92 0.25LPC-14-05 19576M 582359 5799682 507235 0.92 1.24 0.32LPC-14-05 19576M 582359 5799682 507236 1.24 1.44 0.2LPC-14-05 19576M 582359 5799682 507237 1.44 1.8 0.36LPC-14-06 17332M 582324 5799722 507238 0 0.25 0.25LPC-14-06 17332M 582324 5799722 507239 0.25 0.51 0.26LPC-14-06 17332M 582324 5799722 507240 0.51 0.67 0.16LPC-14-06 17332M 582324 5799722 507241 0.67 0.76 0.09LPC-14-06 17332M 582324 5799722 507242 0.76 0.85 0.09LPC-14-06 17332M 582324 5799722 507243 0.85 0.97 0.12LPC-14-07 19576M 582709 5799660 507244 0 0.48 0.48LPC-14-08 19576M 582709 5799663 507245 0 0.4 0.4LPC-14-09 19576M 579808 5800771 507246 0 0.46 0.46LPC-14-09 19576M 579808 5800771 507247 0.46 0.79 0.33LPC-14-09 19576M 579808 5800771 507248 0.79 1.16 0.37LPC-14-09 19576M 579808 5800771 507249 1.16 1.56 0.4LPC-14-09 19576M 579808 5800771 507250 1.56 1.76 0.2LPC-14-10 19576M 579792 5800741 507251 0 0.28 0.28LPC-14-10 19576M 579792 5800741 507252 0.28 0.76 0.48LPC-14-10 19576M 579792 5800741 507253 0.76 1.05 0.29LPC-14-10 19576M 579792 5800741 507254 1.05 1.58 0.53LPC-14-10 19576M 579792 5800741 507255 1.58 1.9 0.32LPC-14-11 19576M 577184 5800953 507256 0 0.36 0.36LPC-14-12 19576M 576814 5800848 507257 0 0.3 0.3LPC-14-13 19576M 576812 5800845 507258 0 0.32 0.32LPC-14-14 19576M 576813 5800846 507259 0 0.27 0.27LPC-14-14 19576M 576813 5800846 507260 0.27 0.45 0.18LPC-14-15 17332M 580757 5800533 507261 0 0.29 0.29LPC-14-16 19576M 579780 5801035 507262 0 0.3 0.3LPC-14-17 19576M 579297 5800860 507263 0 0.21 0.21LPC-14-17 19576M 579297 5800860 507264 0.21 0.44 0.23LPC-14-17 19576M 579297 5800860 507265 0.44 0.83 0.39LPC-14-17 19576M 579297 5800860 507266 0.83 1.11 0.28LPC-14-17 19576M 579297 5800860 507267 1.11 1.58 0.47LPC-14-17 19576M 579297 5800860 507268 1.58 1.88 0.3LPC-14-18 22073M 575767 5801447 507269 0 0.38 0.38LPC-14-18 22073M 575767 5801447 507270 0.38 0.71 0.33LPC-14-18 22073M 575767 5801447 507271 0.71 0.96 0.25LPC-14-18 22073M 575767 5801447 507272 0.96 1.22 0.26LPC-14-18 22073M 575767 5801447 507273 1.22 1.49 0.27LPC-14-18 22073M 575767 5801447 507274 1.49 1.65 0.16

Comments WO SiO2 (%) Al2O3 (%) Fe2O3_T (%) MnO (%) MgO (%) CaO (%) Na2O (%)A14-08533 65.51 16.98 3.93 0.089 0.76 1.98 4.43

Minor mineralization. Very rubbly A14-08533 55.19 11.79 14.71 0.108 0.95 1.73 2.83Mineralized section. Hematite → 7-10%. A14-08533 48.12 8.93 14.89 0.2 1.19 2.69 1.41

Some hematite. A14-08533 66.82 16.11 2.82 0.059 1.2 0.49 6Epidote rocks (15-20% epi ?). A14-08532 73.46 13.86 1 0.017 0.13 0.44 4.29

10% Epi. More felsic. A14-08532 41.98 13.23 16.26 0.228 7.78 9.98 2.08Mineralized section. Yellow min assoc. w/REM 5-7% (ilmenite) metallic non-mag. A14-08532 45.26 14.04 14.24 0.225 5.32 10.03 3.23

Epi - 10%. Some REM from previous samp. A14-08532 66.36 13.52 4.01 0.122 0.78 1.95 5.94Epi 15-20%. Small "vein". A14-08532 64.35 9.35 4.22 0.217 5.97 6.8 1.62

Some REM (<1%). Small portion of next rock within. Very rubbly, sampled together. A14-08532 65.59 13.09 4.41 0.044 2.33 2.23 2.17Epi - 1-2%. A14-08532 58.49 10.5 4.39 0.081 7.07 9.34 2.62Epi - 3-10%. A14-08532 59.68 10.76 4.68 0.079 6.11 9.6 2.56

Same as above. A14-08532 64.82 10.23 3.87 0.07 4.37 7.58 2tr REM? A14-08528 75.45 10.19 4.02 0.052 1.68 0.97 3.1

REM: 1%? Tr? A14-08528 82.67 7.44 2.31 0.049 0.93 1.12 2.48REM: 20-30% Poss allanite (fractures around grains). A14-08528 71.56 6.73 9.11 0.184 0.44 1.49 1.8

Same as first sample. A14-08528 78.3 8.51 3.64 0.053 0.88 1.29 3.2Rubble. A14-08527 48.73 12.08 16.87 0.245 6.93 4.37 3.63

Illmanite REM: 15-20%. Mt present. Hematized. A14-08527 59.88 5.93 24.96 0.275 1.23 1.63 2.79Epi - 1%. A14-08527 52.64 13.43 13.32 0.262 4.64 3.75 5.35

Epi - 1-2%. Qtz vein (1cm). A14-08527 77.2 8.09 2.39 0.072 1.44 2.91 2.63Hematized bands. A14-08525 83.18 6.58 1.64 0.03 0.45 1.1 1.26

REM: 15% (Illmanite?). Hematized A14-08525 77.04 5.74 9.63 0.107 0.22 0.66 2.46REM: <1 % (Illmanite?). Hematized. A14-08525 82.21 9.88 1.17 0.012 0.03 0.11 5.47

REM: 10% (Illmanite?). Hematized. Very qtz rich. A14-08525 90.21 3.83 3.39 0.043 0.1 0.25 1.91REM: <1% (Illmanite?). Hematized. A14-08525 80.59 10.34 1.77 0.019 0.09 0.35 3.38REM: 3% ? (Illmanite?). Hematized. A14-08525 78 10.77 2.44 0.035 0.05 0.26 4.42

Same as first sample. A14-08525 84.68 5.01 1.48 0.028 0.59 1.68 0.84REM: 1-3 (Illmanite). Hematized. High CPS A14-08524 74.11 14.52 1.57 0.014 0.11 1.19 6.98

REM: 1-3 A14-08524 70.91 14.86 1.97 0.013 0.07 0.62 7.28REM: 1-3 A14-08524 75.18 13.94 2.4 0.017 0.13 1.07 6.58

A14-08524 54.07 14.32 10.13 0.208 5.59 6.85 4.43REM <1% A14-08524 67.37 16.88 2.13 0.035 0.93 2.07 6.87

Same as mafic 2 samples ago. A14-08524 48.64 14.81 13.89 0.184 5.58 6.92 4.54Very mineralized. In middle of woods - 20000+CPS. REM: 40% yellow/beige minerals. Weathered & hematized. A14-08523 40.65 4.05 7.85 0.206 1.38 7.03 0.28

300-400 cps peralkaline felsic volcs. Euhedral Mt. A14-08522 72.99 13.1 1.62 0.025 0.26 0.46 3.63A14-08521 81.39 8.07 2.3 0.013 0.79 0.43 2.3

Minor REM (illmanite?) - 1%? A14-08521 75.58 12.98 1.22 0.013 0.08 0.18 4.42REM - 3%? Illmanite bands. Visable yellow mins. A14-08521 73.92 11.77 4.13 0.035 0.06 0.31 5.03

Very piecy, sampled in bulk (all of "F") - going down slope. A14-08521 76.31 8.98 4.21 0.063 0.4 0.57 3.23Same as first sample. A14-08521 78.28 9.29 3.06 0.026 0.61 0.52 3.25Same as last sample. A14-08519 85.53 7.44 1.88 0.015 0.61 0.4 1.6

REM - 2-3% (illmanite?) hematized. A14-08519 73.67 13.73 1.55 0.014 0.05 0.23 4.09REM - 2-3% hematized A14-08519 73.22 14.02 1.12 0.013 0.04 0.21 4.74REM - 2-3% hematized A14-08519 72.74 13.29 1.64 0.01 0.06 0.2 3.14Same as first sample. A14-08519 80.97 8.24 2.59 0.011 0.96 0.79 1.87

Calc-silicate. Layered. Porus. Cut sample A14-08518 54.23 11.42 5.08 0.112 3.86 14.47 2.53Cut sample. Mafics from s-shore. Homogeneous. A14-08512 51.39 14.02 13.79 0.204 4.05 7.45 3.27

Euhedral Mt. cut sample. A14-08511 70.01 14.34 2.67 0.068 0.37 1.15 3.55Euhedral Mt.: two diff felsics (contact). A14-08510 66.95 16.45 2.55 0.094 0.52 1.45 4.24Euhedral Mt.: two diff felsics (contact). A14-08510 66.27 16.09 2.74 0.076 0.59 1.52 4.29

Euhedral Mt. Cut sample. A14-08509 72.91 13.37 1.78 0.045 0.27 0.7 3.2Cut sample. Homogenous. Mafics from N-shore. A14-08508 52.62 14.69 13.89 0.228 4.38 6.81 3.22

A14-08507 80.49 8.15 2.6 0.042 1.1 0.64 2.3Cross-cutting peg (within atzite). Minor REM. Hematized. A14-08507 74.75 13.85 0.85 0.007 0.09 0.33 6.81

REM's strung out (Illmanite? 2-3%) A14-08507 63.01 17.48 6.96 0.03 0.2 0.75 7.77REM's A14-08507 63.93 17.78 6.47 0.105 0.2 0.53 7.19

Minor REM. A14-08507 66.65 18.53 1.04 0.011 0.09 0.17 4.37Same as first sample. A14-08507 78.22 10.44 3.29 0.034 1.07 0.32 2.21

Hematized. Bt-rich band at end (1cm). Euhedral Mt. A14-08506 71.6 13.23 2.06 0.036 0.64 0.83 4Hematized. Euhedral Mt. A14-08506 72.57 12.98 1.79 0.029 0.36 0.59 3.56Hematized. Euhedral Mt. A14-08506 73.67 12.48 2.14 0.032 0.29 0.55 3.42Hematized. Euhedral Mt. A14-08506 72.92 12.97 1.68 0.035 0.26 0.74 3.62Hematized. Euhedral Mt. A14-08506 72.07 13.2 1.61 0.033 0.27 0.69 3.65Hematized. Euhedral Mt. A14-08506 85.22 7.21 0.96 0.013 0.08 0.27 1.86


K2O (%) TiO2 (%) P2O5 (%) LOI (%) Total (%) Sc (ppm) Be (ppm) V (ppm) Cr (ppm) Co (ppm) Ni (ppm) Cu (ppm) Zn (ppm) Ga (ppm) Ge (ppm) As (ppm) Rb (ppm) Sr (ppm) Y (ppm) Zr (ppm)5.63 0.661 0.16 0.66 100.8 8 15 48 < 20 3 < 20 < 10 80 18 1 < 5 160 430 174 7794.8 1.584 0.14 1.36 95.19 6 25 143 < 20 6 < 20 < 10 150 31 5 < 5 139 231 4559 227403.68 2.042 0.09 1.89 85.1 9 24 172 < 20 7 < 20 < 10 240 50 14 21 131 317 16130 303704.17 0.346 0.08 0.99 99.09 5 13 66 < 20 3 < 20 < 10 50 16 1 < 5 139 167 151 3074.93 0.045 0.01 0.45 98.62 2 13 17 < 20 < 1 < 20 < 10 < 30 28 2 5 199 76 46 732.26 3.085 0.51 2.47 99.88 27 5 284 70 58 70 < 10 230 23 2 < 5 81 187 42 2571.83 3.059 0.49 1.75 99.47 26 14 281 70 48 70 < 10 200 25 2 < 5 146 211 129 3452.1 0.976 0.07 0.9 96.72 6 33 43 < 20 3 < 20 10 80 51 5 12 71 143 3706 76554.45 0.559 0.09 1.48 99.11 9 92 46 50 10 < 20 < 10 270 23 2 10 250 134 268 2267.75 0.418 0.04 0.76 98.84 7 23 31 30 5 < 20 < 10 50 33 2 8 355 149 103 1854.62 0.653 0.13 1 98.89 11 25 58 60 13 30 < 10 70 16 1 19 181 191 36 2954.84 0.642 0.12 0.67 99.73 11 10 84 50 12 30 < 10 50 16 2 11 157 222 33 2494.82 0.634 0.13 1.29 99.81 9 5 123 60 9 20 < 10 40 13 1 16 131 209 32 2452.73 0.807 0.12 1.01 100.1 8 5 80 40 7 < 20 < 10 40 13 1 < 5 101 74 37 4191.04 0.309 0.05 0.87 99.26 4 8 29 30 3 < 20 < 10 40 10 1 < 5 42 83 196 5402.5 1.635 0.1 1.06 96.61 3 16 24 < 20 2 < 20 20 150 34 9 22 85 145 8978 66981.38 0.675 0.07 0.6 98.6 6 7 74 40 5 < 20 < 10 70 10 1 < 5 59 93 175 3633.08 2.317 0.37 1.73 100.4 19 24 211 50 48 70 10 220 20 2 < 5 369 207 363 2900.68 0.982 0.05 0.69 99.08 25 48 131 < 20 8 < 20 < 10 340 29 7 8 54 62 2762 3892.55 2.12 0.32 1.21 99.58 19 41 177 50 35 60 < 10 330 25 2 < 5 356 158 272 3803.09 0.466 0.09 1.2 99.57 4 15 43 30 5 < 20 < 10 70 14 1 < 5 159 113 283 3363.72 0.357 0.08 0.4 98.8 3 6 21 20 2 < 20 < 10 < 30 9 < 1 < 5 129 61 144 9090.99 0.619 0.05 0.44 97.95 4 15 16 < 20 < 1 < 20 < 10 90 23 4 6 31 42 1727 40421.25 0.116 0.02 0.11 100.4 < 1 8 < 5 30 < 1 < 20 < 10 < 30 35 2 < 5 50 23 220 4630.38 0.184 0.04 0.18 100.5 2 8 6 20 < 1 < 20 < 10 40 16 2 < 5 15 17 414 52054.08 0.105 0.02 0.19 100.9 < 1 9 7 < 20 < 1 < 20 < 10 < 30 30 2 < 5 176 52 148 12712.71 0.195 < 0.01 0.16 99.04 < 1 14 5 < 20 < 1 < 20 < 10 < 30 30 2 < 5 107 49 445 3113.07 0.23 0.07 0.77 98.44 3 2 23 30 2 < 20 < 10 < 30 6 < 1 < 5 100 50 30 1831.05 0.195 < 0.01 0.41 100.2 1 77 15 < 20 1 < 20 < 10 < 30 49 3 < 5 33 165 655 14851.81 0.171 0.03 0.3 98.05 < 1 49 13 < 20 < 1 < 20 < 10 < 30 58 3 < 5 66 119 742 29040.92 0.222 0.02 0.31 100.8 1 69 27 < 20 2 < 20 < 10 < 30 45 2 < 5 27 157 549 11681.4 1.348 0.16 1.41 99.91 21 50 172 60 42 60 < 10 150 30 2 < 5 90 229 75 3161.17 0.272 0.05 0.83 98.62 4 160 34 < 20 8 < 20 < 10 40 58 2 < 5 83 298 73 1361.19 1.987 0.26 1.33 99.33 30 54 248 50 50 50 < 10 140 27 2 < 5 65 268 39 1681.4 6.834 0.32 1.93 71.94 4 2 132 < 20 7 < 20 20 120 36 15 32 93 122 24670 786505.79 0.307 0.04 0.41 98.64 4 4 18 < 20 1 < 20 < 10 < 30 12 < 1 < 5 184 79 36 2332.75 0.365 0.04 0.55 99 5 2 37 20 4 < 20 < 10 < 30 12 1 < 5 85 73 48 1505.16 0.166 0.07 0.24 100.1 < 1 7 6 < 20 < 1 < 20 < 10 < 30 39 3 < 5 200 54 603 9412.88 0.214 0.03 0.28 98.68 < 1 7 < 5 < 20 < 1 < 20 < 10 50 40 4 < 5 111 51 1417 7252.41 0.683 0.07 0.53 97.45 2 7 18 < 20 1 < 20 < 10 80 39 5 10 87 78 3440 37162.19 0.321 0.03 0.58 98.17 3 6 25 40 2 < 20 < 10 50 21 2 < 5 75 67 562 19571.92 0.331 0.06 1.01 100.8 5 2 37 20 3 < 20 < 10 < 30 11 1 < 5 85 41 31 1354.9 0.094 0.03 0.44 98.8 < 1 7 < 5 < 20 < 1 < 20 < 10 < 30 37 2 < 5 183 62 646 2984.57 0.133 < 0.01 0.31 98.38 < 1 5 < 5 20 < 1 < 20 < 10 < 30 34 2 < 5 156 64 364 1425.88 0.12 0.02 1.29 98.39 < 1 7 6 30 < 1 < 20 < 10 < 30 32 2 < 5 180 67 345 2102.42 0.41 0.08 1.21 99.55 6 2 42 50 5 < 20 < 10 < 30 11 1 < 5 79 52 31 1554.74 0.708 0.18 3.62 101 12 5 60 60 11 < 20 < 10 100 16 2 11 174 243 33 2171.89 1.491 0.49 0.43 98.48 33 2 391 30 41 30 170 130 22 2 < 5 54 574 29 1475.61 0.44 0.09 0.26 98.56 5 4 28 < 20 2 < 20 < 10 50 18 2 < 5 217 133 42 4305.85 0.537 0.11 0.34 99.09 8 3 30 < 20 2 < 20 < 10 60 18 1 < 5 150 206 29 4476.56 0.587 0.1 0.32 99.13 8 3 33 30 3 < 20 10 60 18 2 8 168 231 31 4925.86 0.275 0.05 0.26 98.71 3 4 13 < 20 1 < 20 < 10 30 16 1 < 5 243 114 53 2311.78 1.465 0.39 1.12 100.6 37 2 366 < 20 39 < 20 150 120 22 2 < 5 58 457 32 1472.26 0.435 0.1 0.62 98.74 5 8 40 30 6 < 20 < 10 50 11 1 < 5 145 64 30 1432.15 0.037 0.02 0.41 99.3 < 1 12 11 < 20 < 1 < 20 < 10 < 30 51 2 < 5 81 40 77 2702.36 0.317 0.05 0.54 99.44 2 24 81 < 20 1 < 20 < 10 < 30 76 4 < 5 98 85 255 36473.33 0.296 0.05 0.55 100.4 3 20 85 < 20 1 < 20 < 10 < 30 75 3 < 5 179 70 303 38669.18 0.048 0.02 0.38 100.5 < 1 8 13 < 20 < 1 < 20 < 10 < 30 52 3 < 5 522 108 29 693.61 0.449 0.1 0.96 100.7 7 11 48 30 6 < 20 < 10 50 15 1 < 5 220 61 26 1545.11 0.344 0.1 0.57 98.51 5 7 30 < 20 3 < 20 < 10 30 17 1 < 5 247 122 33 2385.96 0.306 0.07 0.36 98.58 4 6 20 < 20 2 < 20 < 10 < 30 17 1 < 5 290 106 32 2875.78 0.308 0.05 0.38 99.1 4 8 18 < 20 1 < 20 < 10 < 30 16 2 < 5 286 74 52 6265.55 0.306 0.05 0.28 98.43 4 8 17 < 20 1 < 20 < 10 < 30 16 2 < 5 277 87 53 4105.75 0.304 0.02 0.49 98.08 4 8 17 30 2 < 20 < 10 40 16 2 < 5 294 85 38 2673.27 0.109 0.01 0.15 99.16 1 4 8 20 < 1 < 20 < 10 < 30 11 1 < 5 147 39 18 98


Nb (ppm) Mo (ppm) Ag (ppm) In (ppm) Sn (ppm) Sb (ppm) Cs (ppm) Ba (ppm) Bi (ppm) La (ppm) Ce (ppm) Pr (ppm) Nd (ppm) Sm (ppm) Eu (ppm) Gd (ppm) Tb (ppm) Dy (ppm) Ho (ppm) Er (ppm)154 < 2 2.4 < 0.2 12 < 0.5 2.8 1841 < 0.4 23.7 75.6 7.95 36.5 15.5 2.09 20 4.4 31.9 6.8 21.8

2 0.3 63 < 0.5 2.7 1023 < 0.4 428 1190 150 706 327 28.2 459 106 861 204 7037 0.5 80 0.8 4 955 1.4 2320 5570 677 3000 1190 99.2 1720 405 3180 755 2450

154 < 2 1.1 < 0.2 7 < 0.5 3.4 828 < 0.4 82.8 123 20.7 83.6 21.1 2.07 20.2 3.6 25.6 5.6 17.673 < 2 0.6 < 0.2 2 < 0.5 5.7 199 < 0.4 8.4 22.6 3.07 13.9 4.1 0.58 4.4 0.9 6.6 1.6 5.79 3 0.8 < 0.2 2 0.7 4.6 409 0.6 23.1 53.9 7.54 35 8.9 2.48 8.9 1.3 8 1.6 4.6

108 3 1 < 0.2 8 1.2 6.6 293 1.2 28.4 65.7 9.59 46.3 15.4 3.17 18.6 3.5 24 5.2 16.7< 2 0.3 61 1.1 1.8 288 1.9 508 1640 256 1290 519 39.2 591 126 861 186 585

160 < 2 1.1 0.2 46 3 6.5 482 0.8 41.4 112 14.8 64 18.8 2.02 22.1 4.4 30.4 7 24.4111 < 2 0.6 0.2 64 2.3 4.9 644 0.5 16.3 48.2 6.06 26.9 9 0.9 9.6 1.9 13.8 3.1 10.934 < 2 0.9 < 0.2 5 3.1 4.8 559 < 0.4 27 80 7.28 29.1 6.4 1.1 6 1 5.9 1.3 3.722 < 2 0.7 < 0.2 3 2.2 4.3 539 < 0.4 30.4 65.2 8 31.9 6.7 1.15 5.6 1 5.4 1.2 3.472 < 2 1.1 < 0.2 3 3.2 3.5 586 0.6 29.1 59.6 7.46 29.8 6.3 1.16 5.2 0.9 5.2 1.1 3.216 < 2 0.7 < 0.2 4 < 0.5 5.2 577 < 0.4 20 48 6.31 25.6 6.2 0.92 5.3 0.8 5.4 1.1 3.5102 < 2 1.2 < 0.2 6 < 0.5 2.2 230 0.8 40.2 105 13.9 62.5 20.3 1.8 22.4 4.2 29.6 6.5 21.3

< 2 0.6 130 1.7 2.4 263 2.3 589 1700 263 1480 789 66.9 1100 258 1950 446 141051 < 2 < 0.5 < 0.2 6 < 0.5 1.6 308 < 0.4 49.4 125 16.1 65.6 16.5 1.65 15.5 2.6 18.1 3.9 12.8668 < 2 0.5 0.3 45 < 0.5 14.8 417 1 32.9 88 13.8 74.8 35.9 4.21 47.3 10.5 81.7 18.8 61.9

< 2 1 1.7 255 < 0.5 4.3 69 0.9 205 573 89.4 476 249 21.2 362 82.4 663 151 495189 < 2 0.9 0.2 34 < 0.5 12.6 221 0.8 38.3 109 15.9 71.5 23.6 3.08 26.1 5.3 38.2 8.8 29.3277 < 2 < 0.5 < 0.2 8 < 0.5 2.5 493 < 0.4 65.4 179 25.8 115 38.6 3.32 41 8.2 56.4 12.2 38.9142 < 2 4.1 < 0.2 9 < 0.5 2.2 448 < 0.4 22.5 56.1 8.47 38 13.5 1.46 14.5 3.1 22.8 5.3 19.4

< 2 0.6 100 < 0.5 0.8 76 < 0.4 215 693 121 663 302 22.9 360 73.9 532 113 337276 < 2 1.1 < 0.2 8 < 0.5 1.6 68 < 0.4 64.6 150 20.7 94.6 35.7 2.61 39.8 8.5 59.3 12.9 38.2552 < 2 < 0.2 27 < 0.5 < 0.5 37 < 0.4 162 434 64 309 103 7.09 96.4 17.4 111 21.9 64.6179 < 2 < 0.2 14 < 0.5 2.9 271 < 0.4 18.5 53.5 9.09 49.1 22.4 1.69 25.1 5.3 37 8.1 25.6575 < 2 0.5 < 0.2 22 < 0.5 1.2 170 < 0.4 338 727 90.6 360 98.8 6.52 96.9 18.6 130 27.1 82.318 < 2 < 0.5 < 0.2 2 < 0.5 1.5 405 < 0.4 20.2 36.3 5.83 23.2 5.3 0.79 4.4 0.7 4.9 1 3.1616 < 2 < 0.2 37 < 0.5 < 0.5 76 < 0.4 28.1 92.5 13.4 61.6 24.2 1.98 30.3 7.6 57.2 14.3 57.8

< 2 < 0.2 50 < 0.5 0.5 80 < 0.4 40.8 139 21.2 98.3 39.9 3.3 49.9 12.6 96.7 23.7 95.4725 < 2 < 0.2 42 < 0.5 < 0.5 71 < 0.4 26.5 93.9 13.5 64.4 27.5 2.24 34.4 8.8 68.1 16.8 65.9100 < 2 1.2 < 0.2 11 0.9 3.9 139 1.3 13.4 37.9 4.84 20.2 5.6 1.23 6.2 1.3 8.9 2 7.4103 < 2 < 0.5 < 0.2 12 < 0.5 4 178 < 0.4 48.8 133 16.7 52.8 7.9 0.66 4.2 0.7 4.7 1 4.231 < 2 < 0.5 < 0.2 8 0.6 3.4 185 0.9 10 29 3.95 18.6 5.3 1.72 6.1 1.1 6.4 1.3 4.1

4 1 279 1.1 3.2 306 3.6 432 2220 517 3310 1820 155 2740 671 5000 1140 369040 < 2 < 0.5 < 0.2 2 < 0.5 1.8 401 < 0.4 20.5 52.7 5.1 17.5 4.1 0.37 3.6 0.7 5.1 1 3.627 < 2 < 0.5 < 0.2 3 < 0.5 0.9 390 < 0.4 13.6 32.1 4.46 19.4 5.5 0.86 5.8 1.1 7.8 1.7 5.5855 < 2 2.7 < 0.2 9 < 0.5 0.8 290 < 0.4 340 689 79.2 303 72.3 4.88 76.4 17.2 122 27.3 91

< 2 2 < 0.2 39 < 0.5 0.6 196 < 0.4 289 709 93 405 137 9.77 174 41.1 296 66.9 214< 2 < 0.2 39 < 0.5 0.6 214 < 0.4 1060 2490 293 1140 304 20.2 336 80.1 578 133 452

661 < 2 < 0.2 16 0.6 0.9 212 < 0.4 36.8 114 14.7 73 34.1 2.85 49.2 12 95.8 22.5 8110 < 2 < 0.5 < 0.2 2 < 0.5 1.2 349 < 0.4 17.5 38.2 4.69 19.1 4.2 0.74 3.9 0.7 4.8 1.1 3.4654 < 2 0.7 3.2 9 < 0.5 1.1 276 < 0.4 63.2 147 21.2 104 43.6 3.54 62.7 15.4 111 26 85.3293 < 2 < 0.5 < 0.2 5 < 0.5 0.9 257 < 0.4 58.2 121 15.8 71.5 23.8 1.86 30.5 7 49.3 11.3 40.7338 < 2 < 0.5 < 0.2 11 < 0.5 1.4 310 < 0.4 53.5 115 15.7 70.4 24.7 2 30.6 7 49.7 11.3 40.516 < 2 < 0.5 < 0.2 2 0.7 1.7 379 < 0.4 33 58.3 6.89 25.3 5.1 0.98 4.2 0.8 4.8 1 3.411 < 2 < 0.5 < 0.2 3 3.2 4.6 579 1.2 31.5 63.2 7.72 29.9 6.2 1.27 5.6 0.9 5.8 1.2 3.65 < 2 < 0.5 < 0.2 < 1 < 0.5 2.7 1040 < 0.4 27.8 58.2 7.62 31.7 6.3 1.75 5.6 0.9 5.4 1.1 3.120 < 2 1.1 < 0.2 2 < 0.5 2.7 637 < 0.4 104 214 23.7 81.6 12.6 1.06 8.3 1.2 7.3 1.4 4.412 < 2 1.2 < 0.2 1 < 0.5 3 1050 < 0.4 59.3 116 13.2 49.7 8.2 1.52 5.6 0.8 4.9 1 3.121 < 2 2.7 < 0.2 21 < 0.5 3.4 1321 < 0.4 80.4 157 18.8 65.5 10.5 2.02 7.2 1 6 1.2 3.718 < 2 0.6 < 0.2 2 < 0.5 2.4 516 < 0.4 102 199 21.1 71.5 11.4 0.89 8.3 1.4 8.7 1.8 5.66 < 2 < 0.5 < 0.2 1 < 0.5 1.4 824 < 0.4 28.1 60 7.57 32.4 6.4 1.9 6 0.9 5.5 1.1 3.46 < 2 < 0.5 < 0.2 2 < 0.5 4.3 330 < 0.4 15.8 36.6 4.45 17.4 3.8 0.71 3.5 0.6 3.9 0.8 2.773 < 2 0.6 0.3 110 < 0.5 1.3 51 < 0.4 11.8 39.6 5.13 19.3 5.3 0.54 4 1 8 2 9.1255 < 2 1.9 616 < 0.5 1.6 57 < 0.4 88.4 293 39.4 134 26.5 1.9 14.9 3.6 27.6 6.8 33.8278 < 2 1.8 565 < 0.5 2.4 66 < 0.4 59.7 214 28.8 101 22.5 1.75 13.9 3.8 31.4 8.5 46.728 < 2 0.5 0.2 75 < 0.5 5.1 221 < 0.4 4.2 13.2 1.79 7.1 1.7 0.26 1.5 0.4 2.9 0.8 3.99 < 2 0.5 < 0.2 5 < 0.5 5 513 < 0.4 19.2 38.5 4.74 18.7 4 0.72 3.6 0.6 3.9 0.8 2.522 < 2 0.7 < 0.2 5 < 0.5 3.2 362 < 0.4 40.1 99.3 9.62 33.4 6.1 0.5 4.1 0.8 5.1 1 3.425 < 2 0.7 < 0.2 5 < 0.5 3.2 369 < 0.4 36.4 91.7 8.92 30.8 5.7 0.43 4.1 0.8 5.4 1.2 3.837 < 2 1.7 < 0.2 7 < 0.5 3.3 363 < 0.4 39.1 100 9.88 34.2 7.5 0.43 6.2 1.3 9 2.1 6.732 < 2 1.3 < 0.2 4 < 0.5 3.6 356 < 0.4 58.5 131 13.5 47.8 8.6 0.57 6.4 1.2 8.6 1.9 6.225 < 2 2 < 0.2 4 < 0.5 4 366 < 0.4 53.1 116 12.2 40.9 7.3 0.56 5.3 1 6.3 1.4 4.622 < 2 < 0.5 < 0.2 4 < 0.5 2 161 < 0.4 11.2 29.7 2.9 9.9 2.1 0.17 2 0.4 2.7 0.6 2.3


Tm (ppm) Yb (ppm) Lu (ppm) Hf (ppm) Ta (ppm) W (ppm) Tl (ppm) Pb (ppm) Th (ppm) U (ppm) Nb2O5 (%)3.22 18.3 2.3 27.1 12.9 < 1 0.4 75 19.2 9104 585 73.4 757 195 43 0.4 215 596 479 1.061348 1830 212 768 490 235 0.5 510 2270 1660 3.5292.5 14 1.8 13.2 10.3 < 1 0.4 49 27.1 7.60.93 7.2 1.12 4.4 10 < 1 0.8 56 28.2 140.64 3.9 0.63 5.9 0.5 3 0.5 36 2.4 3.62.44 14.6 1.89 9.3 7.5 3 0.7 53 12.9 13.784.7 471 56 227 511 46 0.3 381 1360 763 0.874.13 27.9 4.16 8.7 32.9 < 1 1 75 32.2 7.11.95 13.4 2 7.5 37.6 2 1.7 158 35 170.57 4.1 0.62 7.3 1.8 1 1 46 11.4 2.60.51 3.4 0.55 6 1 < 1 0.9 39 8.5 2.40.48 3.2 0.52 7.4 1 1 0.7 25 8.2 3.30.5 3.4 0.58 10.9 1.8 < 1 0.4 33 9.1 3.33.21 19.2 2.49 15.1 9.6 < 1 0.1 45 30.6 14.8201 1090 123 166 651 32 0.4 582 1260 1250 1.8751.91 11.7 1.65 10.2 2.1 < 1 0.1 58 16.8 5.29.12 52 6.34 10.8 39.4 2 1.7 84 65 64.272.9 404 47.2 24.1 235 14 0.2 196 472 428 0.6634.71 28.7 4.01 16.9 18.5 < 1 1.4 64 38.1 9.25.62 32.7 3.85 10.8 23.5 1 0.6 72 74 303.55 24.5 3.61 43.2 15.2 < 1 0.6 42 75 15.244.8 231 26.3 115 158 7 0.1 144 391 265 0.4645.17 26.4 2.94 10.3 21.9 < 1 0.2 34 41.4 40.39.2 53.1 7.23 100 44.5 2 < 0.1 38 139 69.73.65 20.6 2.57 26 14.3 < 1 0.7 33 26.5 21.811.1 55.9 6.38 10.2 38.8 2 0.3 62 83.1 54.70.45 3.1 0.47 4.9 0.9 < 1 0.4 19 7.9 1.912.3 95.6 15.3 65.9 75.3 17 < 0.1 127 175 28.919.8 154 23.9 165 88.1 7 0.2 151 323 43.8 0.1813.5 102 15.2 62.4 66.6 6 < 0.1 99 187 30.41.46 11.4 1.82 17.3 13.1 1 0.4 52 21.1 7.30.99 9.5 1.7 16.6 111 7 0.3 94 51.6 88.60.63 4.5 0.78 5.3 17 < 1 0.3 41 4.7 10541 3030 331 2500 1000 170 0.4 687 2490 2200 4.4750.57 3.6 0.58 5.3 2 < 1 0.9 15 19.7 3.10.85 5.2 0.76 4.1 1.3 < 1 0.3 8 8.2 3.214 81.7 9.92 27.2 41.3 3 0.7 54 277 75.1

31.3 172 19.9 22.7 67.7 6 0.4 67 322 142 0.37171.4 418 51.8 103 242 13 0.3 196 853 395 0.714.2 88.5 10.4 54.6 39.1 7 0.2 54 140 69.80.54 3.5 0.54 3.4 0.8 < 1 0.3 6 6.4 1.912.8 71.8 8.51 9.9 27.4 2 0.7 49 115 52.66.21 33.4 4.22 4.3 11.9 1 0.6 47 70.7 18.96.26 34.7 4.35 6.5 14.2 2 1 53 70.4 25.60.5 3 0.48 3.9 0.6 < 1 0.6 7 6.1 1.60.55 3.4 0.53 5.3 0.9 4 0.8 25 9.6 2.80.46 3 0.48 3.7 0.3 < 1 0.2 11 3 0.90.67 4.5 0.72 10.1 1.2 < 1 0.8 27 24.7 3.10.44 3.1 0.53 9.4 0.8 < 1 0.5 24 11.6 3.10.57 3.9 0.59 10.4 1.1 5 0.4 45 15 3.70.87 5.9 0.91 6.6 2 < 1 0.9 27 46.1 5.20.49 3.3 0.52 3.9 0.2 < 1 0.3 8 3.2 0.80.47 3.3 0.59 3.4 0.9 < 1 0.7 42 5.5 1.62.36 22.2 3.63 26.2 31.6 < 1 0.4 66 63.6 9.19.68 100 18.5 414 110 3 0.4 138 563 36.314 151 28 451 114 4 0.7 131 695 41.1

1.19 12.2 2.11 8.2 12 < 1 2.2 260 18 2.70.44 3.2 0.57 6.7 1 1 1 44 6.6 1.90.59 4.3 0.7 6.5 2.2 < 1 1.1 26 26.3 3.30.65 5 0.87 9.2 3.2 < 1 1.2 34 34.2 3.71.18 8.2 1.34 16.2 3.4 < 1 1.2 44 35.6 7.41.03 7.6 1.25 11.1 2.6 < 1 1.2 38 36.7 5.50.85 6 0.93 7 2.2 4 0.6 41 29.9 4.60.39 2.6 0.42 3.1 2.4 < 1 0.7 24 12.8 6.1

Channel_ID Lic_Num Easting Northing Chem_Num From_m To_m Length P ROCK TYPE Rock Type 2 RT 2 Perc Grain Size Fabric Mt Perc Pyx Perc Bt Perc Amph Perc L Perc Ti PercLPC-14-18 22073M 575767 5801447 507275 1.65 1.92 0.27 felsic vf fol <1 — <1 — — —LPC-14-19 22073M 575831 5801508 507276 0 0.1 0.1 felsic f fol <1 — 1-2 — — —LPC-14-19 22073M 575831 5801508 507277 0.1 0.23 0.13 felsic f <1 — 15-20 3-5 — —LPC-14-19 22073M 575831 5801508 507278 0.23 0.34 0.11 felsic f fol <1 — <1 — — —LPC-14-20 22073M 575831 5801504 507279 0 0.17 0.17 pegmatite f-c peg <1 — 1 1-3 — <1LPC-14-20 22073M 575831 5801504 507280 0.17 0.35 0.18 mafic m — — 25 25LPC-14-21 22073M 572850 5802859 507281 0 0.5 0.5 felsic f-m fol <1 — 5 — — <1LPC-14-21 22073M 572850 5802859 507282 0.5 0.6 0.1 pegmatite m-c peg 20 — — — <1 3LPC-14-21 22073M 572850 5802859 507283 0.6 1.12 0.52 felsic f-m fol <1 — 5 — — <1LPC-14-22A 22073M 572894 5802807 507284 0 0.78 0.78 felsic f-m fol 1 — 3-5 1-2 — <1LPC-14-22A 22073M 572894 5802807 507285 0.78 0.91 0.13 felsic f-m fol 1 — 3-5 1-2 — <1LPC-14-22A 22073M 572894 5802807 507286 0.91 1 0.09 pegmatite m peg 15-20 — — <1 — 2-3LPC-14-22A 22073M 572894 5802807 507287 1 1.2 0.2 pegmatite f-m — — — 20 — —LPC-14-22A 22073M 572894 5802807 507288 1.2 1.41 0.21 pegmatite f-m peg 10 — <1 5 — 3-5LPC-14-22A 22073M 572894 5802807 507289 1.41 1.56 0.15 pegmatite pegmatite 30 f-m peg 10-15 — — 10-15 tr 3-5LPC-14-22A 22073M 572894 5802807 507290 1.56 1.65 0.09 pegmatite f-m peg 10-15 — — 10-15 tr 3-5LPC-14-22A 22073M 572894 5802807 507291 1.65 1.79 0.14 felsic m fol 5 — 2 3 — 1LPC-14-22A 22073M 572894 5802807 507292 1.79 2.14 0.35 felsic pegmatite 30 f-m fol <1 — 3-5 1 — 4LPC-14-22A 22073M 572894 5802807 507293 2.14 2.3 0.16 felsic f-m fol 2-3 — 15 2-3 — 3-5LPC-14-22A 22073M 572894 5802807 507294 2.3 2.52 0.22 felsic f-m fol <1 — 2-3 3-5 — 1-2LPC-14-22A 22073M 572894 5802807 507295 2.52 2.83 0.31 felsic f-m fol <1 — 2-3 3-5 — 1-2LPC-14-22B 22073M 572894 5802807 507296 0 0.1 0.1 pegmatite m-c peg 3-5 — 1 10 — 5LPC-14-22B 22073M 572894 5802807 507297 0.1 0.22 0.12 pegmatite m peg 20 — 1-2 50 — 5-7LPC-14-22B 22073M 572894 5802807 507298 0.22 0.43 0.21 granite f-m f 7-10 — 5-7 3-5 — 3-5LPC-14-23 22073M 572070 5802942 507299 0 0.35 0.35 felsic f-m fol 1 — 7 — — <1LPC-14-23 22073M 572070 5802942 507300 0.35 0.65 0.3 pegmatite m-c peg 30 1? — — <1 10LPC-14-23 22073M 572070 5802942 507301 0.65 1.03 0.38 felsic f-m fol <1 — 7 — — <1LPC-14-23 22073M 572070 5802942 507302 1.03 1.39 0.36 felsic f-m fol <1 — 5-7 — — <1LPC-14-23 22073M 572070 5802942 507303 1.39 1.54 0.15 pegmatite m-c peg 2 — — — — 2-3

Channel_ID Lic_Num Easting Northing Chem_Num From_m To_m LengthLPC-14-18 22073M 575767 5801447 507275 1.65 1.92 0.27LPC-14-19 22073M 575831 5801508 507276 0 0.1 0.1LPC-14-19 22073M 575831 5801508 507277 0.1 0.23 0.13LPC-14-19 22073M 575831 5801508 507278 0.23 0.34 0.11LPC-14-20 22073M 575831 5801504 507279 0 0.17 0.17LPC-14-20 22073M 575831 5801504 507280 0.17 0.35 0.18LPC-14-21 22073M 572850 5802859 507281 0 0.5 0.5LPC-14-21 22073M 572850 5802859 507282 0.5 0.6 0.1LPC-14-21 22073M 572850 5802859 507283 0.6 1.12 0.52LPC-14-22A 22073M 572894 5802807 507284 0 0.78 0.78LPC-14-22A 22073M 572894 5802807 507285 0.78 0.91 0.13LPC-14-22A 22073M 572894 5802807 507286 0.91 1 0.09LPC-14-22A 22073M 572894 5802807 507287 1 1.2 0.2LPC-14-22A 22073M 572894 5802807 507288 1.2 1.41 0.21LPC-14-22A 22073M 572894 5802807 507289 1.41 1.56 0.15LPC-14-22A 22073M 572894 5802807 507290 1.56 1.65 0.09LPC-14-22A 22073M 572894 5802807 507291 1.65 1.79 0.14LPC-14-22A 22073M 572894 5802807 507292 1.79 2.14 0.35LPC-14-22A 22073M 572894 5802807 507293 2.14 2.3 0.16LPC-14-22A 22073M 572894 5802807 507294 2.3 2.52 0.22LPC-14-22A 22073M 572894 5802807 507295 2.52 2.83 0.31LPC-14-22B 22073M 572894 5802807 507296 0 0.1 0.1LPC-14-22B 22073M 572894 5802807 507297 0.1 0.22 0.12LPC-14-22B 22073M 572894 5802807 507298 0.22 0.43 0.21LPC-14-23 22073M 572070 5802942 507299 0 0.35 0.35LPC-14-23 22073M 572070 5802942 507300 0.35 0.65 0.3LPC-14-23 22073M 572070 5802942 507301 0.65 1.03 0.38LPC-14-23 22073M 572070 5802942 507302 1.03 1.39 0.36LPC-14-23 22073M 572070 5802942 507303 1.39 1.54 0.15

Comments WO SiO2 (%) Al2O3 (%) Fe2O3_T (%) MnO (%) MgO (%) CaO (%) Na2O (%)Hematized. Euhedral Mt. A14-08506 72.97 12.81 1.58 0.025 0.27 0.63 3.39

Sparce euhedral Mt. A14-08505 71.9 13.71 2.02 0.047 0.4 1.05 4.02Mafic-rich band. A14-08505 53.55 18.71 9.54 0.231 3.64 3.49 6.31

Same as first sample w/less bt. A14-08505 73.68 13.54 1.45 0.032 0.3 0.83 3.53Ti assoc w/Am. Euhedral Mt. 3-5m south of LPC-14-19. A14-08503 58.01 18.25 6.19 0.186 2.2 3.33 5

tr-sulph. Homogeneous. A14-08503 44.98 15.69 14.23 0.31 7.05 7.06 2.84hematized fractures throughout A14-08566 69.51 13.93 3.18 0.074 0.68 1.04 4.16

qtz - mt minz A14-08566 63.75 0.74 29.48 0.133 0.29 0.78 0.04same as first sample. A14-08566 69.83 13.67 3.12 0.073 0.7 1.23 3.96

A14-08568 69.41 14.09 2.89 0.105 0.59 1.22 4.26Jog in channel @0.78m. Same rock as above. A14-08568 71.81 13.98 2.75 0.096 0.61 1.29 4.82

All metallic minz might not be mt. (illmanite?), hematized. A14-08568 57.5 9.36 19.22 0.207 0.77 1.94 4.22End of "O" and "E" very rubbly, sampled together. A14-08568 57.67 14.09 12.13 0.267 1.53 2.26 6.26

Hematized fractures. A14-08568 58.51 11.56 15.17 0.307 0.8 2.59 5.154 cm peg within (to small to sample). A14-08568 65.51 13.35 10.56 0.167 0.45 1.7 6.32

Same as above. A14-08568 64.75 11.96 14.03 0.235 0.69 1.91 5.68Mafic-rich bands. A14-08568 67.39 15.73 6.04 0.135 0.32 1.51 7.32

A14-08568 72.39 14.39 1.59 0.056 0.28 0.81 4.27Slightly mineralized section within host. A14-08568 66.95 12.52 6.56 0.214 1.47 2.46 3.93

A14-08568 71.46 13.84 2.77 0.088 0.49 1.14 4.13Jog in channel @ 2.52m (sampled sep.). Same as above. A14-08568 71.54 14.19 2.72 0.092 0.52 1.25 4.19

hematized fractures. A14-08565 58.78 12.91 11.16 0.288 0.89 3.41 6.21hard to determine % of minerals, but highly mineralized. A14-08565 47.52 4.27 31.24 0.63 1.22 5.67 1.78

similar to high REE island? Slightly foliated. A14-08565 63.07 13.09 11.04 0.225 0.44 2.52 6.45euhedral mt. A14-08564 71.16 8.42 10.34 0.052 0.21 0.79 1.78

qtz - mt mineralization. A14-08564 70.62 14.05 2.84 0.043 0.65 1.26 4.47same as first sample A14-08564 73.97 12.58 2.69 0.044 0.61 1.31 4.01same as first sample A14-08564 55.85 1.85 32.19 0.141 0.21 1.98 0.29

qtz-mt minz. (not as mineralized as above peg) A14-08564 70.64 14.39 3.25 0.045 0.52 1.19 4.14


K2O (%) TiO2 (%) P2O5 (%) LOI (%) Total (%) Sc (ppm) Be (ppm) V (ppm) Cr (ppm) Co (ppm) Ni (ppm) Cu (ppm) Zn (ppm) Ga (ppm) Ge (ppm) As (ppm) Rb (ppm) Sr (ppm) Y (ppm) Zr (ppm)6.16 0.333 0.06 0.29 98.54 4 9 18 < 20 2 < 20 < 10 < 30 17 2 < 5 320 76 78 7364.87 0.216 0.07 0.42 98.72 4 5 21 < 20 2 < 20 30 30 19 2 < 5 195 214 26 1272.04 0.69 0.39 1.87 100.5 14 8 138 < 20 26 < 20 30 180 24 2 < 5 222 387 23 795.76 0.167 0.05 0.41 99.74 3 4 15 < 20 2 < 20 30 < 30 17 1 < 5 221 202 19 845.13 0.643 0.19 1.08 100.2 12 13 102 < 20 14 20 820 120 28 2 < 5 305 406 50 2933.29 1.226 0.23 2.02 98.93 33 6 276 40 55 100 2360 180 21 2 < 5 350 386 28 794.96 0.407 0.14 0.57 98.65 7 5 30 < 20 3 < 20 10 50 20 2 < 5 162 191 74 3450.15 1.328 0.05 0.4 97.14 2 < 1 53 20 6 < 20 < 10 410 29 7 9 18 28 5912 44744.83 0.452 0.16 0.48 98.5 7 4 28 < 20 3 < 20 20 50 19 2 < 5 160 195 135 3575.15 0.409 0.11 0.48 98.72 7 8 26 < 20 3 < 20 < 10 60 22 2 < 5 233 176 90 3143.81 0.426 0.12 0.51 100.2 6 7 21 < 20 2 < 20 < 10 70 21 2 < 5 145 146 99 2820.34 0.718 0.34 1.44 96.06 15 22 70 < 20 4 < 20 < 10 270 38 5 6 7 103 1714 208900.6 0.514 0.34 1.33 96.99 10 22 65 < 20 7 < 20 < 10 300 36 3 < 5 17 210 1148 116500.56 0.944 0.28 0.67 96.54 12 27 54 < 20 3 < 20 < 10 300 41 5 6 12 111 2398 136100.67 0.384 0.13 0.51 99.75 13 22 42 < 20 2 < 20 < 10 190 42 4 < 5 12 59 447 54450.48 0.335 0.11 0.45 100.6 23 31 62 < 20 3 < 20 < 10 280 42 4 < 5 8 46 234 12340.9 0.219 0.05 0.35 99.95 8 17 25 < 20 1 < 20 < 10 150 44 3 < 5 15 56 162 8535.46 0.211 0.08 0.42 99.97 4 9 14 < 20 1 < 20 < 10 50 22 2 < 5 237 135 37 1404.1 0.951 0.32 0.5 99.97 15 6 66 < 20 7 < 20 10 140 23 2 < 5 213 157 131 7325.33 0.363 0.13 0.37 100.1 5 6 23 < 20 2 < 20 < 10 60 19 2 < 5 211 178 74 2675.19 0.378 0.14 0.41 100.6 6 5 25 < 20 3 < 20 30 60 19 2 < 5 199 184 48 2701.04 0.918 0.17 0.67 96.45 14 32 37 30 3 < 20 < 10 270 35 6 8 22 157 6973 60610.14 2.446 0.29 0.53 95.73 21 32 87 30 5 < 20 < 10 590 31 9 12 4 68 9186 90190.71 0.833 0.29 0.1 98.76 12 23 38 < 20 2 < 20 < 10 240 44 4 < 5 11 68 504 38054.32 0.753 0.06 0.08 97.99 < 1 6 28 < 20 3 < 20 30 180 26 5 < 5 156 137 3254 34314.77 0.382 0.14 0.3 99.52 5 5 27 < 20 4 < 20 20 30 19 2 < 5 169 214 86 3094.42 0.368 0.11 0.33 100.4 5 4 27 < 20 4 < 20 50 50 18 1 < 5 153 195 105 3020.67 2.158 0.15 -0.19 95.3 < 1 < 1 71 20 7 < 20 < 10 590 34 5 9 21 61 6584 174705.33 0.406 0.13 0.28 100.3 5 6 25 < 20 4 < 20 < 10 70 21 2 < 5 200 233 214 842


Nb (ppm) Mo (ppm) Ag (ppm) In (ppm) Sn (ppm) Sb (ppm) Cs (ppm) Ba (ppm) Bi (ppm) La (ppm) Ce (ppm) Pr (ppm) Nd (ppm) Sm (ppm) Eu (ppm) Gd (ppm) Tb (ppm) Dy (ppm) Ho (ppm) Er (ppm)40 < 2 2.2 < 0.2 7 < 0.5 4 371 < 0.4 51.5 125 13.2 46.1 9.6 0.58 8.1 1.8 12.8 3 10.312 < 2 0.7 < 0.2 2 < 0.5 2.3 629 < 0.4 56 96.2 9.55 31.5 4.9 0.71 3.6 0.6 3.8 0.8 2.810 < 2 < 0.5 < 0.2 2 < 0.5 9 321 < 0.4 30.7 57.8 7.37 30.2 5.4 1.37 3.9 0.6 3.6 0.8 2.310 < 2 < 0.5 < 0.2 1 < 0.5 2 679 < 0.4 41.8 70 6.75 21.6 3.4 0.53 2.5 0.4 2.9 0.6 223 < 2 1.5 < 0.2 3 < 0.5 7.5 551 0.9 86.5 176 19.8 71.1 11.9 1.39 8.5 1.3 7.7 1.5 4.83 5 2.7 < 0.2 1 < 0.5 13 1139 2.9 12.4 26.7 3.83 17.6 4.5 1.54 4.8 0.8 5.2 1.1 3.137 < 2 0.8 < 0.2 3 < 0.5 1.6 782 < 0.4 67.1 147 16 58.8 11.5 1.17 9.8 1.7 11.5 2.5 8.2

3 0.3 55 0.9 1.2 31 < 0.4 567 1560 230 1150 497 37.4 680 160 1170 285 90978 < 2 1 < 0.2 4 < 0.5 2 744 < 0.4 79.9 162 20.2 77.5 16.2 1.63 14.4 2.7 18.1 3.8 12.269 < 2 0.8 < 0.2 5 < 0.5 5.2 642 < 0.4 73.5 156 18.2 67.9 14.4 1.44 12.4 2.4 15.7 3.3 11.142 < 2 0.7 < 0.2 15 < 0.5 2.6 534 < 0.4 51.5 119 16.2 65.5 15 1.52 13 2.4 15.2 3.3 11.1

< 2 0.9 105 < 0.5 < 0.5 98 < 0.4 476 1130 140 597 184 14.3 215 48.3 334 78 267< 2 0.5 49 < 0.5 0.6 147 < 0.4 262 604 80.1 354 116 9.33 143 31.8 219 50.7 175< 2 0.9 99 < 0.5 0.6 115 < 0.4 397 959 131 609 225 18.6 306 71.3 502 115 380

414 < 2 0.7 83 < 0.5 0.7 57 < 0.4 142 371 45.6 192 55.5 4.22 57.9 12.2 82.1 18.5 63.782 < 2 0.9 106 < 0.5 0.5 42 < 0.4 175 369 48.3 190 44.7 3.04 37.5 7.1 43.9 9 28.6123 < 2 1.9 0.4 56 < 0.5 1.1 67 < 0.4 57.9 131 18.8 81.4 23.3 1.85 23.9 4.9 31.5 6.7 2232 < 2 < 0.5 < 0.2 4 < 0.5 4.1 574 < 0.4 31.9 66.9 8.31 30.9 6.7 0.76 4.9 0.9 5.6 1.2 451 < 2 2 < 0.2 6 < 0.5 6.4 495 < 0.4 129 293 37.6 143 29 1.94 20.8 3.6 21.6 4.4 13.922 < 2 0.6 < 0.2 3 < 0.5 3.3 714 < 0.4 69.5 132 14.9 53.4 10 1.02 6.9 1.2 7.3 1.5 4.922 < 2 0.6 < 0.2 3 < 0.5 2.9 694 < 0.4 71.8 140 16 58.2 11.1 1.08 7.5 1.3 7.8 1.6 5.2

< 2 0.9 98 0.5 1.3 99 0.5 131 567 134 923 567 49.7 896 218 1600 370 1180< 2 1.5 184 0.6 < 0.5 66 0.8 255 994 220 1420 772 66.7 1150 264 1890 427 1410

374 < 2 0.8 91 < 0.5 0.7 66 < 0.4 193 462 60.6 257 68.6 5.03 68.7 13.7 88.3 19.1 64.6< 2 < 0.2 38 < 0.5 1 451 < 0.4 173 474 78.4 423 197 17.4 271 67.8 495 119 428

61 < 2 0.9 < 0.2 3 < 0.5 1.4 856 < 0.4 65.2 138 16.5 62.2 12.3 1.26 10.4 1.9 12 2.6 9.257 < 2 0.8 < 0.2 4 < 0.5 1.1 829 < 0.4 69.5 151 18.8 71 15.3 1.38 12.5 2.5 16.3 3.4 11.6

2 0.4 103 0.7 < 0.5 213 < 0.4 664 1580 227 1070 442 36.6 567 134 991 233 841139 < 2 2.5 < 0.2 8 < 0.5 1.9 914 < 0.4 63.3 143 19.1 76.8 20.7 1.93 20.7 4.3 29.4 6.6 22.7


Tm (ppm) Yb (ppm) Lu (ppm) Hf (ppm) Ta (ppm) W (ppm) Tl (ppm) Pb (ppm) Th (ppm) U (ppm) Nb2O5 (%)1.83 12.9 2.05 17.5 3.9 < 1 1.2 40 38.5 6.50.45 3.5 0.61 3.8 1.1 < 1 0.9 28 19.3 3.50.35 2.6 0.48 1.9 0.4 < 1 1 16 1.8 3.20.34 2.5 0.44 2.6 0.9 < 1 1 31 12.2 2.30.77 5.6 0.98 7.9 1.3 < 1 1.7 40 28.2 5.80.44 3 0.51 2.1 < 0.1 < 1 2.2 36 0.7 0.91.25 7.3 1.09 9.4 1.5 < 1 0.6 36 13.9 4.4130 661 80.9 139 219 38 < 0.1 145 962 523 1.4751.83 10.5 1.43 11 3.5 < 1 0.6 36 18.5 5.71.73 10.5 1.52 9.2 5.8 < 1 0.8 34 23.6 8.51.78 11.4 1.68 7.6 2.3 < 1 0.6 27 8.5 2.841 238 33 530 43.6 5 < 0.1 74 223 222 0.315

26.4 150 21 290 25.1 3 < 0.1 70 142 153 0.19554.6 292 38.8 348 61.4 9 < 0.1 79 312 251 0.54910.1 62.4 9.23 139 13.7 < 1 < 0.1 25 65.8 46.94.62 32.3 5.32 35.5 8.3 < 1 < 0.1 11 26.1 5.63.49 22.4 3.71 23.7 7.3 < 1 < 0.1 13 22.7 6.60.65 4.4 0.71 4.5 2.3 < 1 0.9 43 9 4.42.13 13.2 2.08 19.2 3.1 < 1 0.7 32 22.8 6.10.74 5 0.81 6.7 1.1 < 1 0.8 25 15 3.40.79 5.1 0.83 7.7 1.2 < 1 0.8 25 15.4 3.8170 851 87.9 167 155 43 < 0.1 150 760 584 1.636195 981 118 218 212 38 < 0.1 186 929 707 2.079.93 61.8 9.38 104 13.8 < 1 < 0.1 25 49.7 32.965.5 370 46.6 118 128 19 0.7 71 440 209 0.6441.49 9.5 1.44 10.1 2.9 < 1 0.7 34 18.2 5.91.78 10.6 1.54 9.1 3.5 < 1 0.6 55 17.7 5.6129 738 92 573 248 31 0.1 98 795 444 1.2783.68 21.9 2.9 29.6 9.1 < 1 0.8 58 25.8 11.6

APPENDIX C – ASSAY CERTIFICATES

Quality Analysis ... Innovative Technologies

Date Submitted: 06-Nov-14 Invoice No.: A14-08533 Invoice Date: 16-Dec-14 Your Reference: Alterra Resources P.O. Box 214 60 Bowater Avenue Port Hope Simpson NL A0K 4E0 Canada

ATTN: VP of Exploration Randy Miller (res2014)

CERTIFICATE OF ANALYSIS

4 Rock samples were submitted for analysis.

The following analytical package was requested: Code 8-REE Assay Package Major Elements Fusion ICP(WRA)/Trace Elements FusionICP/MS(WRA4B2)

REPORT A14-08533

This report may be reproduced without our consent. If only selected portions of the report are reproduced, permission must be obtained. If no instructions were given at time of sample submittal regarding excess material, it will be discarded within 90 days of this report. Our liability is limited solely to the analytical cost of these analyses. Test results are representative only of material submitted for analysis.

Notes:Total includes all elements in % oxide to the left of total. Footnote: Zr interference on Ag

CERTIFIED BY:

Emmanuel Eseme , Ph.D.Quality Control

ACTIVATION LABORATORIES LTD.

41 Bittern Street, Ancaster, Ontario, Canada, L9G 4V5 TELEPHONE +905 648-9611 or +1.888.228.5227 FAX +1.905.648.9613

E-MAIL [email protected] ACTLABS GROUP WEBSITE www.actlabs.com

Page 1/8

Activation Laboratories Ltd. Report: A14-08533

Results

Analyte Symbol SiO2 Al2O3 Fe2O3(T)

MnO MgO CaO Na2O K2O TiO2 P2O5 LOI Total Sc Be V Cr Co Ni Cu Zn Ga Ge As

Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507210 65.51 16.98 3.93 0.089 0.76 1.98 4.43 5.63 0.661 0.16 0.66 100.8 8 15 48 < 20 3 < 20 < 10 80 18 1 < 5507211 55.19 11.79 14.71 0.108 0.95 1.73 2.83 4.80 1.584 0.14 1.36 95.19 6 25 143 < 20 6 < 20 < 10 150 31 5 < 5507212 48.12 8.93 14.89 0.200 1.19 2.69 1.41 3.68 2.042 0.09 1.89 85.10 9 24 172 < 20 7 < 20 < 10 240 50 14 21507213 66.82 16.11 2.82 0.059 1.20 0.49 6.00 4.17 0.346 0.08 0.99 99.09 5 13 66 < 20 3 < 20 < 10 50 16 1 < 5

Page 2/8


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507210 160 430 174 779 154 < 2 2.4 < 0.2 12 < 0.5 2.8 1841 < 0.4 23.7 75.6 7.95 36.5 15.5 2.09 20.0 4.4 31.9 6.8507211 139 231 4559 22740 2 0.3 63 < 0.5 2.7 1023 < 0.4 428 1190 150 706 327 28.2 459 106 861 204507212 131 317 16130 30370 7 0.5 80 0.8 4.0 955 1.4 2320 5570 677 3000 1190 99.2 1720 405 3180 755507213 139 167 151 307 154 < 2 1.1 < 0.2 7 < 0.5 3.4 828 < 0.4 82.8 123 20.7 83.6 21.1 2.07 20.2 3.6 25.6 5.6

Page 3/8


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th U Nb2O5Unit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm %Lower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1 0.003Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-XR

F507210 21.8 3.22 18.3 2.30 27.1 12.9 < 1 0.4 75 19.2 9.0507211 703 104 585 73.4 757 195 43 0.4 215 596 479 1.061507212 2450 348 1830 212 768 490 235 0.5 510 2270 1660 3.529507213 17.6 2.50 14.0 1.80 13.2 10.3 < 1 0.4 49 27.1 7.6

Page 4/8


QC


MnO MgO CaO Na2O K2O TiO2 P2O5 Sc Be V Cr Co Ni Cu Zn Ga Ge As Rb Sr

Unit Symbol % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 1 1 5 20 1 20 10 30 1 1 5 2 2Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICPDH-1a MeasDH-1a CertNIST 694 Meas 11.36 1.89 0.73 0.013 0.33 42.68 0.88 0.54 0.114 30.21 1648NIST 694 Cert 11.2 1.80 0.790 0.0116 0.330 43.6 0.860 0.510 0.110 30.2 1740DNC-1 Meas 46.80 18.70 9.84 0.147 9.95 11.47 1.90 0.22 0.485 0.07 31 158 270 58 250 80 143DNC-1 Cert 47.15 18.34 9.97 0.150 10.13 11.49 1.890 0.234 0.480 0.070 31 148 270 57 247 70 144.0GBW 07113 Meas 70.73 12.94 3.19 0.140 0.14 0.60 2.50 5.44 0.278 0.05 5 4 5 42GBW 07113 Cert 72.8 13.0 3.21 0.140 0.160 0.590 2.57 5.43 0.300 0.0500 5.00 4.00 5.00 43.0LKSD-3 Meas 90 33 50 40 78LKSD-3 Cert 87.0 30.0 47.0 35.0 78.0OKA-2 MeasOKA-2 CertW-2a Meas 52.24 15.43 10.77 0.165 6.20 11.07 2.20 0.61 1.061 0.12 35 < 1 282 90 42 70 100 70 17 1 < 5 194W-2a Cert 52.4 15.4 10.7 0.163 6.37 10.9 2.14 0.626 1.06 0.130 36.0 1.30 262 92.0 43.0 70.0 110 80.0 17.0 1.00 1.20 190SY-4 Meas 50.06 20.44 6.23 0.108 0.50 8.20 6.92 1.64 0.284 0.13 1 3 10 1203SY-4 Cert 49.9 20.69 6.21 0.108 0.54 8.05 7.10 1.66 0.287 0.131 1.1 2.6 8.0 1191CTA-AC-1 MeasCTA-AC-1 CertBIR-1a Meas 47.62 15.66 11.27 0.171 9.42 13.49 1.79 0.02 0.942 0.02 43 < 1 341 370 52 170 70 17 107BIR-1a Cert 47.96 15.50 11.30 0.175 9.700 13.30 1.82 0.030 0.96 0.021 44 0.58 310 370 52 170 70 16 110NCS DC86312 MeasNCS DC86312 CertZW-C Meas 1050 101ZW-C Cert

1050.000 99

VS-N MeasVS-N CertNCS DC86316 MeasNCS DC86316 CertNCS DC70009(GBW07241) Meas

30 4 990 100 16 11 69 538

NCS DC70009(GBW07241) Cert

30 3.7 960 100 16.5 11.2 69.9 500

OREAS 100a(Fusion) Meas

18 170

OREAS 100a(Fusion) Cert

18.1 169


48 430


48.8 434

JR-1 Meas < 1 < 20 30 17 16 271JR-1 Cert 0.83 1.67 30.6 16.1 16.3 257NCS DC86318 MeasNCS DC86318 CertSX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 Meas

Page 5/8




Unit Symbol % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 1 1 5 20 1 20 10 30 1 1 5 2 2Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICPSARM 3 CertUSZ 42-2006 MeasUSZ 42-2006 CertMethod Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5 < 2Method Blank

QC

Analyte Symbol Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er TmUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05Method Code FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 16 36 0.9 103 5.3 0.60DNC-1 Cert 18.0 38 0.96 118 5.20 0.59GBW 07113 Meas 46 383 498GBW 07113 Cert 43.0 403 506LKSD-3 Meas < 2 2.9 49.5 93.0 46.4 7.9 1.55 0.9 4.7LKSD-3 Cert 2.00 2.70 52.0 90.0 44.0 8.00 1.50 1.00 4.90OKA-2 MeasOKA-2 CertW-2a Meas 19 89 8 < 2 < 0.5 172 < 0.4 23.2 12.6 3.2 1.06 0.6 3.7 0.7W-2a Cert 24.0 94.0 7.90 0.600 0.0460 182 0.0300 23.0 13.0 3.30 1.00 0.630 3.60 0.760SY-4 Meas 119 543 351SY-4 Cert 119 517 340CTA-AC-1 Meas 2300 3340 174 46.4 128CTA-AC-1 Cert 2176 3326 162 46.7 124BIR-1a Meas 15 15 7 2.6 0.55 2.1BIR-1a Cert 16 18 6 2.5 0.55 2.0NCS DC86312 Meas 2360 170 1590 225 34.6 183 35.5 95.5 14.9NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36 96.2 15.1ZW-C Meas 200ZW-C Cert 198VS-N MeasVS-N CertNCS DC86316 MeasNCS DC86316 CertNCS DC70009(GBW07241) Meas

1640 3.1 23.2 62.1 7.53 34.7 12.5 14.3 3.5 20.8 4.4 13.2 2.41


1701 3.1 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


270 464 47.4 25.8 3.79 23.7 4.0 24.1 15.5


260 463 47.1 23.6 3.71 23.6 3.80 23.2 14.9

OREAS 101a 25 826 1370 132 53.0 8.22 6.0 33.6 7.0 20.4 3.15

Page 6/8


Analyte Symbol Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er TmUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05Method Code FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS(Fusion) MeasOREAS 101a(Fusion) Cert

21.9 816 1396 134 48.8 8.06 5.92 33.3 6.46 19.5 2.90

JR-1 Meas 14 4 < 0.5 < 0.2 1.1 22.2 0.5 19.7 49.2 5.68 25.2 6.1 0.31 1.0 6.0 0.72JR-1 Cert 15.2 3.25 0.031 0.028 1.19 20.8 0.56 19.7 47.2 5.58 23.3 6.03 0.30 1.01 5.69 0.67NCS DC86318 Meas 1960 440 768 3220 1720 18.5 2100 457 3020 566 1770 276NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560 1750 270SX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 Meas 1040SARM 3 Cert 978USZ 42-2006 Meas 20800 28300 2340 6280 518 84.9USZ 42-2006 Cert 21100 27600 2300 6500 539 87.22Method Blank < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.05Method Blank

QC

Analyte Symbol Yb Lu Hf Ta W Tl Pb Th U Nb2O5Unit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm %Lower Limit 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1 0.003Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-XR

FDH-1a Meas 943 2530DH-1a Cert 910 2629NIST 694 MeasNIST 694 CertDNC-1 Meas 2.0DNC-1 Cert 2.0GBW 07113 MeasGBW 07113 CertLKSD-3 Meas 2.6 0.41 4.7 0.7 11.4 4.5LKSD-3 Cert 2.70 0.400 4.80 0.700 11.4 4.60OKA-2 Meas 28300OKA-2 Cert 28900.0

00W-2a Meas 2.0 2.3 0.5 < 1 < 0.1W-2a Cert 2.10 2.60 0.500 0.300 0.200SY-4 MeasSY-4 CertCTA-AC-1 Meas 11.7 1.14 4.1CTA-AC-1 Cert 11.4 1.08 4.4BIR-1a Meas 1.7 0.30 0.6BIR-1a Cert 1.7 0.3 0.60NCS DC86312 Meas 86.8 12.0 25.6NCS DC86312 Cert 87.79 11.96 23.6ZW-C Meas 85.4 330 34.3ZW-C Cert 82 320 34

Page 7/8



FVS-N Meas 0.102VS-N Cert 0.10NCS DC86316 Meas 697NCS DC86316 Cert 712NCS DC70009(GBW07241) Meas

16.0 2.31 2200 29.8


14.9 2.4 2200 28.3


2.30 52.0 134


2.26 51.6 135


2.56 38.0 422


2.66 36.6 422

JR-1 Meas 4.6 0.70 4.2 1.8 1.6 20 26.2 8.5JR-1 Cert 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1790 247NCS DC86318 Cert 1840 260.0SX18-01 Meas 0.696SX18-01 Cert 0.695SX18-04 Meas 1.322SX18-04 Cert 1.32SARM 3 Meas 0.147SARM 3 Cert 0.14USZ 42-2006 Meas 1610USZ 42-2006 Cert 1600Method Blank < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1Method Blank < 0.003

Powered by TCPDF (www.tcpdf.org)

Page 8/8







REPORT A14-08532



CERTIFIED BY:





Page 1/8


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507214 73.46 13.86 1.00 0.017 0.13 0.44 4.29 4.93 0.045 0.01 0.45 98.62 2 13 17 < 20 < 1 < 20 < 10 < 30 28 2 5507215 41.98 13.23 16.26 0.228 7.78 9.98 2.08 2.26 3.085 0.51 2.47 99.88 27 5 284 70 58 70 < 10 230 23 2 < 5507216 45.26 14.04 14.24 0.225 5.32 10.03 3.23 1.83 3.059 0.49 1.75 99.47 26 14 281 70 48 70 < 10 200 25 2 < 5507217 66.36 13.52 4.01 0.122 0.78 1.95 5.94 2.10 0.976 0.07 0.90 96.72 6 33 43 < 20 3 < 20 10 80 51 5 12507218 64.35 9.35 4.22 0.217 5.97 6.80 1.62 4.45 0.559 0.09 1.48 99.11 9 92 46 50 10 < 20 < 10 270 23 2 10507219 65.59 13.09 4.41 0.044 2.33 2.23 2.17 7.75 0.418 0.04 0.76 98.84 7 23 31 30 5 < 20 < 10 50 33 2 8507220 58.49 10.50 4.39 0.081 7.07 9.34 2.62 4.62 0.653 0.13 1.00 98.89 11 25 58 60 13 30 < 10 70 16 1 19507221 59.68 10.76 4.68 0.079 6.11 9.60 2.56 4.84 0.642 0.12 0.67 99.73 11 10 84 50 12 30 < 10 50 16 2 11507222 64.82 10.23 3.87 0.070 4.37 7.58 2.00 4.82 0.634 0.13 1.29 99.81 9 5 123 60 9 20 < 10 40 13 1 16

Page 2/8


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507214 199 76 46 73 73 < 2 0.6 < 0.2 2 < 0.5 5.7 199 < 0.4 8.4 22.6 3.07 13.9 4.1 0.58 4.4 0.9 6.6 1.6507215 81 187 42 257 9 3 0.8 < 0.2 2 0.7 4.6 409 0.6 23.1 53.9 7.54 35.0 8.9 2.48 8.9 1.3 8.0 1.6507216 146 211 129 345 108 3 1.0 < 0.2 8 1.2 6.6 293 1.2 28.4 65.7 9.59 46.3 15.4 3.17 18.6 3.5 24.0 5.2507217 71 143 3706 7655 < 2 0.3 61 1.1 1.8 288 1.9 508 1640 256 1290 519 39.2 591 126 861 186507218 250 134 268 226 160 < 2 1.1 0.2 46 3.0 6.5 482 0.8 41.4 112 14.8 64.0 18.8 2.02 22.1 4.4 30.4 7.0507219 355 149 103 185 111 < 2 0.6 0.2 64 2.3 4.9 644 0.5 16.3 48.2 6.06 26.9 9.0 0.90 9.6 1.9 13.8 3.1507220 181 191 36 295 34 < 2 0.9 < 0.2 5 3.1 4.8 559 < 0.4 27.0 80.0 7.28 29.1 6.4 1.10 6.0 1.0 5.9 1.3507221 157 222 33 249 22 < 2 0.7 < 0.2 3 2.2 4.3 539 < 0.4 30.4 65.2 8.00 31.9 6.7 1.15 5.6 1.0 5.4 1.2507222 131 209 32 245 72 < 2 1.1 < 0.2 3 3.2 3.5 586 0.6 29.1 59.6 7.46 29.8 6.3 1.16 5.2 0.9 5.2 1.1

Page 3/8


Results


F507214 5.7 0.93 7.2 1.12 4.4 10.0 < 1 0.8 56 28.2 14.0507215 4.6 0.64 3.9 0.63 5.9 0.5 3 0.5 36 2.4 3.6507216 16.7 2.44 14.6 1.89 9.3 7.5 3 0.7 53 12.9 13.7507217 585 84.7 471 56.0 227 511 46 0.3 381 1360 763 0.870507218 24.4 4.13 27.9 4.16 8.7 32.9 < 1 1.0 75 32.2 7.1507219 10.9 1.95 13.4 2.00 7.5 37.6 2 1.7 158 35.0 17.0507220 3.7 0.57 4.1 0.62 7.3 1.8 1 1.0 46 11.4 2.6507221 3.4 0.51 3.4 0.55 6.0 1.0 < 1 0.9 39 8.5 2.4507222 3.2 0.48 3.2 0.52 7.4 1.0 1 0.7 25 8.2 3.3

Page 4/8


QC



Unit Symbol % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 1 1 5 20 1 20 10 30 1 1 5 2 2Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICPDH-1a MeasDH-1a CertNIST 694 Meas 11.33 1.91 0.73 0.013 0.32 42.75 0.87 0.54 0.124 30.14 1664NIST 694 Cert 11.2 1.80 0.790 0.0116 0.330 43.6 0.860 0.510 0.110 30.2 1740DNC-1 Meas 47.26 18.17 9.55 0.144 9.67 11.48 1.87 0.24 0.494 0.12 31 157 270 56 250 100 80 143DNC-1 Cert 47.15 18.34 9.97 0.150 10.13 11.49 1.890 0.234 0.480 0.070 31 148 270 57 247 100 70 144.0GBW 07113 Meas 72.31 12.99 3.16 0.140 0.15 0.63 2.47 5.42 0.289 0.05 5 4 6 42GBW 07113 Cert 72.8 13.0 3.21 0.140 0.160 0.590 2.57 5.43 0.300 0.0500 5.00 4.00 5.00 43.0LKSD-3 Meas 90 29 50 30 25LKSD-3 Cert 87.0 30.0 47.0 35.0 27.0OKA-2 MeasOKA-2 CertW-2a Meas 52.23 15.09 10.45 0.166 6.20 11.10 2.17 0.62 1.075 0.15 35 < 1 279 80 39 70 80 17 1 < 5 196W-2a Cert 52.4 15.4 10.7 0.163 6.37 10.9 2.14 0.626 1.06 0.130 36.0 1.30 262 92.0 43.0 70.0 80.0 17.0 1.00 1.20 190SY-4 Meas 50.10 20.77 6.17 0.108 0.49 8.13 7.11 1.66 0.297 0.14 1 3 9 1197SY-4 Cert 49.9 20.69 6.21 0.108 0.54 8.05 7.10 1.66 0.287 0.131 1.1 2.6 8.0 1191CTA-AC-1 Meas 60 40CTA-AC-1 Cert 54.0 38.0BIR-1a Meas 47.81 15.95 11.23 0.174 9.61 13.42 1.74 0.02 0.982 0.03 43 < 1 336 380 52 180 130 16 111BIR-1a Cert 47.96 15.50 11.30 0.175 9.700 13.30 1.82 0.030 0.96 0.021 44 0.58 310 370 52 170 125 16 110NCS DC86312 MeasNCS DC86312 CertZW-C Meas 1030 100ZW-C Cert

1050.000 99

VS-N MeasVS-N CertNCS DC70009(GBW07241) Meas

970 100 17 10 65 499


960 100 16.5 11.2 69.9 500


19 170


18.1 169


50 440


48.8 434

JR-1 Meas < 20 < 10 30 17 16 244JR-1 Cert 1.67 2.68 30.6 16.1 16.3 257NCS DC86318 MeasNCS DC86318 CertSX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 MeasSARM 3 CertUSZ 42-2006 Meas

Page 5/8




Unit Symbol % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 1 1 5 20 1 20 10 30 1 1 5 2 2Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICPUSZ 42-2006 CertMethod Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5 < 2Method Blank

QC

Analyte Symbol Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er TmUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05Method Code FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 14 38 118 3.6 4.9 0.60DNC-1 Cert 18.0 38 118 3.6 5.20 0.59GBW 07113 Meas 43 383 494GBW 07113 Cert 43.0 403 506LKSD-3 Meas 2 2.7 2.3 50.0 88.5 43.8 7.9 1.41 4.7LKSD-3 Cert 2.00 2.70 2.30 52.0 90.0 44.0 8.00 1.50 4.90OKA-2 MeasOKA-2 CertW-2a Meas 18 87 < 2 0.7 173 < 0.4 10.1 21.7 0.94 3.4W-2a Cert 24.0 94.0 0.600 0.0460 182 0.0300 10.0 23.0 1.00 3.60SY-4 Meas 116 545 360SY-4 Cert 119 517 340CTA-AC-1 Meas 2330 3580 171 46.8 130 15.2CTA-AC-1 Cert 2176 3326 162 46.7 124 13.9BIR-1a Meas 13 15 < 1 0.6 8 2.4 1.1 0.51 1.9BIR-1a Cert 16 18 0.6 0.58 6 2.5 1.1 0.55 2.0NCS DC86312 Meas 2370 169 1600 235 33.7 187 35.8 100 14.1NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36 96.2 15.1ZW-C Meas 194 258ZW-C Cert 198 260VS-N MeasVS-N CertNCS DC70009(GBW07241) Meas

1700 2.9 41.4 23.3 57.3 7.94 31.1 12.3 15.1 3.2 20.8 4.3 13.5 2.31


1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


26 273 480 48.9 163 25.6 3.88 21.8 3.8 24.4 5.1 15.8 2.52


24.1 260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


22 819 1450 134 417 52.8 8.20 5.6 33.0 6.7 19.9 2.99


21.9 816 1396 134 403 48.8 8.06 5.92 33.3 6.46 19.5 2.90

JR-1 Meas 14 3 < 0.5 < 0.2 3 20.2 0.5 20.1 46.1 6.07 24.1 5.8 0.30 1.0 6.2 1.4 0.68JR-1 Cert 15.2 3.25 0.031 0.028 2.86 20.8 0.56 19.7 47.2 5.58 23.3 6.03 0.30 1.01 5.69 1.11 0.67NCS DC86318 Meas 1990 401 715 3190 1620 18.2 2200 448 2930 557 1720 265NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560 1750 270

Page 6/8


Analyte Symbol Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er TmUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05Method Code FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSSX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 Meas 1010SARM 3 Cert 978USZ 42-2006 Meas 21900 29700 2490 6590 533 88.1USZ 42-2006 Cert 21100 27600 2300 6500 539 87.22Method Blank < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.05Method Blank

QC


FDH-1a Meas 907 2570DH-1a Cert 910 2629NIST 694 MeasNIST 694 CertDNC-1 Meas 2.0DNC-1 Cert 2.0GBW 07113 MeasGBW 07113 CertLKSD-3 Meas 2.6 0.38 10.3 4.2LKSD-3 Cert 2.70 0.400 11.4 4.60OKA-2 Meas 28700OKA-2 Cert 28900.0

00W-2a Meas 0.5 < 1 < 0.1W-2a Cert 0.500 0.300 0.200SY-4 MeasSY-4 CertCTA-AC-1 Meas 10.9 1.15 23.9 4.0CTA-AC-1 Cert 11.4 1.08 21.8 4.4BIR-1a Meas 1.6 < 5BIR-1a Cert 1.7 3NCS DC86312 Meas 87.6 12.2 25.7NCS DC86312 Cert 87.79 11.96 23.6ZW-C Meas 83.1 331 34.3ZW-C Cert 82 320 34VS-N Meas 0.102VS-N Cert 0.10NCS DC70009(GBW07241) Meas

16.1 2.31 2230 30.0


14.9 2.4 2200 28.3

Page 7/8



FOREAS 100a(Fusion) Meas

16.2 2.33 54.1 141


14.9 2.26 51.6 135


19.0 2.66 37.4 432


17.5 2.66 36.6 422

JR-1 Meas 4.9 0.70 4.3 1.9 1.4 23 26.7 8.7JR-1 Cert 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1760 250NCS DC86318 Cert 1840 260.0SX18-01 Meas 0.696SX18-01 Cert 0.695SX18-04 Meas 1.322SX18-04 Cert 1.32SARM 3 Meas 0.147SARM 3 Cert 0.14USZ 42-2006 MeasUSZ 42-2006 CertMethod Blank < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1Method Blank < 0.003


Page 8/8







REPORT A14-08528



CERTIFIED BY:





Page 1/8


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507223 75.45 10.19 4.02 0.052 1.68 0.97 3.10 2.73 0.807 0.12 1.01 100.1 8 5 80 40 7 < 20 < 10 40 13 1 < 5507224 82.67 7.44 2.31 0.049 0.93 1.12 2.48 1.04 0.309 0.05 0.87 99.26 4 8 29 30 3 < 20 < 10 40 10 1 < 5507225 71.56 6.73 9.11 0.184 0.44 1.49 1.80 2.50 1.635 0.10 1.06 96.61 3 16 24 < 20 2 < 20 20 150 34 9 22507226 78.30 8.51 3.64 0.053 0.88 1.29 3.20 1.38 0.675 0.07 0.60 98.60 6 7 74 40 5 < 20 < 10 70 10 1 < 5

Page 2/8


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507223 101 74 37 419 16 < 2 0.7 < 0.2 4 < 0.5 5.2 577 < 0.4 20.0 48.0 6.31 25.6 6.2 0.92 5.3 0.8 5.4 1.1507224 42 83 196 540 102 < 2 1.2 < 0.2 6 < 0.5 2.2 230 0.8 40.2 105 13.9 62.5 20.3 1.80 22.4 4.2 29.6 6.5507225 85 145 8978 6698 < 2 0.6 130 1.7 2.4 263 2.3 589 1700 263 1480 789 66.9 1100 258 1950 446507226 59 93 175 363 51 < 2 < 0.5 < 0.2 6 < 0.5 1.6 308 < 0.4 49.4 125 16.1 65.6 16.5 1.65 15.5 2.6 18.1 3.9

Page 3/8


Results


F507223 3.5 0.50 3.4 0.58 10.9 1.8 < 1 0.4 33 9.1 3.3507224 21.3 3.21 19.2 2.49 15.1 9.6 < 1 0.1 45 30.6 14.8507225 1410 201 1090 123 166 651 32 0.4 582 1260 1250 1.875507226 12.8 1.91 11.7 1.65 10.2 2.1 < 1 0.1 58 16.8 5.2

Page 4/8


QC



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 Meas 11.36 1.89 0.73 0.013 0.33 42.68 0.88 0.54 0.114 30.21 1648NIST 694 Cert 11.2 1.80 0.790 0.0116 0.330 43.6 0.860 0.510 0.110 30.2 1740DNC-1 Meas 46.80 18.70 9.84 0.147 9.95 11.47 1.90 0.22 0.485 0.07 31 158 270 58 250 80DNC-1 Cert 47.15 18.34 9.97 0.150 10.13 11.49 1.890 0.234 0.480 0.070 31 148 270 57 247 70GBW 07113 Meas 70.73 12.94 3.19 0.140 0.14 0.60 2.50 5.44 0.278 0.05 5 4 5GBW 07113 Cert 72.8 13.0 3.21 0.140 0.160 0.590 2.57 5.43 0.300 0.0500 5.00 4.00 5.00LKSD-3 Meas 90 33 50 40LKSD-3 Cert 87.0 30.0 47.0 35.0OKA-2 MeasOKA-2 CertW-2a Meas 52.24 15.43 10.77 0.165 6.20 11.07 2.20 0.61 1.061 0.12 35 < 1 282 90 42 70 100 70 17 1 < 5W-2a Cert 52.4 15.4 10.7 0.163 6.37 10.9 2.14 0.626 1.06 0.130 36.0 1.30 262 92.0 43.0 70.0 110 80.0 17.0 1.00 1.20SY-4 Meas 50.06 20.44 6.23 0.108 0.50 8.20 6.92 1.64 0.284 0.13 1 3 10SY-4 Cert 49.9 20.69 6.21 0.108 0.54 8.05 7.10 1.66 0.287 0.131 1.1 2.6 8.0CTA-AC-1 MeasCTA-AC-1 CertBIR-1a Meas 47.62 15.66 11.27 0.171 9.42 13.49 1.79 0.02 0.942 0.02 43 < 1 341 370 52 170 70 17BIR-1a Cert 47.96 15.50 11.30 0.175 9.700 13.30 1.82 0.030 0.96 0.021 44 0.58 310 370 52 170 70 16NCS DC86312 MeasNCS DC86312 CertZW-C Meas 1050 101ZW-C Cert

1050.000 99


30 4 990 100 16 11 69


30 3.7 960 100 16.5 11.2 69.9


18 170


18.1 169


48 430


48.8 434

JR-1 Meas < 1 < 20 30 17 16JR-1 Cert 0.83 1.67 30.6 16.1 16.3NCS DC86318 MeasNCS DC86318 CertSX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 Meas

Page 5/8




Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSSARM 3 CertUSZ 42-2006 MeasUSZ 42-2006 Cert507226 Orig 78.43 8.52 3.57 0.053 0.88 1.29 3.19 1.39 0.670 0.07 0.60 98.67 6 7 75 30 5 < 20 < 10 70 10 1 < 5507226 Dup 78.16 8.51 3.71 0.053 0.88 1.28 3.20 1.38 0.680 0.08 0.60 98.53 6 7 74 40 5 < 20 < 10 70 10 1 < 5Method Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5Method Blank

QC

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 143 16 36 0.9 103 5.3 0.60DNC-1 Cert 144.0 18.0 38 0.96 118 5.20 0.59GBW 07113 Meas 42 46 383 498GBW 07113 Cert 43.0 43.0 403 506LKSD-3 Meas 78 < 2 2.9 49.5 93.0 46.4 7.9 1.55 0.9 4.7LKSD-3 Cert 78.0 2.00 2.70 52.0 90.0 44.0 8.00 1.50 1.00 4.90OKA-2 MeasOKA-2 CertW-2a Meas 194 19 89 8 < 2 < 0.5 172 < 0.4 23.2 12.6 3.2 1.06 0.6 3.7 0.7W-2a Cert 190 24.0 94.0 7.90 0.600 0.0460 182 0.0300 23.0 13.0 3.30 1.00 0.630 3.60 0.760SY-4 Meas 1203 119 543 351SY-4 Cert 1191 119 517 340CTA-AC-1 Meas 2300 3340 174 46.4 128CTA-AC-1 Cert 2176 3326 162 46.7 124BIR-1a Meas 107 15 15 7 2.6 0.55 2.1BIR-1a Cert 110 16 18 6 2.5 0.55 2.0NCS DC86312 Meas 2360 170 1590 225 34.6 183 35.5NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36ZW-C Meas 200ZW-C Cert 198VS-N MeasVS-N CertNCS DC86316 MeasNCS DC86316 CertNCS DC70009(GBW07241) Meas

538 1640 3.1 23.2 62.1 7.53 34.7 12.5 14.3 3.5 20.8 4.4


500 1701 3.1 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5


270 464 47.4 25.8 3.79 23.7 4.0 24.1

OREAS 100a 260 463 47.1 23.6 3.71 23.6 3.80 23.2

Page 6/8


Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS(Fusion) CertOREAS 101a(Fusion) Meas

25 826 1370 132 53.0 8.22 6.0 33.6 7.0


21.9 816 1396 134 48.8 8.06 5.92 33.3 6.46

JR-1 Meas 271 14 4 < 0.5 < 0.2 1.1 22.2 0.5 19.7 49.2 5.68 25.2 6.1 0.31 1.0 6.0JR-1 Cert 257 15.2 3.25 0.031 0.028 1.19 20.8 0.56 19.7 47.2 5.58 23.3 6.03 0.30 1.01 5.69NCS DC86318 Meas 1960 440 768 3220 1720 18.5 2100 457 3020 566NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560SX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 Meas 1040SARM 3 Cert 978USZ 42-2006 Meas 20800 28300 2340 6280 518 84.9USZ 42-2006 Cert 21100 27600 2300 6500 539 87.22507226 Orig 59 93 177 365 63 < 2 0.6 < 0.2 6 < 0.5 1.6 307 < 0.4 48.3 122 15.9 64.8 16.5 1.67 15.6 2.6 18.4 4.0507226 Dup 58 92 173 361 39 < 2 < 0.5 < 0.2 6 < 0.5 1.6 308 < 0.4 50.6 128 16.3 66.4 16.5 1.63 15.5 2.6 17.7 3.9Method Blank < 2 < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1Method Blank

QC



00W-2a Meas 2.0 2.3 0.5 < 1 < 0.1W-2a Cert 2.10 2.60 0.500 0.300 0.200SY-4 MeasSY-4 CertCTA-AC-1 Meas 11.7 1.14 4.1CTA-AC-1 Cert 11.4 1.08 4.4BIR-1a Meas 1.7 0.30 0.6BIR-1a Cert 1.7 0.3 0.60

Page 7/8



FNCS DC86312 Meas 95.5 14.9 86.8 12.0 25.6NCS DC86312 Cert 96.2 15.1 87.79 11.96 23.6ZW-C Meas 85.4 330 34.3ZW-C Cert 82 320 34VS-N Meas 0.102VS-N Cert 0.10NCS DC86316 Meas 697NCS DC86316 Cert 712NCS DC70009(GBW07241) Meas

13.2 2.41 16.0 2.31 2200 29.8


13.4 2.2 14.9 2.4 2200 28.3


15.5 2.30 52.0 134


14.9 2.26 51.6 135


20.4 3.15 2.56 38.0 422


19.5 2.90 2.66 36.6 422

JR-1 Meas 0.72 4.6 0.70 4.2 1.8 1.6 20 26.2 8.5JR-1 Cert 0.67 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1770 276 1790 247NCS DC86318 Cert 1750 270 1840 260.0SX18-01 Meas 0.696SX18-01 Cert 0.695SX18-04 Meas 1.322SX18-04 Cert 1.32SARM 3 Meas 0.147SARM 3 Cert 0.14USZ 42-2006 Meas 1610USZ 42-2006 Cert 1600507226 Orig 13.1 1.94 11.8 1.65 10.6 2.1 < 1 0.1 59 16.8 5.3507226 Dup 12.6 1.87 11.5 1.64 9.8 2.0 < 1 0.1 58 16.9 5.1Method Blank < 0.1 < 0.05 < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1Method Blank < 0.003


Page 8/8







REPORT A14-08527


Notes:Total includes all elements in % oxide to the left of total.

CERTIFIED BY:





Page 1/8


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507227 48.73 12.08 16.87 0.245 6.93 4.37 3.63 3.08 2.317 0.37 1.73 100.4 19 24 211 50 48 70 10 220 20 2 < 5507228 59.88 5.93 24.96 0.275 1.23 1.63 2.79 0.68 0.982 0.05 0.69 99.08 25 48 131 < 20 8 < 20 < 10 340 29 7 8507229 52.64 13.43 13.32 0.262 4.64 3.75 5.35 2.55 2.120 0.32 1.21 99.58 19 41 177 50 35 60 < 10 330 25 2 < 5507230 77.20 8.09 2.39 0.072 1.44 2.91 2.63 3.09 0.466 0.09 1.20 99.57 4 15 43 30 5 < 20 < 10 70 14 1 < 5

Page 2/8


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507227 369 207 363 290 668 < 2 0.5 0.3 45 < 0.5 14.8 417 1.0 32.9 88.0 13.8 74.8 35.9 4.21 47.3 10.5 81.7 18.8507228 54 62 2762 389 < 2 1.0 1.7 255 < 0.5 4.3 69 0.9 205 573 89.4 476 249 21.2 362 82.4 663 151507229 356 158 272 380 189 < 2 0.9 0.2 34 < 0.5 12.6 221 0.8 38.3 109 15.9 71.5 23.6 3.08 26.1 5.3 38.2 8.8507230 159 113 283 336 277 < 2 < 0.5 < 0.2 8 < 0.5 2.5 493 < 0.4 65.4 179 25.8 115 38.6 3.32 41.0 8.2 56.4 12.2

Page 3/8


Results


F507227 61.9 9.12 52.0 6.34 10.8 39.4 2 1.7 84 65.0 64.2507228 495 72.9 404 47.2 24.1 235 14 0.2 196 472 428 0.663507229 29.3 4.71 28.7 4.01 16.9 18.5 < 1 1.4 64 38.1 9.2507230 38.9 5.62 32.7 3.85 10.8 23.5 1 0.6 72 74.0 30.0

Page 4/8


QC




1050.000 99


30 4 990 100 16 11 69 538


30 3.7 960 100 16.5 11.2 69.9 500


18 170


18.1 169


48 430


48.8 434


Page 5/8





QC


1640 3.1 23.2 62.1 7.53 34.7 12.5 14.3 3.5 20.8 4.4 13.2 2.41


1701 3.1 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


270 464 47.4 25.8 3.79 23.7 4.0 24.1 15.5


260 463 47.1 23.6 3.71 23.6 3.80 23.2 14.9

OREAS 101a 25 826 1370 132 53.0 8.22 6.0 33.6 7.0 20.4 3.15

Page 6/8



21.9 816 1396 134 48.8 8.06 5.92 33.3 6.46 19.5 2.90


QC




Page 7/8




16.0 2.31 2200 29.8


14.9 2.4 2200 28.3


2.30 52.0 134


2.26 51.6 135


2.56 38.0 422


2.66 36.6 422



Page 8/8







REPORT A14-08525



CERTIFIED BY:





Page 1/8


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507231 83.18 6.58 1.64 0.030 0.45 1.10 1.26 3.72 0.357 0.08 0.40 98.80 3 6 21 20 2 < 20 < 10 < 30 9 < 1 < 5507232 77.04 5.74 9.63 0.107 0.22 0.66 2.46 0.99 0.619 0.05 0.44 97.95 4 15 16 < 20 < 1 < 20 < 10 90 23 4 6507233 82.21 9.88 1.17 0.012 0.03 0.11 5.47 1.25 0.116 0.02 0.11 100.4 < 1 8 < 5 30 < 1 < 20 < 10 < 30 35 2 < 5507234 90.21 3.83 3.39 0.043 0.10 0.25 1.91 0.38 0.184 0.04 0.18 100.5 2 8 6 20 < 1 < 20 < 10 40 16 2 < 5507235 80.59 10.34 1.77 0.019 0.09 0.35 3.38 4.08 0.105 0.02 0.19 100.9 < 1 9 7 < 20 < 1 < 20 < 10 < 30 30 2 < 5507236 78.00 10.77 2.44 0.035 0.05 0.26 4.42 2.71 0.195 < 0.01 0.16 99.04 < 1 14 5 < 20 < 1 < 20 < 10 < 30 30 2 < 5507237 84.68 5.01 1.48 0.028 0.59 1.68 0.84 3.07 0.230 0.07 0.77 98.44 3 2 23 30 2 < 20 < 10 < 30 6 < 1 < 5

Page 2/8


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507231 129 61 144 909 142 < 2 4.1 < 0.2 9 < 0.5 2.2 448 < 0.4 22.5 56.1 8.47 38.0 13.5 1.46 14.5 3.1 22.8 5.3507232 31 42 1727 4042 < 2 0.6 100 < 0.5 0.8 76 < 0.4 215 693 121 663 302 22.9 360 73.9 532 113507233 50 23 220 463 276 < 2 1.1 < 0.2 8 < 0.5 1.6 68 < 0.4 64.6 150 20.7 94.6 35.7 2.61 39.8 8.5 59.3 12.9507234 15 17 414 5205 552 < 2 < 0.2 27 < 0.5 < 0.5 37 < 0.4 162 434 64.0 309 103 7.09 96.4 17.4 111 21.9507235 176 52 148 1271 179 < 2 < 0.2 14 < 0.5 2.9 271 < 0.4 18.5 53.5 9.09 49.1 22.4 1.69 25.1 5.3 37.0 8.1507236 107 49 445 311 575 < 2 0.5 < 0.2 22 < 0.5 1.2 170 < 0.4 338 727 90.6 360 98.8 6.52 96.9 18.6 130 27.1507237 100 50 30 183 18 < 2 < 0.5 < 0.2 2 < 0.5 1.5 405 < 0.4 20.2 36.3 5.83 23.2 5.3 0.79 4.4 0.7 4.9 1.0

Page 3/8


Results


F507231 19.4 3.55 24.5 3.61 43.2 15.2 < 1 0.6 42 75.0 15.2507232 337 44.8 231 26.3 115 158 7 0.1 144 391 265 0.464507233 38.2 5.17 26.4 2.94 10.3 21.9 < 1 0.2 34 41.4 40.3507234 64.6 9.20 53.1 7.23 100 44.5 2 < 0.1 38 139 69.7507235 25.6 3.65 20.6 2.57 26.0 14.3 < 1 0.7 33 26.5 21.8507236 82.3 11.1 55.9 6.38 10.2 38.8 2 0.3 62 83.1 54.7507237 3.1 0.45 3.1 0.47 4.9 0.9 < 1 0.4 19 7.9 1.9

Page 4/8


QC




1050.000 99


30 4 990 100 16 11 69 538


30 3.7 960 100 16.5 11.2 69.9 500


18 170


18.1 169


48 430


48.8 434


Page 5/8





QC


1640 3.1 23.2 62.1 7.53 34.7 12.5 14.3 3.5 20.8 4.4 13.2 2.41


1701 3.1 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


270 464 47.4 25.8 3.79 23.7 4.0 24.1 15.5


260 463 47.1 23.6 3.71 23.6 3.80 23.2 14.9

OREAS 101a 25 826 1370 132 53.0 8.22 6.0 33.6 7.0 20.4 3.15

Page 6/8



21.9 816 1396 134 48.8 8.06 5.92 33.3 6.46 19.5 2.90


QC




Page 7/8




16.0 2.31 2200 29.8


14.9 2.4 2200 28.3


2.30 52.0 134


2.26 51.6 135


2.56 38.0 422


2.66 36.6 422



Page 8/8







REPORT A14-08524



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507238 74.11 14.52 1.57 0.014 0.11 1.19 6.98 1.05 0.195 < 0.01 0.41 100.2 1 77 15 < 20 1 < 20 < 10 < 30 49 3 < 5507239 70.91 14.86 1.97 0.013 0.07 0.62 7.28 1.81 0.171 0.03 0.30 98.05 < 1 49 13 < 20 < 1 < 20 < 10 < 30 58 3 < 5507240 75.18 13.94 2.40 0.017 0.13 1.07 6.58 0.92 0.222 0.02 0.31 100.8 1 69 27 < 20 2 < 20 < 10 < 30 45 2 < 5507241 54.07 14.32 10.13 0.208 5.59 6.85 4.43 1.40 1.348 0.16 1.41 99.91 21 50 172 60 42 60 < 10 150 30 2 < 5507242 67.37 16.88 2.13 0.035 0.93 2.07 6.87 1.17 0.272 0.05 0.83 98.62 4 160 34 < 20 8 < 20 < 10 40 58 2 < 5507243 48.64 14.81 13.89 0.184 5.58 6.92 4.54 1.19 1.987 0.26 1.33 99.33 30 54 248 50 50 50 < 10 140 27 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507238 33 165 655 1485 616 < 2 < 0.2 37 < 0.5 < 0.5 76 < 0.4 28.1 92.5 13.4 61.6 24.2 1.98 30.3 7.6 57.2 14.3507239 66 119 742 2904 1090 < 2 < 0.2 50 < 0.5 0.5 80 < 0.4 40.8 139 21.2 98.3 39.9 3.30 49.9 12.6 96.7 23.7507240 27 157 549 1168 725 < 2 < 0.2 42 < 0.5 < 0.5 71 < 0.4 26.5 93.9 13.5 64.4 27.5 2.24 34.4 8.8 68.1 16.8507241 90 229 75 316 100 < 2 1.2 < 0.2 11 0.9 3.9 139 1.3 13.4 37.9 4.84 20.2 5.6 1.23 6.2 1.3 8.9 2.0507242 83 298 73 136 103 < 2 < 0.5 < 0.2 12 < 0.5 4.0 178 < 0.4 48.8 133 16.7 52.8 7.9 0.66 4.2 0.7 4.7 1.0507243 65 268 39 168 31 < 2 < 0.5 < 0.2 8 0.6 3.4 185 0.9 10.0 29.0 3.95 18.6 5.3 1.72 6.1 1.1 6.4 1.3

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507238 57.8 12.3 95.6 15.3 65.9 75.3 17 < 0.1 127 175 28.9507239 95.4 19.8 154 23.9 165 88.1 7 0.2 151 323 43.8507240 65.9 13.5 102 15.2 62.4 66.6 6 < 0.1 99 187 30.4507241 7.4 1.46 11.4 1.82 17.3 13.1 1 0.4 52 21.1 7.3507242 4.2 0.99 9.5 1.70 16.6 111 7 0.3 94 51.6 88.6507243 4.1 0.63 4.5 0.78 5.3 17.0 < 1 0.3 41 4.7 10.0

Page 4/7


QC



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 Meas 10.87 1.93 0.75 0.012 0.33 42.74 0.87 0.55 0.120 30.09 1668NIST 694 Cert 11.2 1.80 0.790 0.0116 0.330 43.6 0.860 0.510 0.110 30.2 1740DNC-1 Meas 46.72 18.56 9.81 0.147 10.01 11.43 1.88 0.23 0.489 0.11 31 155 60 250 80DNC-1 Cert 47.15 18.34 9.97 0.150 10.13 11.49 1.890 0.234 0.480 0.070 31 148 57 247 70LKSD-3 Meas 90 31 50 26LKSD-3 Cert 87.0 30.0 47.0 27.0OKA-2 MeasOKA-2 CertW-2a Meas 52.71 15.43 10.57 0.165 6.27 11.12 2.19 0.62 1.084 0.17 35 < 1 279 100 43 70 110 80 18 1W-2a Cert 52.4 15.4 10.7 0.163 6.37 10.9 2.14 0.626 1.06 0.130 36.0 1.30 262 92.0 43.0 70.0 110 80.0 17.0 1.00SY-4 Meas 49.84 20.53 6.22 0.107 0.49 8.13 6.98 1.65 0.293 0.15 1 3 8SY-4 Cert 49.9 20.69 6.21 0.108 0.54 8.05 7.10 1.66 0.287 0.131 1.1 2.6 8.0CTA-AC-1 Meas 40CTA-AC-1 Cert 38.0BIR-1a Meas 47.38 16.00 11.29 0.174 9.49 13.48 1.79 0.02 0.984 0.03 43 < 1 336 54 170 70 16BIR-1a Cert 47.96 15.50 11.30 0.175 9.700 13.30 1.82 0.030 0.96 0.021 44 0.58 310 52 170 70 16NCS DC86312 MeasNCS DC86312 CertZW-C Meas 1030 97ZW-C Cert

1050.000 99

NCS DC70009(GBW07241) Meas

30 990 100 16 11 70


30 960 100 16.5 11.2 69.9


19 170


18.1 169

JR-1 Meas < 20 30 16 16JR-1 Cert 1.67 30.6 16.1 16.3NCS DC86318 MeasNCS DC86318 Cert507243 Orig 48.86 14.91 13.94 0.186 5.59 6.99 4.52 1.20 1.963 0.26 1.33 99.74 30 54 250 50 50 50 < 10 140 27 2 < 5507243 Dup 48.43 14.70 13.84 0.183 5.57 6.85 4.55 1.19 2.012 0.26 1.33 98.92 30 54 245 50 50 50 < 10 140 27 2 < 5Method Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5

QC

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 146 16 36 109 3.7 0.60

Page 5/7


Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDNC-1 Cert 144.0 18.0 38 118 3.6 0.59LKSD-3 Meas 72 2 2.1 49.8 90.9 43.6 7.6 1.47 4.8LKSD-3 Cert 78.0 2.00 2.30 52.0 90.0 44.0 8.00 1.50 4.90OKA-2 MeasOKA-2 CertW-2a Meas 19 199 20 88 8 < 2 < 0.5 172 < 0.4 10.8 23.0 12.4 3.1 1.03 3.7 0.7W-2a Cert 21.0 190 24.0 94.0 7.90 0.600 0.0460 182 0.0300 10.0 23.0 13.0 3.30 1.00 3.60 0.760SY-4 Meas 1193 117 524 354SY-4 Cert 1191 119 517 340CTA-AC-1 Meas 2380 3570 177 48.0 130 15.0CTA-AC-1 Cert 2176 3326 162 46.7 124 13.9BIR-1a Meas 113 16 15 8 0.7 2.4 0.55 1.8BIR-1a Cert 110 16 18 6 0.63 2.5 0.55 2.0NCS DC86312 Meas 2460 177 1630 237 33.8 183 36.3NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36ZW-C Meas 191 253ZW-C Cert 198 260NCS DC70009(GBW07241) Meas

540 1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4


500 1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81

JR-1 Meas 256 15 4 0.8 < 0.2 3 1.2 21.0 20.7 47.7 5.88 23.9 5.8 0.28 6.1 1.2JR-1 Cert 257 15.2 3.25 0.031 0.028 2.86 1.19 20.8 19.7 47.2 5.58 23.3 6.03 0.30 5.69 1.11NCS DC86318 Meas 1940 401 721 3200 1640 18.5 2160 482 3110 551NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560507243 Orig 65 270 38 169 33 < 2 < 0.5 < 0.2 8 0.6 3.5 184 0.9 10.1 29.3 3.96 18.7 5.3 1.72 6.1 1.1 6.5 1.3507243 Dup 65 266 41 167 30 < 2 < 0.5 < 0.2 8 0.6 3.4 186 0.9 9.9 28.7 3.95 18.6 5.3 1.73 6.1 1.1 6.4 1.3Method Blank < 2 < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1

QC

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a Meas 919 2650DH-1a Cert 910 2629NIST 694 MeasNIST 694 CertDNC-1 Meas 2.0DNC-1 Cert 2.0LKSD-3 Meas 2.6 0.6 11.2 4.7LKSD-3 Cert 2.70 0.700 11.4 4.60OKA-2 Meas 30600OKA-2 Cert 28900.0

00

Page 6/7


Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSW-2a Meas 1.9 2.4 0.5 < 1 < 0.1 2.3 0.5W-2a Cert 2.10 2.60 0.500 0.300 0.200 2.40 0.530SY-4 MeasSY-4 CertCTA-AC-1 Meas 11.2 1.11 22.9 4.5CTA-AC-1 Cert 11.4 1.08 21.8 4.4BIR-1a Meas 1.7 0.6BIR-1a Cert 1.7 0.60NCS DC86312 Meas 95.9 14.5 89.4 12.0 24.5NCS DC86312 Cert 96.2 15.1 87.79 11.96 23.6ZW-C Meas 82.7 329 33.7ZW-C Cert 82 320 34NCS DC70009(GBW07241) Meas

13.2 2.36 16.3 2.35 2300 30.2


13.4 2.2 14.9 2.4 2200 28.3


14.9 2.49 15.8 2.27 54.2 136


14.9 2.31 14.9 2.26 51.6 135

JR-1 Meas 3.9 0.64 4.8 0.66 4.5 1.8 1.3 22 26.0 9.6JR-1 Cert 3.61 0.67 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1710 260 1730 256NCS DC86318 Cert 1750 270 1840 260.0507243 Orig 4.1 0.63 4.6 0.79 5.6 17.0 < 1 0.3 41 4.7 9.9507243 Dup 4.1 0.63 4.4 0.77 5.0 17.0 < 1 0.3 41 4.6 10.0Method Blank < 0.1 < 0.05 < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1


Page 7/7







REPORT A14-08523



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507244 40.65 4.05 7.85 0.206 1.38 7.03 0.28 1.40 6.834 0.32 1.93 71.94 4 2 132 < 20 7 < 20 20 120 36 15 32

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 2 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507244 93 122 24670 78650 4 1.0 279 1.1 3.2 306 3.6 432 2220 517 3310 1820 155 2740 671 5000 1140

Page 3/7


Results


F507244 3690 541 3030 331 2500 1000 170 0.4 687 2490 2200 4.475

Page 4/7


QC



Unit Symbol % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 1 1 5 20 1 20 10 30 1 1 5 2 2Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICPDH-1a MeasDH-1a CertNIST 694 Meas 10.87 1.93 0.75 0.012 0.33 42.74 0.87 0.55 0.120 30.09 1668NIST 694 Cert 11.2 1.80 0.790 0.0116 0.330 43.6 0.860 0.510 0.110 30.2 1740DNC-1 Meas 46.72 18.56 9.81 0.147 10.01 11.43 1.88 0.23 0.489 0.11 31 155 60 250 80 146DNC-1 Cert 47.15 18.34 9.97 0.150 10.13 11.49 1.890 0.234 0.480 0.070 31 148 57 247 70 144.0LKSD-3 Meas 90 31 50 26 72LKSD-3 Cert 87.0 30.0 47.0 27.0 78.0OKA-2 MeasOKA-2 CertW-2a Meas 52.71 15.43 10.57 0.165 6.27 11.12 2.19 0.62 1.084 0.17 35 < 1 279 100 43 70 110 80 18 1 19 199W-2a Cert 52.4 15.4 10.7 0.163 6.37 10.9 2.14 0.626 1.06 0.130 36.0 1.30 262 92.0 43.0 70.0 110 80.0 17.0 1.00 21.0 190SY-4 Meas 49.84 20.53 6.22 0.107 0.49 8.13 6.98 1.65 0.293 0.15 1 3 8 1193SY-4 Cert 49.9 20.69 6.21 0.108 0.54 8.05 7.10 1.66 0.287 0.131 1.1 2.6 8.0 1191CTA-AC-1 Meas 40CTA-AC-1 Cert 38.0BIR-1a Meas 47.38 16.00 11.29 0.174 9.49 13.48 1.79 0.02 0.984 0.03 43 < 1 336 54 170 70 16 113BIR-1a Cert 47.96 15.50 11.30 0.175 9.700 13.30 1.82 0.030 0.96 0.021 44 0.58 310 52 170 70 16 110NCS DC86312 MeasNCS DC86312 CertZW-C Meas 1030 97ZW-C Cert

1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169

JR-1 Meas < 20 30 16 16 256JR-1 Cert 1.67 30.6 16.1 16.3 257NCS DC86318 MeasNCS DC86318 CertSX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 MeasSARM 3 CertMethod Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5 < 2Method Blank

QC

Page 5/7


Analyte Symbol Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er TmUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05Method Code FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 16 36 109 3.7 0.60DNC-1 Cert 18.0 38 118 3.6 0.59LKSD-3 Meas 2 2.1 49.8 90.9 43.6 7.6 1.47 4.8LKSD-3 Cert 2.00 2.30 52.0 90.0 44.0 8.00 1.50 4.90OKA-2 MeasOKA-2 CertW-2a Meas 20 88 8 < 2 < 0.5 172 < 0.4 10.8 23.0 12.4 3.1 1.03 3.7 0.7W-2a Cert 24.0 94.0 7.90 0.600 0.0460 182 0.0300 10.0 23.0 13.0 3.30 1.00 3.60 0.760SY-4 Meas 117 524 354SY-4 Cert 119 517 340CTA-AC-1 Meas 2380 3570 177 48.0 130 15.0CTA-AC-1 Cert 2176 3326 162 46.7 124 13.9BIR-1a Meas 16 15 8 0.7 2.4 0.55 1.8BIR-1a Cert 16 18 6 0.63 2.5 0.55 2.0NCS DC86312 Meas 2460 177 1630 237 33.8 183 36.3 95.9 14.5NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36 96.2 15.1ZW-C Meas 191 253ZW-C Cert 198 260VS-N MeasVS-N CertNCS DC70009(GBW07241) Meas

1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31

JR-1 Meas 15 4 0.8 < 0.2 3 1.2 21.0 20.7 47.7 5.88 23.9 5.8 0.28 6.1 1.2 3.9 0.64JR-1 Cert 15.2 3.25 0.031 0.028 2.86 1.19 20.8 19.7 47.2 5.58 23.3 6.03 0.30 5.69 1.11 3.61 0.67NCS DC86318 Meas 1940 401 721 3200 1640 18.5 2160 482 3110 551 1710 260NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560 1750 270SX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 MeasSARM 3 CertMethod Blank < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.05Method Blank

QC

Page 6/7



FDH-1a Meas 919 2650DH-1a Cert 910 2629NIST 694 MeasNIST 694 CertDNC-1 Meas 2.0DNC-1 Cert 2.0LKSD-3 Meas 2.6 0.6 11.2 4.7LKSD-3 Cert 2.70 0.700 11.4 4.60OKA-2 Meas 30600OKA-2 Cert 28900.0

00W-2a Meas 1.9 2.4 0.5 < 1 < 0.1 2.3 0.5W-2a Cert 2.10 2.60 0.500 0.300 0.200 2.40 0.530SY-4 MeasSY-4 CertCTA-AC-1 Meas 11.2 1.11 22.9 4.5CTA-AC-1 Cert 11.4 1.08 21.8 4.4BIR-1a Meas 1.7 0.6BIR-1a Cert 1.7 0.60NCS DC86312 Meas 89.4 12.0 24.5NCS DC86312 Cert 87.79 11.96 23.6ZW-C Meas 82.7 329 33.7ZW-C Cert 82 320 34VS-N Meas 0.102VS-N Cert 0.10NCS DC70009(GBW07241) Meas

16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135

JR-1 Meas 4.8 0.66 4.5 1.8 1.3 22 26.0 9.6JR-1 Cert 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1730 256NCS DC86318 Cert 1840 260.0SX18-01 Meas 0.696SX18-01 Cert 0.695SX18-04 Meas 1.322SX18-04 Cert 1.32SARM 3 Meas 0.147SARM 3 Cert 0.14Method Blank < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1Method Blank < 0.003


Page 7/7







REPORT A14-08522



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507245 72.99 13.10 1.62 0.025 0.26 0.46 3.63 5.79 0.307 0.04 0.41 98.64 4 4 18 < 20 1 < 20 < 10 < 30 12 < 1 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507245 184 79 36 233 40 < 2 < 0.5 < 0.2 2 < 0.5 1.8 401 < 0.4 20.5 52.7 5.10 17.5 4.1 0.37 3.6 0.7 5.1 1.0

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507245 3.6 0.57 3.6 0.58 5.3 2.0 < 1 0.9 15 19.7 3.1

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169

JR-1 Meas < 20 30 16 16 256JR-1 Cert 1.67 30.6 16.1 16.3 257NCS DC86318 MeasNCS DC86318 CertMethod Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5 < 2

QC

Analyte Symbol Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er TmUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05Method Code FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 16 36 109 3.7 0.60DNC-1 Cert 18.0 38 118 3.6 0.59LKSD-3 Meas 2 2.1 49.8 90.9 43.6 7.6 1.47 4.8

Page 5/7


Analyte Symbol Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er TmUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.1 0.05Method Code FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSLKSD-3 Cert 2.00 2.30 52.0 90.0 44.0 8.00 1.50 4.90OKA-2 MeasOKA-2 CertW-2a Meas 20 88 8 < 2 < 0.5 172 < 0.4 10.8 23.0 12.4 3.1 1.03 3.7 0.7W-2a Cert 24.0 94.0 7.90 0.600 0.0460 182 0.0300 10.0 23.0 13.0 3.30 1.00 3.60 0.760SY-4 Meas 117 524 354SY-4 Cert 119 517 340CTA-AC-1 Meas 2380 3570 177 48.0 130 15.0CTA-AC-1 Cert 2176 3326 162 46.7 124 13.9BIR-1a Meas 16 15 8 0.7 2.4 0.55 1.8BIR-1a Cert 16 18 6 0.63 2.5 0.55 2.0NCS DC86312 Meas 2460 177 1630 237 33.8 183 36.3 95.9 14.5NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36 96.2 15.1ZW-C Meas 191 253ZW-C Cert 198 260NCS DC70009(GBW07241) Meas

1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31

JR-1 Meas 15 4 0.8 < 0.2 3 1.2 21.0 20.7 47.7 5.88 23.9 5.8 0.28 6.1 1.2 3.9 0.64JR-1 Cert 15.2 3.25 0.031 0.028 2.86 1.19 20.8 19.7 47.2 5.58 23.3 6.03 0.30 5.69 1.11 3.61 0.67NCS DC86318 Meas 1940 401 721 3200 1640 18.5 2160 482 3110 551 1710 260NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560 1750 270Method Blank < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.05

QC

Analyte Symbol Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a Meas 919 2650DH-1a Cert 910 2629NIST 694 MeasNIST 694 CertDNC-1 Meas 2.0DNC-1 Cert 2.0LKSD-3 Meas 2.6 0.6 11.2 4.7LKSD-3 Cert 2.70 0.700 11.4 4.60OKA-2 Meas 30600OKA-2 Cert 28900.0

00W-2a Meas 1.9 2.4 0.5 < 1 < 0.1 2.3 0.5W-2a Cert 2.10 2.60 0.500 0.300 0.200 2.40 0.530SY-4 MeasSY-4 Cert

Page 6/7


Analyte Symbol Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSCTA-AC-1 Meas 11.2 1.11 22.9 4.5CTA-AC-1 Cert 11.4 1.08 21.8 4.4BIR-1a Meas 1.7 0.6BIR-1a Cert 1.7 0.60NCS DC86312 Meas 89.4 12.0 24.5NCS DC86312 Cert 87.79 11.96 23.6ZW-C Meas 82.7 329 33.7ZW-C Cert 82 320 34NCS DC70009(GBW07241) Meas

16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135

JR-1 Meas 4.8 0.66 4.5 1.8 1.3 22 26.0 9.6JR-1 Cert 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1730 256NCS DC86318 Cert 1840 260.0Method Blank < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1


Page 7/7







REPORT A14-08521



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507246 81.39 8.07 2.30 0.013 0.79 0.43 2.30 2.75 0.365 0.04 0.55 99.00 5 2 37 20 4 < 20 < 10 < 30 12 1 < 5507247 75.58 12.98 1.22 0.013 0.08 0.18 4.42 5.16 0.166 0.07 0.24 100.1 < 1 7 6 < 20 < 1 < 20 < 10 < 30 39 3 < 5507248 73.92 11.77 4.13 0.035 0.06 0.31 5.03 2.88 0.214 0.03 0.28 98.68 < 1 7 < 5 < 20 < 1 < 20 < 10 50 40 4 < 5507249 76.31 8.98 4.21 0.063 0.40 0.57 3.23 2.41 0.683 0.07 0.53 97.45 2 7 18 < 20 1 < 20 < 10 80 39 5 10507250 78.28 9.29 3.06 0.026 0.61 0.52 3.25 2.19 0.321 0.03 0.58 98.17 3 6 25 40 2 < 20 < 10 50 21 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507246 85 73 48 150 27 < 2 < 0.5 < 0.2 3 < 0.5 0.9 390 < 0.4 13.6 32.1 4.46 19.4 5.5 0.86 5.8 1.1 7.8 1.7507247 200 54 603 941 855 < 2 2.7 < 0.2 9 < 0.5 0.8 290 < 0.4 340 689 79.2 303 72.3 4.88 76.4 17.2 122 27.3507248 111 51 1417 725 < 2 2.0 < 0.2 39 < 0.5 0.6 196 < 0.4 289 709 93.0 405 137 9.77 174 41.1 296 66.9507249 87 78 3440 3716 < 2 < 0.2 39 < 0.5 0.6 214 < 0.4 1060 2490 293 1140 304 20.2 336 80.1 578 133507250 75 67 562 1957 661 < 2 < 0.2 16 0.6 0.9 212 < 0.4 36.8 114 14.7 73.0 34.1 2.85 49.2 12.0 95.8 22.5

Page 3/7


Results


F507246 5.5 0.85 5.2 0.76 4.1 1.3 < 1 0.3 8 8.2 3.2507247 91.0 14.0 81.7 9.92 27.2 41.3 3 0.7 54 277 75.1507248 214 31.3 172 19.9 22.7 67.7 6 0.4 67 322 142 0.371507249 452 71.4 418 51.8 103 242 13 0.3 196 853 395 0.700507250 81.0 14.2 88.5 10.4 54.6 39.1 7 0.2 54 140 69.8

Page 4/7


QC




1050.000 99


30 990 100 16 11 70


30 960 100 16.5 11.2 69.9


19 170


18.1 169

JR-1 Meas < 20 30 16 16JR-1 Cert 1.67 30.6 16.1 16.3NCS DC86318 MeasNCS DC86318 CertSX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 MeasSARM 3 Cert507247 Orig 75.28 13.11 1.23 0.013 0.08 0.19 4.44 5.19 0.168 0.07 0.24 100.0 < 1 7 7 < 20 < 1 < 20 < 10 < 30 38 3 < 5507247 Dup 75.89 12.85 1.21 0.013 0.09 0.18 4.41 5.12 0.164 0.07 0.24 100.2 < 1 7 6 < 20 < 1 < 20 < 10 < 30 40 2 < 5Method Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5Method Blank

Page 5/7


QC

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 146 16 36 109 3.7 0.60DNC-1 Cert 144.0 18.0 38 118 3.6 0.59LKSD-3 Meas 72 2 2.1 49.8 90.9 43.6 7.6 1.47 4.8LKSD-3 Cert 78.0 2.00 2.30 52.0 90.0 44.0 8.00 1.50 4.90OKA-2 MeasOKA-2 CertW-2a Meas 19 199 20 88 8 < 2 < 0.5 172 < 0.4 10.8 23.0 12.4 3.1 1.03 3.7 0.7W-2a Cert 21.0 190 24.0 94.0 7.90 0.600 0.0460 182 0.0300 10.0 23.0 13.0 3.30 1.00 3.60 0.760SY-4 Meas 1193 117 524 354SY-4 Cert 1191 119 517 340CTA-AC-1 Meas 2380 3570 177 48.0 130 15.0CTA-AC-1 Cert 2176 3326 162 46.7 124 13.9BIR-1a Meas 113 16 15 8 0.7 2.4 0.55 1.8BIR-1a Cert 110 16 18 6 0.63 2.5 0.55 2.0NCS DC86312 Meas 2460 177 1630 237 33.8 183 36.3NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36ZW-C Meas 191 253ZW-C Cert 198 260VS-N MeasVS-N CertNCS DC70009(GBW07241) Meas

540 1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4


500 1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81

JR-1 Meas 256 15 4 0.8 < 0.2 3 1.2 21.0 20.7 47.7 5.88 23.9 5.8 0.28 6.1 1.2JR-1 Cert 257 15.2 3.25 0.031 0.028 2.86 1.19 20.8 19.7 47.2 5.58 23.3 6.03 0.30 5.69 1.11NCS DC86318 Meas 1940 401 721 3200 1640 18.5 2160 482 3110 551NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560SX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 MeasSARM 3 Cert507247 Orig 197 55 612 926 842 < 2 2.5 < 0.2 9 < 0.5 0.8 292 < 0.4 344 693 79.5 303 72.3 4.95 77.7 17.5 124 27.9507247 Dup 203 54 594 956 869 < 2 2.9 < 0.2 9 < 0.5 0.8 289 < 0.4 336 685 79.0 303 72.4 4.81 75.2 16.9 120 26.7Method Blank < 2 < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1Method Blank

QC

Page 6/7




00W-2a Meas 1.9 2.4 0.5 < 1 < 0.1 2.3 0.5W-2a Cert 2.10 2.60 0.500 0.300 0.200 2.40 0.530SY-4 MeasSY-4 CertCTA-AC-1 Meas 11.2 1.11 22.9 4.5CTA-AC-1 Cert 11.4 1.08 21.8 4.4BIR-1a Meas 1.7 0.6BIR-1a Cert 1.7 0.60NCS DC86312 Meas 95.9 14.5 89.4 12.0 24.5NCS DC86312 Cert 96.2 15.1 87.79 11.96 23.6ZW-C Meas 82.7 329 33.7ZW-C Cert 82 320 34VS-N Meas 0.102VS-N Cert 0.10NCS DC70009(GBW07241) Meas

13.2 2.36 16.3 2.35 2300 30.2


13.4 2.2 14.9 2.4 2200 28.3


14.9 2.49 15.8 2.27 54.2 136


14.9 2.31 14.9 2.26 51.6 135

JR-1 Meas 3.9 0.64 4.8 0.66 4.5 1.8 1.3 22 26.0 9.6JR-1 Cert 3.61 0.67 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1710 260 1730 256NCS DC86318 Cert 1750 270 1840 260.0SX18-01 Meas 0.696SX18-01 Cert 0.695SX18-04 Meas 1.322SX18-04 Cert 1.32SARM 3 Meas 0.147SARM 3 Cert 0.14507247 Orig 92.5 14.2 82.1 10.1 26.2 41.3 3 0.7 54 278 75.2507247 Dup 89.6 13.9 81.2 9.75 28.1 41.2 2 0.7 54 277 74.9Method Blank < 0.1 < 0.05 < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1Method Blank < 0.003


Page 7/7







REPORT A14-08519



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507251 85.53 7.44 1.88 0.015 0.61 0.40 1.60 1.92 0.331 0.06 1.01 100.8 5 2 37 20 3 < 20 < 10 < 30 11 1 < 5507252 73.67 13.73 1.55 0.014 0.05 0.23 4.09 4.90 0.094 0.03 0.44 98.80 < 1 7 < 5 < 20 < 1 < 20 < 10 < 30 37 2 < 5507253 73.22 14.02 1.12 0.013 0.04 0.21 4.74 4.57 0.133 < 0.01 0.31 98.38 < 1 5 < 5 20 < 1 < 20 < 10 < 30 34 2 < 5507254 72.74 13.29 1.64 0.010 0.06 0.20 3.14 5.88 0.120 0.02 1.29 98.39 < 1 7 6 30 < 1 < 20 < 10 < 30 32 2 < 5507255 80.97 8.24 2.59 0.011 0.96 0.79 1.87 2.42 0.410 0.08 1.21 99.55 6 2 42 50 5 < 20 < 10 < 30 11 1 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507251 85 41 31 135 10 < 2 < 0.5 < 0.2 2 < 0.5 1.2 349 < 0.4 17.5 38.2 4.69 19.1 4.2 0.74 3.9 0.7 4.8 1.1507252 183 62 646 298 654 < 2 0.7 3.2 9 < 0.5 1.1 276 < 0.4 63.2 147 21.2 104 43.6 3.54 62.7 15.4 111 26.0507253 156 64 364 142 293 < 2 < 0.5 < 0.2 5 < 0.5 0.9 257 < 0.4 58.2 121 15.8 71.5 23.8 1.86 30.5 7.0 49.3 11.3507254 180 67 345 210 338 < 2 < 0.5 < 0.2 11 < 0.5 1.4 310 < 0.4 53.5 115 15.7 70.4 24.7 2.00 30.6 7.0 49.7 11.3507255 79 52 31 155 16 < 2 < 0.5 < 0.2 2 0.7 1.7 379 < 0.4 33.0 58.3 6.89 25.3 5.1 0.98 4.2 0.8 4.8 1.0

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507251 3.4 0.54 3.5 0.54 3.4 0.8 < 1 0.3 6 6.4 1.9507252 85.3 12.8 71.8 8.51 9.9 27.4 2 0.7 49 115 52.6507253 40.7 6.21 33.4 4.22 4.3 11.9 1 0.6 47 70.7 18.9507254 40.5 6.26 34.7 4.35 6.5 14.2 2 1.0 53 70.4 25.6507255 3.4 0.50 3.0 0.48 3.9 0.6 < 1 0.6 7 6.1 1.6

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08518



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507256 54.23 11.42 5.08 0.112 3.86 14.47 2.53 4.74 0.708 0.18 3.62 101.0 12 5 60 60 11 < 20 < 10 100 16 2 11

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507256 174 243 33 217 11 < 2 < 0.5 < 0.2 3 3.2 4.6 579 1.2 31.5 63.2 7.72 29.9 6.2 1.27 5.6 0.9 5.8 1.2

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507256 3.6 0.55 3.4 0.53 5.3 0.9 4 0.8 25 9.6 2.8

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08512



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507257 51.39 14.02 13.79 0.204 4.05 7.45 3.27 1.89 1.491 0.49 0.43 98.48 33 2 391 30 41 30 170 130 22 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507257 54 574 29 147 5 < 2 < 0.5 < 0.2 < 1 < 0.5 2.7 1040 < 0.4 27.8 58.2 7.62 31.7 6.3 1.75 5.6 0.9 5.4 1.1

Page 3/7


Results


Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08511



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507258 70.01 14.34 2.67 0.068 0.37 1.15 3.55 5.61 0.440 0.09 0.26 98.56 5 4 28 < 20 2 < 20 < 10 50 18 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507258 217 133 42 430 20 < 2 1.1 < 0.2 2 < 0.5 2.7 637 < 0.4 104 214 23.7 81.6 12.6 1.06 8.3 1.2 7.3 1.4

Page 3/7


Results


Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08510



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507259 66.95 16.45 2.55 0.094 0.52 1.45 4.24 5.85 0.537 0.11 0.34 99.09 8 3 30 < 20 2 < 20 < 10 60 18 1 < 5507260 66.27 16.09 2.74 0.076 0.59 1.52 4.29 6.56 0.587 0.10 0.32 99.13 8 3 33 30 3 < 20 10 60 18 2 8

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507259 150 206 29 447 12 < 2 1.2 < 0.2 1 < 0.5 3.0 1050 < 0.4 59.3 116 13.2 49.7 8.2 1.52 5.6 0.8 4.9 1.0507260 168 231 31 492 21 < 2 2.7 < 0.2 21 < 0.5 3.4 1321 < 0.4 80.4 157 18.8 65.5 10.5 2.02 7.2 1.0 6.0 1.2

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507259 3.1 0.44 3.1 0.53 9.4 0.8 < 1 0.5 24 11.6 3.1507260 3.7 0.57 3.9 0.59 10.4 1.1 5 0.4 45 15.0 3.7

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08509



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507261 72.91 13.37 1.78 0.045 0.27 0.70 3.20 5.86 0.275 0.05 0.26 98.71 3 4 13 < 20 1 < 20 < 10 30 16 1 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507261 243 114 53 231 18 < 2 0.6 < 0.2 2 < 0.5 2.4 516 < 0.4 102 199 21.1 71.5 11.4 0.89 8.3 1.4 8.7 1.8

Page 3/7


Results


Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08508



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507262 52.62 14.69 13.89 0.228 4.38 6.81 3.22 1.78 1.465 0.39 1.12 100.6 37 2 366 < 20 39 < 20 150 120 22 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507262 58 457 32 147 6 < 2 < 0.5 < 0.2 1 < 0.5 1.4 824 < 0.4 28.1 60.0 7.57 32.4 6.4 1.90 6.0 0.9 5.5 1.1

Page 3/7


Results


Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08507



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507263 80.49 8.15 2.60 0.042 1.10 0.64 2.30 2.26 0.435 0.10 0.62 98.74 5 8 40 30 6 < 20 < 10 50 11 1 < 5507264 74.75 13.85 0.85 0.007 0.09 0.33 6.81 2.15 0.037 0.02 0.41 99.30 < 1 12 11 < 20 < 1 < 20 < 10 < 30 51 2 < 5507265 63.01 17.48 6.96 0.030 0.20 0.75 7.77 2.36 0.317 0.05 0.54 99.44 2 24 81 < 20 1 < 20 < 10 < 30 76 4 < 5507266 63.93 17.78 6.47 0.105 0.20 0.53 7.19 3.33 0.296 0.05 0.55 100.4 3 20 85 < 20 1 < 20 < 10 < 30 75 3 < 5507267 66.65 18.53 1.04 0.011 0.09 0.17 4.37 9.18 0.048 0.02 0.38 100.5 < 1 8 13 < 20 < 1 < 20 < 10 < 30 52 3 < 5507268 78.22 10.44 3.29 0.034 1.07 0.32 2.21 3.61 0.449 0.10 0.96 100.7 7 11 48 30 6 < 20 < 10 50 15 1 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507263 145 64 30 143 6 < 2 < 0.5 < 0.2 2 < 0.5 4.3 330 < 0.4 15.8 36.6 4.45 17.4 3.8 0.71 3.5 0.6 3.9 0.8507264 81 40 77 270 73 < 2 0.6 0.3 110 < 0.5 1.3 51 < 0.4 11.8 39.6 5.13 19.3 5.3 0.54 4.0 1.0 8.0 2.0507265 98 85 255 3647 255 < 2 1.9 616 < 0.5 1.6 57 < 0.4 88.4 293 39.4 134 26.5 1.90 14.9 3.6 27.6 6.8507266 179 70 303 3866 278 < 2 1.8 565 < 0.5 2.4 66 < 0.4 59.7 214 28.8 101 22.5 1.75 13.9 3.8 31.4 8.5507267 522 108 29 69 28 < 2 0.5 0.2 75 < 0.5 5.1 221 < 0.4 4.2 13.2 1.79 7.1 1.7 0.26 1.5 0.4 2.9 0.8507268 220 61 26 154 9 < 2 0.5 < 0.2 5 < 0.5 5.0 513 < 0.4 19.2 38.5 4.74 18.7 4.0 0.72 3.6 0.6 3.9 0.8

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507263 2.7 0.47 3.3 0.59 3.4 0.9 < 1 0.7 42 5.5 1.6507264 9.1 2.36 22.2 3.63 26.2 31.6 < 1 0.4 66 63.6 9.1507265 33.8 9.68 100 18.5 414 110 3 0.4 138 563 36.3507266 46.7 14.0 151 28.0 451 114 4 0.7 131 695 41.1507267 3.9 1.19 12.2 2.11 8.2 12.0 < 1 2.2 260 18.0 2.7507268 2.5 0.44 3.2 0.57 6.7 1.0 1 1.0 44 6.6 1.9

Page 4/7


QC




1050.000 99


30 990 100 16 11 70


30 960 100 16.5 11.2 69.9


19 170


18.1 169

JR-1 Meas < 20 30 16 16JR-1 Cert 1.67 30.6 16.1 16.3NCS DC86318 MeasNCS DC86318 Cert507265 Orig 63.95 17.17 6.92 0.030 0.20 0.76 7.98 2.45 0.315 0.05 0.54 100.4 2 24 83 < 20 1 < 20 < 10 < 30 77 4 < 5507265 Dup 62.06 17.79 6.99 0.030 0.20 0.74 7.56 2.26 0.318 0.04 0.54 98.52 2 24 79 < 20 1 < 20 < 10 < 30 74 4 < 5Method Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5

QC

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 146 16 36 109 3.7 0.60

Page 5/7


Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDNC-1 Cert 144.0 18.0 38 118 3.6 0.59LKSD-3 Meas 72 2 2.1 49.8 90.9 43.6 7.6 1.47 4.8LKSD-3 Cert 78.0 2.00 2.30 52.0 90.0 44.0 8.00 1.50 4.90OKA-2 MeasOKA-2 CertW-2a Meas 19 199 20 88 8 < 2 < 0.5 172 < 0.4 10.8 23.0 12.4 3.1 1.03 3.7 0.7W-2a Cert 21.0 190 24.0 94.0 7.90 0.600 0.0460 182 0.0300 10.0 23.0 13.0 3.30 1.00 3.60 0.760SY-4 Meas 1193 117 524 354SY-4 Cert 1191 119 517 340CTA-AC-1 Meas 2380 3570 177 48.0 130 15.0CTA-AC-1 Cert 2176 3326 162 46.7 124 13.9BIR-1a Meas 113 16 15 8 0.7 2.4 0.55 1.8BIR-1a Cert 110 16 18 6 0.63 2.5 0.55 2.0NCS DC86312 Meas 2460 177 1630 237 33.8 183 36.3NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36ZW-C Meas 191 253ZW-C Cert 198 260NCS DC70009(GBW07241) Meas

540 1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4


500 1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81

JR-1 Meas 256 15 4 0.8 < 0.2 3 1.2 21.0 20.7 47.7 5.88 23.9 5.8 0.28 6.1 1.2JR-1 Cert 257 15.2 3.25 0.031 0.028 2.86 1.19 20.8 19.7 47.2 5.58 23.3 6.03 0.30 5.69 1.11NCS DC86318 Meas 1940 401 721 3200 1640 18.5 2160 482 3110 551NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560507265 Orig 99 85 253 3670 252 < 2 2.0 632 < 0.5 1.7 56 < 0.4 91.1 301 40.5 137 26.7 1.98 15.0 3.7 27.9 6.9507265 Dup 97 85 257 3625 258 < 2 1.9 601 < 0.5 1.5 58 < 0.4 85.7 286 38.4 130 26.3 1.82 14.7 3.6 27.3 6.8Method Blank < 2 < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1

QC

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a Meas 919 2650DH-1a Cert 910 2629NIST 694 MeasNIST 694 CertDNC-1 Meas 2.0DNC-1 Cert 2.0LKSD-3 Meas 2.6 0.6 11.2 4.7LKSD-3 Cert 2.70 0.700 11.4 4.60OKA-2 Meas 30600OKA-2 Cert 28900.0

00

Page 6/7


Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSW-2a Meas 1.9 2.4 0.5 < 1 < 0.1 2.3 0.5W-2a Cert 2.10 2.60 0.500 0.300 0.200 2.40 0.530SY-4 MeasSY-4 CertCTA-AC-1 Meas 11.2 1.11 22.9 4.5CTA-AC-1 Cert 11.4 1.08 21.8 4.4BIR-1a Meas 1.7 0.6BIR-1a Cert 1.7 0.60NCS DC86312 Meas 95.9 14.5 89.4 12.0 24.5NCS DC86312 Cert 96.2 15.1 87.79 11.96 23.6ZW-C Meas 82.7 329 33.7ZW-C Cert 82 320 34NCS DC70009(GBW07241) Meas

13.2 2.36 16.3 2.35 2300 30.2


13.4 2.2 14.9 2.4 2200 28.3


14.9 2.49 15.8 2.27 54.2 136


14.9 2.31 14.9 2.26 51.6 135

JR-1 Meas 3.9 0.64 4.8 0.66 4.5 1.8 1.3 22 26.0 9.6JR-1 Cert 3.61 0.67 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1710 260 1730 256NCS DC86318 Cert 1750 270 1840 260.0507265 Orig 34.1 9.70 101 18.6 418 110 3 0.4 139 573 36.6507265 Dup 33.6 9.65 99.2 18.3 409 110 3 0.4 138 552 35.9Method Blank < 0.1 < 0.05 < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1


Page 7/7


Date Submitted: 06-Nov-14 Invoice No.: A14-08506 (i) Invoice Date: 09-Dec-14 Your Reference: Alterra Resources P.O. Box 214 60 Bowater Avenue Port Hope Simpson NL A0K 4E0 Canada





REPORT A14-08506 (i)



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507269 71.60 13.23 2.06 0.036 0.64 0.83 4.00 5.11 0.344 0.10 0.57 98.51 5 7 30 < 20 3 < 20 < 10 30 17 1 < 5507270 72.57 12.98 1.79 0.029 0.36 0.59 3.56 5.96 0.306 0.07 0.36 98.58 4 6 20 < 20 2 < 20 < 10 < 30 17 1 < 5507271 73.67 12.48 2.14 0.032 0.29 0.55 3.42 5.78 0.308 0.05 0.38 99.10 4 8 18 < 20 1 < 20 < 10 < 30 16 2 < 5507272 72.92 12.97 1.68 0.035 0.26 0.74 3.62 5.55 0.306 0.05 0.28 98.43 4 8 17 < 20 1 < 20 < 10 < 30 16 2 < 5507273 72.07 13.20 1.61 0.033 0.27 0.69 3.65 5.75 0.304 0.02 0.49 98.08 4 8 17 30 2 < 20 < 10 40 16 2 < 5507274 85.22 7.21 0.96 0.013 0.08 0.27 1.86 3.27 0.109 0.01 0.15 99.16 1 4 8 20 < 1 < 20 < 10 < 30 11 1 < 5507275 72.97 12.81 1.58 0.025 0.27 0.63 3.39 6.16 0.333 0.06 0.29 98.54 4 9 18 < 20 2 < 20 < 10 < 30 17 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507269 247 122 33 238 22 < 2 0.7 < 0.2 5 < 0.5 3.2 362 < 0.4 40.1 99.3 9.62 33.4 6.1 0.50 4.1 0.8 5.1 1.0507270 290 106 32 287 25 < 2 0.7 < 0.2 5 < 0.5 3.2 369 < 0.4 36.4 91.7 8.92 30.8 5.7 0.43 4.1 0.8 5.4 1.2507271 286 74 52 626 37 < 2 1.7 < 0.2 7 < 0.5 3.3 363 < 0.4 39.1 100 9.88 34.2 7.5 0.43 6.2 1.3 9.0 2.1507272 277 87 53 410 32 < 2 1.3 < 0.2 4 < 0.5 3.6 356 < 0.4 58.5 131 13.5 47.8 8.6 0.57 6.4 1.2 8.6 1.9507273 294 85 38 267 25 < 2 2.0 < 0.2 4 < 0.5 4.0 366 < 0.4 53.1 116 12.2 40.9 7.3 0.56 5.3 1.0 6.3 1.4507274 147 39 18 98 22 < 2 < 0.5 < 0.2 4 < 0.5 2.0 161 < 0.4 11.2 29.7 2.90 9.9 2.1 0.17 2.0 0.4 2.7 0.6507275 320 76 78 736 40 < 2 2.2 < 0.2 7 < 0.5 4.0 371 < 0.4 51.5 125 13.2 46.1 9.6 0.58 8.1 1.8 12.8 3.0

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507269 3.4 0.59 4.3 0.70 6.5 2.2 < 1 1.1 26 26.3 3.3507270 3.8 0.65 5.0 0.87 9.2 3.2 < 1 1.2 34 34.2 3.7507271 6.7 1.18 8.2 1.34 16.2 3.4 < 1 1.2 44 35.6 7.4507272 6.2 1.03 7.6 1.25 11.1 2.6 < 1 1.2 38 36.7 5.5507273 4.6 0.85 6.0 0.93 7.0 2.2 4 0.6 41 29.9 4.6507274 2.3 0.39 2.6 0.42 3.1 2.4 < 1 0.7 24 12.8 6.1507275 10.3 1.83 12.9 2.05 17.5 3.9 < 1 1.2 40 38.5 6.5

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08505



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507276 71.90 13.71 2.02 0.047 0.40 1.05 4.02 4.87 0.216 0.07 0.42 98.72 4 5 21 < 20 2 < 20 30 30 19 2 < 5507277 53.55 18.71 9.54 0.231 3.64 3.49 6.31 2.04 0.690 0.39 1.87 100.5 14 8 138 < 20 26 < 20 30 180 24 2 < 5507278 73.68 13.54 1.45 0.032 0.30 0.83 3.53 5.76 0.167 0.05 0.41 99.74 3 4 15 < 20 2 < 20 30 < 30 17 1 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507276 195 214 26 127 12 < 2 0.7 < 0.2 2 < 0.5 2.3 629 < 0.4 56.0 96.2 9.55 31.5 4.9 0.71 3.6 0.6 3.8 0.8507277 222 387 23 79 10 < 2 < 0.5 < 0.2 2 < 0.5 9.0 321 < 0.4 30.7 57.8 7.37 30.2 5.4 1.37 3.9 0.6 3.6 0.8507278 221 202 19 84 10 < 2 < 0.5 < 0.2 1 < 0.5 2.0 679 < 0.4 41.8 70.0 6.75 21.6 3.4 0.53 2.5 0.4 2.9 0.6

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507276 2.8 0.45 3.5 0.61 3.8 1.1 < 1 0.9 28 19.3 3.5507277 2.3 0.35 2.6 0.48 1.9 0.4 < 1 1.0 16 1.8 3.2507278 2.0 0.34 2.5 0.44 2.6 0.9 < 1 1.0 31 12.2 2.3

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08503



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507279 58.01 18.25 6.19 0.186 2.20 3.33 5.00 5.13 0.643 0.19 1.08 100.2 12 13 102 < 20 14 20 820 120 28 2 < 5507280 44.98 15.69 14.23 0.310 7.05 7.06 2.84 3.29 1.226 0.23 2.02 98.93 33 6 276 40 55 100 2360 180 21 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507279 305 406 50 293 23 < 2 1.5 < 0.2 3 < 0.5 7.5 551 0.9 86.5 176 19.8 71.1 11.9 1.39 8.5 1.3 7.7 1.5507280 350 386 28 79 3 5 2.7 < 0.2 1 < 0.5 13.0 1139 2.9 12.4 26.7 3.83 17.6 4.5 1.54 4.8 0.8 5.2 1.1

Page 3/7


Results

Analyte Symbol Er Tm Yb Lu Hf Ta W Tl Pb Th UUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.1 0.05 0.1 0.04 0.2 0.1 1 0.1 5 0.1 0.1Method Code FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507279 4.8 0.77 5.6 0.98 7.9 1.3 < 1 1.7 40 28.2 5.8507280 3.1 0.44 3.0 0.51 2.1 < 0.1 < 1 2.2 36 0.7 0.9

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC


Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC



Page 6/7



16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08566



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507281 69.51 13.93 3.18 0.074 0.68 1.04 4.16 4.96 0.407 0.14 0.57 98.65 7 5 30 < 20 3 < 20 10 50 20 2 < 5507282 63.75 0.74 29.48 0.133 0.29 0.78 0.04 0.15 1.328 0.05 0.40 97.14 2 < 1 53 20 6 < 20 < 10 410 29 7 9507283 69.83 13.67 3.12 0.073 0.70 1.23 3.96 4.83 0.452 0.16 0.48 98.50 7 4 28 < 20 3 < 20 20 50 19 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507281 162 191 74 345 37 < 2 0.8 < 0.2 3 < 0.5 1.6 782 < 0.4 67.1 147 16.0 58.8 11.5 1.17 9.8 1.7 11.5 2.5507282 18 28 5912 4474 3 0.3 55 0.9 1.2 31 < 0.4 567 1560 230 1150 497 37.4 680 160 1170 285507283 160 195 135 357 78 < 2 1.0 < 0.2 4 < 0.5 2.0 744 < 0.4 79.9 162 20.2 77.5 16.2 1.63 14.4 2.7 18.1 3.8

Page 3/7


Results


F507281 8.2 1.25 7.3 1.09 9.4 1.5 < 1 0.6 36 13.9 4.4507282 909 130 661 80.9 139 219 38 < 0.1 145 962 523 1.475507283 12.2 1.83 10.5 1.43 11.0 3.5 < 1 0.6 36 18.5 5.7

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC

Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC

Page 6/7





16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08568



CERTIFIED BY:





Page 1/8


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507284 69.41 14.09 2.89 0.105 0.59 1.22 4.26 5.15 0.409 0.11 0.48 98.72 7 8 26 < 20 3 < 20 < 10 60 22 2 < 5507285 71.81 13.98 2.75 0.096 0.61 1.29 4.82 3.81 0.426 0.12 0.51 100.2 6 7 21 < 20 2 < 20 < 10 70 21 2 < 5507286 57.50 9.36 19.22 0.207 0.77 1.94 4.22 0.34 0.718 0.34 1.44 96.06 15 22 70 < 20 4 < 20 < 10 270 38 5 6507287 57.67 14.09 12.13 0.267 1.53 2.26 6.26 0.60 0.514 0.34 1.33 96.99 10 22 65 < 20 7 < 20 < 10 300 36 3 < 5507288 58.51 11.56 15.17 0.307 0.80 2.59 5.15 0.56 0.944 0.28 0.67 96.54 12 27 54 < 20 3 < 20 < 10 300 41 5 6507289 65.51 13.35 10.56 0.167 0.45 1.70 6.32 0.67 0.384 0.13 0.51 99.75 13 22 42 < 20 2 < 20 < 10 190 42 4 < 5507290 64.75 11.96 14.03 0.235 0.69 1.91 5.68 0.48 0.335 0.11 0.45 100.6 23 31 62 < 20 3 < 20 < 10 280 42 4 < 5507291 67.39 15.73 6.04 0.135 0.32 1.51 7.32 0.90 0.219 0.05 0.35 99.95 8 17 25 < 20 1 < 20 < 10 150 44 3 < 5507292 72.39 14.39 1.59 0.056 0.28 0.81 4.27 5.46 0.211 0.08 0.42 99.97 4 9 14 < 20 1 < 20 < 10 50 22 2 < 5507293 66.95 12.52 6.56 0.214 1.47 2.46 3.93 4.10 0.951 0.32 0.50 99.97 15 6 66 < 20 7 < 20 10 140 23 2 < 5507294 71.46 13.84 2.77 0.088 0.49 1.14 4.13 5.33 0.363 0.13 0.37 100.1 5 6 23 < 20 2 < 20 < 10 60 19 2 < 5507295 71.54 14.19 2.72 0.092 0.52 1.25 4.19 5.19 0.378 0.14 0.41 100.6 6 5 25 < 20 3 < 20 30 60 19 2 < 5

Page 2/8


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507284 233 176 90 314 69 < 2 0.8 < 0.2 5 < 0.5 5.2 642 < 0.4 73.5 156 18.2 67.9 14.4 1.44 12.4 2.4 15.7 3.3507285 145 146 99 282 42 < 2 0.7 < 0.2 15 < 0.5 2.6 534 < 0.4 51.5 119 16.2 65.5 15.0 1.52 13.0 2.4 15.2 3.3507286 7 103 1714 20890 < 2 0.9 105 < 0.5 < 0.5 98 < 0.4 476 1130 140 597 184 14.3 215 48.3 334 78.0507287 17 210 1148 11650 < 2 0.5 49 < 0.5 0.6 147 < 0.4 262 604 80.1 354 116 9.33 143 31.8 219 50.7507288 12 111 2398 13610 < 2 0.9 99 < 0.5 0.6 115 < 0.4 397 959 131 609 225 18.6 306 71.3 502 115507289 12 59 447 5445 414 < 2 0.7 83 < 0.5 0.7 57 < 0.4 142 371 45.6 192 55.5 4.22 57.9 12.2 82.1 18.5507290 8 46 234 1234 82 < 2 0.9 106 < 0.5 0.5 42 < 0.4 175 369 48.3 190 44.7 3.04 37.5 7.1 43.9 9.0507291 15 56 162 853 123 < 2 1.9 0.4 56 < 0.5 1.1 67 < 0.4 57.9 131 18.8 81.4 23.3 1.85 23.9 4.9 31.5 6.7507292 237 135 37 140 32 < 2 < 0.5 < 0.2 4 < 0.5 4.1 574 < 0.4 31.9 66.9 8.31 30.9 6.7 0.76 4.9 0.9 5.6 1.2507293 213 157 131 732 51 < 2 2.0 < 0.2 6 < 0.5 6.4 495 < 0.4 129 293 37.6 143 29.0 1.94 20.8 3.6 21.6 4.4507294 211 178 74 267 22 < 2 0.6 < 0.2 3 < 0.5 3.3 714 < 0.4 69.5 132 14.9 53.4 10.0 1.02 6.9 1.2 7.3 1.5507295 199 184 48 270 22 < 2 0.6 < 0.2 3 < 0.5 2.9 694 < 0.4 71.8 140 16.0 58.2 11.1 1.08 7.5 1.3 7.8 1.6

Page 3/8


Results


F507284 11.1 1.73 10.5 1.52 9.2 5.8 < 1 0.8 34 23.6 8.5507285 11.1 1.78 11.4 1.68 7.6 2.3 < 1 0.6 27 8.5 2.8507286 267 41.0 238 33.0 530 43.6 5 < 0.1 74 223 222 0.315507287 175 26.4 150 21.0 290 25.1 3 < 0.1 70 142 153 0.195507288 380 54.6 292 38.8 348 61.4 9 < 0.1 79 312 251 0.549507289 63.7 10.1 62.4 9.23 139 13.7 < 1 < 0.1 25 65.8 46.9507290 28.6 4.62 32.3 5.32 35.5 8.3 < 1 < 0.1 11 26.1 5.6507291 22.0 3.49 22.4 3.71 23.7 7.3 < 1 < 0.1 13 22.7 6.6507292 4.0 0.65 4.4 0.71 4.5 2.3 < 1 0.9 43 9.0 4.4507293 13.9 2.13 13.2 2.08 19.2 3.1 < 1 0.7 32 22.8 6.1507294 4.9 0.74 5.0 0.81 6.7 1.1 < 1 0.8 25 15.0 3.4507295 5.2 0.79 5.1 0.83 7.7 1.2 < 1 0.8 25 15.4 3.8

Page 4/8


QC




1050.000 99


30 990 100 16 11 70


30 960 100 16.5 11.2 69.9


19 170


18.1 169

JR-1 Meas < 20 30 16 16JR-1 Cert 1.67 30.6 16.1 16.3NCS DC86318 MeasNCS DC86318 CertSX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 MeasSARM 3 Cert507285 Orig 71.77 13.95 2.74 0.096 0.61 1.28 4.84 3.81 0.419 0.12 0.51 100.2 6 7 21 < 20 2 < 20 < 10 80 21 2 < 5507285 Dup 71.85 14.01 2.76 0.096 0.61 1.29 4.80 3.82 0.432 0.12 0.51 100.3 6 7 21 < 20 2 < 20 < 10 70 21 2 < 5507295 Orig 71.54 14.19 2.72 0.092 0.52 1.25 4.19 5.19 0.378 0.14 0.41 100.6 6 5 25 < 20 3 < 20 30 60 19 2 < 5507295 Split 72.10 13.88 2.66 0.090 0.52 1.25 4.23 5.17 0.373 0.15 0.41 100.8 6 5 26 < 20 3 < 20 30 60 20 2 < 5Method Blank < 20 < 1 < 20 < 10 < 30 < 1 < 1 < 5Method Blank

Page 5/8


QC

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSDH-1a MeasDH-1a CertNIST 694 MeasNIST 694 CertDNC-1 Meas 146 16 36 109 3.7 0.60DNC-1 Cert 144.0 18.0 38 118 3.6 0.59LKSD-3 Meas 72 2 2.1 49.8 90.9 43.6 7.6 1.47 4.8LKSD-3 Cert 78.0 2.00 2.30 52.0 90.0 44.0 8.00 1.50 4.90OKA-2 MeasOKA-2 CertW-2a Meas 19 199 20 88 8 < 2 < 0.5 172 < 0.4 10.8 23.0 12.4 3.1 1.03 3.7 0.7W-2a Cert 21.0 190 24.0 94.0 7.90 0.600 0.0460 182 0.0300 10.0 23.0 13.0 3.30 1.00 3.60 0.760SY-4 Meas 1193 117 524 354SY-4 Cert 1191 119 517 340CTA-AC-1 Meas 2380 3570 177 48.0 130 15.0CTA-AC-1 Cert 2176 3326 162 46.7 124 13.9BIR-1a Meas 113 16 15 8 0.7 2.4 0.55 1.8BIR-1a Cert 110 16 18 6 0.63 2.5 0.55 2.0NCS DC86312 Meas 2460 177 1630 237 33.8 183 36.3NCS DC86312 Cert 2360 190 1600 225.0 34.6 183 36ZW-C Meas 191 253ZW-C Cert 198 260VS-N MeasVS-N CertNCS DC70009(GBW07241) Meas

540 1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4


500 1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81

JR-1 Meas 256 15 4 0.8 < 0.2 3 1.2 21.0 20.7 47.7 5.88 23.9 5.8 0.28 6.1 1.2JR-1 Cert 257 15.2 3.25 0.031 0.028 2.86 1.19 20.8 19.7 47.2 5.58 23.3 6.03 0.30 5.69 1.11NCS DC86318 Meas 1940 401 721 3200 1640 18.5 2160 482 3110 551NCS DC86318 Cert 1960 430 740 3430 1720 18.91 2095 470 3220 560SX18-01 MeasSX18-01 CertSX18-04 MeasSX18-04 CertSARM 3 MeasSARM 3 Cert507285 Orig 147 146 98 280 43 < 2 0.7 < 0.2 15 < 0.5 2.6 535 < 0.4 51.9 120 16.2 67.0 14.9 1.56 13.0 2.4 15.1 3.3507285 Dup 144 147 100 284 42 < 2 0.6 < 0.2 15 < 0.5 2.7 533 < 0.4 51.2 119 16.1 64.1 15.1 1.48 12.9 2.4 15.3 3.3507295 Orig 199 184 48 270 22 < 2 0.6 < 0.2 3 < 0.5 2.9 694 < 0.4 71.8 140 16.0 58.2 11.1 1.08 7.5 1.3 7.8 1.6507295 Split 202 181 47 280 22 < 2 0.6 < 0.2 3 < 0.5 2.9 695 < 0.4 70.6 137 16.0 57.6 10.6 1.04 7.7 1.3 8.0 1.7Method Blank < 2 < 1 < 2 < 0.5 < 0.2 < 1 < 0.5 < 0.5 < 0.4 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.05 < 0.1 < 0.1 < 0.1 < 0.1

Page 6/8


Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MSMethod Blank

QC



00W-2a Meas 1.9 2.4 0.5 < 1 < 0.1 2.3 0.5W-2a Cert 2.10 2.60 0.500 0.300 0.200 2.40 0.530SY-4 MeasSY-4 CertCTA-AC-1 Meas 11.2 1.11 22.9 4.5CTA-AC-1 Cert 11.4 1.08 21.8 4.4BIR-1a Meas 1.7 0.6BIR-1a Cert 1.7 0.60NCS DC86312 Meas 95.9 14.5 89.4 12.0 24.5NCS DC86312 Cert 96.2 15.1 87.79 11.96 23.6ZW-C Meas 82.7 329 33.7ZW-C Cert 82 320 34VS-N Meas 0.102VS-N Cert 0.10NCS DC70009(GBW07241) Meas

13.2 2.36 16.3 2.35 2300 30.2


13.4 2.2 14.9 2.4 2200 28.3


14.9 2.49 15.8 2.27 54.2 136


14.9 2.31 14.9 2.26 51.6 135

JR-1 Meas 3.9 0.64 4.8 0.66 4.5 1.8 1.3 22 26.0 9.6JR-1 Cert 3.61 0.67 4.55 0.71 4.51 1.86 1.56 19.3 26.7 8.88NCS DC86318 Meas 1710 260 1730 256NCS DC86318 Cert 1750 270 1840 260.0SX18-01 Meas 0.696SX18-01 Cert 0.695SX18-04 Meas 1.322SX18-04 Cert 1.32

Page 7/8



FSARM 3 Meas 0.147SARM 3 Cert 0.14507285 Orig 11.0 1.77 11.4 1.66 7.5 2.3 < 1 0.6 27 8.7 2.8507285 Dup 11.2 1.80 11.4 1.70 7.7 2.2 < 1 0.6 28 8.3 2.8507295 Orig 5.2 0.79 5.1 0.83 7.7 1.2 < 1 0.8 25 15.4 3.8507295 Split 5.2 0.78 5.2 0.83 7.4 1.2 < 1 0.8 25 15.6 3.9Method Blank < 0.1 < 0.05 < 0.1 < 0.04 < 0.2 < 0.1 < 1 < 0.1 < 5 < 0.1 < 0.1Method Blank < 0.003


Page 8/8







REPORT A14-08565



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507296 58.78 12.91 11.16 0.288 0.89 3.41 6.21 1.04 0.918 0.17 0.67 96.45 14 32 37 30 3 < 20 < 10 270 35 6 8507297 47.52 4.27 31.24 0.630 1.22 5.67 1.78 0.14 2.446 0.29 0.53 95.73 21 32 87 30 5 < 20 < 10 590 31 9 12507298 63.07 13.09 11.04 0.225 0.44 2.52 6.45 0.71 0.833 0.29 0.10 98.76 12 23 38 < 20 2 < 20 < 10 240 44 4 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507296 22 157 6973 6061 < 2 0.9 98 0.5 1.3 99 0.5 131 567 134 923 567 49.7 896 218 1600 370507297 4 68 9186 9019 < 2 1.5 184 0.6 < 0.5 66 0.8 255 994 220 1420 772 66.7 1150 264 1890 427507298 11 68 504 3805 374 < 2 0.8 91 < 0.5 0.7 66 < 0.4 193 462 60.6 257 68.6 5.03 68.7 13.7 88.3 19.1

Page 3/7


Results


F507296 1180 170 851 87.9 167 155 43 < 0.1 150 760 584 1.636507297 1410 195 981 118 218 212 38 < 0.1 186 929 707 2.070507298 64.6 9.93 61.8 9.38 104 13.8 < 1 < 0.1 25 49.7 32.9

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC

Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC

Page 6/7





16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7







REPORT A14-08564



CERTIFIED BY:





Page 1/7


Results



Unit Symbol % % % % % % % % % % % % ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 0.01 0.01 0.01 0.001 0.01 0.01 0.01 0.01 0.001 0.01 0.01 1 1 5 20 1 20 10 30 1 1 5Method Code FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507299 71.16 8.42 10.34 0.052 0.21 0.79 1.78 4.32 0.753 0.06 0.08 97.99 < 1 6 28 < 20 3 < 20 30 180 26 5 < 5507300 70.62 14.05 2.84 0.043 0.65 1.26 4.47 4.77 0.382 0.14 0.30 99.52 5 5 27 < 20 4 < 20 20 30 19 2 < 5507301 73.97 12.58 2.69 0.044 0.61 1.31 4.01 4.42 0.368 0.11 0.33 100.4 5 4 27 < 20 4 < 20 50 50 18 1 < 5507302 55.85 1.85 32.19 0.141 0.21 1.98 0.29 0.67 2.158 0.15 -0.19 95.30 < 1 < 1 71 20 7 < 20 < 10 590 34 5 9507303 70.64 14.39 3.25 0.045 0.52 1.19 4.14 5.33 0.406 0.13 0.28 100.3 5 6 25 < 20 4 < 20 < 10 70 21 2 < 5

Page 2/7


Results

Analyte Symbol Rb Sr Y Zr Nb Mo Ag In Sn Sb Cs Ba Bi La Ce Pr Nd Sm Eu Gd Tb Dy HoUnit Symbol ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppmLower Limit 2 2 2 4 1 2 0.5 0.2 1 0.5 0.5 3 0.4 0.1 0.1 0.05 0.1 0.1 0.05 0.1 0.1 0.1 0.1Method Code FUS-MS FUS-ICP FUS-ICP FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-ICP FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS FUS-MS507299 156 137 3254 3431 < 2 < 0.2 38 < 0.5 1.0 451 < 0.4 173 474 78.4 423 197 17.4 271 67.8 495 119507300 169 214 86 309 61 < 2 0.9 < 0.2 3 < 0.5 1.4 856 < 0.4 65.2 138 16.5 62.2 12.3 1.26 10.4 1.9 12.0 2.6507301 153 195 105 302 57 < 2 0.8 < 0.2 4 < 0.5 1.1 829 < 0.4 69.5 151 18.8 71.0 15.3 1.38 12.5 2.5 16.3 3.4507302 21 61 6584 17470 2 0.4 103 0.7 < 0.5 213 < 0.4 664 1580 227 1070 442 36.6 567 134 991 233507303 200 233 214 842 139 < 2 2.5 < 0.2 8 < 0.5 1.9 914 < 0.4 63.3 143 19.1 76.8 20.7 1.93 20.7 4.3 29.4 6.6

Page 3/7


Results


F507299 428 65.5 370 46.6 118 128 19 0.7 71 440 209 0.644507300 9.2 1.49 9.5 1.44 10.1 2.9 < 1 0.7 34 18.2 5.9507301 11.6 1.78 10.6 1.54 9.1 3.5 < 1 0.6 55 17.7 5.6507302 841 129 738 92.0 573 248 31 0.1 98 795 444 1.278507303 22.7 3.68 21.9 2.90 29.6 9.1 < 1 0.8 58 25.8 11.6

Page 4/7


QC




1050.000 99


30 990 100 16 11 70 540


30 960 100 16.5 11.2 69.9 500


19 170


18.1 169


QC

Page 5/7



1.2 1610 3.3 44.7 24.5 60.6 7.94 33.3 12.9 15.5 3.2 21.3 4.4 13.2 2.36


1.8 1701 3.1 41 23.7 60.3 7.9 32.9 12.5 14.8 3.3 20.7 4.5 13.4 2.2


276 491 49.0 158 25.5 3.70 21.4 3.7 23.7 5.0 14.9 2.49


260 463 47.1 152 23.6 3.71 23.6 3.80 23.2 4.81 14.9 2.31


QC

Page 6/7





16.3 2.35 2300 30.2


14.9 2.4 2200 28.3


15.8 2.27 54.2 136


14.9 2.26 51.6 135



Page 7/7

APPENDIX D – PERSONNEL AND CONTRACTORS

Personnel and Contractors Personnel: Randy Miller – V.P. Exploration Suzanne Butler – Geologist Brian Penney – Labourer Blair Penney – Labourer Gerald Rumbolt - Labourer Karen Sooley – Admin Contractors: Activation Laboratories

(i) Preparation,lab,in,Happy,Valley2Goose,Bay,,NL,(ii) Analytical,lab,in,Ancaster,,ON,

,

Documents

APPENDIX A – EXPENDITURES BY LICENSE · 2 ! Table&of&Contents& 1.#INTRODUCTION