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Appendix G
Report entitled New Orleans Municipal Yacht Harbor Sediment
Sampling and Analysis Investigation Report, dated February 2017
NEW ORLEANS MUNICIPAL YACHT HARBOR SEDIMENT SAMPLING AND ANALYSIS
INVESTIGATION REPORT
NEW ORLEANS, LOUISIANA
Prepared for:
MOFFATT & NICHOL
BATON ROUGE, LOUISIANA
FEBRUARY 2017
17170 Perkins Road Baton Rouge, Louisiana 70810
{225) 755-1000
CK Project No. 14436
TABLE OF CONTENTS
New Orleans Municipal Yacht Harbor
Sediment San1pling and Analysis
Section Page
1.0 INTRODUCTION ............................................................................................................ 1 2.0 SAMPLE COLLECTION .................................................................................................... 1
3.0 INVESTIGATION RESULTS .............................................................................................. 2
3.1 Site Geology and Hydrology ............................................................................... 2 3.2 Analytical Results and Evaluation ...................................................................... 2
4.0 SUMMARY AND CONCLUSIONS .................................................................................... 3
Figure
1 Site Location Map 2 Sample Location Map
Table 1 Sediment Analytical Summary 2 SPLP Summary
Appendix A Laboratory Reports
LIST OF FIGURES
LIST OF TABLES
LIST OF APPENDICES
CK Associates
1.0 INTRODUCTION
New Orleans Municipal Yacht Harbor Sediment Sampling and Analysis
Moffatt & Nichol is managing repairs to infrastructure damaged by Hurricane Katrina at the
New Orleans Municipal Yacht Harbor (Figure 1). CK Associates (CK) was retained to conduct sampling and analysis of the sediment prior to initiation of dredging activities. Moffatt & Nichol
may place the dredged material on an adjacent upland permitted area within the West End
proper. Sampling and analysis of the sediment surface was requested to determine concentrations of potential constituents of concern (COCs) within the material to be dredged.
The dredge activities planned include the removal of one foot of sediment on the west side of
the dredge area and two feet of sediment removal on the east side.
Sampling and analysis of sediments within the Municipal Yacht Harbor was previously
conducted in 2009. The current sampling and analysis was conducted within a portion of the
area that was sampled in 2009 (Figure 2). Sediment samples were analyzed for the original list
of COCs analyzed in 2009.
2.0 SAMPLE COLLECTION
Ten samples were collected within the area to be dredged (Figure 2) on January 11 and 13,
2017. The sample locations were evenly spaced within the dredging area in order to capture sediment samples representative of the sediment material to be removed. Samples were
collected manually with a Ponar dredge deployed from a work boat platform.
A sufficient volume of sediment material was collected from each location to conduct the requested analyses and associated quality assurance and quality control samples (QA/QC).
Each sample was collected with a Ponar dredge and emptied into a stainless steel pan on the
boat deck. Samples were collected directly into laboratory-provided containers appropriate for the requested analyses. Samples collected for volatile constituents were collected first into
pre-weighed Terracore sampling kits. One duplicate, matrix spike, and matrix spike duplicate
sample were collected and analyzed. One sample of rinsate water was collected on each sampling day. All samples were labeled with unique sample identification, recorded on a chain
of-custody form, and placed into iced coolers for transport to the analytical laboratory.
CK personnel donned new, clean sampling gloves prior to handling samples or sampling
equipment. All non-disposable sampling equipment was decontaminated prior to arriving on
site and between sample locations. All unused sediment and rinsate water was returned to the
harbor.
The analyses that were completed in the 2009 evaluation were requested for all samples.
These include the Louisiana Department of Environmental Quality's (LDEQ) Risk Evaluation
Corrective Action Program (RECAP) regulated metals, volatile organic compounds (VOCs),
semivolatile organic compounds (SVOCs), Total Petroleum Hydrocarbon (TPH) Volatile Phase
Hydrocarbons (VPH) and Extractable Phase Hydrocarbons (EPH), hexavalent chromium, pesticides, cyanide, and nitrate. Moisture content was conducted on each sample, and all
1 CK Associates
New Orleans Municipal Yacht Harbor Sediment Sampling and Analysis
analytical results were reported on a dry weight basis. All analyses were completed by a LDEQaccredited laboratory, TestAmerica, in Pensacola, Florida. Analyses were conducted using the following methodologies:
• VOCs by EPA Method 8260
• SVOCs by EPA Method 8270 • VPH/EPH by MADEP
• Metals by EPA Methods 6010 & 7470 • Hexavalent chromium by EPA Method 7196 • Pesticides by EPA Methods 8011 & 8081 • Cyanide by EPA Method 9012 and Standard Methods 335.2 • Nitrate by Standard Methods 353.2
3.0 INVESTIGATION RESULTS
3.1 Site Geology and Hydrology
Based on observations made during sampling, the sampled harbor bottom consisted of fine grained, poorly consolidated mud. The eastern-most sample (CK-10) consisted of fine grained sand with live clams and shells.
3.2 Analytical Results and Evaluation
Laboratory analytical results for the sediment samples are summarized in Table 1. The
laboratory analytical data reports are included in Appendix A.
Sediment analytical results were compared to limiting RECAP screening standards. The
limiting RECAP screening standard for each COC is the more conservative of Soil_SSni (protective of a residential scenario) and Soil_SSGW (protective of the soil to groundwater risk pathway). Arsenic and lead were detected in excess of limiting RECAP screening standards in four samples. No other analyzed COCs were detected in excess of limiting RECAP screening standards.
Arsenic was detected at CK-2 at 14 milligrams per kilogram (mg/kg), which exceeds the
RECAP Soil_SSni concentration of 12 mg/kg. Because the RECAP Soil_SSni is based on a background concentration, RECAP allows for the mean concentration of the analyzed arsenic concentrations to be compared to the standard. The mean of the 11 collected
samples is 9.07 mg/kg, which is below the limiting RECAP screening standard concentration for arsenic.
Lead was detected in excess of the RECAP Soil_SSGW in three samples (CK-1, CK-1 Dup, and CK-3). A Synthetic Precipitation Leaching Procedure (SPLP) analysis of the sample exhibiting the highest lead concentration (CK-1) was conducted. The SPLP result was compared to the RECAP Groundwater Class 1 (GWl) standard multiplied by 20 in
2 CK Associates
New Orleans Municipal Yacht Harbor
Sediment Sampling and Analysis
accordance with RECAP guidance. The results are summarized in Table 2. The detected SPLP concentration of 0.025 milligrams per liter (mg/L) does not exceed the GWl x 20 value of 0.3 mg/L; therefore, the detected lead concentrations can be compared to the limiting Soil_SSni standard of 400 mg/kg. Lead concentrations do not exceed 400 mg/kg in any of the sampled sediment.
Due to the high moisture content of the samples (ranging from 24.9% at CK-10 to 79.1% at CK-4), detected concentrations were reported on a dry weight basis. The adjustment for moisture content caused elevated reporting limits in some samples for some COCs. None of these COCs were detected. The elevated reporting limits exceed the Soil_SSGW for 1,1,2,2-tetrachloroethane, 1,1,2-trichloroethane, 1,1-dichloroethene, l,2-dibromo-3-chloropropane, methylene chloride, and aniline. The reporting limit for thallium exceeds the Soil_SSni for most of the samples.
4.0 SUMMARY AND CONCLUSIONS
CK performed sediment sampling and analysis at the New Orleans Municipal Yacht Harbor in order to determine current concentrations of potential COCs within the material to be dredged.
Arsenic was detected in one sample in excess of the limiting screening standard concentration, but the average of all samples did not exceed the limiting screening standard.
Lead was detected in three samples in excess of the limiting screening standard concentration (Soil_SSGW). The sample exhibiting the highest lead concentration was further analyzed for SPLP lead. The results of the SPLP analysis indicated that the lead concentration is protective of the soil to groundwater risk pathway. None of the samples contained lead concentrations in excess of the Soil_SSni standard.
Seven COCs were reported as not detected at a reporting limit that exceeded the RECAP limiting standard. The reporting limits were elevated due to the dry weight correction applied to the analytical results. There is no indication that these COCs are present in the sampled material.
The sediment sampling and analyses indicate that the sampled sediment does not contain any analyzed COCs in excess of RECAP limiting screening standards. Concentrations present in the sampled material are protective of potential receptors in a non-industrial use scenario.
3 CK Associates
FIGURES
Moffat & Nichol Baton Rouge, Louisiana
New Orleans Municipal Yacht Harbor Sediment Sampling and Analysis
Orkans P<lrish Site Location Map
Orleans Parish
Drawn: CPVAMl0.4 Checked: JAL
0 3,000 6,000
Feet • esri CK ASSOCIATES
i,~,\-{,Off.~O"i (,,,,,,,!>eh
:::: ""'.'.:::""~
A roved: JAL
Date:
f)i.vg. No.:
01/31/20_"!_? ___ "'
A14436-0l
Reference: U.S.G.S 24K Series Quad Map, Spanish Fort, lA. Figure 1
Legend
,t;? Sample Points
Dredge Limits
0 225
Feet
Imagery: USDA FSA, NA!P 2015.
4$0
N
+ s
• esri P•t\o.,
N~h'"''" ""'"
Moffat & Nichol Baton Rouge, Louisiana
New Orleans Municipal Yacht Harbor Sediment Sampling and Analysis
Sample Location Map
Orleans Parish
Drawn: CPVAMl0.11 Checked: JAL
A roved: JAL
Daw: 01/31/2017
Dwg. No.: A14436-02
Figure 2
TABLES
,, <;
~~11~1~ ;;};t;f} '.fiti
3::: ... 0 ~' 0 ... <» '>" O\' <T> m C1>
~~~:~~~ ii:!
~ " 0 025 )g o o~.· ~ ~ .
~ ~ ;'!; ~ ;'!; $'?~'?'?
""
"' "' ~ 0 °' O•. C() w N r<
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8 8 '? • ~ ci ci
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•"s~ ""gw tj~ 000 v.<?vvv'ij
~ ~ "' ;; '?'?'?'?
::.1"'"' <?'??'?
~ ~ :;;;' ;; '?'?'?'?
~ ~;;:; ~ '? '? '? '?
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~>
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~8". 8, ~ 8 .. B '? ';:; •
Analyte Units Xylenes, Total mg/Kg
Zinc mg/Kg
Fl: MS and/or MSD Recovery Is outside accept~nce limits.
fZ, MS/MSD RPO exceeds control limits
•: LCS or LCSO i$ outside acceptance limits.
Soll_SSGW
''° 2800
J: Detected concentration is between the MDL and RDL; value is estimated
bold font Indicates a detected COC
highlighed concentrations ~ceed R~CAP limiting standard
CK-l
l/ll/2017 Soil_S$ni ll;lOAM
" <:0.0070
2300 ''°
Tablo l New Or!oan$ Municipal Yacht Harbor
S11dlm•mt Analyti~al Summary
CK·l Oupli<:ato CK·2 CK·3
l/ll/2017 l/ll/2017 1/11/2017 12:00 PM ll:40AM 12:15 PM
<:0.0069 <:0.0098 <:0.0078
'" "' '"
CK~ CK·S CK·G CK-7 CK-S CK·9 CK·lO
1/11/2017 1/11/2017 1/13/2017 l/13/2017 l/13/2017 1/13/2017 1/13/2017
12:30 PM l:lS PM 9:30AM 9:4SAM 10:10 AM l0'.2SAM 10'.45 AM
<:0.0099 <:0.16 <:0.0049 <:0.0080 <:0.0039 <0.0049 <0.0026
'" 150 ''° 200 " 93 "
Page S of S
Analyte Units
CK-1 RECAP GWl 1/11/2017
x20 ll:lOAM
Table 2
New Orleans Municipal Yacht Harbor
SPLP Summary
J: Detected concentration is between the MDL and RDL; value is estimated
APPENDIX A
LABORATORY REPORTS
The tparaand at th
This inten
Resu
est results in this repoit meet all 2003 NELAC and 2009 TN! requirements for accredited meters, exceptions are noted in this report. This repott may not be reproduced except in fufl, with Vfritten approval front the laboratory For questions please contact the Project Alfanager e e-mail address or telephone number fisted on this page.
report has been electronically signed and authorized by the signato1y. Electronic signature is ded to be the legally binding eqwVafent of a traditionally handwritten signature.
lts relate only to the items tested and tile san1pfe(s) as received by tile Jaboraloty.
THE LEADER IN ENVIRONMENTAL TESTING
ANAL YTICAl REPORT TestAmerica Laboratories, Inc. TestAmerica Pensacola 3355 Mclemore Drive Pensacola, FL 32514 Tel: (850)474-1001
TestArnerica Job ID: 400-132540-1 Client Project/Site: Moffat & Nichol
For: C-K Associates 17170 Perkins Road Baton Rouge, Louisiana 70810
Attn: Jennifer Lindquist
C}--W~ Authorized for release by: 21112017 3:17:01 PM
Jason Wilson, Project Manager I (251 )706-3217 [email protected]
Client: C-K Associates Project/Site: Moffat & Nichol
Table of Contents
TestAmerica Job ID: 400-132540-1
Cover Page .................. _ . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71 Chronicle .. _ . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124 Certification Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 135 Chain of Custody. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 136
Page 2 of 140 TestAmerica Pensacola
2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
Job ID: 400-132540-1
Laboratory: Tes!America Pensacola
Narrative
Comments No additional comments.
Receipt The samples were received on 1/12/2017 9:21 AM, 1/12/2017 4:57 PM and 1/14/2017 8:32 AM: the samples arrived in good condition, properly preserved and, \vhere required, on ice. The ten1peratures of the 8 coolers at receipt time were 1.0° C, 1.9° C, 2.0° C, 2.1° C, 2.2° c, 2.4° C, 2.7° C and 4.0° C.
GC/MSVOA Method(s) 8260C: The laboratory control sample (LCS) for analytical batch 400-338529 recovered outside control limits for one analyte. This analyte was biased high in the LCS and was not detected in the associated samples: therefore, the data have been reported.
Method(s) 8260C: Sample RB-2 (400-132650-6) contains met11ylene chloride. Reanalysis was performed with concurring results.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA Method(s) 8270D: The method blank for preparation batch 400-338284 and analytical batch 400-338574 contained Diethyl phthalate, Bis(2-ethylhexyl) phthalate and Di-n-octyl phthalate above the method detection limit. This target analyte concentration was less than the reporting limit {RL); therefore, re-extraction andfor re-analysis of samples was not performed.
Method(s) 8270D: The %RPD of the laboratory control standard duplicate (LCSD) for preparation batch 400-338284 recovered outside control limits for the following analytes: 2,4-0initrophenol and Pentachlorophenol.
Method(s) 8270D: The matrix spike I matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-338556 and analytical batch 400-3387 41 were outside control limits. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.CK-5 (400-132588-6[MS]) and CK-5 (400-132588-6[MSD))
Method(s) 8270D: The method blank for preparation batch 400-340079 and analytical batcll 400-340421 contained Di-n-octyl phthalate above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction andfor re-analysis of samples was not performed.
Method(s) 8270D: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation batch 400-340079 recovered outside control limits for the following analytes: 2,4-Dinitrophenol.
Method(s) 8270D: The laboratory control sample duplicate (LCSD) for preparation batch 400-339125 and 400-340079 and analytical batch 400-339188 recovered outside control limits for the flagged ana!ytes. The associated sample(s) was re-prepared andtor re-analyzed outside holding time. Both sets of data have been reported.
Method(s) 8270D: The method blank for preparation batch 400-339125 and analytical batch 400-339188 contained Diethyl phthalate and Di-n-octyJ phthalate above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re~analysis of samples was not performed.
Method(s) 82700 LL: Three surrogates are used for thls analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria without performing re-extractionfre-analysis. The following sample contained an allowable nun1ber of surrogate compounds outside limits: (MB 400-33828411-A). These results have been reported and qualified.
No additional analytical or quality issues were noted, other than those described above or in the Definitions!Glossary page.
GCVOA No analytical or quality issues were noted, other than those described in the DefinitlonstGlossary page.
Case Narrative
Job Narrative 400-132540-1
TestAmerica Job ID: 400-132540-1
Page 3 of 140 TestAmerica Pensacola
211/2017
Client: C-K Associates ProjecUSite: Moffat & Nichol
Job ID: 400-132540-i (Continued)
Laboratory: TestAmerica Pensacola (Continued)
Case Narrative TestAmerica Job ID: 400-132540-1
GC Semi VOA Method(s) 80818: Physical properties (viscosity, color, odor) of the following sample(s) extract preclude concentrated analysis \Vhich would jeopardize instrumentation. Minimal dilution with elevated Rls is reported. CK-1 (400-132588-1), CK-2 (400-132588-2), Duplicate (400-132588-3), CK-3 (400-132588-4) and CK-4 (400-132588-5).
Method{s) MA-EPH: The fractionation surrogates 2-Bromonaphthalene and/or 2-Fluorobiphenyl are outside control limits for the following samples: RINSATE 1 (400-132540-1 ), RB-2 (400-132650-6) and (LCSD 400-33926213-A). These surrogates are used only to indicate separation between the aliphatic and aromatic phases of the fractionation process and do not reflect recoveries from the extractions process. As these surrogates are present in the aromatic samples and not present in the aliphatic, these results have been reported.
No additional ana!yUcal or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals Method(s) 60108, 6010C: The matrix spike I matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-338528 and analytical batch 400-338847 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry Method(s) 353.2: The matrix spike I matrix spike duplicate (MSIMSD) recoveries for preparation batch 400-338576 and analytical batch 400·338609 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample {LCS) recovery was within acceptance limits.
Method(s) 353.2: The sample duplicate precision for the following san1ple associated with preparation batch 400-338576 and analytical batch 400-338609 was outside control limits: CK-5 (400-132588-6[MSD]) and (400-132588-L-1-C MSD).
Method(s) 353.2: The following sample showed a negative result greater than the absolute value of the reporting limit for CK-7 (400-132650·2). These samples were re.analyzed with a dilution and were non-detect. The diluted sample is reported as the primary analysis with the undiluted sample being reported as a secondary result.
Method(s) 7196A: The matrix spike I matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-339244 and analytical batch 400·339470 were outside control limits. sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample {LCS) recovery was within acceptance limits.
Method(s) 90128: The matrix spike duplicate (MSD) recoveries for preparation batch 400-339068 and analytical batch 400-339005 were outside control limits. Non-homogeneity is suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep Method(s} 3520C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSDIDUP) associated with preparation batch 400-338429.
Method{s) 3520C: Insufficient sample volume \Vas available to perform a matrix spike/matrix spike duplicate/sample duplicate (MSIMSDIDUP) associated with preparation batch 400-339262.
Method(s) 3520C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSDIDUP) associated with preparation batch 400-339262.
Method(s) 3520C: Insufficient sample volume \vas available to perform a matrix splke/matrix spike duplicate/sample duplicate (MS/MSDIDUP) associated with preparation batch 400-338239.
Method(s) 3520C: Insufficient sample volume was available to perfonn a matrix spike/matrix spike duplicate/sample duplicate
Page 4of140 T estAmerica Pensacola
2/112017
Case Narrative Client: C-K Associates ProjecUSite: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Job ID: 400-132540-1 (Continued)
Laboratory: TestAmerica Pensacola (Continued)
(MS/MSD/DUP) associated with preparation batch 400-338284.
Method(s) 3520C: Insufficient sample volume \Vas available to perfonn a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 400-339054.
Method(s) 3520C: Insufficient sample volume \Vas available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 400-339125.
Method(s) 3520C: Insufficient sample volume \Vas available to perforn1 a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 400-340079.
Method(s) 3520C: The following sample was re-prepared outside of preparation holding time due to low LCSD: RB-2 (400-132650-6).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Lab Admin No analytical or quality issues were noted, other than those described ln the Definitions/Glossary page.
Page 5 of 140 TestAmerica Pensacola
2/112017
Client: C-K Associates ProjecUSite: Moffat & Nichol
Sample Summary TestAmerica Job ID: 400-132540-1
Lab Sample ID Client Sarnple ID Matrix Collected Received 400-132540-1 RINSATE 1 Water 01/11/1713:20 01112117 09:21
400-132588-1 CK-1 Solid 01/11/1711:10 01/12117 16:57
400-132588-2 CK-2 Solid 01/11117 11:40 01112117 16:57
400-132588-3 Duplicate Solid 01/11/17 12:00 01112117 16:57
400-132588-4 CK-3 Sol!d 01/11/17 12:15 01/12117 16:57 400-132588-5 CK-4 Solid 01/1111712:30 01/1211716:57
400-132588-6 CK-5 Solid 01/11117 13:15 01/1211716:57
400-132650-1 CK-6 Solid 01/13117 09:30 01/14/17 08:32
400-132650-2 CK-7 Solid 01/13117 09:45 01/14117 08:32 400-132650-3 CK-8 So!id 01113117 10:10 01/14117 08:32
400-132650-4 CK-9 Solid 01/13/17 10:25 01114117 08:32
400-132650-5 CK-10 Solid 01/13117 10:45 01114117 08:32
400-132650-6 RB-2 Water 01/1311711:00 01114117 08:32
Page 6 of 140
TestAmerica Pensacola
2/112017
m
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project!Site: Moffat & Nichol
Client Sample ID: RINSATE 1 Lab Sample ID: 400-132540-i Date Collected: 01111/17 13:20 Matrix: Water Date Received: 01112117 09:21
Method: 8260C - Volatile Organic Compounds by GCIMS E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
1, 1, 1,2-Tetrachloroethane <0.00052 0.0010 0.00052 mg/L 01/16/17 09:43 1
1, 1, 1-Trichloroethane <0.00050 0.0010 0.00050 mg/L 01/16/17 09:43
1, 1,2,2-Tetrachloroethane <0.00050 0.0010 0.00050 mg/L 01/16/17 09:43
1, 1,2-Trich!oroethane <0.00050 0.0050 0.00050 mg/L 01/16/17 09:43
1, 1-Dich!oroethane <0.00050 0.0010 0.00050 mg/L 01116117 09:43
1, 1-Dichloroethene <0.00050 0.0010 0.00050 mg/L 01/16117 09:43
1,2,4-Trichlorobenzene <0.00082 0.0010 0.00082 mg IL 01116/17 09:43
1,2-0ibromo-3-Ch!oropropane <0.0015 0.0050 0.0015 mg/L 01116/17 09:43
1,2-Dich!orobenzene <0.00050 0.0010 0.00050 mg/L 01116117 09:43
1,2-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01/16117 09:43
1,2-Dichloropropane <0.00050 0.0010 0.00050 mg/L 01116/17 09:43
1,3-Dich!orobenzene <0.00054 0.0010 0.00054 mg/L 01116/17 09:43
1,4-Dichlorobenzene <0.00064 0.0010 0.00064 mg/L 01116117 09:43
2-Butanone (MEK) <0.0026 0.025 0.0026 mg/L 01/16/17 09:43
4-Methyl-2-pentanone (MIBK) <0.0018 0.025 0.0018 mg IL 01116117 09:43
Acetone <0.010 0.025 0.010 mg/L 01116117 09:43
Benzene <0.00038 0.0010 0.00038 mgll 01/16/17 09:43
Bromoform <0.00071 0.0050 0.00071 mg/L 01116117 09:43
Bromomethane <0.00098 0.0010 0.00098 mg/L 01116/17 09:43
Carbon disulfide <0.00050 0.0010 0.00050 mg/L 01116117 09:43
Carbon tetrachloride <0.00050 0.0010 0.00050 mg/L 01/16117 09:43
Chlorobenzene <0.00050 0.0010 0.00050 mg/L 01116/17 09:43
Ch!orodibromomethane <0.00050 0.0010 0.00050 n1g/L 01116117 09:43
Chloroethane <0.00076 0.0010 0.00076 mg IL 01116/17 09:43
Chloroform <0.00060 0.0010 0.00060 mg/L 01116/17 09:43
Ch!oromethane <0.00083 0.0010 0.00083 mg IL 01116/17 09:43
cis· 1,2·Dich!oroethene <0.00050 0.0010 0.00050 mg/L 01116117 09:43
cis-1,3·Dichloropropene <0.00050 0.0050 0.00050 mg/L 01/16/17 09:43
Oich/orobromomethane <0.00050 0.0010 0.00050 mg/L 01116117 09:43
Ethylbenzene <0.00050 0.0010 0.00050 mg/L 01/16117 09:43
lsobutyl alcohol <0.010 0.025 0.010 mg/L 01/16/17 09:43
Methyl tert·butyl ether <0.00074 0.0010 0.00074 mg/L 01/16117 09:43
Methylene Chloride <0.0030 0.0050 0.0030 mg/L 01/16117 09:43
Styrene <0.0010 0.0010 0.0010 mg/L 01116/17 09:43
Tetrach!oroethene <0.00058 0.0010 0.00058 mg IL 01116117 09:43
Toluene <0.00070 0.0010 0.00070 mg/L 01116/17 09:43
trans· 1,2-Dichloroethene <0.00050 0.0010 0.00050 mg/L 01/16/17 09:43
trans· 1,3·Dich!oropropene <0.00050 0.0050 0.00050 mg/L 01116117 09:43
Trichloroethene <0.00050 0.0010 0.00050 mg/L 01116/17 09:43
Trich!orofluoromethane <0.00052 0.0010 0.00052 mg IL 01116/17 09:43
Vinyl chloride <0.00050 0.0010 0.00050 mg IL 01116117 09:43
Xy!enes, Total <0.0016 0.010 0.0016 mg/L 01116117 09:43
Surrogate %Recovery Qualifier Lltnlts Prepared Analyzed DI/ Fae
4-Bromoffuorobenzene 101 78-118 0111611709:43 1
Dibromofluoromethane 103 81 - 121 0111611709:43
Toluene-dB (Surr) 102 80.120 01116117 09:43
TestAmerica Pensacola
Page 7 of 140 2/1/2017
Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: RINSATE 1 Date Collected: 01111/1713:20 Date Received: 01/12/17 09:21
Method: 82700 LL. Semivolatile Organic Compounds by GCIMS ·Low Level Analyte Result Qualifier RL MDL Unit Acenaphthene <0.000030 0.00019 0.000030 mgfl
Acenaphthylene <0,000042 0.00019 0.000042 mg/L
Anthracene <0.000030 0.00019 0.000030 mg/L
Benzo[a]anthracene <0.000043 0.00019 0.000043 mg/L Benzo[a]pyrene <0.000040 0.00019 0.000040 mg/L
Benzo[b}fluoranthene <0.000032 0.00019 0.000032 mg/L
Benzo[k]fluoranthene
Chrysene
Dibenz(a,h)anthracene
Fluoranthene
Fluorene
lndeno[1,2,3-cd]pyrene
2-Methylnaphtha!ene
Naphthalene
Phenanthrene
Pyrene
Surrogate 2·Fluorobiphenyl
Nitrobenzene-d5 Terphenyi-d14
<0.000094 <0.000070 <0.000047
<0.000064 <0.00010
<0.000041
<0.000057 <0.000089 <0.000034
<0.000038
%Recovery Qual/fier
92
84 107
0.00019
0.00019 0.00019
0.00019 0.00019 0.00019
0.00019 0.00019 0.00019 0.00019
Ll1nlts 15-122
19-130
33-138
Method: 82700 • Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Anillne <-0.,0036 0.0094
1, 1'-Biphenyl <0.00016 0.0094 Bis(2·ch!oroethyl)ether
bis (2-ch!oroisopropyl) ether
Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
2-Ch!oropheno!
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate 2,4-Dimethylpheno!
Dimethyl phtha!ate
1,3-Dinitrobenzene
2,4-Dinitrophenot
2.4-Dinitrotoluene
2,6-Dinitrotoluene
Oi-n-octyl phthafate Hexachlorobenzene
Hexachlorobutadiene
Hexach!orocyclopentadiene
Hexachloroethane
lsophorone
2-Nitroaniline
<0.0025
<0.00015
0.0064 J B <0.00018
<0.0032
<0.00013 <0.0021
<0.00016
<0.0025
<0.0028
0.00067 J B <0.0033
<0.00016 <0.00094 <0.0032
<0.0018 <0.0018
0.00019 J B <0.00016
<0.00052
<0.0025 <0.0040
<0.00013 <0.0021
0.0094 0.0094
0.0094 0.0094 0.0094 0.0094
0.0094 0.0094
0.0094 0.0094
0.0094 0.0094 0.0094
0.0094 0.028
0.0094 0.0094
0.0094 0.0094
0.0094 0.019
0.0094
0.0094 0.0094
0.000094 mg/L
0.000070 m9/L 0.000047 m9/L
0.000064 m9/L 0.00010 m9/L
0.000041 mg/L
0.000057 mg/L 0.000089 mg/L 0.000034 mg/L
0.000038 m9/L
MDL Unit 0.0036 mg/L
0.00016 mg/L 0.0025 mg/L
0.00015 mg/L
0.0019 mg/L
0.00018 mg/L 0.0032 mg/L
0.00013 mgiL 0.0021 mg/L
0.00016 mg/L
0.0025 mg/L 0.0028 mg/L
0.00023 mg/L 0.0033 mg/L
0.00016 mg/L
0.00094 mg/L 0.0032 mg/L 0.0018 mg/L
0.0018 mg/L 0.00016 mg/L 0.00016 mg/L
0.00052 mg/L 0.0025 mglL 0.0040 mg/L
0.00013 mg/L 0.0021 mg/L
Page 8 of 140
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132540-1 Matrix: Water
D Prepared
01112117 16:23 0111211716:23
Analyzed
01116/17 18:58 01116/17 18:58
0111211716:23 01/16/1718:58
0111211716:23 01/1611718:58 01/1211716:23 01/16/17 18:58 01/1211716:23 0111611718:58
01/12117 16:23 01116117 18:58 01/12117 16:23 0111611718:58 01/12117 16:23 0111611718:58 01112117 16:23 01116/17 18:58
01112117 16:23 01/16117 18:58 0111211716:23 01/16/1718:58
01/12117 16:23 01/16/17 18:58 01/1211716:23 01/16/17 18:58 01/12117 16:23 01/16/1718:58
01/1211716:23 01/1611718:58
Prepared
0111211716:23
0111211716:23
Analyzed
0111611718:58
0111611718:58
0111211716:23 0111611718:58
Oil Fae
1
1
Oil Fae
1
D Prepared Analyzed 01116/17 21:32
01116/17 21:32
Oii Fae
1 01/1211716:23
01/1211716:23 01/1211716:23 01116117 21:32 0111211716:23 01116117 21:32
0111211716:23 01116117 21:32 0111211716:23 01116117 21:32 01/1211716:23 01116/17 21:32 01/12/1716:23 01/16/17 21:32
0111211716:23 01/16/17 21:32 01/1211716:23 01/16/17 21:32
0111211716:23 01116117 21:32 0111211716:23 01/16/17 21:32
01/1211716:23 01116117 21:32 01112117 16:23 01116117 21:32
01/1211716:23 01116117 21:32 0111211716:23 01116117 21:32 01/1211716:23 01116/17 21:32
01/1211716:23 01116/17 21:32 01/1211716:23 01/16/17 21:32
01112117 16:23 01/16/17 21:32 01/1211716:23 01/16/17 21:32
0111211716:23 0111611721:32 0111211716:23 01116117 21:32 0111211716:23 01116117 21:32 0111211716:23 01116117 21:32 0111211716:23 0111611721:32
T estAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Client Sample ID: R!NSATE 1 Lab Sample ID: 400-132540-1 Date Collected: 01/11/i? 13:20 Matrix: Water Date Received: 01/12117 09:21
Method: 82700 - Semivolatile Organic Compounds (GC/MS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
3-Nitroaniline <0.0017 0.0094 0.0017 mg/L 01/1211716:23 01/16/17 21:32 1 4-Nitroani!ine <0.0014 0.0094 0.0014 m9/L 01/12117 16:23 01/16117 21:32
Nitrobenzene <0.00012 0.0094 0.00012 mg/L 01/1211716:23 01/16/17 21:32
4-Nitropheno1 <0.0020 0.0094 0.0020 m9/L 01/12117 16:23 01/16117 21:32 N-Nitrosodi-n-propylamine <0.0031 0.0094 0.0031 mg/L 01/1211716:23 01/16/17 21:32
N-Nitrosodiphenylamine <0.00017 0.0094 0.00017 mg/L 01/1211716:23 01116117 21:32
Pentachloropheno! <0.0013 0.019 0.0013 mg/L 01/12117 16:23 01116/17 21:32
Phenol <0.0025 0.0094 0.0025 mg/L 01 /12117 16:23 01116/17 21:32
1,2,4,5-T etrachlorobenzene <0.00017 0.0094 0.00017 mg/L 01/1211716:23 01/16117 21:32
2,3,4,6-T etrachlorophenol <0.0015 0.0094 0.0015 mg/L 01/12117 16:23 01/1611721:32
1,2,4-Trichlorobenzene <0.00017 0.0094 0.00017 m9/L 01112117 16:23 01/16117 21:32 2,4 ,5-Trichlorophenol <0.0035 0.0094 0.0035 mg IL 01112117 16:23 01116/17 21:32
2,4 ,6-Trichlorophenol <0.0033 0.0094 0.0033 mg/L 01/1211716:23 01/16/17 21:32
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae
2-Ffuorobiplienyl 72 46-124 0111211716:23 01116117 21:32 1 2-Fluorophenol 47 13-113 0111211716:23 01116117 21:32
Nitrobenzene-d5 73 36- 126 0111211716:23 01116117 21:32
Phenol-d5 66 17 -127 0111211716:23 01116117 21:32 Terphenyl-d14 98 44 - 149 01112117 16:23 01116117 21:32
2,4, 6-T ribromophenol 70 26-150 0111211716:23 01116117 21:32
Method: MAVPH. Massachusetts• Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae C6-C8 A!iphatics <0.030 0.030 0.030 mg/L 01/19/17 22:24
C8-C 10 AHphatics <0.050 0.050 0,050 mg/L 01/19/17 22:24
C8-C10 Aromatics <0.025 0.025 0.025 m9/L 01/19/17 22:24
Surrogate %Recovery Qualifier Lim/ls Prepared Analyzed DJ/ Fae 8,a,a-Trifluorotoluene (fid) 101 70-130 01119117 22:24 1
a,a,a-Trifluorotoluene (pid) 103 70-130 01119117 22:24 1
Method: 8011 • EDB, DBCP, and 1,2,3-TCP (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae 1,2-Dibromo-3-Ch!oropropane <D.0000056 0.000031 0.0000056 mg/L 01/23/1716:25 01127/17 00:09 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae 4-Bron1ofluorobenzene 113. 51-149 0112311716:25 01127117 00:09 1
Method: 8081 B • Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae
Aldrin <0.0000012 0.000019 0.0000012 mg/L 01/1211716:15 01/19/1713:41 1
alpha-BHC 0.0000042 J B 0.000019 0.0000014 m9/L 01/1211716:15 01/19/1713:41 1 beta-BHC <0.0000012 0.000019 0.0000012 m9/L 0111211716:15 01/19/17 13:41
delta-BHC 0.0000084 JB 0.000019 0.0000008 mg/L 01/1211716:15 01/1911713:41
1 gamma-BHC (Undane) <0.0000096 0.000019 0.0000096 mg/L 01/1211716:15 01119/17 13:41
alpha-Chlordane <0.0000016 0.000019 0.0000016 mg/L 0111211716:15 01119117 13:41
gamin a-Chlordane 0.0000034 J 0.000019 0.0000012 mg/L 01/1211716:15 01119/1713:41 4,4'-DDD <0.0000012 0.000019 0.0000012 m9/L 01/1211716:15 01119/1713:41
TestAmerica Pensacola
Page 9of140 2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Client Sample !D: RINSATE 1 lab Sample !D: 400-132540-1 Date Collected: 01111/1713:20 Matrix: Water Date Received: 01112/17 09:21
Method: 8081 B • Organochlorlne Pesticides (GC) (Continued)
Ee
1 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fa
4,4'-DDE <0.00000085 0.000019 0.0000008 mg/L 01/12/1716:15 01/19/17 13:41
5 4,4'-DDT <0.0000015 0.000019 0.0000015 mg/L 01/12/1716:15 01/19/1713:41
Dieldrin 0.0000043 JB 0.000019 0.0000012 mg/L 01/12/1716:15 01/19/1713:41
Endosu!fan I <0.0000012 0.000019 0.0000012 mg/L 01/12/1716:15 01/19/17 13:41
Endosulfan H <0.0000028 0.000019 0.0000028 mg/L 01/12/1716:15 01/19/17 13:41
Endosulfan sulfate <0.00000081 0.000019 0.0000008 mg/L 01/12/1716:15 01/19/17 13:41 1
Endrin <0.0000012 0.000019 0.0000012 mg/L 01/12/1716:15 01/19/1713:41
Endrin aldehyde <0.0000011 0.000019 0.0000011 mgll 01/12/1716:15 01/19117 13:41
Endrin ketone <0.0000015 0.000019 0.0000015 mg/L 01112/1716:15 0111911713:41
Heptachlor <0.0000012 0.000019 0.0000012 mg/L 01/12/1716:15 0111911713:41
Heptach!or epoxide <0.0000012 0.000019 0.0000012 mg/L 01/12/1716:15 01119/17 13:41
Methoxychlor <0.0000016 0.000019 0.0000016 mg/L 01112/1716:15 01/19/17 13:41
Toxaphene <0.00012 0.0012 0.00012 mg/L 01/12/1716:15 0111911713:41
Surrogate %Recovery Qualifier Lin1its Prepared Analyzed Di/ Fae
DCB Decachforobiphenyl 55 10-130 0111211716:15 0111911713:41 1
Tetrachloro·m·xylene 99 43-130 0111211716:15 01119117 13:41
Method: MA-EPH • Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
C10-C12 A!iphatlcs <0.047 0.047 0.047 mg/L 01120/17 15:54 01126117 17:25 1
C12-C16 Aliphatics <0.047 0.047 0.047 mg/L 0112011715:54 01126117 17:25
(;16-C35 Aliphatics <0.047 0.047 0.047 mg/L 01120/1715:54 01/26117 17:25
C10·C12 Aromatics <0.047 0.047 0.047 mg IL 01/2011715:54 0112611719:59
C12-C16 Aromatics <0.047 0.047 0.047 mg/L 01/2011715:54 0112611719:59
C16-C21 Aromatics <0.047 0.047 0.047 mg/L 0112011715:54 01126117 19:59
C21-C35 Aromatics <0.047 0.047 0.047 mg IL 01/20/17 15:54 0112611719:59
Surrogate %Recovery Qualifier Limits Prepared Analyzed DJ/ Fae
1-Chlorooctadecane 89 40. 140 01120117 15:54 0112611717:25 1
o-Terphenyl 63 40.140 0112011715:54 01126117 19:59 1
2-Bromonapht/1alene 14 40-140 01120117 15:54 0112611719:59
2-Fluorobiphenyl 46 40.140 0112011715:54 0112611719:59
Method: 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed OJI Fae Silver <0.0020 0.0050 0.0020 mg IL 01113117 08:50 01/16/1717:16 1
Arsenic <0.0040 0.010 0.0040 mg/L 01113/17 08:50 0111611717:16 1
Barium <0.0020 0.010 0.0020 mg/L 01113/17 08:50 01116117 17:16
Beryllium <0.0010 0.0030 0.0010 mg/L 01/13/17 08:50 01116117 17:16
Cobalt <0.0030 0.010 0.0030 mg/L 01113/17 08:50 01116117 17:16
Chromium <0.0020 0.010 0.0020 mg/L 01/13/17 08:50 01116117 17:16
Copper <0.0020 0.020 0.0020 mg/L 01/13/17 08:50 01116117 17:16
Nickel <0.0030 0.0050 0.0030 mg/L 01/13/1708:50 01/16117 17:16
Lead <0.0020 0.010 0.0020 mg/L 01113/17 08:50 01/16117 17:16
Selenium <0.0040 0.020 0.0040 mg/L 01113/17 08:50 01/16/1717:16
Tham um <0.0040 0.010 0.0040 mg/L 01113117 08:50 0111611717:16
Vanadium <0.0030 0.020 0.0030 mg IL 01/13/17 08:50 01/16/1717:16
Zinc <0.0080 0.020 0.0080 mg/L 01113/17 08:50 0111611717:16
TestAmerica Pensacola
Page 10of140 211/2017
Client: C-K Associates ProjecUSite: Moffat & Nichol
Method: 7470A - Mercury {CVAA) Analyfe Result
Mercury <0.000070
General Chemistry Analyte Result
Cyanide, Total <0.0035
Nitrate Nitrite as N <0,018
Chromium, hexavalent <0.0065
Client Sample Results
Qualifier RL MDL Unit
0.00020 0.000070 mg/l
Qualifier RL MDL Unit
0.0050 0.0035 mg/L
0.050 0.018 mg/L
0.010 0.0065 mg/L
Page 11 of 140
TestAmerica Job ID: 400-132540-1
D Prepared Analyzed Di! Fae
01113/17 08:15 01113117 12:58
E D Prepared Analyzed Oil Fae
01117117 09:30 01117117 14:18 1
01/13117 13:30 1
01112/17 10:56
TestAmerica Pensacola
21112017
Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: CK-1 Date Collected: 01/11117 11:10 Date Received: 01/1211716:57
Method: 8260C • Volatile Organic Compounds by GCIMS Analyte Result Qualifier 1, 1, 1,2-Tetrachloroethane <0.0092 1, 1, 1 -Trichloroethane 1, 1,2,2-T etrach!oroethane 1, 1,2-Trichloroethane 1, 1-Dlch!oroethane 1.1-Dichloroethene 1,2-Dibronio-3-Chloropropane
1,2-Dich!orobenzene 1,2-Dlchtoroethane 1,2-Dichloropropane
1,3-Dichlorobenzene 1,4-Dich!orobenzene Acetone Benzene Bromoform Bromomethane Carbon disulfide
Carbon tetrachloride
Ch!orobenzene Chtorodibromomethane
Chloroethane Chloroform Chloromethane
cis-1,2-Dich!oroethene cis-1 ,3-Dichloropropene Dichlorobromomethane
Ethylbenzene Methyl tert-butyl elher Methylene Chloride 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK)
Styrene Tetrachloroethene
Toluene trans, 1 ,2-Dich!oroethene
trans· 1, 3·Dlchf oropropene Trich!oroethene
Trichlorofluoromethane
Vinyl chloride Xy!enes, Total 1,2,4-Trichlorobenzene
lsobutyl alcohol
Surrogate 4-Bromoffuorobenzene Dibromoffuoromethane
Toluene-dB (Surr)
<0.0040
<0.0092
<0.0092
<0.0031 <0.0092
<0.012
<0.0026 <0.0030
<0.0092 <0.0035 <0.0092
0.20 <0.0025 <0.0092 <0.0092
<0.0092 <0.0062
<0.0019
<0.0092 <0.0092
<0.0092 <0.0037 <0.0028
<0.0044 <0.0092
<0.0022
<0.0037 <::0.037
0.030 J <0.018
<0.0037
<0.0092 <0.0037
<0.0092 <0.0092 <0.0037
<0.0092
<0.0092 <0.0070 <0.0074 <0.037
%Recovery Qualifier
100
102
94
RL 0.018 0.018 0.018
0.018 0.018 0.018
O.D18
0.018 0.018 0.018
0.018 0.018 0.092
0.018
0.018 0.018
0.018 O.D18
0.018 0.018 0.018
0.018 0.018
0.018 0.018 0.018
0.018 0.018
0.055 0.092 0.092
0.018 0.018
0.018
0.018
0.018 0.018
0.018 0.018
0.037 0.018 0.092
Li1nils
72-122
79-123
80-120
Page 12of140
MOL Unit 0.0092 mg/Kg 0.0040 mg/Kg
0.0092 mg/Kg 0.0092 mg/Kg
0.0031 mg/Kg 0.0092 mg/Kg
0.012 mg/Kg 0.0026 mg/Kg 0.0030 mg/Kg 0.0092 mg/Kg
0.0035 mg/Kg 0.0092 mg/Kg
0.027 mg/Kg
0.0025 mg/Kg
0.0092 mg/Kg 0.0092 mg/Kg
0.0092 mg/Kg
0.0062 mg/Kg 0.0019 mg/Kg 0.0092 mg/Kg 0.0092 mg/Kg
0.0092 mg/Kg 0.0037 mg/Kg 0.0028 mg/Kg
0.0044 mg/Kg 0.0092 mg/Kg 0.0022 mg/Kg
0.0037 mg/Kg 0.037 mg/Kg 0.022 mg/Kg 0.018 mg/Kg
0.0037 mg/Kg 0.0092 mg/Kg 0.0037 mg/Kg
0.0092 mg/Kg
0.0092 mg/Kg 0.0037 mg/Kg
0.0092 mg/Kg
0.0092 mg/Kg 0.0070 mg/Kg 0.0074 mg/Kg
0.037 mg/Kg
TestAmerica Job ID 400-132540-1
Lab Sample ID: 400-132588-1 Matrix: Solid
Percent Solids: 31.8
D Prepared Analyzed " 01/22117 07:44 01/22117 11:25 <) 01/22/17 07:44 01/22/1711:25
" 01/22117 07:44 01/22/1711:25 " 01/22117 07:44 01/22117 11:25
" 01/2211707:44 01/2211711:25 0 01/2211707:44 01/2211711:25
" 01/2211707:44 01/22/1711:25
" 01/22117 07:44 01/22117 11:25 ::> 01/22117 07:44 01/22117 11:25
" 01/22117 07:44 01/22/1711:25
'" 01/22117 07:44 01/22/1711:25 " 01/22117 07:44 01/2211711:25
" 01122117 07:44 01/2211711:25 " 01/22117 07:44 01/2211711:25
" 01/22117 07:44 01/2211711:25
"' 01/22117 07:44 01/2211711:25 ,, 01/2211707:44 01/2211711:25
" 01/22117 07:44 01/22/17 11:25 " 01/22117 07:44 01/22117 11:25 "' 01/22117 07:44 01/2211711:25 ,,, 01/22117 07:44 01/22117 11:25
" 01/22117 07:44 01/2211711:25 '" 01/22117 07:44 01/22117 11:25 " 01/22117 07:44 01/2211711:25
" 01/22117 07:44 01/22/17 11:25 " 01/2211707:44 01/2211711:25
" 01/22117 07:44 01/22117 11:25
"' 01/2211707:44 01/2211711:25 " 01/2211707:44 01/22/1711:25 " 01/2211707:44 01/2211711:25 ::: 01/22117 07:44 01/22117 11:25
" 01/22117 07:44 01/22/17 11:25 " 01/2211707:44 01/2211711:25
" 01/22117 07:44 01/2211711:25 ,, 01/22117 07:44 01/22117 11:25
(< 01/22117 07:44 01/22117 11:25 " 01/22117 07:44 01/22117 11:25 ,, 01/2211707:44 01/2211711:25
1) 01/2211707:44 01/2211711:25
"' 01/2211707:44 01/2211711:25 D 01/2211707:44 01/2211711:25
" 01/2211707:44 01/2211711:25
Prepared Analyzed
01122/1707:44 0112211711:25
0112211707:44 0112211711:25
0112211707:44 0112211711:25
Oil Fae
1
1
1 1
Di/ Fae
1
TestAmerica Pensacola
2/112017
Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: CK-1 Date Collected: 01111/1711:10 Date Received: 01/12/17 16:57
Method: 82700 - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene
Acenaphthylene
Aniline Anthracene Benzo[a]anthracene
Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,ijperylene Benzo[k]fluoranthene
1, 1 '-Biphenyl Bis(2-chloroethy!)ether bis (2-ch!oroisopropyl) ether
Bis(2-ethylhexyl) phlhalate
Butyl benzyl phthalate 4-Chloroaniline 2-Ch!oronaphtha!ene
2-Chlorophenol
Chrysene Dibenz(a,h)anthracene
Dibenzofuran 3,3'-Dlchlorobenzidine
2,4-Dich!oropheno1 Diethyl phthalate 2,4-Dimethylphenol
Dimethyl phthalate 1,3-Dinllrobenzene 2,4-Dinitrophenol
2,4-Dinitroto!uene 2,6-Dinltrotoluene Di-n-octyl phthalate
Fluoranthene
Fluorene Hexachlorobenzene
Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane
lndenof1 ,2,3-cdJpyrene
lsophorone 2-Methylnaphthalene Naphthalene 2-Nitroani!ine
3-Nitroaniline 4-Nitroaniline
Nitrobenzene 4-Nitropheno! N-Nitrosodi-n-propy!amine N-Nitrosodiphenylan1ine
Pentach!orophenol
Phenanthrene
<0.10
<0.10
<0.13
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.89
<0.10
<0.10
<0.10
<0.10
<0.10
<0.31
<0.10
<0.20
<0.31
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
<0.34
<0.34
<0.10
<0.20
<0.10
1.0 1.0 1.0
1.0 1.0
1.0 1.0
1.0 1.0 1.0
1.0 1.0 1.0 1.0 1.0
1.0 1.0
1.0 1.0
1.0
1.0
1.0 1.0
1.0 1.0 1.0
3.0 1.0 1.0 1.0
1.0 1.0 1.0
1.0 1.0 1.0 1.0
1.0
1.0 1.0
1.0
1.0 1.0
1.0 1.0 1.0
1.0 2.0 1.0
Page 13of140
MDL Unit
0.10 mg/Kg 0.10 mg/Kg 0.13 mg/Kg
0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg
0.89 mg/Kg 0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.31 mg/Kg 0.10 mg/Kg
0.20 mg/Kg 0.31 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg 0.10 mg/Kg
0.10 mg/Kg
0.34 mg/Kg 0.34 mg/Kg 0.10 mg/Kg 0.20 mg/Kg 0.10 mg/Kg
TestAmerica Job ID 400-132540-1
Lab Sample ID: 400-132588-1 Matrix: Solid
Percent Solids: 31.8
D Prepared Analyzed " 01/16/1709:16 01/18/1716:05 " 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05
" 01/16/17 09:16 01/18/17 16:05 "' 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/17 16:05 ':' 01/16/17 09:16 01/18/17 16:05 ;) 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05 ,, 01/16/17 09:16 01/18/17 16:05 ,,, 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/17 16:05 ,, 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/1716:05 ;:; 01/16/17 09:16 01/18/1716:05
" 01/16117 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/1716:05 ,, 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05
'" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05
" 01116/17 09:16 01/18/1716:05 ,, 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/1716:05
" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05
" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/1716:05 l'.l. 01/16/17 09:16 01/18/1716:05
" 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/17 16:05 " 01/16/17 09:16 01/18/17 16:05
" 01/16/17 09:16 01/18/1716:05 " 01/16/17 09:16 01/18/17 16:05
Dllfac E 1
1
T estAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: CK-1 Date Collected: 0111111l 11 :i O Date Received: 0111211716:57
Method: 82700 • Semivolatile Organic Compounds (GCIMS) (Continued) Analyte Result Qualifier RL MDL Unit Phenol <0.10 1.0 0.10 mg/Kg
Pyrene 1,2,4, 5-T etrachlorobenzene
2,3,4,6-T etrachlorophenol 1,2 ,4-TrlchJorobenzene 2,4,5-Trichlorophenol 2,4,6-Trich!orophenol
Surrogate 2-Fluorobiphenyl 2-F/uorophenol
Nitrobenzene-d5 Phenol-d5 Teiphenyl-d14
2, 4,6-Ttibromophenol
<0.10
<0.10
<0.10
<0.10
<0.10
<0.10
%Recovery Qualifier
92
94
82
89 109
122
1.0 1.0
1.0
1.0
1.0
1.0
Limits 27-127
25-128
15- 136
29-130
24-146
10-150
0.10 mg/Kg
0.10 mg/Kg
0.10 mg/Kg
0.10 mgiKg
0.10 mg/Kg
0.10 n1g/Kg
Method: MAVPH. Massachusetts. Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit C6-C8Atiphatics <17 17 17 mg/Kg C8-C 10 Aliphatics <29 29 29 mg/Kg
C8-C10 Aromatics
Surrogate
a,a,a-Trifluorotoluene (fid) a,a,a-Trifluorototuene (pid)
<14
%Recovery Quallfler
77
80
Method: 8081 B • Organochlorine Pesticides (GC) Analyte Result Qualifier
Aldrin <O .0095 alpha-BHC <0.0037
beta-BHC
delta-BHC
gamma-BHC (Undane) alpha-Chlordane gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dleldrin Endosulfan I Endosulfan II Endosu!fan sulfate
Endrin Endrin aldehyde
Endrin ketone Heptachlor Heptachlor epoxide Methoxychlor
Toxaphene
<0.0078
<0.0050 <0.0034
<0.0044
<0.0042
<0.0030
<0.0042
<0.012
<0.0056
<0.0033
<0.0036
<0.0033
<0.0030
<0.0045
<0.0054
<0.0037
<0.0070
<0.0051
<0.45
14
Limits 70-130
70-130
RL 0.026
0.026
0.026
0.026
0.026
0.026 0.026
0.026
0.026
0.026
0.026
0.026
0.026
0.026
0.026
0.026
0.026
0.026
0.026
0.026
1.6
Page 14 of 140
14 mg/Kg
MDL Unit 0.0095 mg/Kg
0.0037 mg/Kg
0.0078 mg/Kg
0.0050 mg/Kg
0.0034 mg/Kg
0.0044 mg/Kg
0.0042 mg/Kg
0.0030 mg/Kg
0.0042 mg/Kg
0.012 mg/Kg
0.0056 mg/Kg
0.0033 mg/Kg
0.0036 mg/Kg
0.0033 mg/Kg
0.0030 mg/Kg
0.0045 mg/Kg
0.0054 mg/Kg
0.0037 mg/Kg
0.0070 mg/Kg
0.0051 mg/Kg
0.45 mg/Kg
TestAmerica Job ID 400-132540-1
Lab Sample ID: 400-132588-1 Matrix: Solid
Percent Solids: 31.8
D Prepared
" 01116117 09:16 ,, 01116117 09:16
Analyzed 01118117 16:05
01118/17 16:05
" 01116117 09:16 01118117 16:05
" 01116117 09:16 01118117 16:05 !) 01116117 09:16 01118117 16:05
" 01116117 09:16 0111811716:05
" 01116117 09:16 01118117 16:05
Prepared Analyzed
01118117 09:16 01/18/1716:05
0111811709:16 0111811716:05
0111811709:16 0111811716:05
01118117 09:16 01118117 16:05 01118117 09:16 01/18117 16:05
0111811709:16 0111811716:05
D Prepared Analyzed
" 0111611711:00 0111611718:19
" 0111611711:00 01116117 18:19
" 0111611711:00 0111611718:19
Prepared Analyzed
0111811711:00 01118117 18:19
01116117 11:00 01118117 18:19
O Prepared Analyzed ~ 01116117 09:24 0111711718:11
" 01116117 09:24 01117117 18:11
l) 01116117 09:24 01117/17 18:11
l) 01116117 09:24 01117117 18:11
" 01116117 09:24 0111711718:11
" 01116117 09:24 01117117 18:11
1:1 01116117 09:24 01117117 18:11
" 01116117 09:24 01117117 18:11
" 0111611709:24 0111711718:11
" 01116117 09:24 0111711718:11
" 01116117 09:24 0111711718:11
l) 01116117 09:24 0111711718:11
" 01116117 09:24 0111711718:11
"' 01116117 09:24 01117117 18:11
l'.I 0111611709:24 0111711718:11
" 01116117 09:24 01117117 18:11
" 01116117 09:24 0111711718:11
,, 01116117 09:24 0111711718:11
" 01116117 09:24 01117117 18:11
" 0111611709:24 0111711718:11
" 01116117 09:24 0111711718:11
DltFac E 1
DJ/ Fae 1
1
DU Fae 50
50
50
DI/ Fae
50 50
Oil Fae 5 5 5 5 5
5
5 5 5 5 5 5 5 5 5 5 5 5 5
5 5
TestAmerica Pensacola
21112017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Client Sample ID: CK-4 Lab Sample ID: 400-132588-5 Date Collected: 0111111712:30 Matrix: Solid Date. Received: 0111211716:57 Percent Solids: 20.9
Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae
Phenol <0.16 1.6 0.16 mg/Kg 0:1 01116117 09:16 01117117 14:21 1
Pyrene 0.16 J 1.6 0.16 mg/Kg " 01/16117 09:16 01/17117 14:21 1
1,2,4,5-T etrachtorobenzene <0.16 1.6 0.16 mg/Kg " 01/16117 09:16 01/17/17 14:21
2,3,4,6-T etrachlorophenol <0.16 1.6 0.16 mg/Kg " 01116/17 09:16 01117/17 14:21
1,2,4-Trichtorobenzene <0.16 1.6 0.16 mg/Kg ;) 01/16/17 09:16 01/17/17 14:21
2,4,5-Trichlorophenol <0.16 1.6 0.16 mg/Kg f; 01/16/17 09:16 01/17117 14:21
2,4 ,6-Trichlorophenol <0.16 1.6 0.16 mg/Kg " 01/16/17 09:16 01/17117 14:21
Surrogate %Recovery Qualifier Lin1its Prepared Analyzed Di/ Fae
2-Ffuorobiphenyl 52 27 -127 01116117 og:16 0111711714:21 1
2-Fluorophenol 71 25-128 01116117 og:16 01117117 14.·21 1
Nitrobenzene-d5 56 15-136 0111611709:16 01117117 14:21 1
Pheno!-d5 73 29-130 01116117 og:16 01117117 14:21 1
Terphenyl-d14 56 24-146 01116117 og:16 01117117 14:21
2,4, 6· Tribromopflenof 75 10-150 01116117 og:16 01117117 14:21
Method: MAVPH ·Massachusetts -Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
C6HC8 AHphatics <26 26 26 mg/Kg " 01/16/1711:00 01/16/17 22:17 50
C8-C10 Aliphatics <43 43 43 mg/Kg " 0111611711:00 01/16/17 22:17 50
C8·C10 Aromatics <21 21 21 mg/Kg l) 01/1611711:00 01/16/17 22:17 50
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
a,a,a-Trifluorotoluene (fid) 75 70-130 0111611711:00 01116117 22:17 50
a,a,a· Trifluorotoluene (pid) 75 70-130 0111611711:00 01116117 22:17 50
Method: 8081 B - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae
Aldrin <0.014 0.040 0.014 mg/Kg " 01/16117 09:24 01/17117 20:12 5
alpha-BHC <0.0056 0.040 0.0056 mg/Kg n 01/16/17 09:24 01/17117 20:12 5
beta-BHC <0.012 0.040 0.012 mg/Kg ;) 01/16117 09:24 01/17/17 20:12 5
delta-BHC <0.0075 0.040 0.0075 mg/Kg l) 01/16117 09:24 01/17/17 20:12 5
gammaHBHC (Undane} <0.0051 0.040 0.0051 mg/Kg " 01116117 09:24 01/17117 20:12 5
alpha-Chlordane <0.0065 0.040 0.0065 mg/Kg " 01/16/17 09:24 01117117 20:12 5
gamma-Chlordane <0.0063 0.040 0.0063 mg/Kg >:i 01116/17 09:24 01117117 20:12 5
4,4'-DDD <0.0044 0.040 0.0044 mg/Kg l) 01116/17 09:24 01/17117 20:12 5
4,4'-DDE <0.0063 O.D40 0.0063 mg/Kg " 01/16/17 09:24 01/17117 20:12 5 4,4'-DDT <0.018 0.040 0.018 mg/Kg -l) 01/16/17 09:24 01/17/17 20:12 5
Dieldrin <0.0084 0.040 0.0084 mg/Kg l~ 01116/17 09:24 01117/17 20:12 5
Endosulfan t <0.0049 0.040 0.0049 mg/Kg " 01/16117 09:24 01/17/17 20:12 5
Endosulfan H <0.0054 0.040 0.0054 mg/Kg ,, 01/16/17 09:24 01/17117 20:12 5
Endosu!fan sulfate <0.0049 0.040 0.0049 mg/Kg -l'.l 01/16117 09:24 01/17/17 20:12 5
Endrln <0.0044 0.040 0.0044 mg/Kg » 01116117 09:24 01/17117 20:12 5
Endrln aldehyde <0.0068 0.040 0.0068 mg/Kg l) 01116117 09:24 01117117 20:12 5
Endrin ketone <0.0082 0.040 0.0082 mg/Kg ~ 01/16117 09:24 01117117 20'.12 5
Heptachlor <0.0056 0.040 0.0056 mg/Kg 1.'I 01/16/17 09:24 01/17117 20:12 5
Heptachlor epoxide <0.011 0.040 0.011 mg/Kg l) 01116/17 09:24 01/17117 20:12 5
Methoxychlor <0.0077 0.040 0.0077 mg/Kg l) 01116/17 09:24 01117117 20:12 5
Toxaphene <0.68 2.3 0.68 mg/Kg " 01116/17 09:24 01/17/17 20:12 5
TestAmerica Pensacola
Page 30 of 140 21112017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol
Client Sample ID: CK-4 Lab Sample ID: 400-132588-5 Date Collected: 01/11/1712:30 Matrix: Solid Date Received: 01/12/1716:57 Percent Solids: 20.9
Surrogate %Recovery Qualifier Lfrnlts Prepared Analyzed DI/ Fae E DCB Decachlorobipheny/ 41 26- 129 01116117 09:24 01117117 20:12 5 Tetrachforo-m-xylene 41 31-122 01116117 09:24 01117117 20:12 5
Method; MA-EPH • Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MOL Unit 0 Prepared Analyzed Oil Fae c10-c12 Aliphatics <7.5 7.5 7.5 mg/Kg " 01/19/17 07:20 01/24/17 18:59 1
C10-C12 Aromatics <7.5 7.5 7.5 mg/Kg " 01/19/17 07:20 01/24/17 23:11 C12-C16 Aliphatics <7.5 7.5 7.5 mg/Kg " 01/19/17 07:20 01/24/17 18:59
C12-C16 Aromatics <7.5 7.5 7.5 mg/Kg ;;i 01/19/17 07:20 01/24/17 23:11
C16-C35 Aliphatics 34 7.5 7.5 mg/Kg "' 01/19/17 07:20 01/24/17 18:59
C21-C35 Aromatics <7.5 7.5 7.5 mg/Kg ':' 01/19/17 07:20 01/24/17 23:11
C16-C21 Aromatics <7.5 7.5 7.5 mg/Kg " 01/19/17 07:20 01/24/17 23:11
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae 1-Clllorooctadecane 80 40-140 0111g117 07:20 0112411718:59 1
o-Terphenyl 84 40-140 0111g117 07:20 01124117 23:11 1
Method; 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae
Silver <0.93 2.3 0.93 mg/Kg ,, 01/15/1711:30 01/16/1716:08 1
Arsenic 12 4.7 1-9 mg/Kg ,, 01/15/1711:30 01/16/17 16:08 1
Barium 150 4.7 0.93 mg/Kg ,, 01115/1711:30 01/16/17 16:08
Beryllium 0.85 J 1-4 0-47 n1g/Kg l) 01/15/1711:30 01/16/17 16:08
Cobalt 9.9 4.7 1.4 mg/Kg " 01/15/1711:30 01116/17 16:08
Chromium 24 4.7 0.93 mg/Kg " 01/15/1711:30 01/16117 16:08
Copper 98 9.3 0.93 mg/Kg " 01/15/17 11:30 01/16/1716:08
Nickel 28 2.3 1-4 mg/Kg " 01/15/1711:30 01/16/1716:08
Lead 75 4-7 0.93 mg/Kg l) 01/15/1711:30 01/16/17 16:08
Selenium 2-1 J 9.3 1.9 mg/Kg ,, 01115/1711:30 01/16/17 16:08
Thallium <1.9 4.7 1.9 mg/Kg " 01/15/17 11 :30 01/16/17 16:08
Vanadium 29 9.3 1-4 mg/Kg " 01/15/1711:30 01/16/17 16:08
Zinc 250 9.3 3.7 mg/Kg " 0111511711:30 01/16/1716:08
Method: 7471A - Mercury (CVAA) Analyte Result Qualifier RL MOL Unit D Prepared Analyzed Oil Fae
Mercury 0.047 0.013 0.0077 mg/Kg 01/15/17 12:43 01/16/17 09:56 1
General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae Chromium, hexavalent <12 18 12 mg/Kg -r.1 01120/1717:00 01/23/17 12:07 1
Cyanide, Total <D.62 1.2 0.62 mg/Kg " 01/18/1710:53 01/18/17 17:37 1
Percent Moisture 79.1 0.1 0.1 % 01/16/1712:37
General Chemistry. Soluble Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae Nitrate Nitrite as N <1.7 4.8 1.7 n1g/Kg " 01116/17 12:21 1
TestAmerica Pensacola
Page 31 of 140 21112017
Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: CK-5 Date Collected: 0111111713:15 Date Received: 01112/1716:57
Method: 8260C • Volatile Organic Compounds by GC/MS Analyte Result Qualifier 1, 1, 1,2-Tetrachloroethane
1, 1, 1-Trichforoethane
1, 1,2,2-Tetrachloroethane
1, 1.2-Trichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
1,2-Dibromo-3-Chforopropane
1,2-Dich!orobenzene
1,2-Dichloroethane
1.2-Dichloropropane
1,3-Dichlorobenzene 1,4-Dichlorobenzene
Acetone
Benzene Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene Ch!orodibromomethane
Chloroethane
Chloroforn1 Chloromethane
cis-1,2-Dichloroelhene
cis-1,3-Dich!oropropene
Dichlorobromomethane
Ethy!benzene
Methyl tert-buty! ether
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2·pentanone (MIBK)
Styrene
Tetrachloroethene
Toluene trans-1,2-Dichloroethene
trans-1,3-Dlch!oropropene
Trich!oroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes. Total 1,2,4-Trichlorobenzene
tsobutyl alcohol
Surrogate
4-Bromof/uorobenzene Dibromoffuoromet/Jane
Toluene-dB (Surr)
<0.21
<0.093
<0.21
<0.21
<0.070
<0.21 <0.28
<0.060
<0.069
<0.21
<0.080 <0.21
<0.61
<0.056
<0.21
<0.21
<0.21
<0.14
<0.044 <0.21
<0.21
<0.21 <0.084
<0.064
<0.10
<0.21
<0,051
<0.084
<0.84 <0.50
<0.42
<0.084
<0.21
0.62 <0.21
<,0.21
<0.084
<0.21
<0.21
<0.16
<0.17
<0.84
%Recovery Quallfler
98
95
104
RL 0.42 0.42
0.42
0.42
0.42
0.42
0.42
0.42 0.42
0.42
0.42
0.42
2.1
0.42
0.42 0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.42
1.3 2.1
2.1
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.42
0.84
0.42
2.1
Lllnlts
72-122
79-123
80-120
Page 32 of 140
MDL Unit 0.21 mg/Kg
0.093 mg/Kg
0.21 mg/Kg
0.21 mg/Kg
0.070 mg/Kg
0.21 mg/Kg
0.28 mg/Kg
0.060 mg/Kg
0.069 mg/Kg
0.21 mg/Kg
0.080 mg/Kg 0.21 mg/Kg
0.61 mg/Kg
0.056 mg/Kg
0.21 mg/Kg 0.21 mg/Kg
0.21 mg/Kg
0.14 mg/Kg
0.044 mg/Kg
0.21 mg/Kg
0.21 mg/Kg
0.21 mg/Kg
0.084 mg/Kg
0.064 mg/Kg
0.10 mg/Kg
0.21 mg/Kg
0.051 mg/Kg
0.084 mg/Kg
0.84 mg/Kg
0.50 mg/Kg
0.42 mg/Kg
0.084 mg/Kg 0.21 mg/Kg
0.084 mg/Kg
0.21 mg/Kg
0.21 mg/Kg
0.084 mg/Kg
0.21 mg/Kg
0.21 mg/Kg
0.16 mg/Kg 0.17 mg/Kg
0.84 mg/Kg
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132588-6 Matrix: Solid
Percent Solids: 48.8
D Prepared
" 01119117 08:59
" 01119117 08:59
Analyzed 01119/17 12:21
01119117 12:21
" 01119117 08:59 01119117 12:21 0 01119117 08:59 01119/17 12:21
:) 01119/17 08:59 01119117 12:21 <) 01119/1708:59 0111911712:21
,, 01119/17 08:59 01119/1712:21
" 01119/17 08:59 01119/17 12:21 " 01/19/17 08:59 01/19117 12:21
0 01119/17 08:59 01119/17 12:21
" 01119/17 08:59 01119/1712:21 ,,, 01/19/17 08:59 01/19/17 12:21
" 01/19/17 08:59 01/19/1712:21
" 01119/17 08:59 01119/17 12:21
" 01/19/17 08:59 01/19/17 12:21
" 01/19/17 08:59 01/19/17 12:21
" 01/19/17 08:59 01/19/17 12:21
" 01119/17 08:59 01/19/17 12:21
" 01119/17 08:59 01119/17 12:21 " 01119117 08:59 01/1911712:21
" 01/19/17 08:59 01119117 12:21
<) 01/19/17 08:59 01/19/1712:21
" 01119117 08:59 01/19117 12:21
" 01/19/17 08:59 01/19/17 12:21 ,, 01/19/17 08:59 01/19/17 12:21
" 01/19/17 08:59 01/19/17 12:21
:) 01/19/17 08:59 01/19/1712:21
" 01119/17 08:59 01/19/17 12:21 J) 01119/17 08:59 01/1911712:21
" 01/19/17 08:59 01/19/1712:21
" 01119/17 08:59 01119117 12:21
" 01119/17 08:59 0111911712:21
" 01119/17 08:59 01119117 12:21
·O 01/19/17 08:59 01/19117 12:21
" 01/19/17 08:59 01/19/1712:21
" 01/19/17 08:59 01/19117 12:21
Q 01/19/17 08:59 01/19/17 12:21 ,,, 01/19/17 08:59 01/19/17 12:21
{: 01/19/17 08:59 01/19/17 12:21
" 01119117 08:59 01/19117 12:21
" 01/19/17 08:59 01/1911712:21
" 01119117 08:59 01119/17 12:21
Prepared
01119117 08:59
01119117 08:59
Analyzed
01119117 12:21
0111911712:21
01119117 08:59 0111911712:21
DU Fae 50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50 50
50
50
50
50
50
50 50
50
50 50
50
50
50 50
50
50
50
50
50
Dlf Fae
50
50
50
TestAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: CK-5 Date Collected: 01/11/1713:15 Date Received: 01/12/1716:57
Method: 82700 • Semivolatife Organic Compounds (GC/MSJ Analyte Result Qualifier RL
Acenaphthene <0.066 0.66
AcenaphthyJene
Aniline Anthracene
Benzo[a]anthracene
Benzo{a]pyrene
Benzo[b ]fluoranthene Benzo[g,h,iJpery!ene Benzo[k]fluoranthene
1, 1 '-Biphenyl Bis(2-ch!oroethy!)ether bis (2-ch!oroisopropyf) ether Bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
4-Ch!oroaniline 2-Chloronaphlhalene
2-Chlorophenol
Chrysene Dibenz{a,h)anthracene
Dibenzofuran 3,3'-0ich!orobenzidine
2,4-Dichlorophenor Diethyl phthalate 2,4-Dimethylpheno!
Dimethyl phthalate 1,3-Dinitrobenzene 2,4-Dinitropheno!
2,4-Din!trotoluene 2,6-Dinitroto!uene Di-n-octyl phthalate
Fluoranthene
Fluorene Hexach!orobenzene
Hexachlorobutadiene Hexachlorocyclopentadiene Hexach!oroethane lndeno[1,2,3-cdJpyrene
lsophorone
2-Methylnaphlhalene Naphthalene
2-Nitroaniline 3-Nitroanmne 4-Nitroaniline
Nitrobenzene 4-Nitrophenol N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine
Pentachlorophenol Phenanthrene
<0,066
<0.086
<0.066
0.084 J 0.11 J 0.26 J
<0.066 <0.066
<0.066
<0.066
<0.066 <0.066
<0.066 <0.066
<0.066
<0.066
0.13 J <0.066
<0.066
<0.066
<0.066 <0.066 <0.066
<0.066
<0.066
<0.58 F2 F1 <0.066 <0.066
<0.066
0.27 J <0.066 <0.20
<0.066 <0.13 F1
<020 <0.066 <0.066
<0.066 <0.066
<0.066
<0.066
<0.066 <0.066
<0.22
<0.22 <0.066
<0.13
<0.066
0.66
0.66 0.66 0.66 0.66
0.66
0.66 0.66
0.66 0.66 0.66
0.66 0.66 0.66 0.66
0.66
0.66 0.66
0.66 0.66
0.66 0.66
0.66
0.66 0.66
2.0
0.66 0.66 0.66
0.66 0.66 0.66
0.66
0.66 0.66
0.66 0.66
0.66 0.66
0.66 0.66 0.66 0.66
0.66
0.66 0.66
1.3 0.66
Page 33 of 140
MDL Unit 0.066 mg/Kg 0.066 mg/Kg 0.086 mg/Kg
0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg 0.58 mg/Kg
0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg
0.066 mg/Kg 0.20 mg/Kg
0.066 mg/Kg
0.13 mg/Kg 0.20 mg/Kg
0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg
0.066 mg/Kg
0.066 mg/Kg 0.066 mg/Kg 0.066 mg/Kg
0.22 mg/Kg
0.22 mg/Kg 0.066 mg/Kg
0.13 mg/Kg 0.066 mg/Kg
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132588-6 Matrix: Solid
Percent Solids: 48.8
D Prepared Analyzed Oii Fae E c 01/16/17 09:16 01/17/17 14:54
" 01/16/17 09:16 01/17/17 14:54 ,, 01/16/17 09:16 01/17/1714:54
!) 01/16/17 09:16 01/1711714:54 ,, 01/16/1709:16 01/17/1714:54
... 01/16/1709:16 01/17/17 14:54
0 01/16/17 09:16 01/17/17 14:54 ::: 01/16/17 09:16 01/17/1714:54 •:: 01/16/17 09:16 01/17/1714:54 :;; 01/16/17 09:16 01/17/17 14:54
b 01/16/17 09:16 01/1711714:54 ,,, 01/16/1709:16 01/17/1714:54
,, 01/16/17 09:16 01/1711714:54
;) 01/16/17 09:16 01/1711714:54 " 01/16/17 09:16 01/17/17 14:54 0 01/16/17 09:16 01/17/17 14:54
'" 01/16/17 09:16 01/17117 14:54 " 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/17/1714:54 ,, 01/16/17 09:16 01/17/1714:54
,, 01/16/1709:16 01/17/1714:54
" 01/16/17 09:16 01/17/17 14:54 " 01/16/17 09:16 01/17/17 14:54
" 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/1711714:54
" 01/16/17 09:16 01/17/1714:54 :;' 01/16/17 09:16 01/17/1714:54
'" 01/16/17 09:16 01/1711714:54 " 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/17/1714:54
'" 01/16/17 09:16 01/17/1714:54 ,, 01/16/17 09:16 01/1711714:54
" 01/16/17 09:16 01/1711714:54 <) 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/1711714:54
" 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/17/1714:54
" 01/16117 09:16 01/17/1714:54 " 01/16/17 09:16 01117/1714:54 " 01/16/17 09:16 01/1711714:54
" 01116/17 09:16 01/1711714:54 " 01116/17 09:16 01/17/1714:54
'" 01/16/17 09:16 01/1711714:54 " 01/16/17 09:16 01/17/1714:54 " 01/16/17 09:16 01/1711714:54 " 01/16/17 09:16 01/17/1714:54
" 01/16/17 09:16 01/1711714:54 p 01/16/17 09:16 01/17/1714:54
1
1
TestAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1
Project/Site: Moffat & Nichol
Client Sample ID: CK-5 Lab Sample ID: 400-132588-6 Date Collected: 0111111713:15 Matrix: Solid Date Received: 0111211716:57 Percent Solids: 48.8
Method: 8270D - Semivolalile Organic Compounds (GCIMS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Phenol <0.066 0.66 0.066 mg!Kg >,\ 01116117 09:16 01117117 14:54 1
Pyrene 0.23 J 0.66 0.066 mg/Kg "' 01116/17 09:16 01117117 14:54
1,2,4 ,5-T etrachlorobenzene <0.066 0.66 0.066 mg/Kg i) 01116117 09:16 01117117 14:54
2,3 ,4, 6-T etrachlorophenol <0.066 0.66 0.066 mg/Kg " 01116/17 09:16 01117/17 14:54
1,2,4-Trichlorobenzene <0,066 0,66 0.066 mg/Kg (> 01116/17 09:16 01117117 14:54
2,4,5-Trich!orophenol <0.066 0,66 0.066 mg/Kg {l 01116/17 09:16 01117117 14:54 1
2,4,6-Trlchforopheno! <0.066 0.66 0.066 mg/Kg 0 01116/17 09:16 01117117 14:54 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed DiJ Fae 2-Fluorobip/Jenyl 58 27-127 011161170g_16 0111711714:54 1
2-Fluorophenol 72 25-128 01116117 09:16 01117117 14:54 1
Nitrobenzene-d5 57 15-136 01116117 og:16 01117117 14:54 1
Phenol-d5 74 29-130 011161170g:16 0111711714:54
Terpheny/-d14 65 24-146 01116117 og:16 0111711714:54
2,4,6c Tribromopbenol 82 10-150 011161170g:16 01117117 14:54
Method: MAVPH - Massachusetts -Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae C6-C8 Aliphatics <7.3 7.3 7.3 mg/Kg ,, 0111611711:00 01117/1710:52 50
C8-C 10 A!lphatics <12 12 12 mgiKg ,, 0111611711:00 01117117 10:52 50
C8-C10 Aromatics <6.1 6.1 6.1 mg/Kg " 0111611711:00 01117117 10:52 50
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae a,a,a-Trifluorotoluene (fid) 79 70-130 0111611711:00 01117117 10:52 50
a,a,a· Trifluorotoluene (pid) 81 70-130 0111611711:00 0111711710:52 50
Method: 8081 B - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dilfac
Aldrin <0.0024 0.0068 0.0024 mg/Kg " 01116117 09:24 01117117 21:10 2 alpha·BHC <0.00096 0.0068 0.00096 mg/Kg " 01116117 09:24 01117117 21:10 2 bela-BHC <0.0020 0.0068 0.0020 mg/Kg " 01116117 09:24 01117117 21:10 2
della-BHC <0.0013 0.0068 0.0013 mg/Kg '" 01116117 09:24 01117117 21:10 2
gamma-BHC (Undane) <0.00088 0.0068 0.00088 mg/Kg n 01116/17 09:24 01117117 21:10 2
alpha-Chlordane 0.0014 J 0.0068 0.0011 mg/Kg 0 01116117 09:24 01117117 21:10 2
gamma-Chlordane 0.0025 J 0.0068 0.0011 mg/Kg '" 01116/17 09:24 01117117 21:10 2
4,4'-DDD <0.00076 0.0068 0.00076 mg/Kg " 01116117 09:24 01117117 21:10 2 4,4'-DDE <0.0011 0.0068 0.0011 mg/Kg " 01116117 09:24 01117117 21:10 2
4.4'-DDT <0.0031 0.0068 0.0031 mg/Kg ;) 01116117 09:24 01117117 21:10 2
Dieldrin <0.0014 0.0068 0.0014 mg/Kg i:I 01116117 09:24 01117117 21:10 2
Endosulfan I <0.00084 0.0068 0.00084 mg/Kg n 01116/17 09:24 01117117 21:10 2
Endosu!fan II <0.00092 0.0068 0.00092 mg/Kg " 01116/17 09:24 01117117 21:10 2
Endosutfan sulfate <0.00084 0.00!38 0.00084 mg/Kg ;) 01116/17 09:24 01117117 21:10 2
Endrin <0.00076 0.0068 0.00076 mg/Kg ,, 01116/17 09:24 01117117 21:10 2
Endrin aldehyde <0.0012 0.0068 0.0012 mg/Kg ~l 01116117 09:24 01117117 21:10 2
Endrin ketone <0.0014 0.0068 0.0014 mg/Kg 0 01116117 09:24 01117/17 21:10 2
Heptachlor <0.00096 0.0068 0.00096 mg/Kg ,, 01116117 09:24 01117/17 21:10 2
Heplachlor epoxide <0.0018 0.0068 0.0018 mg/Kg " 01116117 09:24 01117117 21:10 2
Methoxychlor <0.0013 0.0068 0.0013 mg/Kg n 01116117 09:24 01117117 21:10 2
Toxaphene <0.12 0.40 0.12 mg/Kg " 01116117 09:24 01117117 21:10 2
TestAmerica Pensacola
Page 34 of 140 2/112017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol
Client Sample ID: CK-5 Lab Sample ID: 400-132588-6 Date Collected: 01111117 13:15 Matrix: Solid Date Received: 0111211716:57 Percent Solids: 48.8
Surrogate %Recovery Quallfler Lltnfts Prepared Analyzed DJ/ Fae El DCB Decachlorobiphenyl 62 26-129 01116117 09:24 01117117 21:10 2
Tetrach/oro-m-xylene 62 31- 122 01116117 09:24 01117117 21:10 2
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
C1O-C12 A!iphatics <3.3 3.3 3.3 mg/Kg ., 01119/17 07:20 01124117 18:02 1
C10-C12 Aromatics <3.3 3.3 3.3 mg/Kg " 01119117 07:20 01124117 22:14
C12-C16 Aliphatics <3.3 3.3 3.3 mg/Kg ::1 01/19117 07:20 01124/1718:02
C12-C16 Aromatics <3.3 3.3 3.3 mg/Kg z:: 01/19/17 07:20 01124117 22:14
C16-C35 Aliphatics 11 3.3 3.3 mg/Kg ::1 01119117 07:20 01/24/17 18:02
C21 ·C35 Arornatics 3.5 3.3 3.3 mg/Kg n 01119117 07:20 01124117 22:14
C16-C21 Aromatics <3.3 3.3 3.3 rng/Kg 0 01119117 07:20 01/24117 22:14
Surrogate %Recovery Qualifier Limits Prepared Analyzed D/I Fae 1-Chlorooctadecane 83 40-140 01119117 07:20 0112411718:02 1
o-Terphenyl 70 40-140 01119117 07:20 01124117 22:14
Method: 6010C - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Silver <0.37 0.93 0.37 mg/Kg D 01/1511711:30 0111611716:11 1
Arsenic 12 1.9 0.74 mg/Kg :) 01/1511711:30 01116117 16:11
Barium 120 1.9 0.37 mg/Kg ,, 0111511711:30 0111611716:11
Beryllium 0.33 J 0.56 0.19 mg/Kg '" 0111511711:30 01116/1716:11
Cobalt 4.8 1.9 0.56 mg/Kg 0 0111511711:30 0111611716:11
Chromium 26 1.9 0.37 mg/Kg (.) 01115/1711:30 01/1611716:11
Copper 44 3.7 0.37 mg/Kg ,,
0111511711:30 0111611716:11
Nickel 12 0.93 0.56 mg/Kg '" 0111511711:30 01116117 16:11
Lead 64 1.9 0.37 mg/Kg 1:i 0111511711:30 01116117 16:11
Selenium 1.3 J 3.7 0.74 mg/Kg "' 01/15/1711:30 01/16117 16:11
Thallium <0.74 1.9 0.74 mg/Kg " 0111511711:30 01/1611716:11 1
Vanadium 14 3.7 0.56 mg/Kg q 01/1511711:30 0111611716:11
Zinc 150 3.7 1.5 mg/Kg " 01/1511711:30 0111611716:11
Method: 7471A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Merc_ury 0.052 0.012 0.0074 mg/Kg 01115117 12:43 01116117 09:57 1
General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed OJI Fae
Chromium, hexavalent <5.8 F1 8.3 5.8 mg/Kg ~\ 01120/1717:00 01123/17 12:03 1
Cyanide, Total <0.27 F1 0.51 0.27 mg/Kg o;:- 01/1811710:53 01/18117 17:30
Percent Moisture 51.2 0.1 0.1 % 0111611712:37
General Chemistry - Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Nitrate Nitrite as N <0.74 F1 F2 2.1 0.74 mg/Kg " 01/1611712:22 1
Tes!America Pensacola
Page 35 of 140 2/112017
Client Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol
Client Sample ID: CK-6 Date Collected: 01/13/17 09:30 Date Received: 01/14/17 08:32
Method: 8260C • Volatile Organic Compounds by GC/MS Analyte Result Qualifier 1, 1, 1,2-Tetrachloroethane <0.0065 1, 1, 1-Trichloroethane <0.0029
1,1,2,2-Tetrach!oroethane
1, 1,2-Trichforoethane
1, 1-Dich!oroethane 1, 1-0ich!oroethene
1,2-Dibromo-3-Ch loropropane
1,2-Dlchlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene 1,4-Dich!orobenzene
Acetone Benzene
Bromofonn Bromomethane
Carbon disulfide Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chforofom1 Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene Dichlorobromomethane
Ethylbenzene
Methyl tert-butyl ether
Methylene Chloride
2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK)
Styrene Tetrach!oroethene
Toluene trans..:1,2-Dich!oroethene
trans· 1,3·Dichloropropene
Trichloroethene
Trichlorofluoron1ethane
Vinyl chloride
Xy!enes, Total 1,2,4-Trichf orobenzene
lsobutyl alcohol
Surrogate
4-Bromonuorobenzene
Dibromoffuoromethane
Toluene-dB (Surr)
<0.0065 <0.0065
<0.0022 <0.0065
<0.0086
<0.0018
<0.0021 <0.0065
<0.0025 <0.0065
0.30 <0.0017
<0.0065
<0.0065
0.023 <0.0044
<0.0014
<0.0065
<0.0065 <0.0065 <0.0026 <0.0020
<0.0031 <0.0065
<0.0016
<0.0026
<0.026
0.022 J <0.013
<0.0026 <0.0065
0.0037 J <0.0065 <0.0065
<0.0026 <0.0065
<0.0065 <0.0049 <0.0052
<0.026
%Recovery Qualifier
104
96
111
RL 0.013 0.013
0.013 0.013
0.013 0.013 0.013
0.013 0.013 0.013
0.013 0.013 0.065 0.013
0.013 0.013
0.013
0.013 0.013 0.013
0.013
0.013 0.013
0.013 0.013 0.013
0.013 0.013
0.039 0.065
0.065
0.013 0.013
0.013 0.013
0.013 0.013 0.013
0.013 0.026 0.013 0.065
Lim/rs
72-122
79-123
80.120
Page 36of140
MOL Unit 0.0065 mg/Kg 0.0029 mg/Kg
0.0065 mg/Kg 0.0065 mg/Kg
0.0022 mg/Kg 0.0065 mg/Kg
0.0066 mg/Kg 0.0016 mg/Kg 0.0021 mg/Kg
0.0065 mg/Kg 0.0025 mg/Kg 0.0065 mg/Kg 0.019 mg/Kg
0.0017 mg/Kg 0.0065 mg/Kg 0.0065 mg/Kg 0.0065 mg/Kg
0.0044 mg/Kg 0.0014 mg/Kg 0.0065 mg/Kg
0.0065 mg/Kg
0.0065 mg/Kg 0.0026 mg/Kg
0.0020 mg/Kg
0.0031 mg/Kg 0.0065 mg/Kg
0.0016 mg/Kg
0.0026 mg/Kg 0.026 mg/Kg 0.016 mg/Kg 0.013 mg/Kg
0.0026 mg/Kg 0.0065 mg/Kg
0.0026 mg/Kg
0.0065 mg/Kg 0.0065 mg/Kg 0.0026 mg/Kg 0.0065 mg/Kg
0.0065 mg/Kg
0.0049 mg/Kg 0.0052 mg/Kg
0.026 mg/Kg
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-i Matrix: Solid
Percent Solids: 51.9
O Prepared
" 01119/17 06:59 Q 01/19/17 06:59
Analyzed 01/19/17 15:35 01/19/1715:35
" 01119111 o8·.59 0111911115:35 " 01/19/17 08:59 01/19/17 15:35 ;) 01/19/1708:59 01/1911715:35 ;) 01/19/17 08:59 01119117 15:35
" 01/19/1708:59 01/19/1715:35
" 01/19/17 08:59 01/19/17 15:35 {l 01/19117 08:59 01/19/1715:35
;) 01/19/17 08:59 01/19/1715:35 l) 01/19/17 08:59 0111911715:35 ;;, 01119/17 08:59 01/19/17 15:35
" 01119/17 06:59 01/19117 15:35 " 01/19/17 08:59 01/19/17 15:35
" 01119117 08:59 01/19/17 15:35 " 01/19/17 08:59 01/19/17 15:35
" 01119117 08:59 01/19/17 15:35
" 01/19/17 08:59 01/19/1715:35 " 01119/1708:59 01/19/1715:35 ;) 01119/1706:59 01/1911715:35
0 01/19/17 06:59 01/19/17 15:35
I) 01119117 08:59 01/1911715:35 ·(.\ 01/19/17 08:59 01/19/1715:35
;) 01/19117 08:59 01/19/1715:35
" 01/19117 08:59 01/19/1715:35 ,, 01/19/17 08:59 01/19117 15:35
" 01119/17 08:59 01/19/17 15:35 ,, 01119/1708:59 0111911715:35
Q 01119/1706:59 01/1911715:35 " 01119/17 08:59 01119/17 15:35 ,,, 01119/17 08:59 01/19117 15:35
,,, 01/19/17 06:59 01/19117 15:35 " 01/19117 08:59 01/19/17 15:35
i) 01/19117 08:59 01119117 15:35 ,, 01119/17 08:59 01/19/1715:35
" 01119/17 08:59 01/19/17 15:35 " 01/19/17 08:59 01/19117 15:35 1) 01/19/1708:59 01/19/1715:35 ;) 01/19/1706:59 01/1911715:35
" 01/19117 08:59 01/19/17 15:35 ,, 01/19117 06:59 01/19/1715:35
" 01/19117 08:59 01/19/1715:35
Prepared Analyzed
0111911708:59 0111911715:35
01119117 08:59 0111911715:35
01119117 08:59 0111911715:35
Oil Fae 1
1
1
DI/ Fae
1
T estAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates Projecl/Site: Moffat & Nichol
Client Sample ID: CK-6 Date Collected: 01113/17 09:30 Date Received: 01114/17 08:32
Method: 82700 - Semivotatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene Acenaphthylene
Aniline Anthracene
Benzo[a]anthracene
Benzofa]pyrene Be nzo{b ]flu o ra nthe ne Be nzo[g ,h, i] pery le ne Benzo[k]fluoranthe_ne 1, 1'-Biphenyl
Bis(2-ch!oroethyl)ether bis (2-ch!oroisopropyl) ether
Bis(2-<1thylhexyl) phthalate Butyl benzyl phthalate 4-Chloroanmne 2-Chloronaphlhalene
2-Chlorophenol
Chrysene Dibenz(a,h)anthracene
Oibenzofuran 3,3'-Dichlorobenzidine
2,4-Dich!orophenol Diethyl phthalate
2,4-Dimethylpheno!
Dimethyl phtha!ate 1,3-Dinitrobenzene
2,4-Dinitrophenol 2,4-Dinitrototuene 2,6-Dinitrotoluene
Oi-n-octyl phthalate
Fluoranthene Fluorene
Hexachforobenzene
Hexachlorobuladiene
Hexach!orocycJopeotadiene Hexachforoethane
lndeno[1,2,3-cd]pyrene lsophorone 2-Methylnaphlha!ene Naphthalene 2-Nitroaniline
3-NitroanU!ne 4-Nitroanillne
Nitrobenzene
4-Nitrophenol N-Nitrosodi-n-pfqpylamine N-Nitrosodiphenylamine
Pentachforophenol
Phenanthrene
<0.063
<0.063
<0.082
<0.063 <0.063
0.28 J 0.38 J 0.16 J 0.15 J
<0.063
<0.063
<0.063
0.15 J 0.071 J
<0.063
<0.063
<0.063
0.25 J <0.063
<0.063
<0.063
<0.063 <0.063
<0.063
<0.063
<0.063 <0.55
<0.063
<0.063
<0.063
0.44 J <0.063
<0.19
<0.063
<0.13
<0.19
0.15 J <0.063
<0,063
<0.063
<0.063
<0.063
<0.063 <0.063
<0.21
<0.21
<0.063
<0.13
0.18 J
0.63
0.63
0.63
0.63 0.63
0.63 0.63
0.63 0.63
0.63 0.63
0.63
0.63
0.63 0.63
0.63
0.63
0.63 0.63
0.63
0.63
0.63 0.63
0.63
0.63
0.63
1.9
0.63
0.63
0.63
0.63
0.63 0.63
0.63
0.63 0.63
0.63
0.63 0.63
0.63 0.63
0.63 0.63
0.63 0.63
0.63 0.63
1.3 0.63
Page 37 of 140
MDL Unit 0.063 mg/Kg
0.063 mg/Kg
0.082 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.55 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.19 mg/Kg
0.063 mg/Kg
0.13 mg/Kg
0.19 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.21 mg/Kg
0.21 mg/Kg
0.063 mg/Kg
0.13 mg/Kg
0.063 mg/Kg
T estAmerica Job ID 400-132540-1
Lab Sample ID: 400-132650-1 Matrix: Solid
Percent Solids: 51.9
D Prepared
" 01/18/17 09:33 " 01/18117 09:33
Analyzed
01119117 00:09
01119117 00:09
" 01/16/17 09:33 01119117 00:09
" 01/18/17 09:33 01119117 00:09 " 0111811709:33 01119117 00:09 ,, 01118/1709:33 01/19117 22:14
"' 01118/17 09:33 01119117 22:14
:) 01/18/17 09:33 01119/17 22:14 n 01118117 09:33 01/19/17 22:14
l) 01/16117 09:33 01119/17 00:09
" 01/18/17 09:33 01119117 00:09 :) 01/18117 09:33 01119117 00:09 {> 01/18117 09:33 01119117 00:09
,, 0111811709:33 01119117 00:09
" 01118/1709:33 01119117 00:09
" 01118117 09:33 01119117 00:09 ,, 01/18/17 09:33 01/19/17 00:09
,, 01/18117 09:33 01/19/17 00:09
" 01118/17 09:33 01/19117 22:14 :) 01/18117 09:33 01/19/17 00:09 ,, 01118117 09:33 01119117 00:09
" 01118/17 09:33 01119117 00:09 D 01118/17 09:33 01119117 00:09
" 01/18117 09:33 01/19117 00:09
"' 01/18/17 09:33 01/19117 00:09
" 01/18117 09:33 01119117 00:09 " 01118117 09:33 01/19117 00:09
" 01/18117 09:33 01119/17 00:09
" 01/18117 09:33 01119117 00:09
" 01/18/17 09:33 01119117 00:09
" 01118117 09:33 01119117 00:09
"' 01118117 09:33 01/19117 00:09 p 01118/17 09:33 01/19117 00:09
" 01118/1709:33 01/19117 00:09 i) 01/18117 09:33 01/19/17 00:09 " 01/18/17 09:33 01119117 00:09 p 01/18/17 09:33 01119117 22:14
0 01118/17 09:33 01119/17 00:09
'" 01/18117 09:33 01119117 00:09 0 01118/17 09:33 01119117 00:09
" 01118/17 09:33 01119117 00:09 " 01118/17 09:33 01/19117 00:09
" 01118/17 09:33 01/19/17 00:09 "' 01/18/17 09:33 01119/17 00:09 ,, 01/18/17 09:33 01119/17 00:09
" 01118117 09:33 01/19/17 00:09 " 01118/17 09:33 01119117 00:09
" 01118/17 09:33 01119117 00:09 n 01118/17 09:33 01119117 00:09
Dilfac E 1
1
1
TestAmerica Pensacola
211/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Client Sample ID: CK-6 Lab Sample ID: 400·-132650-1 Date Collected: 01113117 09:30 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 51.9
Method: 82700 • Semivolatile Organic Compounds (GC/MS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Di! Fae
Phenol <0.063 0.63 0.063 mg/Kg " 01 /18/17 09:33 01/19/17 00:09 1
Pyrene 0,58 J 0.63 0.063 mg/Kg "' 01/18/17 09:33 01/19/17 00:09
1,2,4,5-T etrach!orobenzene <0.063 0.63 0.063 mg/Kg "' 01/18/17 09:33 01/19/17 00:09
_2,3, 4, 6-T etrachf orophenol <0.063 0.63 0.063 mg/Kg " 01/18/17 09:33 01/19/17 00:09
1,2,4-Trichlorobenz:ene <0.063 0.63 0.063 mg/Kg r; 01/18/1709:33 01/19/17 00:09
2,4 ,5· Trichlorophenot <0.063 0.63 0.063 mg/Kg ,, 01/18/17 09:33 01/19/17 00:09
2,4 ,6-Trichlorophenol <0.063 0.63 0.063 mg/Kg '" 01/18/17 09:33 01/19/17 00:09
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
2-Fluorobiphenyl 51 27. 127 01118117 09:33 01119117 00:09 1
2-Fluorophenol 57 25.128 01118117 09:33 01119117 00:09 1
Nitrobenzene-d5 45 15.136 01118117 09:33 01119117 00:09
P/1enof-d5 57 29-130 01118117 09:33 01119117 00:09 1
Terpheny!-<114 75 24-146 01118117 09:33 01119117 00:09
2,4,6-Tribromophenof 61 10-150 01118117 09:33 01119117 00:09
Method: MAVPH • Mas.sachusetts ·Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Di! Fae C6-C8 A!iphatics <12 12 12 mg/Kg " 01/16/17 11:30 01/17/17 00:17 50
C8-C10 Aliphatics <20 20 20 mg/Kg -t,; 01/16/1711:30 01117117 00:17 50
C8-C10 Aromatics <10 10 10 mg/Kg " 01/16/1711:30 01/17117 00:17 50
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI! Fae
a,a,a-Trifluorotoluene (fid) 79 70.130 0111611711:30 01117117 00:17 50
a,s,a-Trif/uorotoluene (pid) 78 70-130 01116117 11:30 01117117 00:17 50
Method: 80816 • Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Aldrin <0.0023 0.0064 0.0023 mg/Kg " 01/18/1712:42 01/19/17 21:49 2
alpha-BHC <0.00090 0.0064 0.00090 mg/Kg " 01/18/1712:42 01/19/17 21:49 2
beta-BHC <0.0019 0.0064 0.0019 mg/Kg ') 01/18/1712:42 01/19/17 21:49 2
delta-BHC <0.0012 0.0064 0.0012 mg/Kg " 01/18/1712:42 01/19/17 21:49 2
gamma-BHC {Lindane) <0.00083 0.0064 0.00083 mg/Kg !) 01/18/1712:42 01/19/17 21:49 2
alpha-Chlordane 0.0028 J 0.0064 0.0011 mg/Kg " 01/18/1712:42 01/19/17 21:49 2
gamma-Chlordane 0.0080 0.0064 0.0010 mg/Kg J::I 01/18/1712:42 01/19/17 21:49 2
4,4'-DDD 0.0020 J 0.0064 0.00071 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2
4,4'-DDE 0.0019 J 0.0064 0.0010 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2
4.4'-DDT <0.0029 0.0064 0.0029 mg/Kg ,, 01/18/1712:42 01/19/17 21:49 2
Dieldrin 0.0038 J 0.0064 0.0014 mg/Kg i) 01/18/1712:42 01/19/17 21:49 2
Endosulfan I <0.00079 0.0064 0.00079 mg/Kg " 01/18/1712:42 01/19/1721:49 2
Endosulfan II <0.00086 0.0064 0.00086 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2
Endosulfan sulfate <0.00079 0.0064 0.00079 mg/Kg ,, 01/18/1712:42 01/19/17 21:49 2
Endrin <0.00071 0.0064 0.00071 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2
Endrin aldehyde <0.0011 0.0064 0.0011 mg/Kg " 01/18/1712:42 01/19/17 21:49 2
Endrin ketone <0.0013 0.0064 0.0013 mg/Kg " 01/18/1712:42 01/19/17 21:49 2
Heptachlor <0.00090 0.0064 0.00090 mg/Kg ,, 01/18/17 12:42 01/19/17 21:49 2
Heptachlor epoxide <0.0017 0.0064 0.0017 mg/Kg " 01/18/17 12:42 01/19/17 21:49 2
Methoxychlor <0.0012 0.0064 0.0012 mg/Kg " 01/18/1712:42 01/19/17 21:49 2
Toxaphene <0.11 0.38 0.11 mg/Kg ,, 01/18/17 12:42 01/19/17 21:49 2
TestAmerica Pensacola
Page 38 of 140 2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol
Client Sample ID: CK-6 Lab Sample ID: 400-132650-1 Date Collected: 01113117 09:30 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 51.9
Surrogate %Recovery Qua/If/er Limits Prepared Analyzed DJ/ Fae E DCB Decachlorobiphenyl 45 26- 129 01118117 12:42 01119117 21:49 2
Tetrachloro-m-xylene 41 31-122 0111811712:42 01119117 21:49 2
Method: MA·EPH ·Massachusetts. Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DH Fae C10-C12 A!iphatics <3.0 3.0 3.0 mg/Kg '" 01/19/17 07:20 01/24/17 19:57 1
C10-C12 Aromatics <3.0 3.0 3.0 mg/Kg '" 01/19/17 07:20 01/25/17 00:08
C12-C16 A!iphatics <3.0 3.0 3.0 mg/Kg ,, 01/19/17 07:20 01/24117 19:57
C12-C16 Aromatics <3.0 3.0 3.0 mg/Kg Q 01/19/17 07:20 01/25/17 00:08
C16-C35 Aliphatics 45 3.0 3.0 mg/Kg " 01/19/17 07:20 01/24/17 19:57
C21~C35_Aromatics 21 3.0 3.0 mg/Kg '" 01/19/17 07:20 01125/17 00:08
C16~C21 Aromatics 5.2 3.0 3.0 n1g/Kg 1:1 01/19/17 07:20 01/25/17 00:08
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
1-Chlorooctadecane 98 40-140 01119117 07:20 0112411719:57 1
o-Terphenyl 98 40-140 01119117 07:20 01125117 00:08
Method: 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae
Silver <0.35 0.88 0.35 mg/Kg l) 01116/17 08:55 01/17/1713:01 1
Arsenic 7.1 1.8 0.71 mg/Kg " 01/16/17 08:55 01/17/17 13:01
Barium 87 F1 1.8 0.35 mg/Kg l) 01/16/17 08:55 01/17/1713:01
Beryllium 0.37 J 0.53 0.18 mg/Kg l) 01/16/17 08:55 01/17/17 13:01
Cobalt 4.1 1.8 0.53 mg/Kg l) 01/16/17 08:55 01/17/17 13:01
Chromium 11 1.8 0.35 mg/Kg " 01/16/17 08:55 01/17/17 13:01
Copper 37 3.5 0.35 mg/Kg " 01/16117 08:55 01/17/17 13:01
Nickel 12 0.88 0.53 mg/Kg " 01/16/17 08:55 01/17/1713:01
Lead 42 1.8 0.35 mg/Kg ,, 01/16/17 08:55 01/17/17 13:01
Seleniun1 0.87 J 3.5 0.71 mg/Kg " 01/16/17 08:55 01117/17 13:01
Thallium <0.71 1.8 0.71 mg/Kg " 01/16/17 08:55 01/17/17 13:01
Vanadium 11 3.5 0.53 m9IK9 " 01/16/17 08:55 01/17/1713:01
Zinc 130 3.5 1.4 mg/Kg " 01/16/17 08:55 01/17/17 13:01
Method: 7471A. Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae
Mercury 0.066 0.013 0.0078 mg/Kg 01/15/17 12:43 01/16/17 12:14
General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae
Chro1nlun1, hexavalent <4.4 6.3 4.4 n1g/Kg " 01/20/17 17:00 01/23/17 12:07 1
Cyanide, Total <0.24 0.46 0.24 mg/Kg ;" 01/1811710:53 01/18/17 17:37
Percent Moisture 48.1 0.1 0.1 % 01/17/17 14:08
General Chemistry ·Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae
Nitrate Nitrite as N <0.69 1.9 0.69 mg/Kg ,, 01/16/17 12:26 1
TestAmerica Pensacola
Page 39 of 140 2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Client Sample ID: CK-7 Lab Sample ID: 400-132650-2 Date Collected: 01/13/17 09:45 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 23.3
Method: 8260C. Volatile Organic Compounds by GCIMS E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae 1, 1, 1,2-Tetrach!oroethane <0.010 0.021 0.010 mg/Kg " 01/19/17 08:59 01/19/1715:58 1 1. 1, 1-Trichloroethane <0.0046 0.021 0.0046 mg/Kg 0 01/19/17 08:59 01/19/1715:58
1, 1 ,2 ,2-Tetrachloroethane <0.010 0.021 0.010 mg/Kg 0 01/19/17 08:59 01/19/17 15:58
1, 1,2-Trichforoethane <0.010 0.021 0.010 mg/Kg 0 01/19/17 08:59 01/19/17 15:58
1, 1-Dich!oroethane <0.0035 0.021 0.0035 mg/Kg 0 01/19/17 08:59 01/19/17 15:58
1, 1-Dich!oroethene <0.010 0.021 0.010 mg/Kg 0 01/19/17 08:59 01/19/17 15:58
1,2-Dibromo-3-Chloropropane <0.014 0.021 0.014 mg/Kg ,, 01/19/17 08:59 01/19/17 15:58
1.2-Dichlorobenzene <0.0030 0.021 0.0030 mg/Kg (.J: 01/19/17 08:59 01/19/17 15:58
1,2-Dich!oroethane <0.0034 0.021 0.0034 mg/Kg o:i 01/19/17 08:59 01/19/17 15:58
1,2-Dichloropropane <0.010 0.021 0.010 mg/Kg ;:; 01/19/17 08:59 01/19/1715:58
1,3-Dichlorobenzene <0.0040 0.021 0.0040 mg/Kg " 01119/17 08:59 01/19/1715:58
1,4-Dich!orobenzene <0.010 0.021 O.D10 mg/Kg 1;1 01/19/17 08:59 01/19/17 15:58
Acetone 0.16 0.10 0,031 mg/Kg 0 01/19/17 08:59 01/19/1715:58
Benzene 0.0031 J 0.021 0.0028 mg/Kg " 01 /19/17 08:59 01/19/1715:58
Bromoform <0.010 0.021 0.010 mg/Kg n 01/19/17 08:59 01/19/17 15:58
Bromomethane <0.010 0.021 0.010 mg/Kg -[,< 01 /19117 08:59 01/19/17 15:58
Carbon disulfide 0.011 J 0.021 0.010 mg/Kg p 01/19/17 08:59 01/19/17 15:58
Carbon tetrachloride <0.0071 0.021 0.0071 mg/Kg l:i' 01/19/17 08:59 01/19/1715:58
Chlorobenzene <0.0022 0.021 0.0022 mg/Kg " 01119/17 08:59 01/19/1715:58
Ch!orodibromomethane <0.010 0.021 0.010 mg/Kg 0. 01/19/17 08:59 01/19/17 15:58
Chloroethane <0.010 0.021 0.010 mg/Kg p 01119/17 08:59 01/19/17 15:58
Chloroform <0.010 0.021 omo mg/Kg l'.\ 01/19/17 08:59 01/19/1715:58
Ch!oromethane <0.0042 0.021 0.0042 mg/Kg ·r,! 01/19/17 08:59 01/19/17 15:58
cis-1,2-Dichloroethene <0.0032 0.021 0.0032 mg/Kg '" 01/19117 08:59 01/19/17 15:58
cis-1,3-Dichloropropene <0,0050 0.021 0.0050 mg/Kg " 01 /19/17 08:59 01/19/17 15:58
Dichlorobromomethane <0.010 0.021 0.010 mg/Kg ,,, 01 /19117 08:59 01/19/17 15:58
Ethylbenzene <0.0026 0.021 0.0026 mg/Kg ~ 01119/17 08:59 01/19/17 15:58
Methyl tert-butyl ether <0.0042 0.021 0.0042 mg/Kg -i:i 01119117 08:59 01/19/17 15:58
Methylene Chloride <0,042 0.063 0.042 mg/Kg ,, 01/19/17 08:59 01/19/1715:58
2-Butanone (MEK) <0.025 0.10 0.025 mg/Kg 1.1 01/19/17 08:59 01/19/1715:58
4-Methyl-2-pentanone (MIBK} <0.021 0.10 0.021 mg/Kg ·J:i 01/19/17 08:59 01/19/1715:58
Styrene <0.0042 0.021 0.0042 mg/Kg {l; 01/19/17 08:59 01/19/17 15:58 T etrachloroethene <0.010 0.021 0.010 mg/Kg p 01/19/17 08:59 01/19117 15:58
Toluene 0,0050 J 0.021 0.0042 mg/Kg ·f.< 01/19/17 08:59 01119/1715:58
trans-1,2-Dichloroethene <0.010 0.021 0.010 mg/Kg i,! 01/19117 08:59 01/19/17 15:58
trans-1,3-Dlch!oropropene <0.010 0.021 omo mg/Kg " 01/19/17 08:59 01/19/17 15:58
Trichloroethene <0.0042 0.021 0.0042 mg/Kg " 01/19/17 08:59 01/19/17 15:58
Trich!orofluoromethane <0,010 0.021 0.010 mg/Kg l) 01/19117 08:59 01/19/17 15:58
Vinyl chloride <0.010 0.021 0.010 mg/Kg '" 01/19/17 08:59 01/19/17 15:58
Xylenes, Total <0,0080 0.042 0.0080 mg/Kg " 01119117 08:59 01/19/1715:58
1,2,4-Trichlorobenzene <0.0084 0.021 0.0084 mg/Kg .;;i: 01/19/17 08:59 01/19/1715:58
lsobuty1 alcohol <0.042 0.10 0.042 mg/Kg ·l;! 01/19/17 08:59 01/19/1715:58
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae
4-Bromof/uorobenzene 112 72-122 01119117 08:59 0111911715:58 1
Dibromofluorometl1ane 97 7g_123 01119117 08:59 01119117 15:58 1
Toluene-dB (Surr) 108 BO- 120 01119117 08:59 0111911715:58
TestAmerica Pensacola
Page 40 of 140 2/1/2017
Client Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol
Client Sample ID: CK-7 Date Collected: 01/13/17 09:45 Date Received: 01/14/17 08:32
Method: 82700 • Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene Acenaphthylene
Aniline Anthracene Benzo[a]anthracene
Benzo[a]pyrene Benzo[b }flu o ra nthene Benzo[g,h,i]perylene Benzo[k]fluoranthene
1, 1 '-Biphenyl 81s(2-chloroethyl}ether
bis (2-chloroisopropyl) ether
Bis(2-ethylhexyl) phthalate Butyl benzyl phtha!ate
4-Chloroaniline
2-Ch!oronaphthalene
2-Chloropheno!
Chrysene Oibenz{a,h)anthracene
Oibenzofuran
3,3'-Dichlorobenzidine
2,4-Dlchlorophenol
Diethyl phthalate
2,4-Dimethylpheno!
Dimethyl phthalate 1,3-Dinitrobenzene 2,4-Dfnitropheno! 2,4-Dlnitroto!uene
2,6-0inltrotoluene Di·n-octyl phthalate
Fluoranthene Fluorene Hexachlorobenzene
Hexach!orobutadiene
HexachJorocyclopentadiene Hexachloroethane
Jndeno[1,2,3-cdJpyrene
lsophorone 2-Methylnaphthalene Naphthalene
2-Nitroaniline
3-Nitroanifine 4-Nltroaniline Nitrobenzene
4-Nitrophenol N-Nitrosodi-n-propy!amine N-Nitrosodiphenylamine
Pentach1orophenol
Phenanthrene
<0.14
<0.14
<0.18
<0.14
<0.14
0.21 J 0.27 J
<0.14
<0.14
<0.14
<0.14
<0.14
0.53 J <0.14 <0.14
<0.14
<0.14
<0.14
<D.14
<0.14
<0.14
<0.14
<0.14
<0.14
<0.14
<0.14
<1.2
<D.14
<0.14
<0.14
0.34 J <0.14 <D.42
<0.14
<0.28
<0.42
<0.14
<0.14
<0.14
<0.14
<0.14
<0.14 <0.14
<0.14
<D.46
<0.46
<0.14
<0.28
0.23 J
1.4
1.4
1.4
1.4
1.4
1.4
1.4
1.4 1.4
1.4
1.4 1.4
1.4
1.4 1.4
1.4
1.4
1.4
1.4
1.4
1.4
1.4 1.4
1.4
1.4
1.4
4.1
1.4
1.4
1.4
1.4
1.4 1.4
1.4
1.4
1.4 1.4
1.4
1.4
1.4
1.4
1.4
1.4
1.4
1.4
1.4
1.4
2.8
1.4
Page 41of140
MDL Unit 0.14 mg/Kg
0.14 mg/Kg
0.18 mg/Kg
0.14 mg/Kg 0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg 0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg 0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
1.2 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg 0.42 mg/Kg
0.14 mg/Kg
0.28 mg/Kg 0.42 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.14 mg/Kg
0.46 mg/Kg
0.46 mg/Kg 0.14 mg/Kg
0.28 mg/Kg
0.14 mg/Kg
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-2 Matrix: Solid
Percent Solids: 23.3
D Prepared Analyzed " 01/18/17 09:33 01/19/17 00:41 ,, 01/18/17 09:33 01/19/17 00:41
0 01/18/17 09:33 01/19/17 00:41
n 01/18/17 09:33 01/19/17 00:41
"' 01/18/17 09:33 01/19/17 00:41 ,, 01/18/17 09:33 01/19/17 22:44
l) 01/18/17 09:33 01/19/17 22:44
" 01/18/17 09:33 01/19/17 22:44 r:r 01/18/17 09:33 01/19/17 22:44
"' 01/18/17 09:33 01/19/17 00:41 n 01/18/1709:33 01/19/1700:41
.o 01/18/17 09:33 01/19/17 00:41
,, 01/18/17 09:33 01/19/17 00:41
:.\ 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
"' 01/18/17 09:33 01/19/17 00:41
,, 01/18/17 09:33 01/19/17 00:41
l) 01/18/17 09:33 01/19/17 00:41 01/18/17 09:33 01/19/17 22:44
,, 01/18/17 09:33 01/19/17 00:41
... 01/18/17 09:33 01/19/17 00:41
p 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
() 01/18/17 09:33 01/19/17 00:41 ,, 01/18/17 09:33 01119/1700:41
" 01/18/17 09:33 01/19/17 00:41 ,, 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
,, 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
1:, 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 22:44
"' 01/18/17 09:33 01/19/17 00:41 " 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
"' 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/1700:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
" 01/18/17 09:33 01/19/17 00:41
p 01/18/17 09:33 01/19/17 00:41
DllFac E 1
TestAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates Tes!America Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Client Sample ID: Cl<-7 Lab Sample ID: 400-132650-2 Date Collected: 01113/17 09:45 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 23.3
Method: 8270D • Semivolatile Organic Compounds (GC/MS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Phenol <0.14 1.4 0.14 mg/Kg r:i 01/18/17 09:33 01/19/17 00:41 1
Pyrene 0.39 J 1.4 0.14 mg/Kg 0::< 01/18/17 09:33 01/19/17 00:41
1,2, 4, 5-T etrachlorobenzene <0.14 1.4 0.14 mg/Kg " 01/18/17 09:33 01/19/17 00:41
2,3,4,6-T etrachlorophenol <0.14 1.4 0.14 mg/Kg t; 01/18/17 09:33 01/19/17 00:41
1,2,4-Trichlorobenzene <0.14 1.4 0.14 mg/Kg {! 01/18/17 09:33 01/19/17 00:41 1
2,4 ,5· Trichlorophenol <D.14 1.4 0.14 mg/Kg " 01/18/17 09:33 01/19/17 00:41
2,4,6-Trichloropheno! <0.14 1.4 0.14 mg/Kg 0 01/18/17 09:33 01/19/17 00:41
Surrogate %Recovery Qualifier Limits Prepared Analyzed DH Fae
2-Fluorobiphenyl 56 27 -127 01118117 09:33 01119117 00:41 1
2-F/uorophenof 64 25-128 0111811709:33 01119117 00:41 1
Nitrobenzene-d5 54 15-136 01118117 09:33 01119117 00:41 1
Phenol-d5 67 29-130 01118117 09:33 01119117 00:41 1
Terphenyl·d14 82 24-146 01118117 09:33 01119117 00:41
2,4,6-Tribromophenol 76 10-150 01118117 09:33 01119117 00:41
Method: MAVPH ·Massachusetts· Vol_atile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DU Fae
C6-C8 Aliphatics <25 25 25 mg/Kg '" 01/16/1711:30 01/17/17 01:16 50
C8-C10 Afiphatics <42 42 42 mg/Kg -):! 0111611711:30 01/17/17 01:16 50
C8-C10 Aromatics <21 21 21 mg/Kg " 01116/1711:30 01/17117 01:16 50
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae
a,a,a-Trifluorotoluene (fid) 72 70-130 0111611711:30 01117117 01:16 50
a,e,a-Trifluorotoluene (pid) 74 70-130 0111611711:30 01117117 01:16 50
Method: 8081 B • Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DU Fae
Aldrtn <0.0026 0.0072 0.0026 mg/Kg " 01/23117 08:05 01/2611715:18 1
alpha-BHC <0.0010 0.0072 0.0010 mg/Kg n 01123117 08:05 01/26117 15:18
beta-BHC <0.0021 0.0072 0.0021 mg/Kg -;) 01 /23/17 08:05 01/26/17 15:18
della-BHC <0.0014 0.0072 0.0014 mg/Kg " 01/23/17 08:05 01/26/1715:18
gamma-BHC (Lindane) <0.00094 0.0072 0.00094 mg/Kg " 01/23/17 08:05 01/26/1715:18
alpha-Chlordane 0.0062 J 0.0072 0.0012 mg/Kg " 01/23/17 08:05 01126117 15:18
gamma-Chlordane 0.010 0.0072 0.0011 mg/Kg :::i 01/23/17 08:05 01/26/17 15:18
4,4'-000 0.0045 J 0.0072 0.00081 mg/Kg " 01/23/17 08:05 01/26/1715:18
4,4'-DDE 0.0060 J 0.0072 0.0011 mg/Kg " 01/23/17 08:05 01/26/17 15:18
4.4'-DDT <0.0033 0.0072 0.0033 mg/Kg .r,1 01/23117 08:05 01/26/1715:18
Dieldrin 0.011 0.0072 0.0015 mg/Kg '·~ 01 /23/17 08:05 01/26/17 15:18
Endosulfan l <0.00089 0.0072 0.00089 mg/Kg " 01/23/17 08:05 01/26/1715:18
Endosu!fan II <0.00098 0.0072 0.00098 mg/Kg " 01/23/17 08:05 01/26/1715:18 1
Endosulfan sulfate <0.00089 0.0072 0.00089 mg/Kg r,, 01 /23117 08:05 01/26/17 15:18 1
Endrin <0.00081 0.0072 0.00081 mg/Kg " 01/23/17 08:05 01/26/1715:18
Endrln aldehyde <0.0012 0.0072 0.0012 mg/Kg " 01/23/17 08:05 01/26/17 15:18
Endrin ketone <0.0015 0.0072 0.0015 mg/Kg " 01/23/17 08:05 01/26/1715:18
Heptachlor <0.0010 0.0072 0.0010 mg/Kg ;;1 01/23/17 08:05 01/26/17 15:18
~eplachlor epoxide <0.0019 0.0072 0.0019 mg/Kg " 01/23/17 08:05 01126117 15:18
MethoxYchlor <0.0014 0.0072 0.0014 mg/Kg p 01/23/17 08:05 01/26/17 15:18
Toxaphene <0.12 0.43 0.12 mg/Kg " 01/23/17 08:05 01/26/17 15:18
T estAmerica Pensacola
Page 42 of 140 2/1/2017
Client Sample Results Client C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: CK-7 Lab Sample ID: 400-132650-2 Date Collected: 01/13/17 09:45 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 23.3
Surrogate %Recovery Qualifier Limits Prepared Analyzed DJ/ Fae E DCB Decachlorobipf)enyl 44 26-129 01123117 08:05 01/26117 15:18 1
Tetrachloro-m-xylene 49 31-122 01123117 08:05 01126117 15:18
Method: MA-EPH -Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL .Unit D Prepared Analyzed Oil Fae
C10-C12 Aliphatics <6.9 6.9 6.9 mg/Kg f) 01/19/17 07:20 01/24/17 20:07 1
C10-C12 Aromatics <6.9 6.9 6.9 mg/Kg {) 01/19/17 07:20 01/25/17 00:18 1
C12-C16 Aliphatics <6.9 6.9 6.9 mg/Kg t:l 01/19/17 07:20 01/24/17 20:07
C12-C16 Aromatics <6.9 6.9 6.9 mg/Kg {.l 01/19/17 07:20 01/25/17 00:18
C16-C35 Aliphatics 75 6.9 6.9 mg/Kg n 01/19/17 07:20 01/24/17 20:07
C21.C35 Aro1natics 12 6.9 6.9 mg/Kg {l 01/19/17 07:20 01/25/17 00:18
C16-C21 Aromatics <6.9 6.9 6.9 mg/Kg ;) 01/19/17 07:20 01/25/17 00:18
Surrogate %Recove:ry Qualifier Lirnlts Prepared Analyzed DH Fae 1-Chlorooctadecane 86 40-140 01119117 07:20 01124117 20:07 1
crTerphenyl 81 40-140 01119117 07:20 01125117 00:18 1
Method; 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Silver <0.80 2.0 0.80 mg/Kg n 01/16/17 08:55 01/17/17 13:16
Arsenic 9.4 4.0 1.6 mg/Kg '" 01/16/17 08:55 01/17/1713:16
Bariun1 310 4.0 0.80 mg/Kg 1) 01/16/17 08:55 01/17/17 13:16
Beryllium 0.71 J 1.2 0.40 mg/Kg i:1 01/16/17 08:55 01/17/17 13:16
Cobalt 9,9 4.0 1.2 mg/Kg \) 01/16/17 08:55 01/17/17 13:16
Chromium 22 4_.o 0.80 mg/Kg " 01/16/17 08:55 01/17/17 13:16
Copper 68 8.0 0.80 mg/Kg " 01/16/17 08:55 01/17/1713:16
Nickel 24 2.0 1.2 mg/Kg l) 01/16/17 08:55 01/17/1713:16
Lead 90 4.0 0.80 mg/Kg ::t 01/16/17 08:55 01/17/17 13:16
Selenium 2.3 J 8.0 1.6 mg/Kg " 01/16/17 08:55 01/17/1713:16
Thallium <1.6 4.0 1.6 mg/Kg " 01/16/17 08:55 01/17/1713:16
Vanadium 27 8.0 1.2 mg/Kg " 01/16/17 08:55 01117/17 13:16
Zinc 200 8.0 3.2 mg/Kg J) 01/16/17 08:55 01/17/17 13:16
Method: 7471A ·Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Mercury 0.043 0.013 0.0078 mg/Kg 01/15/1712:43 01/16/17 12:16 1
General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Chromium, hexavalent <11 15 11 mg/Kg <> 01/20/1717:00 01/23/17 12:07 1
Cyanide, Total <0.56 1.1 0.56 mg/Kg .;:; 01/18/1710:53 01/18/17 17:37 1
Percent Moisture 76.7 0.1 0.1 % 01/17/17 14:08
General Chemistry • Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed OJI Fae
Nitrate Nitrite as N <1.5 4.3 1.5 mg/Kg n 01/16/1712:27 1
Nitrate Nitrite as N <7.7 21 7.7 mg/Kg \;!' 01/16/17 12:32 5
TestAmerica Pensacola
Page 43 of 140 2/112017
Client Sample Results Client: C-K Associates Projecl/Site: Moffat & Nichol
Client Sample ID: CK-8 Date Collected: 01/1311710:10 Date Received: 01/14117 08:32
Method: 8260C ·Volatile Organic Compounds by GC/MS Analyte Result Qualifier
1, 1, 1,2-Tetrach!oroethane <0.0052
1, 1, 1-Trlchloroethane 1,1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1, 1-Dich!oroethane 1, 1-Dichloroethene 1,2-Dibromo-3-Chloropropane
1,2·Dichlorobenzene 1,2-Dich!oroethane
1,2-Dichloropropane
1,3-Dichlorobenzene 1,4-Dich!orobenzene
Acetone Benzene Brornoform Bromomethane
Carbon disulfide
Carbon tetrachloride
Ch!orobenzene
Chlorodibromomethane
Chloroethane
Chloroform Chlorornethane cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dlchlorobromomethane
Ethylbenzene
Methyl tert-butyl ether
Methylene Chloride 2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene T etrachtoroethene
Toluene
trans-1,2-Dich!oroethene
trans-1,3-Dichloropropene
Trich!oroethene Trichtorofluoromethane
Vinyl chloride
Xylenes, Total 1,2 ,4-Trichlorobenzene
lsobutyl alcohol
Surrogate
4-Bromofluorobenzene Dibromof/uorometl1ane
Toluene-dB (Surr)
<0.0023
<0.0052 <0.0052
<0.0017 <0.0052
<0.0068
<0.0015
<0.0017
<0.0052
<0.0020
<0.0052
0.064 <0.0014
<0.0052 <0.0052
<0.0052 <0.0035
<0.0011
<0.0052
<0.0052 <0.0052 <0.0021
<0.0016
<0.0025
<0.0052 <0.0013
<0.0021 <0.021
<0.012
<0.010
<0.0021
<0.0052
<0.0021 <0.0052
<0.0052 <0.0021
<0.0052
<0.0052 <0.0039
<0.0041 <0.021
%Recovery Qualifier
101
102
95
RL 0.010 0.010
0.010 0.010
0.010 0.010
0.010 0.010 0.010
0.010 0.010 0.010
0.052 0.010
0.010 0.010 0.010
0.010
0.010 0.010
0.010
0.010 0.010
0.010
0.010 0.010
0.010
0.010 0.031 0.052
0.052 0.010 0.010
0.010 0.010 0.010
0.010 0.010 0.010
0.021 0.010
0.052
Lllnlts
72-1.22
79-123
80-120
Page 44 of 140
MDL Unit
0.0052 mg/Kg 0.0023 mg/Kg 0.0052 mg/Kg 0.0052 mg/Kg
0.0017 mg/Kg 0.0052 mg/Kg 0.0068 mg/Kg
0.0015 mg/Kg 0.0017 mg/Kg
0.0052 mg/Kg
0.0020 mg/Kg 0.0052 mg/Kg
0.015 mg/Kg 0.0014 mg/Kg
0.0052 mg/Kg 0.0052 mg/Kg
0.0052 mg/Kg
0.0035 mg/Kg 0.0011 mg/Kg 0.0052 mg/Kg 0.0052 mg/Kg
0.0052 mg/Kg 0.0021 mg/Kg 0.0016 mg/Kg
0.0025 mg/Kg 0.0052 mg/Kg
0.0013 mg/Kg
0.0021 mg/Kg
0.021 mg/Kg 0.012 mg/Kg
0.010 mg/Kg
0.0021 mg/Kg 0.0052 mg/Kg
0.0021 mg/Kg
0.0052 mg/Kg 0.0052 mg/Kg 0.0021 mg/Kg 0.0052 mg/Kg
0.0052 mg/Kg 0.0039 mg/Kg 0.0041 mg/Kg 0.021 mg/Kg
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-3 Matrix: Solid
Percent Solids: 46.4
D Prepared
" 01/22117 07:44 " 01/22117 07:44
Analyzed 01/2211713:31 01/22117 13:31
" 01/22117 07:44 01122117 13:31 " 01/22117 07:44 01/22117 13:31
" 01/22117 07:44 01122117 13:31 ,, 01/22117 07:44 01/2211713:31
" 01/22117 07:44 01/2211713:31 v 01/22117 07:44 01/22117 13:31 " 01/22117 07:44 01/2211713:31
" 01/22117 07:44 01/22117 13:31 ,, 01/22117 07:44 01/22/17 13:31 ;) 01/22117 07:44 01/22117 13:31
" 01/22117 07:44 01/22117 13:31 " 01/22117 07:44 01/2211713:31
" 01/22117 07:44 01/2211713:31 ,, 01/22117 07:44 01/22117 13:31 ,, 01/22117 07:44 01/22/1713:31
" 01/22117 07:44 01/22/1713:31 " 01/22117 07:44 01/22/17 13:31 " 01122117 07:44 01/22117 13:31 " 01/22117 07:44 01/22117 13:31 ,, 01/22117 07:44 01/22117 13:31
1:1 01/22117 07:44 01/22117 13:31 (; 01/22117 07:44 0112211713:31
" 01122117 07:44 01/2211713:31 "' 01/22117 07:44 01/22/17 13:31 ,, 01/22117 07:44 01/22117 13:31
i) 01/22117 07:44 01/22117 13:31 ,, 01/22117 07:44 01/22/1713:31
" 01/22117 07:44 01/2211713:31 ,, 01/22117 07:44 01/2211713:31
" 01/22117 07:44 01/22117 13:31 " 01/22117 07:44 01/22/17 13:31 ,, 01/22117 07:44 01/2211713:31
,, 01/22117 07:44 01122117 13:31
;) 01122117 07:44 01/22117 13:31
" 01/22117 07:44 01/2211713:31 ,, 01/22117 07:44 01/22117 13:31
" 01/22117 07:44 01/2211713:31 " 01/22117 07:44 01/2211713:31 " 01/22117 07:44 01/2211713:31 " 01/22117 07:44 01/22117 13:31
Prepared
01122117 07:44
01122117 07:44
Analyzed
01122117 13:31
0112211713:31
01122117 07:44 0112211713:31
Oii Fae
1
DI/ Fae
1
TestAmerica Pensacola
2/112017
Client Sample Results Client: C-K Associates Projecl/Site: Moffat & Nichol
Client Sample ID: CK-8 Date Collected: 01/13/1710:10 Date Received: 01114117 08:32
Method: 82700 • Semivolatlle Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene <0.069 0.69 Acenaphthylene
Aniline Anthracene Benzo[aJanthracene Benzo[a]pyrene
Benzo{b ]fluoranthene Benzo[g,h,iJperylene BenzofkJfluoranthene 1, 1'-Biphenyl Bis(2-ch!oroethyl)ether bls (2-chloroisopropyl) ether
Bis(2-ethylhexyl).phthalate Butyl benzyl phthalate 4-ChloroaniHne 2-Chloronaphtha!ene
2-Ch!orophenol
Chrysene Oibenz{a,h)anthracene
Dibenzofuran 3,3'-Dichlorobenzidine
2,4-Dich!orophenol Diethyl phthalate
2.4-Dime!hylphenol
Dimethyl phthalate 1,3-Dinitrobenzene
2,4-Dinitrophenol 2,4-Dlnitroto!uene 2,6-Dinitrotofuene
Di-n-octyl phthalate Fluoranthene
Fluorene Hexach!orobenzene
Hexachlorobutactiene
Hexachlorocyclopentadiene Hexach!oroethane lndeno[1,2,3-cd]pyrene
lsophorone 2-Methylnaphthalene Naphthalene 2-Nltroani!ine
3-Nitroani!ine 4-Nitroaniline
Nitrobenzene
4-Nitropheno! N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
<0.069
<0.091 <0.069 <0.069
<0.069
0.086 J <0.069
<0.069
<0.069
<0.069
<0.069
0.093 J <0.069
<0.069
<0.069
<0.069
<0.069 <0.069
<0.069
<0,069
<0.069
<:0.069
<:Q.069
<0.069 <0.069 <:0.61
<0.069
<0.069 <0.069 <0.069
<0.069
<:0.21
<0.069
<0.14
<:0.21
<0.069 <0.069 <0.069
<0.069
<0.069 <0.069
<0.069
<0.069
<0.23
<0.23 <0.069
<0.14
<0.069
0.69
0.69
0.69 0.69
0.69 0.69
0.69 0.69 0.69
0.69 0.69
0.69 0.69 0.69 0.69
0.69
0.69 0.69
0.69 0.69
0.69 0.69 0.69
0.69 0.69
2.1
0.69 0.69 0.69 0.69
0.69 0.69
0.69 0.69 0.69 0.69
0.69
0.69 0.69
0.69 0.69 0.69 0.69
0.69 0.69 0.69
1.4
0.69
Page 45 of 140
MDL Unit 0.069 mg/Kg 0.069 mg/Kg
0.091 mg/Kg 0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg
0.61 mg/Kg
0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg 0.21 mg/Kg
0.069 mg/Kg
0.14 mg/Kg 0.21 mg/Kg
0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg 0.069 mg/Kg
0.069 mg/Kg 0.23 mg/Kg
0.23 mg/Kg 0.069 mg/Kg 0.14 mg/Kg
0.069 mg/Kg
Tes!America Job ID: 400-132540-1
Lab Sample ID: 400-132650.-3 Matrix: Solid
Percent Solids: 46.4
D Prepared Analyzed Oil Fae IIl) 01/1811709:33 01/19/17 01:14 ;) 01/18117 09:33 01119/17 01:14
" 01/16/17 09:33 01/19/17 01:14 ~ 01118/17 09:33 01/19117 01:14 " 01/18/17 09:33 01/19/17 01:14
" 01/18/1709:33 01/19/17 23:14 " 01118/1709:33 01119117 23:14 ,, 01118/17 09:33 01119117 23:14 ,,, 01/18/17 09:33 01119117 23:14 ,, 01/18/17 09:33 01119/17 01:14
" 01118/17 09:33 01/19/17 01:14 1) 01118/17 09:33 01/19/17 01:14
•:• 01/18/17 09:33 01/19117 01:14
" 01118/17 09:33 01/19117 01:14 " 01118/1709:33 01/19/17 01:14 ,, 01/18/1709:33 01/19/17 01:14
'" 01/18/17 09:33 01/19/17 01:14 " 01/18/1709:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 23:14 " 01/18/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14
" 01118/17 09:33 01/19117 01:14 " 01116117 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14
" 01/1811709:33 01/19/17 01:14 " 01/18/1709:33 01119/17 01:14 " 01/18/17 09:33 01/19/17 01:14 :) 01/18/17 09:33 01/19/17 01:14
" 01118/17 09:33 01119/17 01:14 " 01/18/17 09:33 01119/17 01:14 " 01/18/1709:33 01/19/1701:14
'" 01/18/17 09:33 01119/17 01:14 " 01/18/17 09:33 01/19/17 01:14
" 01/18/17 09:33 01/19/17 01:14 " 01118/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14
" 01/18/17 09:33 01119/17 23:14 " 01/18/1709:33 01119/1701:14 " 01/18/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14
" 01118/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14 " 01118/17 09:33 01/19117 01:14 " 01/16/17 09:33 01/19/17 01:14
" 01118/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01:14 " 01/18/17 09:33 01/19/17 01 :14 " 01/18/17 09:33 01/19/17 01:14
" 01118/17 09:33 01/19/17 01:14
Tes!America Pensacola
211/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol
Client Sample ID: CK-8 Lab Sample ID: 400-132650-3 Date Collected: 0111311710:10 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 46.4
Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae Phenol <0.069 0.69 0.069 mg/Kg ,, 01118117 09:33 01119117 01:14 1
Pyrene 0.069 J 0.69 0.069 mg/Kg ,, 01118/17 09:33 01/19/17 01:14
1,2,4,5-Tetrachlorobenzene <0,069 0.69 0.069 mg/Kg " 01/18117 09:33 01/19/17 01:14
2,3,4,6-T etrachlorophenol <0.069 0.69 0.069 mg/Kg " 01/18/17 09:33 01119117 01:14 1,2,4-Trichlorobenzene <0,069 0.69 0.069 mg/Kg •:• 01/18117 09:33 01/19/17 01:14
2.4 ,5-Trichlorophenol <0.069 0.69 0.069 mg/Kg '" 01/18/1709:33 01/19117 01:14
2,4,6-Trichlorophenol <0.069 0.69 0.069 mg/Kg " 01118117 09:33 01119117 01:14
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae 2-Fluorobiphenyl 51 27 -127 01118117 09:33 01119117 01:14 1
2-Ffuorophenol 59 25-128 01118117 09:33 01119117 01:14
Nitrobenzene-d5 47 15 -136 01118117 09:33 01119117 01:14
P/1enol-d5 61 29-130 01118117 09:33 01119117 01:14
Terphenyl-d14 76 24- 146 01118117 09:33 01119117 01:14
2,4,6-Tribromopflenol 63 10-150 01118117 09:33 01119117 01:14
Method: MAVPH - Ma.ssachusetts - Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae C6-C8 Aliphatics <12 12 12 mg/Kg " 01/16/1711:30 01117117 02:16 50 CB-C 10 Aliphatics <19 19 19 mg/Kg " 01116/1711:30 01117117 02:16 50
C8-C10 Aromatics <9.7 9.7 9.7 mg/Kg J) 01116/1711:30 01117117 02:16 50
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae a,a,a-Trifluorotoluene (fid) 83 70-130 0111611711:30 01/17117 02:16 50
a,a,a-Tn"fluorotoluene (pid) 86 70-130 0111611711:30 01117117 02:16 50
Method: 8081 B - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae Aldrin <0.0026 0.0073 0.0026 mg/Kg " 01/1811712:42 01/19/17 22:50 2
alpha-BHC <0.0010 0.0073 0.0010 mg/Kg " 01118117 12:42 01119/17 22:50 2 beta-BHC <0.0021 0.0073 0.0021 mg/Kg ,, 01118/1712:42 01/19/17 22:50 2
della·BHC <0.0014 0.0073 0.0014 mg/Kg " 0111811712:42 01119117 22:50 2
-gamma-BHC (Undane) <0.00094 0.0073 0.00094 mg/Kg " 01118/1712:42 01119117 22:50 2 alpha-Chlordane <0.0012 0.0073 0.0012 mg/Kg " 01118/17 12:42 01119117 22:50 2
gamma-Chlordane <0.0012 0.0073 0.0012 mg/Kg ;:i 01118117 12:42 01119117 22:50 2
4,4'-DDD 0.00084 J 0.0073 0.00082 mg/Kg " 01118/1712:42 01/19/17 22:50 2
4,4'-DDE <0.0012 0.0073 0.0012 mg/Kg " 01/18/17 12:42 01119/17 22:50 2
4,4'-DDT <0.0033 0.0073 0.0033 mg/Kg " 01/18/1712:42 01119/17 22:50 2 Dieldrin <0.0015 0.0073 0.0015 mg/Kg ;) 01/18/1712:42 01119117 22:50 2
Endosulfan I <0.00090 0.0073 0.00090 mg/Kg " 01/18/1712:42 01119/17 22:50 2
Endosu!fan II <0.00099 0.0073 0.00099 mg/Kg " 01/1811712:42 01/19/17 22:50 2
Endosulfan sulfate <0.00090 0.0073 0.00090 mg/Kg l'J 01118/1712:42 01/19117 22:50 2
Endrin <0.00082 0.0073 0.00082 mg/Kg " 01118/1712:42 01119117 22:50 2
, Endrin aldehyde <0.0012 0.0073 0.0012 mg/Kg J) 01/18/1712:42 01/19/17 22:50 2 Endrin ketone <0.0015 0.0073 0.0015 mg/Kg " 01/18/1712:42 01119117 22:50 2
Heptachlor <0.0010 0.0073 0.0010 mg/Kg ,, 01118/1712:42 01/19117 22:50 2
Heptachlor epoxide <0.0019 0.0073 0.0019 mg/Kg " 01/18/1712:42 01119117 22:50 2
Methoxychlor <0.0014 0.0073 0.0014 mg/Kg " 01118/1712:42 01119117 22:50 2 Toxaphene <0.12 0.43 0.12 mg/Kg 0 01118/1712:42 01/19117 22:50 2
TestAmerica Pensacola
Page 46 of 140 2/112017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: CK-8 Lab Sample ID: 400-132650-3 Date Collected: 01/13/1710:10 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 46.4
Surrogate %RecovetY Qua/If/er Limits Prepared Analyzed Dil Fae E DCB Decachlorobiphenyl 58 26-129 0111811712;42 01119117 22:50 2
Tetrachloro-m·xylene 52 31-122 01118117 12:42 01119117 22:50 2
Method: MA-EPH - Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
c10.c12 A!iphatlcs <3.4 3.4 3.4 mg/Kg ,, 01/19/17 07:20 01/24/17 20:17 1
C10-C12 Aromatics <3.4 3.4 3.4 mg/Kg "' 01/19/17 07:20 01/25/17 00:27 1
C 12-C 16 AHphatics <3.4 3.4 3.4 mg/Kg " 01/19/17 07:20 01/24/17 20:17
C12-C16 Aromatics <3.4 3.4 3.4 mg/Kg " 01/19/17 07:20 01/25/17 00:27
C16-C35 Aliphatics 17 3.4 3.4 mg/Kg n 01/19/17 07:20 01/24/17 20:17
C21-C35 Aromatics <3.4 3.4 3.4 mg/Kg n 01/19117 07:20 01 /25/17 00:27
C16-C21 Aromatics <3.4 3.4 3.4 mg/Kg " 01/19/17 07:20 01/25/17 00:27
Surrogate %Recovery Qualifier L/111/ts Prepared Analyzed Di/ Fae
1-Clllorooctadecane 85 40-140 0111911707:20 01124117 20:17 1
o-Terphenyl 78 40-140 01119117 07:20 01125117 00.27
Method: 601 OC - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Silver <0.40 1.0 0.40 mg/Kg 0 01/16/17 08:55 01/17/1713:20 1
Arsenic 4.3 2.0 0.80 mg/Kg ,, 01/16/17 08-.55 01/17/1713:20
Barium 88 2.0 0.40 mg/Kg " 01/16/17 08:55 01/17/1713:20
Beryllium 0.36 J 0.60 0.20 mg/Kg " 01/16/17 08:55 01/17/1713:20
Cobalt 5.0 2.0 0.60 mg/Kg " 01/16/1708:55 01/17/17 13:20
Chromium 11 2.0 0.40 mg/Kg " 01/16/1708:55 01/17117 13:20
Copper 19 4.0 0.40 mg/Kg u 01/16/17 08:55 01/17/17 13:20
Nickel 12 1.0 0.60 mg/Kg " 01/16/17 08:55 01/17/17 13:20
Lead 30 2.0 0.40 mg/Kg " 01/16/17 08:55 01/17/17 13:20
Selenium <0.80 4.0 0.80 mg/Kg " 01 /16/17 08:55 01/1711713:20
Thallium <D.80 2.0 0.80 mg/Kg " 01/16/17 08:55 01/17/1713:20
Vanadium 1Z 4.0 0.60 mg/Kg " 01/16/17 08:55 01/17/1713:20
Zinc 84 4.0 1.6 mg/Kg ,, 01/16/17 08:55 01/17/1713:20
Method: 7471A ·Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Mercury 0.031 0.012 0.0075 mg/Kg 01/15/1712:43 01/16/1712:17 1
General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae
Chromium, hexavalent <5.5 7.9 5.5 mg/Kg ,,, 01/20/17 17:00 01/23/1712:07 1
Cyanide, Total <0.29 0.55 0.29 mg/Kg " 01/18/1710:53 01/18/1717:37
Percent Moisture 53.6 0.1 0.1 % 01/1711714:08
General Chemistry - Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae
Nitrate Nitrite as N 0.99 J 2.2 0.78 mg/Kg ,, 01/16/17 12:28 1
TestAmerica Pensacola
Page 47 of 140 211/2017
Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: CK-9 Date Collected: 01/13/1710:25 Date Received: 01114/17 08:32
Method: 8260C • Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL 1, 1, 1,2-Tetrachloroethane <0.0064 0_013
1, 1, 1-Trichloroethane 1,1,2,2-Tetrachloroethane
1, 1,2-Trich!oroethane 1, 1-Dichloroethane 1, 1-Dichloroethene 1.2-Dibromo-3-Ch!oropropane
1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane
1,3-Dlch!orobenzene 1.4-Dichlorobenzene
Acetone Benzene Bromoforrn Bromomethane
Carbon disulfide Carbon tetrachloride
Chlorobenzene Chlorodibromomethane
Chloroethane
Chloroform Chloromethane
cis-1,2-Dichloroethene cis-1,3-Dich!oropropene Dichlorobromomethane
Ethylbenzene Methyl tert-butyl ether
Methylene Chloride 2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene T etrach!oroethene
Toluene trans-1,2-Dichloroethene trans-1,3-Dich!oropropene Trichloroethene Trich!orofluoromethane
Vinyl chloride Xylenes, Total 1,2.4-Trichlorobenzene
lsobutyl alcohol
Surrogate
4-Bromofluorobenzene Dibromofluorometl1ane
Tofuene-08 (Sun-)
<0.0028
<0.0064 <0.0064
<0.0021 <0.0064
<0.0085 <0.0018
<0.0021 <0.0064
<0.0024 <0.0064
0.15 <0.0017 <0.0064
<0.0064
0.0078 J <0.0044 <0.0013
<0.0064 <0.0064 <0.0064
<0.0026
<0.0019
<0.0031 <0.0064
<0.0016
<0.0026 <0.026 <0.015
<0.013
<0.0026 <0.0064 <0.0026
<0.0064
<0.0064 <0.0026
<0.0064 <0.0064 <0,0049
<0.0051 <0.026
%Recovery Qualifier
117
93
112
0.013
0.013 0.013
0.013 0.013 0.013
0.013 0.013 0.013 0.013 0.013
0.064 0.013
0.013 0.013
0.013
0.013 0.013 0.013
0.013 0.013 0.013 0.013
0.013 0.013 0.013
0.013
0.038 0.064 0.064 0.013 0.013
0.013 0.013
0.013 0.013
0.013
0.013 0.026 0.013 0.064
Llfnits 72-122
79-123
80-120
Page 48 of 140
MDL Unit 0.0064 mg/Kg 0.0028 mg/Kg 0.0064 mg/Kg
0.0064 mg/Kg
0.0021 mg/Kg 0.0064 mg/Kg
0.0085 mg/Kg 0.0018 mg/Kg 0.0021 mg/Kg
0.0064 mg/Kg 0.0024 mg/Kg 0.0064 mg/Kg
0.019 mg/Kg
0.0017 mg/Kg 0.0064 mg/Kg 0.0064 mg/Kg 0.0064 mg/Kg
0.0044 mg/Kg
0.0013 mg/Kg 0.0064 mg/Kg
0.0064 mg/Kg
0.0064 mg/Kg 0.0026 mg/Kg
0.0019 mg/Kg
0.0031 mg/Kg 0.0064 mg/Kg
0.0016 mg/Kg
0.0026 mg/Kg 0.026 mg/Kg 0.015 mg/Kg 0.013 mg/Kg
0.0026 mg/Kg 0.0064 mg/Kg
0.0026 mg/Kg
0.0064 mg/Kg 0.0064 mg/Kg 0.0026 mg/Kg 0.0064 mg/Kg
0.0064 mg/Kg
0.0049 mg/Kg 0.0051 mg/Kg
0.026 mg/Kg
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-4 Matrix: Solid
Percent Solids: 52.0
O Prepared Analyzed " 01/19/17 08:59 01119/17 16:47 Q 01/19/17 08:59 01119117 16:47
" 01/19/17 08:59 01/19/17 16:47
" 01/19/17 08:59 01/19/1716:47 l) 01/19/17 08:59 01/19117 16:47
" 0111911708:59 01/19/1716:47
'" 01119117 08:59 01/19/17 16:47 " 01119/17 08:59 01/19/1716:47 l) 01119/17 08:59 01/19117 16:47
i:i 01119/17 08:59 01/19/1716:47
" 01/19/17 08:59 01/19/1716:47 l) 01/19/17 08:59 01/19/17 16:47
" 01/19/17 08:59 01/19/17 16:47
" 01/19/17 08:59 01119/17 16:47 " 01/19/17 08:59 01119/1716:47 " 01/19/17 08:59 01/19117 16:47 " 01/19/17 08:59 01/1911716:47
" 01/19/17 08:59 01/19/17 16:47 " 01119117 08:59 01/19/17 16:47 n 01/19/17 08:59 01/19/17 16:47
" 01119/17 08:59 01/19/17 16:47 l) 01119/17 08:59 01/19/17 16:47
" 01/19/17 08:59 01/19/17 16:47
" 01/19/17 08:59 01/19/17 16:47 Q 01119/17 08:59 01/19/17 16:47 " 01/19/17 08:59 0111911716:47
" 01/19/17 08:59 01119/1716:47 " 01/19/17 08:59 01/1911716:47 l) 01/19117 08:59 01119/1716:47 " 01/19/17 08:59 01/19/17 16:47
"' 01/19/17 08:59 01/19/17 16:47 ,, 01119117 08:59 01/19/1716:47
" 01/19/17 08:59 01/19/17 16:47 :) 01/19/1708:59 01/19/1716:47
" 01/19/17 08:59 01/19/17 16:47 '" 01/19/17 08:59 01/19/17 16:47 " 01/1$117 08:59 01/19/1716:47 ,, 01/19/17 08:59 01/19/1716:47
"' 01/19/17 08:59 01/19117 16:47 " 01119/17 08:59 0111911716:47 " 01/19117 08:59 01/19/1716:47 ,, 01/19117 08:59 01119117 16:47
Prepared 01119117 08:59
01119117 08:59
Analyzed 01119117 16:47
0111911716:47
01119117 08:59 01119117 16:47
Oil Fae
1
DJ/ Fae
1
TestAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: CK-9 Dat<l Collected: 0111311710:25 Date Received: 01114/17 08:32
Method: 82700 • Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene <0.063 0.63 Acenaphthylene
Aniline Anthracene Benzo[a]anthracene
Benzo[a]pyrene Benzo[b ]flu ora nthene Benzo[g,h,i]perylene
Benzo[k]fluoranthene 1, 1 '-Biphenyl
8is(2-chloroethy!)ether bis {2-chloroisopropyl) ether
Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate 4-Chloroanilfne 2-Chloronaphtha!ene
2-Ch!orophenol
Chrysene Dibenz(a.h}anthracene Dibenzofuran
3,3'-Dlch!orobenzidine 2,4-Dichforophenol Diethyl phthalate 2,4-Dimethy!phenol
Dimethyl phthalate 1,3-Dlnltrobenzene 2,4-Dinitropheno!
2,4-Dlnitrotoluene 2,6-Dinitroto!uene
Oi~n·octyl phthalate
Fluoranthene
Fluorene Hexachlorobenzene
Hexachlorobutad!ene
Hexach!orocyclopentadiene Hexachloroethane
lndeno[1,2,3-cd]pyrene lsophorone 2-Methylnaphtha!ene Naphthalene 2-Nitroani!ine 3-Nitroaniline 4-Nltroaniline
Nitrobenzene 4-Nitrophenol
N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
<0.063
<0.082
<0.063
<0.063
0.18 J 0.24 J 0.10 J 0.12 J
<0.063
<0.063 <0.063
0.089 J <0.063
<0.063
<0.063
<0.063
0.14 J <0.063
<0.063
<0.063
<0.063 <0.063 <0.063
<0.063
<0.063
<0.55 <0.063 <0.063
0.073 J 0.29 J
<0.063
<0.19
<0.063 <0.13
<0.19
0.091 J <0.063
<0.063
<0.063
<0.063
<0.063
<0.063 <0.063
<0.21
<0.21
<0.063 <0.13
0.12 J
0.63
0.63 0.63 0.63
0.63
0.63 0.63 0.63
0.63 0.63 0.63 0.63
0.63 0.63
0.63
0.63 0.63 0.63 0.63
0.63
0.63 0.63
0.63
0.63 0.63
1.9 0.63 0.63
0.63 0.63
0.63 0.63
0.63
0.63 0.63 0.63 0.63
0.63 0.63 0.63
0.63 0.63
0.63 0.63
0.63 0.63
1.3 0.63
Page 49of140
MDL Unit 0.063 mg/Kg 0.063 mg/Kg 0.082 mg/Kg
0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg 0.063 mg/Kg 0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg 0.063 mg/Kg 0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg
0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg 0.063 mg/Kg 0.063 mg/Kg
0.55 mg/Kg 0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg 0.19 mg/Kg
0.063 mg/Kg
0.13 mg/Kg 0.19 mg/Kg
0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg 0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg 0.063 mg/Kg
0.063 mg/Kg 0.21 mg/Kg
0.21 mg/Kg 0.063 mg/Kg
0.13 mg/Kg 0.063 mg/Kg
TestAmerica Job ID: 400-132540-1
Lah Sample ID: 400-132650-4 Matrix: Solid
Percent Solids: 52.0
0 Prepared Analyzed
r; 01118/17 09:33 01/19/17 01:47 :: 01118/17 09:33 01/19117 01:47
" 01118117 09:33 01119117 01:47 0 01/18/17 09:33 01/19/1701:47 ,, 01118117 09:33 01/19117 01:47
,, 01118/17 09:33 01/19117 23:44
0 01118117 09:33 01119117 23:44 ,, 01118/17 09:33 01119/17 23:44 ,, 01118/17 09:33 01119117 23:44
,, 01118/17 09:33 01/19/17 01:47
" 01118/17 09:33 01/19/17 01:47 " 01118/17 09:33 01/19/17 01:47 :) 01118/17 09:33 01/19/17 01:47 ,, 01118/17 09:33 01/19117 01:47 ,, 01/18117 09:33 01/19/17 01:47
" 01/18/17 09:33 01119117 01:47 ,, 01/18/17 09:33 01/19/17 01:47
!) 01118/17 09:33 01119117 01:47 " 01/18/17 09:33 01119117 23:44 ,, 01118/17 09:33 01119117 01:47
,,, 01118/17 09:33 01/1911701:47
" 01118117 09:33 01119/17 01:47 " 01/18/17 09:33 01/19/17 01:47 " 01/18/17 09:33 01/19117 01:47 ,, 01118/17 09:33 01/19/17 01:47
" 01/18117 09:33 01119/17 01:47 " 01118/1709:33 01/19/1701:47 ,, 01118/17 09:33 01/19/17 01:47 (j 01/18/17 09:33 01/19/17 01:47
" 01/18117 09:33 01/19/17 01:47 " 01118/17 09:33 01119117 01:47
" 01/18/17 09:33 01119/17 01:47 " 01118117 09:33 01119/17 01:47
" 01/18/17 09:33 01/1911701:47 {j 01/18117 09:33 01/19/17 01:47 ,, 01118/17 09:33 01119/17 01:47
" 01/18/17 09:33 01119117 23:44 {j 01118/17 09:33 01119/17 01:47 " 01118/17 09:33 01/19/1701:47 ,, 01118/17 09:33 01119/17 01:47
" 01/18/17 09:33 01/19/1701:47 " 01/18/1709:33 01/1911701:47 " 01118/17 09:33 01/19/17 01 :47 " 01/18117 09:33 01/19/17 01:47
" 01118117 09:33 01/19/17 01:47
" 01/18117 09:33 01/19/17 01:47 " 01118117 09:33 01119/17 01:47
" 01118/17 09:33 01/19117 01:47 " 01/18/17 09:33 01/19117 01:47
Ollfac E 1
1
1
1
1
TestAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecUSite: Moffat & Nichol
Client Sample ID: CK-9 Lab Sample ID: 400-132650-4 Date Collected: 01113117 10:25 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 52.0
e
1 E Method: 8270D • Semivotatite Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fa
Phenol <0.063 0.63 0.063 mg/Kg ::1 01/18/17 09:33 01/19/17 01:47
Pyrene 0.37 J 0.63 0.063 mg/Kg ::: 01/18/17 09:33 01/19/17 01:47
1,2,4, 5-T etrach1orobenzene <0.063 0.63 0.063 mg/Kg " 01/18/17 09:33 01/19/17 01:47
2,3,4,6-T etrachlorophenol <0.063 0.63 0.063 mg/Kg f) 01/18/17 09:33 01/19/17 01 :47
1,2,4-Trichlorobenzene <0.063 0.63 0.063 mg/Kg (l 01/18/17 09:33 01/19/17 01:47
2.4,5-Trichlorophenol <0.063 0.63 0.063 mg/Kg " 01/18/17 09:33 01/19/1701:47
2,4 ,6-Trichlorophenol <0.063 0.63 0.063 mg/Kg D 01/18/17 09:33 01/19/17 01:47
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
2-Fluorobiphenyl 67 27 -127 0111811709:33 01119117 01:47 1
2-Fluorophenol 68 25-128 01118117 og:33 01119117 01:47 1
Nitrobenzene-d5 56 15-136 0111811709:33 01119117 01:47 1
PJJenol-d5 68 29-130 01118117 09:33 01119117 01:47 1
Teiphenyl-d14 111 24-146 01118117 09:33 01119117 01:47
2,4,6· Tribromophenot 67 10-150 01118117 09:33 01119117 01:47
Method: MAVPH ·Massachusetts· Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
C6·C8 A!iphatics <15 15 15 mg/Kg " 01/16/17 11 :30 01/17/17 03:16 50
CB-C10 Al!phatics <26 26 26 mg/Kg :) 01116/1711:30 01/17/17 03:16 50
C8-C10 Aromatics <13 13 13 mg/Kg " 01/16/1711:30 01/17/17 03:16 50
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae
a,a,a-Trifluorotoluene (fid) 93 70-130 0111611711:30 01117117 03:16 50
a,a,a-Trifluorotoluene (pid) 92 70-130 0111611711:30 0111711703:16 50
Method: 8081 B • Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DllFac
Aldrin <0.0023 0.0065 0.0023 mg/Kg (~ 01/18/1712:42 01/19/17 23:20 2
alpha-BHC <0.00092 0.0065 0.00092 mg/Kg " 01/18/1712:42 01/19/17 23:20 2
beta-BHC <0.0019 0.0065 0.0019 mg/Kg ,,, 01/18/1712:42 01/19/17 23:20 2
della-BHC <0.0012 0.0065 0.0012 mg/Kg " 01/18/1712:42 01/19/17 23:20 2
gamma-BHC (Undane) <0.00085 0.0065 0.00085 mg/Kg n 01/18/1712:42 01/19/17 23:20 2
alpha-Chlordane <0.0011 0.0065 0.0011 mg/Kg 0 01/18/1712:42 01/19/17 23:20 2
gamma-Chlordane 0.0010 J 0.0065 0.0010 mg/Kg 0 01/18/1712:42 01119117 23:20 2
4,4'-DDD 0.00085. J 0.0065 0.00073 mg/Kg " 01/18/1712:42 01/19/17 23:20 2
4,4'-DDE 0.0010 J 0.0065 0.0010 mg/Kg " 01/18/1712:42 01/19/17 23:20 2
4,4"-DDT <0.0030 0.0065 0.0030 mg/Kg " 01/18/1712:42 01119/17 23:20 2
Dieldrin <0.0014 0.0065 0.0014 mg/Kg ,,, 01/18/1712:42 01/19/17 23:20 2
Endosulfan I <0.00081 0.0065 0.00081 mg/Kg " 01/18/1712:42 01/19/17 23:20 2
Endosulfan II <0.00089 0.0065 0.00089 mg/Kg " 01118/1712:42 01/19/17 23:20 2
Endosulfan sulfate <0.00081 0.0065 0.00081 mg/Kg ,, 01/18/1712:42 01/19/17 23:20 2
Endr!n <0.00073 0.0065 0.00073 mg/Kg ,, 01/18/1712:42 01/19/17 23:20 2
Endrin aldehyde <0.0011 0.0065 0.0011 mg/Kg " 01/18/1712:42 01/19/17 23:20 2
Endrin ketone <0.0013 0.0065 0.0013 mg/Kg 0 01/18/17 12:42 01/19/17 23:20 2
Heptach!or <0.00092 0.0065 0.00092 mg/Kg o;i 01/18/17 12:42 01/19/17 23:20 2
Heptach!or epoxide <0.0017 0.0065 0.0017 mg/Kg " 01/18/17 12:42 01/19/17 23:20 2
Methoxychlor <0.0013 0.0065 0.0013 mg/Kg " 01/18/17 12:42 01/19/17 23:20 2
Toxaphene <0.11 0.38 0.11 mg/Kg t,1 01/18/1712:42 01/19/17 23:20 2
TestAmerica Pensacola
Page 50 of 140 211/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1
ProjecVSite: Moffat & Nichol
Client Sample ID: CK-9 Lab Sample ID: 400-132650-4 Date Collected: 01113/17 10:25 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 52.0
e
a
2
2
ae
m Surrogate %Recovery Qua/If/er Limits Prepared Arralyzed DI/ F
DCB Decar;hlorobiphenyl 57 26- 129 01118117 12:42 01119117 23:20
Tetrachloro-m-xylene 52 31-122 0111811712:42 01119117 23:20
Method: MA-EPH • Massachusetts • Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MOL Unit 0 Prepared Analyzed Oil F
C10-C12Aliphatics <3.1 3.1 3.1 mg/Kg ,, 01/19/17 07:20 01/24/17 20:37 1C10-C12 Aromatics <3.1 3.1 3.1 mg/Kg ;) 01/19/17 07:20 01/25/17 00:46
C12-C16 AHphatics <3.1 3.1 3.1 mg/Kg l) 01/19/17 07:20 01/24/17 20:37 C12-C16 Aromatics <3.1 3.1 3.1 mg/Kg 0 01/19/17 07:20 01/25/17 00:46
C16-C35 Aliphatics 20 3.1 3.1 mg/Kg ;) 01/19/17 07:20 01/24/17 20:37
C21-C35 Aro1natics 10 3.1 3.1 mg/Kg ;:< 01119/17 07:20 01/25/17 00:46
C-16-C21 Aromatics 4.3 3.1 3.1 mg/Kg " 01119/17 07:20 01/25/17 00:46
Surrogate %Recovety Qualifier Limits Prepared Analyzed Di/ Fae
t~Chlorooctadecanc 86 40-140 01119117 07:20 01124117 20:37 1
o-Terphenyl 74 40-140 01119117 07:20 01125117 00:46
Method: 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae
Silver <0.36 0.89 0.36 mg/Kg 0 01/16/17 08:55 01/17/17 13:23 1
Arsenic 4.5 1.8 0.72 mg/Kg " 01/16/17 08:55 01/17117 13:23 1
Barium 100 1.8 0.36 mg/Kg ,, 01/16/17 08:55 01/17/17 13:23
Beryllium 0.37 J 0.54 0.18 mg/Kg !;! 01/16/17 08:55 01/17/17 13:23
Cobalt 5.4 1.8 0.54 mg/Kg " 01/16117 08:55 01/17/17 13:23
Chromium 12 1.8 0.36 mg/Kg ,".} 01/16/1708:55 01/17/1713:23
Copper 23 3.6 0.36 mg/Kg ,, 01/16/17 08:55 01/17/1713:23
Nickel 12 0.89 0.54 mg/Kg ,,, 01/16/17 08:55 01/17/17 13:23
Lead 37 1.8 0.36 mg/Kg ::: 01/16/17 08:55 01/17/17 13:23
Selenium 0.83 J 3.6 0.72 mg/Kg (l 01/16/17 08:55 01/17/17 13:23
Thallium <0,72 1.8 0.72 mg/Kg n 01/16/17 08:55 01/17/17 13:23 1
Vanadium 13 3.6 0.54 mg/Kg n 01/16/17 08:55 01/17/17 13:23
Zinc 93 3.6 1.4 mg/Kg "' 01/16/17 08:55 01/17/17 13:23
Method: 7471A - Mercury (CVAAJ Analyte Result Qualifier RL MOL Unit D Prepared Analyzed Dll Fae
Mercury 0.053 0.013 0.0078 mg/Kg 01/15117 12:43 01/16/1712:19 1
General Chemistry Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae Chromium, hexava!ent <5.2 7.5 5.2 mg/Kg ,, 01/20/1717:00 01/23/17 12:07 1
Cyanide, Total <0.23 0.45 0.23 mg/Kg ;;i 01/18/17 10:53 01/18/17 17:37 1
Percent Moisture 48.0 0.1 0.1 % 01/17/17 14:08 1
General Chemistry - Soluble Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oii Fae
Nitrate Nitrite as N 1.1 J 1.9 0.69 mg/Kg i:1 01/16/17 12:29 1
TestAmerica Pensacola
Page51 of140 2/1/2017
Client Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol
Client Sample ID: CK-10 Date Collected: 01/13/1710:45 Date Received: 01/14/17 08;32
Method: 8260C - Volatile Organic Compounds by GC/MS Analyte Result Qualifier 1, 1, 1,2-Tetrachloroethane <0.0034 1,1,1-Trich!oroethane <0.0015
1,1,2,2-Tetrachloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethane 1, 1-Dlch!oroethene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dich!oroethane 1,2-Dlchloropropane
1,3-Dichlorobenzene 1.4-Dich!orobenzene
Aceto_ne Benzene Bromofonn Bromomethane
Carbon-disulfide Carbon tetrachloride
Chlorobenzene Chlorodibromomethane
Chloroethane
Chlorofom1 Ch!oromethane
cis-1,2-Dlchloroethene
cis-1,3-Dichloropropene Dichlorobromomethane
Ethylbenzene Methyl tert-butyl ether
Methylene Chloride 2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene Telrachloroethene
Toluene trans--1,2-Dich!oroethene trans-1,3-Dlchf oropropene Trichloroethene Trich!orofluoromethane
Vinyl chloride Xy!enes, Total 1, 2,4· Trichlorobenzene
lsobutyl alcohol
Surrogate 4-Bromofluorobenzene Dibromofluoromethane Toluene-dB (Surr)
<0.0034 <0.0034
<0.0011
<0.0034
<0.0045
<0.00098 <0.0011
<0.0034
<0.0013 <0.0034
0.036 <0.00092
<0.0034
<0.0034
0.015 <0.0023
<0.00071
<0.0034 <0.0034
<0.0034 <0.0014
<0.0010
<0.0016
<0.0034
<0.00084
<0.0014
<0.014
<0.0082
<0.0069
<0.0014 <0.0034
<0.0014 <0.0034
<0.0034
<0.0014 <0.0034
<0.0034 <0.0026
<0.0027
<0.014
%Recovery Qualifier 107
109
101
RL 0.0069 0.0069
0.0069
0.0069
0.0069 0.0069
0.0069
0.0069
0.0069 0.0069
0.0069 0.0069
0.034
0.0069
0.0069 0.0069
0.0069
0.0069
0.0069
0.0069 0.0069
0.0069
0.0069
0.0069
0.0069 0.0069
0.0069
0.0069
0.021
0.034
0.034
0.0069 0.0069
0.0069
0.0069
0.0069 0.0069
0.0069 0.0069
0.014 0.0069
0.034
Lfmlts 72-122
79-123
80-120
MDL Unit
0.0034 mg/Kg 0.0015 mg/Kg
0.0034 mg/Kg
0.0034 mg/Kg
0.0011 mg/Kg 0.0034 mg/Kg
0.0045 mg/Kg 0.00098 mg/Kg
0.0011 mg/Kg 0.0034 mg/Kg
0.0013 mg/Kg 0.0034 mg/Kg
0.010 mg/Kg
0.00092 mg/Kg
0.0034 mg/Kg 0.0034 mg/Kg
0.0034 mg/Kg
0.0023 mg/Kg
0.00071 mg/Kg
0.0034 mg/Kg
0.0034 mg/Kg
0.0034 mg/Kg
0.0014 mg/Kg
0.0010 mg/Kg 0.0016 mg/Kg
0.0034 mg/Kg
0.00084 mg/Kg
0.0014 mg/Kg
0.014 mg/Kg
0.0082 mg/Kg
0.0069 mg/Kg
0.0014 mg/Kg 0.0034 mg/Kg
0.0014 mg/Kg 0.0034 mg/Kg
0.0034 mg/Kg 0.0014 mg/Kg
0.0034 mg/Kg
0.0034 mg/Kg
0.0026 mg/Kg 0.0027 mg/Kg
0.014 mg/Kg
Page 52 of 140
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-5 Matrix: Solid
Percent Solids: 75.1
O Prepared Analyzed " 01119117 08:59 0111911717:13 ,, 01119117 08:59 0111911717:13
l.l 01119117 08:59 0111911717:13 ,, 01119117 08:59 01119117 17:13
" 01119117 08:59 01119117 17:13 ,, 01119117 08:59 0111911717:13
p 01119117 08:59 0111911717:13
,, 01119117 08:59 0111911717:13 l) 01119117 08:59 0111911717:13
,, 01119117 08:59 0111911717:13
u 01119117 08:59 0111911717:13
::: 01119117 08:59 0111911717:13
" 01119117 08:59 01119117 17:13
" 01119117 08:59 01119117 17:13
" 01119117 08:59 0111911717:13
" 01119117 08:59 01119117 17:13
" 01119117 08;59 01119117 17:13
u 01119117 08:59 0111911717:13
" 01119117 08:59 0111911717:13 n 01119117 08:59 01119117 17:13
" 01119117 08:59 01119117 17:13
" 01119117 08:59 0111911717:13 " 01119117 08:59 0111911717:13
" 01119117 08:59 01119117 17:13 n 01119117 08:59 01119117 17:13
" 01119117 08:59 0111911717:13
l) 01119117 08:59 0111911717:13
" 01119117 08:59 0111911717:13 ;) 01119117 08:S9 0111911717:13 ,, 01119117 08:59 0111911717:13
i:: 01119117 08:59 0111911717:13
0 01119117 08:59 0111911717:13 " 01119117 08:59 01119117 17:13
0 01119117 08:59 0111911717:13
,, 01119117 08:59 0111911717:13
ll 01119117 08:59 0111911717:13
" 01119117 08:59 0111911717:13 ,,, 01119117 08:59 0111911717:13
,, 01119117 08:59 0111911717:13
" 01119117 08:59 0111911717:13 " 01119117 08:59 0111911717:13 i:i 01119117 08:59 0111911717:13
Prepared Analyzed
0111911708;59 0111911717:13
01119117 08:59 0111911717:13
01119117 08:59 0111911717:13
Oil Fae
1
1
1
Dfl Fae 1
1
TestAmerica Pensacola
211/2017
Client Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol
Client Sample ID: CK-10 Date Collected: 01/13/1710:45 Date Received: 01/14/17 08:32
Method: 82700 -.Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene Acenaphthylene
Aniline Anthracene Benzo[a]anthracene
Benzofa]pyrene Be nzo{b ]flu ora nthe ne Benzofg,h,iJperylene Benzo[k]fluoranthene
1, 1 '-Biphenyl Bis(2-chloroethy!)ether bis (2-ch1oroisopropyl) ether Bis(2-ethylhexyl) phthalate
Butyl benzyl phthafate 4-Chloroaniline 2-Chloronaphtha!ene
2-Ch!orophenol
Chrysene Dibenz(a,h)anthracene
Dibenzofuran 3,3'-Dichlorobenzidine
2,4-Dich!orophenol Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate 1,3-Dlnitrobenzene 2,4-Dinitrophenol 2,4-Dinltrotoluene 2,6-Dinitroto!uene
Di-n-octyl phtha!ate
Fluoranthene Fluorene Hexachforobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene Hexach!oroethane lndeno[1,2,3-cd]pyrene
Jsophorone 2-Methylnaphthalene Naphthalene
2-Nitroaniline 3-Nitroanillne 4-Nitroaniline Nitrobenzene
4-Nitropheno! N-Nitrosodi-n-propyfamine N-Nitrosodiphenylamine Pentach!orophenol Phenanthrene
<0.043
<0.043
<0.055 <0.043
<0.043
0.058 J 0.076 J
<0.043 <0.043
<0.043 <0.043 <0.043
<0.043
<0.043 <0.043
<0.043
<0.043 <0.043
<0.043 <0.043
<0.043 <0.043
<0.043 <0.043
<0.043
<0.043
<0.37 <0.043 <0.043
<0.043
0.066 J <0.043
<0.13
<0.043
<0.085 <0.13
<0.043 <0.043 <0.043 <0.043 <0.043
<0.043
<0.043 <0.043
<0.14
<0.14
<0.043 <0.085 <0.043
0.43 0.43
0.43 0.43 0.43
0.43 0.43 0.43 0.43
0.43 0.43 0.43 0.43
0.43 0.43 0.43
0.43 0.43 0.43 0.43
0.43
0.43 0.43
0.43 0.43
0.43 1.3
0.43
0.43 0.43 0.43
0.43 0.43
0.43
0.43 0.43 0.43
0.43 0.43 0.43
0.43 0.43 0.43 0.43 0.43
0.43 0.43
0.85 0.43
Page 53 of 140
MDL Unit 0.043 mg/Kg 0.043 mg/Kg
0.055 mg/Kg
0.043 mg/Kg 0.043 mg/Kg
0.043 mg/Kg 0.043 mg/Kg
0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg
0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg
0.043 mg/Kg
0.043 mg/Kg 0.043 mg/Kg
0.043 mg/Kg
0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg
0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg
0.37 mg/Kg
0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg
0.043 mg/Kg 0.13 mg/Kg
0.043 mg/Kg 0.085 mg/Kg 0.13 mg/Kg
0.043 mg/Kg
0.043 mg/Kg
0.043 mg/Kg 0.043 mg/Kg
0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg 0.043 mg/Kg
0.14 mg/Kg 0.14 mg/Kg
0.043 mg/Kg 0.085 mg/Kg
0.043 mg/Kg
Tes!America Job ID: 400-132540-1
Lab Sample ID: 400-132650-5 Matrix: Solid
Percent Solids: 75,1
D Prepared Analyzed
" 01/18117 09:33 01/19/17 02:20 " 01118/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/19/17 02:20
" 01/18117 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/20/17 00:15
" 01/18/1709:33 01/20/17 00:15 01/18/17 09:33 01/20/17 00:15
" 01/18/17 09:33 01/20/17 00:15 ,, 01/18/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01/19/17 02:20 " 01/18/1709:33 01/19/1702:20 ,, 01/18117 09:33 01/19/17 02:20
" 01/18117 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/20/17 00:15
" 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/19/1702:20
" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/1709:33 01/19/17 02:20
,, 01/18/17 09:33 01/19/17 02:20
" 01118/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01/19/17 02:20 1:> 01/18/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,, 01/18/17 09:33 01/19/17 02:20
,, 01/18/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01/19117 02:20
" 01/18/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/20/17 00:15
" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01119117 02:20 " 01/18/17 09:33 01119/17 02:20 " 01/18/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20 ,,, 01/18/17 09:33 01/19/17 02:20
" 01118/17 09:33 01/19/17 02:20
" 01/18/17 09:33 01/19/17 02:20 " 01/18/17 09:33 01/19/17 02:20
DilFac E 1
1
1 1
1
Tes!America Pensacola
2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: CK-10 Lab Sample ID: 400-132650-5 Date Collected: 01/13/1710:45 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 75. 1
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Phenol <0.043 0.43 0.043 mg/Kg ,, 01/18/17 09:33 01/19/17 02:20 1
Pyrene 0.094 J 0.43 0.043 mg/Kg ,,, 01/18/17 09:33 01/19/17 02:20
1,2, 4, 5-T etrach!orobenzene <0.043 0.43 0.043 mg/Kg n 01/18/17 09:33 01119/17 02:20
2,3,4,6-T etrachlorophenol <0.043 0.43 0.043 mg/Kg " 01/18/17 09:33 01119117 02:20
1,2,4-Trichtorobenzene <0.043 0.43 0.043 mg/Kg 0 01/18117 09:33 01/19117 02:20
2,4,5-Trichlorophenol <0.043 0.43 0.043 mg/Kg <) 01/18117 09:33 01119/17 02:20
2,4,6-Trichlorophenol <0.043 0.43 0.043 mg/Kg ~ 01118117 09:33 01/19/17 02:20
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluorobipl1enyl 67 27 - 127 0111811709:33 01119117 02:20 1
2-Fluorophenol 76 25-128 01118117 09:33 01119117 02.·20
Nitrobenzene-d5 63 15-136 01118117 09:33 01119117 02:20
Phenol-d5 77 29-130 01118117 09:33 01119117 02:20 1
Teipheny/-d14 96 24-146 01118117 og:33 01119117 02:20
2, 4,6-Tribromopflenol 84 10-150 01118117 09:33 01119117 02:20
Method: MAVPH - Massachusetts -Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
C6-C8 AHphatics <11 11 11 mg/Kg " 01116117 11:30 01117117 04:15 50
CB-C 10 Atiphatics <18 18 18 mg/Kg -1:< 0111611711:30 01/17117 04:15 50
C8-C10 Aromatics <9.2 9.2 9.2 mg/Kg ,, 0111611711:30 01117117 04:15 50
surrogate %Recovery Quallfier Limits Prepared Analyzed Di/ Fae
a,a,a-Triffuorotoluene (fid) 113 70-130 01116117 11:30 01117117 04:15 50
a,a,a-Ttifluorotofuene (pid) 113 70-130 01116117 11:30 01117117 04:15 50
Method: 80816. Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Aldrin <0.0016 0.0045 0.0016 mg/Kg " 01118/17 12-.42 01119117 23:50 2
alpha-BHC <0.00063 0.0045 0.00063 mg/Kg " 0111811712:42 01119117 23:50 2
beta-BHC <0.0013 0.0045 0.0013 mg/Kg ,, 01118/17 12:42 01119/17 23:50 2
delta-BHC <0.00084 0.0045 0.00084 mg/Kg 0 01118117 12:42 01119/17 23:50 2
gamma-BHC (Lindane) <0.00058 0.0045 0.00058 mg/Kg " 01118117 12:42 01119117 23:50 2
alpha-Chlordane <0.00074 0.0045 0.00074 mg/Kg " 01/18/17 12:42 01119117 23:50 2
gamma-Chlordane 0.00078 J 0.0045 0.00071 mg/Kg '·' 01/1811712:42 01/19/17 23:50 2
4,4'-DDD 0.00055 J 0.0045 0.00050 mg/Kg " 01118117 12:42 01119117 23:50 2
4,4'-DDE <0,00071 0.0045 0.00071 mg/Kg ,, 01/1811712:42 01119117 23:50 2
4,4'-DDT <0.0020 0.0045 0.0020 mg/Kg ,, 01118/1712:42 01/19/17 23:50 2
Dieldrin <0.00095 0.0045 0.00095 mg/Kg i:i 0111811712:42 01119117 23:50 2
Endosulfan I <0.00055 0.0045 0.00055 mg/Kg " 01/18/1712:42 01119117 23:50 2
Endosulfan 11 <0.00061 0.0045 0.00061 mg/Kg " 01118/1712:42 01119117 23:50 2
Endosu!fan sulfate <0.00055 0.0045 0.00055 mg/Kg {l 01/18/1712:42 01119/17 23:50 2
Endrin <0.00050 0.0045 0.00050 mg/Kg :? 01118/1712:42 01/19/17 23:50 2
Endrin aldehyde <0.00076 0.0045 0.00076 mg/Kg " 01118117 12:42 01/19117 23:50 2
Endrin ketone <0.00092 0.0045 0.00092 rng/Kg " 01118/17 12:42 01119/17 23:50 2
Heptachlor <0.00063 0.0045 0.00063 mg/Kg 1:; 01/18117 12:42 01/19/17 23:50 2
Heptachlor epoxide <0.0012 0,0045 0.0012 mg/Kg 0 01118/17 12:42 01/19117 23:50 2
Methoxychtor <0.00087 0.0045 0.00087 mg/Kg p 01/18117 12:42 01/19117 23:50 2
Toxaphene <0.076 0.26 0.076 mg/Kg f.! 01/18117 12:42 01119117 23:50 2
TestAmerica Pensacola
Page 54 of 140 2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: CK-10 Lab Sample ID: 400-132650-5 Date Collected: 01113/1710:45 Matrix: Solid Date Received: 01114/17 08:32 Percent Solids: 75.1
Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae E DCB Decachlorobiphenyl 50 26-129 01118117 12:42 01119/17 23:50 2
Tetrachloro-m-xylene 45 31-122 0111811712:42 01119117 23:50 2
Method: MA-EPH. Massachu.setts ·Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
C10·C12 Aliphatics <2.1 2.1 2.1 mg/Kg " 01119117 07:20 01/24/17 20:47
C10-C12 Aromatics <2.1 2.1 2.1 mg/Kg i.' 01/19/17 07:20 01/25/17 00:55
C12-C16 Aliphatics <2.1 2.1 2.1 mg/Kg 0 01/19/1707:20 01/24/17 20:47
C12-C16 Aromatics <2.1 2.1 2.1 mg/Kg " 01/19/17 07:20 01/25/17 00:55
C16-C35 Aliphatics 10 2.1 2.1 mg/Kg "' 01/19/17 07:20 01/24117 20:47
C21 ·C35 Aro1natics 2.7 2.1 2.1 mg/Kg " 01/19/17 07:20 01/25/17 00:55
C16-C21 Aromatics <2.1 2.1 2.1 mg/Kg " 01/19/17 07:20 01/25/17 00:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
1-Chlorooctadecane 96 40-140 0111g/17 07:20 01124117 20:47 1
o~ Terphenyl 78 40-140 0111g117 07:20 01125117 00:55 1
Method: 6010C ·Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Silver <0.25 0.62 0.25 mg/Kg " 01/16/17 08:55 01/17/1713:26
Arsenic 2.5 1.2 0.50 mg/Kg o. 01/16/17 08:55 01/17/17 13:26
Barium 58 1.2 0.25 mg/Kg " 01/16/17 08:55 01/17/1713:26
Beryllium 0.20 J 0.37 0.12 mg/Kg " 01/16/17 08:55 01/17/17 13:26
Cobalt 3.4 1.2 0.37 mg/Kg " 01/16/1708:55 01/17/17 13:26
Chromium 6.1 1.2 0.25 mg/Kg " 01/16/17 08;55 01/17/17 13:26
Copper 10 2.5 0.25 mg/Kg " 01/16/17 08:55 01/17/1713:26
Nickel 6.6 0.62 0.37 mg/Kg " 01/16/17 08:55 01/17/17 13:26
Lead 39 1.2 0.25 mg/Kg " 01/16/17 08:55 01/17/17 13:26
Selenium <0.50 2.5 0.50 mg/Kg " 01/16/17 08:55 01/17/1713:26
Thallium <0.50 1.2 0.50 mg/Kg " 01/16/17 08:55 01/17/1713:26
Vanadium 7.5 2.5 0.37 mg/Kg " 01/16/17 08:55 01/17/17 13:26
Zinc 61 2.5 0.99 mg/Kg ,, 01/16/17 08:55 01/17/1713:26
Method: 7471A ·Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oii Fae
Mercury 0.041 0.013 0.0077 mg/Kg 01/15/1712:43 01/16/17 12:20 1
General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Chromium, hexavalent <3.4 F1 4.9 3.4 mg/Kg ,, 01/20/17 17:00 01/23/1712:07 1
Cyanide, Total <0.17 0.33 0.17 mg/Kg ,, 01/18/1710:53 01/18/1717:37 1
Percent Moisture 24.9 0.1 0.1 % 01117/1714:08
General Chemistry· Soluble Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Nitrate Nitrite as N <0.48 F1 1.3 0.48 mg/Kg " 01/16/17 12:30 1
TestAmerica Pensacola
Page 55 of 140 211/2017
Client Sample Results Client: C-K Associates Tes!America Job ID: 400-132540-1 ProjecUSite: Moffat & Nichol
Client Sample ID: RB-2 Lab Sample ID: 400-132650-6 Date Collected: 0111311711:00 Matrix: Water
Date Received: 01114117 08:32
Method: 8260C ·Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed OH Fae1, 1, 1.2-Tetrachloroethane <0.00052 0.0010 0.00052 mg/L 01/17/1716:13 11, 1, 1-Trichloroethane <0.00050 0.0010 0.00050 mg/l 01/17/17 16:13
1. 1 ,2,2-T etrach!oroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
1, 1,2-Trichloroethane <0.00050 0.0050 0.00050 mg/L 01/17/17 16:13
1, 1-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
1, 1-Dich!oroethene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
1,2,4-Trich!orobenzene <0.00082 0.0010 0.00082 mg/L 01/17/17 16:13
1, 2-Dibromo-3-Ch!oropropane <0.0015 0.0050 0.0015 mg/L 01/17/17 16:13
1,2-Dichlorobenzene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
1,2-Dich!oroethane <D.00050 0.0010 0.00050 mg/L 01/17/1716:13
1,2-Dich!oropropane <0.00050 0.0010 0.00050 mg/L 01/17/1716:13
1,3-0lchlorobenzene <0.00054 0.0010 0.00054 mg/L 01/17/1716:13
1.4-Dichlorobenzene <0.00064 0.0010 0.00064 mg/L 01/17/17 16:13
2-Butanone (MEK) <0.0026 0.025 0.0026 mg!L 01/17/17 16:13
4-Methyl-2-pentanone (MIBK) <0.0018 0.025 0.0018 mg/L 01/17/17 16:13
Acetone <0.010 0.025 0.010 mg/L 01/17/17 16:13
Benzene <0.00038 0.0010 0.00038 mg/L 01117/17 16:13
Bromoform <0.00071 0.0050 0.00071 mg/L 01/17/17 16:13
Bromomethane <0.0009B 0.0010 0.00098 mg/l 01117/17 16:13
Carbon disulfide <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
Carbon tetrachloride <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
Chlorobenzene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
Chlorodibromomethane <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
Ch!oroethane <0.00076 0.0010 0.00076 mg/L 01/17/17 16:13
Chloroform <0.00060 0.0010 0,00060 mg/L 01/17117 16:13
Ch1oromethane <0.00083 0.0010 0.00083 mg/L 01/17/17 16:13
cls-1,2-Dichloroethene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
ds-1,3-Dichloropropene <0.00050 0.0050 0.00050 mg/L 01/1711716:13
Dichlorobromomethane <0.00050 0.0010 0.00050 mg/L 01117/1716:13
Ethylbenzene <0.00050 0.0010 0.00050 mg/L 01/17/1716:13
lsobutyl alcohol <0.010 0.025 0.010 mg/L 01/17/17 16:13
Methyl tert-butyl ether <0.00074 0.0010 0.00074 mg/L 01/17/1716:13
Methylene Chloride 0.0066 0.0050 0.0030 mg/L 01/17/17 16:13
Styrene <0.0010 0.0010 0.0010 mg/L 01/17/17 16:13
T e!rach!oroethene <0.00058 0.0010 0.00058 mg/L 01/17117 16:13
Toluene <0.00070 0.0010 0.00070 mg/L 01/17/1716:13
trans-1,2-Dichloroethene <0.00050 0.0010 0.00050 mg/L 0111711716:13
trans-1,3-Dichloropropene <0.00050 0.0050 0.00050 mg/L 01/17/1716:13
Trichloroethene <0.00050 0.0010 0.00050 mg/L 01/17/17 16:13
Trich!orofluoromethane <0.00052 0.0010 0.00052 mg/L 01/17/17 16:13
Vinyl chloride <0.00050 0.0010 0.00050 mg/L 01/17/1716:13
Xylenes, Total <0.0016 0.010 0.0016 mg/L 01/17/17 16:13
Surrogate %Recovery Qua/Iner Lilnits Prepared Analyzed DI/ Fae
4-Bromotluoro_benzene 98 78-118 01117117 16:13 1
Dibromoffuoromethane 105 81-121 0111711716:13
Toluene-dB (Surr) 99 80-120 0111711716:13
Tes!America Pensacola
Page 56 of 140 2/1/2017
m
Client: C-K Associates ProjecVSite: Moffat & Nichol
Client Sample ID: RB-2 Date Collected: 0111311711:00 Date Received: 01/14/17 08:32
Client Sample Results
Method: 82700 LL. Semivolatlle Organic Compounds by GC/MS ·Low Level Analyte Result Qualifier RL MDL Unit Acenaphthene <0.000031 0.00019 0.000031 mg/l Acenaphthylene <0.000043 0.00019 0.000043 mg/L
Anthracene Benzo[a]anthracene Benzo[a]pyrene
Benzo[b]fluoranthene Benzo[k]fluoranthene
Chrysene Oibenz(a,h)anthracene
Fluoranthene Fluorene lndeno[1,2,3-cd]pyrene
2-Methylnaphtha!ene
Naphthalene Phenanthrene
Pyrene
Surrogate
2-F/uorobiphenyl Nitrobenzene-d5 Terphenyl-d14
<0.000031
<0.000044 <0.000040
<0.000033
<0.000096 <0.000071 <0.000048
<0.000065
<0.00011 <0.000041
<0.000058 <0.000090 <0.000035 <0.000038
%Recovery Qualifier 92
77
110
0.00019 0.000031 mg/L 0.00019 0.000044 mg/L 0.00019 0.000040 mg/L 0.00019 0.000033 mg/L
0.00019
0.00019 0.00019 0.00019
0.00019 0.00019
0.00019 0.00019 0.00019
0.00019
Limits 15-122
19-130
33-138
0.000096 mgfl
0.000071 mg/L 0.000048 mg/L 0.000065 mg/L
0.00011 mg/L 0.000041 mglL 0.000058 mg/L
0.000090 mg/L 0.000035 mg/L
0.000038 mg/L
Method: 82700 • Semivola!ile Organic Compounds (GC/MS) Analyte Result Qualifier RL Aniline <0.0037 6.0096
1, 1'-Biphenyl <0.00016 0.0096 Bis(2-chloroethyl)ether <0,0026 0.0096
Pis (2-ch!oro!sopropyl) ether Bis(2-ethythexyl) phthalate
Butyl benzyl phthalate 4-Ch!oroaniline 2-Chloronaphthalene
2-Chlorophenol Olbenzofuran 3,3'-Dichlorobenzidine
2,4-Dtchlorophenol Diethyl phtha!ate 2,4-Dimethylphenol Dimethyl phthalate
1,3-Dinitrobenzene 2,4-Dinitropheno! 2,4-Dlnitrotoluene
2,6-Dinitroto!uene Di-n-octyl phthalate Hexachlorobenzene Hexachlorobutadiene
Hexach!orocyclopentadlene Hexachloroethane lsophorone 2-Nitroanifine
<0.00015 <0.0019
<0.00018 <0.0033
<0.00013
<0.0021 <0.00016
<0.0025
<0.0029
<0.00023 <0.0034
<0.00016 <0.00096
<0.0033
<0.0018 <0.0018
<0.00016 <0.00016
<0.00053
<0.0025 <0.0040
<0.00013 <0.0021
0.0096
0.0096 0.0096 0.0096 0.0096
0.0096 0.0096 0.0096
0.0096 0.0096 0.0096 0.0096
0.0096 0.029
0.0096
0.0096 0.0096 0.0096 0.0096
0.019 0.0096
0.0096 0.0096
MDL Unit 0.0037 mg/L
0.00016 mg/L 0.0026 mg/L
0.00015 mg/L
0.0019 mg/L 0.00018 mg/L
0.0033 mg/L
0.00013 mg/L 0.0021 mg/L
0.00016 mg/L 0.0025 mg/L
0.0029 mg/L 0.00023 mglL
0.0034 mg/L 0.00016 mg/L
0.00096 mglL 0.0033 mg/L
0.0018 mg/L 0.0018 mg/L
0.00016 mg/L 0.00016 mg/L 0.00053 mg/L
0.0025 mg/L 0.0040 mg/L
0.00013 mg/L 0.0021 mg/L
Page 57 of 140
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-6 Matrix: Water
D Prepared Analyzed 01119/17 15:31 01124/17 16:27 01119/1715:31 01124117 16:27 0111911715:31 01124117 16:27
01119/1715:31 0112411716:27 0111911715:31 01124/1716:27
01119/1715:31 0112411716:27 01119/17 15:31 01124/17 16:27
01/19/17 15:31 0112411716:27 0111911715:31 01/24/17 16:27 01119/17 15:31 0112411716:27
01119/17 15:31 01124117 16:27 0111911715:31 01124117 16:27
01119/1715:31 01124117 16:27 01119117 15:31 01124117 16:27 01119/1715:31 01124/1716:27 01119/1715:31 01124117 16:27
Prepared
0111911715:31
0111911715:31
Analyzed
0112411716:27
0112411716:27
0111911715:31 0112411716:27
DllFac E 1
DH Fae
O Prepared Analyzed Oil Fae 0111911715:31 0112511710:06 01119/1715:31 0112511710:06 01119/1715:31 01125/1710:06
01119/1715:31 01125117 10:06 01119/1715:31 01125/1710:06
01119/1715:31 01125/17 .10:06 01119/1715:31 0112511710:06
01119/1715:31 0112511710:06
01119/1715:31 01/2511710:06 01/19/17 15:31 01125/1710:06
01119/17 15:31 01/25117 10:06
01119/1715:31 0112511710:06 0111911715:31 01125/1710:06 01119/1715:31 0112511710:06 0111911715:31 01/2511710:06
01119/1715:31 01125/1710:06 0111911715:31 01/2511710:06 01119/1715:31 01125/1710:06 01119/1715:31 0112511710:06
01119/1715:31 01125117 10:06 0111911715:31 01125/1710:06
01119/1715:31 01/25117 10:06
0111911715:31 01125117 10:06 0111911715:31 01125/1710:06 01119117 15;31 0112511710:06
01119/17 15:31 01125117 10:06
TestAmerica Pensacola
2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: RB-2 Date Collected: 01/13/1711:00 Date Received: 01 /14/17 08:32
Client Sample Results
Method: 8270D • Semivolatile Organic Compounds (GC/MSJ (Continued) Analyte Result Qualifier RL MDL Unit 3-Nftroaniline <0.0017 0.0096 0.0017 mg/L
4-Nitroanl!ine Nitrobenzene 4-Nitrophenol N-Nitrosodi-n-propy!amine N-Nitrosodiphenyramine Pentachlorophenot Phenol 1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trich!oropheno!
Surrogate 2-Fluorobiphenyl
2-Fluorophenol Nitrobenzene-dS
Pheno!-d5 Terphenyf-d14
2,4,6-Tribromophenol
<0.0014
<0.00013 <0.0020 <0.0032
<0.00017 <0.0013 <0.0025
<0.00017
<0.0015 <0.00017
<0.0036
<0.0034
%Recovery Qualifier
78 65 75
75 96
75
0.0096
0.0096 0.0096 0.0096
0.0096 0.019
0.0096 0,0096
0.0096 0.0096 0.0096
0.0096
Limits 46-124
13-113
36-126
17 -127
44-149
26-150
0.0014 mg/L
0.00013 mg/L
0.0020 mg/L 0.0032 mg/L
0.00017 mg/L 0.0013 mg/L
0.0025 mg/L 0.00017 mg/L 0.0015 mg/L
0.00017 mg/L 0.0036 mg/L
0.0034 mg/L
Method: 8270D - Semivolatile Organic Compounds (GCIMSJ • RERA Analyte Result Qualifier RL MDL Unit Aniline <0.0035 H Cl.0093 0.0035 mg/L
1,1'-Biphenyl <0.00016 H 0.0093 0.00016 mg/L Bis(2-chloroethyl)ether <0.0025 H 0.0093 0.0025 mg/L
bis (2-chloroisopropy!) ether
8is(2~ethylhexyl) phtha!ate Butyl benzyl phthalate 4-Chloroanmne 2-Ch!oronaphthalene 2-Chloropheno!
Dibenzofuran 3,3'-Dichlorobenzfdine 2,4-0ich!orophenol Diethyl phthalate 2.4-Dimethylphenol
Dimethyl phtha!ate 1,3-Dinitrobenzene 2,4-Dlnllrophenol
2,4-Dinitrototuene 2,6-Dinitrotoluene Di-n-octyl phthalate Hexach1orobenzene
Hexachlorobutadiene Hexach!orocyclopentadiene Hexachloroethane lsophorone
2-Nitroan!line
<0.00015 H
<0.0019 H <0.00018 H
<0.0031 H <0.00013 H
<0.0020 H <0.00016 H
<0.0024 H
<0.0028 H <0.00022 H
<0.0032 H
<0.00016 H <0.00093 H <0.0031 H'
<0.0018 H <0.0018 H
<0.00016 H
<0.00016 H <0.00051 H
<0.0024 H <0.0039 H
<0.00013 H <0.0020 H
0.0093
0.0093 0.0093
0.0093
0.0093 0.0093 0.0093
0.0093 0.0093 0.0093 0.0093
0.0093 0.0093 0.028
0.0093 0.0093 0.0093
0.0093
0.0093
0.019 0.0093 0.0093 0.0093
0.00015 mg/L
0.0019 rng/L 0.00018 mg/L
0.0031 mg/L
0.00013 mg/L
0.0020 mg/L 0.00016 mg/L
0.0024 mg/L
0.0028 mg/L 0.00022 rng/L
0.0032 mg/L 0.00016 mg/L
0.00093 mg/L 0.0031 mg/L 0.0018 mg/L 0.0018 mg/L
0.00016 mg/L 0.00016 mg/L
0.00051 mg/L
0.0024 mg/L 0.0039 mg/L
0.00013 mg/L
0.0020 mg/L
Page 58 of 140
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-6 Matrix: Water
D Prepared Analyzed OJI Fae E 01/19/1715:31 01/25/17 10:06
D
01/19/1715:31 01/25/1710:06
01/19/1715:31 01/25/1710:06 01/19/1715:31 01/25/1710:06 01/19/1715:31 01/2511710:06 01/1911715:31 01/25117 10:06
01/19/1715:31 01/25/17 10:06 01/19/17 15:31 01/25/17 10:06 01/1911715:31 01/25/1710:06
01/1911715:31 01125/1710:06 01119/1715:31 01/2511710:06 01/19/1715:31 01/25117 10:06
01/19/1715:31 01/25/1710:06
Prepared
0111911715:31
0111911715:31
Analyzed
01125117 10:06
0112511710:06
0111911715:31 0112511710:06
0111911715:31 0112511710:06
01119117 15:31 0112511710:06
0111911715:31 0112511710:06
Prepared 01/27/1711:20
01/27/1711:20
Analyzed 01/3111716:30
01/31/1716:30 01/27/1711:20 01/31/1716:30
01/27/1711:20 01/31/1716:30
01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/17 16:30
01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30
01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30
01127/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30 0112711711:20 01/31/17 16:30
01/27/1711:20 01/31/17 16:30 01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31117 16:30
01/27/1711:20 01/31/1716:30 01/2711711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30
01/27/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30
01127/1711:20 01/31/1716:30 01/27/1711:20 01/31/1716:30
01/27/1711:20 01/31/1716:30 01/27/1711:20 01/3111716:30
1
1
DI/ Fae
1
1
Oil Fae 1
1
1
1
1
1
TestAmerica Pensacola
2/1/2017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecUSite: Moffat & Nichol
Client Sample ID: RB-2 Lab Sample ID: 400-132650-6 Date Collected: 01/13/1711 :00 Matrix: Water Date Received: 01/14/17 08:32
Method: 8270D • Semivolatile Organic Compounds (GC/MS). RERA (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae 3-Nitroaniline <0.0017 H 0.0093 0.0017 mg/L 0112711711:20 01131/17 16:30 1
4-Nitroanjllne <0.0014 H 0.0093 0.0014 mg/L 0112711711:20 01131/17 16:30
Nitrobenzene <0.00012 H 0.0093 0,00012 mg IL 01127117 11:20 01131117 16:30
4-Nitrophenol <0.0019 H 0.0093 0.0019 mg IL 0112711711:20 01131117 16:30
N-Nitrosodi-n-propylamine <0.0031 H 0.0093 0.0031 mg/L 0112711711:20 01131117 16:30
N-Nitrosodfphenylamine <0.00017 H 0.0093 0.00017 mgll 0112711711:20 01131117 16:30
Pentach!orophenol <0.0013 H 0.019 0.0013 mg/L 01127117 11 :20 01131117 16:30
Phenol <0.0024 H 0.0093 0.0024 mg/L 01127/1711:20 01131117 16:30
1,2, 4 ,5-T etrach!orobenzene <0.00017 H 0.0093 0.00017 mg/L 0112711711:20 01131117 16:30
2,3 ,4, 6-T etrachlorophenol <0.0015 H 0.0093 0.0015 mg/L 01127/1711:20 01131117 16:30
1,2,4-Trichlorobenzene <0.00017 H 0.0093 0,00017 mg/L 01127/1711:20 01131117 16:30
2,4,5-Trich!oropheno! <0.0034 H 0.0093 0.0034 mg/L 01127/1711:20 0113111716:30
2,4,6-Trichloropheno! <0.0032 H 0.0093 0.0032 mg/L 01127/1711:20 01/31/17 16:30
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
2-Fluorobiphenyf 68 46- 124 0112711711:20 01131117 16:30 1
2-Fluorophenol 48 13-113 0112711711:20 0113111716:30 1
Nifrobenzene-d5 69 36-126 0112711711:20 0113111716:30
Phenol-d5 64 17-127 0112711711:20 01131117 16:30 1 Terpheny/-d14 87 44-149 0112711711:20 01131117 16:30 1
2,4,6-Tribromophenol 68 26-150 0112711711:20 0113111716:30
Method: MAVPH. Massachusetts - Volatile Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDI. Unit D Prepared Analyzed Oil Fae C6-C8 A!iphatics <0.030 0.030 0.030 mg IL 01/19117 23:24 1
C8-C10 Aliphatics <0.050 0.050 0.050 mgll 01/19117 23:24 C8-C10 Aromatics <0.025 0.025 0.025 mg/L 01/19/17 23:24
Surrogate %Recovery Qualifier Limits Prepared Analyzed DJ/ Fae a,a,a-Trifluorotoluene (fid) 101 70-130 01119117 23:24 1
a,a,a-Trifluoroto!uene (pid) 105 70-130 01119117 23:24
Method: 8011 • EDB, DBCP, and 1,2,3-TCP (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
1, 2-Dibromo-3-Chloropropane <0.0000056 0.000030 0.0000056 mg/L 01/2311716:25 01/27/17 00:38 1
Surrogate %Recovety Qualifier Limits Prepared Analyzed DJ/ Fae 4-Bromofluorobenzene 105 51-149 0112311716:25 01127117 00:38 1
Method: 80818 - Organochlorine Pesticides (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DllFae
Aldrin <0.0000011 0.000018 0.0000011 mg/L 01119/1710:03 01124117 13:06 1
alpha-BHC <0.0000013 0.000018 0.0000013 mg/L 01119/1710:03 01/24/17 13:06
beta-BHC <0.0000011 0.000018 0.0000011 mg IL 01/19/1710:03 01/24/17 13:06
de!ta-BHC <0.00000076 0.000018 0.0000007 mg/L 01/19/1710:03 01124/17 13:06
6 gamma-BHC (Undane) <0.0000091 0.000018 0.0000091 mg/L 01/19/1710:03 01/24117 13:06
alpha-Chlordane <0.0000015 0.000018 0.0000015 mg/L 01/19/1710:03 01/24/1713:06
gamma-Chlordane <0.0000012 0.000018 0.0000012 mg/L 01/1911710:0> 01124/1713:06
4.4'-DDD <0.0000011 0.000018 0.0000011 mg/L 01/19/1710:03 01/24/17 13:06
TestAmerica Pensacola
Page 59 of 140 2/112017
Client Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: RB-2 Lab Sample ID: 400-132650-6 Date Collected: 01/13/1711 :OO Matrix: Water Date Received: 01/14/17 08:32
Method: 8081 B - Organochlorine Pesticides (GC) (Continued) E Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
4,4'-DDE <0.00000080 0.000018 0.0000008 mg/L 01/19/1710:03 01/24/17 13:06 1 0
4,4'-DDT <0.0000014 0.000018 0.0000014 mg/L 01/19/17 10:03 01/24/1713:06
Dieldrin <0.0000011 0.000018 0.0000011 mg/L 01/19/1710:03 01/24/17 13:06
Endosulfan I <0.0000011 0.000018 0.0000011 mg/L 01/19/17 10:03 01/24/17 13:06
Endosu!fan II <0.0000027 0.000018 0.0000027 mg/L 01/19117 10:03 01/24/1713:06
Endosulfan sulfate <0.00000076 0.000018 0.0000007 mg/L 01/19/1710:03 01124/17 13:06 6
Endrln <0.0000011 0.000018 0.0000011 mg/L 0111911710:03 01/24/1713:06
Endrin aldehyde <0.0000010 0.000018 0.0000010 mg/L 01/19/1710:03 01/24117 13:06
Endrin ketone <0.0000014 0.000018 0.0000014 mg/L 01/19/17 10:03 01/24/1713:06
Heptachlor <0.0000011 0.000018 0.0000011 mg/L 01/19/17 10:03 01/24/1713:06
Heptach!or epoxlde <0.0000012 0.000018 0.0000012 mg/L 01/19/17 10:03 01/24/17 13:06
Methoxych!or <0.0000015 0.000018 0.0000015 mg/L 01/19/1710:03 01/24/1713:06
Toxaphene <0.00011 0.0011 0.00011 mg/L 01/19/1710:03 01/24/17 13:06
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
DCB Decachlorobiphenyl 48 10- 130 01119117 10:03 0112411713:06 1
Tetrachloro-m·xy/ene 64 43 .130 01119117 10:03 01124117 13:06
Meth.od: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae C10-C12 Aliphatrcs <0.048 0.048 0.048 mg/L 01/2011715:54 01/26/17 17:34 1
C12-C16 A!iphatics <0.048 0.048 0.048 mg/L 01/20/1715:54 01/26/17 17:34
C16-C35 Alip_hatics <0.048 0.048 0.048 mg/L 01/2011715:54 01/26/1717:34
C10-G12 Aromatics <0.048 0.048 0.048 mg/L 01120117 15:54 01/26/17 20:09
C12-C16 Aromatics <0.048 0.048 0.048 mg/L 01/20/17 15:54 01/26/17 20:09
C16-C21 Aromatics <0.048 0.048 0.048 mg/L 01/20/1715:54 01/26/17 20:09
C21-C35 Aromatics <0.048 0.048 0.048 mg/L 01/20/17 15:54 01/26/17 20:09
Surrogate %Recovery Qualifier Limits Prepared Analyzed Oil Fae
1~Chlorooctadecane 97 40-140 01120117 15:54 0112611717:34 1
o-Terphenyl 81 40-140 0112011715:54 01126117 20:09 1
2-Bromonaphthalene 20 40-140 01120117 15:54 01126117 20:09
2-Ffuorobiphenyl 60 40-140 01120117 15:54 01126117 20:09
Method: 6010C - Metals (ICP) Analyte Result Qualifier RL MDL Vnlt D Prepared Analyzed Oil Fae
Silver <0.0020 0.0050 0.0020 mg/L 01/18/17 10:09 01/19/1716:25 1
Arsenic <0.0040 0.010 0.0040 mg/L 01/18/1710:09 01/19117 16:25
Barium 0.0026 J 0.010 0.0020 mg/L 01/18/17 10:09 01/19/17 16:25
Beryllium <0.0010 0.0030 0.0010 mg/L 01/18/1710:09 01/19/17 16:25
Cobalt <0.0030 0.010 0.0030 mg/L 01/18/1710:09 01/19/17 16:25
Chromium <0.0020 0.010 0.0020 m9/L 01/18/1710:09 01/19/1716:25
Copper <0.0020 0.020 0.0020 mg/l 01/18/1710:09 01/19/17 16:25
Nickel <0.0030 0.0050 0.0030 mg/L 01/18/1710:09 01/19/17 16:25
Lead <0.0020 0.010 0.0020 mg/L 01/18/17 10:09 01/19/1716:25
Selenium <0.0040 0.020 0.0040 mg IL 01/18/17 10:09 01/19/1716:25
Tham um <0.0040 0.010 0.0040 mg/L 01/18/17 10:09 01/19/1716:25
Vaqadium <0.0030 0.020 0.0030 mg/L 01/18/17 10:09 01/19/17 16:25
Zinc 0.020 0.020 0.0080 m9/L 01/18/17 10:09 01/19/17 16:25
TestAmerica Pensacola
Page 60 of 140 21112017
Client: C-K Associates ProjecVSite: Moffat & Nichol
Method: 7470A ·Mercury (CVAA) Analyte Result
Mercury <0.000070
General Chemistry Analyte Result
Cyanide, Total <0.0035
Nitrate Nitrite as N <0.018
Chromium, hexava!ent <0.0065
Client Sample Results
Qual!fier RL MDL Unit 0.00020 0.000070 mg/L
Qualifier RL MDL Unit
0.0050 0.0035 mgll 0.050 O.D18 mg/L
0.010 0.0065 mg IL
Page 61 of 140
TestAmerica Job ID: 400-132540-1
D Prepared Analyzed Oii Fae 01116117 16:27 01118117 13:46 1
El D Prepared Analyzed Dllfac 01117/17 09:30 01117117 14:24 1
01116117 09:36
01114117 09:18
TestAmerica Pensacola
2/1/2017
Definitions/Glossary Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Qualifiers
GC/MSVOA Qualifier Qualifier Description
LCS or LCSD is outside acceptance limlts.
J Result is less than Jhe RL but greater than or equal to the fl.1DL and the concentration is an approximate value.
GC/MS Semi VOA Quallfler Qualifier Description
RPO of the LCS and LCSO exceeds the control limits
8 Compound wasJound in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value,
F1 MS and/or MSD Recovery is outside acceptance limits.
F2 MSJMSD RPO exceeds control limits
LCS or LCSD is outside acceptance limits.
H Sample was prepped or analyzed beyond the specified holding time
x Surrogate is outside control limits
GCSemiVOA Quallfler Qualifier Description
B Compound was found in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
LCS or LCSD is outside acceptance limits.
Metals Qualifier Quallfler Description
J Result is less 'than ·the RL but greater than or equal to the MDL and the concenfration is an approximate va!Ue.
F1 MS andior MSD Recovery is outside acceptance limits.
General Chemistry Qualifier Qual_lfier Description
F1 MS and/or t.1SD Recovery is outside acceptance Hmits.
F2 MS/MSD RPO exceeds control limits
J Result ls Jess than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
• Listed under the "D" column to designate that the result Is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Oil Fae Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re·analysis, Re·extraction, or additional lniUa! metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum dete'ctable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit {or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
Page 62of140
T estAmerica Pensacola
2/1/2017
Definitions/Glossary Client: C-K Associates ProjecVSite: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Glossary (Continued)
Abbreviation These commonly used abbreviations may or may not be present In this report.
RPO Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEO Toxicity Equivalent Quotient (Dioxin)
Page 63of140
TestAmerica Pensacola
2/1/2017
Surrogate Summary Client: C-K Associates Project/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: 8260C - Volatile Organic Compounds by GGIMS Matrix: Solid Prep Type: Total/NA
Lab Sample ID Client Sample ID 400-132588-1 CK-1 400-132588-2 CK-2
400-132588-3 Duplicate 400-132588-4 CK-3
400-132588-5 CK-4 400-132588-6 CK-5
400-132588-6 MS CK-5
400-132588-6 MSD CK-5 400-132650-1 CK-6 400-132650-2 CK-7
400-132650-3 CK-8 400-132650-4 CK-9
400-132650-5 CK-10
LCS 400-339082/15-A Lab Control Sample
LCS 400-33933012-A Lab Control Sample MB 400-339082/14-A Method Blank
MB 400-33933011-A Method Blank
Surrogate Legend BFB = 4·Bromofluorobenzene DBFf\1 = Dibromofluoromethane
TOL = Tofuene·d8 (Surr)
Percent Surrogate Recovery (Acceptance Limits}
BFB DBFM TOL (72-122) (79-123) (80-120)
100 102 94 100 103 91
102 104 94 99 102 94 104 102 94 98 95 104
100 98 104 98 102 101 104 96 111 112 97 106
101 102 95 117 93 112
107 109 101
97 104 104
93 105 97 95 100 105
96 100 93
Method: 8260C - Volatile Organic Compounds by GGIMS Matrix: Water Prep Type: Total/NA
Lab Sample ID 400-132540-1
400-132650-6
LCS 400-33852911002
LCS 400-33877111002
MB 400-33852914
MB 400-338771/4
Surrogate Legend
Cllent Sample ID RINSATE 1 RB-2
Lab Control Sample
Lab Control Sample
Method Blank Method Blank
BFB = 4·Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene..c.fB (Surr)
BFB
(78-118) 101
98
97
93
98
99
Percent Surrogate Recovery (Acceptance Lin1its)
DBFM TOL
(81-121) (B0-120) 103 102
105
108
104
104
103
99
98
95 99
100
Method: 82700 • Semivolatile Organic Compounds (GCIMS) Matrix: Solid Prep Type: Total/NA
Lab Sample ID 400~ 132588~ 1 400-132588-2
400-132588-3
Client Sample JD CK-1 CK-2
Duplicate
Percent Surrogate Recovery (Acceptance Limits)
FBP
(27-127) 92
49 71
2FP (25-128)
94 73
74
Page 64 of 140
NBZ PHL TPH TBP (15-136) (29-130) (24-146) (10-150)
82 89 109 122
77 75
82
81
78
96
85 93
TestAmerica Pensacola
21112017
Surrogate Summary Client: C-K Associates ProjecVSite: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued) Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
FSP 2FP NSZ
Lab Sample ID Client Sample ID (27-127} (25-128} (15-136}
400-132588-4 CK'3 75 80 67 400-132588-5 CK-4 52 71 56
400-132588-6 CK-5 58 72 57
400-132588-6 MS CK-5 77 78 68
400-132588-6 MSD CK-5 90 86 77 400-132650-1 CK-6 51 57 45 400-132650-2 CK-7 56 64 54 400-132650-3 CK-8 51 59 47 400-132650-4 CK-9 67 68 56 400-132650-5 CK-10 67 76 63
LCS 400-33855619-A Lab Control Sample 78 74 67
MB 400-338556110-A Method Blank 91 88 78
Surrogate Legend
FBP = 2-Fluorobiphenyl 2FP = 2-Fluorophenol
NBZ = Nitroben2ene-d5 PHL = Phenol-d5
TPH = Terphenyl-d14
TSP= 2,4,6-Tribromophenol
Method: 82700 - Semivolatile Organic Compounds (GCIMS) Matrix: Water
PHL TPH TSP
(29-130) (24-146) (10-150}
82 87 98
73 56 75
74 65 82
78 96 98
87 113 112
57 75 61
67 82 76
61 76 63
68 111 67
77 96 84
75 100 99
89 118 104
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits}
Lab Sample ID 400-132540-1
400-132650-6
400-132650-6 - RERA
LCS 400-33828412-A
LCS 400-33912512-A
LCS 400-34007912-A
LCSD 400-33828413-A
LCSD 400-33912513-A
LCSD 400-34007913-A
MB 400-33828411-A
MB 400-33912511-A
MB 400-34007911-A
Surrogaie Legend FBP = 2-Fluorobipheny! 2FP = 2-Fluorophenol NBZ = Nitrobenzene-d5 PHL = Phenol-dS TPH = Terphenyl-d14
Client Sample ID RINSATE 1
RB-2
RB-2
Lab Control Sample Lab Control Sample
Lab Control Sample Lab Control Sample Dup
Lab Control Sample Dup
Lab Control Sample Oup Method Blank Method Blank
Method Blank
TSP = 2,4,6-Tribromophenol
FBP
(46-124)
72
78
68
69
85
64 74
91
74
76
91
66
2FP
(13-113}
47
65
48
48
66
30
60
35
58
61
42
38
Page 65 of 140
NBZ PHL TPH TSP
(36-126} (17-127) (44-149) (26-150}
73 66 98 70
75 75 96 75
69 64 87 68
70 67 92 80
81 57 95 95
66 58 76 68
75 74 101 88
85 42 107 53
78 76 90 79
76 73 104 78
88 54 112 61
69 57 88 28
TestAmerica Pensacola
2/1/2017
Surrogate Summary Client: C-K Associates Project/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: 82700 LL - Semivolatile Organic Compounds by GCIMS ·Low Level Matrix: Water Prep Type: Total/NA
Lab Sample ID 400-132540-1
400-132650-6
LCS 400-33828412-A
LCS 400-33912512-A
LCSD 400-33828413-A
LCSD 400-339125/3-A
MB 400-338284/1-A
MB 400-33912511-A
surrogate Legend
FBP = 2~Fluorobiphenyl
NBZ ::::: Nitrobenzene-d5
TPH = Terphenyl-d14
Client Sample ID RINSATE 1
RB-2
Lab Control Sample Lab Control Sample
Lab Control Sample Oup Lab Control Sample Dup Method Blank
Method Blank
FBP
(15-122)
92
92
80
114
86
105
108
116
Percent surrogate Recovery (Acceptance Lln1lts)
NBZ TPH
(19-130) (33-138)
M 107
77 110 91
100
92
91
100
101
89
132
92
117 140 x 135
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Matrix: Solid Prep Type: Total/NA
Lab Sainple ID Client Sainple ID 400-132588-1 CK-1
400-132588-2 CK-2
400-132588-3 Duplicate 400-132588-4 CK-3
400-132588-5 CK-4
400-132588-6 CK-5
400-132588-6 MS CK-5
400-132588-6 MSD CK-5
400-132650-1 CK-6
400-132650-2 CK-7
400-132650-3 CK-8
400-132650-4 CK-9
400-132650-5 CK-10
LCS 400-33860412-A lab ContrQI Sample LCSD 400-33860413-A Lab Control Sample Oup
MB 400-338604/1-A Method Blank
Surrogate Legend
TFT = a,a,a-TrifJuoroto!uene (fid)
TFT2
(70-130)
77
74
79
76 75
79
79
94
79
72
83
93
113
107
100
75
Percent Surrogate Recovery (Acceptance Limits)
TFT1
(70-130)
80
75
79
77
75
81
79
93
78
74
86
92
113
109
101
76
Method: MAVPH • Massacliusetts. Volatile Petroleum Hydrocarbons (GC) Matrix: Water Prep Type: Total/NA
Lab Sample ID 400-132540-1
400-132650-6
LCS 400-33905713
LCSD 400-339057/4
Client Sample IP RINSATE 1
RB-2
Lab Control Sample Lab Control Sample Dup
TFT2
(70-130)
101
101
107
105
Percent Surrogate Recovery (Acceptance Limits)
TFT1
(70-130)
103
105
108
107
TestAmerica Pensacola
Page 66 of 140 2/112017
Surrogate Summary Client: C-K Associates ProjecVSite: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: MAVPH • Massachusetts ·Volatile Petroleum Hydrocarbons (GC) (Continued) Matrix: Water Prep Type: Total/NA
Lab sample ID MB 400:339657/2
Surrogate Legend
Client Sample ID Method Blank
TFT = a,a,a-Trifluorotoluene (fid)
TFT2
(70-130)
106
Method: 8011. EDB, DBCP, and 1,2,3-TCP (GC) Matrix: Waler
Lab Sample ID 400-132540-1
400-132650-6
LCS 400-339493/2-A
LCSD 400-339493/3-A
MB 400-339493/1-A
Surrogate Legend
Client Sample ID RINSATE 1
RB-2
Lab Control sample Lab Control Sample Dup Method Blank
BFB = 4-Bromofluorobenzene
BFB1
(51-149)
113
105
97
108
109
Method: 80818 • Organoch!orine Pesticides (GC) Matrix: Solid
Lab Sample ID Client Sample ID 400-132588-1 CK-1
400-132588-2 CK-2
400-132588-3 Duplicate 400-1325884 CK-3
400-132588-5 CK-4
400-132588-6 CK-5
400-132588-6 MS CK-5
400-132588-6 MSD CK-5
LCS 400-338557/9-A Lab Control Sample MB 400-338557/10-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl TCX = Tetrachloro-m-xylene
OCB1 (26-129)
53
46
62
48
41
62
81
67
86
99
Method: 8081 B • Organochlorine Pesticides (GC) Matrix: Solid
DCB2
Lab Sample 10 Client Sample ID (26-129)
400-132650-1 CK-6 45 400-132650-2 CK-7 44 400-132650-3 CK-8 58
Percent Surrogate Recovery (Acceptance Limits)
TFT1
(70-130)
106
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits} TCX1
(31-122)
46
44
52
42
41
62
83
68
85
95
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TCX2 (31-122)
41
49
52
TestAmerica Pensacola
Page 67 of 140 2/112017
Surrogate Summary Client C-K Associates Projecl/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: 80818 • Organochlorine Pesticides (GC) (Continued) Matrix: Solid Prep Type: Total/NA
Lab Sample ID 400:1:i2sso-4
400-132650-5
Surrogate Legend
Client Sample ID CK-9
CK-10
DCB = DCB Decachtorobiphenyl
TCX = Tetrachloro-m-xylene
DCB2
(26-129)
57
50
Method: 80818 • Organochlorine Pesticides (GC) Matrix: Water
Lab Sample ID Client Sample ID 400-132540-1 RINSATE 1
400-1326.50-6 RB-2
LCS 400-33823912-A Lab Control Sample LCS 400-33905412-A Lab Control Sample LCSD 400-33823913-A Lab Control Sample Oup LCSD 400-33905413-A Lab Control Sample Dup MB 400-33823911-A Method Blank MB 400-33905411 ·A Method Blank
Surrogate Legend
DCB == DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
DCB1
(10-130)
55
48
67
53
52
106
56
93
Percent Surrogate Recovery (Acceptance Limits)
TCX2
(31-122)
52
45
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TCX1
(43-130)
99
64
88
77
91
68
99
69
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
1COD1
Lab Sample ID Client Sample ID (40-140)
400-132588-1 CK-1 88
400-132588-2 CK-2 86
400-132588-3 Duplicate 1.0J 400-132588-4 CK-3 96
400-132588-5 CK-4 80
400-132588-6 CK-5 83
400-132588-6 MS CK-5 88 400-132588-6 MSD CK-5 82
400-132650-1 CK-6 98
400-132650-2 CK-7 86 400-132650-3 CK-8 85
400-132650-4 CK-9 86
400-132650-5 CK-10 96 LCS 400-339010114-A Lab Control Sample 98
LCSD 400-339010115-A Lab Control Sample Dup 106
MB 400.-339010116-A Method Blank 95
Surrogate Legend
TestAmerica Pensacola
Page 68 of 140 2/1/2017
Surrogate Summary Client: C-K Associates Project/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
1COD = 1-Ch!orooctadecane
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits) OTPH1
Lab Sample ID Cllent Sample ID (40-140)
400-132588-1 CK-1 66
400-132588-2 CK-2 79
400-132588-3 Duplicate 94
400-132588-4 CK-3 72
400-132588-5 CK-4 84
400-132588-6 CK-5 70
400-132588·6 MS CK-5 86
400-132588-6 MSD CK-5 99
400-132650-1 CK-6 98
400-132650-2 CK-7 81
400-132650-3 CK-8 78
400-132650-4 CK-9 74
400-132650-5 CK-10 78
LCS 400-339010/14-A Lab Control Sample 123
LCSD 400-339010/.15-A Lab Control Sample Oup 118
MB 400-339010/16-A Method Blank 83
Surrogate Legend
OTPH = o·Terphenyl
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Matrix: Water Prep Type: Total/NA
Percent surrogate Recovery (Acceptance Limits}
Lab Sample ID 400-132540-1
400-132650-6
LCS 400-339262/2-A
LCSD 400-339262/3-A
MB 400-33926211-A
Surrogate Legend
Client Sample ID RINSATE 1
RB-2
Lab Control Sample Lab Control Sample Dup Method Blank
1 COD = 1-Chlorooctadecane
1COD1
(40-140)
89
97
84
81
79
Method: MA~EPH - Massachusetts - Extractable Petro.leum Hydrocarbons (GC) Matrix: Waler Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits}
Lab Sample ID 400-132540-1
400-132650-6
LCS 400-339262/2-A
LCSD 400-339262/3-A
MB 400-339262/1-A
Surrogate Legend
Client Sample 10 RINSATE 1
RB-2
Lab Control San1ple Lab Control Sample Dup
Method Blank
OTPH1
(40-140)
63
81
85
83
73
2BN1 FBP1
(40-140) (40-140)
14 46
20 60
50 121
32 74
57 119
Page 69of140
TestAmerica Pensacola
2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
OTPH::: o-Terphenyl 2BN = 2-Bromonaphthalene FBP ::: 2-Fluorobipheny!
Surrogate Summary
Page 70 of 140
TestAmerica Job ID: 400-132540-1
TestAmerica Pensacola
2/1/2017
QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Method: S260C - Volatile Organic Compounds by GC/MS
Lab Sample ID: MB 400-338529/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis.Batch: 338529
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dll Fae
1, 1, 1,2-Tetrachloroethane <0.00052 0.0010 0.00052 mg/L 01116117 09:19 1 1, 1, 1 -Trichloroethane <0.00050 0.0010 0.00050 mg/L 01116117 09:19
1, 1,2,2-Tetrachloroethane <0.00050 0.0010 0.00050 mg/L 01116117 09:19
1, 1,2-Trichloroethane <D.00050 0.0050 0.00050 mgll 01116117 09:19 E 1, 1-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01116117 09:19
1, 1-Dich!oroethene <0.00050 0.0010 0.00050 mg/L 01116117 09:19
1,2-Dibron10-3-Ch!oropropane <0.0015 0.0050 0.0015 mg/L 01116117 09:19
1,2-0ich)orobenzene <0.00050 0.0010 0.00050 mg/L 01116117 09:19
1,2-Dichloroethane <0.00050 0.0010 0.00050 mg IL 01116117 09:19
1,2-Dich!oropropane <0.00050 0.0010 0.00050 mg IL 01116117 09:19
1,3-Dichlorobenzene <0.00054 0.0010 0.00054 mg/L 01116117 09:19
1.4-Dichlorobenzene <0.00064 0.0010 0.00064 mg/L 01116117 09:19
Acetone <0.010 0.025 0.010 mg IL 01116117 09:19
Benzene <0.00038 0.0010 0.00038 mg/L 01116117 09:19
Bromofonn <0.00071 0.0050 0.00071 mg/L 01116117 09:19
Bromomethane <0.00098 0.0010 0.00098 mg/L 01116117 09:19
Carbon disulfide <0.00050 0.0010 0.00050 mg IL 01116117 09:19
Carbon tetrachloride <0.00050 0.0010 0.00050 mgll 01116117 09:19
Chlorobenzene <0.00050 0.0010 0.00050 mg/L 01116117 09:19
Chlor.odib'romonlethane <0.00050 0.0010 0.00050 mg IL 01116117 09:19
Chloroethane <0.00076 0.0010 0.00076 mQIL 01116117 09:19
Chloroform <0.00060 0.0010 0.00060 mg/L 01116117 09:19
Chloromethane <0.00083 0.0010 0.00083 mg IL 01116117 09:19
cis· 1,2·Dichloroethene <0.00050 0.0010 0.00050 mg IL 01116117 09:19
Cis· 1, 3·Dich!oropropene <0.00050 0.0050 0.00050 mg IL 01116117 09:19
Dichlorobromomethane <0.00050 0.0010 0.00050 mg IL 01116/17 09:19
2-Butanone (MEK) <0.0026 0.025 0.0026 mgll 01116117 09:19
Ethylbenzene <0.00050 0.0010 0.00050 mg/L 01116117 09:19
4-Methyl-2-pentanone (MIBK) <0.0018 0.025 0.0018 mgll 01116117 09:19
Methyl tert·butyl ether <0.00074 0.0010 0.00074 mg/L 01116117 09:19
Methylene Ch.loride <0.0030 0.0050 0.0030 mg/L 01116117 09:19
Styrene <0.0010 0.0010 0.0010 mgll 01116117 09:19
Tetrach!oroethene <0.00058 0.0010 0.00.058 mg IL 01116117 09:19
Toluene <0.00070 0.0010 0.00070 mg IL 01116117 09:19
trans· 1,2·Dichloroethene <0.00050 0.0010 0.00050 mg IL 01116117 09:19
trans· 1,3·Dfchloropropene <0.00050 0.0050 0.00050 mg IL 01116117 09:19
Trichtoroethene <0.00050 0.0010 0.00050 mg/L 01116117 09:19
Trichlorofluoromethane <0.00052 0.0010 0.00052 mg IL 01116117 09:19
1,2,4·Trichtorobenzene <0.00082 0.0010 0.00082 mg/L 01116117 09:19
Vinyl chloride <0.00050 0.0010 0.00050 mg/L 01116117 09:19
lsobutyl alcohol <0.010 0.025 0.010 mg/L 01116117 09:19
Xylenes, Total <0.0016 0 . .010 0.0016 mg IL 01116/17 09:19
MB MB Surroga.te %Recovery Qualifier Limits Prepared Analyzed Dll Fae 4·Bromofluorobehzene 98 78-118 01116117 09:19 1
Dibromoffuoromethane 104 81-121 01116117 09:19 1
Toluene-dB (SutT) gg 80-120 01116117 09:19
TestAmerica Pensacola
Page71 of140 2/1/2017
Client: C-K Associates ProjecVSite: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 8260C ·Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCS 400·33852911002 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 338529
Spike LCS LCS %1Rec.
Analyte Added Result Qualifier Unit D 0/oRec Limits 1, 1, 1,2-Tetrachloroethane 0.0500 0.0516 mg/L 103 67 -131
1, 1, 1 -Trichloroethane 0.0500 0.0505 mg/L 101 68-130
1, 1,2,2-Tetrachloroethane 0.0500 0.0511 mg/L 102 70-131
1, 1,2-Trichloroethane 0.0500 0.0482 mg IL 96 70-130
1, 1-Dichloroethane 0.0500 0.0521 mg/L 104 70-130 1, 1-Dich!oroethene 0.0500 0.0603 mg/L 121 63-134
1,2-Dlbromo-3-Chloropropane 0.0500 0.0589 mg/L 118 54-135
1,2-Dichlorobenzene 0.0500 0.0479 mg IL 96 67 -130 1,2-Dich!oroethane 0.0500 0.0492 mg/L 98 69-130
1,2-Dichloropropane 0.0500 0.0468 mglL 94 70-130
1,3-Dichlorobenzene 0.0500 0.0467 mg/L 93 70-130
1,4-Dich!orobenzene 0.0500 0.0469 mg/L 94 70-130
Acetone 0.200 0.251 mg/L 125 43-160
Benzene 0.0500 0.0491 mglL 98 70- 130
Bromofonn 0.0500 0.0713 mg/L 143 57 -140 Bromomethane 0.0500 0.0496 mg/L 99 10-160
Carbon disulfide 0.0500 0.0562 mg IL 112 61 - 137
Carbon tetrachloride 0.0500 0.0580 mg/L 116 61 - 137
Ch!orobenzene 0.0500 0.0479 mg/L 96 70-130
Chlorodibromomethane 0.0500 0.0564 mg IL 113 67 -135
Chloroethane 0.0500 0.0522 mg/L 104 55-141
Ch!orofonn 0.0500 0.0507 mglL 101 69-130
Chloromethane 0.0500 0.0500 mglL 100 58-137
cis-1,2-Dichloroethene 0.0500 0.0513 mg/L 103 68-130
cis-1,3-Dichloropropene 0.0500 0.0475 mg IL 95 69-132
Dichlorobromomethane 0.0500 0.0511 mglL 102 67-133
2·Butanone (MEK) 0.200 0.203 mg IL 102 61-145
Ethylbenzene 0.0500 0.0480 mg/L 96 70-130
4-Methyl-2-pentanone (MIBK) 0.200 0.202 mglL 101 69-138 Methyl tert-butyl ether 0.0500 0.0497 mg/L 99 66-130
Methylene Chloride 0.0500 0.0532 mg/L 106 66-135
Styrene 0.0500 0.0445 mg IL 89 70-130
Tetrachloroethene 0.0500 0.0544 mg IL 109 65-130
Toluene 0.0500 0.0469 mg/L 94 70-130
trans-1,2-Dichloroethene 0.0500 0.0544 mg/L 109 70-130
trans-1,3-Dich!oroprppene 0.0500 0.0458 mg/L 92 63-130 Trichloroethene 0.0500 0.0519 mg IL 104 70-130
Trichlorofluoromethane 0.0500 0.0546 mg IL 109 65-138
1,2,4~Trichlorobenzene 0.0500 0.0492 mg/L 98 60-140
Vinyl chloride 0.0500 0.0538 mg/L 108 59-136 Xylenes, Total 0.100 0.0940 mg/L 94 70-130
LCS LCS Surrogate %Recovery Qualifier Limits
4-Bromonuorobenzene 97 78-118
Dibromoftuoromethane 108 81" 121 Toluene-dB (Surr) 98 80-120
TestAmerica Pensacola
Page 72 of 140 2/1/2017
E1
QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol
Method: 8260C ·Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: MB 400-338771/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 338771
MS MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
1, 1, 1,2-Tetrach!oroethane <0.00052 0.0010 0.00052 mg/L 01/17/17 15:21 1 1, 1, 1-Trichloroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21
1, 1,2,2-Tetrachloroethane <0.00050 0.0010 0.00050 mg/L 01/17/1715:21
1, 1,2-Trichloroethane <0.00050 0.0050 0.00050 mg/L 01/17/1715:21
E 1, 1-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21
1, 1-Dichloroethene <0.00050 0.0010 0.00050 rng/L 01/17/17 15:21
1,2-Dibromo-3-Ch!oropropane <0.0015 0.0050 0.0015 mg/L 01/17/17 15:21
1,2-Dichlorobenzene <0.00050 0.0010 0.00050 mg/L 01/17/1715:21
1,2-Dichloroethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21
1,2-Dichloropropane <0.00050 0.0010 0.00050 mg/L 01/17/1715:21
1,3-Dich!orobenzene <0.00054 0.0010 0.00054 mg/L 01/17/17 15:21
1,4-Dichlorobenzene <0.00064 0.0010 0.00064 mg/L 01/17/17 15:21
Acetone <0.010 0.025 0.010 mg/L 01/17/17 15:21
Benzene <0.00038 0.0010 0.00038 mg/L 01/17/17 15:21
Bromoform <0.00071 0.0050 0.00071 mg/L 01/17/17 15:21
Bromomethane <0.00098 0.0010 0.00098 mg/L 01/17/1715:21
Carbon disulfide <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21
Carbon tetrachloride <0.00050 0.0010 0.00050 mg/L 01/17/1715:21
Chlorobenzene <0.00050 0.0010 0.00050 mg/L 01/17/1715:21
Chlorodibromon1ethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21
Ch!oroethane <0.00076 0.0010 0.00076 mg/L 01/17/17 15:21
Chloroform <0.00060 0.0010 0.00060 mg/L 01/17/17 15:21
Chloromethane <0.00083 0.0010 0.00083 mg/L 01/17/17 15:21
cis-1 ,2-Dich!oroethene <0.00050 0.0010 0.00050 mg/L 01/17/1715:21
cis-1,3-Dichloropropene <0.00050 0.0050 0,00050 mg/L 01/17/17 15:21
Dichlorobromomethane <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21
2-Butanone (MEK) <0.0026 0.025 0.0026 mg/L 01/17/17 15:21
Ethylbenzene <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21
4-Methyl-2-pentanone (MIBK) <0.0018 0.025 0.0018 mg/L 01/1711715:21
Methyl tert-butyl ether <0.00074 0.0010 0.00074 mg/L 01/17/17 15:21
Methylene Chloride <0.0030 0.0050 0.0030 mg/L 01/17/17 15:21
_Styrene <0.0010 0.0010 0.0010 mg/L 01/17/17 15:21 Tetrachloroethene <0.00058 0.0010 0.00058 mg/L 01/17/1715:21
Toluene <0.00070 0.0010 0.00070 mg/L 01/17/1715:21
trans-1,2-Dichloroethene <0.00050 0.0010 0.00050 mg/L 01117/1715:21
trans-1,3-Dich loropropene <0.00050 0.0050 0.00050 mg/L 01/17/1715:21
Trichloroethene <0.00050 0.0010 0.00050 mg/L 01117/1715:21
Trichlorofluoro1nethane <0.00052 0.0010 0.00052 mg/L 01/17/1715:21
1,2,4-Trichlorobenzene <0.00082 0.0010 0.00082 mg/L 01/17/17 15:21
Vinyl chloride <0.00050 0.0010 0.00050 mg/L 01/17/17 15:21
lsobutyl alcohol <0.010 0.025 0.010 mg/L 01/17/1715:21
Xylenes, Total <0.0016 0.010 0.0016 mg/L 01/17/17 15:21
MB MB Surrogate %Recovery Qualifier Limits _Pre pa, red Analyzed DI/ Fae
4-Brotnofluorobenzene 99 78-118 0111711715:21 1
Dibromofluoro1nethane 103 81.121 0111711715:21
Toluene--d8 (Surr) 100 80-120 01117117 15:21
TestAmerica Pensacola
Page 73 of 140 2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: S260C ·Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCS 400-338771/1002 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 338771
Spike LCS LCS o/oRec. Analyte Added Result Qualifier Unit D 0/oRec Limits 1, 1, 1,2-Tetrachloroethane 0.0500 0.0475 mg/L 95 67 -131 1, 1, 1-Trichloroethane 0.0500 0.0506 mg/L 101 68 -130
1, 1,2,2-Tetrach!oroethane 0.0500 0.0407 n1g/L 81 70-131 1, 1,2-Trichloroethane 0.0500 0.0445 mg/L 89 70 -130
1, 1-Dich!oroethane 0.0500 0.0526 mg/L 105 70-130
1, 1-Dichforoethene 0.0500 0.0598 mg/L 120 63-134
1,2-Dibromo-3-Ch!oropropane 0.0500 0.0458 mgll 92 54-135
1,2-Dich!orobenzene 0.0500 0.0427 mg/L 85 67 -130 1,2-Dichloroethane 0.0500 0.0472 mg IL 94 69 -130
1,2-Dichloropropane 0.0500 0.0470 mg IL 94 70-130
1,3-Dich!orobenzene 0.0500 0.0439 mg IL 88 70-130
1,4-Dichlorobenzene 0.0500 0.0422 mg/L 84 70-130 Acetone 0.200 0.215 mg/L 108 43-160
Benzene 0.0500 0.0500 mg/L 100 70 -130
Bromofonn 0.0500 0.0578 mg/L 116 57 .140
Bromomethane 0.0500 0.0433 mg/L 87 10-160
Carbon disulfide 0.0500 0.0575 mg/L 115 61-137
Carbon tetrachloride 0.0500 0.0583 mg/L 117 61 -137
Ch!orobenzene 0.0500 0.0470 mg IL 94 70-130
Chlorodibromon1ethane 0.0500 0.0508 mg IL 102 67 -135
Chloroethane 0.0500 0.0519 mg/L 104 55-141
Chloroform 0.0500 0.0505 n1g/l 101 69 -130
Chloromethane 0.0500 0.0484 1ng/l 97 58-137
cis-1,2-0ichloroethene 0.0500 0.0502 mg/L 100 68-130
cis-1,3-Dichloropropene 0.0500 0.0467 mg IL 93 69-132
Dichlorobromomethane 0.0500 0.0494 mg/L 99 67 -133
2-Butanone (MEK) 0.200 0.184 mg/L 92 61-145
Ethyfbenzene 0.0500 0.0482 mglL 96 70.130
4-Methyl-2-pentanone (MIBK) 0.200 0.184 mg/L 92 69-138
Methyl tert-butyl ether 0.0500 0.0465 mg/L 93 66-130
Methylene Chloride 0.0500 0.0585 mg IL 117 66 -135
Styrene 0.0500 0.0441 mg/L 88 70-130
T etrachloroethene 0.0500 0.0565 mglL 113 65 -130
Toluene 0.0500 0,0465 mg/L 93 70 -130
trans-1,2-Dichloroethene 0.0500 0.0548 mg IL 110 70.130
trans-1,3-Dich!oropropene 0.0500 0.0425 mg/L 85 63-130 Trichloroethene 0.0500 0.0544 mg IL 109 70 .130
Trichlorofluoromethane 0.0500 0.0515 mg IL 103 65-138
1,2,4-Trichlorobenzene 0.0500 0.0443 mg/L 89 60 -140
Vinyl chloride 0.0500 0.0525 mg/L 105 59-136
Xylenes, Total 0.100 0.0934 mg/L 93 70-130
LCS LCS Surrogate %Recoyery Qualifier Limits 4~Bromofluorobenie,ne 93 78-118 Dibromofluoromethane 104 81- 121 Toluene-dB (Surr) 95 80-120
TestAmerica Pensacola
Page 74 of 140 2/1/2017
E
QC Sample Results Client: C-K Associates ProjecUSite: Moffat & Nichol
Method: S260C ·Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: MB 400·339082114-A Matrix: Solid Analysis Batch: 339083
Analyte
1, 1, 1,2-T etrach!oroethane 1, 1, 1-Trichloroethane
1, 1,2,2-Tetrach!oroethane 1, 1,2-Trichloroethane
1, 1-Dichloroethane 1, 1-Dlchloroethene
1,2-Dibromo-3-Chforopropane
1,2-Dichlorobenzene 1,2-Dichloroethane
1,2-Dichloropropane 1,3-Dichlorobenzene
1,4-D!chlorobenzene Acetone Benzene Bromofonn Bromomethane Carbon disulfide
Carbon tetrachloride
Chlorobenzene Chlorodibromomethane
Chloroethane
Chloroform Ch!oromet11ane
cis-1,2-Dich!oroethene c!s-1,3-Dichloropropene
Dichforobromomethane 2-Butanone (MEK)
Ethyfbenzene
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Methylene Chloride Styrene Tetrach!oroethene
Toluene trans-1,2-Dichloroethene
trans-1,3-Dichloropropene Trichloroethene Trichtorofluoromethane
1,2,4-Trichtorobenzene Vinyl chloride lsobutyl alcohol Xylenes, Total
Surrogate 4-Bromofluorobenzene
Dibromofluoromethane Toluene-dB (Surr)
MB MB Result Qualifier
<0.0025 <0.0011
<0.0025 <0.0025
<0.00083 <0.0025
<0.0033
<0.00071 <0.00082
<0.0025 <0.00095
<0.0025 <0.0073
<0.00067
<0.0025 <0.0025 <0.0025
<0.0017 <0.00052 <0.0025
<0.0025 <0.0025 <0.0010
<0,00076
<0.0012 <0.0025 <0.0060
<0.00061
<0.0050 <0.0010
<0,010
<0.0010 <0.0025
<0.0010 <0.0025
<0,0025 <0.0010 <0.0025
<0.0020 <0.0025
<0.010
<0.0019
MB MB %Recovery Qualifier
95 100
105
RL 0.0050 0.0050 0.0050 0.0050
0.0050 0.0050 0.0050
0.0050 0.0050 0.0050
0.0050
0.0050 0.025
0.0050 0.0050 0.0050
0.0050 0.0050
0.0050 0.0050 0.0050
0.0050 0.0050 0.0050
0.0050 0.0050 0.025
0.0050
0.025 0.0050
0.015 0.0050 0.0050
0.0050 0.0050
0.0050 0.0050
0.0050
0.0050 0.0050
0.025
0.010
Limits 72 .122
79-123 BO- 120
MDL Unit 0.0025 mg/Kg 0.0011 mg/Kg
0.0025 mg/Kg 0.0025 mg/Kg
0.00083 mg/Kg 0.0025 mg/Kg
0.0033 mg/Kg
0.00071 mg/Kg 0.00082 mg/Kg
0.0025 mg/Kg 0.00095 mg/Kg
0.0025 mg/Kg 0.0073 mg/Kg
0.00067 mg/Kg
0.0025 mg/Kg 0.0025 mg/Kg
0.0025 mg/Kg 0.0017 mg/Kg
0.00052 mg/Kg 0.0025 mg/Kg 0.0025 mg/Kg
0.0025 mg/Kg 0.0010 mg/Kg
0.00076 mg/Kg 0.0012 mg/Kg
0.0025 mg/Kg 0.0060 mg/Kg
0.00061 mg/Kg
0.0050 mg/Kg 0.0010 mg/Kg
0.010 mg/Kg
0.0010 mg/Kg 0.0025 mg/Kg
0.0010 mg/Kg
0.0025 mg/Kg
0.0025 mg/Kg 0.0010 mg/Kg
0.0025 mg/Kg 0.0020 mg/Kg 0.0025 mg/Kg
0.010 mg/Kg
0.0019 mg/Kg
Page 75 of 140
TestAmerica Job ID: 400-132540-1
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339082
D Prepared Analyzed 01/19/17 08:59 01/19/17 11:47 01/19/1708:59 01/19/1711:47
01/19/17 08:59 01/19/1711:47 01/19/17 08:59 01/19/17 11:47
01/19/17 08:59 01/19/17 11:47 01/19/17 08:59 01/19/1711:47
01/19/17 08:59 01/19/1711:47
01/19/17 08:59 01/19/1711:47 01/19/17 08:59 01/19/1711:47 01/19/1708:59 01119/1711:47
01/19/17 08:59 01/19/1711:47
01/19117 08:59 01/19/17 11:47 01/19/17 08:59 01/19/1711:47
01/19/1708:59 01/19/1711.:47 01/19117 08:59 01/19/1711:47 01/19/17 08:59 01/19/1711:47 01/19/17 08:59 01/19/1711:47
01/19/17 08:59 01/19/1711:47
01/19/17 08:59 01/19/1711:47 01/19/1708:59 01/19/1711:47
01/19/1708;59 01/19/1711:47
01/19/17 08:59 01/19/1711:47 01119117 08:59 01119/1711:47
01/19/17 08:59 01119/1711:47
01119/1708:59 01/19/1711:47 01119/17 08:59 01/1911711:47 01/19/17 08:59 01/19/1711:47 01/19/1708:59 01/19/1711:47
01/19/17 08:59 01/19/17 11:47 01/19/17 08:59 01/19/17 11:47
01/19117 08:59 01119/1711 :47
01/19/1708:59 01119/1711:47 01/19/17 08:59 01/1911711:47
01/19117.08:59 01119/1711:47 01/19/17 08:59 01119/1711:47
01/19117.08:59 01119/1711:47 01119117 08:59 01/1911711:47
01/19/1708:59 01/1911711:47 01/19117 08:59 01/19/1711:47
01/19/17 08:59 01/1911711:47 01/19/17 08:59 01119/17 11:47
01/19/1708;59 0111911711:47
Prepared Analyzed 0111911708.'59 0111911711:47
01119117 08:99 0111911711:47
01119117 08:59 0111911711:47
Oil Fae
1
DI! Fae 1 1
1
TestAmerica Pensacola
2/1/2017
Client: C-K Associates Project/Site Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 8260C ·Volatile Organic Compounds by GC/MS {Continued)
Lab Sample ID: LCS 400·339082115-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 339083 Prep Batch: 339082
Spike LCS LCS 0/oRec. Analyte Added Result Qualifier Unit D 0/oRec Limits 1, 1, 1,2-Tetrachloroethane 0.0500 0.0492 mg/Kg 96 65-130
1, 1, 1 -Tr!chloroethane 0.0500 0.0479 mg/Kg 96 63-130
1, 1,2,2-Tetrach!oroethane 0.0500 0.0500 mg/Kg 100 60-131
1, 1,2-Trichloroethane 0.0500 0.0489 mg/Kg 98 65-130
1, 1 -Dichloroethane 0.0500 0.0484 mg/Kg 97 59-130
1, 1 -Dich!oroethene 0.0500 0.0489 mg/Kg 98 55-137
1,2-Dibromo-3-Ch!oropropane 0.0500 0.0468 n1g/Kg 94 49 -130
1,2-Dichlorobenzene 0.0500 0.0495 mg/Kg 99 64 -130
1,2-Dichforoethane 0.0500 0.0472 mgl!<g 94 62-130
1,2-Dichloropropane 0.0500 0.0477 mg/Kg 95 64-130
1,3-Dichlorobenzene 0.0500 0.0467 mg/Kg 97 66-13.0
1,4-Dichlorobenzene 0.0500 0.0483 mg/Kg 97 65-130
Acetone 0.200 0.197 mg/Kg 98 46-160
Benzene 0.0500 0.0476 mg/Kg 95 65-130
Bromofonn 0.0500 0.0455 mg/Kg 91 52-136
Bromomethane 0.0500 0.0644 mg/Kg 129 12-160
Carbon disulfide 0.0500 0.0455 mg/Kg 91 46-141
Carbon tetrachloride 0.0500 0.0491 n1g/Kg 98 60-130
Ch!orobenzene 0.0500 0.0495 mg/Kg 99 70-130
Chlorodibromomethane 0.0500 0.0463 mg/Kg 97 58-132
Chloroethane 0.0500 0.0493 mg/Kg 99 55-134
Chforofonn 0.0500 0.0476 mg/Kg 95 62-130
Chloromethane 0.0500 0.0461 mg/Kg 92 49-136
cis-1,2-Dichloroethene 0.0500 0.0467 mg/Kg 93 53-135
cis· 1,3-Dich!oropropene 0.0500 0.0456 mg/Kg 91 61-130
Dichlorobromomethane 0.0500 0.0466 mg/Kg 93 61-130
2-Butanone (MEK) 0.200 0.200 mg/Kg 100 55-130
Ethylbenzene 0.0500 0.0494 mg/Kg 99 70-130
4-Methyl-2-pentanone (MIBK) 0.200 0.193 mg/Kg 96 56-130
Methyl tert-butyl ether 0.0500 0.0434 mg/Kg 87 63-130
Methylene Chloride 0.0500 0.0429 mg/Kg 86 57. 132
Styrene 0.0500 0.0490 mg/Kg 98 66-130
Tetrach!oroethene 0.0500 0.0461 mg/Kg 92 67 -130
Toluene 0.0500 0.0495 mg/Kg 99 70-130
trans-1,2-Dichloroethene 0.0500 0.0483 mg/Kg 97 58 .134
trans-1,3-Dichloropropene 0.0500 0.0452 mg/Kg 90 60-130
Trichloroethene 0.0500 0.0508 mg/Kg 102 65-130
TrichlorofJuoromethane 0.0500 0.0453 mg/Kg 91 61 -136
1,2,4-Trichlorobenzene 0.0500 0.0487 mg/Kg 97 56-138
Vlnyl chloride 0.0500 0.0472 mg/Kg 94 52-132
Xylenes, Total 0.100 0.0975 mg/Kg 97 70-130
LCS LCS Surrogate %Recovety Quallfler Limits 4-Bromonuorobenzene 97 72-122 Dibromonuoromethane 104 79-123 ToJuene-<.:18 (Surr) 104 80-120
TestAmerica Pensacola
Page 76 of 140 2/112017
E
Client: C-K Associates ProjecUSite: Moffat & Nichol
QC Sample Results
Method: 8260C - Volatile OrganicCompounds byGC/MS (Continued)
Lab Sample ID: 400-132588-6 MS Matrix: Solid Analysis Batch: 339083
Analyte
1, 1, 1,2-Tetrachloroethane 1, 1, 1-Trichloroethane
1, 1,2,2-Tetrachloroethane 1, 1 ,2-Trichloroethane
1, 1-Dich!oroethane 1, 1-Dlchloroethene 1,2-Dibromo-3-Chloropropane
1,2-Dich!orobenzene 1,2-Dichloroethane
- 1,2-Dichloropropane
1,3-Dichlorobenzene 1,4-Dichlorobenzene Acetone Benzene
Bromofonn Bromomet!iane Carbon disulfide Carbon tetrachloride
Chlorobenzene Ch!orodibromomethane
Chloroethane
Chloroform Ch!oromethane
_cis-1,2-Dichloroethene ds-1,3-Dichloropropene
Dichlorobron1omethane Ethylbenzene Methyl tert-butyl ether
Methylene Chloride 2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene Tetrachloroethene
Toluene trans-1,2-Dichloroethene
trans-1,3-Dichforopropene Trich!oroethene
Trichlorofluoron1ethane Vinyl chloride
Xy!enes. Total 1,2,4-Trichlorobenzene
surrogate 4-c:Bromonuorobenzene Dibromonuoron;etbane To/uene-d8 (Surr)
Sample San1ple
Result Qualifier
<0.21 <0.093 <0.21
<0.21
<0.070 <0.21 <0.28
<0.060 <0.069
<0.21 <0.080
<0.21 <0.61
<0.056 <0.21
<0.21
<0.21
<0.14
<0.044 <0.21
<0.21
<0.21 <0.084
<0.064 <0,10 <D.21
<0.051 <0.084 <0.84
<0.50 <0.42
<0.084 <0.21
0.62 <0.21 <0.21
<0,084
<0.21 <0.21
<0.16
<0.17
MS MS %1(ecov_ety Qu_allfler
100
98 104
Spike
Added 4.21 4.21 4.21
4.21
4.21 4.21
4.21
4.21 4.21
4.21 4.21
4.21 16.8 4.21
4.21 4.21
4.21 4.21
4.21 4.21 4.21
4.21
4.21 4.21 4.21
4.21 4.21 4.21
4.21 16.8
16.8
4.21 4.21
4.21 4.21
4.21 4.21 4.21
4.21 8.42 4.21
Limits
72-122 79-123 80-120
MS MS Result Quallfler
4J4 3.88
4.75 4.34
3.75 3.88 4.21
5.00 3.98
4.04
4.88
4.88 16.1 4.07
4.04 4.52
3.45 3.95
4.34 4.06
2.53
4.12 3.85 3.94 3.75
3:91 4.29 3.61
3.82 16.1
15.4 4.37 4.28
4.88 4.06
3.87 4.31
4.25
3.75 8.60 4.71
Page 77 of 140
Unit
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
n1g/Kg mg/Kg
mg/Kg
mg/Kg
n1g/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
TestAmerica Job ID: 400-132540-1
D ,,
Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 339082 0/oRec. Limits
37 -130 92 41-130
113 10-149
103 37 -130 89 41-130 92 39-138
100 14 -132 119 20-130
95 37-130 g6 39-130
116 22-130
116 21-130 96 10-160
97 38-131 96 24-136
107 10-160
82 29-141 94 36-134
103 37-130 97 32-132 60 36-139
98 39-130 92 35-136 94 32-135
89 34-130 93 37-130
102 35-130
86 34-132 91 36-132 96 19-139
92 21-144 104 31 -130 102 27 -147
101 42-130
96 40-134 92 31-130
103 34-144
101 41-143
89 35-136 102 35-130 112 10-141
TestAmerica Pensacola
21112017
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Method; 82GOC ·Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: 400-132588·6 MSD Matrix: Solid Analysis Batch: 339083
Analyte
1, 1, 1,2-T etrachloroethane 1, 1, 1 -Trichloroethane 1, 1,2,2-Tetrach!oroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethane 1, 1-Dich!oroethene 1,2-Dibromo-3-Ch!oropropane
1,2-Dichlorobenzene 1,2-Dich!oroethane
1,2-Dlchloropropane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Acetone Benzene
Bromofonn Bromomethane
Carbon disulfide Carbon tetrachloride
Chlorobenzene Ch!orodibromomethane Chloroethane
Chloroform Chloromethane cis-1,2-Dfchloroethene
cis-1,3-Dlchloropropene Dichlorobromomethane
Ethylbenzene Methyl tert-butyl ether Me1hylene Chloride 2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene Tetrach1oroethene
Toluene trans-1,2-Dich loroethene
trans-1, 3-Dich loropropene Trichloroethene Trichtorofluoromethane
Vinyl chloride Xy!enes, Total 1,2,4-Trichlorobenzene
Su"Qgate 47Brom_ofluorobenzene Dibromofluoromethane To/uene.<f8 (Surr)
Sample San1ple Result Qualifier
<0.21 <0.093 <0.21 <0.21
<0.070 <0.21
<0.28
<0.060
<0.069 <0.21
<0.080 <0.21 <0.61
<0.056
<0.21 <0.21
<0.21
<0.14
<0.044 <0.21
<0.21
<0.21
<0.084
<0.064 <0.10
<0.21 <0.051
<0.084 <0.84 <0.50
<0.42
<0.084 <0.21
0.62 <0.21 <0.21
<0.084
<0.21
<0.21 <0.16
<0.17
MSD MSD %Recovery Qualifier
98 102 101
Spike Added
4.21 4.21
4.21 4.21
4.21 4.21
4.21 4.21 4.21 4.21
4.21 4.21 16.8
4.21 4.21 4.21
4.21 4.21
4.21 4.21 4.21
4.21 4.21
4.21
4.21 4.21 4.21
4.21 4.21 16.8 16.8
4.21 4.21
4.21 4.21
4.21 4.21
4.21
4.21 8.42 4.21
Limits
72-122 79.123 80.120
MSD MSD Result Qualifier Unit
4.30 mg/Kg
4.23
4.63 4.34
3.99 4.44
4.17
4.82 4.31
4.29 4.62
4.70 17.3 4.33
3.98 4.71
3.76 4.23
4.34 4.00 2.57
4,36 4.25 4.23
4.07
4.16 4.30 3.94
4.18 17.2
16.6
4.38 425 4.78
4.41 3.87 4.42
4.43 4.10 8.64
4.52
mg/Kg mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
1ng/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
Page 78 of 140
TestAmerica Job ID: 400-132540-1
Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 339082 VoRec. RPO
D t'/oRec ~:t 102
Limits 37 .130
{I 100 41-130 ,, 110 10.149
;:r 103 37 .130
" 95 41-130 " 106 39.138 1:1 99 14-132
,, 115 20.130
l) 102 37.130
" 102 39-130 ,,, 110 22.130
,,, 112 21-130
" 103 10 .160 ,,, 103 38.131 ,,, 95 24 .136
" 112 10.160 a 89 29.141 1,1 100 36.134
1:r 103 37-130
" 95 32.132
" 61 36.139 ,, 104 39.130
" 101 35.136
" 101 32 .135
" 97 34.130 ,,, 99 37 .130
" 102 35.130 p 94 34.132
" 99 36.132 1) 102 19.139
" 99 21.144
" 104 31.130 ,,, 101 27 -147
" 99 42-130 " 105 40.134 ;) 92 31-130 ,, 105 34 .144
" 105 41-143
" 97 35.136
" 103 35-130 " 107 10 -141
RPO Limit 4 34 8 3
0 6
14
4
8
6 6
4
7 6
2 4
9 7
0 2
2
6 10
7
8 6 0
9
9 6
7 0
2 8
0 2 4
9 0 4
40
44
~! B 37
38
40 32
35
41
40 38 36
34 47 39
44
37 34
42 35 41
35 35
34
46 31
38 41
39
39 44 37
38
34 42
42 43 39 53
TestAmerica Pensacola
2/1/2017
Client: C-K Associates ProjecVSite: Moffat & Nichol
QC Sample Results
Method: 8260C • Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: MB 400·339330/1 ·A Matrix: Solid Analysis Batch: 339331
Analyte 1, 1, 1,2-Tetrachloroethane 1, 1, 1-Trichtoroethane
1, 1,2,2-Tetrachloroethane 1, 1,2-Trichloroethane
1, 1-Dichloroethane 1, 1-Dichloroethene 1,2-Dibromo-3-Chloropropane
1,2-Dichlorobenzene 1,2-Dichloroethane
1,2-Dich!oropropane
1,3-Dichlorobenzene 1,4-Dichlorobenzene Acetone Benzene
Brornoform Bromomethane Carbon disulfide
Carbon tetrachloride
Chlorobenzene Chlorodfbromomethane
Chloroethane Chloroform Ch1oromethane .cis-1,2-Dtchloroethene cis-1,3-Dichloropropene
Dichlorobromomethane 2-Butanone (MEK)
Ethylbenzene 4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Methylene Chloride
Styrene Tetrachloroethene Toluene trans· 1,2 -Dich!oroethene
trans· 1,3-Dichloropropene Ttichloroethene Trich!orofluoromethane 1,2,4-Trichlorobenzene Vinyl chloride lsobutyl alcohol
Xylenes, To~al
surrogate 4-Bromonuorobenzene Dibromofluoromet/1ane Toluene-dB (Surr)
MB MB Result Qualifier
<0.0025 <0.0011
<0.0025 <0.0025
<0.00083 <0.0025
<0.0033
<0.00071 <0.00082
<0.0025 <0.00095
<0.0025 <0.0073
<0.00067
<0.0025 <0.0025 <0.0025 <0.0017
<0.00052 <0.0025
<0.0025 <0.0025 <0.0010
<0.00076 <0.0012
<0.0025 <0.0060
<0.00061
<0.0050 <0.0010
<0.010
<0.0010 <0.0025
<0.0010 <0.0025
<0.0025 <0.0010
<0.0025
<0.0020
<0.0025 <0.010
<0.0019
MB MB %Recovery Qualifier
96
100 gJ
RL 0.0050 0.0050
0.0050
0.0050
0.0050 0.0050
0.0050
0.0050 0.0050
0.0050
0.0050
0.0050 0.025
0.0050 0.0050 0.0050 0.0050
0.0050
0.0050 0.0050 0.0050
0.0050 0.0050
0.0050 0.0050
0.0050 0.025
0.0050
0.025 0.0050
0.015
0.0050 0.0050 0,0050
0.0050
0.0050 0.0050
0.0050 0.0050 0.0050 0.025
0.010
Llmlts 72-122
7g_1z3
80-120
MDL Unit 0.0025 mg/Kg 0.0011 mg/Kg
0.0025 mg/Kg 0.0025 mg/Kg
0.00083 mg/Kg 0.0025 mg/Kg 0.0033 mg/Kg
0.00071 mg/Kg 0.00082 mg/Kg
0.0025 mg/Kg
0.00095 mg/Kg
0.0025 mg/Kg 0.0073 mg/Kg
0.00067 mg/Kg
0.0025 mg/Kg 0.0025 mg/Kg
0.0025 mg/Kg 0.0017 mg/Kg
0.00052 mg/Kg 0.0025 mg/Kg 0.0025 mg/Kg
0.0025 mg/Kg 0.0010 mg/Kg
0.00076 mg/Kg
0.0012 mg/Kg 0.0025 mg/Kg 0.0060 mg/Kg
0.00061 mg/Kg
0.0050 mg/Kg 0.0010 mg/Kg
0.010 mg/Kg 0.00.10 mg/Kg 0.0025 mg/Kg
0.0010 mg/Kg 0.0025 mg/Kg
0.0025 mg/Kg 0,0010 mg/Kg
0.0025 mg/Kg
0.0020 mg/Kg 0.0025 mg/Kg 0.010 mg/Kg
0.0019 mg/Kg
Page 79 of 140
TestAmerica Job ID: 400-132540-1
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339330
0 Prepared Analyzed Oil Fae 01122117 07:44 01122117 09;19 01122117 07:44 01/22117 09:19
01/22117 07:44 01122117 09:19 01/22117 07;44 01122/17 09:19
01/22117 07:44 01/22117 09;19 01122/17 07:44 01/22117 09:19
01122117 07:44 01/22/17 09:19
01122117 07:44 01122117 09:19 01/2211707:44 01/22117 09:19
01122117 07:44 01/22117 09:19 01/22117 07:44 01/22117 09:19
01/22117 07:44 01/22117 09:19 01/22117 07:44 01/22/17 09:19 01/22117 07:44 01/22/17 09:19
01122117 07:44 01/22/17 09:19 01122117 07:44 01/22/17 09:19
01122117 07:44 01/22117 09:19
01/22117 07:44 01122/17 09:19 01/22117 07:44 01122/17 09:19 01122117 07:44 01/22117 09:19
01122117 07:44 01/22117 09:19 01/22117 07:44 01/22117 09:19 01/22117 07:44 01/22117 09:19
01122117 07:44 01/22117 09:19 01/22117 07:44 01/22/17 09:19
01/22117 07:44 01122/17 09:19 01/22117 07:44 01122117 09:19 01/22/17 07:44 01122117 09:19
01/22117 07:44 01/22/17 09:19 01/22117 07:44 01/22117 09:19
01122117 07:44 01/22117 09:19
01122117 07:44 01/22117 09:19 01122117 07:44 01122/17 09:19 01/22117 07:44 01122/1709:19
01/22117 07:44 01122117 09:19
01/22117 07:44 01/22117 09:19 01/22117 07:44 01/22117 09:19
01/22117 07:44 01/22117 09:19 01122117 07:44 01/22117 09:19
01122117 07:44 01/22/17 09:19 01122117 07:44 01/22/17 09:19
01/22117 07:44 01/22117 09:19
Prepared Analyzed 01122117 07:44 01122117 09;19
01122117 07:44 01/22117 09:19
01122117 07:44 01122117 09:19
1
1
DI/ Fae 1 1
TestAmerica Pensacola
2/1/2017
E
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 8260C "Volatile Organic Compounds by GCIMS (Continued)
Lab Sample ID: LCS 400-33933012-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 339331 Prep Batch: 339330
Spike LCS LCS O/oRec.
Analyte Added Result Qualifier Unit D 0/oRec Limits
1, 1, 1,2-T etrachloroethane 0.0500 0.0495 mg/Kg 99 65 .130
1, 1, 1-Trichloroethane 0.0500 0.0496 mg/Kg 99 63-130
1, 1,2,2-Tetrachloroethane 0.0500 0.0481 mg/Kg 96 60-131
1, 1,2-Trichloroethane 0.0500 0.0470 mg/Kg 94 65-130
1, 1-Dichforoethane 0.0500 0.0502 mg/Kg 100 59-130
1, 1-Dichloroethene 0.0500 0.0509 n1g/Kg 102 55-137
1,2-Dibromo-3-Ch!oropropane 0.0500 0.0501 mg/Kg 100 49- 130
1,2-Dichlorobenzene 0.0500 0.0479 mg/Kg 96 64-130
1,2-0ichloroethane 0.0500 0.0503 mg/Kg 101 62-130
1,2-Dich!oropropane 0.0500 0.0487 mg/Kg 97 64.130
1,3-DichJorobenzene 0.0500 0.0488 mg/Kg 98 66-130
1,4-0lchlorobenzene 0.0500 0.0487 mg/Kg 97 65-130
Acetone 0.200 0.201 mg/Kg 100 48-160
Benzene 0.0500 0.0494 mg/Kg 99 65. 130
Bromofonn 0.0500 0.0493 mg/Kg 99 52-136
Bromomethane 0.0500 0.0587 mg/Kg 117 12 .160
Carbon disulfide 0,0500 0.0488 mg/Kg 98 46-141
Carbon tetrachloride 0.0500 0.0510 019/Kg 102 60-130
Chlorobenzene 0.0500 0.0489 mg/Kg 98 70-130
Chforodibromome~h~ne 0.0500 0.0504 mg/Kg 101 58-132
Chloroethane 0.0500 0.0533 mg/Kg 107 55 -134
Chloroform 0.0500 0.0497 mg/Kg 99 62-130
Chlorornethane 0.0500 0.0517 mg/Kg 103 49-136
cis-1,2-Dichloroethene 0.0500 0.0484 mg/Kg 97 53-135
cis-1,3-Dichf oropropene 0.0500 0.0490 mg/Kg 98 61 - 130
Oichlorobromomethane 0.0500 0.0505 mg/Kg 101 61-130
2-Butanone (MEK) 0.200 0.233 mg/Kg 116 55 .130
Ethylbenzene 0.0500 0.0484 mg/Kg 97 70-130
4-Methyl-2-pentanone (MIBK) 0.200 0.215 mg/Kg 107 58-130
Methyl tert-butyl ether 0.0500 0.0506 mg/Kg 101 63 .130
Methylene Chloride 0.0500 0.0537 mg/Kg 107 57 -132
Styrene 0.0500 0.0471 mg/Kg 94 68-130
Tetrachloroethene 0.0500 0.0524 mg/Kg 105 67 -130
Toluene 0.0500 0.0474 mg/Kg 95 70 .130
trans-1,2-Dichloroethene 0.0500 0.0533 mg/Kg 107 58-134
trans-1,3-Dichloropropene 0.0500 0.0476 mg/Kg 95 60-130
Trichloroethene 0.0500 0.0525 mg/Kg 105 65-130
Trichlorofluoromethane 0.0500 0.0506 mg/Kg 101 61-136
1,2,4-T richlorobenzene 0,0500 0.0528 mg/Kg 106 56-138
Vinyl chloride 0.0500 0.0529 mg/Kg 106 52-132
Xylenes, Total 0.100 0.0946 mg/Kg 95 70 .130
LCS LCS surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene 93 72-122 Dibromofluoromethane 105 79-123
Toluene-dB (Surr) 97 80-120
TestAmerica Pensacola
Page 80 of 140 2/1/2017
E
Client: C-K Associates ProjecVSite: Moffat & Nichol
QC Sample Results
Method: 82700 • Semivo!atile Organic Compounds (GC/MS)
Lab.Sample ID: MB 400-338284/1 ·A Matrix: Water Analysis Batch: 338574
Analyte
An Hine 1, 1 '-Bipheny! Bis(2-chloroethyl)ether bis (2~chloroisopropyl) ether Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate 4-Chtoroani!ine 2-Chloronaphthalene 2-Ch!orophenol Dlbenzofuran 3,3'-Dich!orobenzidine 2,4-Dichlorophenol Diethyl phthafate 2,4-Dimethylphenof Dimethyl phthalate 1,3~Dinitrobenzene
-2,4-Dinitropheno! 2,4-Dinitroto!uene 2,6-Dinllrotoluene Di-n-octyl phthalate Hexach!orobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane lsophorone 2-Nitroaniline ,3-Nitroanmne 4-Nitroanillne Nitrobenzene 4-Nitrophenol N-Nitrosodi.n-propylamine N~Nitrosodiphenylamine
PentilQhlorophenol
Phenol 1,2,4,5-Tetrachlorobenzene 2,3,4,6-Tetrachlorophenol 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2.4,6· Trichloropheno!
Surrogate 2-Fluoroblphenyl
2-Fluorophenol Nitrobenzene·df5 P/Jehol-d5 Terpheny/-d14
2,4,6-Tribromophenol
MB MB Result Qualifier
<0.0038 <0.00017 <0.0027
<0.00016 0.00598 J
<0.00019 <0.0034
<0.00014 <0.0022
<0.00017
<0.0026
<0.0030 0.000429 J <0.0035
<0.00017 <0.0010
<0.0034 <0.0019
<0.0019 0.000230 J <0.00017 <0.00055
<0.0026
<0.0042 <0.00014
<0.0022 <0.0018
<0.0015 <0.00013
<0.0021
<0.0033 <0.00018 <0.0014
<0.0026 <0.00018
<0.0016 <0.00018
<0.0037
<0.0035
MB MB %Recovery Qualifier
76 61
76
73
104
78
RL 0.010 0.010
0.010 0.010
0.010 0.010
0.010
0.010 0.010
0.010
0.010
0.010 0.010 0.010
0.010 0.010 0.030
0.010 0.010 0.010
0.010 0.010 0.020
0.010 0.010
0.010 0.010 0.010
0.010 0.010
0.010
0.010 0.020 0.010
0.010
0.010 0.010
0.010 0.010
Limits 46-124
13-113 36-126
17 -127
44-149
26-150
MDL Unit 0.0038 mg/L
0.00017 mg/L 0.0027 mg/L
0.00016 mg/L
0.0020 mg/L 0.00019 mg/L 0.0034 mg/L
0.00014 mg/L 0.0022 mg/L
0.00017 mgil
0.0026 mg/L
0.0030 mg/L 0.00024 mg/L
0.0035 mg/L 0.00017 mg/L
0.0010 mg/L
0.0034 mg/L 0.0019 mg/L
0.0019 mg/L 0.00017 mg/L 0.00017 mg/L
0.00055 mg/L 0.0026 mg/L
0.0042 mg/L 0.00014 rngil
0.0022 mg/L 0.0018 mg/L 0.0015 mg/L
0.00013 mg/L 0.0021 mg/L
0.0033 mg/L 0.00018 mg/L 0.0014 mg/L
0.0026 mg/L 0.00018 mg/L
0.0016 mg/L 0.00018 mg/L
0.0037 mg/L
0.0035 mg/L
Page 81 of 140
TestAmerica Job ID: 400-132540-1
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338284
O Pr_epared Analyzed 01/1211716:23 01/16/17 19:51 01/1211716:23 01/16/17 19:51
01/1211716:23 01/16/1719:51 01/1211716:23 01/16/1719:51
01/12117 16:23 01/16/17 19:51 01/1211716:23 01/16/1719:51
01/12117 16:23 01/16/1719:51
01/12117 16:23 01/16/1719:51 01/12/1716:23 01/16117 19:51
01/1211716:23 01/16/1719:51 01/1211716:23 01/16/17 19:51
01/1211716:23 01/16/1719:51 0111211716:23 01/16/17 19:51 01/1211716:23 01/16/1719:51
01/1211716:23 01/16/1719:51 01/1211716:23 01/16/1719:51
01/1211716:23 01/16/17 19:51 01/12117 16:23 01/16/17 19:51
01/12117 16:23 01/16/17 19:51 01/1211716:23 01/16/17 19:51
01/1211716:23 01/16/17 19:51 01/1211716:23 01/16/1719:51 01/1211716:23 01/16/1719:51
01/1211716:23 01/16/17 19:51 01/1211716:23 01/16/17 19:51
01/1211716:23 01/16/17 19:51 .01/1211716:23 01/16/17 19:51 01/1211716:23 01/16/17 19:51
01/1211716:23 01116117 19:51 0111211716:23 01116117 19:51
0111Z/1716:23 01116/1719:51
0111211716:23 01/1611719:51 01/1211716:23 01116/17 19:51 0111211716:23 01116117 19:51
0111211716:23 01116/17 19:51 0111211716:23 01116117 19:51 0111211716:23 01116117 19:51 .0111211716:23 01116117 19:51
0111211716:23 01116117 19:51
Prepared Analyzed 0111211716:23 0111611719:51
0111211716:23 01116117 19:51
0111211716:23 0111611719:51
0111211716:23 01116117 19:51
0111211716:23 0111611719:51
0111211716:23 01116117 19:51
Oil Fae 1
1
Dif Fae 1
TestAmerica Pensacola
2/1/2017
B
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 82700 • Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 400·338284/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 338574 Prep Batch: 338284
Spike LCS LCS il/nRec. Analyte Added Result Qualifier Unit D 0/oRec Limits
Aniline 0.120 0.0908 mg/L 76 10-150 Bis(2-chloroethyl)ether 0.120 0.0988 mg/L 82 55-130 bis (2-ch!oroisopropyl) ether 0.120 0.0961 mg IL 80 39-136 Bis(2-ethythexyl) phthalate 0.120 0.145 mg/L 121 62-139 Butyl benzyl phthatate 0.120 0.133 mg/L 111 59-145 4-Chloroaniline 0.120 0.0828 rng/L 69 10 -150 2-Chloronaphtha!ene 0.120 0.0989 mg/L 82 62-130 2-Chlorophenol 0.120 0.0894 mg/L 74 60-130 Dlbenzofuran 0.120 0.104 rng/L 87 69-130 2,4-Dich!orophenol 0.120 0.100 mg/L 84 50-130 Diethyl phthalate 0.120 0.109 rng/L 91 60-133 2,4-0imethylphenol 0.120 0.0845 rng/L 70 52-132 Dimethyl phthalate 0.120 0.104 rng/L 87 69-130 2,4-Dinitropheno! 0.240 0.0607 mg/L 25 15-150 2,4-Dinitrotoluene 0.120 0.110 mg/L 92 66-140 2,6-Dinltroto!uene 0.120 0.107 rng/L 89 70-130 Di-n-octyl phthalate 0.120 0.129 rng/L 108 57 -148 Hexach!orobenzene 0.120 0.104 mg/L 87 67-132
Hexachlorobutadiene 0.120 0.0943 mg/L 79 34 -150 Hexachlorocyclopentadiene 0.120 0.0447 rng/L 37 1 -150 Hexachloroethane 0.120 0.0937 rng/L 78 34-133 lsophorone 0.120 0.101 mg/L 84 60-130 2-Nitroani!ine 0.120 0.106 mg/L 88 30-130 3-Nitroaniline 0.120 0.0943 rng/L 79 10-150 4-Nitroaniline 0.120 0.107 rng/L 89 10-150 Nitrobenzene 0.120 0.0966 mg/L 81 55-130 4-Nitrophenol 0.240 0.148 mg/L 62 31-150 N-Nitrosodi-n-propylamine 0.120 0.100 rng/L 83 55-130 N-Nitrosodiphenylamine 0.119 0.0990 mg/L 83 36-150 Pentachlorophenol 0.240 0.143 mg/L 60 46-136 Phenol 0.120 0.0930 rng/L 77 34-137 1,2,4-Trichlorobenzene 0.120 0.0979 rng/L 82 57 -130 2,4 ,5-Trichlorophenol 0.120 0.101 mg/L 84 67 -130
2,4,6-Trichlorophenol 0.120 0.0997 mg/L 83 67 -130
LCS LCS Surrogate %Recovery Qualifier Limits
2-FJuorobipheny/ 69 46-124 2-Fluorophenol 48 13-113 Nifrobenzene-d5 70 36-126 Phenol-d5 67 17 -127 Terphenyl-d14 92 44-149 2,4,6-Tribromophenol 80 26-150
TestAmerica Pensacola
Page 82of140 2/1/2017
a
QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Method: 82700 - Semivolatile Organic Compotmds (GC/MS) (Continued)
Lab Sample ID: LCSD 400-338284/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 338574 Prep Batch: 338284
Spike LCSO LCSO 0/oRec. RPO Analyte Added Result Qualifier Unit 0 0/oRec Limits RPO Limit Aniline 0.120 0.102 mg/l 85 10-150 11 30 Bis(2-chloroethyl)ether 0.120 0.104 mg/L 87 55-130 5 30 bis (2-chloroisopropyl) ether 0.120 0.101 mg IL 84 39-136 5 30 Bis(2-ethylhexyl) phthalate 0.120 0.143 mg/L 119 62-139 30
E Butyl benzyl phthalate 0.120 0.146 mg IL 122 59-145 9 30 4-Chloroaniline 0.120 0.105 rng/l 87 10-150 23 30 2-Chloronaphtha!ene 0.120 0.108 mg/L 90 62-130 9 30 2-Chlorophenol 0.120 0.0970 mg/L 81 60-130 8 30 DibenzofUran 0.120 0.112 mgll 94 69-130 8 30 2,4-Dich!orophenol 0.120 0.108 mg/L 90 50-130 7 30 Diethyl phtha!ate 0.120 0.119 mg/L 99 60-133 9 30
2,4-0lmethylphenol 0.120 0.0900 rng/L 75 52-132 6 30 Dimethyl phtha!ate 0.120 0.114 mglL 95 69-130 9 30 2,4-Dinitrophenol 0.240 0.113 rng/L 47 15-150 60 30
2,4-Dinitroto!uene 0.120 0.122 mg/l 101 66-140 10 30 2,6-Dinitrotoluene 0.120 0.117 mg IL 97 70-130 9 30 Di-n-octyl phthalate 0.120 0.144 rng/L 120 57 -148 11 30
Hexachlorobenzene 0.120 0.112 n1g/L 93 67 -132 7 30
Hexachtorobutadiene 0.120 0.102 rng/L 85 34' 150 8 30 Hexachlorocyclopentadiene .0.120 0.0489 mg/L 41 1-150 9 30
Hexachloroethane 0.120 0.101 mgll 84 34-133 7 30 lsophorone 0.120 0.109 mg/L 91 60-130 8 30 2-Nitroaniline 0.120 0.115 mg/L 96 30-130 9 30
3-Nitroaniline 0.120 0.106 mg/L 89 10-150 12 30 4-Nitroaniline 0.120 0.115 mg IL 96 10-150 8 30 Nitrobenzene 0.120 0.103 mg/L 86 55-130 7 30 4-Nitrophenol 0.240 0.177 mg IL 74 31 -150 18 30 N-Nitrosodi-n-propylamine 0.120 0.105 mg/L 88 55-130 5 30 N-Nitrosodiphenylamine 0.119 0.108 mg IL 91 36-150 8 30 Pentachloropheno1 0.240 0.217 mg/L 90 46-136 41 30 Phenol 0.120 0.0994 mg/L 83 34-137 7 30
1,2,4-Trichlorobenzene 0.120 0.103 mg IL 86 57-130 5 30 2,4,5-Trichlorophenol 0.120 0.115 mg IL 96 67 -130 13 30
2.4 ,6-Trichloropheno! 0.120 0.108 mg IL 90 67" 130 8 30
LCSD LCSD Surrogate %Recovery Quallfler Llrnlrs 2-Ffuorobiphenyl 74 46-124 2-Ffuorophenol 60 13-113 Nitrobenzene-d5 75 36-126 Phenol-d5 74 17 -127 Terpl1enyf·d14 101 44-149 2,4,6-Tribromophenol 88 26-150
Tes!America Pensacola
Page 83 of 140 2/1/2017
Client: C-K Associates ProjecVSite: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 8270D - Semivolatile Organic Compotmds (GC/MS) (Continued)
Lab Sample ID: MB 400·338556110-A Matrix: Solid Analysis Batch: 338741
A_nalyte Acenaphthene Acenaphthylene
Aniline Anthracene Benzo[a]anthracene Benzo[a]pyrene
Benzo[b]f!uoranthene
Benzo[g,h.iJperylene Benzofk]fluoranthene
1,1'-Biphenyl
Bis(2-chloroethyl)ether
bis (2-ch!oroisopropyl) ether Bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
4-Chloroaniline 2-Chloronaphthalene
2-Ch!orophenof
Chrysene Dibenz(a.h)anthracene Dibenzofuran 3,3'-Dichlorobenzidine
2.4-Dichlorophenol Diethyl phthalate
2,4-Dimethylpheno! Dimethyl phthalate 1,3-0lnitrobenzene
2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitroto!uene Di-n-octyl phthalate
Fluoranthene
Fluorene Hexachlorobenzene
Hexachlorobutadiene Hexachlorocyclopentadiene
Hexachloroethane lndeno[1,2,3-cdJpyrene
lsophorone 2~Methylnaphthalene
Naphthalene 2~Nitroanmne
3-Nitroaniline 4-Njtroanifine Nitrobenzene 4-Nitrophenol
N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine
Pentachlorophenol
MB MB Result Qualifier <0.033 <0.033 <0.043
<0.033
<0.033 <0.033
<0.033
<0.033 <0.033
<0.033 <0.033
<0.033 <0.033
<0.033
<0.033 <0.033
<0.033 <0.033
<0.033 <0.033
<0.033
<0.033 <0.033
<0.033
<0.033
<0.033 <0.29
<0.033
<0.033 <0.033
<0.033 <0.033
<0.10
<0.033 <0.066
<0.10 <0.033
<0.033
<0.033 <0.033
<0.033 <0.033
<0.033 <0.033
<0.11
<0.11 <0.033 <0.066
RL 0.33 0.33 0.33 0.33
0.33 0.33 0.33
0.33 0.33 0.33
0.33
0.33 0.33 0.33 0.33 0.33
0.33 0.33
0.33 0.33 0.33
0.33 0.33 0.33
0.33 0.33 0.99
0.33 0.33 0.33
0.33 0.33 0.33
0.33 0.33
0.33 0.33
0.33
0.33 0.33 0.33
0.33 0.33 0.33
0.33 0.33 0.33 0.66
Page 84 of 140
MDL Unit 0.033 mg/Kg 0.033 mg/Kg 0.043 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg
0.29 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg
0.10 mg/Kg
0.033 mg/Kg 0.066 mg/Kg
0.10 mg/Kg 0.033 mg/Kg
0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg
0.033 mg/Kg
0.033 mg/Kg 0.033 mg/Kg 0.033 mg/Kg
0.11 mg/Kg 0.11 mg/Kg
0.033 mg/Kg 0.066 mg/Kg
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338556
D Prepared Analyzed 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/1711712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 0111711712:42 01/16/17 09:16 01/17/17 12:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/17 12:42 01/16/17 09:16 01/17/1712:42
01/16/17 og:16 01/17/1712:42
01116/17 09:16 01/17/1712:42 01/.16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/17 12:42
01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01117/1712.:42 01/16/17 09:16 01/1711712:42
01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/1709:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42 01/16/17 09:16 01/17/1712:42
Dllfac 1
1
1
TestAmerica Pensacola
2/112017
Client: C-K Associates ProjecVSite: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: S270D • Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 400-338556/10-A Matrix: Solid Analysis Batch: 338741
MB MB
Analyte Result Qualifier
Ptienanthrene <0.033 Phenol <0.033 Pyrene <0.033 1,2,4, 5~ T etrachlorobenzene <0.033
2, 3 ,4, 6-T etrach1orophenol <0.033 1,2,4-Trichlorobenzene <0.033 2,4,5-Trichlorophenol <0.033 2,4,6-Trichlorophenol <0.033
MB MB Surrogate %Recovery 2-FluOiobipheny/ 2-FluorophenoJ Nitrobenzene-d5 Phenol-d5 Terphenyl-d14
2,4,6-Tribromophenol
Lab Sample ID: LCS 400-338556/9-A Matrix: Solid Analysis Batch: 338741
Anatyte Acenaphthene Acenaphthylene Aniline
Anthracene Benzo[a]anthracene Benzofa]pyrene Benzo[b]fluoranthene Benz'o[g,h,i]perylene Benzo[k]fluoranthene Bi_s(2-chloroethyl_)ether bls (2-ch!oroisopropyl) ether Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate 4-Chloroanlline 2-Chloronaphthalene 2-Chlorophenol Chrysene Oibenz(a,h)anthracene
Dibenzofuran 2,4-Dlch!orophenol Diethyl phthalate 2.4-Dimethylphenol Dimethyl phthalate 2,4-Dlnitrophenol 2,4-Dinitrotoluene 2,6-Dinitroto!uene
91
88
78
89
118
104
Qualifier
Client Sample ID: Method Blanf{ Prep Type: Total/NA Prep Batch: 338556
RL MDL Unit D Prepared Analyzed Oil Fae 0.33 0.033 mg/Kg 01/16/17 09:16 01/17/1712:42 1 0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42 0.33 0.033 mg/Kg 01/16/17 09:16 01/17/1712:42
0.33 0.033 mg/Kg 01116/17 09:16 01/17/17 12:42
0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42 0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42
0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42
0.33 0.033 mg/Kg 01/16/17 09:16 01/17/17 12:42
Limits Prepared Analyzed Dlf Fae
27-127 01/16117 09:16 0111711712:42 1
25-128 01116117 og:16 0111711712:42 1
15-136 01116117 09:16 0111711712:42
29 •. 130 0111611709:16 0111711712:42 1 24.146 01116117 09:16 0111711712:42 1
10-150 01116117 09:16 0111711712:42 1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338556
Spike LCS LCS o/oRec. Added Result Qualifier Unit D o/oRec Limits
1.99 1.54 mg/Kg 78 50-130
1.99 1.56 mg/Kg 78 50-130 1.99 1.22 mg/Kg 61 34.130
1.99 1.62 mg/Kg 81 50 .130
1.99 1.75 mg/Kg BB 50-130 1.99 1.60 mg/Kg 81 50-130 1.99 1.60 mg/Kg 81 50-130
1.99 1.84 mg/Kg 92 50 .132
1.99 1.57 mg/Kg 79 50 .130
1.99 1.36 mg/Kg 68 37 -130 .1.99 1.28 mg/Kg 64 14-149
1.99 1.86 mg/Kg 93 62-140 1.9.9 1.73 mg/Kg 87 57 .139
1.99 1.28 mg/Kg 64 29-130 1.99 1.47 mg/Kg 74 60-130
1.99 1.37 mg/Kg 69 57-130 1.99 1.74 mg/Kg 88 50-130 1.99 1.72 mg/Kg 87 43-133
1.99 1.56 mg/Kg 78 37 .137
1.99 1.61 mg/Kg 81 56-130 1.99 1.32 mg/Kg 66 63.130
1.99 1.44 mg/Kg 72 43-130
1.99 1.58 mg/Kg 79 65.130
3.98 1.84 mg/Kg 46 10.130
1.99 1.65 n1g/Kg 83 56.130
1.99 1.56 mg/Kg 79 65-130
TestAmerica Pensacola
Page 85 of 140 2/112017
El
QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Method: 82700 - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 400-338556/9-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 338741 Prep Batch: 338556
Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits bi-n-ociyl phthalate 1.99 1.81 mg/Kg 91 57 -140 Fluoranthene 1.99 1.70 mg/Kg 85 50-130 Fluorene 1.99 1.62 mg/Kg 82 50-130 Hexachlorobenzene 1.99 1.71 mg/Kg 86 44-136 a Hexachlorobutadiene 1.99 1.49 mg/Kg 75 44-130 Hexachlorocyclopentadiene 1.99 1.50 mg/Kg 76 1-150
Hexachloroethane 1.99 1.22 mg/Kg 61 44-130
lndeno[1,.213-cd]pyrene 1.99 1.75 mg/Kg 88 43-131 lsophorone 1.99 1.41 mg/Kg 71 48-130 '2-Methylnaphtha1ene 1.99 1.58 mg/Kg 79 50-130
Naphtha.Jene 1.99 1.39 mg/Kg 70 45-130
2-NitroaniUne 1.99 1.43 mg/Kg 72 46-133 3-Nitroanmne 1.99 1:29 mg/Kg 65 10-150 4-Nitroanillne 1.99 1.29 mg/Kg 65 10-150 Nitrobenzene 1.99 1.31 mg/Kg 66 49-130 4-Nitrophenaf 3.98 2.78 mg/Kg 70 10-150 N-Nitrosodi-n-propylam!ne 1.99 1.28 mg/Kg 64 44-130 N-Nitrosodiphenylamine 1.97 1.48 mg/Kg 75 49-148
Pentachlorophenol 3.98 2.90 mg/Kg 73 10-150 Phenanthrene 1.99 1.60 mg/Kg 80 5-130
Phenol 1.99 1.36 n1g/Kg 68 43-130 Pyrene 1.99 1.84 mg/Kg 92 47 -135
1,2,4M T rlchlor_obenzene 1.99 1..47 mg/Kg 74 50-112 2,4,5-TrichlorophenoJ 1.99 1.7.6 mg/Kg 88 51 -130 2,4 ,6~ Trichlorophenol 1.99 1.78 mg/Kg 90 57 -130
LCS LCS
Surrogate %Recovery Qua/If/er Limits 2MF1Uoroblphenyl 78 27-127 2-Fluorophenol 74 25-128 Nitrobenzene-d5 67 15-136 ·Phenol-<15 75 29-130 Terpheny/,d14 100 24-146 2,4;6-Tribromopheno/ 99 10-150
Lab Sample ID: 400-132588-6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA
· Analysis Batch: 338741 Prep Batch: 338556 Sample sample Spike MS MS 0/oRec.
Analyte Result Qualifier Added Result Qualifier Unit D o/aRec Limits
Acenaphthene <0.066 3.99 3.16 mg/Kg ·l:f- 79 40-140
Acenaphthylene <0.066 3.99 3.19 mg/Kg i) 80 40-140 Aniline <0.086 3.99 2.51 mg/Kg " 63 40-140
Anthracene <0.066 3.99 3.21 n1g/Kg 1:( 81 40-140
Benzo[a]anthracene 0.084 J 3.99 3.40 mg/Kg ·i:i 83 40-140
Benzo[a)pyrene 0.11 J 3.99 3.20 mg/Kg " 77 40-140 Ben.io[b]fluoranthene 0.26 J 3.99 3.45 mg/Kg " 80 40-140 Benzo[g,h,iJperylene <0.066 3.99 2.28 mg/Kg ·>:i 57 40-140 Benzo[k]fluoranthene <0,066 3.99 3.50 mg/Kg i) 88 40-140
TestAmerica Pensacola
Page 86of140 2/1/2017
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued)
Lab Sample ID: 400-132588-6 MS Matrix: Solid Analysis Batch: 338741
Analyte Bis(2°-Chf6'i6.ettiyl)'e.tlier bls (2-ch!oroisopropyl) ether Bis(2-ethylhexyl) phthalate Butyl benzyl phthalate 4-Ch!oroanlline 2-Chloronaphtha!ene 2-Chloropheno! Chrysene Dibenz_(a,h)anthracene Dibenzofuran 2,4-Pichlorophenol Diethyl phthalate 2,4-Dimethylphenol Dimethyl phthalate 2,4-Dinitropheno! 2,4-Dinitroto/uene 2,6-Dinitrotoluene Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene HexaChlorobutS:diene Hexi;ichlo_ro<;yclopentadiene Hexachloroethane lndenof1 ,2,3.-cd}pyrene
Jsophorone 2-Methylnaphthalene Naphthalene 2-Nitroaniline 3-Nitroanmne 4-N!troaniline Nitrobenzene 4-Nitrophen·ol N-Nitrosodi-n-propylamlne N-Nit~osodiphenylamine
Pentachloropheno.1 Phenanthrene Phenol Pyrene 112,4-Trichlorobenzene 2,4 ,5· Trlchlorophenol 2,4,6-Trichlorophenol
Surrogate ·2~FiiiO'TObtP6eny1
2-Fluo'rophe.hol NitroQenzene-dS Phenol-d5
Sample Sample Result Qualifier <0.066
<0.066 <0.066
<0.066
<0.066
<0.066
<0.066
0.13 J
<0.066 <0.066
<0.066
<0.066 <0.066
<0.066
<0.58 F2 F1
<0.066
<0.066
<0.066
0.27 J
<0.066
<0.20
<0.066
<0.13 F1
<0.20
<0.066
<0.066 <0.066
<0.066
<0.066
<0.066 <0.066
<0.066
<0.22 <0.22
<0.066
<0.13 <0.066
<0.066
0.23 J
<0.066
<0.066
<0.066
MS MS %Recovery Qualifier
77 78 68
78
Spike Added
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3 .. 99
7.97
3.99 3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3.99
3,99
7.97 3,99
3.95 7,97
3.99 3.99
3.99
3.99 3.99
3.99
Li mils 27.127 25.128
15.136
29-130
MS MS Result Qualifier Unit
2.99 mg/Kg
2.75
3.77
3.52
2.59
3.03
3.02
3.45
2.54
3.13
3.47
2.71
3.17
3.35
2.92 F1
3.32 3.19
3.56
3.37
3.27
3.31
2.99
0.741 F1 2.10
2.46
3.05
3.28
2.90
3.10
2.68
2.59
2.82 5.89
2.79
2.99
6.02
3.20 3.04
3.74
3.00 3.65
3.83
mg/Kg mg/Kg
mg/Kg
mg/Kg mg/Kg
mg/Kg
mg/Kg
mg/Kg mg/Kg
mg/Kg
mg/Kg mg/Kg
mg/Kg
mg/Kg
mg/Kg n1g/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg mg/Kg
nig/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg mg/Kg
mg/Kg
Page 87 of 140
Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338556
D o/oRec 1::i 75
O/oRec.
Limits
40-140
69 40-140
95 40-140
88 40.140
65 40-140 76 40.140
76 40-140
83 40-140
64 40-140
79 40-140
87 40-140
68 40-140
79 40-140
84 40.140
37 40-140
83 40-140 80 40.140
89 40.140
78 40-140 82 40.140
83 40-140
75 40-140
19 40-140
53 40-140 62 40.140
76 40.140
82 40-140 73 40.140
78 40.140
67 40-140
65 40-140
71 40.140
74 40-140
70 40-140
76 40.140
76 40-140
80 40-140 76 40.140
88 40.140
75 40-140 92 40.140
96 40-140
TestAmerica Pensacola
2/1/2017
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: 82700 • Semivolatile Organic Compounds (GCIMS) (Continued)
Lab Sample ID: 400-132588-6 MS Matrix: Solid Analysis Batch: 338741
Surrogate Terphenyl-d14 2,4,6-Tribromophenol
MS MS %Recovery Qualifier
g5
g8
Lab Sample ID: 40.0-132588-6 MSD Matrix: So.lid Analysis Batch: 338741
Analyte Acenaphthene
Acenaphthy/ene Aniline Anthracene Benzo[a]anthracene
Benzo[a]pyrene Benzo[b]fluoranthene. Benzo[g,h,i]perylene
Benzo[k]fluoranthene Bis(2-chloroethyl)ether
bis (2-chlorolsopropyl) ether Bis(2-ethylhexyl) phthalate
Butyl benzyl Pht.ha!ate 4-Chloroaniline
2-Chio'ronaphthalene 2-Ch!oropheno!
Chrysene Dibenz(a,h)anthracene Dibenzofuran 2,4-Dlchtorophenol Diethyl phthalate 2,4-Dimethylphenol
Dimethyl phthalate 2,4-0initrophenol 2,4-0initrotoluene
2,6-0initroto!uene Di-n-octyl phthalate Fluoranthene Fluorene
Hexachlorobenzene
Hexachlorobutadiene Hexachlorocyclopentadiene Hexach!oroethane
lndeno[1,2,3·cd]pyrene
lsophorone 2-Methylnaphthalene'
Naphthalene
2-Nitroaniline 3-Nitroanillne 4-NitroanHine
sample sample
Result Qualifier
<0.066 <0.066
<0.086 <0.066 0.084 J
0.11 J
0.26 J <0.066
<0.066 <0.066 <0.066 <0.066
<0.066 <0.066
<0.066 <0.066
0.13 J <0.066
<0.066 <0.066 <0.066
<0.066
<0.066 <0.58 F2 F1
<0.066
<0.066 <0,066
0.27 J <0.066
<0.20
<0.066 <0.13 F1
<0.20 <0.066 <0.066 <0.066
<0.066 <0.066 <0.066 <0.066
Lf1nits 24-146
10-150
Spike
Added 4.08
4.08 4.0.8 4.08 4.08
4.08
4.08 4.08
4.08 4.08 4.08
4.08
4.08 4.08
4.08
4.08
4.08 4.08
4.08 4.08 4.08
4.08
4.08
8.16 4.08 4.08 4.08
4.08 4.08
4.08
4.08 4.08
4.08
4.08 4.08
4.08
4.08
4.08 4.08 4.08
MSD MSD
Result 3.33
3.36 2.47
3.42 3.75 3.54
3.71 2.71 3.83
2.94
2.77 3.96
3.68 2.64 3.17
3.00 3.74 2.93
3.31
3.53
2.78 3.17
3.43
Qualifier Unit
4.14 F2 3.47
3.31
3.73 3.77
3.45 3:53
3.14 0.823 F1
2.07
2.86 3.04
3.41
2.9g 3.13 2.73
2.66
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
n1g/Kg mg/Kg
mg/Kg
mg/Kg
mg/l<;g
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
n1g/Kg mg/Kg
Page 88 of 140
Client Sample JD: CK-5 Prep Type: Total/NA Prep Batch: 338556
Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338556 °lo Rec. RPO
D %Rec
" 82
" 82
Limits 40-140
40 -140 60 40-140 84 40-140
90 40-140 84 40-140
85 40-140 66 40.140
94 40-140 72 40-140 68 40-140
97 40-140
90 40-140 65 40-140
78 40-140
74 40-140 3g 40-140
72 40-140
81 40-140 86 40-140 68 40-140 78 40-140
84 40-140
51 40-140 85 40-140
81 40-140 91 40.140 86 40-140 85 40.140
86 40-140
77 40-140 20 40-140 51 40 .140
70 40-140 75 40-140 84 40.140
73 40.140
77 40-140 67 40-140 65 40.140
RPO 5
5 2 6
10 10
7
17 g
2
1
5
5 2
5
8
14 5
2
3
0
2
35 4
4
5 11
5
6 5
10
1
15 0 4
3
2
3
Limit 30
30
30 30 30
30 30 30 30
30 30
30 30 30 30
30 30 30
30 30 30 30
30
30 30 30
30 30
30
30
30 30 30
30 30 30 30
30 30
30
TestAmerica Pensacola
21112017
Client: C-K Associates Projecl/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: ll270D - Semivo!atile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 400-132588-6 MSD Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338556
Matrix: Solid Analysis Batch: 338741
Analyte Nitrobenzene 4-Nitrophenol N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene
Phenol
Pyrene 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4 ,6-Trichlorophenol
Surrogate 2-Fluorobiphenyl 2-Fluorophenof Nitrobenzene-d5 Phenol-d5 Terphenyl-d14 2, 4,6-Tribromophenol
sample Sample
Result Qualifier
<0.066 <0.22
<0.22
<0.066 <0.13
<0.066
<0.066
0.23 J <0.066 <0.066
<0.066
MSD MSD
%Recovery Qualifier 90 86 77
87 113
112
Lab Sample ID: MB 400-339125/1-A Matrix: Water Analysis Batch: 339188
Analyte Aniline 1, 1'-Siphenyl Bis(2-chloroethyl)ether bis (2-ch!oroisopropyl) ether
Bis(2-ethylhexyl) phthalate _Butyl benzyl phthalate 4-Chlqroanl!ine
2-Ch!oronaphthalene
2-Chlorophenol Dibenzofuran 3,3'-Dich!orobenzidlne 2,4-Dich1orophenol
Diethyl phthalate 2,4-Dimethylphenol Dimethyl phthalate 1,3-Dinitrobenzene 2,4-Dinitrophenol
2.4-Dinitrotoluene 2,6-Dinltroto!uene
Di-n-octyl phthalate Hexachloroi;>enzene
Hexachlorobutadiene Hexachlorocyclopentadiene
MB MB Result Qualifier
<0.00095 <0.000043 <0.00068
<0.000040
0.0123 <0.000048
<0.00085
<0.000035
<0.00055 <0.000043 <0.00065 <0.00075
0.00009.32 J <0.00088
<0.000043
<0.00025 <D.00085
<0.00048
<0.00048
0.000574 J <0.000043
<0.00014 <0.00065
Spike
Added
4.08 8.16 4.08
4.05
8.16 4.08
4.08 4.08
4.08 4.08 4.08
Limits
27 .127
25-128 15-136 2g.130
24-146 10-150
RL 0.0025
0.0025 0.0025 0.0025
0.0025
0.0025 0.0025
0.0025
0.0025 0.0025 0.0025 0.0025
0.0025 0.0025 0.0025 0.0025 0.0075
0.0025 0.0025
0.0025 0.0025
0.0025 0.0050
MSD MSD
Result Qualifier Unit 2.86 mg/Kg 6.11
2.78 3.12 6.38 3.42 3.01
4.22 3.13 3.75 3.90
MDL Unit
0.00095 mg/L
0.000043 mg/L 0.00068 mg/L
0.000040 mg/L
0.00050 mg/L
0.000048 fl1QIL 0.00085 mg/L
0.000035 mg/L
0.00055 mg/L
0.000043 mg/L 0.00065 mgll
0.00075 mg/L
0.000060 mg/L 0.00088 mg/L
0.000043 mg/L
0.00025 mg/L 0.00085 mg/L 0.00048 mg/L 0.00048 mg/L
0.000043 mg/L 0.000043 mglL 0.00014 mg/L
0.00065 mg/L
mg/Kg mg/Kg
mg/Kg
mg/Kg mg/Kg
mg/Kg mg/Kg
mg/Kg mg/Kg
mg/Kg
Page 89 of 140
%Rec. RPO
D %Rec
" 7o Limits RPO Linllt 40-140 1 30
75 40.140 4 30 68 40-140
77 40-140
78 40-140 84 40.140
74 40-140
98 40-140 77 40-140 92 40-140 96 40.140
0
4
6 7
12
4
3
2
30 30
30 ~ 30 ll;Jll 30 30
30 30 30
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339125
O Prepared Analyzed 01119/17 15:31 01120117 15:57
0111911715:31 0112011715:57 01/19/17 15:31 01120117 15:57
0111911715:31 01120117 15:57 01119/17 15:31 0112011715:57
01/1911715:31 01/2011715:57 01/19117 15:31 0112011715:57
011.1911715:31 0112011715:57 01/19/1715:31 01120/17 15:57
01119/1715:31 01/20/1715:57 0111911715:31 01/20117 15:57
01/1911715:31 01/20117 15:57 0111911715:31 01120117 15:57 01/19/17 15:31 01120/17 15:57 01/19/1715:31 0112011715:57
01/19/1715:31 01120117 15:57 01119/1715:31 01120117 15:57 01/1911715:31 01/2011715:57
01/1911715:31 01120117 15:57 01/19/17 15:31 01120117 15:57 0111911715:31 0112011715:57 01/19/1715:31 01120/1715:57
0111911715:31 01120117 15:57
011 Fae 1
Tes!America Pensacola
2/112017
Client: C-K Associates ProjecUSite: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 82700 - Semivolatile Organic Compounds (GCIMS) (Continued)
Lab Sample ID: MB 400-339125/1-A Client Sample ID; Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 339188 Prep Batch: 339125
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Hexachloroethane <0.0011 0.0025 0.0011 mg IL 01/19/1715:31 0112011715:57 1
lsophorone <0.000035 0.0025 0.000035 mg IL 01119/1715:31 0112011715:57
2-N!troaniline <0.00055 0.0025 0.00055 mg/L 01/19/1715:31 01120/17 15:57
3-Nitroanmne <0.00045 0.0025 0.00045 mglL 01/19/1715:31 01120117 15:57
4-Nltroanfline <0.00038 0.0025 0.00038 mg IL 01/19/1715:31 01120/1715:57
Nitrobenzene <0.000033 0.0025 0.000033 mg IL 01/19/1715:31 01120/1715:57
4-Nitrophenol <0.00053 0.0025 0.00053 mg IL 01/1911715:31 01120/17 15:57
N-Nitrosodi-n-propylamine <0.00083 0.0025 0.00083 mg IL 0111911715:31 01120117 15:57
N-Nitrosodiphenylamine <0.000045 0.0025 0.000045 mg IL 0111911715:31 01120117 15:57
Pentachforophenol <0.00035 0.0050 0.00035 mg IL 01119/1715:31 01120/17 15:57
Phenol <0.00065 0.0025 0.00065 mg IL 01119/1715:31 01120/17 15:57
1.2,4, 5-Tetrachlorobenzene <0.000045 0.0025 0.000045 mg IL 01119/1715:31 01120117 15:57
2,3 ,4, 6-T etrachlorophenol <0.00040 0.0025 0.00040 mg IL 01/19/1715:31 01120117 15:57
1,2,4· Trichlorobenzene <0.000045 0.0025 0.000045 mg IL 01/19/1715:31 0112011715:57
2,4,5-Trichlorophenol <0.00093 0.0025 0.00093 mg IL 01/19/1715:31 0112011715:57
2,4,6-Trichloropheno! <0.00088 0.0025 0.00088 mg IL 01/19/1715:31 0112011715:57
MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae
2-Fluorobiphenyl 91 46 .124 0111911715:31 0112011715:57 1
2-Fluorophenol 42 13.113 0111911715:31 0112011715:57
Nitrobenzene-d5 BB 36-126 0111911715:31 01/2011715:57
Phenol-dS 54 17 -127 0111911715;31 01120117 15:57 1
Terphenyl..<J14 112 44-149 0111911715:31 01120117 15:57
2,4,6-Tribromophenol 6.1 26-150 0.111911715:31 0112011715:57
Lab Sample ID: LCS 400-3.39125/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis .Batch; 339188 Prep Batch: 339125
Spike LCS LCS o/aRec. Analyte Added Result Qualifier Unit D o/oftec Limits
Aniline 0.120 0.0882 m9IL 74 21.120
Bis(2-chloroethyl)et11er 0.120 0.0872 mg IL 73 44 -120
bis (2-chloroisopropyl) ether 0.120 0.0928 mg IL 77 33-121
Bis(2-ethylhexyl) phthalate 0.120 0.137 mg IL 114 52, 147
Butyl benzyl phthalate 0.120 0.110 mg IL 91 54-133
4-Chloroaniline 0.120 0.0918 mg IL 76 26-120
2-Ch!oronaphthalene 0.120 0.0944 mg/L 79 52.121
2-Chlorophenol 0.120 0.0753 mg IL 63 40-120
Oibenzofuran 0.120 0.0993 mg/L 83 56-122
2,4-Dichlorophenot 0.120 0.0945 mg IL 79 49-120
Diethyf phthalate 0.120 0.109 mg IL 91 50 .137
2,4-Dimethylphenol 0.120 0.0811 mg IL 68 48-120
Dimethyl phthalate 0.120 0.0981 mg IL 82 57 -124
2,4-Dinitropheno! 0.240 0.0392 mg IL 16 10-150
2,4-Dinitrotoluene 0.120 0.107 mg IL 89 54-142
2,6-Dinitroto!uene 0.120 0.0996 mg IL 83 55-130
Di-n-octyl phthalate 0.120 0.117 mg/L 97 57 .138
Hexachlorobenzene 0.120 0.0999 mg/L 83 52-129
TestAmerica Pensacola
Page 90 of 140 2/1/2017
E
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results Tes!America Job ID: 400-132540-1
Method: 82700 - Semivo!atile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 400-33912512-A Client sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 339188 Prep Batch: 339125
Spike LCS LCS 0/oRec.
Analyte Added Result Qualifier Unit 0 0/oR~c Limits Hexach!orobutadiene .0.120 0.0835 mg/L 70 45-120 Hexachlorocyclopentadlene 0.120 0.0553 mg/L 46 10-134 Hexachloroethane 0.120 0.0772 mg/L 64 41-120 lsophorone 0.120 0.0931 mg/L 78 48.120 2-Nitroaniline 0.120 0.101 mg/L 84 51-145 3-Nitroan!line 0.120 0.0995 n1g/L 83 37 .127 4-Nitroani!ine 0.120 0.101 mg/L 84 36-137 Nitrobenzene 0.120 0.0904 mg/L 75 45-120 4-Nitropheno! 0.240 0.106 mg/L 44 23-146 N-Nitrosodi-n-propylamine 0.120 0.0934 mg/L 78 45-120 N-Nitrosodiphenylamine 0.119 0.0959 mg/L 81 54-120 Pentachlorophenof 0.240 0.0916 mg/L 38 31-130 Phenol 0.120 0.0614 mg/L 51 40-120 1,2,4-Trichlorobenzene 0.120 0.0855 mg/L 71 47 -120 2,4,5-Trichlorophenol 0.120 0.103 mg/l 86 51 -136 2,4,6-Trichloropheno! 0.120 0.0918 mg/L 77 50-127
LOS LOS
Surrogate %Recovery Qualifier Limits 2-Fluorobiphenyl 85 46-124 2-Fluorophenol 66 13-113 Nitrobenzene-d5 81 36-126 Phenoi-d5 57 17 -127
Terphenyl-d14 95 44-149 2,4,6-Tribromophenol 95 26-150
Lab Sample ID: LCSD 400-339125/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 339188 Prep Batch: 339125
Spike LCSO LCSO o/oRec. RPO Analyte Added Result Qualifier Unit 0 %Rec Limits RPO Limit Aniline 0.120 0.0929 mg/L 77 21-120 5 30 Bis(2-chloroethyl}ether 0.120 0.0906 mg/L 76 44 - 120 4 30 bis {2-chloroisopropyl) ether 0.120 0.0971 mg/L 81 33-121 5 30 Bis(2-ethylhexyl) phthalate 0.120 0.129 mg/L 107 52-147 6 30 Butyl benzyl phthatate 0.120 0.121 mg/L 101 54-133 10 30 4-Ch!oroaniline 0.120 0.0964 mg/L 80 26-120 5 30 2-Chloronaphthalene 0.120 0.0996 n1g/L 83 52-121 5 30 2-Chloropheno! 0.120 0.0593 1119/L 49 40-120 24 30 Dfbenzofuran 0.120 0.106 mg/L 88 56-122 6 30 2,4-Dichlorophenol 0.120 0.0502 mg/L 42 49-120 61 30 Diethyl phtha!ate 0.120 0.114 mg/L 95 50-137 4 30 2,4-Dimetliylphenol 0.120 0.0817 mg/L 68 48-120 30 Dimethyl phthalate 0.120 0.102 mg/L 85 57 -124 4 30 2,4-Dinltrophenol 0.240 <0.0034 mg/L 0 10-150 200 30 2,4-Dinitrotoluene 0.120 0.107 mg/L 89 54-142 0 30 2,6-Dfnitrotoluene 0.120 0.103 mg/L 86 55-130 4 30 01-n-octyl phthalate 0.120 0.122 mg/L 101 57 .138 4 30 Hexachlorobenzene 0.120 0.112 mg/L 94 52-129 12 30
Tes!America Pensacola
Page 91 of 140 2/1/2017
E
QC Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Dup al/NA 9125
RPO Llnlit
30
30 30 30
30
30 30
30 30 30 30
30 30
30 30
30
E
Method: 82700 - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 400-339125/3-A Matrix: Water Analysis Batch: 339188
Analyte Hexachlorobu!adiene Hexachlorocyclopentadiene Hexachloroethane lsophorone 2-Nltroaniline 3-Nitroaniline
4-Nitroani!ine
Nitrobenzene 4-Nitrophenol N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine
Pentachlorophenor Phenol 1,2,4-Trichlorobenzene
2,4 ,5-Trichlorophenol 2,4,6-Trichloropheno!
Surrogate
2-Fluorobiphenyl 2-Fluorophenol Nitrof)eniene-d5 Pl1enol-d5 Terphenyl-d14 2,4,6-Tribromophenol
LCSD LCSD
%Recovety Qualifier 91
35 85 42
107
53
Lab Sample ID: MB 400-34007911-A Matrix: Water Analysis Batch: 340421
Analyte
Aniline 1, 1'-Biphenyl Bis(2-chloroethyl)ether
bis (2-chloroisopropyl} ether Bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene 2-Chlorophenol
Dibenzofuran
3,3'-Dichlorobenzldlne 2,4-Dich!orophenol Diethyl phthalate
2,4-Dimethylphenol Dimethyl phthalate
1,3-0initrobenzene
2,4-Dinitrophenol 2,4-Dinitrotoluene
MB MB
Result auallfler
<0.00095
<0.000043 <0.00068
<0.000040 <0.00050
<0.000048 <0.00085
<0.000035 <0.00055
<0.000043 <0.00065
<0.00075
<0.000060
<0.00088
<0.000043 <0.00025 <0.00085
<0.00048
Client Sample ID: Lab Control SamplePrep Type: TotPrep Batch: 33
LCSD LCSD Spike
Added
0.120 0.120 0.120
0.120
0.120 0.120
0.120 0.120
0.240 0.120 0.119
0.240 0.120
0.120
0.120 0.120
Result Qualifier Unit
0.0880 mg/L
Limits
46-124
13-113 36-126
17 - 127 44-149 26 • .150
RL 0.0025
0.0025 0.0025
0.0607 0.0810
0.0963 0.111 0.113 0.106
0.0943
0.0196 0.0974
0.114
0.0709 0.0450
0.0899 0.0420
0.0500
MDL Unit
0.00095 mg/L
0.000043 mg/L
0.00068 mg/L
0.0025 0.000040 mg/L
0.0025 0.00050 mg/L
0.0025 0.000048 mg/L
0.0025 0.00085 mglL
0.0025 0.000035 mg/L
0.0025 0.00055 mg/L
0.0025 0.000043 mg/L
0.0025 0.00065 mg/L
0.0025 0.00075 mg/L
0.0025 0.000060 mg/L
0.0025 0.00088 mg/L
0.0025 0.000043 mg/L
0.0025 0.00025 m9/L
0.0075 0.00085 mg/L
0.0025 0.00048 mg/L
Page 92 of 140
mg IL
mg/L
mg IL
mg IL
mg/L
mg/L
mg/L
mg/L mg/L
mg/L
mglL
mg/L
mglL
mgll
m9/L
%1Rec. D o/oRec Limits RPO
73
51 45.120 5
10-134 9 68 41-120 5
80 48.120 3
92 51 -145 9 94
88
79
37 -127 36.137
45-120 8 23-146
81 45.120
95 54-120
30 31-130 38 40-120
75 47 -120 35 51-136
42 50-127
13
5
4
138 4
17
25
31 5
84
59
Client Sample ID: M.ethod Blank Prep Type: Total/NA Prep Batch: 340079
D Prepared Analyzed 01127/1711:20 01/31/1718:31 01/27/1711:20 01/31/1718:31 01/27/1711:20 01131/1718:31
01/27/1711:20 01/31/1718:31 01/27/1711:20 01/31/1718:31 01/27/1711;20 01131/1718:31 01/27/1711:20 01/31/1718:31
01/27/1711:20 01/31/1718:31 01/27/1711:20 01/31/17 .18:31 01/27/1711:20 01131/1718:31
01127/1711:20 0113111718:31
01127/1711:20 01/31/1718:31 01127/1711:20 01/31/1718:31 01/2711711:20 01/31/17 .18:31
01/27/1711:20 01131117 18:31
01127/1711:20 01/:l1/1718:31 0112711711:20 01131/1718:31 01/27/1711:20 0113111718:31
011 Fae 1
TestAmerica Pensacola
211/2017
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 82700 - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 400-340079/1-A Matrix: Water Analysis Batch: 340421
MB MB
Anatyte Result Qualifier 2,6-Din!troto!uene <0.00048 Di-n-octyl phthalate 0.000602 J Hexachlorobenzene <0.000043
Hexachforobutadiene <0.00014
Hexachlorocyclopentadiene <0.00065 Hexach1oroethane <0.0011
lsophorone <0.000035 2-NltroaniHne <0.00055
3-Nitroani!ine <0.00045 4-Nitroaniline <0.00038
Nitrobenzene <0.0Q0033 4-Nitrophenol <0.00053 N-Nitrosodi-n-propylamine <0.00083
N~Nitrosodiphenylamine <0.Q00045
Pentachlorophenol <0.00035 Phenol <0.00065 1,2,4,5-T etrachlorobenzene <0.000045
2,3,4,6-Tetrachlorophenol <0.00040 1,2,4-Trichlorobenzene <0.000045 2,4,5-Trlchforophenol <0.00093
2,4,6-Trichlorophenol <0.00088
MB MB Surrogate %Recovery Qualifier 2-Fluorobiphenyl 66
2-Fluorophenol 38
Nitrobenzene-d5 69
Pheno!-d5 57 Terpheny/-d14 88
2,4,6-Tribromopheno! 28
Lab Sample ID: LCS 400-340079/2·A Matrix: Water Analysis Batch: 340421
Analyte Aniline 8is(2-chloroethyl)ether
bis (2-chlorolsopropyl} ether Bis(2-ethythexyl) phthalale
Butyl benzyl phthatate 4-Chloroaniline
2-Chloronaphthalene 2-Ch!orophenol
Dlbenzofuran 2,4-Dich!orophenol Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
RL MDL Unit 0.0025 0.00048 mg/L
0.0025 0.000043 mg/L
0.0025 .0.000043 rng/L
0.0025 0.00014 rng/L
0.0050 0.00065 rng/L
0.0025 0.0011 rng/L
0.0025 0.000035 mg/l
0.0025 0.00055 mg/L
0.0025 0.00045 rng/L
0.0025 0.00038 mg/L
0.0025 0.000033 mg/L
0.0025 0.00053 mg/L
0.0025 0.00083 mg/L
0.0025 0.000045 mg/L
0.0050 0.00035 mg/L
0.0025 0.00065 mg/L
0.0025 0.000045 mg/L
0.0025 0.00040 mg/L
0.0025 0.000045 mg/L
0.0025 0.00093 mg/L
0:0025 0.00088 mg/L
Limits 46" 124
13-113
36-126
17 -127
44.149
26-150
Spike LCS LCS
Added Result Qualifier
0.0300 0.0181
0.0300 0.0206
0.0300 0.0251 0.0300 0.0261
0.0300 0.0259 0.0300 0.0159
0.0300 0.0197
0.0300 0.0157 0.0300 0.0206
0.0300 0.0196 0.0300 0.0227
0.0300 0.0177
0.0300 0.0201
Page 93 of 140
D
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 340079
Prepared 01127/1711:20
0112711711:20 01127/1711:20
01/27/1711:20 0112711711:20 01127/1711:20 0112711711:20
0112711711:20 0112711711:20
01/27/17 11:20
01127/1711:20
01/27/1711:20 01/2711711:20
01/27/1711:20
01/27/1711:20
01/2711711:20 01/27/1711:20
01/27/1711:20
01/27/1711:20 01/27/1711:20
01127/1711:20
Prepared 0112711711:20
0112711711:20
0112711711:20
0112711711:20
01127117 11 :20
0112711711:20
Analyzed 01131117 18:31
01131117 18:31 0113111718:31
01131117 18:31
0113111718:31 01131117 18:31
01131117 18:31
0113111718:31
01131/17 18:31 0113111718:31
01131/17 18:31
01131/17 18:31 01131/17 18:31
01131/17 18:.31
01131117 18:31
01131/1718:31 01131/17 18:31
01131/17 18:31
01131/17 18:31 01131/1718:31
01131/1718:31
Analyzed
01131117.18:31
0113111718:31
0113111718:31
0113111718:31
0113111718:31
0113111718:31
OJI Fae 1
DJ/Fae
1
1 1
1
1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 340079 '%Rec.
Unit mgll
mg/L
mg/L
mg/L
rng/L
mg/L
mg/L
mg/L
mg/L
mg IL
rng/L
mg/L
mg/L
D o/oRec 60
69
84 87 86
53
66 52
69
65 76
59
67
Limits 21-120
44-120
33-121 52-147
54-133 26-120
52-121
40-120 56-122
49.120 50-137
48-120
57 -124
TestAmerica Pensacola
2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 82700 - Semivo!ati!e Organic Compounds {GC/MS) (Continued)
Lab Sample ID: LCS 400-340079/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 340421 Prep Batch: 340079
Spike LCS LCS o/oRec. Analyte Added Result Qualifier Unit 0 %Rec Limits 2,4-Dinltrophenol 0.0600 0.0121 mg IL 20 10-150 2.4-Dinitrotoluene 0.0300 0.0210 n1g/l 70 54-142 2,6-Dinitroto!uene 0.0300 0.0194 mg/L 65 55-130 Pi-n-octyl phthalate 0.0300 0.0249 mg/L 83 57 -138 Hexachlorobenzene 0.0300 0.0198 mg IL 66 52-129 Hexachlorobutadiene 0.0300 0.0188 mg/L 63 45-120 Hexach!orocyclopentadiene 0.0300 0.00416 J mg/L 14 10-134 Hexachloroethane 0.0300 0.0209 mg/L 70 41-120
lsophorone 0.0300 0.0208 mg/L 69 48-120 2-Nitroaniline 0.0300 0.0234 mg IL 78 51.145
3-Nitroaniline 0.0300 0.0200 mg IL 67 37 -127
4-Nltroaniline 0.0300 0.0198 mg IL 66 36-137 Nitrobenzene 0.0300 0.0207 mg/L 69 45-120 4-Nitrophenol 0.0600 0.0411 mg IL 69 23 .146
N-Nitrosodi-n-propylamine 0.0300 0.0240 mg IL 80 45-120 N-Nitrosodiphenylamine 0.0298 0.0199 mg/L 67 54-120
Pentachlorophenol 0.0600 0.0239 mg IL 40 31-130 Phenol 0.0300 0.0176 mglL 59 40 .120 1,2,4-Trichlorobenzene 0.0300 0.0187 mg/L 62 47 -120 2,4,5· Trichlorophenol 0.0300 0.0201 mg/L 67 51-136 2,4,6-Trich!orophenol 0.0300 0.020:) mg IL 68 50-127
LCS LCS :surrogate %Recovery Qua/Iner Limits 2-Fluorobipl1eny/ 64 46-124
2-Fluorophenol 30 13-113 Nitrobenzene-d5 66 36.126
Phenol-d5 58 17 -127 Tel)Jhenyl-d14 76 44-149 2,4,6-Tribromophenof 68 26-150
Lab Sample ID: LCSD 400-340079/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 340421 Prep Batch: 340079
Spike LCSO LCSO 0/oRec. RPO Analyte Added Result Qualifier Unit 0 o/oRec Limits RPO Limit Aniline 0.0300 0.0201 mg/L 67 21-120 11 30 Bis(2-chloroethyl)ether 0.0300 0,0233 mg IL 78 44-120 12 30
bis (2-chloroisopropyl) ether 0.0300 0.0285 mg/L 95 33-121 12 30 Bis(2-ethylhexyl) phthalate 0.0300 0.0288 mg IL 96 52-147 10 30 Butyl benzyl phthalate 0.0300 0.0282 mg/L 94 54 .133 9 30 4-Chloroaniline 0.0300 0.0178 mg IL 59 26.120 11 30 2-Chloronaphthalene 0.0300 0.0220 mglL 73 52-121 11 30 2-Chlorophenol 0.0300 0.0208 mg/L 69 40-120 28 30 Dlbenzofuran 0.0300 0.02:)3 mglL 78 56-122 12 30 2,4-Dichlorophenol 0.0300 0.0232 mg IL 77 49-120 17 30 Diethyl phthalate 0.0300 0.0265 mg/L 88 50-137 15 30 2,4-0imethylphenol 0.0300 0.0193 mg IL 64 48-120 9 30 Dimethyl phthalate 0.0300 0.0227 mg/L 76 57 -124 ·12 30
TestAmerica Pensacola
Page 94 of 140 2/1/2017
II
QC Sample Results Client: C-K Associates Project/Site; Moffat & Nichol
TestArnerica Job ID: 400-132540-1
Method: 82700 - Semivolatile Organic Compounds (GCIMS).(Continued)
Lab Sample ID: LCSD 400-340079/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 340421 Prep Batch: 340079
Spike LCSD LCSD o/oRec. RPO Analyte Added Result Qualifier Unit D 0/C)Rec Limits RPO Limit
2,4-Dinitrophenol 0.0600 0.0250 mg/L 42 10-150 70 30 2,4-Dinitrotoluene 0.0300 0.0239 mg/L 80 54 .142 13 30 2,6-Dinitrotpluene 0.0300 0.0218 mg/L 73 55-130 12 30
Di-n-octyl phthalate 0.0300 0.0283 mg/L 94 57 -138 13 30
Hexachlorobenzene 0.0300 0.0218 mg/L 73 52-129 10 30 Hexach!orobutadiene 0.0300 0.0211 mg/L 70 45-120 12 30
Hexachlorocyclopentadiene 0.0300 0.00510 mg/L 17 10-134 20 30
Hexachloroethane 0.0300 0.0233 mg/L 78 41 -120 11 30 lsophorone 0.0300 0.0238 mg/L 79 48-120 14 30 2-Nitroanlline 0.0300 0.0264 mg/L 88 51 -145 12 30
3-Nltroanifin'e 0.0300 0.0223 mg/L 74 37 .127 11 30
4-Nitroaniline 0.0300 0.0228 mg/L 76 36 .137 14 30 Nitrobenzene 0.0300 0.0233 mg/L 78 45-120 12 30
4-Nitrophenol 0.0600 0.0474 mg/L 79 23 .146 14 30
N-NitrosodJ-n-propylamine 0.0300 0.0269 mg/L 90 45-120 11 30
N-Nitrosodiphenylamine 0.0298 0.0222 mg/L 75 54-120 11 30
Pentachlorophenol 0.0600 0.0321 mg/L 54 31 -130 29 30 Phenol 0.0300 0.0216 mg/L 72 40-120 21 30
1,2.4-Trichlorobenzene 0.0300 0.0210 mg/L 70 47 -120 12 30 2,4,5-Trichlorophenol 0.0300 0.0231 mg/L 77 51 -136 14 30 2,4,6-Trichlorophenol 0.0300 0,0234 mg/L 78 50-127 14 30
LCSD LCSD Surrogate %Recovery Qualifier Limits 2~Fluorobfphenyl 74 46-124 2-Fluorophenol 58 13.113
Nitrobenzene-d5 78 36-126
Phenof-d5 76 17 -127 Terphenyl-d14 90 44-149 2, 4,6-Tribromophenol 79 26-150
Method: .82700 LL - Semivolatile Organic Compounds by GC/MS - Low Level
Lab Sample ID: MB 400·338284/1-A Client Sample ID: Methoc;I Blank Matrix: Water Prep Type; Total/NA Analysis Batch: 338569 Prep Batch: 338284
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae Acenaphthene <0.000032 0.00020 0.000032 mg/L 01/1211716:23 01/16/1717'40
Acenaphthylene <0.000045 0.00020 0.000045 mg/L 01/12117 16:23 01/16/1717:40
Anthracene <0.000032 0.00020 0.000032 mg/L 01/1211716:23 01/16/1717:40
Benzq[a]anthracene <0.000046 0.00020 0.000046 mg/L 01/12117 16:23 01/16/1717:40
Benzo[a]pyrene <0,000042 0.00020 0.000042 mg/L 01/1211716:23 01/16/1717:40
Benzo[b]fluoranthene <0.000034 0.00020 0.000034 mg/L 01/12117 16:23 01/16/1717:40
Benzo[k}fluoranthene <0.00010 0.00020 0.000.10 mg/L 01/1211716:23 01/16/1717:40
Chrysene <0.000074 0.00020 0.000074 mg/L 01/1211716:23 01/16/1717:40
Dibenz(a,h)anthracene <0.000050 0,00020 0.000050 mg/L 01/1211716:23 01/16/1717:40
Fluoranthene <0.000068 0,00020 0.000068 mg/L 01/1211716:23 01/16/1717:40
Fluorene <0.00011 0.00020 0.00011 mg/L 01/1211716:23 01/16/1717:40
TestArnerica Pensacola
Page 95 of 140 2/1/2017
E
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 82700 LL - Semivolati!e Organic Compounds by GC/MS - Low Level {Continued)
Lab Sample ID: MB 400-33828411-A Matrix: Water Analysis Batch: 338569
MB MB
Analyte Result Qualifier
lnden6(1 ,2,3-cd]pyrene <0.000043
2·Methylnaphthalene <0.000060 Naphthalene <0.000094
Phenanthrene <0.000036
Pyrene <0.000040
MB MB Surrogate %Recovery Qualifier
2·Fluorobiphenyl 108
Nitrobenzene-d5 100
Terphenyl-d14 140 x
Lab Sample ID: LCS 400·33828412-A Matrix: Water Analysis Batch:_ 3.3.8569
Analyte Acenaphthene
Acenaphthylene
Anttiracene Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzofk]fiuoranthene
Chrysene Dibenz{a,h)anthrace_ne Fluoranthene
Fluorene
lndeno[ 1,2,3·cd]pyrene 2·Methylnaphthatene
Naphthalene
Phenanthrene
Pyrene
Surrogate 2~Fluorobiphenyl
Nitrobenzene-dS
Terp/1eny/-d14
LCS LCS
%Recovety Qua/If/er 80
91
89
Lab .Sample ID: LCSD 400-33828413-A Matrix: Wa_ter Analysis Balch: 338569
Analyte Acenaphthene
Acenaphthylene
Anthracene
Benzo[a]anthracene Benzo[a]pyrene
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338284
RL MDL Unit D Prepared Analyzed Oil Fae
0.00020 0.000043 mg/L 01/1211716:23 01116117 17:40 1 0.00020 0.000060 mg/L 0111211716:23 01116117 17:40 0.00020 0.000094 mg/L 0111211716:23 0111611717:40
0.00020 0.000036 mg/L 01/1211716:23 01116117 17:40
0.00020 0.000040 mg IL 0111211716:23 01116117 17:40
Ll1nlts Prepared Analyzed Dll Fae
15-122 0111211716:23 01116117 17:40 1
19-130 0111211716:23 0111611717:40 1
33 -138 0111211716:23 01116117 17:40
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338284
Spike LCS LCS 0/oRec.
Added Result Qualifier Unit D 0/oRec Limits
0.120 0.116 mg/L 96 41-120
0.120 0.124 mg/L 103 44 -120 0.120 0.122 mg/L 102 49 -120
0.120 0.124 mg/L 103 61-135
0.120 0.125 mg/L 104 52-120
0.120 0.126 mg/L 105 53-134
0.120 0.123 mg/L 102 57 -134
0.120 0.120 mg/L 100 55 -122
0.120 0.122 mg IL 102 48. 146
0.120 0.125 mg IL 104 54-128
0.120 0.116 mg IL 97 45-125
0.120 0.120 mg/L 100 43-142
0.120 0.120 mg/L 100 32-124
0.120 0.112 mg IL 93 39.125
0.120 0.120 mg/L 100 48-120
0.120 0.130 mg/L 108 48-132
Limits 15-122
19-130
33-138
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 338284
Spike LCSD LCSD o/oRec. RPO Added Result Qualifier Unit D o/ciRec Limits RPO Limit
0.120 0.120 mg IL 100 41-120 4 56 0.120 0.130 mg IL 108 44-120 5 56
0.120 0.134 mglL 112 49-120 9 51
0.120 0.127 n1g/L 106 61-135 3 49 0.120 0.131 mg/L 109 52.120 5 50
TestAmerica Pensacola
Page 96 of 140 2/112017
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QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: 8270D LL. Semivolatile Organic Compounds by GC/MS ·Low Level (Continued)
Lab Sample ID: LCSD 400-338284/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 338569 Prep Batch: 338284
Spike LCSO LCSO o/oRec, RPO Analyte Added Result Qualifier Unit 0 o/oRec Limits RPO Limit Benz6[b]fiuoranthene 0.120 0.133 mg IL 111 53-134 6 54
Benzo[kJfluoranthene 0.120 0.134 mg IL 111 57-134 8 52 Chrysene 0.120 0.129 mg IL 107 55-122 7 50 Oibenz(a,h)anthracene 0.120 0.131 mgll 109 48-146 6 50 Fluoranthene 0.120 0.136 mg/L 113 54-128 8 52 Fluorene 0.120 0.126 mglL 105 45-125 8 56 lndeno[1 ,2,3-cd]pyrene 0.120 0.128 mg/L 107 43-142 7 51 2-Methylnaphthalene 0.120 0.124 mg IL 104 32-124 3 57 Naphthalene 0.120 0.119 mg IL 100 39-125 6 56 Phenanlhrene 0.120 0.129 mg/L 107 48-120 7 56 Pyrene 0.120 0.141 mg IL 117 48-132 8 52
LCSD LCSD Surrogate %Recovery Quaflfler Limits 2-Fluorobipl1enyl 86 15-122
Nifrobenzene-d5 92 19-130
Terphenyl-d14 92 33-138
Lab Sample ID: MB 400-33912511-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 339599 Prep Batch: 339125
MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed 011 Fae Ac~naphthene <0.000032 0.00020 0.000032 mg IL 0111911715:31 01124117 15:18 1 Acenaphthylene <0.000045 0.00020 0.000045 mg/L 01119/1715:31 01/24/17 15:18 Anthracene <0.000032 0.00020 0.000032 mg/L 0111911715:31 01/24/17 15:18
Benzo[a]anthracene <0.000046 0.00020 0.000046 mg/L 01/1911715:31 01124/17 15:18
Benzo[a]pyrene <0.000042 0.00020 0.000042 mg/L 01119/1715:31 01/24/17 15:18
Benzo{b]fluoranthene <0.000034 0.00020 0.000034 mg/L 01119/1715:31 01/24117 15:18 Benzo[k]fluoranthene <0.00010 0.00020 0.00010 mg/L 01/19/1715:31 01124117 15:18
Chrysene <0.000074 0.00020 0.000074 mg/L 0111911715:31 0112411715:18
Dibenz(a,h)anthracene <0.000050 0.00020 0.000050 mg IL 01/19/1715:31 01/2411715:18
Fluoranthene <0.000068 0.00020 0.000068 mg/L 01/1911715:31 0112411715:18 Fluorene <0.00011 0.00020 0.00011 mg/L 01/19/1715:31 01124/17 15:18
lndeno[1,2,3-cdJpyrene <0.000043 0.00020 0.000043 mg/L 0111911715:31 01124/17 15:18 2-Methylnaphthalene <0.000060 0.00020 0.000060 mg/L 01/1911715:31 01/24/1715:18 Naphthalene <0.000094 0.00020 0.000094 mg/L 01/19/1715:31 01/24/1715:18
Phenanthrene <0.000036 0.00020 0.000036 mg/L 01/19/1715:31 01124117 15:18
Pyrene <0.000040 0.00020 0.000040 mg/L 01119/1715:31 01124117 15:18
MB MB Surrogate %Recovery Qua/If/er Limits Prepared Analyzed Dlf Fae
2-Ffuorobiplienyl 116 15-122 01119117 15:31 01124117 15:18 1
Nitrobenzene-dS 101 19-130 01119117 15:31 0112411715:18 1 Terphenyl-d14 135 33-138 0111911715:31 01124117 15:18
TestAmerica Pensacola
Page 97 of 140 2/1/2017
B
Client: C-K Associates Projecl/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: 82700 LL - Semivolatite Organic Compounds by GC/MS - low Level (Continued)
Lab Sample ID: LCS 400-33912512-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 339599 Prep Batch: 339125
Spike LCS LCS 0/oRec. Analyte Added Result Qualifier Unit 0 0/oRec Limits Acenaphthene 0.120 0.127 mg/L 106 41-120 Acenaphthylene 0.120 0.126 mg/L 105 44-120
Anthracene 0.120 0.125 n1g/L 104 49-120 Benzo[a]anthracene 0.120 0.129 mgfL 108 61 .135
Benzo[aJpyrene 0.120 0.120 mg/L 100 52-120 Benzo{b}fluoranthene 0.120 0.124 mg/L 103 53 .134
Benzo[k]fluoranthene 0.120 0.116 mg/L 97 57-134
Chrysene 0.120 0.116 mg/L 97 55 - 122 Dibenz(a,h)a_nthracene 0.120 0.132 mg/L 110 48-146
Fluoranthene 0.120 0.130 mg/L 109 54 .128
Fluorene 0.120 0.129 mg/L 107 45-125
lndeno[1,2,3·cd]pyrene 0.120 0.127 mg/L 106 43-142 2~Methylnaphthalene 0.120 0.121 mg/L 101 32-124 Naphthalene 0.120 0.111 mg/L 92 39-125
Phenanthrene 0.120 0.131 mg/L 109 48-120 Pyrene 0.120 0.135 mg/L 113 48-132
LCS LCS
Surrogate %Recovety Quallfler Limits 2-Fluoro!Jiphenyl 114 15-122 Nitrobenzene-05 100 19-130
Terpllenyl·d-14 132 33-138
Lab Sample ID: LCSD 400-33912513-A Client Sample ID: Lab Control Sample Dup Matrix; Water Prep Type: Total/NA Analysis Batch: 339599 Prep Batch: 339125
Spike LCSO LCSO o/oRec. RPO Analyte Added Result Qualifier Unit 0 o/aRec Limits RPO Limit Acenaphthene 0.120 0.115 mg/L 96 41-120 10 56 Acenaphthylene 0.120 0.115 mg/L 96 44-120 9 56 Anthracene 0.120 0.111 mg/L 92 49-120 12 51 Benzofa]anthracene 0.120 0.116 mg/L 97 61-135 11 49 Benzo{a]pyrene 0.120 0.109 mg/L 91 52-120 10 50 Benzo[b)fiµoranthene 0.120 0.112 mg/L 94 53-134 10 54 Benzo[k]fluoranthene 0.120 0.104 mg/L 87 57 -134 11 52 Chrysene 0.120 0.103 mg/L 86 55-122 12 50 Dlbenz(a,h)anthracene 0.120 0.114 mg/L 95 48-146 15 50 Fluoranthene 0.120 0.118 mg/L 98 54-128 10 52 Fluorene 0.120 0.116 mg/L 96 45-125 11 56 lndeno[ 1,2,3-cd]pyrene 0.120 0.110 mg/L 92 43-142 14 51 2~Methy1naphthalene 0.120 0.112 mg/L 93 32-124 8 57 Naphthalene 0.120 0.103 mg/L 86 39-125 7 56 Phenanthrene 0.120 0.118 mg/L 99 48-120 10 56 Pyrene 0.120 0.121 mg/L 101 48-132 11 52
LCSD LCSD Surrogate %Recovery Quallfler Lfmlts 2-Fiuorohiphenyl 105 15-122 Nitrobenze11e-d5 91 19-130
TestAmerica Pensacola
Page 98 of 140 21112017
E
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nicllol
TestAmerica Job ID: 400-132540-1
Method: 82700 LL - Semivolatile Organic Compounds by GCIMS. Low Level (Continued)
Lab Sample ID: LCSD 400-339125/3-A Matrix: Water Analysis Batch: 339599
Surrogate Terphenyl-d14
LCSD LCSD %Recovery Qualifier
117
Lirnits
33-138
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 339125
Method: MAVPH - Massachusetts • Volatile Petroleum Hydrocarbons (GC)
Lab Sample ID: Ms 400-338604/1-A Matrix: Solid Analysis Batch: 338571
MB MB Analyte Result Qualifier C6-C8 Aliphatics <1.5
C8-C10 Aliphatics <2.5 C8-C 10 Aromatics <t3,
MB MB Surrogate %Recovery Qualifier a,a,a-Trifluorotoluene (fid) 75 a,a,a-Trifluorotoluene (pid) 76
Lab Sample ID: LC.S 400-338604/2-A Matrix: Solid Analysis Batch: 338571
Analyte CB-C 1 O Aromatics
C5-C8 Aliphatics
C9-C12 AllphaUcs
Surrogate a,a,a-Trifluorotoluene (fid)
a,a,a-Trifluorotoluene (pid)
LCS LC$ %Recovery Qualifier
107
.109
Lab Sample IP: LCSD 400-338604/3-A Matrix: Solid Analysis Batch: 338571
Analyte CB-C 1 O Aromatics
C5-C8 Aliphatics
C9-C12 Allphatics
Surrogate a,a,a-Trifluorotoluene (fid)
a,a,a-TrifluorotoJuene (pid)
LCSD LC.SD %Recov~ry 'Qualifier
100
101
RL 1.5 2.5
1.3
Lltnlts
70-130
70. 130
Spike LCS
Added Result
2.50 2.57 15.0 13.0
17.5 16.8
Limits 70-130
70-130
Spike LCSD Added Result
2.50 2.39
15.0 12.4
17.5 15.2
Limits 70-130
70-130
Page 99 of 140
MDL Unit 1.5 mg/Kg
2.5 mg/Kg
1.3 mg/Kg
LCS Qualifier
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338604
D Prepared Analyzed OJI Fae 0111611710:30 0111611.712:45 50 01/16117 10:30 01/16117 12:45 50 0111611710:30 01/16117 12:45 50
Prepared Analyzed Dll Fae 01111!/1710'30 01116117 12:45 50
0111611710:30 01116117 12:45 50
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338604 o/oRec.
Unit
mg/Kg
mg/Kg
mg/Kg
D %Rec Limits
10:3 70-130 87 70-130
96 70-130
Client Sample ID: Lab Contro.I Sample Pup Prep Type: Total/NA Prep B.atch: 338604
LCSD Qualifier Unit
mg/Kg
mg/Kg
mg/Kg
o/oRec. RPO 0 %Rec Limits RPO Limit
96 70-130 7 25
83 70-130 87 70.130
5 10
25
25
TestAmerica Pensacola
2/1/2017
Client: C-K Associates ProjecUSite: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: MAVPH. Massachusetts. Volatile Petroleum Hydrocarbons (GC) (Continued)
Lab Sample ID: 400-132588·6 MS Matrix: Solid Analysis Batch: 338571
Sample San1ple
Analyte Result Qualifier C8-C10 Aromatics <6.1
C5-C8 Aliphatics <13
C9-C12 A!iphatics <6_9
MS MS Surrogate %Recovery QuallfJer a,a,a-Ttifluorotoluene (fid) 79 a,a,a-Trifluorototuene (pid) 79
Lab Sample ID: 400-132588-6 MSD Matrix: Solid Analysis Batch: 338571
Sample Sample
Analyte Result Quallfler C8-C10 Aromatics <6.1
C5-C8 Aliphatics <13
C9-C12 Alfphatics <6.9
MSD MSD
Surrogate %Recovery Qualifier
8,a,a-Trifluorotoluene (fid) 94 fJ,a,a-Trifluorotoluene (pid) 93
La.b Sample ID: MB 400-339057/2 Matrix: Water Analysis Batch: 339057
MB MB
Analyte Result Qualifier
C6-C8 Aliphatics <0.030
C8-C10 Aliphatics <0.050
C8-C10 Aromatics <0.025
MB MB Surrogate %Recovery Qualifier
a,a,a-Trifluoroto/uene (fid) 106. a,a,a-Trifluorotoluene (pid) 106
Lab Sample ID: LCS 400-3390.57/3 Matrix: Waler Analysis Batch: 339057
Analyte
C8-C10 Aromatics
C5-C8 AHphatics _C9-C12 Aliphatics
Surrogate
a,a,a-Trifluorotoluene (fid)
a,a,a-Trifluorotoluene (pid)
LCS LCS
%Recovery Qualifier
107 108
Spike
Added
12.2
73.4
85.7
Limits 70-130
70-130
Spike
Added
.12.2
73.4
85.7
Limits 70-130 70-130
RL
0.030
0.050
0.025
Limits to: 130
70-130
Spike
Added
o.o5oo 0.300
0.350
Limits 70-130 70-130
MS MS
Result Qualifier
11.6
56.3
68.2
MSD MSD
Result Quallfler
13.2
66.6
76.4
MDL Unit
0.030 mg/L
0.050 mg/L
0.025 mg/L
LCS LCS
Result Qualifier
0.0474
0.259
0.319
Page 100 of 140
Unit mg/Kg
mg/Kg
nig/Kg
Unit
mg/Kg
mg/Kg
mg/Kg
D
Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338604 0/oRec.
0 o/oRec Limits i;1 94 70-130 0 77 70-130 ·l:l 80 70-130
Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 338604 o/oRec. RPO
0 o/oRec Limits RPO Limit n 108 70-130 13 25 .1;1 91 70-130 17 25 n 89 70-130 11 25
Client Sample ID: Meth<>d Blank Prep Type: T<>tal/NA
Prepared Analyzed Oil Fae
0111911713:26 1
01/19/17 13:26
01/19/1713:26
Prepared Analyzed DI/ Fae 0171911113.'26 1 0111911713:26
Client Sample ID: Lab C<>ntrol Sample Prep Type: Total/NA
%Rec. Unit 0 ~%Rec j..lmlts
mg/L 95 70-130
mg/L 86 70-130
mg/L 91 70-130
TestAmerica Pensacola
2/1/2017
E
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Tes!America Job ID: 400-132540-1
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Lab Sample ID: LCSO 400-339057/4 Matrix: Water Analysis Batch: 339057
Analyte CB-C1 O Aromatics
C5-C8 A!iphatics
C9-C12 Aliphatics
Surrogate a,a,a-Trif/uorotoluene (fid)
8,a,a-Trifluorotoluene (pid)
LCSD LCSD %Recovery Qualifier
105
107
Spike
Added
0.0500 0.300
0.350
Lltnlts
70-130
70-130
Method: 8011 - EDS, DBCP, and 1.,2,3-TCP (GC)
Lab Sample ID: MB 400-339493/1-A Matrix: Water Analysis Batch: 339878
MB MB
LCSD
Result
0.0488 0.260
0.327
LCSD
Qualifier
Client Sample ID: Lab Control Sample Oup Prep Type: Total/NA
Unit mg/L
mg/L
n1g/L
o/oRec. RPO 0 0/oRec Limits RPO Limit
98 70-130 3 25 87 70-130 1 25 93 70-130 3 25
Client sample ID: Method Blank Prep Type: T.otal/NA Prep Batch: 339493
-Analyte
1,2-Dibromo-3-Chloropropane
Result Qualifier <0.0000055
RL MOL Unit O Prepared Analyzed DU Fae 0.000030 0.0000055 mg/L 0112311716:25 01126117 21:11 1
Surrogate 4-Bromof/uorobenzene
MB MB
%Recovery Qua/If/er 109
Limits
51-149
Lab Sample ID: LCS 400-339493/2-A Matrix: Water Analysis Batch: 339878
'Analyte
1,;2-Dibromo-3-Ch!oropropane
Surrogate -4-Bromofluorobenzene
LCS LCS %Recovery Qualifier
97
Lab Sample JO: LCSO 400-33949313-A Matrix: Water Analysis Batch: 339878
Analyte 1,2-Dibromo-3-Chloropropane
Surrogate
4·Bromof/uorobenzene
LCSD LCSD %Recovety Qualifier
108
Spike Added
0.000100
Limit~
51-149
Spike Added
0.000100
Limits
51-149
LCS LCS
Prepared Analyzed Dlf Fae 01123/1716:25 01126117 21:11 1
Client Sample 10: Lab Control Sample Prep Type: Total/NA Prep Batch; 339493 o/oRec.
Result Qualifier Unit 0 o/oRec Limits
0.000111 mg/L 111 60-140
Client Sample lO: Lab ControJ Sample Oup Prep Type: TotaJ/JllA Prep Batch: 33.9493
LCSD LCSO
Result Qualifier Unit 0.000117 mg/L
0 %Rec 117
0/oRec. RPO Limits RPO Limit 60-140 5 30
Tes!America Pensacola
Page 101 of 140 2/1/2017
E
QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Method: 80818 • Orga11ochlori11e Pesticides (GC)
Lab Sample JD: MB 400-338239/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 339079 Prep Batch: 338239
MB MB
Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed DH Fae Aldrin <0.00000030 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/17 12:25 1
0 alpha-BHC 0.00000102 J 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/17 12:25
6
E beta-BHC <0.00000030 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/1712:25
0 delta-BHC 0.00000176 J 0.0000050 0.0000002 mg/L 01/12/1713:08 01/19/1712:25
1 gamma-BHC (Undane) <0.0000025 0.0000050 0.0000025 mg/L 01 /12/17 13:08 01/19/1712:25 -atpt}a-Chlordane <0.00000042 0.0000050 0.0000004 mg/L 01/12/1713:08 01119/1712:25
2 gamma-Chlordane <0.00000032 0.0000050 0.0000003 mg IL 01/12/1713:08 0111911712:25
2 4,4'-DDE <0.00000022 0.0000050 0.0000002 mg IL 01112/1713:08 01/19117 12:25
2 Dieldrin 0.000000678 J 0.0000050 0.0000003 mg/L 01 /12/17 13:08 01/19/17 12:25
0 Endosulfan I <0.00000030 0.0000050 0.0000003 mg/L 01112/17 13:08 01/19/17 12:25
0 Endosulfan l I <0.00000074 0.0000050 0.0000007 mg/L 01/12/1713:08 01/19/17 12:25
4 Endosu!fan sulfate <0.00000021 0.0000050 0.0000002 mg/L 01/12/1713:08 01/19/17 12:25
1 Endrin <0.00000030 0.0000050 0.0000003 mg/L 01/1211713:08 01/19/1712:25
0 Endrin aldehyde <0.00000028 0.0000050 0.0000002 mg/L 01/12/1713:08 01119/17 12:25
8 Endrin ketone <0.00000038 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/17 12:25
8 Heptachlor <0.00000031 0.0000050 0.0000003 mg/L 01/12/1713:08 01/19/1712:25
1 Heptachlor epoxide <0.00000032 0.0000050 0.0000003 mg/L 01/12117 13:08 01/19/1712:25
2 Methoxychlor <0.00000041 0.0000050 0.0000004 mg/L 01/12/1713:08 01/19/17 12:25
1 Toxapheoe <0.000030 0.00030 0,000030 mg/L 0111211713:08 01/19/17 12:25
MS MS $urrogate %Recove_ty Qua/If/er Limits Prepared Analyzed Dll Fae DCB Decachlorobipheny/ 56 10-130 0111211713:08 0111911712:25 1
Tetrachloro-m-xyJene gg 43-130 0111211713:08 0111911712:25 1
. Lab Sample ID: LCS 400-338239/2-A Client Sample ID: Lab Control Sampl!! Matrix: Water Prep Type: Total/NA Analysis Saleh: 339079 Prep Batch: 338239
Spike LCS LCS o/GRec. Analyte Mded Result Qualifier Unit 0 %Rec Limits
Aldrin 0.000500 0.000445 mg/L 89 52-150 alpila-BHC 0.000500 0.000403 mg/L 81 50 -150 beta-BHC 0.000500 0.000409 mg/L 82 58-150 delta-BHC 0.000500 0.000377 mg/L 75 42 .150 gamma~BHC {Lindane) 0.000500 0.000389 n1g/L 78 53-150 alpha-Chlordane 0.000500 0.000416 mg/L 83 63 .150
TestAmerica Pensacola
Page 102of140 2/1/2017
QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Method: 80818 • Organochlorine Pesticides (GCJ (Continued)
Lab Sample ID: LCS 400-338239/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 339079 Prep Batch: 338239
Spike LCS LCS o/oRec. Analyte Added Result Qualifier Unit D o/oRec Limits gamm·~-·ch10fd8rie 0.000500 0.000362 mg/L 72 62-150
4.4'·DDE 0.000500 0.000408 mg IL 82 65-150 Die!drln 0.000500 0.000373 mg IL 75 64-150
Endosulfan l 0.000500 0.000367 mg IL 73 40-127
B Endosulfan II 0.000500 0.000415 mg IL 83 40-135
Endosurran sulfate 0.000500 0.000400 n1g/L 80 50-150 Endrin 0.000500 0.000402 mg IL 80 63-150
Endrin aldehyde 0.000500 0.000424 mg/L 85 40-150 Endrln ketone 0.000500 0.000392 mg/L 78 52-150 Heptachlor 0.000500 0.000402 mg/L 80 59-150
Heptachlor epoxid€? 0.000500 0.000386 mg/L 77 63 .150
Methoxychlor 0.000500 0.000424 mg IL 85 57 -150
LCS LCS Surrogate %Recovery Qualifier Limits
bcB Decachlorobiphenyl 67 10-130 Tetrachforo-m-xylene 88 43-130
Lab Sample ID: LCSD 400-33823913-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 339079 Prep Batch: 338239
Spike LCSD lCSD o/oRec. RPO Analyte Added Result auaHfler Unit D o/oRec Limits RPO Limit Aldrin 0.000500 0,000462 mg/L 92 52-150 4 40 alpha-BHC 0.000500 0.000407 mg/L 81 50-150 40 bela·BHC 0.000500 0.000404 mg IL 81 58-150 1 40 delta-BHC 0.000500 0.000370 mg IL 74 42-150 2 40 gamma-BHC (Lindane) 0.000500 0.000383 mg IL 77 53-150 2 40 alpha-Chlordane 0.000500 0.000412 mg/L 82 63-150 40 gamma-Chlordane 0.000500 0.000355 mg/L 71 62-150 2 40 4.4'-DDE 0.000500 0.000399 mg IL 80 65-150 2 40
Dieldrin 0.000500 0.000360 mg/L 72 64-150 4 40 Endosulfan J 0.000500 0.000356 mg/L 71 40-127 3 40 Endosulfan II 0.000500 0.000386 mg IL 77 40-135 7 40
Enqosu!fan sulfate O.OOQ500 0.000362 mg IL 72 50-150 10 40
Endrin 0.000500 0.000380 mg/L 76 63-150 6 40 'Endrin a)dehyde 0.000500 0.000391 mg/L 78 40-150 8 40
Endrin ketqne 0,000500 0.000347 mg/L 69 52-150 12 40 Heptach!or 0.000500 0.000389 mg IL 78 59-150 3 40 Heptachtor-epoxlde 0.000500 0.000382 mg/L 76 63-150 40 Methoxychlor 0.000500 0.000368 mg/L 74 57 -150 14 40
LCSD LCSD Surrogate %Recovery Qualifier Limits
DCB Decacf11orobipheny/ 52 10-130 TetraCh/oro-m-xylene 91 43-130
TestAmerica Pensacola
Page 103of140 2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results
Method: 808113 • Organoch!orine Pesticides (GC) (Continued)
Lab Sample ID: MB 400·338557/10-A Matrix: Solid Analysis Batch:.338801
MB MB Analyte Result Qualifier
Aldrin <0.00061
alpha-BHC <0.00024
beta-BHC <0.00050
delta-BHC <0.00032
gamma-BHC (Undane) <0.00022
alpha-Chlordane <0.00028
gamma-Chlordane <0.00027
4,4'-DDD <0.00019
4,4'-DDE <0.00027
4,4'-DDT <0.00077
Dietdrin <0.00036
Endosulfan I <0.00021
Endosulfan II <0.00023
Endosulfan .sulfate <0.00021
Endrin <0.00019
Endrin aldehyde <0.00029
Endrln ketone <0.00035
Heptachlor <0.00024
Heptachlor epoxide <0.00045
Methoxychlor <0.00033
Toxaphene <0.029
MB MB Surrogate %Recovery Qualifier ·ocB DecaCh!orobiphenyJ
Tetrachlorcrm-xy!_ene
Lab Sample ID; LCS 4!l0·338557/9·A Matrix; S.olid Analysis £latch: 338801
g9
95
RL MDL 0.0017 0.00061
0.0017 0.00024
0.0017 0.00050
0.0017 0.00032
0.0017 0.00022
0.0017 0.00028
0.0017 0.00027
0.0017 0.00019
0.0017 0.00027
0.0017 0.00077
0.0017 0.00036
0.0017 0.00021
0.0017 0.00023
0.0017 0,00021
0.0017 o.0001g
0.0017 0.00029
0.0017 0.00035
0.0017 0.00024
0.0017 0.00045
0.0017 0.00033
0.10 0.029
Limits 26-129 31-122
Spike LCS LCS
Unit mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
D
TestAmerica Job ID: 400-132540-1
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338557
Prepared
01/16/17 09:24
01/16117 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01116/17 09:24
01 /16/17 09:24
01 /16/17 09:24
01/16/17 09:24
.01116/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
01/16/17 09:24
Analyzed
01/17/17 19:18
01/17/17 19:18
01/17/17 19:18
01/17/1719:18
01117117 19:18
01/17/17 19:18
01/17/1719:18
01/17/1719:18
01/17/17 19:18
01/17/1719:18
01/17/1719:18
01/17/1719:18
01/17/17 19:18
01/17/17 19:18
01/17/17 19:18
01/17/17 19:18
01/17/17 19:18
01/17/1719:18
01/17/1719:18
01/17/17 19:18
01/17/1719:18
Oil Fae
1
1
Prepared Analyzed DI/ Fae
01116117 09:24 0111711719:18 1 011161.17 09:24 0111711719:18 1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep flatch: 338557 %Rec.
An~lyte Added Result Qualifier Unit D 1%Rec Limits Aldrin
alpha-BHC beta-BHC delta-BHC gamma-BHC (lindane)
alpha-Chlordane
gamma·Chtordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Die!drin
Endosulfan I
Endosulfan II Endosulfan sulfate
Endrin
Endrfn aldehyde
Endrfn ketone
0.0333 0.0452
0.0333 0.0291
0.0333 0.0325
0.0333 0.0328
0.0333 0.0288
0.0333 0.0327
0.0333 0.0330
0.0333 0.0343
0.0333 0.0392
0.0333 0.0353
0.0333 0.0398
0.0333 0.0324
0.0333 0.0353
0.0333 0.0303
0.0333 0.0335
0.0333 0.0345
0.0333 0.0313
Page 104of140
mg/Kg 136 47 -137
mg/Kg 87 50-148
mg/Kg 98 46-133
mg/Kg 98 10-162
mg/Kg 86 50-148
mg/Kg 98 35.134
mg/Kg 99 39-146 mg/Kg 103 46.152
n1g/Kg 118 49-148
mg/Kg 106 44 -168 mg/Kg 119 41-164
mg/Kg 97 50-141
mg/Kg 106 47 -148
mg/Kg 91 50 -145
mg/Kg 100 45-159
mg/Kg 103 10.190
mg/Kg 94 48-159
T estAmerica Pensacola
2/112017
QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Method: 8081 B • Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCS 400.338557/9-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 338801 Prep Batch: 338557
Spike LCS LCS %Rec. ·Analyte Added Result Qualifier Unit D o/oRec Limits HePt8ch.lor 0.0333 0.0292 mg/Kg 87 46-158 Heptachlor epoxide 0.0333 0.0330 mg/Kg 99 49-148 Methoxych!or 0.0333 0.0329 mg/Kg 99 40.164
LCS LCS B Surrogate %Recovery Quafifier Limits
DCB Decachlorobiphenyl 86 26-129 Tetrachforo-1n-xylene 85 31-122
Lab.Sample ID: 400.132588.6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 338801 Prep Batch: 338557
Sample Sample Spike MS MS 0/oRec. Analyte Result Qualifier Added Result Qualifier Unit D 0/oRec Limits Aldrin <0.0024 0.0681 0.0735 mg/Kg
,, 1b8 10-154 alpha-BHC <0.00096 0.0681 0.0548 mg/Kg " 80 15-152 beta-BHC <0.0020 0.0681 0.0625 mg/Kg " 92 10.160 della-BHC <0.0013 0.0681 0.0612 mg/Kg " 90 10-160 gamma-BHC (Lindane) <0.00088 0.0681 0.0521 mg/Kg i) 77 26-142 alpha-Chlordane 0.0014 J 0.0681 0.0714 mg/Kg " 103 10-160 gamma-Chlordane 0.0025 J 0.0681 0.0718 mg/Kg " 102 10-160 4,4'-DDD <0.00076 0.0681 0.0694 mg/Kg :l;l 102 13-146 4,4'-DDE <0.0011 0.0681 0.0799 mg/Kg " 117 23-143
4,4'-DDT <0.0031 0.0681 0.0685 mg/Kg " 101 10-160
Die!drln <0.0014 0.0681 0.0649 mg/Kg " 95 10-160 Endosulfan I <0.00084 0.0681 0.0593 mg/Kg ·.t;t 87 10.160
Endosu!fan II <0.00092 0.0681 0.0736 mg/Kg ,, 108 10-160 Endosulfan sulfate <0.00084 0.0681 0.0591 mg/Kg " 87 27 -143 Endrln <0.00076 0.0681 0.0659 mg/Kg " 97 20-156 Endrln aldehyde <0.0012 0.0681 0.0611 mg/Kg i) 90 14-160 Endrin ketone <0.0014 0.0681 0.0618 mg/Kg " 91 31.155
Heptachlor <0.00096 0.0681 0.0539 mg/Kg " 79 10-160 ,Hept~chlor epoxide <0.0018 0.0681 0.0655 mg/Kg " 96 10-160 Methoxychtor <0.0013 0.0681 0.0610 mg/Kg ~;; 90 10-160
MS MS Surrogate %Recovery Quaflfler Limits DCB Decachlorobiphenyl 81 26-129 Tetrachloro~tn-xylene 83 31-122
Lab Sample ID: 400'132586·6 MSD Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 336801 Prep Batch: 338557
Sample Sarnple Spike MSD MSD 0/oRec. RPO Analyte Result Qualifier Added Result Qualifier Unit D o/oRec Limits RPO Limit
Aldrin <0.0024 0.0681 0.0665 mg/Kg -l~ 98 10 .154 10 60 alpha-BHC <0.00096 0.0681 0.0539 mg/Kg " 79 15-152 2 60 bela-BHC <0.0020 0.0681 0.0552 mg/Kg " 81 10-160 12 60 delta-BHC <0.0013 0.0681 0.0530 mg/Kg " 78 10-160 14 60 gamrna-BHC (Undane) <0.00088 0.0681 0.0489 mg/Kg " 72 26-142 6 60
TestAmerica Pensacola
Page 105 of 140 2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results
Method: SOS1B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: 400-132588-6 MSD Matrix: Solid Analysis Batch: 338801
MSD MSD Analyte alpha-Chlordane gamma-Chlordane 4,4'-DDD
4,4'-DDE 4,4'-DDT
Sample Result 0.0014
Sample
Qualifier J
Spike
Added
0.0681 0.0681 0.0681 0.0681
0.0681 0.0681
0.0681
0.0681 0.0681 0.0681 0.0681
0.0681 0.0681 0.0681
0.0681
Result Qualifier Unit
Die!drin Endosulfan I
Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde
Endrin ke~qne Heptachlor Heptachlor _epoxfde Methoxychlor
Surrogate
DCB Decachlorobiphenyl Tetrachloro-m-xylene
0.0025 J <0.00076
<O.Q011
<0.0031 <0.0014
<0.00084
<0.00092 <0.00084 <0.00076
<0.0012
<0.0014 <0.000.96
<0.00.18 <0.0013
MSO MSO
%Recovery Qualifier 61 68
Lab Sample ID: MB 400-33905411-A Matrix: Water Analysis .Batch: 339554
Analyte Aldrin
alpha-BHC
beta-BHC
df;llta-BHC
gamma-BHC (Undane) alpha~Chlordane
gamma~Ch!ordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
MB MB Result Qualifier
<0.00000030
<0.00000036
<0.00000030
<0.00000021
<0.0000025
<0.00000042
<0,00000032
<0.00000030
<0.00000022
<0.00000039
<0.00000030
<0.00000030
<0.00000074
0.0597 mg/Kg
Limits
26-129
31-122
0.0589 0.0617
0.0622 0.0528 0.0599
0.0525 0.0560
0.0481 0.0594 0.0518
0.0513 0.0486 0.0596
0.0480
RL MDL Unit
0.0000050 0.0000003 mg/L 0
0.0000050 0.0000003 mg/L 6
0.0000050 0.0000003 mg/L 0
0.0000050 0.0000002 mg/L 1
0.0000050 0.0000025 mg/L
0.0000050 0.0000004 mgll 2
0.0000050 0.0000003 mg/L 2
0.0000050 0.0000003 mg/L 0
0.0000050 0.0000002 mg/L 2
0.0000050 0.0000003 mg/L 9
0.0000050 0.0000003 mg/L 0
0.0000050 0.0000003 mg/L 0
0.0000050 0.0000007 mg/L 4
Page 106of140
mg/Kg mg/Kg
mg/Kg
mg/Kg n1g/Kg
mg/Kg mg/Kg
mg/Kg mg/Kg mg/Kg
mg/Kg mg/Kg
mg/Kg
mg/Kg
TestAmerica Job ID: 400-132540-1
Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338557 %Rec. RPO
D o/cRec Limits RPO Limit
" 86 10-160 16 60 83 10-160 91 13-146
91 23-143 78 10.160 88 10-160 77 10.160 82 10.160
71 27-143 87 20-156
76 14-160
75 31-155 71 10.160
87 10-160 70 10.160
20 12
25 26 8
12
27 20 10 17
19 10 9
24
60 88
86
43 E 60 60
49 60 60 37
60 60 60
47
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339054
0 Prepared Analyzed 011 Fae b1ii9i1i10:03 01124117 11:48 1
0111911710:03 01/24/1711:48
0111911710:03 01124/1711:48
01119/1710:03 01124/17 11:48
01/1911710:03 01/24/1711:48
01/1911710:03 01124/17 11:48
01/19/1710:03 01/24/1711:48
01/19/1710:03 01124/1711:48
01/19/1710:03 01/24117 11:48
01/19/1710:03 01124/1711:48
01/19/1710:03 0112411711:48
01119/1710:03 0112411711:48
01119/1710:03 0112411711:48
TestAmerica Pensacola
2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results
Method: 80818 • Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: MB 400-33905411-A Matrix: Water Analysis Batch: 339554
MB MB
Analyte Result Qualifier RL MDL
Endosulfan sulfate <0.00000021 0.0000050 0.0000002 1
Endrin <0.00000030 0.0000050 0.0000003 0
Endrin aldehyde <0.00000028 0.0000050 0.0000002 8
Endrin ketone <0.00000038 0.0000050 0.0000003 8
Heptachlor <0.00000031 0.0000050 0.0000003 1
Heptachlor epoxlde <0.00000032 0.0000050 0.0000003 2
Methoxychlor <0.00000041 0.0000050 0.0000004 1
Toxaphene <0.000030 0.00030 0.000030
MB MB Surrogate %Recovery Qua/Iller Limits
DCB Decachlorobiphenyl 93 10. 130
Tetrachloro-m-xylene 69 43-130
Lab Sample ID: LCS 400-339054/2-A Matrix: Water Analysis Batch: 339554
Spike LCS LCS
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Analyte Added Result Qualifier
Aldrln 0.000500 0.000398 alpha-BHC 0.000500 0.000408 beta-BHC 0.000500 0.000367 delta-BHC 0.000500 0.000446 gamma-BHC (Undane) 0.000500 0.000394 alpha-Chlordane 0.000500 0.000391 gamma-Chlordane 0.000500 0.000422 4,4'-DDD 0.000500 0.000421 4,4'-DDE 0.000500 0.000505 4,4'-DDT 0.000500 0.000387 Dieldrin 0.000500 0.000440 Endosulfan I 0.000500 0.000422 Endosu!fan IJ 0.000500 0.000396 Endosulfan sulfate 0.000500 0.000368 Endrln 0.000500 0.000418 Endr!n aldehyde 0.000500 0.000353 Endrin ketone 0.000500 0.000363
Heptachlor 0.000500 0.000348 Heptachlor epoxide 0.000500 0.000418 Methoxychlor 0.000500 0.000373
LOS LOS Surrogate %Recovery Quill/tier Limits
DCB Decac/1/orobiphenyl 53 10-130 Tetrac/1/oro·m·xylene 77 43.130
Page 107of140
TestAmerica Job ID: 400-132540-1
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339054
D Prepared Analyzed Dll Fae
01119117 10:03 01124117 11:48 1
01119/1710:03 01/24/1711:48
01/1911710:03 01/2411711:48 1 E 01119/1710:03 01/24/1711:48
01/19/17 10:03 01/2411711:48
0111911710:03 01/2411711:48
0111911710:03 0112411711:48
01119/17 10:03 0112411711:48
Prepared Analyzed DI/ Fae 0111911710:03 0112411711:48 1 0111911710:03 0112411711:48
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 339054 D/oRec.
Unit D 0/oRac Limits
mg/L 80 52 -150 mg/L 82 50.150
mg/L 73 58.-150
mg/L 89 42-150 mg/L 79 53-150 mg/L 78 63 -150
mg/L 84 62 -150 mg/L 84 58 -150 mg/L 101 65 -150
mg/L 77 59 -150 mg/L 88 64 -150 mg/L 84 40.127
mg/L 79 40.135
mg/L 74 50 -150
mg/L 84 63-150 mg/L 71 40 -150 mg/L 73 52 .150
mg/L 70 59.150
mg/L 84 63 .150 mg/L 75 57 -150
TestAmerica Pensacola
2/1/2017
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results
Method: 808113 - Organochlorine Pesticides (GC) (Continued)
TestAmerica Job ID: 400-132540-1
Lab Sample ID: LCSD 400·339054/3·A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 339554 Prep Batch: 339054
Spike LCSD LCSD 0/oRec. RPO
Analyte Added Result Qualifier Unit D o/oRec Limits RPO Lirnlt Aldrin 0.000500 0.000403 mg/L 81 52-150 40 alpha-BHC 0.000500 0.000412 mg IL 82 50-150 40 beta-BHC 0.000500 0.000402 mg IL 80 58-150 9 40 delta-BHC 0.000500 0.000457 mg IL 91 42-150 3 40 gamma-BHC (Lindane) 0.000500 0.000412 mg/L 82 53-150 4 40 alpha-Chlordane 0.000500 0.000414 mg IL 83 63-150 6 40 gamma-Chlordane 0.000500 0.000450 n1g/L 90 62-150 6 40
4.4'-DDD 0.000500 0.000454 mg/L 91 58-150 8 40 4.4'-DDE 0.000500 0.000500 mg IL 100 65-150 40
4,4'.DDT 0.000500 0.000417 mg IL 83 59-150 7 40
Dieldrin 0.000500 0.000472 mgll 94 64-150 7 40
Endosulfan l 0.000500 0.000447 mglL 89 40-127 6 40 Endosulfan II 0.000500 0.000429 mg/L 86 40-135 8 40 Endosu!fan sulfate 0.000500 0.000395 mg IL 79 50-150 7 40
Endrin 0.000500 0.000453 mg/L 91 63 .150 8 40
Endrin aldehyde 0.000500 0.000387 mg/L 77 40-150 9 40
Endrin ketone 0.000500 0.000386 mglL 77 52.150 6 40
Heptach!or 0.000500 0.000373 mgll 75 59-150 7 40
Heptachlor epoxide 0.000500 0.000440 mglL 88 63-150 5 40 Methoxychlor 0.000500 0.000385 mg/L 77 57 .150 3 40
LCSD LCSD Surrogate %Recovery Qualifier' Limits DCB lJecachforobiphenyi 106 10·~ 130
Tetrachloro-m-xylene 68 43-130
Method: MA-EPH - Massachusetts • Extractable Petroleum Hydrocarbons (GC)
Lab Sample ID: MB.400·339010/16-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 339632 Prep Batch: 339010
MB MB Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed 011 Fae C10-C12 Aliphatics <1.6 1.6 1.6 mg/Kg 01119117 07:20 01/2411717:14 1 C12~C16 Aliphatics <1.6 1.6 1.6 mg/Kg 01119/17 07:20 0112411717:14
C16-C35 Aliphatics <1.6 1.6 1.6 mg/Kg 01119117 07:20 0112411717:14
MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed DI/ Fae 1-Cl1forooctadecane 95 40-140 01119117 07:20 0112411717:14 1
Lab Sample ID: MB 400-339010/16-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 339633 Prep Batch: 339010
MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae c10-c12 Aromatics <1.6 1.6 1.6 mg/Kg 01119/17 07:20 01124117 21:26 1 C12-C16 Aromatics <1.6 1.6 1.6 mg/Kg 01/19117 07:20 01124117 21:26
C21-C35 Aromatics <1.6 1.6 1.6 mg/Kg 01119117 07:20 01124117 21:26
TestAmerica Pensacola
Page 108of140 2/112017
m
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: MA-EPH - Massachw:;etts - Extractable Petroleum Hyctrncarbons {GC) (Continued)
Lab Sample ID: MB 400-339010/16-A Matrix: Solid Analysis Batch: 339633
MB MB
Analyte Result Qualifier
C16-C21 Aromatics <1.6
MB MB Surrogate %Recovery Qualifier o-Terphenyl 83
Lab Sample ID: LCS 400-339010/14-A Matrix: Solid Analysis Batch: 339632
Analyte
C9-C18 Aliphatics
C19-C36 A!lphatics
'Surrogate 1-Chlorooctadecane
LCS LCS %Recovery Quallfler
98
Lab Sample ID: LCS 400-339010/14-A Matrix: Solid Analysis Batch: 339633
Analyte C11-C22 Aromatics
Surrogate o-Terphenyl
LCS LCS %Recovery Qualifier
123
Lab Sample ID: LCSD 400-339010/15.-A Matrix: Solid Analysis Batch: 339632
Analyte C9-C18 Aliphatics
C19·C36 Aliphatics
Surrogate 1-Ch!orooctadecane
LCSD LCSD %Recovery Qualifier
106
Lab Sample ID: LCSD 400-339010/15-A Matrix: Solid Analysis Batch: 339633
Analyte C11-C22 Aromatics
surrogate
O:.ierriHenYl
LCSD LCSD %Recovery Qualifier
118
RL 1.6
Limits 40-140
Spike
Add.ed
20.0 26.6
Llrnlts
40 • .140
Spike
Added 56.6
Limits 40-140
Spike
Added 19.9
26.5
Limits 40 -1.40
Spike
Added 56.4
Ll1nlts
4o:T46
MDL Unit 1.6 mg/Kg
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339010
0 Prepared Analyzed OJI Fae 01119/17 07:20 01/24/17 21:26 . 1
Prepared Analyzed
01119117 07:20 01124117 21:26 Dlf Fae
1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 339010
LCS LCS 0/oRec.
Result Qualifier Unit D 0;11Rec Lilnlts 10.5 mg/Kg 53 40-140 24.4 mg/Kg 92 40-140
Client Sample ID: Lab Control Sample
LCS
Result 65.0
LCSO
Result 11.4 26]
Prep Type: Total/NA Prep Batch: 339010
LCS 0/oRec. Qualifier Unit D o/oRec Limits
mg/Kg 115 40-140
Client Sample ID: Lab Control Sample Oup Prep Type: To.tal/NA Prep Batch: 339010
LCSD o/oRec. RPO Qualifier Unit D 11/oRec Lhnlts RPO Limit
mg/Kg 57 40.140 9 50 mg/Kg 100 40-140 9 50
Client Sample ID: Lab Control Sample Dup Prep Type: Total/N.A Prep Batch: 339010
LCSD LCSD %1Rec. RPO
Res_ult Qualifier Unit D 0/oRec Limits RPO Limit 62.8 mg/Kg 111 40-140 4 50
TestAmerica Pensacola
Page 109of140 2/1/2017
Client: C-K Associates Project/Site: Moffat & Nicl1ol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: MA-EPH • Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Lab Sample ID: 400·132588·6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 339632 Prep Batch: 339010
Sample Sample Spike MS MS OfoRec. Aoalyte Result Qualifier Added Result Qualifier Unit 0 0/aRec Limits C19-C36 Aliphatics 12 54.7 70.5 mg/Kg ;:;; 108 40-140
C9-C18 Al!phatics <3.3 41.0 20.2 mg/Kg ;;r 49 40-140
MS MS
Surrogate %Recovery Qualifier Limits 1-Chlorooctadecane 88 40-140
Lab Sample ID: 400·132588-6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 339633 Prep Batch: 339010
Sample Sample Spike MS MS 0/oRec.
Analyte Result Qualifier Added Result Qualifier Unit 0 o/oRec Limits
C11-C22 Aromatics <6.1 116 142 mg/Kg n 123 40-140
MS MS
Surrogate %Recovery Qualifier Limits o-Ter{>h'eriyl 86 40-140
Lab Sample JD: 400·.132588·6 MSD Client Sample ID: CK-5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 339632 Prep Batch: 339010
Sample Sample Spike MSO MSD 0/nRec. RPO
Analyte Result Qualifier Added Result Qualifier Unit D 'Yo Rec Limits RPO Limit
C19-C36 Aliphatics 12 54.1 61.4 mg!Kg {( 92 40-140 14 50
C9-C18 Aliphatics <3.3 40.6 20.0 mg/Kg ·t:I 49 40-140 50
MSD MSD
Surrogate %Recovery Qualifier Limits
1-Chlorooctadecane 82 40.140
Lab Sample ID: 400·132588·6 MSD Client Sample 10: CK·5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 339633 Prep Batch: 339010
Sample Sample Spike MSO MSD o/oRec. RPO
Analyte Result Qualifier Added Result Qualifier Unit D o/oRec 1-lmlts RPO Limit
C11-C22 Aromatics <6.1 115 119 mg/Kg ~:i 103 40-140 18 so MSD MSD
Surrogate %Recovery Qualifier Limits o-Terpheny/ 9g 40-140
Lab Sample ID: MB 400-339262/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 339948 Prep Batch: 339262
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
C10-C12Aliphatics <0.050 0.050 0.050 mg/L 0112011715:54 0112611716:56 1
C12-C16 Aliphallcs <0.050 0.050 0.050 mg/L 01120/1715:54 01126117 16:56
C16-C35 Allphatics <0.050 0.050 0.050 mg/L 0112011715:54 0112611716:56
TestAmerica Pensacola
Page 110 of 140 2/1/2017
B
Client: C-K Associates Project/Site: Moffat & Nichol
QC Sample Results TestAmerica Job ID: 400-132540-1
Method: MA-EPH ~Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Lab Sample ID: MB 400-33926211 ·A Matrix: Water Analysis Batch: 339948
Surrogate
1-ChlorOoctadecane
MB MB %Recovery Qualifier
79
Lab Sample ID: MB 400-33926211-A Matrix: Water Analysis Batch: 339950
MB
Analyte Result
C10-C12 Aromatics <0.050 C12-C16 Aromatics <D.050
C21-C35 Aromatics <0.050 C16-C21 Aromatics <0.050
MB Surrogate %Recovery o-Terphenyi 73 2-Bromonaphthalene 57
2-Fluorobiphenyl 119
Lab Sample ID: LCS 400-33926212-A Matrix: Water Analysis Batch: 339948
Analyte
C9-C18 Allphatics
C19-C36 Aliphatics
MB
Qualifier
MB Qualifier
Surrogate f.·Chloroociadecane
LCS LCS
%Recovery Qualifier 84
Lab Sample ID: LCS 400-339262/2-A Matrix: Water Analysis Batch: 339950
Analyte C11-C22_Aromatics
Surrogate
o-Terpheny/ 2-Bromonaphthalene 2-Fluorobiphenyl
LCS LCS %Recovery Qualifier
85 50
121
Lab Sample ID: LCSD 400·339262/3-A Matrix: Water Analysis Batch: 339948
Aoalyte C9'C18 Aliphatics
C19·C36 Aliphatics
Limits 40.140
RL
0.050 0.050
0.050 0.050
Limits 40.140
40 •. 140
40.140
Spike
Added
0.300 0.400
Limits 40.140
Spike
Added 0.850
Limits 40-140
40-140
40.140
MDL Unit 0.050 mg/L 0.050 mg/L
0.050 mg/L
0.050 mg/L
LCS LCS
Result Qualifier 0.199
0.317
LCS LCS
Result Qualifier 0.701
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339262
Prepared Analyzed Dll Fae 01120117 15:54 0112611716:56 1
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339262
D Prepared Analyzed Dll Fae 01/20/17 15:54 01/26/17 19:30 01/20/1715:54 01126/17 19:30
01/20/17 15:54 01/26/1719:30 01/20/17 15:54 01/26/1719:30
Prepared Analyzed Dll Fae 0112011715:54 0112611719:30 1
0112011715:54 01126117 19:30
01120117 15:54 0112611719:30
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 339262 o/oRec.
Unit D 0/oRec Lhnlts mg/L 66 40 .140
mg/L 79 40 -140
Client Sample ID: Lab Control Sample Prep Type; Total/NA Prep Batch: 339262 o/oRec.
Unit D 0/oRec Limits
mg/L 82 40.140
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Bati;h:. 339262
Spike LCSD LCSD 0/oRec. RPO Added Result Ouallfler Unit D %Rec Limits RPO Limit
0.300 0.274 mg/L 91 40.140 32 50 0.400 0.331 mg/L 83 40.140 4 50
TestAmerica Pensacola
Page 111 of140 2/1/2017
B
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Method: 6010C - Metals (ICP) (Continued)
Lab Sample ID: LCS 400-338333/2-A Matrix: Water Analysis Batch: 338689
-Analyte
Lead
Selenium Thallium Vanadium
· Zinc
Lab Sample ID: MB 400·338440/1 ·A Matrix: Solid Analysis Balch: 338689
MB MB Result Qualifier
<0.20
<D.40
<0.20
Spike
Added
1.00
1.00 1.00
1.00 1.00
LCS
Result 1.01
0.986 0.995
1.04 1.04
LCS
Qualifier
MDL Unit
0.20 mg/Kg
0.40 mg/Kg
0.20 mg/Kg
TestAmerica Job ID: 400-132540-1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338333 o/oRec.
Unit D o/eRec Limits mg/L 101 80-120
mg/L 99 80-120 mg/L 99 80.120
mg/L 104 80.120
mg/L 104 80-120
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338440
D Prepared Analyzed DU Fae 01115/1711:30 01/16/1715:32 1 01/15/1711:30 01/16/17 15:32
01/15/1711:30 01116/17 15:32
Analyte Silver -Arsenic
Barium Beryllium Cobalt
Chromium Copper
Nickel Lead
Selenium Thallium Vanadium Zinc
<0.099
RL 0.50
0.99 0.99 0.30 0.99
0.99 2.0
0.099 mg/Kg 01/15/1711:30 01/16/1715:32 <0.30
<0.20 <0.20
<0.30
<0.20
<0.40 <0.40
<0.30
<D.79
Lab Sample ID: LCS 400-338440/2-A Matrix: Solid Analysis Batch: 338689
Analyt_e Silver
Arsenic Barium Berymum Cobalt
Chromium Copper Nickel
Lead
Selenium Thallium
Vanadium Zinc
Spike
Added
49.7
99.4 99.4 49.7
99.4 99.4 99.4 99.4
99.4
99.4 99.4
99.4
99.4
0.50
0.99
2.0 0.99
2.0
2.0
LCS
Result
51.5
104
107 53.4
101
107 105
103 101
99.4 99.6
107 105
Page 113 of 140
0.30 mg/Kg 01/15/1711:30 01/16/17 15:32
0.20 mg/Kg 01/15/1711:30 01/16/17 15:32 0.20 mg/Kg 01/15/1711:30 01/16/1715:32
0.30 mg/Kg 01/15/1711:30 01/16/17 15:32
0.20 mg/Kg 01/15/1711:30 01/16/17 15:32
0.40 mg/Kg 01/15/1711:30 01/16/17 15:32
0.40 mg/Kg 01115/17 11 :30 01/16/1715:32
0.30 mg/Kg 01/15/1711:30 01/16/17 15:32
0.79 mg/Kg 01/15/1711:30 01/16/17 15:32
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338440
LCS o/oRec. Qualifier_ Unit D 0/oRec Limits
mg/Kg 104 80-120 mg/Kg 105 80-120 mg/Kg 108 80-120 mg/Kg 107 80-120 mg/Kg 102 80-120 mg/Kg 107 80-120 mg/Kg 106 80-120 mg/Kg 104 80-120 mg/Kg 102 80.120 mg/Kg 100 80-120 mg/Kg 100 80-120
mg/Kg 107 80-120 mg/Kg 106 80-120
TestAmerica Pensacola
2/1/2017
E
QC Sample Results Client: C-K Associates Projecl/Site: Moffat & Nichol
Method: 6010C. Metals (ICP) {Continued)
Lab Sample ID: 400-132588-6 MS Matrix: Solid Analysis Batch: 338689
Analyte
Silver Arsenic Barium Beryllium Cobalt Chromium Copper
Nickel Lead Selenium
Thamum Vanadium Zinc
Sample Sample
Result Qualifier
<0.37 12
120 0.33 J
4.8 26
44
12 64
1.3 J <0.74
14 150
Lab Sample ID: 400-132588-6.MSD Matrix: Solid Analysis Batch: 338689
Analyte Silver Arsenic Barium Beryllium Cobalt Chromium Copper
Nickel Lead
Selenium Tham um Vanadium Zinc
Sample Sample
Result Qualifier <0.-37
12
120 0.33 J
4.8 26 44
12 64 1.3 J
<0.74
14 150
Lab Sample ID; MB 400-338528/1-A Matrix: Solid Analysis Batch: 338847
Analyte
Silver Arsenic
Barium Beryllium Cobalt Chromium Copper
Nickel Lead
Selenium
MB MB Result Qualifier
<0.19
<0.39 <0.19
<0.097
<0.29
<0.19
<0.19
<0.29 <0,19
<0.39
Spike
Added 93.6 187
187 93.6
187 187
187
187 187
187 187
187 187
Spike
Added 93.5 187
187 93.5
187 187 187
187 187 187
187 187 187
RL 0.49 0.97 0.97
0.29
0.97 0.97
1.9 0.49 0.97
1.9
MS MS
Result Qualifier
94.4 202
304 96.9
198 217 243
208 253
184
186
210 325
MSD MSD
Unit mg/Kg
mg/Kg
mg/Kg mg/Kg
mg/Kg mg/Kg mg/Kg
mg/Kg mg/Kg
mg/Kg mg/Kg
n1g/Kg mg/Kg
Result Qualifier Unit 93.4 mg/Kg 198 mg/Kg
299 mg/Kg
95.9 mg/Kg
195 mg/Kg 212 mg/Kg
234 mg/Kg
205 mg/Kg 244 mg/Kg 180 mg/Kg
185 mg/Kg
208 mg/Kg 343 mg/Kg
MDL Unit 0.19 mg/Kg 0.39 mg/Kg
0.19 mg/Kg 0.097 mg/Kg
0.29 mg/Kg 0.19 mg/Kg
0.19 mg/Kg 0.29 mg/Kg 0.19 mg/Kg 0.39 mg/Kg
Page 114 of 140
TestAmerica Job ID: 400-132540-1
Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338440 o/oRec.
0 o/oRec Llrnits l.\ 101 75-125
" 101 75-125 l) 101 75-125 l) 103 75 .125 ,, 103 75-125
" 102 75-125 ;;1 106 75-125
l) 105 75-125
" 101 75-125
" 97 75-125 l) 99 75-125
'~ 105 75-125
" 92 75-125
Client Sample ID: CK-5 Prep Type: Total/NA Prep Batch: 338440 O/oRec. RPO
D 0/oRec Llrnits <1 100 75-125
RPO Limit
20 " 100 75-125 2 20
" 98 75-125 2 20 i:1 102 75-125 20 ;;1 102 75-125 1 20 u 99 75-125 2 20
" 102 75-125 4 20 1:1 103 75-125 1 20 " 96 75-125 4 20 l) 95 75-125 2 20 l) 99 75-125 20 ,, 104 75-125 1 20 " 101 75-125 5 20
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338528
0 Prepared Analyzed Oil Fae
01116/17 08:55 01/17/1712:45 1 01/16/17 08:55 01/17/1712:45
01/W17 08:55 01/17117 12:45
01/16/17 08:55 01/17/17 12:45 01/16/17 08:55 01/17/1712:45 01/16/17 08:55 01/17/17 12:45
01/16/17 08:55 01/17/17 12:45
01/16/17 08:55 01/17/17 12:45 01/16/17 08:55 01/17/17 12:45 01/16117 08;55 01117/1712:45
TestAmerica Pensacola
2/1/2017
QC Sample Results Client: C-K Associates TestAmerica Job JD: 400-132540-1 Project/Site: Moffat & Nichol
Method: 6010C - Metals (ICP) (Continued)
Lab Sample ID: MB 400-338528/1-A Client Sample JD: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 338847 Prep Batch: 338528
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Thallium <0.39 0.97 0.39 mg/Kg 01/16/17 08:55 01/17/17 12:45 1 Vanadium <0.2~ 1.9 0.29 mg/Kg 01/16/17 08:55 01/17/1712:45
Zinc <0.78 1.9 0.78 mg/Kg 01/16/17 08:55 01/17/17 12:45
Lab Sample ID: LCS 400·338528i2·A Client Sample ID: Lab Control Sample E Matrix: Solid Prep Type: Total/NA Analysis Batch: 338847 Prep Batch: 338528
Spike LCS LCS o/oRec.
Analyte Added Result Qualifier Unit D 0/oRec Limits
Silver 48.4 50.5 mg/Kg 104 80 -120 Arsenic 96.8 102 mg/Kg 105 80.120
Barium 96.8 105 mg/Kg 108 80.120
Beryllium 48.4 52.4 mg/Kg 108 80.120
Cobalt 96.8 99.7 mg/Kg 103. 80-120 Chromium 96.8 104 mg/Kg 107 80.120
Copper 96.8 103 mg/Kg 107 80.120
Nickel 96.8 101 mg/Kg 104 80.120 Lead 96.8 99.8 mg/Kg 103 80.120
Selenium 96.8 97.8 mg/Kg 101 80 .120
Thallium 96.8 99.4 mg/Kg 103 80.120
Vanadium 96.8 104 mg/Kg 108 80.120
Zinc 96.8 103 mg/Kg 106 80.120
Lab Sample ID: 400·132650·1 MS Client Sample ID: CK-6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 338847 Prep Batch: 338528
Sample Sample Spike MS MS o/11Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits
Silver <0.35 88.3 88.9 mg/Kg " 101 75.125
Arsenic 7.1 177 180 mg/Kg ,,
98 75 .125
Bariwn 87 F1 177 313 F1 mg/Kg J~ 128 75.125
Beryllium 0.37 J 88.3 89.9 mg/Kg " 101 75 .125
Cobalt 4.1 177 187 mg/Kg i'.l 104 75-125
Chromium 11 177 190 mg/Kg ~:1 101 75 .125
Copper 37 177 207 mg/Kg i;i 96 75.125
Nickel 12 177 195 mg/Kg ,, 104 75 .125
Lead 42 177 242 mg/Kg " 113 75.125
Selenium 0.87 J 177 169 mg/Kg ·1:1 95 75 .125
Thallium <0.71 177 178 mg/Kg 1~ 101 75.125
Vanadium 11 177 197 mg/Kg " 105 75 .125
Zinc 130 177 267 mg/Kg " 80 75.125
Lab Sample ID: 400·132650·1 MSD Client Sample ID: CK·6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 338847 Prep Batch: 338528
Sarnple Sample Spike MSD MSD o/aRec. RPO
Analyte Result Qualifier Added Result Qualifier Unit D (l/oRec Limits RPO Limit
Silver <0.35 88.9 89.3 mg/Kg j) 100 75 .125 0 20 Arsenic 7.1 178 183 mg/Kg ,, 99 75 .125 2 20
Tes!America Pensacola
Page 115of140 2/1/2017
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Method: 6010C ·Metals (ICP) (Continued)
Lab Sample ID: 400-132650-1 MSD Matrix: Solid Analysis Batch: 338847
Analyte Barium Beryllium
Cobalt
Chroinium
Copper
Nickel
Lead
Selenium Thallium
Vanadiun1 Zinc
Sample Sample
Result Qualifier 87 F1
0.37 J 4.1
11
37 12
42 0.87 J
<0.71
11
130
Lab Sample ID: MB 400-33889311-A Matrix: Water Analysis Batch: 339167
Analyte
Silver
Arsenic
Barium
Beryllium
Cobalt
Chromium
Copper
Nickel
Lead
Selenium
Thallium
Vanadium
Zinc
MB MB Result Qualifier
<0.0020
<0.0040
<0.0020
<0.0010 <0.0030 <0.0020
<0.0020 <0.0030
<0.0020 <0.0040
<0.0040 <0.0030
<0.0080
Lab Sample ID: LCS 400-338893/2-A Matrix: Water Analysis Batch: 339167
Analyte Silver
Arsenic
Barium Beryllium Cobalt
Chromium
Copper
Nickel
Lead
Se!enlum
ThatHum Vanadiurn
Zinc
Spike
Added
178
88.9 178
178
178 178 178
178
178 178
178
RL 0.0050
0.010 0.010
0.0030 0.010 0.010
0.020 0.0050
0.010 0.020
0.010 0.020
0.020
Spike
Added a.sod
1.00
1.00 0.500
1.00
1.00
1.00 1.00
1.00 1.00
1.00 1.00
1.00
MSD MSD
Result Qualifier Unit 316 F1 mg/kg
91.1 mg/Kg
189 mg/Kg
192
249 197
219
174 179 198 264
MDL Unit 0.0020 mg/L
0.0040 mg/L
0.0020 mg/L
0.0010 mg/L
0.0030 mg/l
0.0020 mg/L
0.0020 mg/L
0.0030 mg/L
0.0020 mg/L
0.0040 mg/L
0.0040 mg/L
0.0030 mg/L
0.0080 mg/l
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
TestAmerica Job ID: 400-132540-1
Client Sample ID: CK-6 Prep Type; Total/NA Prep Batch: 338528 %Rec. RPO
D 0/oRec Limits RPO Limit
" 129 75-125 20 " 102 75-125 ;/ 104 75-125 ,, 102 75-125
" 119 75-125 ::i 104 75-125
"' 99 75-125
" 97 75-125 !;1: 101 75-125 l) 105 75-125
78 75-125
19
10
3
20 20
20
20 E 20 20
20
20 20
20
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338893
O Prepared Analyzed Oil Fae 01/18/1710:09 01/19/1715:39 1 01118/1710:09 01/19/17 15:39
01118/1710:09 01/19/1715:39
01118/1710:09 01/19/1715:39 01/18/1710:09 01/19/1715:39
01118/1710:09 01/19/1715:39
01118/1710:09 01/19/1715:39 01/18/1710:09 01/19/1715:39
01118/17 10:09 01/19/1715:39
01118/1710:09 01/19/1715:39
01118/1710:09 01/19/1715:39 01/18/17 10:09 01/19/17 15:39 01/18/1710:09 01/19/1715:39
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep B:itch: 338893
LCS LCS
Result Qualifier Unit 0.499 mg/L
1.03
1.05 0.526 0.999
1.04 1.03 1.03 1.01
0.988 1.00 1.04 1.03
mg/l
mg/L
mg/l
mg/L
mg/L
mg/L
mg IL
mg/L
mg/L
mg IL mg/L
mg/L
0 °/oRec 100
0/oRec.
Limits
80-120 103 80-120 105 80-120
105 80-120 100 80-120
104 80-120
103 80-120 103 80-120
101 80-120
99 80-120 100 80-120 104 80-120
103 80-120
TestAmerica Pensacola
Page 116of140 21112017
QC Sample Results Client: C-K Associates Projecl/Site: Moffat & Nichol
Method: 7470A ·Mercury (CVAA)
Lab Sample ID: MB 400-337923/14-A Matrix: Water Analysis Batch: 338420
MB MB Analyte
Mercury Result Qualifier
<0.000070
Lab Sample ID: LCS 400-337923/15-A Matrix: Waler Analysis Balch: 338420
Analyte Mercury
Lab Sample ID: MB 400-338653/14-A Matrix: Water Analysis Batch: 338941
MB MB Analyte
Mercury Result Qualifier
<0.000070
Lab Sample ID: LCS 400-338653/15-A Matrix: Water Analysis Batch: 338941
Analyte
Mercury
Method: 7471A ·Mercury (CVAA)
Lab Sample ID: MB 400·337950/14-A Matrix: Solid Analysis Balch: 338612
A_nalyte
Mercury
MB Mil Result _Quallfi_er
<0.0075
Lab sample ID: LCS 400-337950/15-A Matrix: Solid Analysis Batch: 3386.12
Analyte Mercury
Lab Sample ID: 400-132588'6 MS Matrix: Solid Analysis Batch: 338612
Analyte
Mercury
Sample Sample Result Qualifier 0.052
RL MDL Unit
TestAmerica Job ID: 400-132540-1
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 337923
D Prepared Analyzed Oil Fae 0.00020 0.000070 mg/L 01/13/17 08:15 01/13/1712:31 1
Spike
Added 0.00101
Client Sample ID: Lab Control Sample
LCS LCS
Result Qualifier Unit 0.000880 mg/L
RL MOL Unit
Prep Type: Total/NA 11!!1 Prep Batch: 337923 El o/oRec.
D 0/oRec Limits
87 80-120
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338653
D Prepared Analyzed 011.Fac 0.00020 . 0.000070 mg/L b1116i1116:11 01/1811712:35 1
Spike
Added
0.00101
Spike
Added
0.0631
Spike
Added 0.131
RL Q.012
LCS LCS
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338653 %1Rec.
Result Qualifier Unit D %Rec Limits
0.()0110 mg/L
MOL Unit 0.0075 mg/Kg
109 80-120
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 337950
O Prepared Analyzed DH Fae 01/15/17 12:43 01116/17 09:21 1
LCS LCS
Client Sample ID: Lab C~mtrol sample Prep Type: Total/NA Prep Batch: 337950 0/oRec.
Result Qualifler Unit 0.0618 mg/Kg
MS MS Result Qualifier Unit 0.200 mg/Kg
D %Rec _Llo:iits 98 80-120
Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 337950 0/oRec.
O 0;0Rec Lltnlts
113 80-120
TestAmerica Pensacola
Page 117 of 140 2/1/2017
QC Sample Results Client: C-K Associates Projecl/Site: Moffat & Nichol
TestAmerica Job ID: 400-132540-1
Method: 7471A. Mercury (CVAA) (Continued)
Lab Sample ID: 400-132588-6 MSD Matrix: Solid Analysis Batch: 338612
Analyte
Mercury
Sa1nple Sample
Result Qualifier
0.052
Lab Sample ID: MB 400-338513/14-A Matrix: Solid Analysis Batch: 338612
MB MB Analyte Mercury
Result Qualifier
<0.0085
Lab Sample ID: LCS 400-338513/1 S·A Matrix: Solid Analysis Batch: 338612
Analyte tvfercury
Method: 335.2. Cyanide, Total
Lab Sample ID: MB 400-338793/1 ·A Matrix: Water Analysis Batch: 338792
MB MB Analyte Cyanide, Total
Result Qualifier <0.0035
Lab Sample ID: LCS 400-338793/2-A Matrix: Water Analysis Balch: 338792
Anatyte Cyanide, Total
Method: 353.2 - Nitrogen, Nitrate-Nitrite
Lab Sample ID: MB 400-338427/7 Matrix: Water Analysis Batch: 338427
Analyte Nitrate Nitrite as N
Lab Sample ID: LCS 400·338427/23 Matrix: Water Analysis Batch: 338427
Analyte Nitrate Nitrite as N
MB MB Result Qualifier .:::Q.018
Spike
Added 0.132
RL 0.014
Spike
Added 0.0709 .
RL 0.0050
Spike
Added 0.274
Spike
Added 0.500
RL o.oso
MSD MSD
Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 337950 WaRec. RPO
Result Qualifier Unit D o/aRec Limits RPO Limit 0.168 mg/Kg 89 80.120 17 20
MDL Unit 0.0085 mg/Kg
Client Sample ID: Method Blank Prep Type: Total/NA 11!1 Prep Batch: 338513 U
O Prepared Analyzed Oil Fae
01115/1712:43 01/16/1710:03 1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338513
LCS LCS o/oRec.
Result Qualifier Unit D o/oRec Limits
0~0688 mg/Kg 97 80-120
MDL Unit 0.0035 mg/L
LCS LCS
Client.Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 338793
D Prepared Analyzed Oil Fae 01117/17 09:30 Oi/17117 14:18 1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 338793 °!oRec.
Result Qualifier Unit
0.306 mg/L
D 0/ 0Rec Limits
112 1s-12s
MOL Unit 0.018 mg/L
Client Sample ID: Method Blank Prep Type: Total/NA
0 Prepared Analyzed Oil Fae 01/13/1713:24 1
Client Sample ID: Lab Control Sample Prep Type: Total/NA
LCS LCS
Result Qualifier Unit 0.498 mg/L
0/GRec. D %Rec Limits
100 90-110
TestAmerica Pensacola
Page 118of140 2/1/2017
QC Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol
Method: 353.2 • Nitrogen, Nitrate-Nitrite (Continued)
Lab Sample ID: MRL 400-33842716 Matrix: Water Analysis Batch: 338427
Analyte
Nitrate Nitrite as N
Lab Sample ID: MB 400-338579/14 Matrix: water Analysis Batch: 338579
Analyte
Nitrate Nitrite as N
Lab Sample ID: LCS 400-338579115 Matrix: Water Analysis Batch: 338579
Analyte NJfrafe-NHrne-as N
Lab .Sample ID: MRL 400·338579/13 Matrix: Water Analysis Batch: 338579
Analyte
Nitrate Nitrite as N
Lab Sample ID: MRL 400-338609/6 Matrix: Solid Analysis Batch: 338609
Analyle
Nitrate Nitrite as N
Lab Sample ID: MB 400-338576/1-A Matrix: Solid Analysis Batch: 338609
Analyte
Nitrate Nitrite as N
MB MB
Result Qualifier <0.018
MB MB
Result Qualifier
<0.36
Lab. Sample.ID: LCS 400-338576/2-A Matrix: Solid Analysis Batch: 338609
Analyte Nltraie -Nitrite as N
Lab Sample ID: 400-132588-1 MS Matrix: S.olid Analysis Batch: 338609
Analyte
Nitrate Nitrite as N
Sample Sample
Result Qualifier
9.6 F1 F2
Spike
Added
0.0500
Spike
Added
0.500
Spike
Added 0.0500
Spike Ad.de.ct
0.0500
Spike Added
100
Spike
Added 62.9
RL
0.050
RL 1.0
TestAmerica Job ID: 400-132540-1
Client Sample ID: Lab Control Sample Prep Type: Total/NA
MRL MRL
Result Qualifier Unit 0.0540 mg/L
MDL Unit 0.018 mg/L
~%Rec.
o 1%Rec Limits
108 50.150
Client Sample ID: Method Blank Prep Type: Total/NA
D Prepared Analyzed Oil Fae
01116117 09:23 1
Client Sample ID: Lab Control $ample Prep Type: _Total/NA
LCS LCS
Result Qualifier Unit
0.49'.l mg/L
%Rec.
D o/oRec Limits
99 90:110
Client Sample ID: Lab Control Sample Prep Type: Total/NA
MRL MRL
Result Qualifier Unit
0.0370 J mg/L
0/oRec.
D %Rec Llrnlts
74 50-150
Client Sample ID: Lab Control Sample Prep Type: Total/NA
MRL MRL Result Qualifier Unit
0.0360 J mg/Kg
MDL Unit 0.36 mg/Kg
0/oRec.
0 o/oRec Limits
72 50-150
Client Sample ID: Method Blank Prep Type: Soluble
0 Prepared Analyzed Oil Fae
0111611712:14 1
Client Sample ID: Lab Control Sample Prep Type: SoJuble
LCS LCS Result Qualifier Unit
9.96 mg/Kg
MS MS
Result Qualifier Unit
5.22 F1 mg/Kg
%Rec.
D 0/oRec Limits 100 90-110.
Client Sample I[): CK-1 Prep Type: Soluble
o/oRec. O 0/ 0 Rec Limits ~ -7 90-110
TestAmerica Pensacola
Page 119 of 140 2/1/2017
QC Sample Results Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Lab Sample ID: 400-132588-1 MSD Client Sample ID: CK.1 Matrix: S.olid Prep Type: Soluble Analysis Batch: 338609
Sample Sample Spike MS.O MSO 1>/oRec. RPO Analyte Result Qualifier Added Result Ouallfler Unit 0 %Rec Limits RPO Limit Nitrate Nitrite as N 9.6 F1 F2 62.9 7.05 F1 F2 mg/Kg " -4 90" 110 30 6
Lab Sample ID: 400-132588-6 MS Client Sample ID: CK-5 Matrix: Solid Prep Type: Soluble Analysis Batch:.338609
Sample sample Spike MS MS %1Rec.
Analyte Result Qualifier Added Result Qualifier Unit 0 0/oRec Limits D Nitrate Nitrite as N <0.74 F1 F2 41.0 33.2 F1 mg/Kg " 81 90" 110
Lab Sample ID; 400-132588-6 MSD Client Sample ID: .CK-5 Matrix: Solid Prep Type: Soluble Analysis Batch: 338609
Sample Sample Spike MSD MSO 0/oRec. RPO
Anaiyte Result Qualifier Added Result Qualifier Unit 0 °A> Rec Limits RPD Limit Nitrate Nitrite_as N <0.74 F1 F2 41.0 35.8 Ff F2 mg/Kg ~ 87 90-110 8 6
Lab Sample ID: 400-132650-5 MS Client Sample ID: CK-10 Matri)(: Solid Prep Type: Soluble Analysis Batch: 338609
Sample Sample Spike MS MS o/nRec.
Analyte Result Qualifier Added Result Qualifier Unit 0 %Rec Limits
Nitrate Nitrite as N <0.48 F1 26.6 2.42 F1 mg/Kg " 9 90 -110
Lab Sample ID: 400-132650-5 MSD Client Sample ID: CK-10 Matrix: Solid Prep Type: Soluble Analysis Batch: 338609
Sample Sample Spike MSO MSO 0/oRec. RPO Analyte Result Qualifier Added Result Qualifier Unit 0 0/oRec Limits RPO Limit Nitrate Nitrite as N <0.48 F1 26.6 2.34 F1 mg/Kg ·)~ 9 90" 110 3 6
Method: 7196A ·Chromium, Hexavalent
Lab Sample ID: MB 400-339244/6-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 339470 Prep Batch: 339244
MB MB
Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Oil Fae
Chromium, .hexavalent <3.3 4.7 3.3 mg/Kg 01/20/17 17:00 01/23/1712:03 1
Lab Sample.ID: LCS 400-339244/7-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 339470 Prep Batch: 339244
Spike LCS LCS o/oRec.
Analyte Added Result Qualifier Unit 0 0/oRec Limits
Chromium, hexava!ent 94.6 so:3 mg/Kg 85 80-120
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QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Method: 7196A - Chromium, Hexavalent (Continued)
Lab Sample ID: MRL 400-33924415-A Matrix: Solid Analysis Batch: 339470
Spike MRL MRL
Analyte Added Result Qualifier
Chromium, hexavalent 0.0500 0.0434
Lab Sample ID: 400-132588·.6 MS Matrix: Solid Analysis Batch: 339470
Sample Sample Spike MS MS
Analyte Result Qualifier Added Result Qualifier
Ghromium, hexavalent <5.8 F1 151 <5.3 F1
• Lab Sample ID: 400.132588·6 MSD Matrix: Solid Analysis Batch: 339470
Sa1nple Sample Spike MSO MSO
Analyte Result Qualifier Added Result Qualifier Chi-onii.Um, 'tlexav81e·nt <5.8 F1 178 <6.2 F1
Lab Sample ID: 400-132650·5 MS Matrix: Solid Analysis Batch: 339470
Sa1nple Sample Spike MS MS
A.nalyte Result Quallfier Added Result Qualifier
Chromium, hexavalent <3.4 F1 113 <4.0 F1
Lab Sample ID: 400-132650·5 MSD Matrix: Solid Analysis Batch: 339470
Sample Sample Spike MSO MSD
Analyte Result Qualifier Added Result Ql!alifle,t
thfofnlum, h~xavalerlt <3.4 F1 105 <'3.7 F1
Lab Sample 1.D: MB 400-339253/6 Matrix: Water Analysis Batch: 339253
MB MB
Analyte Result Qualifier RL MDL Unit
Chromium, hexavalent <0.0065 0.010 0.0065 mg IL
Lab Sample ID: LCS 400-339253/7 Matrix: Water Analysis Batch: 339253
Spike LCS LCS
Analyte Added Result Qualifier
Chromium, hexavalent 0.200 0.217
Lab Sample ID: 400-132650·6 MS Matrix: Water Analysis Batch: 339253
Sarnple Sample Spike MS MS
Analyte Result Qualifier Added Result aualltier Chromium, hexavalerlt <0.0065 0.200 0.208
Page 121 of 140
TestAmerica Job ID: 400-132540-1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 339244 O/oRec.
Unit D 0/oRec Limits mg/L 87 50-150
Client Sample ID: CK-5 Prep Type: Total/NA m Prep Batch: 339244 o/oRec.
Unit D 0/oRec Limits
mg/Kg i) 0 75-125
Client Sample ID: CK·5 Prep Type: Total/NA Prep Batch: 339244 o/oRec. RPO
Unit D 0/oRec Limits RPO Limit
mg/Kg " 0 75-125 NC 25
Client Sample ID: CK-10 Prep Type: Total/NA Prep Batch: 339244 0/oRec.
Unit D o/oRec Limits mg/Kg 1) 0 75-125
Client Sample ID: CK·10 Prep Type: Total/NA Prep Batch: 339244 0/oRec. RPO
Unit D 0/oRec Limits RPO Limit
mg/Kg p 0 75-125 NC 25
Client Sample ID; Method Blank Prep Type: Total/NA
D Prepared Analyzed DU Fae 01114117 09:18 1
Client Sample ID: Lab Control Sample Prep Type: Total/NA
%Rec. Unit D %Rec Limits
mg/L 109 90-110
Client Sample ID: RB-2 Prep Type: Total/NA
%Rec.
Unit 0 %Rec Limits
mglL 104 85-115
TestAmerica Pensacola
21112017
QC Sample Results Client: C-K Associates Project/Site: Moffat & Nichol
Lab Sample ID: 400-132650-6 MSD Matrix: Water Analysis Batch: 339253
Analyte Chromium, hexavalent
Sample Sample
Result Qualifier
<0.0065
Lab Sample ID: MB 400-339274/6 Matrix: Water Analysis Batch: 339274
Analyte
Chromium, hexava!ent
MB MB
Result Qualifier
<0.0065
Lab Sample ID: LCS 400.33927 4/7 Matrix: Water Analysis Batch: 339274
Analyte Chromium, hexava!ent
Lab Sample ID: MRL 400-339274/3 Matrix: Water Analysis .Batch: 339274
Analyte Chromium, hexavalent
Lap Sample ID: 400·132540·1 MS Matrix: Water Analysis Batch: 339274
Sample Sample Analyte Result Qualifier Chromium, hexavalent <0.0065
Lab Sample ID: 400-132540·1 MSD Matrix: Water Analysis Batch: 339274
S'ample Sample
Analyte Result Qualifier Chromi'um, hexava!ent <0.6065
Spike
Added 0.200
Spike
Added 0.200
Spike
Added
0.0100
Spike
Added
0.200
Spike
Added
0.200
Me_thod: 90128 • Cyanide,Total andor Amenable
Lab Sample ID: MB 400'339098/1-A Matrix: Solid Analysis Batch: 339005
Analyte Cyanide, Total
MB MB Result Qualifier <0.12
RL
0.010
RL 0.24
MSD MSD
Result Qualifier Unit 0.207 mg/L
MDL Unit 0.0065 mg/L
D
TestAmerica Job ID: 400-132540-1
Client Sample ID: RB-2 Prep Type: Total/NA
0/oRec. O 0/oRec Limits
103 85-115
RPO
RPO Limit 1 9
Clie.nt Sample ID: Method Blank Prep Type: Total/NA
Prepared Analyzed 01/12117 10:22
OJI Fae
Client Sample ID: Lab Control Sample Prep Type: Total/NA
LCS LCS
Result Qualifier Unit 0.211 mg/L
o/oRec.
0 %Rec Limits 105 90-110
Client Sample ID: Lab Control Sample Prep Type: Total/NA
MRL MRL
Result Qualifier Unit
0.0132 mgiL
MS
Result
0.210
MSD
Result 0.220
MS
Qualifier
MSD
Qualifier
MDL Unit 0.12 mg/Kg
Unit
mg/L
Unit
niiJ/l.
0/oRec.
D 0/oRec Limits
132 50-150
Client Sample ID: RINSATE 1 Prep Type: Total/NA
0/oRec.
D 0/oRec Limits 105 85-115
Client Sample ID: RINSATE 1 Prep Type: Total/NA
0/oRec. RPO
D o/oRec Limits RPO Limit 110 85-115 5 9
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 339068
0 Prepared Analyzed 011 Fae 01/18/1710:53 01/18/17 17:30 1
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QC Sample Results Client: C-K Associates ProjecUSite: Moffat & Nichol
Method: 90128. Cyanide, Total andor Amenable (Continued)
Lab Sample ID: LCS 400-339068/2-A Matrix: Solid Analysis Batch: 339005
Spike LCS LCS
Analyte Added Result Qualifier
Cyanide, Total 13.6 14.7
Lab Sample ID: 400-132588-6 MS Matrix: Solid Analysis Batch: 339005
Sample Sample Spike MS MS
Analyte Result Qualifier Added Result Qualifier
Cyanide, Total <0.27 F1 20.1 12.3
Lab Sample 1.D: 400°132588·6 MSD Matrix: Solid Analysis Batch: 339005
Sa1nple Sample Spike MSO MSO
Analyte Result Qualifier Added Result Qualifier Cyanide, Total <!>:it F1 19.5 10.9 Fi
Lab Sample ID: 400°132650-5 DU Matrix: Solid Analysis Batch: 339005
S_ample Sample DU DU Analyte Result Qualifier Result Qualifier Cyanide, Total <0.17 <0.17
Page 123of140
Tes!America Job ID: 400-132540-1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 339068 %1Rec.
Unit D o/e1Rec Limits mg/Kg 108 75-125
Client Sample ID: CK-5 Prep Type: Total/NA
E Prep Batch: 339068 o/oRec.
Unit D o/oRec Limits mg/Kg -(! 61 57 -136
Client Sample ID: CK·5 Prep Type; Total/NA Prep Batch: 339068 1%Rec. RPO
Unit D O/GRec Limits RPO Limit
mg/Kg " 56 57 .136 12 20
Client Sample ID: CK-10 Prep Type: Total/NA Prep Batch: 339068
RPO
Unit 0 RPO Limit
mg/Kg -!;! NC
Tes!America Pensacola
2/1/2017
Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: RINSATE 1 Lab Sample ID: 400-132540-1 Date Collected: 01111/1713:20 Matrix: Water Date Received: 01112/17 09:21
Batch Batch Diiution Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Analysis 8260C 338529 01/16/17 09:43 CLN TALPEN
Total/NA Prep 3520C 338284 01/12/1716:23 KLR TAL PEN
Total/NA Analysis 82700 338574 01/16/17 21:32 MAM TAL PEN
Total/NA Prep 3520C 338284 01/12/1716:23 KLR TAL PEN
Total/NA Analysis 82700 LL 338569 01/16/1718:58 S1S TAL PEN
Total/NA Analysis MAVPH 339057 01/19/17 22:24 MKA TAL PEN
E Total/NA Prep 8011 339493 01 /23/17 16:25 KH1 TAL PEN
Total/NA Analysis 8011 339878 01/27/17 00:09 KH1 TAL PEN
Total/NA Prep 3520C 338239 01/12/1716:15 KLR TALPEN
Total/NA Analysis 8081B 339079 0111911713:41 MAM TAL PEN
Total/NA Prep 3520C 339262 01 /20/17 15:54 KLR TAL PEN
Total/NA Analysis MA-EPH 339948 01126/17 17:25 RM TALPEN
Total/NA Prep 3520C 339262 01/20/1715:54 KLR TALPEN
Total/NA Analysis MA,EPH 339950 0112611719:59 RM TALPEN
Total/NA Prep 3010A 338333 01 /13/17 08:50 RJB TALPEN
Total/NA Analysis 6010C 338689 01/16/17 17:16 RJB TAL PEN
Total/NA Prep 7470A 337923 01/1311708:15 JAP TALPEN
Total/NA Analysis 7470A 338420 01/13/1712:58 JAP TALPEN
Total/NA Prep Oistill/CN 338793 01/17/17 09:30 BAB TAL PEN
Total/NA Analysis 335.2 338792 01/17117 14:18 BAB TALPEN
Total/NA Analysis 353.2 338427 01/13/1713:30 KJR TALPEN
Total/NA Analysis 7196A 339274 01/12/1710:56 JLB TALPEN
Client Sample ID: CK-1 Lab Sample ID: 400~132588-1 Date Collected: 0111111711:10 Matrix: Solid Date Received: 01/12117 16:57
Batch Batch Dllutlon Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 7471A 337950 01/15/17 12:43 JAP TALPEN
Total/NA Analysis 7471A 338612 01/16/17 09:31 JAP TALPEN
Total/NA Analysis Moisture 338696 01/17/1710:20 JNJ TALPEN
Client Sample ID: CK-1 Lab Sample ID: 400-132588-1 Date Collected: 01/11/1711:10 Matrix: Solid Date Received: 01/1211716:57 Percent Solids: 31.8
Batch Batch Diiution Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 5035 339330 01/22117 07:44 RS TAL PEN
Total/NA Analysis 8260C 339331 01/22/1711:25 RS TALPEN
Total/NA Prep 3546 338556 01/16/17 09:16 RDT TAL PEN
Total/NA Analysis 82700 338849 01/18/1716:05 KJA TALPEN
Total/NA Prep 5035 338604 01/16/1711:00 MKA TAL PEN
Total/NA Ana'lysis MAVPH 50 338571 01/16/1718:19 MKA TALPEN
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Client: C-K Associates ProjecUSite: Moffat & Nichol
Batch Batch
Method
3546
8081B
Prep Type
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Soluble Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Type
Prep Analysis
Prep
Analysis
Prep Analysis
Prep Analysis
Leach
Analysis
Prep
Analysis
Prep
Analysis
3546
MA-EPH
3546
MA-EPH
3050B
6010C
DJ Leach 353.2
3060A
7196A
90128
9012B
Client Sample ID: CK-2 Date Collected: 01111117 11 :40 Date Received: 01/1211716:57
Prep Type
Total/NA Total/NA
Total!NA
Batch Type
Prep Analysis
Analysis
Batch
Method
7471A
7471A
Moisture
Client Sample ID: CK-2 Date Collected: 0111111711:40 Date Received: 0111211716:57
Prep Type
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Soluble Soluble
Total/NA
Total/NA
Batch
Type
Prep Analysis
Prep Analysis
Prep Analysis
Prep Analysis
Batch Method
5035
8260C
3546
82700
5035 MAVPH
3546
8081B
Prep 3546
Analysis MA~EPH
Prep 3546
Analysis MA-EPH
Prep 3050B
Analysis 6010C
Leach DI Leach Analysis 353.2
Prep 3060A
Analysis 7196A
Run
Run
Run
Lab Chronicle
Dilution Factor
5
Dilution Factor
Dllutlpn Factor
so
5
TestAmerica Job ID: 400-132540-1
Batch Prepared Number or Analyzed Analyst Lab 338557 01116117 09:24 RDT TAL PEN
338706 0111711718:11 TD
339010 01/19117 07:20 RDT
339632 0112411718:11 RM
339010 01119/17 07:20 RDT
339633 01124/17 22:24 RM
338440 0111511711:30 DN1
338689 01116/17 15:45 RJB
338576 01116117 09:57 KJR
338609 01/1611712:16 KJR
339244 0112011717:00 CLM
339470 01123/1712:03 CLM
339068 01/1811710:53 BAB
339005 0111811717:31 BAB
TAL PEN
TAL PEN
TAL PEN
TALPEN
TAL PEN
TAL PEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
L11b Sample ID: 400-132588•2 Matrix: Solid
Batch Prepared Number or Analyzed Analyst 337950 0111511712:43 JAP
338612 01116117 09:33 JAP
338607 0111611712:37 CJP
Lab
TAL PEN
TALPEN
TALPEN
Lab Sample ID: 400-132588•2 Matrix:. s.oli<J
Percent Solids.: 23.2
Batch Prepared Number or Analyzed Analy$t Lab 339330 01/22117 07:44 RS TAL PEN
339331 01/22/1711:50 RS
338556 01116117 09:16 RDT
338849 0111811716:38 KJA
338604 01/1611711:00 MKA
338571 01/1611719:18 MKA
338557 01/16117 09:24 RDT
338706 0111711718:41 TD
339010 01/19117 07:20 RDT
339632 01/2411718:21 RM
339010 01119117 07:20 RDT
339633 01/24/17 22:33 RM
338440 01/15/1711:30 DN1
338689 01116/17 15:48 RJB
338576 01116117 09:57 KJR
338609 01/16/1712:18 KJR
339244 01120117 17:00 CLM
339470 01/2311712:03 CLM
TALPEN
TAL PEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TALPEN
TestAmerica Pensacola
Page 125of140 2/1/2017
Lab Chronicle Client: C-K Associates Tes!America Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: CK-2 Lab Sample ID: 400-132588-2 Date Collected: 01/11/1711:40 Matrix: Solid Date Received: 01/12/17 16:57 Percent Solids: 23.2
Batch Batch Dllutlon Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
'rotellNA Prep 9012B 339068 01/18/17 10:53 BAB TALPEN
Total/NA Analysis 9012B 339005 01/18/1717:31 BAB TALPEN
Client Sample ID: Duplicate Lab Sample ID: 400-13258$-3 Date Collected: 01/11/1712:00 Matrix: Solid Date Received: 01/12/1716:57
Batch Batch Dilution Batch Prepared B Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
TotallNA Prep 7471A 337950 01/1511712:43 JAP TALPEN
Total/NA Analysis 7471A 338612 01/16/17 09:35 JAP TALPEN
TotallNA Analysis Moisture 338607 01/16/1712:37 CJP TALPEN
Client Sample ID: Duplicate Lab Sample ID: 400-132588-3 Date Collected: 01/11/1712:00 Matrix: Solid Date Received: 01/12/1716:57 Percent Solids: 32. 7
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
TotallNA Prep 5035 339330 01122/17 07:44 RS TAL PEN
TotallNA Analysis 8260C 339331 01/22/1712:15 RS TALPEN
Total/NA Prep 3546 338556 01/16117 09:16 ROT TAL PEN
Tota!INA Analysis 82700 338849 01118/1717:12 KJA TAL PEN
TotallNA Prep 5035 338604 01/16/17 11:00 MKA TALPEN
Total/NA Analysis MAVPH 50 338571 01116117 20:18 MKA TALPEN
Total/NA Prep 3546 338557 01/16117 09:24 ROT TALPEN
TotallNA Analysis 8081B 5 338706 01/17/1719:11 TD TAL PEN
. TotallNA Prep 3546 339010 01119117 07:20 ROT TALPEN
Total/NA Analysis MA·EPH 339632 01/24/1718:31 RM TAL PEN
Total/NA Prep 3546 33.9010 01/19/17 07:20 ROT TALPEN
TotallNA Analysis MA-EPH 339633 01/24/17 22:43 RM TALPEN
TotallNA Prep 3050B 338440 01/15/1711:30 ON1 TALPEN
Total/NA Analysis 6010C 338689 01/16/1715:51 RJB TAL PEN
Soluble Leach DI Leach 338576 01/16/17 09:57 KJR TALPEN
Soluble Analysis 353.2 338609 01/16/17 12:19 KJR TALPEN
TotallNA Prep 3060A 339244 01/20/1717:00 CLM TALPEN
Tota!INA Analysis 7196A 339470 01/23/1712:03 CLM TALPEN
Total/NA Prep 9012B 339068 01/18/1710:53 BAB TALPEN
TotallNA Analysis 9012B 339005 01/18/1717:31 BAB TALPEN
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Page 126 of 140 2/1/2017
Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 Projecl/Site: Moffat & Nichol
Client Sample ID: CK-3 Lab Sample ID: 400-132588-4 Date Collected: 01/11/1712:15 Matrix: Solid Date Received: Oi/12/1716:57
Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab tofoiiNii. Prep 7471A 337950 0111511712:43 JAP TAL PEN
Total/NA Analysis 7471A 338612 01116117 09:54 JAP TAL PEN
Total/NA Analysis Moisture 338607 0111611712:37 CJP TALPEN
Client Sample ID: CK-3 Lab Sample ID: 400-132588-4 Date Collected: 01/1111712:15 Matrix: Solid
E Date Received: 01/12/1716:57 Percent Solids: 2S.7
Batch Batch Diiution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 5035 339330 01122117 07:44 RS TAL PEN
Total/NA Analysis 8260C 339331 0112211712:41 RS TALPEN
Total/NA Prep 3546 338556 01116117 09:16 ROT TAL PEN
Total/NA Analysis 82700 338741 01117117 13:48 MAM TAL PEN
Total/NA Prep 5035 338604 0111611711:00 MKA TALPEN
Total/NA Anatysls MAVPH 50 338571 01116117 21:18 MKA TALPEN
Total/NA Prep 3546 338557 01116117 09:24 ROT TAL PEN
Total/NA Analysis 80818 5 338706 0111711719:42 TD TALPEN
Total/NA Prep 3546 339010 01119117 07:20 ROT TALPEN
Total/NA Analysis MA-EPH 339632 0112411718:50 RM TAL PEN
Tota!INA Prep 3546 339010 01119117 07:20 ROT TALPEN
Total/NA Analysis MA-EPH 339633 01124117 23:02 RM TALPEN
Total/NA Prep 3050B 338440 0111511711:30 ON1 TALPEN
Total/NA Analysis 6010C 338689 0111611715:55 RJB TAL PEN
Soluble Leach DJ Leach 338576 01116117 09:57 KJR TALPEN
Soluble Analysis 353.2 3.38609 0111611712:20 KJR TALPEN
Total/NA Prep 3060A 339244 01120117 17:00 CLM TAL PEN
Total/NA Analysis 7196A 339470 0112311712:07 CLM TALPEN
Total/NA Prep 9012B 339068 0111811710:53 BAB TALPEN
Total/NA Analysis 9012B 339005 01118117 17:37 BAB TAL PEN
Client Sample ID: CK-4 Lab Sample ID: 400-132588-5 Date C.ollected: 01/1111712:30 Matriic S.olid Date Re.ceived: 01112/1716:57
Batch Batch Dllutlon Batch Prepared Prep-Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 7471A 337950 01115117 12:43 JAP TALPEN
Total/NA Analysis 7471A 338612 01116117 09:56 JAP TALPEN
Total/NA Analysis Moisture 338607 0111611712:37 CJP TALPEN
TestAmerica Pensacola
Page 127of140 2/1/2017
Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: CK-4 Lab Sample ID: 400-132588,5 Date Collected: 01/11/1712:30 Matrix: Solid Date Received; 01/12/17 16:57 Percent Solids: 20.9
Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 5035 339330 01/22111()7:44 RS TAL PEN
Total/NA Analysis 8260C 339331 01/22/17 13:06 RS TAL PEN
Total/NA Prep 3546 338556 01/16/17 09:16 RDT TAL PEN
Total/NA Analysis 8270D 338741 01/17/1714:21 MAM TAL PEN
Total/NA Prep 5035 338604 01/16/1711:00 MKA TAL PEN
Total/NA Analysis MAVPH 50 338571 01/16/17 22:17 MKA TAL PEN
Total/NA Prep 3546 338557 01/16/17 09:24 RDT TAL PEN m Total/NA Analysis 8081B 5 338706 01/17/17 20:12 TD TAL PEN
Total/NA Prep 3546 339010 01/19/17 07:20 RDT TAL PEN
Total/NA Analysis MA-EPH 339632 01/24/1718:59 RM TAL PEN
Total/NA Prep 3546 339010 01/19/17 07:20 RDT TALPEN
Total/NA _Analysis MA-EPH 339633 01/24/17 23:11 RM TAL PEN
Total/NA Prep 30508 338440 01/15/1711:30 DN1 TAL PEN
Total/NA Analysis 6010C 338689 01/16/1.7 16;08 RJ8 TAL PEN
Soluble Leach DI Leach 338576 01/16/17 09:57 KJR TAL PEN
Soluble Analysis 353.2 338609 01/16/1712:21 KJR TAL PEN
Total/NA Prep 3060A 339244 01/20/1717:00 CLM TALPEN
Total/NA Analysis 7196A 339470 01/23/1712:07 CLM TALPEN
Total/NA Prep 90128 339068 01/18/1710:53 BAB TALPEN
Total/NA Analysis 9012B 339005 01/18/1717:37 BAB TALPEN
Client Sample ID: CK-5 Lab Sample ID: 400-132588-6 Date Collected: 01/11/1713:15 Matrix: Solid Date Received: 01112/1716:57
Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 7471A 337950 01/15/17 12:43 JAP TALPEN
Total/NA Analysis 7471A .338612 01/16/17 09:57 JAP TALPEN
Total/NA Analysis Moisture 338607 01/16/1712:37 CJP TAL PEN
Client Sample ID: CK-5 Lab Sample ID: 400-132588-6 Date Collected: 01/1111713:15 Matrix: Solid Date Received: 01/12/1716:57 Percent Solids: 48 .• 8
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 5035 339082 01119/ft bi\:59 BSW TALPEN
Total/NA Analysis 8260G 50 339083 01/19/1712:21 cs TALPEN
Total/NA Prep 3546 338556 01/16/17 09:16 RDT TALPEN
Total!NA Analysis 8270D 338741 01/1711714:54 MAM TAL PEN
Total/NA Prep 5035 338604 01/16/1711:00 MKA TALPEN
Total/NA Analysis MAVPH 50 338571 01/17/1710:52 MKA TALPEN
Total/NA Prep 3546 338557 01/16/17 09:24 RDT TAL PEN
Total/NA Analysis 80818 2 338801 01/17/1721:10 MAM TAL PEN
TestAmerica Pensacola
Page 128 of 140 2/1/2017
Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 Project/Site: Moffat & Nichol
Client Sample ID: CK•5 Lab Sample ID: 400-1325BB-6 Date Collected: 0111111713:15 Matrix: Solid Date Received: 0111211716:57 Percent Solids: 48.8
Batch Batch Dilution Batch Pr~pared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
total/NA Pi€p 3546 339010 01/19)1701:20 ROT TAL PEN Total/NA Analysis MA-EPH 339632 01124117 18:02 RM TAL PEN
Total/NA Prep 3546 339010 01119117 07:20 ROT TALPEN
Total/NA Analysis MA-EPH 339633 01124117 22:14 RM TALPEN
Total/NA Prep 30508 338440 0111511711:30 ON1 TAL PEN
Total/NA Analysis 6010C 338689 0111611716:11 RJB TAL PEN
Soluble Leach DI Leach 338576 01116117 09:57 KJR TALPEN E -Soluble Analysis 353.2 338609 0111611712:22 KJR TALPEN
Total/NA Prep 3060A 339244 0112011717:00 CLM TALPEN
Total/NA Analysis 7196A 339470 0112311712:03 CLM TALPEN
Total/NA Prep 90128 339068 0111811710:53 BAB TALPEN
Total/NA Ana_lysts 90128 339005 0111811717:30 BAB TAL PEN
C.lient Sample ID: CK-6 Lab Sample ID: 400-132650-1 Date Collected: 01113/17 09:30 Matrix: Solid Date Received: 01/14/17 08:32
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 7471A 338513 ()i/15111'12:43 ON1 TALPEN
Total/NA Analysis 7471A 338612 0111611712:14 JAP TAL PEN
Total/NA Analysis Moisture 338696 0111711714:08 JNJ TAL PEN
Client Sample ID: CK-6 Lab Sample ID: 400-132650-1 Date Collected: 01/13/17 09.:30 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 51.9
Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 50.35 339082 01/19117 08:59 SSW TALPEN
Total/NA Analysis 8260C 339083 0111911715:35 cs TALPEN
TotaUNA Prep 3546 338817 0111811709:33 ROT TAL PEN Total/NA Analysis 82700 338966 01119117 00:09 MAM TAL PEN
Total/NA Prep 3546 338817 01118117 09:33 ROT TAL PEN
Total/NA Analysis 82700 339121 01119117 22:14 KJA TAL PEN
Total/NA Prep 5035 338604 0111611711:30 MKA TALPEN
Total/NA Analysis MAVPH 50 338571 01117117 00:17 MKA TALPEN
Total/NA Prep 3546 338931 0111811712:42 RDT TALPEN
Total/NA Analysis 80818 2 339152 01119117 21:49 TD TALPEN
Total/NA Prep 3546 339010 01119117 07:20 ROT TALPEN
Total/NA Analysis MA-EPH 339632 0112411719:57 RM TALPEN
Total/NA Prep 3546 339010 01119117 07:20 ROT TALPEN
Total/NA Analysis MA-EPH 339633 01125117 00:08 RM TALPEN
Total/NA Prep 30508 338528 01116117 08:55 KWN TALPEN
Total/NA Analysis 6010C 338847 0111711713:01 GESP TALPEN
TestAmerica Pensacola
Page 129 of 140 2/1/2017
Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecVSite: Moffat & Nichol
Client Sample ID: CK-6 Lab Sample ID: 400-132650-1 Date Collected: 01/13/17 09:3.0 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 51.9
Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Soluble Leach o-1·teach 338576 01/16/17 09:57 kJR TAL PEN Soluble Analysis 353.2 338609 01/16/17 12:26 KJR TAL PEN
Total/NA Prep 3060A 339244 01/20/17 17:00 CLM TALPEN
Total/NA Analysis 7196A 339470 01/23/17 12:07 CLM TAL PEN
Total/NA Prep 9012B 339068 01/18/1710:53 BAB TAL PEN
Total/NA Analysis 90128 339005 01/18/1717:37 BAB TAL PEN
Client Sample ID: CK.7 Lab Sample ID: 400-132650-2 E Date Collected: 01 /13/17 09.:45. Matrix: Solid Date Recelved: 01/14/17 08:32
Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 7471A 338513 01/15/17 12:43 DN1 TALPEN
Total/NA Ana!ysls 7471A 338612 01/16/1712:16 JAP TALPEN
Total/NA Analysis Moisture 338696 01/17/1714:08 JNJ TALPEN
Client Sample ID: CK-7 Lab Sample ID: 400-132650-2 Date collected: 01/13/17 09:45 Matrix: Solid Date Received: 01/14/17 08:32 Percent Solids: 23.3
Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 5035 339082 01/19/17 08:59 BSW TALPEN Total/NA Analysis 8260C 339083 01/19/17 15:58 cs TALPEN
Total/NA Prep 3546 338817 01/18/17 09:33 ROT TAL PEN
To.tal/NA Analysis 82700 338966 01/19/17 00:41 MAM TAL PEN
Total/NA Prep 3546 338817 01/18/17 09:33 ROT TALPEN Total/NA Analysis 82700 339121 01/19/17 22:44 KJA TALPEN
TotallNA Prep 503.5 338604 01/16/1711:30 MKA TALPEN
Total/NA Analysis MAVPH 50 338571 01/17/17 01:16 MKA TALPEN
Total/NA Prep 3546 339357 01/23/17 08:05 ROT TAL PEN Total/NA Analysis 8081B 339881 01/26/1715:18 MAM · TAL PEN
Total/NA Prep 3546 339010 01/19/17 07:20 ROT TALPEN
Total/NA Analysis MA-EPH 339632 01/24/17 20:07 RM TALPEN
Total/NA Prep 3546 339010 01/19/17 07:20 ROT TALPEN Total/NA Analysis MA-EPH 339633 01/25/17 00:18 RM TALPEN
Total/NA Prep 3050B 338528 01/16/17 08:55 KWN TALPEN
Total/NA Analysis 6010C 338847 01/17/1713:16 GESP TALPEN
Soluble Leach DI Leach 338576 01/16/17 09:57 KJR TAL PEN
Soluble Analysis 353.2 338609 01/16/17 12:27 KJR TALPEN
Soluble Leach DI Leach 338576 01/16/17 09:57 KJR TAL PEN
Soluble Analysis 353.2 5 338609 01/16/1712:32 KJR TALPEN
Total/NA Prep 3060A 339244 01/20/1717:00 CLM TALPEN
Total/NA Analysis 7196A 339470 01/23/17 12:07 CLM TAL PEN
TestAmerica Pensacola
Page 130of140 21112017
Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1 ProjecUSite: Moffat & Nichol
Client Sample ID: CK-7 Lab Sample ID: 400-132650-2 Date Collected: 01/13/17 09:45 Matrix: Solid Date Received: 01114117 08:32 Percent Solids: 23.3
Batch Batch Diiution Batch Prepared Prep Type Type Method Run Factor Number Or Analyzed Analyst Lab Total/NA Prep 9012B 339068 61/18/1710:5:3 BAB Tl\LPEN Total/NA Analysis 9012B 339005 01/18/1717:37 BAB TALPEN
Client Sample ID:. CK-8 Lab Sample ID: 400-132650-3 Date Collected: 01/13/17 10:10 Matrix: Solid Date Received: 01114117 08:32
Batch Batch Ollutlon Batch Prepared E Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 7471A 338513 01115/1712:43 DN1 TALPEN Total/NA Analysis 7471A 338612 01/16/1712:17 JAP TALPEN
Total/NA Analysis Moisture 338696 01/17/1714:08 JNJ TALPEN
Client Sample ID: CK-8 Lab Sample ID: 400-132650-3 Date Collected: 0111311710:10 Matrix: Solid Date Received: 01/.14/17 08:32 Percent Solids: 46.4
Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Ana:lyst .Lab
Total/NA Prep 5035 339330 01122/17 07:44 RS TALPEN Total/NA Analysis 8260C 339331 01/2211713:31 RS TALPEN
Total/NA Prep 3546 338817 01/18117 09:33 RDT TALPEN
Total/NA Analysis 82700 338966 01/19117 01:14 MAM TALPEN
Total/NA Prep 3546 338817 01/18/17 09:33 RDT TALPEN
Total/NA Analysis 82700 339121 01/19/17 23:14 KJA TALPEN
Total/NA Prep 5035 338604 01/16/1711:30 MKA TALPEN
Total/NA Analysis MAVPH 50 338571 01/17/17 02:16 MKA TALPEN
Total/NA Prep 3546 338931 01118/1712:42 ROT TALPEN
Total/NA Analysis 80818 2 339152 01/19/17 22:50 TD TALPEN
Total/NA Prep 3546 339010 01/19117 07:20 ROT TALPEN
Total/NA Analysis MA-EPH 339632 01/24/17 20:17 RM TALPEN
Total/NA Prep 3546 339010 01/19/17 07:20 ROT TALPEN Total/NA Analysis MA-EPH 339633 01/25117 00:27 RM TALPEN
Total/NA Prep 3050B 338528 01/16/17 08:55 KWN TALPEN
Total/NA Analysis 6010C 338847 01/17/17 13:20 GESP TALPEN
Soluble Leach DI Leach 338576 01/16/17 09:57 KJR TALPEN
Soluble Analysis 353-2 338609 01/16/1712:28 KJR TALPEN
Total/NA Prop 3060A 339244 01/20/17 17:00 CLM TALPEN
Total/NA Analysis 7196A 339470 01/23/1712:07 CLM TALPEN
Total/NA Prep 9012B 339068 01118/1710:53 BAB TALPEN Total/NA Analysis 90128 339005 01/18/17 17:37 BAB TALPEN
TestAmerica Pensacola
Page 131 of 140 2/1/2017
Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132540-1
Project/Site: Moffat & Nichol
Client Sample ID: CK-.9 Lab Sample ID: 400-132650-4 Date Collected: 01/13/1710:25 Matrix: Solid
Date Received: 01/14117 08:32
Batch Batch Diiution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 7471A 338513 01/15/1712:43 ON1 TALPEN
Total/NA Analysis 7471A 338612 01/16/17 12:19 JAP TALPEN
Total/NA Analysis Moisture 338696 01/17/1714:08. JNJ TALPEN
Client Sample ID: CK-9 Lab Sample ID: 400-132650-4 Date Collected: 01/1311710:25 Matrix: Solid
E Date Received: 01114117 08:32 Percent Solids: 52.0
Batch Batch Dllutlon Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 5035 339082 01/19/1708:59 BSW TALPEN
Total/NA Analysis 8260C 339083 01/19/1716:47 cs TALPEN
Total/NA Prep 3546 338817 01/18/17 09:33 ROT TALPEN
Total/NA Analysis 82700 338966 01/19/17 01:47 MAM TAL PEN
Total/NA Prep 3546 338817 01/18/17 09:33 ROT TALPEN
Total/NA Analysis 82700 339121 01/19/17 2.3:44 KJA TAL PEN
Total/NA Prep 5035 338604 01/16/1711 :30 MKA TAL PEN
Total/NA Analysis MAVPH 50 338571 01/17/17 03:16 MKA TAL PEN
Total/NA Prep 3546 338931 01/18/1712:42 ROT TALPEN Total/NA Analysis 80818 2 339152 01/19/17 23:20 TD TAL PEN
Total/NA Prep 3546 339010 01/19/17 07:20 ROT TALPEN
Total/NA Analysis MA-EPH 339632 01 /24/17 20:37 RM TALPEN
Total/NA Prep 3546 339010 01/19/17 07;20 ROT TALPEN Total/NA Analysis MA-EPH 339633 01/25/17 00:46 RM TALPEN
Total/NA Prep 3050B 338528 01/16/17 08:55 KWN TALPEN
Total/NA Analysis 6010C 338847 01/17/1713.:23 GESP TALPEN
Soluble Leach DJ Leach 338576 01/16/17 09:57 KJR TALPEN
Soluble Analysis 353.2 338609 01/16/1712:29 KJR TALPEN
Total/NA Prep 3060A 339244 01/20/17 17:00 CLM TALPEN
Total/NA Analysis 7196A 339470 01/23/17 12:07 CLM TALPEN
Total/NA Prep 9012B 339068 01/18/1710:53 BAB TALPEN
Total/NA Analysis 9012B 339005 01/18/1717:37 BAB TALPEN
Client Sample ID: CK-10 Lab Sample ID: 400-132650-5 Date Collected: 01113/17 10:45 Matrix: Solid
Date Received: 01114117 08:32
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Prep 7471A 338513 01115/1712:43 ON1 TALPEN Total/NA Analysis 7471A 338612 01/16/1712:20 JAP TAL PEN
Total/NA Analysis Moisture 338696 01/17/1714:08 JNJ TALPEN
TestAmerica Pensacola
Page 132of140 2/1/2017
Client: C-K Associates ProjecUSite: Moffat & Nichol
Client Sample ID: CK-10 Date Collected: 0111311710:45 Date Received: 01114/17 08:32
Prep Type Total/NA Total/NA
Total/NA
Total/NA
Total/NA Total/NA
Total/NA Total/NA
Total/NA Total/NA
Total/NA Total/NA
Total/NA Total/NA
Total/NA Total/NA
Soluble Soluble
Total/NA
Total/NA
Total/NA Total/NA
Batch Type Prep Analysis
Prep
Analysis
Prep Analysis
Prep
Analysis
Prep Analysis
Batch
Method 5035 8260C
3546
82700
3546 82700
5035 MAVPH
3546 80818
Prep 3546
Analysis MA-EPH
Prep 3546 Analysis MA-EPH
Prep 3050B Analysis 6010C
Leach DI Leach Analysis 353.2
Prep 3060A
Analysis 7196A
Prep 90128 Analysis 9012B
Client Sample ID: RB-2 Date Collected: 01/13/17 11 :00 Date Received: 01/14/17 08:32
Prep Type Total/NA
Total/NA Total/NA
Total/NA Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA Total/NA
Total/NA Total/NA
Total/NA
Batch
Type Analysis
Prep Analysis
Prep
Analysis
Batch Method
8260C
3520C 82700
3520C
82700
Prep 3520C
Analysis 82700 LL
Analysis MAVPH
Prep 8011
Analysis 8011
Prep 3520C Analysis 8081 B
Prep 3520C
Analysis MA-EPH
Prep 3520C
Lab Chronicle
Run
Run
RERA RERA
Dilution
Factor
50
2
Dilution
Factor 1
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-5 Matrix: Solid
Percent Solids: 75.1
Batch Prepared
Number or Analyzed Ana!Yst Lab 339082 01/19/17 08:59 ElSW TAL PEN 339083 01/19/17 17:13 CS TAL PEN
338817 01/18/17 09:33 RDT
338966 01/19/17 02:20 MAM
338817 01/18/17 09:33 RDT 339121 01/20/17 00:15 KJA
338604 01/16/1711:30 MKA 338571 01/17/17 04:15 MKA
338931 01/18/17 12:42 RDT 339152 01/19/17 23:50 TD
339010 01/19/17 07:20 RDT 339632 01124/17 20:47 RM
339010 01/19/17 07:20 RDT 339633 01/25/17 00:55 RM
338528 01/16/17 08:55 KWN
338847 01/17/1713:26 GESP
338576 01/16/17 09:58 KJR 338609 01/16/1712:30 KJR
339244 01 /20/17 17:00 CLM
339470 01/23/17 12:07 CLM
339068 01/18/1710:53 BAB 339005 01/18/1717:37 BAB
TAL PEN
TAL PEN
TAL PEN TAL PEN
TAL PEN
TAL PEN
TAL PEN TAL PEN
TAL PEN
TAL PEN
TAL PEN TALPEN
TALPEN TALPEN
TALPEN TALPEN
TALPEN
TALPEN
TAL PEN TALPEN
Lab Sample ID: 400-132650-6 Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab 338771 01/17/1716:13 CLN TAL PEN
339125 01/19/1715:31 KLR 339672 01/2511710:06 KJA
340079 01 /27 /17 11 :20 KLR 340421 01/31/1716:30 MAM
339125 01/19/1715:31 KLR 339599 01/24/1716:27 S1S
339057 01/19/17 23:24 MKA
339493 01/23/1716:25 KH1 339878 01/27/17 00:38 KH1
339054 01/19/1710:03 KLR 339554 01 /24/17 13:06 TD
339262 01 /20/17 15:54 KLR 339948 01/26/17 17:34 RM
339262 01/20/1715:54 KLR
TALPEN TALPEN
TAL PEN
TALPEN
TALPEN TAL PEN
TALPEN
TALPEN
TALPEN
TALPEN TALPEN
TALPEN TALPEN
TALPEN
TestAmerica Pensacola
Page 133of140 2/112017
Client: C-K Associates ProjecUSite: Moffat & Nichol
Client Sample ID: RB-2 Date Collected: 0111311711:00 Date Received: 01114117 08:32
Batch Batch Prep Type Type Method Total/NA Analysis MA-EPH
Total/NA Prep 3010A
TotallNA Analysis 6010C
Total/NA. Prep 7470A
TotallNA Analysis 7470A
Total/NA Prep Distill/CN Total/NA Analysis 335.2
Total/NA Analysis 353.2
Total/NA Analysis 7196A
Laboratory References:
Lab Chronicle
Dilution Batch Prepared
Run Factor Number or Analyzed :3:39950 ()1/26117 20:09
338893 01/1811710:09
339167 01/19117 16:25
338653 01116117 16:27
338941 01/18/17 13:46
338793 01/17/17 09:30
338792 01/17117 14:24
338579 01/16/17 09:36
339253 01/14117 09:18
TAL PEN= TestAmerica Pensacola, 3355 Mclemore Drive, Pensacola, FL 32514, TEL (850)474~1001
Page 134of140
TestAmerica Job ID: 400-132540-1
Lab Sample ID: 400-132650-6 Matrix: Water
Analyst Lab
RM TAL PEN
KWN TAL PEN
GESP TALPEN
JAP TALPEN
JAP TALPEN
BAB TALPEN
BAB TALPEN E KJR TALPEN
JLB TALPEN
TestAmerica Pensacola
21112017
Client: C-K Associates ProjecVSite: Moffat & Nichol
Laboratory: TestAmerica Pensacola
Certification Summary
Unless otherwise noted. al! analy!es for tr1is laboratory were covered under each certification be!o\V,
Authority Louisiana
Program NE LAP
EPA Region Certification ID 6 30976
The following analytes are Included in this report, but are not certified under this certification:
Analysts Method Prep Method Matrix Analyte s26ilc 5035 Solid isol>l.ltyl a1c0ho1
The following analytes are included in this report, but certification is not offered by the governing authority:
Analysis Method Prep Method Matrix Analyte 353.2 · Solid Nitrate Nitrite as N 90128 90128 Solid Cyanide, Total MA~EPH 3520C Water C21-C35 Aromatics MA-EPH 3546 Solid C21-C35 Aromatics Moisture Solid Percent Moisture
Page 135 of 140
TestAmerica Job ID: 400-132540-1
Expiration Date 06-30-17
TestAmerica Pensacola
2/112017
"1J
"' <O (l)
~
"' CJ)
Q. ~ ... 0
~ ;::> 0 ~
.....
TestAmerica Pensacola 3355 Mclemore Drive
;Pensacola, FL 32514 Phone (850) 474-1001 Fax (850) 478-2671
Client Information Client Con!act:
f_iennifer Lindquist :company: ,C-K Associates fMdress:: 17170 Perkins Road
n Rouge
;f'horu;!:
""'" ~Jennifer.1indqu1S'"[email protected] Project Name: Moffat & Nichol
""'
!ample Identification }'.,;~;;{:::--.. :;,,.:: · '.:-~·--·~::..-~.- ·~;~_::_.~~~-·;, ~:: ,:~~---·· ·><'-.;··:~~-. :u:-:-1"'0,
~~\:t,j_
Chain of Custody Record
15'"]/oc I r '.iJ...-..JJJb 11.S o-,
Pti.i'ie: ~<' '1.St' /JY.5()
Lab PM:
Wilson, Jason A E-Mait
CarrierTraeking No{sj::
Analysis Requested Due Date Requested:
TAT Requested (days):
PO~
Purchase Order Requested WO#:
f>rofect#:.
40007814 SSOW#;
Matrix (-.
Sample ~
i-IH'I ~ Solid
--Solid --Solid --Solid --Solid --Solid --Solid --Solid
--Solid
Solid 11
z ~
-.:;; ~~
i i ~ ~ ~ _g~~~Sl tu es~g5 ~ -=~~~!:: @ ::; ~ ~ ] g g ~ ~ ~ m ~ N ~
~~~£~:::-; a:itS<tNlma.o ~~~.,.;~~g
~t~~~ .~~J~~~}.~ v
I I I I I I I I
~ ~ ~
::: g t3 r::} Q ~ 0 ~ 0 ' • 0
~ fil ~ Q <( ~ <:> 0 0 0 <:> a ~ ~ ~
~
~ :!
~ 0
c 0 ;;.
l!f 6 7 ii: 0
~ ~ i ~ ~ ~~'.~: ~(. &E ~
J 1../I vl\-'i v
I I I I I
~
~ Q
~ t; ~
TestAmerica TI":!:: l..fu",Dffi_r.{ e,.-v3R0~Af- TE.STJ!'<G
COCNo: 400-61884-25981.1 Page:
Page 1 of3 'JOO#:
I-~ Preservation Codes:
lJ~ A- HCL M - Hexane t;. B-NaOH N-None ji< C-ZnA°"'te O-kNo02
~.t1:'. D- Nitric Acid P - Na204S ~::'.~'; E- NaHS04 Q - NB2S03 ~-~·'; F- MeOH R- Na2S203 ;;gt G-Amchior S - H2S04 ~;~: H -Ascorbic Acid T - TSP Dodecahydrate :;:,q,, 1- lee U -Aceton~ -~ J-OIWater V-MCAA ':"'"'. K-EDTA W-pH4-S 1-" L-EOA Z-Nhor(spocify)
"' Special !nstructionsfNote:
i:":~~:::::.:;;'
R A.00-132540 coc
i~ ~ Sample Disposal (A fee may be assessed if samples are retained longer than 1 month) 1CJCi,ible Hazard lderrtification
" Non-Hazard CJ Rammable OSkin Irritant D Poison B D Unknown CJ Radiological CJ Return To Cfient CJ Disposaf By Lab D Archive For Months
Deliverable Requested: I. !!, Ill, IV, Other (specify)
Empty Kft ReITnquished by:
Relinquished by:
Custody Seals Intact I Custody Seal No.: ti Yes a No
Date:
"baietfirOO'.". Company
I -11-1 omemnie: Company
Dale/Ti.me: company
Special Instructions/QC Requirements:
Time: MethOd of Shipment:
RecQived ti): l°'Jlt?-/17 {)C(ZI W?iif 'D •me: { Com;xiny
Received by: Datefr!!'TI!'!: Company
-~erTem;:um:rture(s)°CandO!Mr~~~ 1<o :7'L& • c.
;i
"U
"' (0 <D
"' .._, Q, ~ ,,. 0
t2 ~
;:;, 0 ~ .._,
TestAmerica Pensacola 3355 Mclemore Drive
Pensacola, FL 32514 '.phone {850) 474-1001 Fax: (850) 478-2671
Client Information
Chain of Custody Record
mJ;;)ohr.">o-> LlbPM:
Wilson, Jason A earner Trac!ting -No(s):
E-Mail: Cl~Cootact
Jennifer Lindquist Cornp:;!ny::
?~ q,:,g (~ liason .. wilson@testamericainc .. com
C-K Associates 'Address: D11<>o.rte Reque$llld:
17170 Perkins Road C<r. iTATRequasted {days): Baton Rouge State, Zlp: LA, 70810 Ft.one: PO#:
Purchase Order Requested
-~ :WO#:
l'[email protected] I ~~ Project Name: ?reject#: ~· Moffat & Nichol 40007814 Site: SSOYV#:
Sample Identification
:-~,;-:,::.,.~.;.: .. ,~;~~:::;.:~~~ :.~-:~--~:;~~~~-~~ ~-~;-~-:;:·:-~:::-->~:"$~.t ,, ... ~:0
R ;.-,o,c.\-e '\ i -11-n 1 1 ?~ I
Matrix
c-. ......
1~11 Solid -Solid -Solid -Solid -Solid -Solid -Solid -Solid -Solid -Solid
z ~ w
I " ~ z • ~
z : ~ !§
~ z E
~· ~
I 'Vf v
Analysis Requested
'""(~'§%!!if''-. .~¥·$_,._,_,_.if"~ - ..... ~---~:,_·-~ii; fi::. -§¥~~~~jt~'.
Test America n-IE~s::m;g,.~~"3-
COCNo:
400-61884-25981 .. 2 Page: Page2of3 Job#:
Proservation Codes:
.... A-HCL
""I-~ B-NaOH C- Zn Acelato
:...., D-Nl'.ficAcid E-NaHS04 F-MeOH
1-.;-1··8.- G· Amchlor ~ H-AscofbbAcid
,~4 ~~:w~ ·~-~.,: K-EDTA
L~EDA :@: ~ .. Other:
M-Hexane N-None 0-AsNa02 P-Na204S Q·Na2S03 R-Na2S203 S- H2S04 T - TSP Dodecallydrate LI-Acetone V-MCAA W-pH4-5 Z- other (Specify)
Special Instructions/Note:
'~.:_ ,-.;-;
[i
&e...,~~:-.:;-;,:_;~-:-~;::,~"*-:s~
'iiiifaible Hazard Identification
D Poison B D Unknown CJ Radiological
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
DRetum To Client CJ Disposal By Lab D Archive For Months Lf-.l Non-Hazard CJ Flammable DSkin Irritant Deliverable Requested: I, !!. JU, IV, Ottier (specffy)
Empty K"rt Relinquished by:
""'"""~"'!\. ... R(i!inquiShea ~
Refi'.lql.lished by:
Custody SeaJs Intact: I Custody Seal No.; !:.. Yes 6. No
Date: Date.Time.:
Ht-!'l Datatnme:
Date.Time:
Special Instructions/QC Requirements:
Method of Shipment
Ccmp""Y
7 012./ Company
Company Received by:, Date/Time: 1co·l"l',pany
Cooler Temporature{.s-} 0c and Other Rerr.arks:
c--~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
-u "' (Q (1)
~
"' (X)
a ~ ... 0
~ '3 0 ~
"
T eslAmerica Pensacola 3355 Mclemore D;ive
Pensacola, FL 32514 Phone {850)474-1001 Fax {850) 478-2671
Chain of Custody Record TestArr1erica TIUi.l..~!ffil!>'ENV!~ITT,;t. ~Tr.<l:G
Sam,,le;: fl./. . n f L3b PM: Client Information /'. ·ftlr:> {'CJ fJ J'l.50'\ WTiscin, Jason A
Carrier T i:Jcking NO(Sf. COCNo:
40Q..61884-25981.1 Cfient Comae<: P otie: LJ ? 0- E-Ma11: JenniferLindquist ,!)~ -i?t> /J7.So · [email protected]
Page: Page 1 of3
Company: Job#: C-K Associates
F;-;::'Perldns Road lTATRoq"°"""'°"' I~ C"r Baton Rouge
DueOate RcquestOO: r--,--,--,--An.,....•~ly"s_i_s r .... .i::.te.d
'.m· y·.· ' ... i .:..
l: ·=
t~~::~tion Cod::_ Hemm N-None O-AsNa02 P-Na2043 0,-N82S03 R-N:.2$203 S-H2s04
&a!e,Zip: LA. 70810
"")'j5 755 /OQO Email: [email protected] Project Name:
Moffat & Nichol 0"";.J.o, 'fo.c~f f/CJhor
PO#. Purchase Order-Requested IWO#:
Project#:
40007814 SSOW#:
~Ji
gr~ q
~~ ~ w
~
1~ -!
400-132588 coc
- '
. I j J ~ ~
O]j!~ w ~I" ~ c
: ~ - -;-g
} ! 3
T ~TSP Dodec:ahydrate U-Acetootl V-MCAA W-pH4-5 Z- other (specil)•)
. ··. ·.-·>.---'.'~~-~-
/lit/--<.. i 1-11-11 I '" 1<i b 1 solid 1 1 1 VJ vr vrvrvr "1 v ;,.,-:;.._
0Y '0
7 I 1.~;.g 0 1 Solid 1 1 x1 v1v'1 vr vrvr vr v
7J /3 ;,5t (!, I Solid I '1:. Solid ~, Solid ~"lg;~
~:;,r.'
-::::::~
-~~ Solid
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
CJ Return To Client DDisposaf By Lab CJ Archive For. Months
Possible Hazard Identification
D Non-Hazard D Flammable DSkin Irritant DPoisonB DUnknown DRa.diofogicaJ Deliverable Requested: I, n, Ill. IV. Other (specify) Special Instructions/QC Requlremerrts:
Empty Kit Relinquished by. Date: Time: ' I
' Method of Shipment: • • ~ !!
Oater~1me: ( '-· .,; /,. £ o-aierrmie; \[ ' ") OO:mpaoy /I. -1:>--11 W#f\l!f.., 1-i "'r 1 c · v y,,.
Jibrv!A) (U,, ""t:'.it-f{ i //;.;_/;/ j(p_ ~-Mt I R!>linquished by.
CustOOy Seals Intact !Custody Seal No.: t;. Yes .6. No
l°"*'JTime; m--. -1comp.a,.,Y , \Receive!l"b}~· T ··--- (Da:!¢JTome: /
eoo0<Tomperarurn<sJ<cs~ 1
. z,Z/O C. ,
Company
2. 7v~ 7K&
"U
"' "' CD ~
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a .... 0
~ '3 0 ~
"
. I ' I TestA~erica .Pensacola 3355 Mclemore Dnve ' Pensacola; FL ~514 Chain of Custody Record ~hone (859)474-1001 Fax (850) 478-2671
Lab PM: CanicrTn"ici:"fng No{~): blient ln~onnation '"'""Pcetv K; r Ii Wilson, Jason A criem CotrtaCt:
1~ennlfer ufidquist f>hone:
2&s-1;ss-100 o '""""' I [email protected] -t-KA.sso~ :Mo-ess: I
17170 PeOOns Road Due D<rte Reqt1=ed:
City.
Baton Rouge !TAT Requested {d<lyS):
.~\:\tj ""' r 1~· j IP,<Chase Ocdec Reque.ted~ I i -• . Ema!l: i [email protected] P1*ctName.: Moffar& rfichol
Si'~ NOLA I ,
Project""#: 40007814 'SSOW#:
I Sample Matrix
Type {~;:· , Sample {C=comp, ~oil,
lSample !kl.entffication Sample Date Time G= rab ITTaT=
i'.~"~::-:·~:'~ ;:-;.~~:: ,;_. ~:;::~·:~;~~~~:~-:.:~~~~'.::.'2~:__ -. If:~~~:.:~;:;~ ;f:::~_,:::·;._, ~~~~%~
c~-& 1I1:3! 11 I oq3r (.;. Solid
r1-?-7 ~--· G- Solid
ci-Z - ~ JOJO G ~""""""
[,J.<- q jQ'JC. r.,. l<;-Cl-1\-to !OUC. r ... s-~6,~ 1100 s vJ
1i§J I~
~alysis Requested
•;.t x u. x ~ n.< u.< >· 0 > 0 a.: ~ .o. .o. ~
:-g~ ~g~ fu :;·~; ;;~:t~ ~ ~ ~ g ~ ~ g ~ ~ ~ ~~~ fil~'.:..g § -~ ·i g .g ~ s g § ~ a ·~ .q- ~ ~ ~ g N ;;. J-~ ·.g ~ . . . . ~. . . v
I II \ I \ I \ nrm 7
f llT }. lv1 vlvlvY
TestAmerica ~L~t."1!0:>.~7,o;t,,'fESTI~
COCNo:
400-B1884-25981.3
::":;~ I of a.. Job#;
I-Prns•Mtt;on coo''"
A-He!.. M-Hexane B-NaOH N-Ncnc C-ZnAC9!a!9 O-AsN302 D - Nitric Acid P- Na204S E - NaHS04 Q- Na2SO$ F-MeOH R-Na2S203 G • Amehlor S - H2S04 H -Ascorbic />.cid T ·ISP Doclecahydrate 1 - roe u-Acetone J-DIWa!er V-MCAll. K-EDTA W-pH.4-5 t.·EDA Z-olt:et{speeiM
r.
Special [nstructions!Note:
~~~~:~·:·::~~::;;:;:2~~~1
m ---------
400.132550 coc ---
PO$Sibte Hazard Identification
CJ No~Hat:ard D Rammable CJSkin Irritant CJ Poisofl B D Unknown DRadiologlcal
Sample_Dis-poSir( (A fee may be assessed if samples are retained longer than 1 month)
D Re.tum To:Qfient D Di5P0.sal Bv Lab D Archive For Months Deliverable Requested: I, 11, Ill, JV, Other (specify}
. . I Em~ kjt Relinquished by;
Fl'PY, ""~nz.::: ~ . " , .. R'"''''"j'"_:' Vl~ 21. v
• ,,,-.Jil
Ref"'GlJWie<lby:. l I
Custtj:ly Seals Intact ICµstody Seal No..: 6. r"fes · b. No
'"
IDate:
j113J17 !-Jth-~l O.fo("rr~'".2 -\~
tc..-l 1 I -4b , Datefnrr.e: 1
C".Qmpany
~/,1 \ 1-\
Company
'Special !nstructio)1s/QC Requirements: i
Time:
R(i"'_"" iJ ,#/./ R"""""""" Iv /}
--···-1 . .,...,
R='-<d°'cf/ F/7/
Melhiid of ShipriWlt:
Date/Time
l /,",//7 O'ateffime:
ll\if/n
dJ- Compa~J't·
I Company'"
l:>o'L Com~ny I)'.\
=·~"""'j'"'"'·c-ll"''"°""""' t .o·c-' t «re. -'2 _o·c 2 , \ ·c. 'I?G.
I I
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~ j;:; 0 ~ -...
: I TestAmerica Pensacola . I -3355 McLrmore Drive
l(ensaco!~ FL 32514 Phone {8~) 474-1001 Fax (850) 478-2671
Client frtformation Cfient COr!bi:t:
~ennffer ljndquist
Chain of Custody Record
Wl!son, Jason A "'·- f<CA.v 1-<J rl<.. lab PM:
E-Ma:l: f lffillnn_wi~on@testamericai~c.com
Phone· t
. a.2<:,-1S'S-f600
Carrier Tracking No(s):
Test America nu;:~ II'< GN'lilaO~.o,l,. TSS>fNC,1
COCNo:
400-61884-25981.4 Paga:
Pa9~ 01.z:f'..a Ob#:
:Company: !
C-K Asso~ates j Analysis Requested iMaress: I 17170 Pej1<ins Road
~" I BalonRoi;ige ~Zip::; LA, 7081tj Ph00$:
! I ,Email: I [email protected] Project Naflie:
:Moffat & ~icho! ·~e: ND'-k
Due Date Requested:
TAT Requested (days):
Pb#: Purchase Order Requested WO#;
Projec:.#:.
;40007814 SSOW*
Sample Type
(O:comp, J Sample Sam le ~enfrfication Sample Date Time G= tab' ~{{':@~~;;:i:<;:~'-~~~~~·:...~v, -,..- -~·~."._.,.~1"~, -~ > o'< ""·~tf/'.:-:-;_ 4:;,~-;:~~~:;i}" • ··~:::~~1 ~~
Matrix c-. ,.,.., ,._..,
~B-~ 11 12fr1 llloo r-.-1;.~ So!ld
Watec
Wat..-
Wat..-
.::'.;;..~ ~·;:,~pf>;;_<--..:r.·"f'_ ~-..;::;,· .;:::!;~ '~""'l'"f~~=•"'"'
Preservation Codes:
A->-lCI.. .,,, B-NaOH
~'i{"· C <Zn Acetate ~ D·Nltf.cAOd ~~ E-NaHS04 <·~~ F-MeQH !J.<i>i G-Amch\or ~ H-AscorbicAcid 4~ !-foe
J-DIW-aw,r K·EDTA L·EOA
M- He:oane
N--0-AsNa02 P-Na204$ O-Na2So3 R-Na2S203 S-H2S04 T -TSP Dodet:ahydra\e U-Acek.ine V-MCM W-pl-14-5 Z:-olher(spedfy}
l""w. flJ #$1JJ '.iC!. e,,_en ict ,
!~~, Special Instructions/Note:
... ~'.
li
_;;.,..
' I ' I ~
I
•
11 •. "" ,
' ! , I I '
Possibfb Ha:rard fdentification
D Noli-Hazard CJ Rammable DSkfn Irritant D Poison B CJ Unknown D Radiological
jDe1iVerab!e Requested: 1, l!,.11!, IV, Other (specify)
Empty Kit Relinquished by:
;R°'"llt~ j • , • . . 'jR.Ooq,.. byc (fl/!lf Jj_ ' 1/1 .,,.-//
~' Rei;nq,,;s.'iQd t>y:. i
I ' Gust.of!~ Seals Intact: fCUsi:ody Seal No.:
Ll (Yes 4 No
-,Sample Dispos<il (A fee maybe assessed if samples are reteined longer than 1 month)
CJ Return To blient D Disposal By Leb CJ Archive For Months Special lnstructiohs/QG Requirements~
I (Time: fMe>lhoci of Shipment -
Cc:mpany -~
eom,,.,.,,
R~"t::~~ R.-.byc ! jl
RecelvOOby: I I
Cooler Tempei3ture(s) °C and Other Remar1cs:
I
'''+-'''
~~i~.--f~
Da~/17 r9. Com~ ;t:-Oatarr.Tne: ' COOi~y
DatE:/Tiine:: &pany
.-.. .,,.-
Tpaanat
Tin
R
THE LEADER IN ENVIRONMENTAL TESTING
ANAL YTICAl REPORT TestAmerica Laboratories, Inc. TestAmerica Pensacola 3355 Mclemore Drive Pensacola, FL 32514 Tel: (850)474-1001
Tes!America Job ID: 400-132588-2 CHent Project/Site: Moffat & Nichol
For: C-K Associates 17170 Perkins Road Baton Rouge, Louisiana 70810
g,-w:1-.-Attn: Jennifer Lindquist
Authorized for release by: 211412017 1.:52:23 PM
Jason Wilson, Project Manager I (251 )706-3217 [email protected]
he test results in this report meet all 2003 NELAC and 2009 TN! (equirements for accredited rameters,- exceptions are noted in this report. Tl1is report· may not be reproduced except in full, ct with written .approval fron1 the laboratory. For questions please contact the.Project Manager t/1e e~maif address or telephone nurnber listed on this page.
his ·report has been electronically Sig.ned and authorized by the signatory. Electronic signature is tended to be the legaf/y binding equivalent of a traditionally handwritten signature.
esults relate only to the items tested and the sample(s) as received by the laboratory.
Client C-K Associates Project/Site: Moffat & Nichol
Table of Contents
TestAmerica Job ID: 400-132588·2
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Page 2 of9 T estAmerica Pensacola
2/14/2017
Narrative
Case Narrative Client: C-K Associates Project/Site: Moffat & Nichol
Job ID: 400-132588-2
Laboratory: TestAmerica Pensacola
TestAmerica Job ID: 400-132588-2
Job Narrative 400-132588-2
Comments No additional comments.
Receipt The SE\mples were received on 1/12/2017 4:97 PM; the samples arrived in good condition, properly preserved and, where required, on ice. The tempeJatures of the 3 coolers at receipt time were 2.2° c, 2.4° C and 2.7° C.
Metals No analytical or quality issues were noted, other than those described. in the Definitions/Glossary page.
Organic Prep Method(s) 1312: The sample had a noticeable amount of water in it, however the sub-sample did not yield any filtrate from the wet sample. An unaccounted difference of 7 .7 percent between the initial sub-sample and the final portion applied to pressure filtration indicates towards a loss of liquid. The affected sample is as follows: CK-1 (400-132588-1).
No additional analytical or quality issues were noted, other than those descrlbed above or in the Definitions/Glossary page.
Page 3 of9 TestAmerica Pensacola
2/14/2017
Client: C-K Associates Project/Site: Moffat & Nichol
Lab Sample ID
400-132588-1
Client Sample ID
CK-1
Matrix
So!ld
Collected
01/11/1711:10
Received
01/12117 16:57
Sample Summary
Page4 of9
T estAmerica Pensacola
2/14/2017
TestAmerica Job ID: 400-132588-2
Client: C-K Associates Project/Site: Moffat & Nichol
Client Sample ID: CK-1 Date Collected: 0111111711:1.0 Date Received: 01112/1716:&7
Method: 6010C ·Metals (ICP) • SPLP East Analyte Result Quallfier RL
0.010
MDL Unit
0.0020 mgfL Lead 0.0025 J
0
TestAmerica Job ID: 400-132588-2
Lab Sample ID: 400-132588-1 Matrix: Solid
Prepared
02110/17 08:54
Analyzed
02/10/17 17:03
011 Fae
1
Client Sample Results
Page 5of9
TestAmerica Pensacola
2/14/2017
Definitions/Glossary Client: C-K Associates ProjecVSite: Moffat & Nichol
TestAmerica Job ID: 400-132588-2
Qualifiers
Metals
Quallner Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present In this report.
• Listed under the "D~ column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free liquid
CNF Contains no Free liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fae Dilution Factor
DL, RA, RE, IN Indicates a Dilution,. Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concenlration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable ~oncentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL If shown)
POL Practical Quantitafion Limit
QC Quality Control
RER Relative error ratio
RL Reporting limit or Requested Limit (Radiochemistry)
RPO Relative Percent Differen'ce, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEO Toxicity Equivalent Quotient (Dioxin)
Page 6 of9
T estAmerica Pensacola
2114/2017
QC Sample Results Client: C-K Associates ProjecVSite: Moffat & Nichol
Method: 6010C ·Metals (ICP)
Lab Sample ID: LCS 400-34174412-A Matrix: Solid Analysis Batch: 341902
Analyte
Lead
Lab Sample ID: LB 400-34142411-D Matrix: Solid Analysis Batch: 341902
Anatyte
Lead
Lab Sample ID: 400-132588-1 MS Matrix: Solid Analysis Batch: 341902
LB LB
Result Qualifier
<0.0020
Sample Sample
Analyte Result Qualifier
Lead 0.0025 J
Lab Sample ID: 400-132588-1 MSD Matrix: Sollcl Analysis Batch: 341902
Sample Sample
Analyte Result Quallfler
Lead 0.0025 J
Spike
Added
1.00
Spike
Added
1.00
Spike
Added
1.00
RL 0.010
LCS LCS
Result Qualifier Unit
0.890 mglL
MOL Unit
0.0020 mgfL
MS MS Result Quallfier
0.929
MSO MSO
Rt!sult Qualifier
0.913
Unit
mg/L
Unit
mgfL
Page 7 of9
TestAmerica Job ID: 400-132588-2
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 341744
o/nRec.
O o/PRec Limits
89 B0-120
Client Sample ID: Method Blank B Prep Type: SPLP East
o Prep_ared
02/10/17 08:!54
D %Rec
93
Prep Batch: 341744
Analyzed
02110/17 16:47
Dll Fae
1
Client Sample ID: CK-1 Prep Type: SPLP East
Prep Batch: 341744 0/aRec.
Limits
75 - 125
Client Sample ID: CK-1 Prep Type: SPLP East
Prep Batch: 341744 %Rec, RPO
Limits
75 - 125
RPO Limit
2 20
TestAmerica Pensacola
2114/2017
Lab Chronicle Client: C-K Associates TestAmerica Job ID: 400-132588-2
ProjecUSite: Moffat & Nichol
Client Sample ID: CK-1 Lab Sample ID: 400-132588-1 Date Collected: 01/11/1711:10 Matrix: Solid Date Received: 01/12/17 16:57
Batch Batch 011 1n1t1a1 Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab SPLP East Leach 1312 77.13g 1542 ml 341424 02/08117 11:10 RMC TAL PEN
SPLP East Prep 30:10A 50 ml 50mL 341744 02110/17 08:54 KWN TAL PEN
SPLP East Analysis 6010C 341902 02110/17 17:03 SEH TAL PEN
Client Sample ID: Method Blank Lab Sample ID: L8400-341424/1-D B Date Collected: NIA Matrix: Solid Date Received: N/A
Batch Batch 011 lnltlal Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab SPLP East Leach 1312 100.00 g 2000 ml 341424 02108117 11:10 RMC TAL PEN
SPLP East Prep 3010A 50ml 50ml 341744 02/10/17 OB:54 KWN TAL PEN
SPLP East Analysis 60100 341902 02/10/17 16:47 SEH TAL PEN
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-3417 44/2-A Date Collected: N/A Matrix: Solid Date Received: N/A
Batch Batch 011 Initial Flnar Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 3010A SO ml 50 ml 341744 02/10117 08:54 KWN TALPEN
Total/NA Analysis 60100 341902 02/10117 17:00 SEH TAl PEN
Client Sample ID: CK·1 Lab Sample to: 400-132588-1 MS Date Collected: 01/11/17 11:10. Matrix: Solid
Date Received: 01/12/17 16:57
Batch Batch 011 Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Nu.mber or Analyzed AnalYS:t Lab SPLP East Leach 1·312· 77.139 1542 ml 34'1';i24 02/08/1711:10 RMC ... TAL PEN
SPlP East Prep 3010A 50 ml 50ml 341744 02/10/17 08:54 KWN TAl PEN
SPLP East Ana.lysis ~010C 341902 02/10/1717:12 SEH TAl PEN
Client Sample ID: CK-1 Lab Sample ID: 400-132588-1 MSD Date Collected: 01/11/1711:10 Matrix: Solid
Date Received: 01/12/1716:57
Batch Batch 011 Initial Flnal Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed -Analyst Lab SPLP East Leach 1312 77.13g 1542 ml 341424 02/08/17"11:10 RMc TAL PEN
SPLP East Prep 3010A 50 ml 50mL 341744 02!10/17 08:54 KWN TAL PEN
SPLP East Analysis 60100 341902 02/10/17 17:15 SEH TAL PEN
Laboratory References:
TAl PEN= TestAmerica Pensacola, 3355 Mclemore Drive, Pensacola, FL 32514, TEL (850)474-1001
TestAmerica Pensacola
Page 8 of9 2/14/2017
-0
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Q, ID
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T es'tAmerica Pensacola 3355 McLemore O)ive
Pensacola, FL32514 Phone {850) 474-1001 Fax {850) 478-2671
Chain of Custody Record
Som"-;· "/ . fl , f /' il-tfo (d J.r, fl50'\
Lcl>?M: CamerTr:ickins No(s); Client Information Wilson, Jason A C~entConiact:
!Jennifer Lindquist Pli"d;".!;is- 13''? /6'30 E-Majl:
[email protected] company: C-K Associates
IM'= I I' r7170 Perkins RoodTAT Req=stcd (day:>); c°" Due Date RequestOO::
Baton Rouge iState. Zio: LA, 70810 Phone:
~.:!5 ?55 fOQO Email: [email protected];om Project Name;
Moffat & Nichol
5'.";J_o, Yo.c~f fiqhor
P01'
Purchase Order Requested WO#:
Project#.:
40007814 SSON#:
Sample Matrix Type .(--.....
Sample ~ Sampkl Identification Sam le Date
1 lTAnalysisT.j-
1
,. ·~ l· ; I' -· ,,
I 400..132588 coc -! -..1-~~ n.
~ g <()I -
z
i I ~ > • ~ £: .! z
it I I,; ~ .:i:: ~ •• _ .,,, .. =
g 111 ~: ~.~ ~- !: ~ ';_~!
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:<~. -
• g ~- ~ ..I
'.§ :ii ~ ~l ~ 8 5 ~ m .g ~ o . .., a
0
• <:goo-<~ g 0 0 :;:: 12: 0
~~~g_;:~ ttl <>.· 0 :m 0 ·~~g~~~ r~.:i;l~~ .. gg
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TestArnerica n-tli. :.EA-"'B': •1' Sr."!l~ONJ..SW~ 'f!:ST;:<!G
COCNo:
1400-61884-25981.1 Page: Page 1 of3 Jo!:>#;
:·f.;;1: Preservation Codei:
~;r ;=~~H ~~~=r.e '\."~ C-ZnAcetate O-A$N302 ·:~,.,.m 0- NltricAcid ~4> E- NaHS04 ~";0 F-~OH · ',~·~: G - Amch1or I~~~/ H-AscortlicAcid :'/~~,, I-lea ~~ J-D1Water ·,o· K-EDTA
0 ··""'~
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P·Na2CKS Q-Na2S03 R-r-r..zs2os S-H2S04 T ~TSP D:x,iecahydrate u -A<:e:JJ~ V-MCAA W-pH4-5 Z - o!her (specify)
~1-.;.·~:A ~ m. Special lnstructions/Note:
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Sample Disposal (A fee may be assessed if samples are retained fongertharr 1 month)
D Retum To Client CJ Disposal By Lab D Archive For Months
Possible Hazard ldentific<ition
ONon-Hazard DRammabfe DSAfnlrritant DPoisonB 0 unknown DRadiofogicaJ
DeliYerable Requested:!, U, !I!, IV, Other (specify) Special !nstructtons!QC Requirements:
Einpty Kit Relinquished by: jDate: jTime: ~ jMe1hOO <ifShipnent
Custody Seals Intact I Custody Seal No.: t:,. Yes /:. No
v
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