ASSESSMENT AND CORRECTIVE MEASURES TREMONT LANDFILL · quality data from assessment monitoring dating back to January, 1990. A Corrective Measures Study (CMS) for the Tremont Landfill

I rcnionl I il\ Landfill SiteDoc. #76 "..

STATUS OF

ASSESSMENT AND CORRECTIVE MEASURES

TREMONT LANDFILL

Prepared for

TREMONT LANDFILL COMPANYTremont City, Ohio

Prepared by

EAGON& ASSOCIATES, INC.Worthington, Ohio

February 6,1997

Submitted by:

Frank L. MajchszakHydrogeologist

Approved by:

Herbert B. Eagon,/rf CJHydrogeologist

EAGON & ASSOCIATES, INC.100 Old Wilson Bridge Road, Suite 320

Worthington, Ohio 43085(614)888-5760

TABLE OF CONTENTS

Page

INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

BACKGROUND . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . i

CURRENT ACTIVITIES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

RESULTS OF GROUND-WATER QUALITY SAMPLING . . . . . . . . . . . . . . . . . . . . . . . . . 3

DETERMINATION OF RATE, EXTENT, AND CONCENTRATION . . . . . . . . . . . . . . . . 4

SUMMARY OF APPENDIX I AND APPENDIX H ORGANIC COMPOUNDDETECTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

TARGET CONCENTRATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

REFERENCES CITED . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

FIGURES

Figure 1. Monitoring Well Location MapFigure 2. Water Levels and Flow Directions on June 5, 1996Figure 3. Water Levels and Flow Directions on November 25,1996Figure 4. Hydrographs of Wells Located in and East of the Assessment AreaFigure 5. Hydrographs of Wells Located in and West of the Assessment Area

TABLES

Table 1. Water-Level Elevation DataTable 2. Summary of Analytical Results _Table 3. Results of Statistical AnalysisTable 4. Summary of Appendix I and Appendix n Organic Compound DetectionsTable 5. Parameters Requiring Target Concentrations

APPENDICES

Appendix A. Analytical Results and Field MeasurementsAppendix B. Trend PlotsAppendix C. Correspondence Dated July 10,1992

Eagon & Associates, Inc. -i- February 5, 1997

INTRODUCTION

The purpose of this report is to present the results of the annual assessment sampling of the

Tremont Landfill, which was performed on November 25,1996. The location of the assessment areais shown in Figure 1. This report also fulfills the requirement for a Quarterly Assessment/Corrective Measures Activities Report for the Fourth Quarter, 1996 (October - December) and

includes the semi-annual determination of the rate, extent, and concentration of leachate-derivedconstituents in the ground water. Tables 1 and 2 include the most recent water level and water-

quality data, respectively. Also included is an updated list of constituents for which correctivemeasures target concentrations are required. A revision to the Corrective Measures Study (CMS)with the appropriate modifications to the target concentrations is being prepared by Hull andAssociates, Inc. and will be submitted separately.

BACKGROUND

The findings of a ground-water assessment for the Tremont Landfill performed in accordance

with OAC 3745-27-10 (dated March 1,1990) were submitted to the Ohio Environmental ProtectionAgency (OEPA) in January, 1992. The final assessment report (Eagon, 1992) included ground-waterquality data from assessment monitoring dating back to January, 1990. A Corrective MeasuresStudy (CMS) for the Tremont Landfill (Hull, 1992) was prepared pursuant to OAC 3745-27-10 (F)(dated March 1,1990) and was submitted to OEPA in July, 1992.

The CMS included an assessment of the risks posed to locafresidents, site workers, andnearby environmental receptors. The pathway analysis indicated that a viable exposure pathway to

local residences was not present, nor could a future pathway be reasonably postulated within or

outside Facility boundaries. The potential ecological effects associated with discharge of ground

water to Chapman Creek were evaluated by analysis of available ambient water quality criteria, and

Eagon & Associates, Inc. -1- February 5, 1997

it was concluded that degradation of the stream had not occurred. Even in the absence of

implementing corrective measures, conditions at the Facility at the time that the CMS was submitted,

did not pose unacceptable risks to the public health or to the environment.

By early 1994, all of the corrective measures proposed in the CMS were implemented except

the final cap on the landfill, and ground-water extraction with off-site treatment and disposal. The

construction of the final cap was completed in May, 1995. During a meeting regarding the TremontLandfill Closure Plan on July 18, 1994, OEPA requested that the Facility consider source controlas an additional corrective measure. In response to this request, the recommended correctivemeasures were modified to include source control in a phased approach; with Phase n (source-control pumping) and Phase in (ground-water extraction) to be implemented, if necessary (Eagon,1994).

The phased approach was considered appropriate because, by late 1994, it appeared thatcorrective measures already employed were working. The target concentrations proposed hi the1992 CMS essentially had been achieved and it seemed prudent to allow more time for those

corrective measures to become fully effective (Eagon, 1994). Through June 1995 the trend inconcentrations of most constituents of concern were generally downward, and no primary MCLswere exceeded in wells located closest to the apparent source of leachate-derived contaminants(Eagon, 1995).

Action levels and criteria for implementation of Phases n and in were proposed (Eagon,1995). However, Ohio EPA requested that the list of constituents for which target concentrationsare required, be revised based upon statistical analysis of the assessment water-quality data. Aminimum of four sets of data are required for statistical analysis. With the June 1996 semiannualsampling event, the Facility had acquired four data sets with which meet the criteria of OAC 3745-

27-10 (dated June 1,1994) for the assessment wells.


The data from the downgradient assessment monitoring wells A89-2, A89-3S, A89-3D, A91-

4S, A91-7S, and M-2 have been statistically evaluated using interwell comparisons (Eagon, 1996).Statistical methods used to evaluate the water-quality data are explained and discussed in the August

8,1996 report. Complete results of the statistical testing are included in Appendix C of that report.Table 3 (from Eagon, 1996) summarizes the results of the statistical testing for inorganic parameters

which had at least four observations at the time of testing. All Appendix I organic compounds thathistorically have been detected above reporting limits hi any assessment well are listed on Table 2.

CURRENT ACTIVITIES

In addition to normal post-closure care and maintenance, the only assessment activitiesperformed on site during the fourth quarter 1996 (October - December) were the annual samplingof assessment wells perfonned on November 25, and the associated measurement of water levels inwells and gas probes in and adjacent to the assessment area. The laboratory results of the waterquality analyses are included in Appendix A. The water-level data are included in Table 1 alongwith previously-collected measurements.

RESULTS OF GROUND-WATER QUALITY SAMPLING

Water quality data for the November 25,1996 sampling event are listed in Table 2, which

includes data from assessment wells dating back to 1990. Only the Volatile Organic Compounds(VOC) that have been detected in the assessment wells are listed in Table 2. Similarly, inorganicparameters that were below the detection limits in all wells for all samplings are not included inTable 2.

Updated trend plots for the most important assessment parameters and assessment wells are

presented in Appendix B. The trend lines have the effect of mathematically normalizing (by linearregression analysis) the data collected after July, 1992 and, therefore, represent water-quality trends

since implementation of corrective measures. As shown on the graphs, current trends generally


continue to be downward. The exceptions for inorganic parameters are slightly increasing trends for

TDS at wells A89-2 and A89-3D and for chloride at wells A89-3S and A89-3D. The chloride trend

at M-2 is downward. The only organic constituents which show a slightly increasing trend are

chloroethane at M-2 and 1,1 dichloroethane at A89-3S. However, the November 1996 chloroethaneresults were non-detect (<1.0 (tg/f) in both M-2 and A89-3S. 1,1 dichloroethane results were non-

detect (<0.5 g/f) in M-2 and 6.1 fig/t in well A89-3S. Neither compound has an established MCL.

DETERMINATION OF RATE. EXTENT. AND CONCENTRATION

Figures 2 and 3 show the direction of ground-water flow in and near the assessment area atthe time of the last two sampling events (June 5,1996 and November 25,1996). The gradients anddirection of ground-water flow represented by these maps are consistent with maps submitted inprevious status reports (Eagon, 1994, 1995 and 1996). The consistency of up/down gradientrelationships among various wells, and the synchronous nature of water-level fluctuations, isillustrated by Figures 4 and 5 which are updated hydrographs of various well groupings. Conditions

in the assessment area are characterized as consistent and the November 1996 data indicates thatthere has been no appreciable change in the rate or extent of contaminant migration.

The degree of variability in the concentrations illustrated by the water-quality data

compilation (Table 2) and the updates of the water quality trend plots in Appendix B is fairly small.The concentrations of arsenic, iron, benzene, chloroethane, and o-dichlorobenzene (1,2) are trendingdownward at well A89-2 near the property line. Only TDS is showing a slightly increasing trendat this location. However, the concentration of TDS is trending slightly downward near the inferredsource area (wells M-2 and A89-3S) or slightly upward in the case of well A89-3D. The

concentrations of most VOCs in the source area also are trending downward, the exceptions being

slight increases in chloroethane in M-2 and 1,1 dichloroethane in A89-3S. In spite of the slightlyincreasing trendline, the actual chloroethane concentration in M-2 was lower in June, 1996 than in

November, 1995 and was non-detect in the most recent (November 1996) sampling. No VOCs haveever been detected in A89-3D.


SUMMARY OF APPENDIX I AND APPENDIX II ORGANIC COMPOUND

DETECTIONS

Table 4 lists all Appendix I and Appendix II organic compounds that were detected in themost recent (November 25, 1996) sampling. Nearly all of the detected compounds are on the

Appendix I list, which is a subset of the Appendix II list The sample labeled 96-300 is a blindduplicate from well A89-2. As seen on Table 4, duplication of the Appendix I results is excellent.However, this in not the case for Bis (2 ethylhexyl) phthalate and Di-n-octyl phthalate, which are

the only two Appendix n compounds detected hi any of the assessment wells sampled on November25, 1996. In the case of each of the phthalate compounds reported to be present hi the A89-2sample, neither was reported above the detection limit in the blind duplicate sample (96-300).

Bis (2 ethylhexyl) phthalate was the only non-Appendix I, Appendix n organic compoundreported hi previous Appendix n samplings. Phthalates are known to be ubiquitous in theenvironment and difficult to quantitate at low concentrations. These and other facts weredocumented in a letter dated July 10,1992 and addressed to Mr. Brian Nickel of the OEPA SWDO.A copy of this letter is included in Appendix C of this report.

The field/method blank, which is labeled FB-1, (consisting of a freshly opened bottle ofdistilled water in which latex gloves and bailer string used for sampling are immersed for a short

time) has a higher reported concentration (11.0 /ig/f) of bis (2 ethylhexyl) phthalate than any of theassessment wells. The detection of carbon disulfide in the field/method blank also is consistent withprevious demonstrations that we have made Unking sporadic detections of carbon disulfide hi groundwater samples with the use of unpowdered latex gloves for sampling. (We also determined that

powdered gloves, which we do not use for sampling, may introduce much higher levels of carbondisulfide, possibly other organic compounds, and zinc).


TARGET CONCENTRATIONS

The parameters which have been determined to be above background concentrations, and

require target concentrations to be set, are listed in Table 5. Of the 23 analytes on the list, five

(Numbers 74,75,76,78, and 79) were added subjectively because statistical analysis could not be

performed. These analytes are on the annual sampling list and only three sets of unfiltered data have

been collected since changing sampling procedures after June 1,1994. All five parameters have

concentrations which are above the concentrations at upgradient well M-4 and are, therefore, added

to the list If subsequent statistical analysis, based on additional water-quality data, demonstratesthat any of the five parameters is not above background, it subsequently can be deleted from thetarget concentrations list

Target concentrations previously proposed are being reviewed and target concentrations will

be established for parameters that have been added to the list in accordance with OAC 3745-27-10

(F) dated June 1, 1994. A new list of proposed target concentrations along with proposed action

levels and criteria for implementation of Phase n and Phase HI corrective measures will be submitted

in a revision to the CMS.


REFERENCES CITED

Eagon & Associates, Inc., 1992. Ground Water Assessment, Tremont Landfill, Tremont City,Ohio, consultants Report, 36 pgs., 25 figures, 8 tables, 8 appendices.

Eagon & Associates, Inc., 1994. Status of Assessment and Corrective Measures (Appendix G) inGround-Water Monitoring Plan, Tremont Landfill, Clark County, Ohio. Consultants Report,22 pgs., 4 figures, 4 tables, 8 appendices.

Eagon & Associates, Inc., 1995. Status of Assessment and Corrective Measures, TremontLandfill. Consultants Report, 13 pgs., 8 figures, 4 tables, 1 appendix.

Eagon & Associates, Inc., 1996. Status of Assessment and Corrective Measures, TremontLandfill. Consultants Report, 6 pgs., 5 figures, 4 tables, 3 appendices.

Hull & Associates, Inc., 1992. Corrective Measures Study for the Tremont Landfill Facilitylocated on Snyder-Domer Road, German Township, Clark County, Ohio. ConsultantsReport, 85 pgs., 24 figures, 11 tables, 2 appendices.


FIGURES

100 0 100 200 300 400

GRAPHIC SCALE FEET

iECENQ

o DETECTION MONITORING WELL

• ASSESSMENT MONITORING WELL

D SPECIAL PURPOSE WELL

r

SEDIMENTATION BASIN

ASSESSMENT AREA-

CHAPMAN CREEK

FIGURE 1. MONITORING WELL LOCATION MAP

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91-S986.00

SOIL BORINGS

GAS MONITOR PROBES

MONITORING WELLS

RESIDENTIAL WELLS

CREEK MEASURING POINTS

WATER LEVEL CONTOUR

FLOW LINE

MEASURED WATER LEVELS

FIGURE 2. WATER LEVELS AND FLOW DIRECTIONS ON JUNE 5. 1996

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91-S•$.985.09

SOIL BORINGS

• GAS MONITOR PROBES

MONITORINC WELLS

O RESIDENTIAL WELLS

X CREEK MEASURING POINTS

— 983-" WATER LEVEL CONTOURaow LINE

SCALE IN FEET

FIGURE 3. WATER LEVELS AND FLOW DIRECTIONS ON NOVEMBER 25, 1996

988EAGON& ASSOCIATES. INC. 988

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A91-8S

A91-9S

H 982

98104/01/91 10/01/91 04/01/92 JO/01/92 04/01/93 10/01/93 04/01/94 10/01/94 04/01/95 10/01/95 04/01/96 10/01/96 04/01/97

TRZMONT/ASSESS6.GRF TREMONT LANDFILL ASSESSMENTFIGURE 4. HYDROGRAPHS OF WELLS LOCATED IN AND EAST OF THE ASSESSMENT AREA

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04/01/91 10/01/91 04/01/92 10/01/92 04/01/93 10/01/93 04/01/94 10/01/94 04/01/95 10/01/95 04/01/96 10/01/96 04/01/97

TREMONT LANDFILL ASSESSMENTFIGURE 5. HYDROGRAPHS OF WELLS LOCATED IN AND WEST OF THE ASSESSMENT AREA

TABLES

TABLE 1.WATER-LEVEL ELEVATION DATATREMONT LANDFILL ASSESSMENT

PAOE10P2

iliDATE

04/22/9105/22/9105/31/9106/03/9106/12/9106/20/91

07/120108/200109/240110/23/9112/020101/08/9202/2(0203/300204/29/9207/14/9208/31/9210/05/9211/09/9201/25/9302/08/9304/27/9306/020307/200310/27/9301/24/9402/04/9404/11/9411/28/9401/30/9504/03/9506/01/9507/27/9510/05/9511/27/9501/17/9606/05/96

98421984.17984.0698341983.769903898431984.669873698430984.4798429984.12983539844098431984.77984.489S4.72984.18984.1698431984.68

*9843698423984.65984.449843098433984.46985.16

11/25/96 98430

98734

98738987279(7.11987.02

9(652987.03987.44987329873998728987.16986.97986.74987399873198743987.49987.63

9(7.47987.67

986.70986.75987.11986.92986.83986.79986.91987.65986.73

9(239

98X56

98X46

984209(4.15 98231

984.10 98224984.05 9(22398348 9(231984.06 9823398422 98X43

98435 98X5198435 98X65984.41 98X83

98429 983.05984.04 98231983.84 98X16983.74 98223

984.68 98321

98431 98230984.72 9832098421 98239

983.0298X139(229

98423 98X7498437 983.05

98X02984.12 98X16984.01 98X17984.48 98243984.13 98X86

984.01 98X67

984.08 98X8398431 983.09985.45 98327984.12 98230

ilii

98X96

983.05

98X71

98X4298X3998X4398X4598X3998X5698X6298X7698X94983.2798X4598230982399833798X659833598X53983.1698X319(233982499832898X1498X299822798X92983.0498X7698X91983269833598X57

98331

983.14 98320983.08 983.13983.08 983.149(3.18 9(32498320 9832498327 98332

98332 9833898330 98337983.68 983.74984.18 98428

983.19 98325

983.04 983.10

983.11 983.19

984.16 98422983.40 983.45984.14 9842098328 98334983.92 983.98

983.49 98332984.03 984.11

98X94 98X9998X96 983.02983.63 983.67984.06 984.19

983.46 98332983.62 983.6998428 98430984.17 9842}98332 98337

98324983329833798336983.749842898325983.10983.1898424983.469842298335984.00

98334984.13

9(3.00983.01983.69984.1798331983.68984329842598337

98X70

98X68

98236

98X4798X4198X41982319823398X6098X679824598X97983.4598X479823498X41983.4398X679833998236983.1998X2998X749(2419833398X1798X2998X3198X909833698X87983.01983.679833498X67

98X84

98X82

98X70

98X59982349823498X6398X6598X71

98X7998X97983.09

98337

98237

98X45

98X53

98334

98X78

983.4998X66

98328

98X40

9824598X90983.43

98225

98X38

98X39

98X99

983.44

98X96

983.10983.78983.6398X77

985.76

985.10

984.96

98443

9843598428984.17984.06

98357984.46

985.0198448985.06

984.67

984.61

984.41

984.18

98633

98539

98634

985 .29

98537

984.45

985.13

98538986.4398347

9843298433

98441

98436

984.44

984.48984.699S5.4S98435

983.42

98X76

98X71

98X60

98X4598X379(2339(23798X4298232

98X6598X7698X99

98X93

98X44

98X28

98232

98332

98X759833498X60

983.1298X259(237983.029(32198X09982269823198X9498X7298X63

98X80983.059833298X50

98244 98X0998X16 981.95

98X12 981.97

98X02 98144

98151 9814198145 9803698145 981.6498153 981.6198157 9814998X06 981.93

98X13 981.7898229 981.9498X43 981.80

98X76 981.9598148 981.71981.75 981.63

98143 981.7298X82 98X0898X09 981.7698X80 98X10

98158 981.7998X64 981499815898X179(237 9(14798X76 98X18981.67981.78 98149981.79 9813998X37 981.8898X62 981.77

98X22 980.90

98X37 981.7498257 98X2398X84 981.8798X06 98137

'H-l WM* repltcfdby MW-IR OM S/24/94. The tew meimriagpoimt clcvttioi it 1013.64

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TABLE 1 (cont'd)WATER-LEVEL ELEVATION DATATREMONT LANDFILL ASSESSMENT

PAGE 2 OF 2

MlDATE

04/22/9105/22/9105/31/9106/03/9106/12/9106/20/9107/12/9108/20/9109/20/91100319112/02/9101/08/9202/28/9203/30/9204/29/9207/14/9208/31/9210/05/9211/09/9201/25/9302/08/9304/27/9306/02/9317/2Q/9310/27/93>l/24/940/04/94H/ll/9411/28/94H/30/9S

H/03/95W/01/9S)7/27/9S10/05/9511/27/95IV17/96>6/OS/9611/25/96

984.11

983.41

9833898325

9*3.1598347983.089*3.199(3219*3269*3339*331983.96984.18983.18983.02983.12984.16983.42984.159832998353982.96983479(3309(445(9*30)9)(9*251)(9*346)(9*338)(984.03)(983.43)

(98338)983.90(984.13)

(<98329)

983.45 98X7098243 98X00

98X77 981.95

98X68 98146

9(230 9*1449*2.41 9(24698X41 9*15098X42 9*1.699(2.47 9(14098235 98X4098X70 9(23098X7* 9822998345 98X6698244 98X7598X51 98146

98236 9815298239 9*1.7898321 9833698X78 98X1898329 9832098X66 981.93983.13 981.7098233 98X11

9*23* 9*2299(349 98X669(34* 9*2419*2449*236 9*3.179SX41 9*1.98983.01 9823498X63 98X0198X72 9814498X88 981.9798X96 98X4798333 98X1598X56 981.92

:vx -:-.•;-:• :-:-:-;•:-: v: -x •:•:•;•;•:•:•:-:•: ;-. -:•:•:••Ttf'i'j'i'JL ''-&•'• 'fWU pii'il -;

9*5.73984.84

984.72

9*4319*4.16 9*3479*4.14 9(3459*4.19 9*3.929*4.17 983.919*42* 984.0098437 9*4.089*435 9*426985.11 984.6798523 985.00

98430 984.12

98423 983.9198426 983.9598534 985.1698449 984.42

98533 985.16984.64 984.2598539 984.99

984.10

9*4.699*454 9*4339*5.40 9*540983.92984.11 98340984.16 983.82985.17 984.69984.95 984.78

984.10

984.61 98430984.94 984.77985.64 985.15984.40 984.06

iiliiil

983.61983.61983.70983.69983.80983.87984.0398438984.7298348

983.67

983.7398447984.1798448984.00984.70

984309*4.69

9833798339984.44984.49

983.94

984.14984.4998448983.8*

9(333 9*33*9*332 983389(341 9*3319(341 9(3.479*3.72 9*33*9*3.7* 983449*357 9*3459*42* 9*4.039*4.73 984.63983.75 983349(335 983399*3.62 9*3.479*4.79 9*4379*443 9*3.789*4.77 9*4359(347 9*3.679(437 9*433

9(4.12 9(3459(443 984.4*

9(3.45 9(3279(3.46 9(3309*427 9*4.019*433 984339*344 983.7398443 983.909*447 984.91984.73 9*4319*3.76 9(3.61

9*3439*3439(3.149*3.149(3239*32*9*3.47983.60984.13983.1298X989*3.069*4499*3329*4.069832198343

9(3.409*35*

982489*24998333984.04983.4398339984379*4.119*325

9*1469*1469*1549*15*9*24798X149823098X4498X7898148

981.76

98144

98X8398X1098X8198X0098X65

9*23*98X76

9*1439*14398X4098X679822698X42983.0098X8898X09

9(0419(1579(1549*23598X6598X4998X6598X6598X809822698X1698X219(3.05982399*3.0198X40

98X63

98X724(3.16

9*23*98X099*24098X119813298X29983.489823598X15

9*4429*4479*4529*4579*458985.0798529985.49986.1598524985.13985.169862098532986.18985.43986.07985279*6.159(53798630

985.759*630984.90985.05986.97986.00985.09

flfllii

9*4.7*9*4409*4469*4479*446984.91985.12

985.72984.86984.79

984.88

985.65985.09985.66985.0798539

985.18986.02

985.0098533986.10984.47

984.6698739985.4198445

976309763097636976.40976.419763397643

975.259763897634976.6197731976.63977.11976.61

977.11

97646• 977.46

97636976.76977.66976.14

97635

976.98

• M-lwiireplicedbyMW-lR 01 8/24/94. The aevr men vrimgfoitt elenliot a 1013.64

remont\w-lelev2.wk3; 05-Feb-97 Eagon & Associates, Inc.

TABLE 2.SUMMARY OF ANALYTICAL RESULTS

ASSESSMENT PARAMETERS - JANUARY 1990 TO PRESENT

Alkalinity, TotalArsenic, Dissolved/Total"Calcium, Dissolved/Total ••ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total* •Magnesium, Dissolved/Total'*Manganese, Dissolved/Total"Nitrogen, AmmoniaPotassium, Dissolved/Total**Residue, T. Fit. (Diss.)Sodium," Dissolved/Total* •SulfateTotal Kjeldahl N (TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead, PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (a» N)pH, LabSulfide, Total (as H,S)Zinc, ZnBenzeneChlorobenzeneChloroethane1 , 1 - Dichloroethaneas - 1 ,2- Dichloroethyleneo-Dichlorobenzene (1,2)p- Dichlorobenzene (1,4)p-Xylenem-Xylene

millmg/1ug/1mg/1mg/1mg/1mg/1ntuug/1mg/1ug/1mg/1mg/1mg/1mg/1mg/1mg/1mg/1ug/1ug/1ug/1UMHOug/1ug/1ug/1mg/1mg/1S.U.mg/1ug/1Ug/1ug/1ug/1Ug/1ug/1ug/1ug/1ug/1ue/1

:' WiVip |i|i pw^&ip^p;:;|»|E| ^ ^ | l^p^lpliip

931 996 942<3 <2 <5

270 240 260350 367 320

94 94

12500 13300 13500100 100 100

110 <751.83 1.75

8.6 6.21650 1630 1590250 247 26093 76 40

3.06 2.9 2.7234 46 26

0.5 <0.54.2 3.51.7 1.623 2.7

<0.5 <0.5| 5.4 7.9

1.2 1.72.4* <2.0*2.4* <2.0»

111040

<5440300180

180002001301.416.0

1590250

692.57

30

812 502 938<5 10 6

235 290 240250 350 27092 99 110

12000 15300 1400093 110 9289 120

1.44 1.52 1.297.0

1600 1490 1540250 280100 160 50

Z69 3.10 2.2866 27 29

980 980 1000<3 <5 6

230 220 220266 262 313110 160 210

12000 13000 1300096 92 93

110 110 1101.07 1.05 1.326.9 9.1 4.5

1598 1628 1580270 260 260

52 51 492.99 3.19 3.11

31 28 30

13 <0.51.4 2.1

<1.0 <1.01.5 1.7

<0.5 <0.52.6 3.0

<0.5 0.7<1.0 <1.0<1.0 <1.0

10004.5221317<20

1390093

1011.256.6

140028057.63.46

30

1010<3

213280244

1400089.61001.157.2

145026049.82.56

33

1.36.92.74.6

<0.519.45.2

<1.0<1.0

965<3

214252182

1370089.4

941.367.9

155025939.73.04

32

0.82.9

<0.51.9

<0.56.81.2

<0.5<0.5

1020<3

218272155

1450088.8

930.967.3

163026251

2.8534

1.46.00.71.7

<0.513.72.4

<0.5<0.5

ND - Not DetectedAquatech method 524.2 detection limits are 0.5/ig/l for each of the ten volatile organic compounds (VOC's).Method 8270 detection limits are 2.0/ug/1 for Bis(2 ethylhexyl)phthalate.• Prior to the July 1991 sampling, P-xylene and m-xylene could not be separately quantified. Detection limits and concentration

reported prior to July 1991 are for both compounds combined.•• Samples no longer field-filtered starting 11/29/94.1 Total Xylene it reported as a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0/j.g/t.

n«lrtiZ.»tS, 29-)«n-» P«|»lof9 Eigoa* A»otu tti, lot



PARANfETEfiii^lllliil!Alkalinity, TotalArsenic, Dissolved/Total"Calcium, Dissolved/Total"ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total* •Magnesium, Dissolved/Total**Manganese, Dissolved/Total* •Nitrogen, AmmoniaPotassium, Dissolved/Total* •Residue, T. Fit. (Di».)Sodium, Dissolved/Total"SulfateTotal Kjeldahl N (TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead, PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (as N)pH, LabSulfide, Total (as H^S)Zinc, ZnBenzeneChlorobenzeneChloroethane1,1-Dichloroethanecis - 1 ,2 - Dichloroethyleneo- Dichlorobenzene (1,2)p- Dichlorobenzene (1,4)p-Xylcnem -Xylene

îiiiiitllimg/lug/1mg/lmg/lmg/lmg/lntuug/1mg/lug/1mg/lmg/lmg/lmg/lmg/lmg/lmg/lug/1ug/1ug/1UMHOug/1ug/1ug/1mg/lmg/lS.U.mg/lug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

mi1070

5.8210

<2.0279314

105012700

90.493

0.958.4

158026950

2.8433

<0.52.01.41.4

<0.55.71.0

<0.5<0.5

3.4

25216880

76013700

87.586

0.936.4

1640259

, 51

33428

<0.5<0.5

0.81.1

<0.523

<0.5<0.5<0.5

ill«wii

979<3.0207241211105400

1440086.9

850.766.5

154028446

2.7828

0.91.91.11.3

<0.56.41.0

<0.5<0.5

765<3.021729385

101410

1490093.3

690.906.9

140058345

2.2634

1.55.61.51.9

<0.514.22.5

<0.5<0.5

iiiIPf

1030<3.0185221

9481

15013900

79.162

0.876.7

146035394

2.4129

<0.51.31.31.4

<0.54.91.0

<0.5<0.5

siWBSSiS&BifSS

Plbliii;1060<3.020344.330490

22015200

82.976

0.767.7

135031048

3.3624

0.61.01.41.4

<0.54.20.8

<0.5<0.5

10709.5240298131

58525900

9933750.945.9

160024262

2260.817

3190151450

<0.05<0.05

6.8

68<1.0

2.0<1.0<0.5<0.5

6.3<1.0<1.0<1.0

104011

21019383

31720000

1001860.935.9

151023287

1820.97.5

212

6.250

<0.05<0.05

6.3

249<1.0<1.0<1.0<0.5<0.5<2.0<2.0<1.0<1.0

Bill1110<3.017230368

15715600

76.498

0.856.2

1530217260

155<0.5<5.0

<102.9

<20<0.05

60<1.0

1.32.81.2

<0.57.21.5

<1.0<1.0

Iliiiiiiiii:tf^miiimm1070 1040<3.0 3.2156 205123 18255 100

247 22015100 18400

68.4 87.4103 164

0.85 0.774.4 5.2

1390 1600151 189130 130

121 135<0.5 0.9<5.0 <5.02200 2420<10 104.9 5.7

<20 220.07 0.05

6.6 6.630.42

77 117<1.0 <1.0<1.0 <1.0

1.3 <1.0<0.5 <0.5<0.5 <0.5<1.0 <2.0 '<1.0 <2.0 '<1.0 <2.0 '<1.0 <2.0 l

ND - Not DetectedAquatech method 524.2 detection limits are 0.5/ig/l for each of the ten volatile organic compounds (VOC's)Method 8270 detection limits are 2.0/xg/l for Bis(2 ethylhexyl)phthalate.• Prior to the July 1991 sampling, P-xylene and m-xylene could not be separately quantified. Detection limits and

concentrations reported prior to July 1991 are for both compounds combined.•• Sample* no longer field-filtered starting 11/29/94.1 Total Xylene is reponed as a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0/xg/l.

Pip 2 o

TABLE 2.SUMMARY OF ANALYTICAL

ASSESSMENT PARAMETERS - JANUARYRESULTS1990 TO PRESENT

Alkalinity, Total mg/1Arsenic, Dissolved/Total* * ug/1Calcium, Dissolved/Total" mg/1Chloride mg/1COD mg/1COD, Dissolved mg/1Turbidity ntuIron, Dissolved/Total* • ug/1Magnesium, Dissolved/Total" mg/1Manganese, Dissolved/Total •• ug/1Nitrogen, Ammonia mg/1Potassium, Dissolved/Total" mg/1Residue, T. Fit. (Diss.) mg/1Sodium, Dissolved/Total* • mg/1Sulfate mg/1Total Kjeldahl N (TKN) mg/1Total Organic Carbon mg/1Barium, Ba ug/1Cadmium, Cd ug/1Chromium, Cr ug/1Conductivity, Lab UMHOCopper, Cu ug/1Lead, Pb ug/1Nickel, Ni ug/1Nitrate + Nitrite N mg/1Nitrogen, Nitrite (a» N) mg/1pH, Lab S.U.Sulfidc, Total (aa HjS) mg/1Zinc, Zn ug/1Benzene ug/1Chlorobenzcne ug/1Chloroethane ug/11,1- Dichloroethane ug/1cis-l,2-Dichloroethylene ug/1o-Dichlorobenzene(l,2) ug/1p- Dichlorobenzene (1,4) ug/1p -Xylene ug/1m -Xylene ue/1

lUp ^^^^TO^^^^^^^^^^^^^^^^^^^tjji^^^^^H

562 59353 4494 13540 3621

25000 2390037 54

4300.8

6.1650 650

46 409 13

1.02 1.05.6 9

1

3.77.46.21.90.52,7

NDNDND

63465

1603949

3290051

3100.935.1

3585061

0.945.4

5.28.59.83.4

ND3.1

NDNDND

55082

1302587

2600049

3200.164.960039.0

171.443.8

4.86 4.49.51 17.66.1 5.22.6 2.3

ND ND3.9 4.9

ND 1.1ND NDND ND

54485-M

13031<8

2800050

2900.794.858039.0

70.844.2

4.715.05.92.0

ND5.81.4

NDND

rasxSBsssjSssjIlEJtgljjjBjfiBJas!

75078

1433047

3260053.12620.645.9

65438.114.21.755.5

4.916.66.34.4

ND5.61.6

NDND

^H|H

67371

14429.2

84

3270053.72640.635.7

68238.214.41.715.6

5.21736.23.9

ND7.21.9

NDND

51952

13224.6

77

2920049.42350.545.1

58837.0

30.534.2

4.515.34.6NDNDNDNDNDND

w^^mmm^^mm-mmmifmMmAvmrnmim^mmwmwmm57164

132263316

30026400

47.22480.555.358835.6

90.375.0

3.916.34.51.1

ND5.20.9

NDND

63

29.1—24

29900

0.75

653

5.9

4.218.15.71.8

<O.S5.01.0

<0.5<0.5

63

31.76611

3803300

0.54

72836.0

<1.0

4.419.6<0.5

2.4<0.5

6.0<0.5<0.5<0.5

62561

15128.1

37

3250056.32860.454.868234.9

70.85

5.1

4.123.03.32.1

<0.55.51.1

<0.5<0.5

iH66

29.7

39

25900

0.52

57038.6

7.1

3.921.43.91.3

<0.56.11.1

<0.5<0.5

• A89-100 ii a blind duplicate of A89-2. • A93-400 ii i blind duplicate of AS9-Z• A95-400 ii a blhd duplicate of A89-2. • A96-200 it a blind duplicate of A89-2.•• Sunplet no longer fleU - filtered turfing 11/29/94.1 Total Xylene is reported aa a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0 ng/t.

• A94-400 it a blind duplicate of A89-2.•A95-200ii a blind duplicate of AJ9-2.

Pip] of 9 Eifao A Auodtttt, lot



Alkalinity, Total mg/1Arsenic, Dissolved/Total* • ug/1Calcium, Dissolved/Total* • mg/1Chloride mg/1COD mg/1COD, Dissolved mg/1Turbidity ntuIron, Dissolved/Total" ug/1Magnesium, Dissolved/Total** mg/1Manganese, Dissolved/Total" ug/1Nitrogen, Ammonia mg/1Potassium, Dissolved/Total** mg/1Residue, T. Fit. (Diss.) mg/1Sodium, Dissolved/Total•• mg/1Sulfate mg/1Total Kjeldahl N (TKN) . mg/1Total Organic Carbon mg/1Barium, Ba ug/1Cadmium, Cd ug/1Chromium, Cr ug/1Conductivity, Lab UMHOCopper, Cu ug/1Lead, Pb ug/1Nickel, Ni ug/1Nitrate + Nitrite N mg/1Nitrogen, Nitrite (as N) mg/1pH, Lab S.U.Sulfide, Total (as HjS) mg/1Zinc, Zn ug/1Benzene ug/1Chlorobenzene ug/1Chloroethane ug/11,1-Dichloroethane ug/1cis -1,2 - Dichloroethylene ug/1o-Dichlorobenzene(l,2) ug/1p—Dichlorobenzene (1,4) ug/1p-Xylene ug/1m-Xylene______________ug/1

(1

30.2

41

26200

0.50

59238.7

7.9

43

353

28

25600

0.51

57435.8

4.9

4334.5

67

3320

0.43

63840.5

4.6

3.620.53.61.2

<0.56.01.2

<0.5<0.5

4321.6<0.5

1.2<0.5

5.81.2

<0.5<0.5

4.023.95.01.3

<0.56.01.2

<0.5<0.5

4735.9

24

3480

0.43

62842.1

4.5

3.119.74.51.30.64.80.9

<0.5<0.5

54244

11528.9

32

19121800

41.0190

0.504.060233.5

<5

625<0.5<5.0824<10

<2.0<20

<0.05<0.05

6.7

3.624.31.13.0

<0.57.8

54047

12028.9

14

20622800

42.8199

0.464.258834.9<5.0

651<0.5<5.0803

<2.0<20

<0.05<0.05

6.7

6.522.4

2.9<0.5

7.71.0

61540

12133.6

14

16724000

45.92000.614.073432.5

8

631<0.5<5.01140

<2.0<20

<0.05<0.05

6.5

2.9133

<0.5<0.52.8

<2.0

57442

1283Z9

11

14026200

42.9206

0.57<2.0706

33.87

696<0.5<5.01150

<2.0<20

<0.05<0.05

6.6

2.913.8

<0.5<0.5

3.9

58255

11630.2

14

13622700

42.71970393.762531.9

<5

683<0.5<5.0

3.919.75.70.9

<0.55.8

59152

12931.5

14

11824900

4732190394.061034.8

<5

736<0.5<5.0

<2.0 <2.0<20 <20

<0.05 <0.05

3.918.54.01.0

<0.55.6

65138

12932.8

14

32827300

46.2236

0.513.3693

30.9<2

709<0.5<5.01130

<2.0<20

<0.05

6.5

4.728.53.71.3

<0.55.41.2

67237

12533.5

16

31326400

45.0230

0.453.265728.9

3

<2.0<20

<0.05

6.5

5.230.43.91.1

<0.55.31.4

57360

12949

<20

18024500

44.1222

0.364.1718

37.1<5

682 697<0.5 <0.5<5.0 <5.01130 1020

<2.0<20

<0.05

6.65<0.05

<104.328

<1.0<0.5<0.5'4.2

<2.0 l

<2.0 '<2.0 '

• A89-100 ia a blind dvpHcatt of AS9-Z • A93-400 li a blfad duplicate of AS9-2.• A95-400 U a blind duplicate of A89-2. • A96-200 ia a blind duplicate of AS9-X•• Samples no longer Held - filtered itirting 11/29/94.1 Total Xylene is reported as a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0pg/l.

• A94-4001* * blind duplicate of A89-2.• A95-200 li a blind duplicate of A89-2.

J: 29-Jin-9


:- . '-:•' :. : ,': .;::iv:y:-:-:;:;:;:;X;:>'iv:i:-:i:;:v':'x:•. . •. . : .• : . • . • •'•. .-.vM-.'X': •:•;•:•: •;•: •:•:-:•.•:•:•:•;•.•.•.•.•

EfBfcllltiti^lii', TotalDissolved/Total"Dissolved/Total* •

solved

lolved/Total"im, Dissolved/Total* *te, Disaolved/Total"Ammoniai, Dissolved/Total ••T. Fit. (Diss.)Dissolved/Total"

Idahl N (TKN)anic Carbonla,Cdn, Crdty, Lab*u

Nitrite NNitrite (as N)

Dial (ai HjS)

izeneaneoroethaneJichloroethyleneTjbenzene (1,2)•obenzene (1,4)

:

iiilllllilllfilllmg/lug/1mg/lmg/lmg/lmg/lntuug/1mg/lug/1mg/lmg/lmg/lmg/lmg/lmg/lmg/lug/1ug/1ug/1UMHOug/1ug/1ug/1mg/lmg/lS.U.mg/lug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

520 780<5 10

210 18077 19986 110

5100 680057 73

170 1900.19 0.971.9 3.7

988 1270100 190.047 56

0.77 1.7017 23.0

i

ND ND NDND ND NDND ND NDND ND NDND ND NDND ND NDND ND NDND ND NDND ND ND

6586.417715894

715070.12350.183.4

1080140.056.10.7420.0

NDNDNDNDNDNDNDNDND

ifiii iiiisiiiri6614.6190148158

749070.82230.202.7

1070153.046.6

<0.1019.0

NDNDNDNDNDNDNDNDND

m7056.2182154655675

732069.72160.133.0

1120147.0

600.6321.0

NDNDNDNDNDNDNDNDND

m7.3

143

181

7120

0.18

1090155.0

20.0

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

&M6.3

138655290

7940

0.07

1190147

21

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

WAbt65953189180

97

85107532150.133.4

120015769

0.8620

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

5.1

176

97

9090

0.16

1140161

21

<0.5<0.5<0.5

0.7<0.5<0.5<0.5<0.5<0.5

4.6 5.8

148 28.9

48 75

9060 11200

0.17 0.18

1110 1090137 163

18 17

<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<O.S <0.5<0.5 <0.5<0.5 <0.5

751<3.0172211

58

10210100

70.72460.132.6

123013577

173<0.5<5.02370<10<2.0

20<0.05<0.05

6.8

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

11111mm®7809.2144193

59

90862057.92070.083.0

124011473

147<0.5<5.01960<10

<2.0<20

<0.05<0.05

6.9

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

liillmm825

<3.0174213

62

66.910800

75.32300.123.078915371

189<0.5<5.0

<10<2.0

20<0.05

45<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

:iATEL-

840<3.0153206

56

118895067.22080.142.4

118014066

169<0.5<5.02010<10<2.0<20

<0.05

6.6

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

iiwil9im775

<3.017318167

9410800

71.52320.112.7

137015649

176<0.5<5.01940<10<2.0

300.06

6.73<0.05

<10<1.0<1.0<1.0<0.5<0.5<2.0 '<2.0 '<2.0 J

<2.0 '

HH7.0

118

78

13300

1.67

1190194

19

<0.5<0.5

3.80.6

<0.5<0.5<0.5<0.5<0.5

*• Sample* no longer field - filtered starting 11/29/94.1 Total Xylene is reported as a result of Appendix II methodology and (1,2) and (1,4) Dkhlorobenzene are each 2.0Mg/<.

£*/oo Jt Attoattti, toe*, foe



' • " " • - " : :'..'.'• '.•.•.•.•:•.•:•••:'.!••••:••.:; x^1;::':': ;':':":':': ,::'.-.::i :::::j:":\ '-x-:::::

Alkalinity, TotalArsenic, Dissolved/Total* •Calcium, Dissolved/Total' •ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total* •Magnesium, Disaolved/Total"Manganese, Dinolved/Total"Nitrogen, AmmoniaPotassium, Dissolved/Total"Residue, T. Fit. (Diss.)Sodium, Dissolved/Total"SulfateTotal Kjeldahl N (TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead, PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (as N)pH, LabSulfide, Total (a» HjS)Zinc, ZnBenzeneChlorobenzeneChloroethane1,1-Dichloroethanccis- 1,2-Dichloroethyleneo-Dichlorobenzene (1,2)p- Dichlorobenzene (1,4)p -Xylenem -Xylene

mg/1ug/1mg/1mg/1mg/1mg/1ntuug/1mg/1ug/1mg/1mg/1mg/1mg/Img/1mg/1mg/1ug/1ug/1ug/1UMHOug/1ug/1ug/1mg/1mg/1S.U.mg/1ug/1Ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

MM520<5

2107786

510057

1700.191.9

98810047

0.7717

NDNDNDNDNDNDNDNDND

78010

180199110

680073

1900.973.7

1270190.0

561.7023.0

i

ND NDND NDND NDND NDND NDND NDND NDND NDND ND

nmfffiW6586.417715894

715070.12350.183.4

1080140.056.10.7420.0

NDNDNDNDNDNDNDNDND

mam6614.6190148158

749070.82230.202.7

1070153.046.6

<0.1019.0

NDNDNDNDNDNDNDNDND

' 'iP$B588'Si?i2'ii¥i8SS^ iKiSSSiSI-imwiS®

7056.2182154655675

732069.72160.133.0

1120147.0

600.6321.0

NDNDNDNDNDNDNDNDND

7.3

143

181

7120

0.18

1090155.0

20.0

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

6596.3 53

189138 1806552 9790

7940 851075.3215

0.07 0.133.4

1190 1200147 157

690.86

21 20

<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5

m5.1

176

97

9090

0.16

1140161

21

<0.5<0.5<0.5

0.7<0.5<0.5<0.5<0.5<0.5

4.6

148

48

9060

0.17

1110137

18

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

M5.8

28.9

75

11200

0.18

1090163

17

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

Iliiil751

<3.017221158

10210100

70.72460.132.6

123013577

173<0.5<5.02370<10<2.0

20<0.05<0.05

6.8

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

iilli;7809.214419359

90862057.9207

0.083.0

124011473

147<0.5<5.01960<10

<2.0<20

<0.05<0.05

6.9

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

825<3.0

17421362

66.910800

75.32300.123.078915371

189<0.5<5.0

<10<2.0

20<0.05

45<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

ATT^T' '• ' '•'•

840<3.0153206

56

118895067.22080.142.4

118014066

169<0.5<5.02010<10

<2.0<20

<0.05

6.6

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

IIP775

<3.017318167

9410800

71.52320.112.7

137015649

176<0.5<5.01940<10

<2.030

0.06

6.73<0.05

<10<1.0<1.0<1.0<0.5<0.5<2.0 '<2.0 '<2.0'<2.0'

•• Sample* no longer field - filtered starting 11/29/94.1 Total Xylene It reported as a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0 uglt.

.Vreo>oor»o«lr«il«t3; 29- Jic-»7 Pip 7 of» Si/00

TABLE 2.{SUMMARY OF ANALYTICAL RESULTS

ASSESSMENT PARAMETERS - JANUARY 1990 TO PRBSBN1

Alkalinity, TotalArsenic, Dissolved/Total* •Calcium, Dissolved/Total"ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total"Magnesium, Dissolved/Total ••Manganese, Dissolved/Total"Nitrogen, AmmoniaPotassium, Dissolved/Total"Residue, T. Fit. (Diss.)Sodium, Dissolved/Total* *SullateTotal Kjeldahl N (TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead, PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (as N)pH, LabSulfide, Total (as H,S)Zinc,ZnBenzeneChlorobenzeneChloroethane1,1- Dichloro ethaneas- 1,2-Dichloroethyleneo-Dichlorobenzene (1,2)j-Dichlorobenzene (1,4)

p -Xylenem -Xylene

ssiiaSsBsSs;?;IlllllillwmiiM

mg/lug/1mg/lmg/lmg/lmg/lntuug/1mg/lug/1mg/lmg/lmg/lmg/lmg/lmg/lmg/lug/1ug/1ug/1UMHOug/1ug/1ug/1mg/lmg/lS.U.mg/lug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1

6.2

115

48

11700

1.23

1140144

14

<0.5<0.5

3.60.7

<0.5<0.5<0.5<0.5<0.5

4.2

20.7

65

15200

1.00

1120131

12

i

<0.5<0.5

2.6<0.5<0.5<0.5<0.5<0.5<0.5

8733.716014750

15914800

79.11551.626.4

121015595

289<0.5<5.01960<10

<ZO20

<0.05<0.05

6.7

<10<1.0<1.0

3.0<0.5<0.5<1.0<1.0<1.0<1.0

88410

17513343

15515400

88.42321.226.2

129011693

230<0.5<5.01960<103.0

<20<0.05<0.05

6.9

<10<1.0<1.0<1.0

5.5<0.5<1.0<1.0<1.0<1.0

9124.215715446

11214300

79.71501.136.8

99514689

280<0.5<5.0

<105.8

<20<0.05

19<1.0<1.0

4.61.6

<0.5<1.0<1.0<1.0<1.0

913<3.015116449

17613400

73.41901.195.4

120012499

224<0.5<5.02040<10<2.0<20

<0.05

6.5

<10<1.0<1.0

4.11.9

<0.5<1.0<1.0<1.0<1.0

8594.718013949

12015700

84.82331.116.1

136013576

244<0.5<5.01980<10

6<20<0.5

6.660.13

11<1.0<1.0<1.0

6.1<0.5<2.0l

<2.0 '<2.0 l

<2.0 l

• A92-100 and A93-100 are blind duplicate samples of A89-3S.•• Samples no longer field - filtered starting 11/29/94.1 Total Xylene is reported as a result of Appendix II methodology and (1,

and (1,4) Dichlorobenzene are each 2.0îg/l.2)

; 29- J«o-»7 Eigvo A Auoeuttl, /DC



Alkalinity, Total mg/lArsenic, Dissolved/Total" ug/1Calcium, Dissolved/Total" mg/lChloride mg/lCOD mg/lCOD, Dissolved . mg/lTurbidity ntuIron, Dissolved/Total* • ug/1Magnesium, Duwolved/Totar* mg/lManganese, Dlwolved/TotaT* ug/1Nitrogen, Ammonia mg/lPotassium, Dissolved/Total" mg/lResidue, T. Fit. (Diss.) mg/lSodium, Dissolved/Total* • mg/lSulfate mg/lTotal Kjeldahl N (TXN) mg/lTotal Organic Carbon mg/lBarium, Ba ug/1Cadmium, Cd ug/1Chromium, Cr ug/1Conductivity, Lab UMHOCopper, Cu ug/1Lead, Pb ug/1Nickel, Ni ug/1Nitrate + Nitrite N mg/lNitrogen, Nitrite (a» N) mg/IpH, Lab S.U.Sulfide, Total (as H3S) mg/lZinc, Zn ' ug/1Benzene ug/1Chlorobenzene ug/1Chloroethane ug/11,1- Dichloroethane ug/1cis- 1,2 -Dichloroethylene ug/1o-Dichlorobenzene(l,2) ug/1p-Dichlorobenzene (1,4) ug/1p-Xylene ug/1m -Xylene ug/1

11806

170390170

280075

2801.889.1

200049081

4.4857

NDNDNDNDNDNDNDNDND

12008

168376

258078

265

10.21870488883.658

NDND3.3NDNDNDNDNDND

103010

22056

170

380075

3201.797.2

187044038

3.7146

ND NDND ND4.6 ND

ND NDND NDND NDND NDND NDND ND

100020

180185180

820083

4900.198.8

1500330.0

7233124.0

NDNDNDNDNDNDNDNDND

97121

20815693

1010093.83661.327.6

1440253.0

79Z4328.0

NDND3.4

NDNDNDNDNDND

Km|A$Jlp«Bj

9316.0180186258

820087.32491.749.4

1460317.062.93.1730.0

NDND3.5

NDNDNDNDNDND

9295.9182171285

852088.52581.79.3

139032765.21.64

29

NDND2.9

NDNDNDNDNDND

9559.01851579282

20010200

82.83021.698.4

1420236.0

83Z76

28

NDND3.0

NDNDNDNDNDND

iss& iiijK^

8.0

68.8

33

9870

0.59

111096.9

11.0

<0.5<0.5

3.81.4

<0.5<0.5<0.5<0.5<0.5

6.9

79.5

26

10300

0.63

1120101

11.0

<0.5<0.5

3.30.9

<0.5<0.5<0.5<0.5<0.5

5.5

1306955

17010500

1.41

974203

20

<0.5<0.5

2.70.7

<0.5<0.5<0.5<0.5<0.5

9136.6183139

76

1280088.62221.748.4

127020396

3.5023

<0.5<0.5

2.50.6

<0.5<0.5<0.5<0.5<0.5

7.0

118

78

13300

1.67

1190194

19

<0.5<0.5

3.80.6

<0.5<0.5<0.5<0.5<0.5

A92-100 and A93-100 are blind duplicate samples of A89-3S.•• Samplet no longer field - altered starting 11/29/94.1 Total Xylene U reported as a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2,0/*g/l.

Pip 5 of 9 Buna Jt AifKiittt, lot


ASSESSMENT PARAMETERS - JANUARY 1990 TO PRESENT:rv':::::;:;;?i::,?;S:::;?5iiiiillpilll^^mm^mmmmm^mmAlkalinity, TotalArsenic, Dissolved/Total**Calcium, Dissolved/Total"ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total* *Magnesium, Dissolved/Total* •Manganese, Dissolved/Tot al**Nitrogen, AmmoniaPotassium, Dissolved/Total ••Residue, T. Fit. (Diss.)Sodium, Dissolved/Total* •SulfateTotal Kjeldahl N (TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead, PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (a»N)pH, LabSulfide, Total (as HjS)Zinc, ZnBenzeneChlorobenzeneChloroethane1,1 -Dichloroethanecis - 1 ,2 - Dichloroethyleneo -Dichlorobenzene (1,2)p- Dichlorobenzene (1,4)p -Xylenem -Xylene

mg/1ug/1mg/1mg/1mg/1mg/1ntuug/1mg/1ug/1mg/1mg/1mg/1mg/1mg/1mg/1mg/1ug/1ug/1ug/1UMHOug/1ug/1ug/1mg/1mg/1S.U.mg/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

61

30.2

41

26200

0.50

59238.7

7.9

3.620.53.61.2

<0.56.01.2

<0.5<0.5

wBnSqHHBfflSBHWn^S?

43

35.3

28

25600

0.51

57435.8

4.9

i 4-321.6<0.5

1.2<0.5

5.81.2

<0.5<O.S

WfmiMt.43

34.5

67

3320

0.43

63840.5

4.6

4.023.95.013

<0.56.01.2

<0.5<0.5

mmm

4735.9

24

3480

0.43

62842.1

4.5

3.119.74.51.30.64.80.9

<0.5<0.5

jjjjjjjljsgsllsj

54244

11528.9

32

19121800

41.01900.504.060233.5<5

625<0.5<5.0824<10<2.0<20

<0.05<0.05

6.7

<103.6

24.31.13.0

<0.57.8

<1.0<1.0<1.0

54047

12028.9

14

20622800

42.8199

0.464.258834.9<5.0

651<0.5<5.0803<10<2.0<20

<0.05<0.05

6.7

<106.5

22.4<1.0

2.9<0.5

7.71.0

<1.0<1.0

SJ&93B9&93

M9Mv88l5^^Gmmsm61540

12133.6

14

16724000

45.92000.614.073432.5

8

631<0.5<5.01140<10<2.0<20

<0.05<0.05

6.5

<102.9

13.3<1.0<0.5<0.52.8

<ZO<1.0<1.0

SBBHJBlilSiSBi57442

1283X9

11

14026200

42.92060.57<ZO70633.8

7

696<0.5<5.01150<10<ZO<20

<0.05<0.05

6.6

<102.9

13.8<1.0<0.5<0.53.9

<1.0<1.0<1.0

IvXcuusitt^nHHBfiJESwWS;*!:?;-

58255

11630.2

14

13622700

42.71970.393.762531.9

<5

683<0.5<5.0

<10<2.0<20

<0.05

<103.9

19.75.70.9

<0.55.8

<1.0<1.0<1.0

w^^îVw^SsWmm59152

12931.5

14

11824900

47.32190394.061034.8

<5

736<0.5<5.0

<10<2.0<20

<0.05

<103.9

18.54.01.0

<0.55.6

<1.0<1.0<1.0

ffffy. B:Y:;:;'.'';'::

65138

12932.8

14

32827300

46.22360.513.369330.9

<2

709<0.5<5.01130<10<2.0<20

<0.05

6.5

<104.7

28.53.71.3

<0.55.41.2

<1.0<1.0

mmmimmmmmmwmmtmi.

672 57337 60

125 12933.5 49

16 <20

313 18026400 24500

45.0 44.1230 2220.45 0.363.2 4.1657 71828.9 37.1

3 <5

682 697<0.5 <0.5<5.0 <5.01130 1020<10 <10<2.0 <2.0<20 <20

<0.05 <O.OS

6.5 6.65<0.05

<10 <105.2 4.3

30.4 283.9 <1.01.1 <0.5

<0.5 <0.55.3 '4.21.4 <2.0 '

<1.0 <2.0 '<1.0 <2.0 '

• AS9-100 U * blfad d»pUeat« of A89-Z • A93-400 ii a blind duplicate of AS9-2.• A95-400 it a blind duplicate of A89-Z • A96-200 it a blind duplicate of AS9-2.•* Simplei BO longer field - filtered itartiag 11/29/94.1 Total Xylene U reported ai a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0/ig/£

•A94-4001S a blind duplicate of A89-2.• A95-200 U a blind duplicate of AS9-2.

\trcfnonr\»n&lrellwk3: 29-Jan-ff

TABLE 2.SUMMARY OP ANALYTICAL RESULTS


• :-:..':-: :.::iliilSi Sil ^S::i*AitA^TBiiliiM^^^^^Âlkalinity, Total mg/1Arsenic, DUsolved/Total" ug/1Calcium, Dissolved/Total* • mg/1Chloride mg/1COD mg/1COD, Dissolved mg/1Turbidity ntuIron, Dissolved/Total** ug/1Magnesium, Dissolved/Total •• mg/1Manganese, Dissolved/Total" ug/1Nitrogen, Ammonia mg/1Potassium, Dissolved/Total" mg/1Residue, T. Fit. (Diis.) mg/1Sodium, Dissolved/Total •• mg/1Sulfate mg/1Total Kjeldahl N (TKN) mg/1Total Organic Carbon mg/1Barium, Ba ug/1Cadmium, Cd ug/1Chromium, Cr ug/1Conductivity, Lab UMHOCopper, Cu ug/1Lead, Pb ug/1Nickel, Ni ug/1Nitrate + Nitrite N mg/1Nitrogen, Nitrite (a* N) mg/1pH, Lab S.U.SulTide, Total (at H2S) mg/1Zinc, Zn ug/1Benzene ug/1Chlorobenzcne ug/1CbJoroethane ug/11,1-DichIoroethane ug/1tis-l,2-Dichloroethylene ug/1o- Dichlorobenzene (1,2) ug/1p- Dichlorobenzene (1,4) ug/1p-Xylene ug/1m-Xylene ug/1

^JnnffiSBjiffiMmm54015

1408

26

1600051

1300<0.05

2.05709.235

0.241.2

1.7NDNDNDNDNDND2.32.4

ftJE ifihttsSjSfli&fU^&SftÎ-iOJUfîi^^

523 527 546 5759.9 9.5 21 10 11 13166 154 135 159

8.75 9.32 9.52 5.34 5.13 6.0646 <20 <8 16

<8 52 <8 4190 140

IP

34211

159

iniM21

6.06 7.76

30 <20

10800 12200 15600 8090 13000 16400 16400 19100

M13

8.53

<8

2060049.9 48.4 45.5 48.8 48.51730 1520 1260 1320 1320

<0.05 <0.05 0.09 0.09 <0.05 <0.05 <0.05 <0.053.6 4.3 2.2 2.3562 588 594 574 604 6288.3 8.4 8.5 8.3 7.7 8.7

40.2 36.2 35 45

2.36338.745

60810.8

<0.05

5169-4

528 564 • 550 630 58112 14 14 14 13 10 17

130 144 124 143 1318.33 7.49 9.27 7.84 8.86 8.08 23

<8 <8 <8 <8 <20<8 <8

97.7 71.8 55 232 12020400 18700 17100 11000 15400 20600 18500

43.0 45.2 45.1 54.4 50.5952 1200 658 899 845

<0.05 <0.05 <0.05 0.12 <0.05 <0.05 <0.051.1 4.0 5.1 7.5 2.6

564 613 552 679 589 708 6759.3 11.0 9.7 10.0 7.8 7.6 8.6

28 44 44 57 230.42 <0.10 <0.10 <0.20 <0.201.2 1.2 1.8 2.0 3.9 1.9

i

2.1

3.0 1.7 1.2 1.7 1.5 <0.5 <0.5

3.6

1.6ND ND ND <0.5 <0.5 <0.5 <0.5 <0.52.7 1.7 ND 2.4 <0.5 <0.5 <0.5 IJ

ND ND ND <0.5 <0.5 <0.5 <0.5 <0.52.9 ND 0.6 1.1 1.0 <0.5 <0.5 <0.5

ND ND ND <0.5 <0.5 <0.5 <0.5 <0.5ND ND ND <0.5 <0.5 <0.5 <0.5 0.8ND ND ND <0.5 <0.5 <0.5 <0.5 <0.5ND ND ND <0.5 <0.5 <0.5 <0.5 <0.5

<1.0

2.7<0.5

1.8<0.5

1.1<0.5<0.5<0.5<0.5

<1.0 M1000 548 616 490 690<O.S <0.5 <0.5 <0.5 <0.5<5.0 <5.0 <5.0 <5.0 <5.0680 1060 1130 1010<10 <10 <10 <10 16

<2.0 <2.0 <2.0 <2.0 <2.0<20 <20 <20 <20 <20

<0.05 <0.05 <0.05 0.57 <0.05<0.05 <0.05

6.7 7.5 6.5 6.61<0.05

<10 34 38 <10 322.5 1.5 1.6 2.7 2.4 3.2 1.9

<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.01.6 1.2 <1.0 <1.0 3.4 <1.0 <1.0

<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.51.1 0.9 <0.5 <0.5 <0.5 1.1 <0.5

<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <2.0 '<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <2.0 !

<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <2.0 '<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <2.0 '

1A93-300 and A94-100 are blind duplicate tample* of A91-7S.• • Samples no longer Meld - filtered starting 11/29/94.1 Total Xylene is reported as a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0/tg/t,

3; 29- Jifl-77 fit* tot 9 Efgoo



fARAMET^MiiSSÂlkalinity, TotalArsenic, Dissolved/Total* •Calcium, Dissolved/Total"ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total"Magnesium, Dissolved/Total"Manganese, Dissolved/Total"Nitrogen, AmmoniaPotassium, Dissolved/Total* •Residue, T. Fit. (Dias.)Sodium, Dissolved/Total* •SulfateTotal Kjeldahl N (TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead, PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (as N)pH, LabSulfide, Total (as HjS)Zinc, ZnBenzeneChlorobenzeneChloroethane1,1-Dichloroethanecis - 1,2 - Dichloroelhyleneo- Dichlorobenzene (1,2)p- Dichlorobenzene (1,4)>-Xylcnem-Xylene

:;i5:':''i?-S!?B;:;swxs;*:?m:lvwm

mg/1ug/1mg/1mg/1mg/1mg/1ntuug/1mg/1ug/1mg/1mg/1mg/1mg/1mg/1mg/1mg/1ug/1ug/1ug/1UMHOug/1ug/1ug/1mg/1mg/1S.U.mg/1ug/1Ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1UK/I

XvX-X-Xi-S-xftfe1n310<5100

7220

8103296

1.675.0

4325.851

Z03<1.0

NDNDNDNDNDNDNDNDND

HoUIri419i 9

1008

<8

580034

350<0.05

3.13908.046

0.15<1.0

1

NDNDNDNDNDNDNDNDND

mmmmm387<3100

78

<103310

0.132.73766.645

0.51<1.0

NDNDNDNDNDNDNDNDND

492<3.098.710.8<20

<2034.0

74<0.05

2.04345.9

49.41.571.0

NDNDNDNDNDNDNDNDND

315<3.097.89.44220

<2034.2

410.061.7

3286.5

34.70.50<1.0

NDNDNDNDNDNDNDNDND

495<3.010211.2

19<8

1250<4033.5

550.102.63866.745

0.301.7

NDNDNDNDNDNDNDNDND

<3.0

4.92

21

<40

0.05

363

2.2

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

<3.0

4.3133<8

1200<40

0.05

4406.1

4.2

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

masim364

<3.099.95.68

<20

<4034.8

48<0.05

2.14396.258

0.592.0

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

m<3.0

6.65

<20

<40

<0.05

4206.4

3.5

<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5

<3.0 <3.0

7.13 6.00

<8 <8

<40 <40

<0.05 <0.05

418 4185.9 7.6

<1.0 1.8

<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5<0.5 <0.5

iHiiiliiii345

<3.087.26.83<8

0.7562

31.347

<0.052.54425.747

137<0.5

6.6597<10<2.0<200.61

<0.057.2

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

111'i®m346

<3.085.26.80<8

0.8548

30.046

<0.054.75056.953

136<0.5<5.0710<10<2.0<200.78

7.2

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

sAliiiisiiiii408

<3.086.29.45<8

0.3373

33.658

<0.05<2.04207.443

156<0.5<5.0

<10<2.0<200.80

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

VTBJUl^&m$jt374

<3.085.66.2<8

0.40<4033.5

570.07<2.04545.950

152<O.S<5.0773<10

<2.0<20

<0.05

7.0

<10<1.0<1.0<1.0<0.5<0.5<1.0<1.0<1.0<1.0

wmm366 II

<3.098.6

5<20

0.30<4036.8

73<0.05<2.04507.145

175<0.5<5.0731

11<2.0<200.40

7.21<0.05

<10<1.0<1.0<1.0<0.5<0.5<2.0 '<2.0'<2.0 '<2.01ll

• A91-100 la a blind replicate sample of A91-4S•• Sampla no longer field - filtered starting 11/29/94.1 Total Xylene la reported aa a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0/tg/l.

I Of 9

TABLE 3.RESULTS OF STATISTICAL ANALYSES

TREMONT LANDFILL ASSESSMENT

Antimony

Artenic

Bctyfltmn

CotaftCopperLeadNickel&* ftp .ilium

Thallium

Vanadium

Zinc

Amnooia

Chloride

Sodttun

COD

IDS

ToUl Alkalinity

Nitrate-Nitrite

Sulfatc

100

43

0

100

93

90

100

93

80

83

100

100

100

100

70

20

0

0

47

0

0

82

11

>15%ND

>15%ND

(aft/fail

>15%ND

>15%ND

>15%ND

>15%ND

>15%ND

>1S%ND

>1S*ND

>15%ND

>15%ND

>15%ND

>15%ND

>15%ND

>15%ND

(au/Iail

>15%ND

pass/ — —

pass/ —

>15%ND

pass/— fafl

fafl

all pas*

fafl

an pass

an pass

all pass

an pass

an pass

aU pass

Ofl

att pass

aU pass

an pass

aU pass

all pass

fan

fanfail

fafl

faD

an pass

aU pass

AB9-2<afls

M-2fafls

M-2fafls

M-2, AS9-3S, A91-7S fafl

M-2, AS9-3S, A89-3D fail

M-2fafls

M-2, A89-3D fafl

A89-2, AS9-3S; AB9-3D. A91-4S,A91-7S,M-2faflA89-2, A89-3D, A91-7S, M-2 fafl

\tremont\sta tana.wk3;06-Aug-% Eagon & Associates, Inc.

TABLE 4.SUMMARY OF APPENDIX I AND APPENDIX II ORGANIC COMPOUND DETECTIONS

TREMONT LANDFILL 11/25/96 ASSESSMENT SAMPLING

Benzene

Carbon disulfide

Chlorobenzene

1,2 - Dichlorobenzene

1,1 -Dichloroethane

Toluene

Bis (2-ethylhexyl) phthalate

Di-n-octyl phthalate

<5.0

<2.0

<0.5

8.5

43

<5.0

28.0

4.2

3.7

1.1

4.2

<5.0

27.7

4.2

<2.0

<5.0

<2.0

6.1

5.4

2.8

1.9

<5.0

<2.0

<0.5

<2.0

5.2

<2.0

<0.5

1.6

11

\tremont\labres.wk3;05-Feb-97 Eagon & Associates, Inc.

TABLE 5.PARAMETERS REQUIRING TARGET CONCENTRATIONS

TREMONT LANDFILL ASSESSMENT

ArsenicLead*Zinc*BenzeneChlorobenzeneChloroethaneo-Dichlorobenzene (1,2)p-Dichlorobenzene (1,4)1,1- Dichloroethanecis -1,2 - Dichloroethylenep-Xylenem-XyleneAmmoniaChlorideSodiumCODTDSTotal AlkalinityMagnesiumCalciumPotassiumIronManganese

A89-2M-2M-2

A89-2A89-2A89-2M-2M-2

A89-3SA91-7SA91-7SA91-7SA89-3SA89-3S

M-2M-2

A89-3SA89-3S

M-2M-2

A89-3SA89-2A91-7S

7010,00010,000

* Added to parameter list after 6/1/94.•• SMCL \

*** <2.0 TotalXylene

tremont\paratarg.wk3;06-Feb-97 Eagon & Associates, Inc.

APPENDIX A.

ANALYTICAL RESULTS AND FIELD MEASUREMENTS

ASSESSMENT WELL FIELD MEASUREMENTS, TREMONT LANDFILL

iM^mtc>*ii|gi

11/25/96 M-2A89-2A89-3SA89-3DA91-4SA91-7S96-300*

30.4415.4917.3219.7814.1031.1315.49

982.56982.06984.35982.50982.67982.50982.06

6.726.816.996.287.427.746.77

2030102018811853683979

1029

11.513.412.712.811.712.013.2

1880.8316.52.381.652.652.21

•96-300 is a blind duplicate sample from A89-2.

\tremont\l 194afim.wk3;05 - Feb- 97 Eagon & Associates, Inc.

ATELAqua Tech Environmental Laboratories, Inc.

- CERTIFICATE OF ANALYSIS -Client*: 10107

Eagon & Associates Inc100 Old Wilson Bridge RdSuite 320Worthington, OH 43085

Attn: Frank Majchszak

Report Date: 13-Dec-96

Phone: (614)888-5760 Ext:FAX: (614)888-5763

Our Lab #: MAR96-30646Date Logged-In: ll/27/%

Matrix: WaterProject #:

Your Sample ID: M-2Sample Source: Groundwater Monitoring

Client Project #: PO#:Date Submitted to Lab: 11/26796

- COLLECTION INFORMATION -Date/Timely: 11/25/96 11:30 AM VINS

Teat Group EPA Method Test ResultAnalysis

Units Date Analyst WS#

SB-GFAAAS-GFAABA-ICPBE-GFAACD-GFAACR-GFAACO-ICPCU-ICPPB-GFAANI-ICPSE-GFAAAG-GFAATL-GFAA,V-ICPZN-ICPNH3NA-ICPCOD-fflPH-LABTDSALKNO3SO4-IC

3113B/70413113B/7060200.7/60103113B/70913113B/71313113B/7191200.7/6010200.7/60103113B/7421200.7/60103113B/77403113B/77613113B/7841200.7/6010200.7/6010

350.1200.7/6060410.4^7196150.1/9040

160.1SM 2300B

353.2300.0

Antimony, SbArsenic, AsBarium, BaBeryllium, Ber"artmhim CA

Chromium, CrCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilver, AgThallium. TlVanadium, VZinc, ZnNitrogen, Ammonia (as N)Sodium, NaCODpH,LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalNitrate + Nitrite NSulfate, SO4

<3.03.2135

<0.50.9

<5.0<10

105.722

<15.0<1.0<1.0<20117

0.77189100

6.63160010400.05130

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LMG/LMG/LMG/LS.U.

MG/LMG/LMG/LMG/L

12/3/9612/2/9612/3/9612/4/96121619612/3/9612/3/96121319612/3/9612/3/9612/3/96

-12/2/961212/9612/3/9612/3/9612/4/96121519612/3/9611/26/9611/27/9612/9/9612/3/9612/6/96

ROHSMMRCBKRGSMMSMMRCBRCBRCBRGBROHSMMRCBRCBRCBRJASMMBKHMDOMDOKVSRJABKH

13071298134013491382131113401340132413401313129612971340134013181359133312681286139713031385

Lab Number MAR96-30646:Page I

1776 MARION WALDO RD. P.O. BOX 436 MARION. OH 43301-0436PHONE 614-389-5991 1-800-873-2835 FAX 614-389-1481


CERTIFICATE OF ANALYSIS -Lab Number MAR96-30646 -Continuedfrom Previous Page

Test Group EPA Method Test Result UnitsAnalysis

Date Analyst WS#

MG-ICPCA-ICPK-ICPTURBFE-ICPMN-ICPCOND-LCNHGH2SSN-ICPCL-IC

—— ——— —— —— .200.7/6010200.7/6010200.7/6010

180.1200.7/6010200.7/60102510B/9050335.4/9012245.1/7470376.2/9030200.7/6010

300.0

.Magnesium, MgCalcium, CaPotassium, KTurbidityIron,FeManganese, MnConductivity, LabCyanide, Total (as CN)Mercmy, HgSulfide, Total (as H2S)Tin,SnChloride, Cl

87.42055.2

22018400

1642420

< 0.005<0.20.42

<100182

MG/LMG/LMG/LNTUUG/LUG/LuMHOMG/LUG/LMG/LUG/LMG/L

•""———• ———12/3/9612/3/9612/3/9611/27/9612/3/9612/3/9612/3/9612/2/9612/2/96IW/9612/3/9612/6/96

^•^HM^^MM

RGBRGBRGBMDORGBRGBLGRKVSROHLGRSMMBKH

"• • ^134013401340128413401340132712911293133613281385

End of Report

Report Approved By: && 'JyiAA, ^^n>&*^*j

Deborah K. Johnson

Note: The reporting detection lin.it for Selenium is elevated due to matrix

interferences tu ..fchat required serial dilution of the sample.

Lab Number MAR96-30646:Pa£e 2

1776 MARION WALDO RD.PHONE 614-389-5991

P.O. BOX 436 MARION. OH 43301-04361-800-873-2835 FAX 614-389-1481


- CERTIFICATE OF ANALYSIS -Client #: 10107



Report Date: l3-Dec-96

Phone: (614)888-5760 Ext:FAX: (614)888-5763

Our Lab #: MAR96-30647Date Logged-In: 11/27/96


Your Sample ID: A89-2Sample Source: Groundwater Monitoring

Client Project*: POfcDate Submitted to Lab: 11/26/96

- COLLECTION INFORMATION -Date/Time/By: 11/25/96 2:30 PM VINS


Analyst WS#

SB-GFAAAS-GFAABA-ICPBE-GFAACD-GFAACR-GFAACO-ICPCU-ICPPB-GFAANI-ICPSE-GFAAAG-GFAATL-GFAAV-ICPZN-ICPNH3NA-ICPCOD-fflPH-LABTDSALKNO3SO4-IC

31138^0413113B/7060200.7/60103113B/70913113B/71313113B/7191200.7/6010200.7/60103113B/7421200.7/60103113B/77403113B/77613113B/7841200.7/6010200.7/6010

350.1200.7/6060410.4/71%150.1/9040

160.1SM 2300B

353.2300.0

Antimony, SbArsenic, AsBarium, BaBeryllium, Befarimiurn fd

Chromium, CrCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilver, AgThallium, TlVanadium, VZinc, ZnNitrogen, Ammonia (as N)Sodium, NaCODpH,LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalNitrate + Nitrite NSulfate, SO4

<3.060

697<0.5<0.5<5.0<10<10<2.0<20<3.0<1.0<1.0<20<100.3637.1<206.65718573

<0.05<5


MG/LMG/LMG/LMG/L

12/3/9612/2/9612/3/9612/4/9612/6/9612/3/9612/3/9612/3/9612/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/4/%12/5/9612/3/%11/26/9611/27/9612/9/96I2/3/%12/6/96

ROHSMMRCBKRGSMMSMMRGBRGBRCBRCBROHSMMRCBRCBRCBRJA

SMMBKHMDOMDOKVSRJABKH

1307129813401349138213111340134013241340131312%12971340134013181359133312681286139713031385

Lab Number MAR96-30617:Pagc I



- CERTIFICATE OF ANALYSIS -Lab Number MAR96-30647 -Continued from Previous Page


Date Analyst WS#


—— — — — ^——— i200.7/6010200.7/6010200.7/6010

180.1200.7/6010200.7/6010251 OB/9050335.4/9012245.1/7470376.2/9030200.7/6010

300.0

————————————Magnesium, MgCalcium, CaPotassium, KTurbidityIron,FeManganese, MnConductivity, LabCyanide, Total (as CN)Mercury, HgSulfide, Total (as H2S)Tin,SnChloride, Cl

44.11294.1180

24500222

1020< 0.005

<0.2<0.05<100

49

^•^^^MMB^H

MG/LMG/LMG/LNTU

UG/LUG/LuMHOMG/LUG/LMG/LUG/LMG/L

12/3/9612/3/9612/3/9611/27/96121319612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/6/96

—— — _RGBRGBRGBMDORGBRGBLGRKVSROHLGRSMMBKH

M^^M^^

134013401340128413401340132712911293133613281385

End of Report

l\ . /I / a /

Report Approved By: ^/^ falAA' ^>Cno^^>

Deborah K. Johnson

Lab Number MAR96-30647:Pagc 2






Report Date: !6-Dec-96

Phone: (614)888-5760 Ext:FAX: (614)888-5763

Our Lab 0: MAR96-30648Date Logged-In: 11/27/96

Matrix: WaterProjectfc

Your Sample ID: A89-3SSample Source: Groundwater Monitoring

Client Project#: PO#:Date Submitted to Lab: 11/26/96

- COLLECTION INFORMATION -Date/Time/By: 11/25/96 2:00 PM VINS

Test Group EPA Method Test Result AnalysisUnits Date Analyst WS#

SB-GFAAAS-GFAABA-ICPBE-GFAACD-GFAACR-GFAACO-ICPCU-ICPPB-GFAANI-ICPSE-GFAAAG-GFAATL-GFAA „V-ICPZN-ICPNH3NA-1CPCOD-HIPH-LABTDSALKNO3SO4-IC

3113B/704I3113B/7060200.7/60103113B/70913113B/71313113B/7191200.7/6010200.7/60103113B/7421200.7/60103113B/77403113B/77613113B/7841200.7/6010200.7/6010

350.1200.7/6060410.4/7196150.1/9040

160.1SM 2300B

353.2300.0

Antimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdChromium, CrCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilver, AgThallium, TlVanadium, VZinc, ZnNitrogen, Ammonia (as N)Sodium, NaCODpH, LabResidue. Filterable (Dissolved Solids)Alkalinity, TotalNitrate + Nitrite NSulfate, SO4

<3.04.7

244<0.5<0.5<5.0<10<106.0

<20<3.0

-<1.0<1.0<20

111.1113549

6.661360859

<0.0576


MG/LMG/LMG/LMG/L

12/3/9612/2/9612/3/9612/4/9612/6/9612/3/9612/3/9612/3/9612/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/4/9612/5/9612/3/9611/26/961 1/27/9612/9/9612/3/9612/6/96

ROHSMMRGBKRGSMMSMMRGBRGBRGBRGBROHSMMRGBRGBRGBRJA


13071298134013491382131113401340132413401313129612971340134013181359133312681286139713031385

Lab Number MAR96-30648:Pagc I

1776 MARION WALDO RD. P.O. BOX 436PHONE 614-389-5991 1-800-873-2835

MARION, OH 43301-0436FAX 614-389-1481


- CERTIFICATE OF ANALYSIS -Lab Number MAR96-30648 -Continuedfrom Previous Pi•age

Test Group


EPA Method

200.7/6010200.7/6010200.7/6010

180.1200.7/6010200.7/6010251 OB/9050335.4/9012245.1/7470376.2/9030200.7/6010

300.0

Test

Magnesium, MgCalcium, CaPotassium, KTurbidityIron, FeManganese, MnConductivity, LabCyanide, Total (as CN)Mercury, HgSulfide, Total (as H2S)Tin,SnChloride, Cl

Result

84.81806.1120

15700233

1980< 0.005

<020,13

<100139

Units

MG/LMG/LMG/LNTUUG/LUG/L

uMHOMG/LUG/LMG/LUG/LMG/L

AnalysisDate

12/3/9612/3/9612/3/96

11/27/9612/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/6/96

Analyst—— —. —

RCBRCBRCBMIX)RCBRCBLGRKVSROHLGRSMMBKH

ws#•• ^^

134013401340128413401340132712911293133613281385

End of ReportA _ . £

Report Approved By: -Jjh7<aA ^&*+***—i

Deborah K. Johnson

Lab Number MAR96-30648:Page 2

1776 MARION WALDO RD. P.O. BOX 436 MARION, OH 43301-0436PHONE 614-389-5991 1-800-873-2835 FAX 614-389-1481


- CERTIFICATE OF ANALYSIS -Client*: 10107


Report Date: I3-Dec-96




Phone: (614)888-5760 Ert:FAX: (614)888-5763

Your Sample ID: A89-3DSample Source: Groundwater Monitoring

Client Project #: PO#:Date Submitted to Lab: 11/26/96

- COLLECTION INFORMATION -Date/Time/By: 11/25/96 11:10 AM VINS

;


Analyst WS#

SB-GFAAAS-GFAABA-ICPBE-GFAACD-GFAACR-GFAACO-ICPCU-ICPPB-GFAANI-ICPSE-GFAAAG-GFAATL-GFAAV-ICPZN-ICPNH3NA-ICPCX>D-fflPH-LABTDSALKNO3SO4-IC

3113B/70413113B/7060200.7/60103113B/70913113B/71313113B/7191200.7/6010200.7/60103113B/7421200.7/60103113B/77403113B/77613H3B/7841200.7/6010200.7/6010

350.1200.7/6060410.4/7196150.1/9040

160.1SM 2300B

353.2300.0

Antimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdChromium, CrCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilver, Ag.Thallium, TlVanadium, VZinc, ZnNitrogen, Ammonia (as N)Sodium, NaCODpH,LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalNitrate + Nitrite NSulfate, SO4

<3.0<3.0

176<0.5<0.5<5.0<10<10<2.0

30<3.0<1.0<1.0<20<100.1115667

6.7313707750.06

49

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LMG/LMG/LMG/L

S.U.MG/LMG/LMG/LMG/L

12/3/9612/2/9612/3/9612/4/9612/6/9612/3/9612/3/9612/3/9612/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/4/9612/5/9612/3/9611/26/9611/27/9612/9/9612/3/9612/6/96

ROHSMMRGBKRGSMMSMMRGBRCBRGBRGBROHSMMRCBRCBRCBRIASMMBKHMDOMDOKVSRJABKH

13071298134013491382131113401340132413401313129612971340134013181359133312681286139713031385

Lab Number MAR96-30649:Page I



- CERTIFICATE OF ANALYSIS -Lab Number MAR96-30649 -Continued from Previous Page


Date Analyst WS#


200.7/6010200.7/6010200.7/6010

180.1200.7/6010200.7/60102510B/9050335.4/9012245.1/7470376.2/9030200.7/6010

300.0

Magnesium, MgCalcium, CaPotassium, KTurbidityIron,FeManganese, MnConductivity, LabCyanide, Total (as CN)Mercury, HgSulfide, Total (as H2S)Tin,SnChloride, Cl

71.51732.794

10800232

1940< 0.005

<0.2<0.05<100

181

MG/LMG/LMG/LNTU

UG/LUG/LuMHOMG/LUG/LMG/LUG/LMG/L

12/3/9612/3/9612/3/96ll/27/%12/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/6/96

RGBRCBRCBMDORGBRGBLGRKVSROMLGRSMMBKH

134013401340128413401340132712911293133613281385

End of Reportf\ . /) / d J

Report Approved By: &£^<v£/*****~j

Deborah K. Johnson

Lab Number MAR96-30649:Page 2


P.O. BOX 436 MARION, OH 43301-04361-800-873-2835 FAX 614-389-1481






Phone: (614)888-5760 Ext:FAX: (614)888-5763



Your Sample H>: A91-4SSample Source: Groundwater Monitoring

Client Project #: PO#:Date Submitted to Lab: 11/26/96

- COLLECTION INFORMATION-Date/Time/By: 11/25/96 3:20 PM VINS


Analyst WS#

SB-GFAAAS-GFAABA-ICPBE-GFAACD-GFAACR-GFAACO-ICPCU-ICPPB-GFAANI-ICPSE-GFAAAG-GFAA-TL-GFAA „V-ICPZN-ICPNH3NA-ICPCOD-HIPH-LABTDSALKNO3SO4-IC

3113B/70413113B/7060200.7/60103113B/70913113B/71313113B/7191200.7/6010200.7/60103113B/7421200.7/60103113B/77403113B/77613113B/7841200.7/6010200.7/6010

350.1200.7/6060410.4/7196

. 150.1/9040160.1

SM 2300B353.2300.0

Antimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdChromium, CrCobalt, CoCopper, CuLead, PbNickel, NiSelenium, SeSilver, AgThallium, TlVanadium, VZinc, ZnNitrogen, Ammonia (as N)Sodium, NaCODpH, LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalNitrate + Nitrite NSulfate, SO4

<3.0<3.0

175<0.5<0.5<5.0<10

I I<2.0<20

<3.0< 1.0<1.0<20<10

<0.057.1

<207.21450366

0.4045

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LMG/LMG/LMG/L

S.U.MG/LMG/LMG/LMG/L

12/3/9612/2/9612/3/9612/4/9612/6/9612/3/9612/3/9612/3/9612/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/4/9612/5/9612/3/9611/26/961 1/27/9612/9/9612/3/9612/6/96

ROHSMMRGBKRGSMMSMMRGBRCBRGBRCBROHSMMRCBRCBRCBRJA


Lab Number MAR96-306SO:

13071298134013491382131113401340132413401313129612971340134013181359133312681286139713031385

Page 1



- CERTIFICATE OF ANALYSIS -Lab Number MAR96-30650 -Continuedfrom Previous Page


Date Analyst WS#


200.7/6010200.7/6010200.7/6010

180.1200.7/6010200.7/6010251 OB/9050335.4/9012245.1/7470376.2/9030200.7/6010

300.0

-Magnesium, MgCalcium, CaPotassium, KTurbidityIron,FeManganese, MnConductivity, LabCyanide, Total (as CN)Mercury, HgSulfide, Total (as H2S)Tin,SnChloride, Cl

1

36.898.6

<2.00.3

<4073

731< 0.005

<02<0.05<IOO

5

— ^— >_^_MG/LMG/LMG/LNTUUG/LUG/LuMHOMG/LUG/LMG/LUG/LMG/L

12/3/9612/3/9612/3/96

1 1/27/9612/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/6/96

RCBRCBRCBMDORCBRCBLGRKVSROMLGRSMMBKH

134013401340128413401340132712911293133613281385

End of Reportr\ . /)/ / /Report Approved By: J^4>

/ 4^ /C/9« £^0-" -*»/

Deborah K. Johnson

Lab Number MAR96-30650 Page 2



- CERTIFICATE OF ANALYSIS -Client #: (0107



Report Date: !6-Dec-96

Phope: (614)888-5760 Ext:FAX: (614)888-5763



Your Sample ID: A91-7SSample Source: Groundwatcr Monitoring

Client Project #: PO#:Date Submitted to Lib: 11/26796

- COLLECTION INFORMATION -Date/Timely: 11/25/96 3:55 PM VINS

Test Group EPA Method Test ResultAnalysis


SB-GFAAAS-GFAABA-ICPBE-GFAACD-GFAACR-GFAACO-ICPCU-ICPPB-GFAANl-ICPSE-GFAAAG-GFAATL-GFAA „V-ICPZN-ICPNH3NA-ICPCOD-HIPH-LABTDSALKN03SO4-IC

3113B/70413113B/7060200.7/60103113B/70913113B/713I3113B/7191200.7/6010200.7/60103113B/7421200.7/60103113B/77403113B/77613113B/7841200.7/6010200.7/6010

350.1200.7/6060410.4/7196150.1/9040

160.1SM 2300B

353.2300.0

Antimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdChromium, CrCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilver, AgThallium, TlVanadium, VZinc, ZnNitrogen, Ammonia (as N)Sodium, NaCODpH.LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalNitrate + Nitrite NSulfate, SO4

<3.017

690<0.5<0.5<5.0<10

16<2.0<20<3.0<1.0<1.0<20

32<0.05

8.6<206.61675581

<0.0523


MG/LMG/LMG/LMG/L

12/3/9612/2/9612/3/9612/4/9612/6/9612/3/9612/3/9612)3/9612/3/9612/3/9612/3/96

- 12/2/9612/2/9612/3/9612/3/9612/4/9612/3/9612/3/9611/26/9611/27/9612/9/9612/3/9612/6/96

ROHSMMRGBKRGSMMSMMRGBRGBRGBRGBROHSMMRGBRCBRCBRJARCBBKHMDOMDOKVSRJABKH

13071298134013491382131113401340132413401313129612971340134013181340133312681286139713031385

Lab Number MAR96-306S1: Page I


P.O. BOX 4361-800-873-2835

MARION, OH 43301-0436FAX 614-389-1481


CERTIFICATE OF ANALYSIS -Lab Number MAR96-30651 -Continuedfrom Previous Page


Date Analyst WS#


200.7/6010200.7/6010200.7/6010

180.1200.7/6010200.7/60102510B/9050335.4/9012245.1/7470376.2/9030200.7/6010

300.0

Magnesium, MgCalcium, GaPotassium, KTurbidityIron,FeManganese, MnConductivity, LabCyanide, Total (as CN)Mercury, HgSulfide, Total (as H2S)Tin, SnChloride, Cl

50.51312.6120

18500845

1010< 0.005

<0.2<0.05<100

23

MG/LMG/LMG/LNTUUG/LUG/L

uMHOMG/LUG/LMG/LUG/LMG/L

12/3/9612/5/9612/3/96

1 1/27/9612/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/6/96

RGBSMMRGBMDORGBRGBLGRKVSROHLGRSMMBKH

134013591340128413401340132712911293133613281385

End of Report

Report Approved By: jW t/ ^0i. ./T. ^ £^*+a*r*~~jDeboraFK-Johnson

umber MAR96-3065l:Pagt 2







Phone: (614)888-5760 Ext:FAX: (614)888-5763



Your Sample ID: FB-1Sample Source: Groundwater Monitoring

Client Project #: PO#:Date Submitted to Lib: 11/26/96

-COLLECTION INFORMATION -Date/Time/By: 11/25/96 4:15PM VINS

Test Group EPA Method Test ResultAnalysis


SB-GFAAAS-GFAABA-ICPBE-GFAACD-GFAACR-GFAACO-ICPCU-ICPPB-GFAANI-ICPSE-GFAAAG-GFAA.TL-GFAAV-ICPZN-ICPNH3NA-ICPCOD-HIPH-LABTDSALKNO3SO4-IC

3113B/70413113B/7060200.7/60103113B/70913113B/71313113B/7191200.7/6010200.7/60103113B/7421200.7/60103113B/77403113B/77613113B/7841200.7/6010200.7/6010

350.1200.7/6060410.4/7196150.1/9040

160.1SM 2300B

353.2300.0

Antimony, SbArsenic, AsBarium, BaBeryllium, BeCadmium, CdChromium, CrCobalt, CoCopper, CuLead,PbNickel, NiSelenium, SeSilver, AgThallium, TlVanadium, VZinc, ZnNitrogen, Ammonia (as N)Sodium, NaCODpH,LabResidue, Filterable (Dissolved Solids)Alkalinity, TotalNitrate + Nitrite NSulfate, SO4

<3.0<3.0<10<0.5<0.5<5.0<10<102.7

<20<3.0< 1.0<1.0<2016600.15

<0.4<206.01

62<1

<0.05< 5


MG/LMG/LMG/LMG/L

12/3/9612/2/9612/3/9612/4/9612/6/9612/3/9612/3/9612/3/9612/4/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/4/9612/3/9612/3/9611/26/9611/27/9612/9/9612/3/9612/6/96

ROHSMMRGBKRGSMMSMMRGBRCBSMMRGBROHSMMRCBRCBRCBRJARCBBKHMDOMDOKVSRJABKH

13071298134013491382131113401340133913401313129612971340134013181340133312681286139713031385

Lab Number MAR96-30653:Page /



- CERTIFICATE OF ANALYSIS -Lab Number MAR96-30653 -Continuedfrom Previous Page

AnalysisTest Group


EPA Method

200.7/6010200.7/6010200.7/6010

180.1200.7/6010200.7/6010251 OB/9050335.4/9012245.1/7470376.2/9030200.7/6010

300.0

Test

Magnesium, MgCalcium, CaPotassium, KTuibidityIron,FeManganese, MnConductivity, LabCyanide. Total (as CN)Mercuiy.HgSulfide, Total (as H2S)Tin.SnChloride, Cl

Result

<0.10.5

<2.03.443

<1018

< 0.005<0.2

<0.05<100

<5

Units

MG/LMG/LMG/LNTUUG/LUG/LuMHOMG/LUG/LMG/LUG/LMG/L

Date

12/3/9612/5/9612/3/9611/27/9612/3/9612/3/9612/3/9612/2/9612/2/9612/3/9612/3/9612/6/96

Analyst

RCBSMMRCBMDORCBRCBLGRKVSROHLGRSMMBKH

WS#

134013591340128413401340132712911293133613281385

End of Report

Report Approved By: dbpyiAA, /C.^j"™**1^Deborah K. Johnson

Zîfc Number MAR96-30653:Page 2


P.O. BOX 436 MARION. OH 43301-04361-800-873-2835 FAX 614-389-1481

Aqua Tech Environmental Laboratories Inc.

SAMPLE PREPARATION/METHOD SUMMARY FORM

APPENDIX II ANALYSIS

riient: EAGON & ASSOCIATES INCDate Sampled: 11/25/96

Location: M-2

ATEL Sample No.: 96-16814-MELDate Received: 11/26/96

fethod Used Date Extracted Date Analyzed Analyst

JW-846; Method

JW-846; Method

JW-846; Method

iW-846; Method

:w-846; Method

IW-846; Method

8015

8081

8150

8240 (SIM)

8260

8270

N/A

11/26/96

12/02/96

N/A

N/A

11/27/96

12/03/96

12/11/96

12/07/96

11/27/96

12/06/96

12/09/96

DJS

CMR

DAW

JSM

JSM

KJP

6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE. OH 44845-9999PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229

AQUA, TECH ENVIRONMENTAL LABORATORIES, INC.APPENDIX II ANALYSES

Page 1 of 5

Customer Name: EAGON & ASSOCIATES INCSample Description: M-2

ATEL No.: 96-16814-MEL

Compound

AcenaphtheneAcenaphthyl eneAcetoneAcetonitrileAcetophenone2 -Acetylaminof loureneAcroleinAcrylonitrileAldrinAllyl chloride4 - AminobiphenylAnthraceneAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260BenzeneBenzo [a] anthraceneBenzo [b] flouranbheneBenzo [k] flour an then eBenzo [ghi] peryleneBenzo [a] pyreneBenzyl alcoholalpha -BHCseta-BHCielta-BHCjamma-BHC (Lindane)3is (2 -chloroethoxy) methane3is (2 -chloroethyl) ether3is (2 -chXoro-1-methylethyl) ether3is (2-ethylhexyl)phthalate3romochlorome thaneJromodichlorome thane3romof ormJromome thanel-Bromophenyl phenyl etheriutyl benzyl phthalateCarbon disulfideCarbon tetrachloride-hlordane> - Chloroani 1 ine

Concentration-

< 2.0< 2.0< 5.0< 500< 3.0< 5.0< 5.0< 5.0< 0.02< 20.0< 5.0< 2.0< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 1.0< 3.0< 4.0< 4.0< 5.0< 4.0< 5.0< 0.02< 0.02< 0.02< 0.02< 2.0< 2.0< 2.0

8.5< 1.0< 1.0< 1.0< 1.0< 3.0< 2.0< 5.0< 1.0< 0.10< 3.0

Method

ft OT f\oZ / U827082608015827082708240 SIM8240 SIM808182608270827080818081808180818081808180818260827082708270827082708270808180818081808182708270827082708260826082608260827082708260826080818270

6878 S STATE ROUTE 100 • MELMORE. OH 44845 9999

AQUA TECH ENVIRONMENTAL LABORATORIES, INC.APPENDIX II ANALYSES


ATELNo.: 96-16814-MELPage 2 of 5

Compound Concentration-ug/1 (ppb) Method

Chlorobenz eneChlorobenzilatep-Chloro-m-CresolChloro e thaneChloroformChlorome thane2 -Chloronaph thai ene2 -Chlorophenol4-Chlorophenyl phenyl etherChloropreneChrysenem-Cresolo-Cresolp-Cresol2,4-D4,4'-DDD4, 4' -DDE4,4'-DDTDiallateDibenz [a, h] anthraceneDibenzofuranDibromochlorome thanel,2-Dibromo-3-chloropropane (DBCP)1,2-Dibromoethane (EDB)Dibromome thaneDi-a-butyl phthalate1,2 -Dichlorobenzene1,3 -Dichlorobenzene1, 4 -Dichlorobenzene3,3' -Dichlorobenzidinetrans-1, 4-Dichloro-2-buteneDichlorodifluorome thane1, 1-Dichloroe thane1,2 -Dichloroe thane1, 1-Dichloroe thylenecis-1, 2 -Dichloroe thylenetrans-1, 2 -Dichloroe thylene2,4 -Dichlorophenol2,6 -Dichlorophenol1,2 -Dichloropropane1, 3 -Dichloropropane2,2 -Dichloropropane1, 1 -Dichloropropenezis-1, 3 -Dichloropropenetrans-1, 3 -DichloropropeneDieldrinDiethyl phthalateDimethoate

< 1.0< 4.0< 5.0< 1.0< 0.5< 1.0< 1.0< 5.0< 2.0

N.D.< 3.0< 3.0< 3.0< 3.0< 0.10< 0.02< 0.03< 0.03< 3.0< 5.0< 2.0< 1.0< 1.0< 1.0< 1.0< 1.0< 2.0< 2.0< 2.0< 15.0< 1.0< 1.0< 0.5< 0.5< 0.5< 0.5< 0.5< 3.0< 10.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.02< 1.0< 4.0

826082708270826082608260827082708270826082708270827082708150808180818081827082708270826082608260826082708270827082708270826082608260826082608260826082708270826082608260826082608260808182708270

6878 S STATE ROUTE 100 • MELMORE. OH 44845-9999



ATEL No.: 96-16814-MELPage 3 of 5

Compound

p- (Dimethylamino) azobenzene7 , 12 -Dimethylbenz [a] anthracene3,3' -Dimethylbenz idine2,4 -DimethylphenolDimethyl phthalatem-Dinitrobenzene4, 6-Dinitro-o-cresol2,4 -Dini trophenol2,4 -Dini trotoluene2, 6 -Dini tro tolueneDinosebDi-n-octyl phthalateDiphenylamineDisulfotonEndosulfan IEndosulfan IIEndosulfan SulfateEndrinEndrin aldehydeE thy Ib enz eneEthyl methacrylateEthyl methanesulfonateFamphurFlour an theneFlour eneHeptachlorHeptachlor epoxideHexachl or obenz eneHexachlor obu tadi eneHexachlorocyclopentadi eneHexachloroe thaneBexachloropropene2-HexanoneIndeno (1,2,3-cd) pyr eneIsobutyl alcoholIsodrinIsophoroneIsosafroleKeponeStethacrylonitriletfethapyrileneHethoxychlor3 -MethylcholanthreneMethyl ethyl ketoneMethyl iodideMethyl methacrylateMethyl methanesulfonate

Concentration-

< 5.0< 5.0< 5.0< 3.0< 1.0< 5.0< 10.0< 10.0< 4.0< 4.0< 0.05< 1.0< 4.0< 3.0< 0.03< 0.03< 0.03< 0.02< 0.10< 1.0< 5.0< 4.0< 10.0< 2.0< 3.0< 0.03< 0.03< 2.0< 3.0< 5.0< 3.0< 10.0< 10.0< 5.0< 500< 10.0< 1.0< 5.0< 0.10< 100< 5.0< 0.10< 4.0< 10.0< 10.0< 5.0< 4.0

Method

827082708270827082708270827082708270827081508270827082708081808180818O8180818260826082708081827082708081808182708270827082708270826082708015827082708270808182608270808182708260826082608270

6878 S STATE ROUTE 100 • MELMOflE. OH 44845-9999

AQUA TECH ENVIRONMENTAL LABORATORIES, TNC.APPENDIX II ANALYSES

Customer Name: EA6ON & ASSOCIATESSample Description: M-2

INC ATELNo.: 96-16814-MELPage 4 of 5

Compound

2 -MethylnaphthaleneMethyl parathion4 -Methyl - 2 -pentanoneHe thyl en e chlorideNaphthalene1.4- Naph thoquinone1-Naph thy lamine2 -Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2 -Hi trophenol4-HitrophenolN-Hi trosodi -n-butylamineN-NitrosodiethylamineN-HitrosodimethylamineN - Hi t rcsodipheny lamineN-NitrosodipropylamineN -Hi trosome thyl e thalamineN-NitrosopiperidineN-NJLtrosopyrrolidine5-Nitro-o-toluidlneParathionPentachlorobenzenePentachloroni trobenzenePentachlorophenolPhenace tinPhenanthrenePhenolp - PhenylenediaminePhoratePrbnaad.dePropionitrilePyreneSafroleSilvexStyrene2,4,5-T

Concentration -

< 2.0< 3.0< 20.0< 1.0< 2,0< 5.0< 4.0< 4.0< 5.0< 5.0< 5.0< 2.0< 3.0< 10.0< 5.0< 5.0< 10.0< 2.0< 2.0< 5.0< 5.0< 4.0< 5.0< 3.0< 5.0< 10.0< 10.0< 5.0< 2.0< 3.0< 5.0< 3.0< 3.0< 50.0< 3.0 -< 5.0< 0.20< 1.0< 0.20

Method

827082708260826082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270826082708270815082608150



Customer Name: EA6ON & ASSOCIATES INCSample Description: M-2


Compound Concentration- Method

1,2, 4, 5-Tetrachlorobenzene1,1, 1, 2-Tetrachloroethane1,1,2, 2-TetrachloroethaneTe tr achl oroe thy 1 ene2,3,4,6- Te tr achl or opheno 1ThionazinTolueneo-ToluldineToxaphene1,2,4- Tr ichlorobenzene1,1,1-Trichloroe thane1,1,2-TrichloroethaneTrichloroethyleneTirichl orof lAJOtx?m t"rhBn?»2,4,5- Tr ichlorophenol2,4,6- Tr ichlorophenol1,2,3- Tr ichloropropaneo,o,o-Triethyl phosphorothioatesym-TrinitrobenzeneVinyl AcetateVinyl ChlorideXylene (Total)

< 4.0< 1.0< 1.0< 1.0< 10.0< 4.0< 1.0< 5.0< 0.10< 2.0< 1.0< 1.0< 0.5< 1.0< 3.0< 3.0< 1.0< 5.0< 10.0< 10.0< 1.0< 2.0

8270826082608260827080818260827080818270826082608260826082708270826082708270826082608260

All units of concentration are ug/L (ppb)





Clients EAGON & ASSOCIATES INCDate Sampled: 11/25/96Saaple Location: A89-2

ATEL Sample No.s 96-16815-MELDate Received: 11/26/96

Method Used Date Extracted Date Analyzed Analyst

SW-846; Method 8015

SW-846; Method 8081

SW-846; Method 8150

SW-846; Method 8240 (SIM)

3W-846; Method 8260

3W-846; Method 8270

N/A

11/26/96

12/02/96

N/A

N/A

11/27/96

12/03/96

12/11/96

12/07/96

11/27/96

12/06/96

12/09/96

DJS

CMR

DAW

JSM

JSM

KJP

6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229

AQUA TECH ENVIRONMENTAL LABORATORIES, INCAPPENDIX II ANALYSES

Page 1 of 5

Customer Name: EA60N & ASSOCIATESSample Description: A89-2

INC ATELNo.: 96-16815-MEL

Compound

AcenaphtheneAcenaph thy 1 eneAcetoneAcetonitrileAcetophenone2-AcetylaminofloureneAcroleinAcrylonitrileAldrinAllyl chloride4 - AminobiphenylAnthraceneAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260BenzeneBenzo [a] anthraceneBenzo [b] f lourantheneBenzo [Ic] f lourantheneBenzo [ghi] peryleneBenzo [a] pyreneBenzyl alcoholalpha -BHCbeta-BHCdelta -BHCgamma -BHC (Lindane)Bis (2 - chloroe thoxy) methaneBis (2-chloroethyl) etherBis (2-chloro-l-methylethyl) etherBis (2-ethylhexyl)phthalateBromochlorome thaneBromodichlorome thaneBromoformBr omome thane4 - Bromophenyl phenyl etherButyl benzyl phthalateCarbon disulfideCarbon tetrachlorideChlordanep - Chloroani 1 ine

Concentration-

< 2.0< 2.0< 5.0< 500< 3.0< 5.0< 5.0< 5.0< 0.02< 20.0< 5.0< 2.0< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10

4.3< 3.0< 4.0< 4.0< 5.0< 4.0< 5.0< 0.02< 0.02< 0.02< 0.02< 2.0< 2.0< 2.0

3.7< 1.0< 1.0< 1.0< 1.0< 3.0< 2.0< 5.0< 1.0< 0.10< 3.0

Method

8270827082608015827082708240 SIM8240 SIM808182608270827080818081808180818081808180818260827082708270827082708270808180818081808182708270827082708260826082608260827082708260826080818270



Customer Name: EAGON & ASSOCIATES INCSample Description: A89-2



Chl or ob enz eneChlorobenzilatep-Chloro-m-CresolChloroethaneChloroformColor ome thane2 -Chloronaph thai ene2 -Chlorophenol4-Chlorophenyl phenyl etherChloropreneChrysenem-Cresolo-Cresolp-Cresol2,4-D4,4'-DDD4, 4' -DDE4, 4' -DOTDiallateDlbenz [a, h] anthraceneDibenzofuranDibromochlorome thane1,2 -Dibromo- 3 - chloropropane (DBCP)1, 2-Dibromoethane (EDB)DibromomethaneDi-n-butyl phthalate1,2 -Dichlorobenzene1,3 -Dichlorobenzene1,4 -Dichlorobenzene3,3' -Dichlorobenzidinetrans-1, 4 -Dichloro-2 -buteneDichlorodi fluorome thane1,1-Dichloroethane1,2 -Dichloroe thane1,1-Dichloroethylenecis- 1,2 -Dichloroethylenetrans-1, 2 -Dichloroethylene2,4 -Dichlorophenol2 , 6 -Dichlorophenol1,2 -Dichloropropane1, 3 -Dichloropropane2 , 2 -Dichloropropane1, 1-Dichloropropenecis-1, 3 -Dichloropropenetrans-1, 3 -DichloropropeneDieldrinDiethyl phthalateDimethoate

28.0< 4.0< 5.0< 1.0< 0.5< 1.0< 1.0< 5.0< 2.0

N.D.< 3.0< 3.0< 3.0< 3.0< 0.10< 0.02< 0.03< 0.03< 3.0< 5.0< 2.0< 1.0< 1.0< 1.0< 1.0< 1.0

4.2< 2.0< 2.0< 15.0< 1.0< 1.0< 0.5< 0.5< 0.5< 0.5< 0.5< 3.0< 10.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.02< 1.0< 4.0

826082708270826082608260827082708270826082708270827082708150808180818081827082708270826082608260826082708270827082708270826082608260826082608260826082708270826082608260826082608260808182708270

6878 S. STATE ROUTE 100 • MELMORE. OH 44845-9999


Customer Name: EA6ON & ASSOCIATES INCSample Description: A89-2


Compound

p- (Dimethylamino) azobenzene7 ,12 -Dlmethylbenz [a] anthracene3,3' -Dimethylbenzidine2,4 -Dime thy IphenolDimethyl phthalatem-Dlnitrobenzene4, 6-Dinitro-o-cresol2 , 4 -Dinl trophenol2,4 -Dlnitro toluene2, 6 -Dinitro tolueneDinosebDi-n-octyl phthalateDiphenylamineDisulfotonEndosulfan IEndosulfan IIEndosulfan SulfateEndrinEndrin aldehydeEthylbenzeneEthyl methacrylateEthyl methanesulfonateFamphurFlour an theneFlour eneHeptachlorHeptachlor epoxideHexachlorobenzeneHexachlorobu tadi eneHexachlorocyclopentadieneHexachl oroe thaneHexachloropropene2 -HexanoneIndeno (1,2,3- cd) pyreneIsobutyl alcoholIsodrinIsophoroneIsosafroleKeponeMethacryloni tri letfethapyrileneHethoxychlor3 -MethylcholanthreneSfethyl ethyl ketoneKethyl iodideSiethyl methacrylatetfethyl methanesulfonate

Concentration-

< 5.0< 5.0< 5.0< 3.0< 1.0< 5.0< 10.0< 10.0< 4.0< 4.0< 0.05

1.1< 4.0< 3.0< 0.03< 0.03< 0.03< 0.02< 0.10< 1.0< 5.0< 4.0< 10.0< 2.0< 3.0< 0.03< 0.03< 2.0< 3.0< 5.0< 3.0< 10.0< 10.0< 5.0< 500< 10.0< 1.0< 5.0< 0.10< 100< 5.0< 0.10< 4.0< 10.0< 10.0< 5.0< 4.0

Method

82708270827082708270827082708270827082708150827082708270808180818081808180818260826082708081827082708081808182708270827082708270826082708015827082708270808182608270808182708260826082608270

687SS STATE ROUTE 100 • MELMORE. OH 44845-9999


Customer Name: EAGON & ASSOCIATES INCSample Description: A89-2


Compound

2 -MethylnaphthaleneMethyl parathion4 -Methyl - 2 -pentanoneMethylene chlorideNaphthalene1,4 -Naphthoquinone1 -Haphthylamine2 -Naphthylamine2-Nitroaniline3 -Nitroaniline4-HitroanilineNitrobenzene2 -Hitrophenol4 -Hi trophenolN-Hitrosodi -n-butylamineN-NitrosodiethylamineN-NitrosodimethylamineN -Hi trosodiphenylamineH-Ni trosodipropylamineN-NitrosomethylethalamineN-HltrosopiperidineN-Nitrosopyrrolidine5 -Hi tro -o - toluidineParathionPentachlorobenzenePentachloroni trobenzenePentachloropheno 1PhenacetinPhenanthrenePhenolp - PhenylenediaminePhoratePronamidePropionitrilePyreneSafroleSilvexStyrene2,4,5-T

Concentration-

< 2.0< 3.0< 20.0< 1.0< 2.0< 5.0< 4.0< 4.0< 5.0< 5.0< 5.0< 2.0< 3.0< 10.0< 5.0< 5.0< 10.0< 2.0< 2.0< 5.0< 5.0< 4.0< 5.0< 3.0< 5.0< 10.0< 10.0< 5.0< 2.0< 3.0< 5.0< 3.0< 3.0< 50.0< 3.0< 5.0< 0.20< 1.0< 0.20

Method

827082708260826082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270826082708270815082608150



Customer Name: EA6ON & ASSOCIATES INCSample Description: A89-2



1,2, 4, 5-Tetrachlorobenzene1 , 1 , 1 , 2 - Te trachloroe thane1, 1, 2 , 2 -Te trachloroe thaneTe trachloroe thy 1 ene2 , 3 , 4 , 6 - Te trachlorophenolThionazinTolueneo-ToluidineToxaphene1,2, 4-Trichlorobenzene1, 1, 1-Trichloroe thane1,1,2 -Trichloroe thaneTrichloroethyleneTrichlorofluoromethane2,4, 5 -Trichlorophenol2,4, 6 -Trichlorophenol1,2,3 -Trichloropropaneo, o, o -Trie thy 1 phosphorothioatesym-TrinitrobenzeneVinyl AcetateVinyl ChlorideXylene (Total)

< 4.0< 1.0< 1.0< 1.0< 10.0< 4.0< 1.0< 5.0< 0.10< 2.0< 1.0< 1.0< 0.5< 1.0< 3.0< 3.0'< 1.0< 5.0< 10.0< 10.0< 1.0< 2.0

8270826082608260827080818260827080818270826082608260826082708270826082708270826082608260




Client: EA6ON & ASSOCIATES INCATBL Sample No.: 96-16816-MELDate Sampled: 11/25/96Date Received: 11/26/96Date Analyzed: 12/05/96Client ID: TRIP BLANK

Method: SW-846; 8260Sample Type: HATERPercent Solids:Analys t: SPH/JSMProject No.: TREMONT LANDFILL

APPENDIX I VOLATILES

Compound Concentration - ug/1 (ppb)

Acetone <Benzene <Bromochloromethane <Bromodichloromethane <Bromoform <Carbon Disulfide <Carbon Tetrachloride <Chlorobenzene <Chloroe thane <Chloroform <Dibromochloromethane <1,2 -Dibromo - 3 - chloropropane <1,2-Dibromoethane (EDB) <o-Dichlorobenzene <p-Dichlorobenzene <trano-l,4-Dichloro-2-Butene <1, 1-Dichloroet.hane <1,2-Dichloroethane <1,1-Dichloroethene <cis-1, 2 -Dichloroethene <brans - 1 , 2*- Dichloroethene <1,2 -Dichloropropane <3is-l,3-Dichloropropene <brans-1, 3 -Dichloropropene <Ethyl Benzene <2-Hexanone <Bromome thane <Zhlorome thane <Dibromome thane <fethylene Chloride «

: 5.0: 1.0: 1.0: 1.0: 1.0: 5.0: 1.0: 1.0: 1.0: 0.5: 1.0: 1.0: 1.0: 1.0: 1.0: 1.0: 0.5: 0.5: 0.5: 0.5: 0.5: 1.0: 1.0: 1.0: 1.0: 10.0: 1.0: 1.0: 1.0c 1.0

2-Butanone < 10.0lodome thane < 10.04-Methyl-2-Pentanone < 20.0Styrene < l . 01,1,1, 2 -Tetrachloroe thane < 1.01,1,2,2-Tetrachloroethane < 1.0Tetrachloroethene < 1.0Toluene < 1.01, 1, 1-Trichloroe thane < 1.01,1,2-Trichloroethane < 1.0Trichloroethene < 0.5Trichlorof luorome thane < 1.01,2,3- Trichloropropane < 1.0Vinyl Acetate < 10. 0Vinyl Chloride < 1.0Total Xylenes < 2.0

Surrogate Da tat % Recovery

Dibromof luorome thane 107 (70-115)Bromofluorobenzene 91 (86-115)Toluene -d8 91 (88-110)





Jlient: EAGON 6 ASSOCIATES INC•ate Sampled: 11/25/96iample Location: A89-3S


iethod Used Date Extracted Date Analyzed Analyst

W-846;

W-846;

W-846;

W-846;

W-846;

W-846;

Method

Method

Method

Method

Method

Method

8015

8081

8150

8240 (SIM)

8260

8270

N/A

11/26/96

12/02/96

N/A

N/A

11/27/96

12/03/96

12/11/96

12/07/96

11/27/96

12/06/96

12/09/96

DJS

CMR

DAW

JSM

JSM

KJP



Page 1 of 5

Customer Name: EA6ON & ASSOCIATES INCSample Description: A89-3S


Compound

AcenaphtheneAcenaph thy 1 eneAcetoneAcetonltrileAcetophenone2 -Acetylaminof loureneAcroleinAcrylonitrileAldrinAllyl chloride4 ~ AminoblphenylAnthraceneAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260BenzeneBenzo [a] anthraceneBenzo [b] f lour an then eBenzo Ik.} flourantheneBenzo [ghi] peryleneBenzo [a] pyreneBenzyl alcoholalpha-EECbeta-BHClelta-BHCjamma-BHC (Lindane)Bis (2 -chloroethoxy) methaneSis (2 -chloroethyl) etherBis (2 -chloro-1-methylethyl) etherSis (2 -ethylhexyl) phthalate3romochlor ome thane3romodi chl orome thane3romoformSromome thane1-Bromophenyl phenyl etherJutyl benzyl phthalateCarbon disulfideCarbon tetrachloride:hlordane> - Chloroani 1 ine

Concentration -

< 2.0< 2.0< 5.0< 500< 3.0< 5.0< 5.0< 5.0< 0.02< 20.0< 5.0< 2.0< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 1.0< 3.0< 4.0< 4.0< 5.0< 4.0< 5.0< 0.02< 0.02< 0.02< 0.02< 2.0< 2.0< 2.0

5.4< 1.0< 1.0< 1.0< 1.0< 3.0< 2.0< 5.0< 1.0< 0.10< 3.0

Method

8270827082608015827082708240 SIM8240 SIM808182608270827080818081808180818081808180818260827082708270827082708270808180818081808182708270827082708260826082608260827082708260826080818270



Customer Name: EAGON & ASSOCIATES INCSample Description: A89-3S



Chlorobenz eneChlorobenzilatep-Chloro-m-CresolChloroetnaneChloroformChloromethane2 -Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl etherChloropreneChrysenem-Cresolo-Cresolp-Cresol2,4-D4,4'-DDD4, 4' -DDE4, 4' -DOTDiallateDibenz [a, h] anthraceneDibenzofuranD ibromo chlorome thanel,2-Dibromo-3-chloropropane (DBCP)1,2-Dibromoethane (EDB)Dibromome thaneDi-n-butyl phthalate1,2 -Dichlorobenzene1, 3 -Dichlorobenzene1, 4 -Dichlorobenzene3,3' -Dichlorobenzidinetrans - 1 , 4 -Dichloro - 2 -buteneDichlorodif luorome thane1,1-Dichloroethane1,2 -Dichloroe thane1, 1-Dichloroethylenecis-1, 2 -Dichloroe thy 1 enetrans -1,2 -Dichloroethylene2 , 4 -Dichlorophenol2,6 -Dichlorophenol1,2 -Dichloropropane1,3 -Dichloropropane2 , 2 -Dichloropropane1, 1- Dichloropropenecis-1, 3 -Dichloropropenetrans- 1, 3 -DichloropropeneDleldrinDiethyl phthalateDimethoate

< 1.0< 4.0< 5.0< 1.0< 0.5< 1.0< 1.0< 5.0< 2.0

N.D.< 3.0< 3.0< 3.0< 3.0< 0.10< 0.02< 0.03< 0.03< 3.0< 5.0< 2.0< 1.0< 1.0< 1.0< 1.0< 1.0< 2.0< 2.0< 2.0< 15.0< 1.0< 1.0

6.1< 0.5< 0.5 .< 0.5< 0.5< 3.0< 10.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.02< 1.0< 4.0

826082708270826082608260827082708270826082708270827082708150808180818081827082708270826082608260826082708270827082708270826082608260826082608260826082708270826082608260826082608260808182708270


AQUA TECH ENVIRONMENTAL LABORATORIES, INC.APPEMDIX II ANALYSES



Compound

p- (Dime thy lamino) azobenzene7 , 12 -Dime thy Ibenz [a] anthracene3,3' -Dime thy Ibenz idine2,4 -Dime thy IphenolDimethyl phthalatem-Dinitrobenzene4, 6-Dinitro-o-cresol2,4 -Dini trophenol2,4 -Dlnitro toluene2, 6 - Dini tro tolueneDinosebDi-n-octyl phthalateDiphenylamineDisulfotonEndosulfan IEndosulfan IIEndosulfan SulfateEndarinEndrin aldehydeEthylbenzeneEthyl methacrylateEthyl methanesulfonateFamphurFlourantheneFlour eneEeptachlorSeptachlor epoxideBexachlorobenzeneSexachlorobu tadi enelexachlorocyclopen tadi eneiexachloroe thanelexachloropropeneI -HexanoneCndeno (1, 2 , 3 -cd) pyreneCsobutyl alcoholCsodrinCsophoroneCsosafroleCeponelethacrylonitrilele thapyr i 1 enelethoxychlort -Methylcholanthrenelethyl ethyl ketone[ethyl iodide[ethyl methacrylate[ethyl methanesulfonate

Concentration-

< 5.0< 5.0< 5.0< 3.0< 1.0< 5.0< 10.0< 10.0< 4.0< 4.0< 0.05

2.8< 4.0< 3.0< 0.03< 0.03< 0.03< 0.02< 0.10< 1.0< 5.0< 4.0< 10.0< 2.0< 3.0< 0.03< 0.03< 2.0< 3.0< 5.0< 3.0< 10.0< 10.0< 5.0< 500< 10.0< 1.0< 5.0< 0.10< 100< 5.0< 0.10< 4.0< 10.0< 10.0< 5.0< 4.0

Method

82708270827082708270827082708270827082708150827082708270808180818081808180818260826082708081827082708081808182708270827082708270826082708015827082708270808182608270808182708260826082608270





Compound

2 -MethylnaphthaleneMethyl par at hi on4 -Methyl - 2 -pen tanoneMe thy 1 en e chlorideNaphthalene1,4 -Naphthoquinone1 - Naph thy 1 amine2 -Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2 -Nitrophenol4 -NitrophenolN-Nitrosodi-n-butylamineN-NitrosodiethylamineN-Ni trosodimethyl amineN-NitrosodiphenylamineN-Ni trosodipropylamineN-NitrosomethylethalamineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroni trobenzenePentachlorophenolPhenacetinPhenanthrenePhenolp - Phenyl enedi aminePhoratePronamidePropionitrilePyreneSafroleSilvex -Styrene2,4, 5-T

Concentration-

< 2.0< 3.0< 20.0< 1.0< 2.0< 5.0< 4.0< 4.0< 5.0< 5.0< 5.0< 2.0< 3.0< 10.0< 5.0< 5.0< 10.0< 2.0< 2.0< 5.0< 5.0< 4.0< 5.0< 3.0< 5.0< 10.0< 10.0< 5.0< 2.0< 3.0< 5.0< 3.0< 3.0< 50.0< 3.0< 5.0< 0.20< 1.0< 0.20

Method

827082708260826082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270826082708270815082608150


AQUA TECH ENVIRONMENTAL LABORATORIES, INC,APPENDIX II ANALYSES

Customer Name: EAGON & ASSOCIATES INCSample Description: A89-3S ATELNO.: 96-16817-MEL

Page 5 of 5Compound

1, 2 , 4 , 5 -Tetrachlorobenzene1,1, 1,2 -Tetrachloroethane1,1,2,2 -TetrachloroethaneTetrachloroethylene2,3,4, 6 -TetrachlorophenolThionazinTolueneo-ToluidineToxaphene1,2,4-Trichlorobenzene1, 1, 1-Trichloroe thanelf lt 2 -Trichloroe thaneTrichloroethyleneTri chlorof luorome thane2,4,5 -Trichlorophenol2,4,6- Tr ichloropheno 11,2,3 -Trichloropropaneo, o, o -Trie thy 1 phosphorothioatesym- Tr ini trobenz eneVinyl AcetateVinyl ChlorideXylene (Total)

Concentration-

< 4.0< 1.0< 1.0< 1.0< 10.0< 4.0< 1.0< 5.0< 0.10< 2.0< 1.0< 1.0< 0.5< 1.0< 3.0< 3.0< 1.0< 5.0< 10.0< 10.0< 1.0< 2.0

Method00*70o^ / u826082608260827080818260827080818270826082608260826082708270826082708270826082608260






'lient: EAGON & ASSOCIATES INCate Sampled: 11/25/96ample Location: A89-3D


ethod Used Date Extracted Date Analyzed Analyst

W-846; Method 8015

W-846; Method 8081

W-846; Method 8150

W-846; Method 8240 (SIM)

9-846; Method 8260

7-846; Method 8270

N/A

11/26/96

12/02/96

N/A

N/A

11/27/96

12/03/96

12/11/96

12/07/96

11/27/96

12/06/96

12/09/96

DJS

CMR

DAW

JSM

JSM

KJP


AQUA TECH ENVIRONMENTAL IiABORATORIES, INC.APPENDIX II ANALYSES

Page 1 of 5

Customer Name: EA6ON & ASSOCIATESSample Description: A89-3D

INC ATELNo.: 96-16818-MEL

Compound

AcenaphtheneAcenaph thy 1 eneAcetoneAcetonitrileAcetophenone2 -Acetylaminof loureneAcroleinAcrylonitrileAldrlnAllyl chloride4 - AminobiphenylAnthraceneAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260BenzeneBenzo [a] anthraceneBenzo [b] f lourantheneBenzo [k] f lourantheneBenzo [ghl] peryleneBenzo [a] pyreneBenzyl alcoholalpha -BHCbeta-BHCdelta-BBCgaiaoa-BHC (Lindane)B i 0 ( 2 - chloroe thoxy ) me thaneBio (2- chloroe thyl) etherBis (2-chloro-l-methylethyl) ether310 (2-ethylhexyl)phthalate3romochlorome thaneBromodichlorome thane3romoformJromome thanel-Bromophenyl phenyl etherJutyl benzyl phthalateCarbon disulfide!arbon tetrachloride!hlordane>-Chloroaniline

Concentration-

< 2.0< 2.0< 5.0< 500< 3.0< 5.0< 5.0< 5.0< 0.02< 20.0< 5.0< 2.0< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 1.0< 3.0< 4.0< 4.0< 5.0< 4.0< 5.0< 0.02< 0.02< 0.02< 0.02< 2.0< 2.0< 2.0< 2.0< 1.0< 1.0< 1.0< 1.0< 3.0< 2.0< 5.0< 1.0< 0.10< 3.0

Method

8270827082608015827082708240 SIM8240 SIM808182608270827080818081808180818081808180818260827082708270827082708270808180818081808182708270827082708260826082608260827082708260826080818270



Customer Name: EAGON & ASSOCIATES INCSample Description: A89-3D


Compound Concentration- ug/1 (ppb) Method

ChlorobenzeneChlorobenzilatep-Chloro-m-CresolChloroe thaneChloroformChlorome thane2 -Chloronaphthalene2 -Chlorophenol4-Chlorophenyl phenyl etherChloropreneChrysenem-Cresolo-Cresolp-Cresol2,4-D4,4'-DDD4,4' -DDE4, 4' -DOTDiallateDibenz [a, h] anthracene3ibenzo f uranDibromochlorome thane1,2 -Dibromo - 3 - chloropropane (DBCP)L, 2-Dibromoethane (EDB)Dibromome thaneDi-n-butyl phthalateL, 2 -DichlorobenzeneL, 3 -DichlorobenzeneL, 4 -Dichlorobenzene1,3' -Dichlorobenzidine:rans-l, 4 -Dichloro-2 -butene) ichlor odi f luorome thaneL, 1-Dichloroe thaneL, 2 -Dichloroe thaneL, 1-Dichloroe thylene:is -1,2 -Dichloroethylene:rans-l, 2 -Dichloroethylene! , 4 -Dichlorophenol! , 6 -Dichlorophenol., 2 -Dichloropropane., 3 -Dichloropropane: , 2 -Dichloropropane., 1-Dichloropropene!±0-l, 3 -Dichloropropene:rans-l, 3 -Dichloropropenetieldrinilethyl phthalate•imethoate

< 1.0< 4.0< 5.0< 1.0< 0.5< 1.0< 1.0< 5.0< 2.0

N.D.< 3.0< 3.0< 3.0< 3.0< 0.10< 0.02< 0.03< 0.03< 3.0< 5.0< 2.0< 1.0< 1.0< 1.0< 1.0< 1.0< 2.0< 2.0< 2.0< 15.0< 1.0< 1.0< 0.5< 0.5< 0.5< 0.5< 0.5< 3.0< 10.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.02< 1.0< 4.0

826082708270826082608260827082708270826082708270827082708150808180818081827082708270826082608260826082708270827082708270826082608260826082608260826082708270826082608260826082608260808182708270

6878 S STATE ROUTE 100 • MELMORE OH 44845 9999


Customer Name: EA6ON & ASSOCIATES INCSample Description: A89-3D


Compound

p- (Dimethylamino) azobenzene7 ,12 -Dlmethylbenz [a] anthracene3,3' -Dlmethylbenzldlne2,4 -DimethylphenolDimethyl phthalatem-Dini trobenzene4, 6-Dinitro-o-cresol2,4 -Dini trophenol2, 4 -Dinitro toluene2, 6 -Dini tro tolueneDinosebDi-n-octyl phthalateDiphenylamlneDisul£otonEndosulfan IEndosulfan IIBndosul£an SulfateEndrinEndrin aldehydeEthylbenzeneEthyl methacrylateEthyl methanesulfonateFamphurFlour an theneFlour eneHeptachlorHeptachlor epoxideEexachlorobenzeneHexachlorobu tadi eneHexachlorocyclopentadieneHexachloroethaneHexachloropropene2 -HftxnnonflIndeno(l,2,3-cd)pyreneIsobutyl alcoholIsodrinIsophoroneJsosafroleKeponeMethacrylonitrileMe t hapyr i 1 eneMethoxychlor3 -MethylcholanthreneMethyl ethyl JcetoneMethyl iodideMethyl methacrylateMethyl methanesulfonate

Concentration -

< 5.0< 5.0< 5.0< 3.0< 1.0< 5.0< 10.0< 10.0< 4.0< 4.0< 0.05< 1.0< 4.0< 3.0< 0.03< 0.03< 0.03< 0.02< 0.10< 1.0< 5.0< 4.0< 10.0< 2.0< 3.0< 0.03< 0.03< 2.0< 3.0< 5.0< 3.0< 10.0< 10.0< 5.0< 500< 10.0< 1.0< 5.0< 0.10< 100< 5.0< 0.10< 4.0< 10.0< 10.0< 5.0< 4.0

Method

82708270827082708270827082708270827082708150827082708270808180818081808180818260826082708081827082708081808182708270827082708270826082708015827082708270808182608270808182708260826082608270



Customer Name: EAGON & ASSOCIATES INCSample Description: A89-3D


Compound

2 -MethylnaphthaleneMethyl parathion4-Methyl-2-pentanoneMe thy 1 en e chlorideNaphthalene1,4 -Naphthoquinone1 -Naphthylamine2 -Naphthylamine2-Nitroaniline3-Nitroanilinei-NitroanilineNitrobenzene2 -Nitrophenoli-Nitrophenol7-Nitrosodi -n-butylamlneJ-Nitrosodiethylaminel-Nitrosodimethylaminef-NitrosodiphenylamlneJ-NitrosodipropylamineJ-NitrosomethylethalamineT-NitrosopiperidineI-Nitrosopyrrolidine5-Nitro-o-toluidine'arathion'entachlorobenzene•entachloronitrobenzene"entachlor opheno 1'henacetin'henanthrene'henol» - Phenylenediamine•horate'ronamide•ropionitrile•yreneiafroleHlvex:tyrene,4,5-T

Concentration-

< 2.0< 3.0< 20.0< 1.0< 2.0< 5.0< 4.0< 4.0< 5.0< 5.0< 5.0< 2.0< 3.0< 10.0< 5.0< 5.0< 10.0< 2.0< 2.0< 5.0< 5.0< 4.0< 5.0< 3.0< 5.0< 10. 0< 10.0< 5.0< 2.0< 3.0< 5.0< 3.0< 3.0< 50.0< 3.0< 5.0< 0.20< 1.0< 0.20

Method

8270827082608260827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708260 .82708270815082608150



Customer Name: EA6ON & ASSOCIATES INCSample Description: A89-3D


Compound Concentration- Method1,2,4,5-Tetrachlorobenzene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroethylene2,3,4,6-TetrachlorophenolThionazinTolueneo-ToluidineToxaphene1,2,4-Trichlorobenzene1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroethyleneTrichlorofluoromethane2.4.5-Trichlorophenol2.4.6-Trichlorophenol1,2,3-Trichloropropaneo, 0,0-Trie thy 1 phosphorothioatesyn-TrinitrobenzeneVinyl AcetateVinyl ChlorideXylene (Total)

411110.04.01.05.00.102.01.01.00.51.03.03.01.05.010.010.01.02.0

8270826082608260827080818260827080818270826082608260826082708270826082708270826082608260




Client: EA6ONATEL Sample No.Date Sampled:Date Received:Date Analyzed:

& ASSOCIATES INC: 96-16819-MEL11/25/9611/26/9612/05/96

Method: SW-846; 8260Sample Type: WATERPercent Solids:Analyst: SPH/JSMProject No.: TREMONT LANDFILL

Client ID: TRIP BLANK



1,5.1.1.

,0,000

1.00.51.01.01.0

,0.0

1,1.

Acetone < 5.0Benzene < 1.0Bromochloromethane < 1.0Bromodichloromethane < 1.0Bromoform <Carbon Disulfide <Carbon Tetrachloride <Chlorobenzene <Chloroethane <Chloroform <Dibromochloromethane <1,2-Dibromo-3 -chloropropane <1,2-Dibromoethane (EDB) ' <o-Dichlorobenzene <p-Dichlorobenzene <trans-l,4-Dichloro-2-Butene < 1.0J.,1-Dichloroe thane < 0.51,2-Dichloroethane < 0.51.1-Dichloroethene < 0.5cis-1,2-Dichloroethene < 0.5trans-1,2-Dichloroethene < 0.51.2-Dichloropropane < 1.0cis-l,3-Dichloropropene < 1.0trans-1,3-Dichloropropene < 1.0Ethyl Benzene < 1.02-Hexanone < 10.0Bromome thane < 1.0Chloromethane < 1.0Dibromomethane < 1.0Methylene Chloride < 1.0

2-Butanone < 10.0lodomethane < 10.04-Methyl-2-Pentanone < 20.0Styrene < i.o1,1,1,2-Tetrachloroethane < l.o1,1,2,2-Tetrachloroethane < 1.0Tetrachloroethene < l.oToluene < l.o1.1.1-Trichloroethane < l.o1.1.2-Trichloroethane < l.oTrichloroethene < o.5Trichlorofluor omethane < l.o1,2,3-Trichloropropane < l.oVinyl Acetate < 10.0Vinyl Chloride < l.oTotal Xylenes < 2.0

Surrogate Data:

DibromofluoromethaneBromofluorobenzeneToluene-d8

% Recovery

96 (70-115)88 (86-115)96 (88-110)





lients EAGON & ASSOCIATES INCate Sampled: 11/25/96ample Locations A91-4S


ethod Used Date Extracted Date Analyzed Analyst

W-846; Method 8015

W-846; Method 8081

W-846; Method 8150

tf-846; Method 8240 (SIM)

W-846; Method 8260

tf-846; Method 8270

N/A

11/26/96

12/02/96

N/A

N/A

11/27/96

12/03/96

12/11/96

12/07/96

11/27/96

12/06/96

12/10/96

DJS

CMR

DAW

JSM

JSM

KJP



Page 1 of 5



Compound

AcenaphtheneAcenaphthyleneAcetoneAcetonitrileAcetophenone2 -Acetylaminof loureneAero le inAcryloni tr i 1 eAldrinAllyl chloride4 -AminobiphenylAnthraceneAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260BenzeneBenzo [a] anthraceneBenzo [b] flourantheneBenzo [k] flourantheneBenzo [ghi] peryleneBenzo [a] pyreneBenzyl alcoholalpha -BHCbeta-BHCdelta -BHCgamma -BHC (Lindane)Bis (2 - chloroethoxy) methaneBis (2 -chloroethyl) etherBis (2-chloro-l-methylethyl) etherBis (2 - ethylhexyl) phthalateBromochlorome thaneBromodi chlor ome thaneBromoformBromome thane4-Bromophenyl phenyl etherButyl benzyl phthalateCarbon disulfideCarbon tetrachlorideChlordanep-Chloroaniline

Cone en t r a t i on -

< 2.0< 2.0< 5.0< 500< 3.0< 5.0< 5.0< 5.0< 0.02< 20.0< 5.0< 2.0< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 1.0< 3.0< 4.0< 4.0< 5.0< 4.0< 5.0< 0.02< 0.02< 0.02< 0.02< 2.0< 2.0< 2.0< 2.0< 1.0< 1.0< 1.0< 1.0< 3.0< 2.0< 5.0< 1.0< 0.10< 3.0

Method

8270'827082608015827082708240 SIM8240 SIM808182608270827080818081808180818081808180818260827082708270827082708270808180818081808182708270827082708260826082608260827082708260826080818270






Chlorobenz eneChlorobenzilatep - Chloro -m- CresolChloroe thaneChloroformChlor ome thane2 -Chloronaphthalene2 -Chlorophenol4-Chlorophenyl phenyl etherChloropreneChrysenem-Cresolo- Cresolp- Cresol2,4-D4,4'-DDD4, 4' -DDE4, 4 '-DOTDial lateDibenz [a, h] anthraceneDibenzofuranD ibromochlor ome than el,2-Dibromo-3-chloropropane (DBCP)1,2-Dibromoethane (EDB)Dibromome thaneDi-n -butyl phthalate1, 2 -Dichlorobenzene1,3 -Dichlorobenzene1, 4 -Dichlorobenzene3,3' -Dichlorobenzidinetrans-1, 4 -Dichloro-2 -buteneDichlorodi f luorome thane1, 1-Dichloroe thane1,2 -Dichloroe thane1, 1 -Dichloroethylenecis-1, 2 -Dichloroethylenetrans-1, 2 -Dichloroethylene2,4 -Di Chlorophenol2, 6-Dichlorophenol1, 2 -Dichloropropane1,3 -Dichloropropane2,2 -Dichloropropane1, 1- Dichloropropenecis -1,3 -Dichloropropenetrans-1, 3 -DichloropropeneDieldrinDiethyl phthalateDimethoate

< 1.0< 4.0< 5.0< 1.0< 0.5< 1.0< 1.0< 5.0< 2.0

N.D.< 3.0< 3.0< 3.0< 3.0< 0.10< 0.02< 0.03< 0.03< 3.0< 5.0< 2.0< 1.0< 1.0< 1.0< 1.0< 1.0< 2.0< 2.0< 2.0< 15.0< 1.0< 1.0< 0.5< 0.5< 0.5< 0.5< 0.5< 3.0< 10.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.02< 1.0< 4.0

826082708270826082608260827082708270826082706270827082708150808180818081827082708270826082608260826082708270827082708270826082608260826082608260826082708270826082608260826082608260808182708270



Customer Name: EAGON & ASSOCIATES INCSample Description: A91-4S ATELNo.: 96-16820-MEL

Page 3 of 5Compound

p- (Dime thy lamino) azobenzene7 , 12 -Dime thy Ibenz [a] anthracene3,3' -Dime thy Ibenz idine2,4 -Dime thy IphenolDimethyl phthalatem-Dinitrobenzene4, 6-Dinitro-o-cresol2,4 -Dini trophenol2,4-Dinitrotoluene2, 6 -Dini tro tolueneDinosebDi-n-octyl phthalateDiphenylamineDisulfotonEndosulfan IEndosulfan IIEndosulfan SulfateEndrinBndrin aldehydeEthylbenzeneEthyl methacrylateEthyl methanesulfonateFamphurPI ouran theneFlour eneHeptachlorEeptachlor epoxideEexachlorobenz eneSexachlor obu tadi eneSexachlorocyclopentadieneHexachloroethane3exachloropropene2 -HexanoneCndeno (1,2,3- cd) pyreneCsobutyl alcoholCsodrinCsophoroneCsosafroleCeponeiethacrylonitrilefe t hapyr i 1 enelethoxychlor) -Methylcholanthrene1 ethyl ethyl ketonefethyl iodidefethyl methacrylate(ethyl methanesulfonate

Concentration-

< 5.0< 5.0< 5.0< 3.0< 1.0< 5.0< 10.0< 10.0< 4.0< 4.0< 0.05< 1.0< 4.0< 3.0< 0.03< 0.03< 0.03< 0.02< 0.10< 1.0< 5.0< 4.0< 10.0< 2.0< 3.0< 0.03< 0.03< 2.0< 3.0< 5.0< 3.0< 10.0< 10.0< 5.0< 500< 10.0< 1.0< 5.0< 0.10< 100< 5.0< 0.10< 4.0< 10.0< 10.0< 5.0< 4.0

Method

QO*7 f\04. 1 UPOTnO<c / U82708270827082708270827082708270815082708270827080818081808180818081826082608270808182708270808180818270827082708270OO-TAO& 1 \J

826082708015827082708270808182608270808182708260826082608270





Compound

2 -MethylnaphthaleneMethyl parathion4 -Methyl - 2 -pentanoneMethyl en e chlorideNaphthalene1,4 -Naphthoquinone1 -Naphthylamine2 -Naphthylamine2-Nitroaniline3-Nitroaniline4 -NitroanilineNitrobenzene2 -Nitrophenol4 -NitrophenolN-Ni trosodi -n-butylamineN-Ni trosodie thylamineN-NitrosodimethylamineN-NitrosodiphenylamineN-NitrosodipropylamineN-NitrosomethylethalamlneN-NitrosopiperidineN-Ni trosopyrrol idine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloronitrobenzenePentachlorophenolPhenacetinPhenan thr enePhenolp - PhenylenediaminePhoratePronamidePropionitrilePyreneSafroleSilvexStyrene2,4, 5-T

Concentration-

< 2.0< 3.0< 20.0< 1.0< 2.0< 5.0< 4.0< 4.0< 5.0< 5.0< 5.0< 2.0< 3.0< 10.0< 5.0< 5.0< 10,0< 2.0< 2.0< 5.0< 5.0< 4.0< 5.0< 3.0< 5.0< 10.0< 10.0< 5.0< 2.0< 3.0< 5.0< 3.0< 3.0< 50.0< 3.0< 5.0< 0.20< 1.0< 0.20

Method

827082708260826082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270826082708270815082608150





Compound Concentration - Method

1,2,4, 5-Tetrachlorobenzene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroethylene2,3,4,6-TetrachlorophenolThionazinTolueneo-ToluidineToxaphene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1#1,2-TrichloroethaneTrichloroethyleneTrichlorofluoromethane2.4.5-Trichlorophenol2.4.6-Trichlorophenol1,2,3-Trichloropropane0,0,0-Triethyl phosphorothioatesym-TrinitrobenzeneVinyl AcetateVinyl ChlorideXylene (Total)

4111

10.04.01.05.0

0.102.01.1.00

0.51.03.03.01.05.0

10.010.01.02.0

8270826082608260827080818260827080818270826082608260826082708270826082708270826082608260

All units of concentration are ug/L (ppb).





lientt EAGON & ASSOCIATES INCate Sampled: 11/25/96ample Location: A91-7S

ATEL Sample No.: 96-16821-MBLDate Received: 11/26/96

athod Used Date Extracted Date Analyzed Analyst

7-846; Method 8015

7-846; Method 8081

7-846; Method 8150

7-846; Method 8240 (SIM)

T-846; Method 8260

r-846; Method 8270

N/A

11/26/96

12/02/96

N/A

N/A

11/27/96

12/03/96

12/11/96

12/07/96

11/27/96

12/06/96

12/10/96

DJS

CMR

DAW

JSH

JSM

KJP



Page 1 of 5

Customer Name: EAGON & ASSOCIATESSample Description: A91-7S

INC ATEL No.: 96-16821-MEL

Compound

AcenaphtheneAcenaph thyl eneAcetoneAcetonitrileAce tophenone2 -Acetylaminof loureneAcroleinAcrylonitrileAldrinAllyl chloride4 -AminobiphenylAnthraceneAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260BenzeneBenzo [a] anthraceneBenzo [b] f lour ant hen eBenzo [k] f lourantheneBenzo [ghi] peryleneBenzo [a] pyreneBenzyl alcoholalpha -BHCbeta-BHCdelta -BHCgamma -BHC (Lindane)Bis (2 - chloroethoxy) methaneBis (2-chloroethyl) etherBis (2-chloro-l-methylethyl) etherBis (2 -ethylhexyl) phthalateBromochloroxne thaneBromodichlorome thaneBromoformBromome thane4-Bromophenyl phenyl etherButyl benzyl phthalateCarbon disulfideCarbon tetrachlorideChlordanep-Chloroaniline

Concentration-

< 2.0< 2.0< 5.0< 500< 3.0< 5.0< 5.0< 5.0< 0.02< 20.0< 5.0< 2.0< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10

1.9< 3.0< 4.0< 4.0< 5.0< 4.0< 5.0< 0.02< 0.02< 0.02< 0.02< 2.0 •< 2.0< 2.0< 2.0< 1.0< 1.0< 1.0< 1.0< 3.0< 2.0< 5.0< 1.0< 0.10< 3.0

Method

8270827082608015827082708240 SIM8240 SIM808182608270827080818081808180818081808180818260827082708270827082708270808180818081808182708270827082708260826082608260827082708260826080818270






ChlorobenzeneChlorobenzilatep-Chloro-m-CresolChloroethaneChloroformChlorome thane2 -Chloronaphthalene2 -Chlorophenol4-Chlorophenyl phenyl etherChloropreneChrysenem-Cresolo-Cresolp-Cresol2,4-D4, 4 '-ODD4, 4' -DDE4, 4' -DOTDiallateDibenz [a, h] anthraceneDibenzofuranDibromochlorome thanel,2-Dibromo-3-chloropropane (DBCP)1,2-Dibromoethane (EDB)Dibromome thaneDi-n-butyl phthalate1, 2 -Dichlorobenzene1,3 -Dichlorobenzene1, 4 -Dichlorobenzene3,3' -Dichlorobenzidinetrans -1,4 -Dichloro -2 -buteneDichlorodi f luorome thane1, 1 -Dichloroe thane1, 2 -Dichloroe thane1, 1-Dichloroethylenecis-1, 2 -Dichloroe thylenetrans - 1 , 2 -Dichloroe thylene2,4 -Dichlorophenol2 , 6 -Dichlorophenol1, 2 -Dichloropropane1, 3 -Dichloropropane2,2 -Dichloropropane1, 1- Dichloropropenecis-1, 3 -Dichloropropenetrans- 1, 3 -DichloropropeneDieldrinDie thy 1 phthalateDimethoate

< 1.0< 4.0< 5.0< 1.0< 0.5< 1.0< 1.0< 5.0< 2.0

N.D.< 3.0< 3.0< 3.0< 3.0< 0.10< 0.02< 0.03< 0.03< 3.0< 5.0< 2.0< 1.0< 1.0< 1.0< 1.0< 1.0< 2.0< 2.0< 2.0< 15.0< 1.0< 1.0< 0.5< 0.5< 0.5< 0.5< 0.5< 3.0< 10.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.02< 1.0< 4.0

826082708270826082608260827082708270826082708270827082708150808180818081827082708270826082608260826082708270827082708270826082608260826082608260826082708270826082608260826082608260808182708270


AQUA TECH ENVIRONMENTAL LABORATORIES, INCAPPEMDIX II ANALYSES

Customer Name: EAGON & ASSOCIATES INCSample Description: A91-7S ATELNo.: 96-16821-MEL

Page 3 of 5Compound

p- (Dimethylamino) azobenzene7 , 12 -Dime thy Ibenz [a] anthracene3,3' -Dime thy Ibenz idine2,4 -Dime thy IphenolDimethyl phthalatem-Dinitrobenzene4, 6-Dinitro-o-cresol2,4 -Dini trophenol2,4 -Dini tro toluene2, 6 -Dini tro tolueneDinosebDi-n-octyl phthalateDiphenylamineDisulfotonEndosulfan IEndosulfan IIEndosulfan SulfateEndrinEndrin aldehydeE thy Ib enz eneEthyl methacrylateEthyl methanesulfonateFamphurFlour an theneFlour eneHeptachlorEeptachlor epoxideBexachlorobenzeneBexachlorobutadieneBexachlorocyclopentadieneSexachloroe thaneBexachloropropene2-HexanoneEndeno (1,2,3-cd) pyr eneIsobutyl alcoholCsodrin „CsophoroneCsosafroleteponedethacrylonitrilefe thapyr i 1 eneiethoxychlor) -Methylcholanthrenetethyl ethyl ketonefethyl iodidelethyl methacrylate(ethyl methanesulfonate

Concentration-

< 5.0< 5.0< 5.0< 3.0< 1.0< 5.0< 10.0< 10.0< 4.0< 4.0< 0.05< 1.0< 4.0< 3.0< 0.03< 0.03< 0.03< 0.02< 0.10< 1.0< 5.0< 4.0< 10.0< 2.0< 3.0< 0.03< 0.03< 2.0< 3.0< 5.0< 3.0< 10.0< 10.0< 5.0< 500< 10.0< 1.0< 5.0< 0.10< 100< 5.0< 0.10< 4.0< 10.0< 10.0< 5.0< 4.0

Method

00*7 f\Q4 1 U011 r\Of, 1 UPOT AOf: /U

POT f\Of\ 1 U8270POT Aof\ i uPOT AOf\ 1 UOO*7 AOf\ /UPOT rtOf, 1 UOO*7 AOf\ 1 U8150ooTnOf\ / UOO7AOJt /UOOTrto* / uOAO1OUOXQ AO1OUOX8081DAO1OUOXonpiOUOJ.OOCAOÔUOOCAOf\ OUHOT AQ4 1 UO AO1OUOXa*jt AOf\ 1 U00*7 AO£ 1 UAOfllOUOJ.OAfllOUO J.POT AOf\ 1 UPOTAOf, 1 U827082708270oo enOf\o\JPOT AOf] 1 U8015POTAof, 1 U82708270ftfifllou OX

8260po»7Aof, 1 UPAP1OUOX

82708260826082608270





Compound

2 -MethylnaphthaleneMethyl par at hi on4 -Methyl - 2 -pentanoneMethylene chlorideNaphthalene1,4 -Naphthoquinone1 -Naphthylamine2 -Naphthylamine2 -Nitroaniline3 -Nitroaniline4 - Hi troani 1 ineNitrobenzene2 -Nitrophenol4 -NitrophenolN-Nitrosodi-n-butylamineN-NitrosodiethylamineN-NitrosodimethylamineN -Ni trosodiphenylamineN-Ni trosodipropy lamineN-NitrosomethylethalamineN-NitrosopiperidineN-Ni trosopyrrol idine5-Nitro-o-toluidineParathionPentachlorobenz enePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolp - PhenylenediaminePhoratePronamideProp ioni t r i 1 ePyrene3afroleSilvexStyrene2,4, 5-T

Concentration-

< 2.0< 3.0< 20.0< 1.0< 2.0< 5.0< 4.0< 4.0< 5.0< 5.0< 5.0< 2.0< 3.0< 10.0< 5.0< 5.0< 10.0< 2.0< 2.0< 5.0< 5.0< 4.0< 5.0< 3.0< 5.0< 10.0< 10.0< 5.0< 2.0< 3.0< 5.0< 3.0< 3.0< 50.0< 3.0< 5.0< 0.20< 1.0< 0.20

Method

827082708260826082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270826082708270815082608150






1,2,4,5-Tetrachlorobenzene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetby1ene2,3,4,6-TetrachlorophenolThionazinTolueneo-ToluidineToxaphene1,2,4-Trichlorobenzene1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroethyleneTrichlorofluoromethane2.4.5-Trichlorophenol2.4.6-Trichlorophenol1,2,3-Trichloropropaneo,o,o-Triethyl phosphorothioatesym-TrinitrobenzeneVinyl AcetateVinyl ChlorideXylene (Total)

411110.04.01.05.00.102.01.01.00.51.3.3.1.5.10.010.01.02.0

,0.0000

8270826082608260827080818260827080818270826082608260826082708270826082708270826082608260


68/8 S STATE ROUTE 100 • MELMORE. OH 448-15 9999


Client: EAGON & ASSOCIATES INCATBL Sample No.: 96-16822-MELDate Sampled: 11/25/96Date Received: 11/26/96Date Analyzed: 12/05/96Client ID: TRIP BLANK

Method: SW-846; 8260Sample Type: MATERPercent Solids:Analys t: SPH/JSMProject No.: TREMONT LANDFILL



5.1.1.

Acetone <Benzene <Bromochloromethane <Bromodichloromethane <Bromoform <Carbon Disulfide <Carbon Tetrachloride <Chlorobenzene <Chloroethane <Chloroform <Dibromochloromethane <l,2-Dibromo-3-chloropropane <L,2-Dibromoethane (EDB) <3-Dichlorobenzene <p-Dichlorobenzene <trans-1,4-Dichloro-2-Butene <L,1-Dichloroethane <L,2-Dichloroethane <L,1-Dichloroethene <2is-l,2-Dichloroethene <-rans -1, 2*- Di chloroe thene <L,2-Dlchloropropane <:is-l,3-Dichloropropene <;rans-l,3-Dichloropropene <Sthyl Benzene <!-Hexanone < 10.0Jromome thane < 1.0!hlorome thane < 1.0>ibromomethane < 1.0lethylene Chloride < 1.0

000

1.01.05.01.01.01.00.51.000000

0.50.50.50.50.50000

1.1.1.1.1.

1.1.1.1.

2-Butanone <lodonethane <4-Methyl-2-Pentanone <Styrene <1,1,1,2-Tetrachloroethane <1,1,2,2-Tetrachloroethane <Tetrachloroethene <Toluene <1.1.1-Trichloroethane <1.1.2-Trichloroethane <Trichloroethene <Trichlorofluoromethane <1,2,3-Trichloropropane <Vinyl Acetate <Vinyl Chloride <Total Xylenes <

10.010.020.01.1,1,1.

1,1.

,0.0,0,0

1.1.1.0.5

10.01.02.0

Surrogate Data:

DibromofluoromethaneBromofluorobenz eneToluene-d8

% Recovery

999794

(70-115)(86-115)(88-110)





:iienti EAGON & ASSOCIATES INC>ate Sampled: 11/25/96Eanple Location: 96-300


[ethod Used Date Extracted Date Analyzed Analyst

W-846; Method 8015

W-846; Method 8081

W-846; Method 8150

W-846; Method 8240 (SIM)

W-846; Method 8260

W-846; Method 8270

N/A

11/26/96

12/02/96

N/A

N/A

11/27/96

12/03/96

12/11/96

12/07/96

11/27/96

12/06/96

12/10/96

DJS

CMR

DAW

JSM

JSM

KJP



Page 1 of 5

Customer Name: EA6ON & ASSOCIATES INCSample Description: 96-300


Compound

AcenaphtheneAcenaph thy 1 eneAcetoneAcetonitrileAcetophenone2 -Acetylaminof loureneAcroleinAery loni tr i leAldrinAllyl chloride4 - AminobiphenylAnthraceneAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260BenzeneBenzo [a] anthraceneBenzo [b] £lourantheneBenzo [k] flourantheneBenzo [ghi] peryleneBenzo [a] pyreneBenzyl alcoholalpha -BHCbeta-BHCdelta -BHCgamma -BHC (Lindane)Bis (2 - chloroethoacy) methaneBis (2-chloroethyl) etherBis (2-chloro-l-methylethyl) etherBis (2 -ethylhexyl) phthalateBromochlorome thaneBr omodi chlor ome thaneBromoformBromome thane4-Bromophenyl phenyl etherButyl benzyl phthalateCarbon disulfideCarbon tetrachlorideChlordanep-Chloroaniline

Concentration-

< 2.0< 2.0< 5.0< 500< 3.0< 5.0< 5.0< 5.0< 0.02< 20.0< 5.0< 2.0< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10

4.2< 3.0< 4.0< 4.0< 5.0< 4.0< 5.0< 0.02< 0.02< 0.02< 0.02< 2.0< 2.0< 2.0< 2.0< 1.0< 1.0< 1.0< 1.0< 3.0< 2.0< 5.0< 1.0< 0.10< 3.0

Method

8270827082608015827082708240 SIM8240 SIM808182608270827080818081808180818081808180818260827082708270827082708270808180818081808182708270827082708260826082608260827082708260826080818270



Customer Name: EAGON & ASSOCIATES INCSample Description: 96-300


Compound

ChlorobenzeneChlorobenzilatep-Chloro-m-CresolChloroe thaneChloroformChlorome thane2 -Chloronaphthalene2 - Chlorophenol4-Chlorophenyl phenyl etherChloropreneChrysenem-Cresolo-Cresolp-Cresol2,4-D4,4'-DDD4, 4' -DDE4,4'-DDTDiallateDibenz [a,h] anthraceneDibenzofuranDibromo chlorome thane1,2 -Dibromo - 3 - chloropropane (DBCP)1,2-Dibromoethane (EDB)Dibromome thaneDi-n-butyl phthalate1,2 -Dichlorobenzene1,3 -Dichlorobenzene1, 4 -Dichlorobenzene3,3' -Dichlorobenzidinetrans- 1, 4 -Dichloro- 2 -buteneDichlorodi f luorome thane1, 1-Dichloroe thane1, 2-Dichloroethane1, 1-Dichloroe thylenecis-1, 2 -Dichloroethylenetrans - 1 , 2 -Dichloroethylene2,4 -Dichlorophenol2, 6 -Dichlorophenol1,2 -Dichloropropane1,3 -Dichloropropane2,2 -Dichloropropane1, 1 -Dichloropropenecis-1, 3 -Dichloropropenetrans -1, 3 -DichloropropeneDieldrinDiethyl phthalateDimethoate

Concentration-ug/1 (ppb) Method

27.7< 4.0< 5.0< 1.0< 0.5< 1.0< 1.0< 5.0< 2.0

N.D.< 3.0< 3.0< 3.0< 3.0< 0.10< 0.02< 0.03< 0.03< 3.0< 5.0< 2.0< 1.0< 1.0< 1.0< 1.0< 1.0

4.2< 2.0< 2.0< 15.0< 1.0< 1.0< 0.5< 0.5< 0.5< 0.5< 0.5< 3.0< 10.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.02< 1.0< 4.0

82608270827082608260826082708270827082608270827082708270815080818081808182708270827082608260826082608270827082708270827082608260826082608260 -8260826082708270826082608260826082608260808182708270




ATEL No. 96-16823-MELPage 3 of 5

Compound

p- (Dimethylamino) azobenzene7 , 12 -Dime thy Ibenz [a] anthracene3,3' -Dime thy Ibenz idine2 , 4 -Dime thy IphenolDimethyl phthalatem-Dini trobenzene4, 6-Dinitro-o-cresol2 , 4 -Dini trophenol2,4-Dinitrotoluene2, 6 -Dini tro tolueneDinosebDl-n-octyl phthalateDiphenylamineDisnlfotonEndosulfan IEndosulfan IIEndosulfan SulfateEndrinEndrin aldehydeE thy Ibenz eneEthyl methacrylateEthyl methanesulfonateFamphurFlour an theneFloureneHeptachlorHeptachlor epoxideHexachlorobenzeneHexachlorobutadieneHc3nichloroCrycloip¥>ntwdl f*nf*Hexachloroe thaneHexachloropropene2-EexanoneIndeno (1,2, 3 -cd) pyreneIsobutyl alcoholIsodrinIsophoroneIsosafroleKeponeMethacrylonitrileMe thapyr i leneHe thoxychl or3 -MethylcholanthreneMethyl ethyl ketoneMethyl iodideMethyl methacrylateMethyl methanesulfonate

Concentration -

< 5.0< 5.0< 5.0< 3.0< 1.0< 5.0< 10.0< 10.0< 4.0< 4.0< 0.05< 1.0< 4.0< 3.0< 0.03< 0.03< 0.03< 0.02< 0.10< 1.0< 5.0< 4.0< 10.0< 2.0< 3.0< 0.03< 0.03< 2.0< 3.0< 5.0< 3.0< 10.0< 10.0< 5.0< 500< 10.0< 1.0< 5.0< 0.10< 100< 5.0< 0.10< 4.0< 10.0< 10.0< 5.0< 4.0

Method

82708270827082708270827082708270827082708150827082708270808180818081808180818260826082708081827082708081808182708270827082708270826082708015827082708270808182608270808182708260826082608270





Compound

2 -MethylnaphthaleneMethyl parathion4 -Methyl - 2 -pentanoneMethylene chlorideNaphthalene1,4 -Naphthoquinone1 -Naph thylamine2 -Naphthylamine2 -Nitroaniline3-Nitroaniline4 -NitroanilineNitrobenzene2 -Nitrophenol4 -NitrophenolN-Hi trosodi -n-butylamineN-NitrosodiethylamineN-Nitrosodime thylamineN-Ni trosodiphenylamineN-NitrosodipropylamineN-NitrosomethylethalamineN-Ni trosopiper idineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroni trobenzenePen tachlor opheno 1PhenacetinPhenanthrenePhenolp - Phenyl enediamlnePhoratePronamidePropionitrilePyreneSafrole .SilvexStyrene2,4,5-T

Concentration-

< 2.0< 3.0< 20.0< 1.0< 2.0< 5.0< 4.0< 4.0< 5.0< 5.0< 5.0< 2.0< 3.0< 10.0< 5.0< 5.0< 10.0< 2.0< 2.0< 5.0< 5.0< 4.0< 5.0< 3.0< 5.0< 10.0< 10.0< 5.0< 2.0< 3.0< 5.0< 3.0< 3.0< 50.0< 3.0< 5.0< 0.20< 1.0< 0.20

Method

827082708260826082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270826082708270815082608150

6878 S STATE ROUTE JOO • MELMORE. OH 44845 9999


Customer Name: EA6ON & ASSOCIATES INCSample Description: 96-300



1,2,4, 5-Tetrachlorobenzene1,1,1,2- Te trachloroe thane1,1,2,2 -Te trachloroe thaneTe trachloroe thy lene2,3,4, 6 -TetrachlorophenolThionazinTolueneo-ToluidineToxaphene1,2, 4 -Trichlorobenzene1,1,1-Trichloroe thane1,1,2-TrichloroethaneTrichloroethyleneTrichlorofluorome thane2,4, 5 -Trichlorophenol2,4, 6 -Trichlorophenol1,2,3- Tr ichloropropaneo,o,o-Triethyl phosphorothioatesym-TrinitrobenzeneVinyl AcetateVinyl ChlorideXylene (Total)

< 4.0< 1.0< 1.0< 1.0< 10.0< 4.0< 1.0< 5.0< 0.10< 2.0< 1.0< 1.0< 0.5< 1.0< 3.0< 3.0< 1.0< 5.0< 10.0< 10.0< 1.0< 2.0

8270826082608260827080818260827080818270826082608260826082708270826082708270826082608260


6878 S STATE ROUTE 100 • MELMORE. OH «4845-9999




:iient: EAGOM & ASSOCIATES INC•ate Sampled: 11/25/96iample Location: FB-1


iethod Used Date Extracted Date Analyzed Analyst

W-846;

W-846;

W-846;

W-846;

W-846;

W-846;

Method

Method

Method

Method

Method

Method

8015

8081

8150

8240 (SIM)

8260

8270

N/A

11/26/96

12/02/96

N/A

N/A

11/27/96

12/03/96

12/11/96

12/07/96

11/27/96

12/06/96

12/10/96

DJS

CMR

DAW

JSM

JSM

KJP



Page 1 of 5

Customer Name: EA6ON & ASSOCIATES INCSample Description: FB-1


Compound

AcenaphtheneAcenaphthyleneAcetoneAcetonitrileAce tophenone2 -Acetylaminof loureneAcroleinAcrylonitrileAldrinAllyl chloride4. • &*i%4 nni 4 v\Yt An fl

AnthraceneAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260BenzeneBenzo [a] anthraceneBenzo [b] flourantheneBenzo [k] flourantheneBenzo [ghi] peryleneBenzo [a] pyreneBenzyl alcoholalpha -BBCbeta-BHCdelta-BHCgama-BHC (Lindane)Bis (2 -chloroethoxy) methaneBis (2-chloroethyl) etherBis (2-chloro-l-methylethyl) etherBis (2 -ethylhexyl) phthalateBr bmochlorome thaneBromodichlorome thaneBromoformBromome thane4-Bromophenyl phenyl etherButyl benzyl phthalateCarbon disulfideCarbon tetrachlorideChlordanep-Chloroaniline

Concent rat ion -

< 2.0< 2.0< 5.0< 500< 3.0< 5.0< 5.0< 5.0< 0.02< 20.0< 5.0< 2.0< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 0.10< 1.0< 3.0< 4.0< 4.0< 5.0< 4.0< 5.0< 0.02< 0.02< 0.02< 0.02< 2.0< 2.0< 2.011.0

< 1.0< 1.0< 1.0< 1.0< 3.0< 2.0

5.2< 1.0< 0.10< 3.0

Method

8270827082608015827082708240 SIM8240 SIM80818260oorrnO4 1 U82708081808180818081808180818081826082708270827082708270827080818081808180818270

- 8270827082708260826082608260827082708260826080818270



Customer Name: EAGON & ASSOCIATES INCSample Description: FB-1



ChlorobenzeneChlorobenzilatep - Chlor o -m-CresolChlor o e thaneChloroformChlor ome thane2 -Chloronaphthalene2 -Chlorophenol4-Chlorophenyl phenyl etherChloropreneChrysenem-Cresolo-Cresolp-Cresol2,4-04,4'-DDD4, 4' -DDE4, 4' -DOTDiallateDibenz [a, h] anthraceneDibenzofuranDibromochloromethaneL, 2 -Dibromo- 3 - chloropropane (DBCP)L, 2-Dibromoethane (EDB)Dibromome thaneDi-n-butyl phthalateL, 2 -DichlorobenzeneL, 3 -DichlorobenzeneL, 4 -Dichlorobenzene1,3' -Dichlorobenzidine:rans-l, 4-Dichloro-2-butene)ichlorodifluoromethaneL, 1-Dichloroe thane1,2 -Dichloroe thane.,1-Dichloroethyleneiis-1, 2 -Dichloroethylene:rans - 1 , 2 -Dichloroethylene! , 4 -Dichlorophenol! , 6 -Dichlorophenol., 2-Dichloropropane., 3 -Dichloropropane: , 2 -Dichloropropane., 1-Dichloropropene:is-l, 3 -Dichloropropene;rans-l, 3 -Dichloropropene'ieldrin'iethyl phthalate'imethoate

< 1.0< 4.0< 5.0< 1.0< 0.5< 1.0< 1.0< 5.0< 2.0

N.D.< 3.0< 3.0< 3.0< 3.0< 0.10< 0.02< 0.03< 0.03< 3.0< 5.0< 2.0< 1.0< 1.0< 1.0< 1.0< 1.0< 2.0< 2.0< 2.0< 15.0< 1.0< 1.0< 0.5< 0.5< 0.5< 0.5< 0.5< 3.0< 10.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 0.02< 1.0< 4.0

826082708270826082608260827082708270826082708270827082708150808180818081827082708270826082608260826082708270827082708270826082608260826082608260826082708270826082608260826082608260808182708270



Customer Name: EA60N & ASSOCIATES INCSample Description: FB-1


Compound

p- (Dimethylamino) azobenzene7 , 12 -Dime thy Ibenz [a] anthracene3,3' -Dime thy Ibenzidine2,4 -Dime thy IphenolDimethyl phthalatem-Dinitrobenzene4,6-Dinitro-o-cresol2 , 4 -Dini trophenol2,4 -Dini tro toluene2,6 -Dini tro tolueneDinosebDi-n-octyl phthalateDiphenylamineDisulfotonEndosulfan IEndosulfan IIEndosulfan SulfateEndrinEndrin aldehydeEthylbenzeneEthyl methacrylateEthyl methanesulfonateFamphurFlour an theneFlour eneHeptachlorHeptachlor epoxideHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneHexachloropropene? ~Hf»TO*TlrtTl<*Indeno (1,2,3- cd) pyreneIsobutyl alcoholIsodrinIsophoroneIsosafroleKeponeMethacrylonitrileMe thapyr i 1 eneMe thoxy chlor3 -MethylcholanthreneMethyl ethyl ketoneMethyl iodideKethyl methacrylateHe thy 1 methanesulfonate

Cone en t ra t i on -

< 5.0< 5.0< 5.0< 3.0< 1.0< 5.0< 10.0< 10.0< 4.0< 4.0< 0.05< 1.0< 4.0< 3.0< 0.03< 0.03< 0.03< 0.02< 0.10< 1.0< 5.0< 4.0< 10.0< 2.0< 3.0< 0.03< 0.03< 2.0< 3.0< 5.0< 3.0< 10.0< 10.0< 5.0< 500< 10.0< 1.0< 5.0< 0.10< 100< 5.0< 0.10< 4.0< 10.0< 10.0< 5.0< 4.0

Method

82708270827082708270827082708270827082708150827082708270808180818081808180818260826082708081827082708081808182708270827082708270826082708015827082708270808182608270808182708260826082608270



Customer Name: EA6ON & ASSOCIATES INCSample Description: FB-1

ATELNO.: 96-16824-MELPage 4 of 5

Compound

2 -MethylnaphthaleneMethyl par at hi on4 -Methyl - 2 -pentanoneMethylene chlorideNaphthalene1,4 -Naphthoguinone1 -Naph thy lamine2 -Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2 -Nitrophenol4 -NitrophenolN-Nitrosodi -n-butylamineN-NitrosodiethylamineN-NitrosodimethylamineN -Hi trosodipheny 1 amineN-NitrosodipropylamineN-NitrosomethylethalamineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroni trobenzenePentachlorophenolPhenacetinPhenanthrenePhenolp-PhenylenediaminePhoratePronamidePropionitrilePyreneSafroleSilvex 'Styrene2,4,5-T

Concentration-

< 2.0< 3.0< 20.0< 1.0< 2.0< 5.0< 4.0< 4~0< 5.0< 5.0< 5.0< 2.0< 3.0< 10.0< 5.0< 5.0< 10.0< 2.0< 2.0< 5.0< 5.0< 4.0< 5.0< 3.0< 5.0< 10.0< 10.0< 5.0< 2.0< 3.0< 5.0< 3.0< 3.0< 50.0< 3.0< 5.0< 0.20< 1.0< 0.20

Method

827082708260826082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270827082708270826082708270815082608150



Customer Name: EAGON & ASSOCIATES INCSample Description: FB-1



1,2,4,5-Tetrachlorobenzene1,1,1,2-Tetrachloroethane1,1,2,2-Te trachloroe thaneTetrachloroethylene2,3,4,6-TetrachlorophenolThionazinTolueneo-ToluidineToxaphene1,2,4-Trichlorobenzene1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroethyleneTrichloro£luoromethane2.4.5-Trichlorophenol2.4.6-Trichlorophenol1,2,3-Trichloropropaneo,o,o-Triethy1 phosphorothioatesym- Tr ini trobenzeneVinyl AcetateVinyl ChlorideXylene (Total)

411110.04.01.65.00.102.01.01.00.51.03.03.01.05.010.010.01.02.0

8270826082608260827080818260827080818270826082608260826082708270826082708270826082608260

All units of concentration are ug/L (ppb).

G678S STATE ROUTE 100 • MCLMORE. OH 44845 9999


Client: EAGON & ASSOCIATES INCATEL Sample No.: 96-16825-MELDate Sampled: 11/25/96Date Received: 11/26/96Date Analyzed: 12/05/96Client ID: TRIP BLANK

Method: SW-846; 8260Sample Type: HATERPercent Solids:Analyst: SPH/JSMProject No.: TREMONT LANDFILL



Acetone < 5.0Benzene < 1.0Bromochloromethane < 1.0Bromodichlorome thane < 1.0Bromoform < 1.0Carbon Disulfide < 5.0Carbon Tetrachloride < 1.0Chlorobenzene < 1.0Chloroethane < 1.0Chloroform < 0.5Dibromochloromethane < 1.01,2-Dibromo-3 -chloropropane < 1.01,2-Dibromoethane (EDB) < 1.0D-Dichlorobenzene < 1.0p-Dichlorobenzene < 1.0brans-l,4-Dichloro-2-Butene < 1.0L,l-Dichloroethane < 0.5L,2-Dichloroethane < 0.5L,1-Dichloroethene < 0.52is-l,2-Dichloroethene < 0.5;rans-l, 2'-Dichloroethene < 0.5L,2-Dichloropropane < 1.0:is-l,3-Dichloropropene < 1.0:rans-l,3-Dichloropropene < 1.0Sthyl Benzene < 1.0!-Hexanone < 10.0Jromome thane < 1.0:hloromethane < 1.0>ibromomethane < 1.0lethylene Chloride < 1.0

2-Butanone < 10.0lodome thane < 10.04-Methyl-2-Pentanone < 20.0Styrene < 1.01,1,1,2-Tetrachloroethane < 1.01,1,2,2-TetraChloroethane < 1.0Tetrachloroethene < 1.0Toluene < 1.01.1.1-Trichloroethane < 1.01.1.2-Trichloroethane < 1.0Trichloroethene < 0.5Trichlorofluoromethane < 1.01,2,3-Trichloropropane < 1.0Vinyl Acetate < 10.0Vinyl Chloride < 1.0Total Xylenes < 2.0

Surrogate Data:

Dibromo £luoromethaneBromofluorobenzeneToluene-d8

% Recovery

93 (70-115)87 (86-115)93 (88-110)


CHAIN-OF-CUSTODY

Aqua Tech Environmental Laboratories, Inc.

Client Name:

Project Name:

Project No.

Sampler

- I \L•2-'''"-

•Trip

SEND RESULTS TO:Person:Company:Street:City:Phone:ATEL Quote #:

State: Zip:Fax:

Company PO #:

Rdipquuhed by: Dale/Ti '•V

Relinquished by: Dale/Time ReoeivedbyvJ Date/Time

Relinquished by: Date/Tune Received at Dale/Tin

Method of Shipment

Cooler Temperature:

Canton: 5300 Fulton Drive NW Marion: 1776 Marion-Waldo Rd Sanford: 936 N Homer BoulevardCanton. Ohio 447IS Marion. Ohio 43302 Sanford. North Carolina 27330800-635-3222 fax 216^94-2961 800-873-2835 fax 614-389-1481 800-522-2832 fax 919-774-7068

Tucson: 2700 E Bilby Rd Bldg A Melmore: 6878 S State RL 100 Minion 27531 ChanUga DriveTucxon. Arizona 85706 Melmorc. Ohio 44845 VIeJo: Mission Viq'o. Caldomia 92692800-r?9-2835 fax 520-573-6550 800-858-8869 fax419-397-2229 800-263-2261 fax 714-348-1922

CHAIN-OF-CUSTODY


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it g»/ ft 'I /

J- +IZ-(O,A<.-4../V/

SEND RESULTS TO:Person:Company:Street:City:Phone:ATEL Quote #:

State: Zip:Fax:

Company PO #:

R'TJiivwtshtti byi Date/Time Received by: Dajen-jme,

Rdioquuhed by: Date/Tune Dale/Time

Relinquished by; Date/Time Received at Laboratory by: Date/Ti

Comnv:nu: Method of Shipment

Cooler Temperature: Q

Canton: 5300 FuKoo Drive NW M«rlon: 1776 Marion-Waldo Rd Sanfoni: 936 N Homer BoulevariCanton. Ohio 44718 Marion. Ohio 43302 Sanford. North Carolina 27330800-«5-3222 fix 216^94-2961 800-873-2835 fix 614-389-1481 800-522-2832 fax 919-774-7068

Tncson: 2700 E Bilby Rd. Bldg A Melmort: 6878 S Stale Rt 100 MUslon 27531 Chintjga DriveTucson. Arizotu 85706 Melmore. Ohio 44845 Vlejo: Mission Viejo. Califoniii 92692800-879-2835 fix 520-573-6550 800-858-8869 f»x 419-397-2229 800-263-2261 fix 714-348-1922

CHAIN-OF-CUSTODY


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Sampler

/y f>pf*~elix -^ 7 Vif- J •» -///*}

/y/}$"/- 3 S IV ex? /v 3-7

Illo

A ?/ - it itew/X/c: -«*

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SENP RESULTS TO:Person:Company:

Street:City:Phone:ATEL Quote #:

/Of>

State: Zip:.Fax:

Company PO #:

Date/Time Received by: Date/Tii.'/-&£•'A -O

Relinquished by: Date/Time Received Ifr: / V^j Dale/Tune

Relinquished by: Date/Time Received at Laboratory by: Date/T

Comments: e /<f( Method of Shipment

Cooler Temperature:

7^Canton: 5300 Fulton Drive NW Marion: 1776 Marion-Waldo Rd Sanford: 936 N Homer BoulevardCanton. Ohio 44718 Marion, Ohio 43302 Sanford. North Carolina 27330800-635-3222 fax 216-494-2961 800-873-2835 fix 614-389-1481 800-522-2832 fax 919-774-7068

Tiioon: 2700 E Bilby Rd. Bldg. A Melmore: 6878 S Stale RL 100 Mission 27531 ChinUga DriveTucson, Arizona 85706 Melmorc. Ohio 44845 Vlejo: Mission \lejo. California 92692800-879-2835 fix 520-573-6550 800-858-8869 fax 419-397-2229 800-263-2261 fix 714-348-1922


CLIENT: EAGON & ASSOCIATES INC100 OLD WILSON BRIDGE RDWORTHINGTON , OH 43085

ATTN: FRANK MAJCHSZAK

| PROJECT NO. : TREMONT LF |

| PURCHASE ORDER: TREMONT LANDFILL |

DATE OF INITIAL RECEIPT ATLABORATORY: 11/26/96

| SAMPLE INVENTORY

| ATEL NO.

(96-16810-MEL

| 96-16811-MEL

J96-16812-MEL

|96-16813-MEL

| 96 -16 814 -MEL

J96-16815-MEL

(96-16816-MEL

| 96-16 817 -MEL

(96-16818-MEL

| 96 -16819 -MEL

J96-16820-MEL

J96-16821-MEL

(96-16822-MEL

(96-16823-MEL

J96-16824-MEL

|96-16825-MEL

CLIENT NO.

DL-1

TRIP BLANK

L-l

TRIP BLANK

M-2

A89-2

TRIP BLANK

METHOD (S)

APPENDIX I

APPENDIX I

APPENDIX II

APPENDIX I

APPENDIX II

APPENDIX II

APPENDIX I

A89-3S | APPENDIX II

A89-3D | APPENDIX II

TRIP BLANK

A91-4S

A91-7S

TRIP BLANK

96-300

FB-1

TRIP BLANK

APPENDIX I

APPENDIX II

APPENDIX II

APPENDIX I

APPENDIX II

APPENDIX II

APPENDIX I

AUTHORIZED SIGNATURE:

NJB

ORGANIC SECTION CHlfiF6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999

PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229

APPENDIX B.

TREND PLOTS

50EAGON& ASSOCIATES, INC.

g

40

30

25

20

15

10

0

TREMONT ASSESSMENTTRENDS IN IRON DATA

WELL 89-2

1 ' ' ' ' ' * ' ' ' ' ' i ' ' ' ' ' i ' ' ' ' ' i ' ' ' ' ' i ' ' ' ' ' i ' ' ' ' ' i ' ' ' ' ' i ' • ' ' ' | ' ' ' ' ' | ' i i i i | i i i i i | i i i i i |Dec-89 Jun-90 Dec-90 Jun-91 Dec-91 Jun-92 Dec-92 Jun-93 Dec-93 Jun-94 Dec-94 Jun-95 Dec-95 Jun-96 Dec-96

50

45

40

35

30

25

20

15

10

892IRON.CRF1/24/97

u&ofti

100

90

80

70

60

EAGON& ASSOCIATES. INC.

40

30

20

10 -

I

TREMONT ASSESSMENTTRENDS IN ARSENIC DATA

WELL 89-2

100

90

80

70

60

50

40

30

20

10

Dec-89 Jun-90 Dec-90 Jun-91 Dec-91 Jun-92 Dec-92 Jun-93 Dec-93 Jun-94 Dec-94 Jun-95 Dec-95 Jun-96 Dec-96IMAR5EN.ORF

1/24/97

o

Io§u

15

14

13

12

11

10

9

g

7

6

5

EAGON & ASSOCIATES. INC.

TREMONT ASSESSMENTTRENDS IN CHLOROETHANE, BENZENEAND o-DICHLOROBENZENE(l,2) DATA

WELL 89-2

—©— CHLOROETHANE

D BENZENE

A o-DICHLOROBENZENE (1.2)

o-DICHLOROBENZENE( 1.2)Y - B(X) + A

CHLOROETHANEY • B(X) + A

15

14

13

12

11

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9

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3

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1

Dec-89 Jun-90 Dec-90 Jun-91 Dec-91 Jun-92 Dec-92 Jun-93 Dec-93 Jun-94 Dec-94 Jun-95 Dec-95 Jun-96 Dec-96892CHBZ.GRF

1/24/97

f,c

COQ

OQ

Oc/oC/3

O

1000

900

800

700

600

500

400

300

200

100

EAGON & ASSOCIATES. INC.

TREMONT ASSESSMENTTRENDS IN TOTAL DISSOLVED SOLIDS DATA

WELL 89-2

1000

900

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700

600

500

400

300

200

100

Dec-89 Jun-90 Dec-90 Jun-91 Dec-91 Jun-92 Dec-92 Jun-93 Dec-93 Jun-94 Dec-94 Jun-95 Dec-95 Jun-96 Dec-96892TDS.GRF

1/24/97

500EACON & ASSOCIATES, INC.

WQ2oj33U

450 -

400 -

350

300 -

250 -

200 -

150 -

100 -

50 -

TREMONT ASSESSMENTTRENDS IN CHLORIDE DATA

500

450

400

350

300

250

200

150

100

50

0 i i i i i | i i i i i [ i i i i i | i i i i i [ i i i i i | i i i i i [ 'i i i i i | i i i i i [ i i i i i | i i i i i [ i i i i i | i i i i i | i i i i i | i i i i i | i 0

Dec-89 Jun-90 Dec-90 Jun-91 Dec-91 Jun-92 Dec-92 Jun-93 Dec-93 Jun-94 Dec-94 Jun-95 Dec-95 Jun-96 Dec-96CL.GRF1/24/97

•§>

Oc/oQUJ

Ot>oooQ

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2000

1800

1600

1400

1200

1000

800

600

400 h

200 h

EAGON& ASSOCIATES. INC.

0

TREMONT ASSESSMENTTRENDS IN TOTAL DISSOLVED SOLIDS DATA

2000

1800

1600

1400

1200

1000

800

600

400

200

* ' ' ' ' ' [ ' ' ' ' ' [ ' ' ' ' ' ' ' ' ' ' ' ! ' ' ' ' ' I ' ' ' ' ' I ' ' ' ' ' I ' ' ' ' ' I ' ' • ' ' I ' ' ' ' ' I ' I I I I I I I I I I I I I I I I IDec-89 Jun-90 Dec-90 Jun-91 Dec-91 Jun-92 Dec-92 Jun-93 Dec-93 Jun-94 Dec-94 Jun-95 Dec-95 Jun-96 Dec-96

TDS.GRF1/24/97

1'»*_X§H

2H2UJcjOu

NOTE: FOR WELLS REPORTED AS NON-DETECT.\I1 THE VALUE WAS USED.ALL FITS COMPUTED USINO Y- B(X) + A

—0— BENZENE

—A— CHLOROBENZENB

—Q— CHLOROETHANE

Q 1.1-DICHLOROETHANE

<7 o-DICHLOROBENZENE(1.2)

—0— p-DICHLOROBENZENE(l,4)

20

19

18

17

16

15

14

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1

0

Dec-89 Jun-90 Dec-90 Jun-91 Dec-91 Jun-92

EAGON & ASSOCIATES, MC.T

TRENDS IN ORGANIC CONSTITUENTSNEAR THE SUSPECTED SOURCE AREA

M-2

VOCS1/24/97

Dec-92i i i

Jun-93 Dec-93 Jun-94 / Dec-94 Jun-95 Dec-95 Jun-96 Dec-96

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1

0

M-DICHLOROETHANEp-DICHLOROBENZENE<l,4) BENZENE

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t-UJ<_>2OCJ

EAGON & ASSOCIATES. /JVC.i i i i | i i i i r | i i i i i [ i i i i i [ i i i i i [ i M t i [ i i i i i | i i i i i | n i i i | i i i i i [ i i i i i | i i i i i | i i i i i | i i i i i | i.

TRENDS IN ORGANIC CONSTITUENTSNEAR THE SUSPECTED SOURCE AREA

A89-3S

NOTE: FOR WELLS REPORTED AS NON-DETECT.1/2 THE VALUE WAS USED.ALL FITS COMPUTED USING Y- B(X) + A

20 p

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i i i i i I i i i i i I i i i i i I i i T i i I i i i i i I i i i i i I i i i i i I i M i i | i i i n | i i i i i i1 i i i i i i i i i i i i i i

Dec-89 Jun-90 Dec-90 Jun-91 Dec-91 Jun-92 Dec-92 Jun-93 Dec-93 Jun-94 Dec-94 Jun-95 Dec-95 Jun-96 Dec-963SVOCS

1/34/97

CHLOROETHANE

U-DICHLOROETHANE

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0

APPENDIX C.

CORRESPONDENCE DATED JULY 10,1992

EAGON & ASSOCIATES, INC.Consulting Geologists6877 N. High Street, Suite 3021 Worthington, Ohio 430851 (614) Mi-5760

July 10, 1992

Mr. Brian NickelOhio EPASouthwest District Office40 South Main StreetDayton, Ohio 45402

Re: Request to Modify Assessment SamplingTremont Landfill

Dear Brian:

Review of the results of the April assessment sampling showed no significantdifferences from previous assessment sampling events. Therefore, it is proposed thatassessment wells A91-5S, A91-5D, A91-8S, A91-9S, and A91-10S be dropped from the list ofwells to be sampled because the water quality and hydrogeologic data clearly shows that thesewells have not been impacted. Further, model results of the corrective measures studyillustrate that these wells have little potential to be impacted. We are not requesting thatthese wells be plugged and we will continue to take water-level measurements. We willcomplete one year of monthly water-level measurements in July and will be compiling a briefreport presenting these results, as well as a tabulation of the additional water-quality datagenerated since the assessment report of January 1992. We plan to begin the July samplingat Tremont Landfill the week of July 13-17.

A second issue is the continued requirement to include the compound Bis (2-ethylhexyl)phthalate on the list of assessment parameters. This compound is a plasticizer that is used inthe manufacture of a variety_pf plastics to promote flexibility, and it is ubiquitous in theenvironment. It is no surprise that this compound has shown up in low concentrations moreor less'randomly in a few of the assessment wells. The wells are made of plastic, we useplastic bailers, and store them in plastic garbage bags. Much of the other sampling equipment,such as syringes and filters, as well as many of the sample containers themselves are made of,enclosed in, or in contact with, various types of plastic. There is ample opportunity tointroduce this compound into ground-water samples, even under the most controlledconditions. (Distilled water, for instance, which is used to rinse non-dedicated samplingequipment and for other ancillary purposes, is supplied in plastic containers.)

Bis (2-ethylhexyl) phthalate is the single most expensive compound to test for on thelist of assessment parameters because it is a base-neutral/acid extractable (BNA) semi-volatilecompound and requires a separate extraction procedure. As part of both the July and

October, 1991 assessment samplings, 56 other BNA semi-volatile compounds were tested for,and none were present. Common sense indicates that if Bis (2-ethylhexyl) phthalate wereactually present as a contaminant (rather than as a sampling or laboratory artifact) at leastone of the other related compounds would have been detected, also.

Eagon & Associates, Inc. has had experience at another site where the technicalitiesof statistical analysis (rather than some valid indicator of water-quality deterioration) triggeredan assessment sampling. The onjy organic compound that was detected was Bis (2-ethylhexyl)phthalate. Fortunately, the highest concentration was in an upgradient background well atwhich the only possible impact on ground-water quality was the installation of the PVC wellitself.

The US EPA Contract Laboratory Program (CLP) recognizes the ubiquitous nature ofphthalates. For most other compounds, tolerance in method blank samples is equal to themethod detection limit However, in the case of phthalates and certain common organicsolvents, tolerance in method blank samples is five times the method detection limit (BobGlowacky, manager, Aqua Tech Laboratory at Melmore, personal communication).

It is our view that the results of the research that we have conducted related to theoccurrence of the compound Bis (2-ethylhexyl) phthalate more than justifies our request thatthis compound be deleted from the list of assessment parameters. It serves no valid purposeas an indicator parameter, and the substantial incremental cost of its inclusion for which nobenefit is received, cannot be justified. With Ohio EPA's concurrences, we will not analyzefor this compound in the July assessment samples.

Sincerely,

Herbert B. EagoHydrogeologist

HBE/pst

Status of Assessment and Corrective MeasuresTremont Landfill

February 6,1997

100 0 100=fcGRAPHIC SCALE

200 300

1ESQJQ

o DETECTION MONITORING WELL

• ASSESSMENT MONITORING WELL

D SPECIAL PURPOSE WELL

JMW-7SJMW-7D

APPROXIMATELIMIT OF SOLID WASTE

SEDIMENTATION BASIN

ASSESSMENT AREA-

CHAPMAN CREEK

FIGURE 1. MONITORING WELL LOCATION MAP

C:\ACAD\aARKCO\TREMONT2.0WC 01/28/97 LAYER: FW7_«/96

91-S986.00

O SOIL BOWNCS

• GAS MONITOR PROBES

MONITDRINC WEUS

RESIDENTIAL WELLS


M-3982.15- - 982

— 983*" WATER LEVEL CONTOUR

FLOW LINE


SCALE IN FEET

FIGURE 2. WATER LEVELS AND FLOW DIRECTIONS ON JUNE 5. 1996

C:\ACAD\CLARKCO\TROlilOrnZ.DWC 01/20/8' LAYER: nG7_11/95

91-S•$.983.09

SOIL BORINGS

GAS MONITOR PROBES

MONfTORINC WELLS

RESIDENTIAL WELLS


WATER LEVEL CONTOUR

FLOW LINE


FIGURE 3. WATER LEVELS AND FLOW DIRECTIONS ON NOVEMBER 25, 1996

TABLE 2.SUMMARY OP ANALYTICAL RESULTS


•:j §|j ^pl i liil:,Alkalinity, TotalArsenic, Dissolved/Total ••Calcium, Dissolved/Total ••ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total' •Magnesium, Dissolved/Total"Manganese, Dissolved/Total"Nitrogen, AmmoniaPotassium, Dissolved/Total"Residue, T. Fit. (Dis*.)Sodium, Dissolved/Total* •SulfateTotal KjeldahlN(TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead,PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (aa N)pH,LabSulCde, Total (as HjS)Zlnc,ZnBenzeneChlorobenzeneChloroethane1,1- Dichloroethanecii - 1,2-Dichloroethyleneo-Dichtorobenzene (1,2)p- Dichlorobenzene (1,4)p-Xylenem-Xylene

mg/1ug/1mg/1mg/1mg/1mg/1ntuug/1mg/1ug/1mg/1mg/1mg/1mg/1mg/1mg/1mg/1ug/1ug/1ug/1UMHOug/1ug/1ug/1mg/1mg/1S.U.mg/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ne/1

931<3

270350

94

12500100

1.83

165025093

3.0634

1

996<2

240367

13300100110

8.61630247762.946

0.54.21.723

<0.55.41.2

2.4*2.4*

942<5

260320

94

13500100<751.756.2

1590260

402.72

26

<0.53.51.62.7

<0.57.91.7

<2.0*<2.0»

1040<5

440300180

180002001301.416.0

1590250

692.57

30

SSSKaSSSSKi&i^^XjSStjIUjIfltflSSBSjX

812 502 938<5 10 6

235 290 240250 350 27092 99 110

12000 15300 1400093 110 9289 120

1.44 1.52 1.297.0

1600 1490 1540250 280100 160 50

2.69 3.10 2,2866 27 29

•HamH®m980<3

230266110

1200096

1101.076.9

159827052

2,9931

131.4

<1.01.5

<0.52.6

<0.5<1.0<1.0

BEmam980<5

220262160

1300092

1101.059.1

162326051

3.1928

<0.52.1

<1.01.7

<0.53.00.7

<1.0<1.0

|t||igg|&|i&|

10006

220313210

1300093

1101.324.5

1580260

493.11

30

Ilililll

10004.5221317<20

1390093

1011.256.6

140028057.63.46

30

^2:ji8i&S*3f04/9ZlS:

1010<3

213280244

1400089.61001.157.2

145026049.82.56

33

1.36.92.74.6

<0.519.45.2

<1.0<1.0

1i?8:*:?8ii&iSi!5

965<3

214252182

1370089.4

941.367.9

155025939.73.04

32

0.82.9

<0.51.9

<0.56.81.2

<0.5<0.5

Sijviil jiij' :

&$&$$1020

<3218272155

1450088.8

930.967.3

1630262

512.85

34

1.46.00.71.7

<0.513.72.4

<0.5<0.5

ND - Not DetectedAquatech method 524.2 detection limit* are 0.5/xg/l for each of the ten volatile organic compounds (VOC's).Method 8270 detection limits ire 2.0/ig/l for Bii(2 ethylhexyl)phthalatc.• Prior to the July 1991 sampling, P-xylene and m-xylene could not be separately quantified. Detection limits and concentration

reported prior to July 1991 are for both compounds combined.• • Samples no longer Odd-filtered starting 11/29/94.1 Total Xylene Is reported as a result of Appendix H methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0 m/t.

P«p lo f9 B>fM * Auodttft, lot

Alkalinity, Total mg/1Arsenic, Dissolved/Total" ug/1Calcium, Dissolved/Total•• mg/1Chloride mg/1COD mg/1COD, Dissolved mg/1Turbidity ntuIron, Dissolved/Total" ug/1Magnesium, Dissolved/Total* • mg/1Manganese, Dissolved/Total •• ug/1Nitrogen, Ammonia mg/1Potassium, Dissolved/Total** mg/1Residue, T. Fit. (Diss.) mg/1Sodium, Dissolved/Total* • mg/1Sulfate mg/1Total Kjeldahl N (TKN) mg/ITotal Organic Carbon mg/1Barium, Ba ug/1Cadmium, Cd ug/1Chromium, Cr ug/1Conductivity, Lab UMHOCopper, Cu ng/1Lead, Pb ug/1Nickel, Ni ng/1Nitrate + Nitrite N mg/1Nitrogen, Nitrite (as N) mg/1pH, Lab S.U.Sulfide, Total (as HjS) mg/1Zinc, Zn ug/1Benzene ug/1Chlorobenzcne ug/1Chloroethane ug/11,1-Dichloroethane ug/1ris-l,2-Dichloroethylene ug/1o-Dichlorobenzene(l,2) ug/1p-Dichlorobenzene (1,4) ug/1)-Xylene . ug/1m-Xylene______________ug/1



10705.8210<2.027931410501270090.493

0.958.4

158026950

2.8433

<0.52.01.41.4

<0.55.71.0

<0.5<0.5

3.4

25216880760

1370087.586

0.936.4

1640259

i 51

33428

<0.5<0.50.81.1

<0.523

<0.5<0.5<0.5

979<3.0207241211105400

1440086.985

0.766.5

154028446

2.7828

0.91.91.11.3

<0.56.41.0

<0.5<0.5

765<3.021729385101410

1490093369

0.906.9

140058345

2.2634

1.55.61.51.9

<0.514.22.5

<0.5<0.5

1030<3.01852219481150

1390079.162

0.876.7

146035394

2.4129

<0.51.31.31.4

<0.54.91.0

<0.5<0.5

1060<3.020344330490220

1520082.976

0.767.7

135031048

3.3624

0.61.01.41.4

<0.54.20.8

<0.5<0.5

10709.5240298131

585259009933750.945.9

160024262

2260.817

3190151450

<0.05<0.056.8

68

2.0

<0.5<0.563

10401121019383

317200001001860.935.9

151023287

1820.97.52126.250

<0.05<0.0563

249

<0.5<0.5<2.0<2.0

1110<3.017230368

1571560076.498

0.856.2

1530217260

155<0.5<5.0

2.9<20

<0.05

60

1.32.81.2

<0.57.21.5

1070 1040<3.0 3.2156 205123 18255 100

2471510068.41030.854.4

1390151130

121<0.5<S.O2200

4.9<200.07

6.6

2201840087.41640.775.2

1600189130

1350.9

<5.02420105.722

0.05

6.630.42

77 117

1.3 <1.0<0.5 <0.5<0.5 <0.5

<2.0><ZO l

<2.0><2.0l

ND • Not DetectedAquatech method 524.2 detection limits are 0.5/ig/l for each of the ten volatile organic compounds (VOC's).Method 8270 detection limits are 2.0/ig/l for Bis(2 ethylhexyl)phthalate.• Prior to the July 1991 sampling, P-xylene and m-xylene could not be separately quantified. Detection limits and

concentrations reported prior to July 1991 are for both compounds combined.•• Samples no longer field-filtered starting 11/29/94.1 Total Xylene is reported as a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are each 2.0 jig/<.

; »-Jio-»7 Ptfilot9



Alkalinity, TotalArsenic, Dissolved/Total"Calcium, Dissolved/Total"ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total* •Magnesium, Dissolved/Total* •Manganese, Dissolved/Total"Nitrogen, AmmoniaPotassium, Dissolved/Total"Residue, T. Fit. (Din.)Sodium, Dissolved/Total"SulfateTotal KJeldahlN(TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead,PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (aa N)pH. LabSulflde, Total (as HjS)Zinc,ZnBenzeneChlorobenzeneChloroethane1,1-Dichloroethaneds- 1,2-Dichloroethyleneo-Dichlorobenzene (1,2)p- Dichlorobenzene (1,4)3 -Xylenem— Xylene

mg/1ug/1mg/1mg/1mg/1mg/1ntuug/1mg/1ug/1mg/1mg/1mg/1mg/1mg/1mg/1mg/1ug/1ug/1ug/1UMHOug/1ug/1ug/1mg/1mg/1S.U.mg/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1UK/1

jjgjjgfm§B8BBB»"B™BHB iiB^BBffiSB^

562 59353 4494 13540 3621

25000 2390037 54

4300.8

6.1650 65046 409 13

1.02 1.05.6 9

i

3.77.46.21.90.52.7

NDNDND

63465

1603949

3290051

3100.935.13585061

0.945.4

5.28.59.83.4

ND3.1

NDNDND

55082

1302587

2600049

3200.164.9600

39.017

1.443.8

4.86 4.49.51 17.66.1 5.22.6 2.3

ND ND3.9 4.9

ND 1.1ND NDND ND

mBHHliiai

544 750 67385 -M 78 71

130 143 14431 30 29.2<8 47 84

28000 32600 3270050 53.1 53.7

290 262 2640.79 0.64 0.634.8 5.9 5.7580 654 682

39.0 38.1 38.27 14.2 14.4

0.84 1.75 1.714.2 5.5 5.6

4.7 4.915.0 16.65.9 632.0 4.4

ND ND5.8 5.61.4 1.6

ND NDND ND

5.217.36.23.9

ND7.21.9

NDND

51952

13224.6

77

2920049.42350.545.1588

37.03

0.534.2

4.515.34.6

NDNDNDNDNDND

57164

132263316

30026400

47.2248

0.555.3588

35.69

0.375.0

3.916.34.51.1

ND5.20.9

NDND

•Pmemr63

29.1—24

29900

0.75

653

5.9

4.218.15.71.8

<0.55.01.0

<0.5<0.5

ipf63

31.76611

3803300

0.54

72836.0

<1.0

4.419.6

<0.52.4

<0.56.0

<0.5<0.5<0.5

62561

15128.1

37

3250056.32860.454.8682

34.97

0.855.1

4.123.03.32.1

<0.55.51.1

<0.5<0.5

M66

29.7

39

25900

0.52

57038.6

7.1

3.921.43.913

<0.56.11.1

<0.5<0.5

• A89-100 If a blind duplicate of ASS-2. • A93-400 ii a hlkd daplicatt of A*9-Z• A95-400 if a blind duplicate of AS9-Z • A96-200 ii a blind duplicate of AI9-Z•• Stmplct BO kmjer field - filtered lUrdag 11/29/94.1 Total Xylene la reported aa a result of Appendix II methodology and (1,2) and (1,4) Dichlorobenzene are

• A94-400 ia a blind duplicate of AS9-2.* A9S-200 Ii a blind duplicate of AS9-2.

Pip 5 of 9



Alkalinity, Total mg/1Arsenic, Dissolved/Total" ug/1Caldum, Dissolved/Total" mg/1Chloride m|/lCOD mg/1COD, Dissolved mg/1Turbidiry ntuIron, Dissolved/Total* • ug/1Magnesium, DUsolved/Total** mg/1Manganese, Dissolved/Total" ug/1Nitrogen, Ammonia mg/1Potassium, Dissolved/Total* • mg/1Residue, T. Fit. (Diss.) mg/1Sodium, Dissolved/Total* * mg/1Sulfate mg/1Total Kjeldahl N (TKN) . mg/1Total Organic Carbon mg/1Barium, Ba ug/1Cadmium, Cd ug/1Chromium, Cr ug/1Conductivity, Lab UMHOCopper, Cu ug/ILead, Pb ug/1Nickel, Ni ug/1Nitrate + Nitrite N mg/1Nitrogen, Nitrite (as N) mg/1pH, Lab S.U.Sulflde, Total (as HjS) mg/1Zinc, Zn ug/1Benzene ng/1Chlorobenzene ug/1Chloroethane ug/11,1-Dichtoroethane ug/1ds-l,2-Dichloroethylene ug/1o-Dichlorobenzene (1,2) ug/Ip-Dichlorobenzene (1,4) ug/1p-Xylene ng/1m -Xylene nj/l

?ffigfffys:. sgyg^wS/fl^ffHH&fCM 'ft

61 43

§ iliiiiiiiiiiiEBgig^^^^^^^^^^m^^^^^^^^^^^^^^^^V^^

542 540 615 574 582 591 651 672 57343 47 44 47 40 42 55 52 38 37 60

34.5 35.9 115 120 121 128 116 129 129 125 12930.2 353

41 28

28.9 28.9 33.6 32.9 30.2 31.5 32.8 33.5 4932 14 14 11 14 14 14 16 <20

67 24191 206 167 140 . 136 118 328 313 180

26200 25600 3320 3480 21800 22800 24000 26200 22700 24900 27300 26400 2450041.0 42.8 45.9 42.9 42.7 473 46.2 45.0 44.1190 199 200 206 197 219 236 230 222

0.50 0.51 0.43 0.43 0.50 0.46 0.61 0.57 039 039 0.51 0.45 0.364.0 4.2 4.0 <ZO 3.7 4.0 33 3.2 4.1

592 574 638 628 602 588 734 706 625 610 693 657 71838.7 35.8 40.5 42.1 33.5 34.9 32.5 33.8 31.9 34.8 30.9 28.9 37.1

<5 <5.0 8 7 <5 <5 <2 3 <5

7.9 4.9 4.6 4.5625 651 631 696 683 736 709 682 697

<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0824 803 1140 1150 1130 1130 1020<10 <10 <10 <10 <10 <10 <10 <10 <10<ZO <ZO <ZO <2.0 <2.0 <2.0 <2.0 <ZO <ZO<20 <20 <20 <20 <20 <20 <20 <20 <20

<0.05 <0,05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05<0.05 <0.05 <0.05 <0.05

6.7 6.7 6.5 6.6 6.5 6.5 6.65<0.05

<10 <10 <10 <10 <10 <10 <10 <10 <103.6 j 43 4.0 3.1 3.6 6.5 Z9 2.9 3.9 3.9 4.7 5.2 4.3

20.5 21.6 23.9 19.7 24.3 22.4 133 13.8 19.7 18.5 28.5 30.4 283.6 <0.5 5.0 4.5 1.1 <1.0 <1.0 <1.0 5.7 4.0 3.7 3.9 <l.O1.2 12 13 13 3.0 2.9 <0.5 <OJ 0.9 1.0 13 1.1 <0.5

<0.5 <0.5 <0.5 0.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.56.0 5.8 6.0 4.8 7.8 7.7 2.8 3.9 5.8 5.6 5.4 53 4.21.2 1.2 12 0.9 <1.0 1.0 <ZO <1.0 <1.0 <1.0 1.2 1.4 <ZO '

<0.5 <OJ <0.5 <0.5 <1.0 <1.0 <1.0 <I.O <1.0 <1.0 <1.0 <1.0 <ZO l

<0.5 <0.5 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1 0 <ZO '* A89-100 Is a Ufad dlpHcate of A89-2. • A93-400 to « blind dtplkite of AS9-Z • A94-400 is t blind duplicate of AS9-2.• A95-400 Is a blkd diplleatt of A89-2. • A96-200 is a blind duplicate of AS9-Z • A95-200 I* a blind dvpllcate of A*9-Z•• Sabplas ao bagcr field - filtered staring 11/29/94.1 Total Xylene is reported at a result of Appendix II methodology and (1,2) and (1,4) Diehlorobenzene are each 2.0/ig/l.

irtmonrSio«k-«<X-*J; 29- Jta-r Eiftt 4 Auettitti, lot


ASSESSMENT PARAMETERS - JANUARY 1990 TO PRESENT:^>™™:**:»fSS8^S^^^^^ '

AUcalinity, TotalArsenic, Dissolved/Total* •Calcium, Dissolved/Total"ChlorideCODCOD, DissolvedTurbidityIron, Dissolved/Total"Magnesium, Dissolved/Total**Manganese, Dissolved/Total* •Nitrogen, AmmoniaPotassium, Dissolved/Total"Residue, T. Fit. (Dita.)Sodium, Dissolved/Total**SulfiteTotal KjeldahlN(TKN)Total Organic CarbonBarium, BaCadmium, CdChromium, CrConductivity, LabCopper, CuLead,PbNickel, NiNitrate + Nitrite NNitrogen, Nitrite (as N)pH,LabSulflde, Total (as H,S)Zinc, ZnBenzeneChlorobenzeneChloroethane1,1- Dichloroethaneds - 1 ,2 - Dichloroethyleneo-Dichlorobenzene (1,2)p-Dichlorobenzene (1,4)p-Xylenem-Xylene

mg/1ug/1mg/1mg/1mg/1mg/1ntuug/1mg/1ug/1mg/1mg/1mg/1mg/1mg/1mg/1mg/1ug/1ug/1ug/1UMHOug/1ug/1ug/1mg/1mg/1S.U.mg/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1UK/1

^Ho|H9^^ffffifflnflnffiBi

11806

170390170

280075

2801.889.1

200049081

4.4857

NDNDNDNDNDNDNDNDND

HHBBHBiPmPEEniiB

12008

168376

258078

265

10.21870488883.658

NDND3.3

NDNDND

' NDNDND

fSSflroli1030

1022056

170

380075

3201.797.2

187044038

3.7146

NDND4.6

NDNDNDNDNDND

100020

180185180

820083

4900.198.8

1500330.0

7233124.0

ND NDND NDND NDND NDND NDND NDND NDND NDND ND

BJjfflEiSnlB

97121

20815693

1010093.83661.327.6

1440253.0

792.4328.0

NDND3.4

NDNDNDNDNDND

m&mBEJBHS^p

9316.0180186258

8200873249

1.749.4

1460317.0

62.93.1730.0

NDND3.5

NDNDNDNDNDND

mmjMiffllffiffiSJajl

9295.9182171285

852088.52581.793

1390327

65.21.64

29

NDND2.9

NDNDNDNDNDND

BfljBjiB|p|

f«8»*J*«:

9559.01851579282

20010200

82.83021.698.4

1420236.0

832.76

28

NDND3.0

NDNDNDNDNDND

ifii/S88ra

8.0

68.8

33

9870

0.59

111096.9

11.0

<0.5<0.5

3.81.4

<0.5<0.5<0.5<0.5<0.5

6.9

79.5

26

10300

0.63

1120101

11.0

<0.5<0.5

3.30.9

<0.5<:0.5<0.5<0.5<0.5

mm5.5

1306955

17010500

1.41

974203

20

<0.5<0.5

2.70.7

<0.5<0.5<0.5<0.5<0.5

m9136.6183139

76

1280088.62221.748.4

127020396

3.5023

<0.5<0.5

2.50.6

<0.5<0.5<0.5<0.5<0.5

SI

7.0

118

78

13300

1.67

1190194

19

<0.5<0.5

3.80.6

<0.5<0.5<0.5<0.5<0.5

• A92-100 and A93-100 are blind duplicate sample* of A89-3S.• • Sample* no longer field - filtered starting 11/29/94.1 Total Xylene if reported aa a result of Appendix n methodology and (1,2) and (1,4) Dichlorobenrene are each 2.Qpg/(.

»r 9 Etfoo A Aitodtni. In

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ASSESSMENT AND CORRECTIVE MEASURES TREMONT LANDFILL · quality data from assessment monitoring dating back to January, 1990. A Corrective Measures Study (CMS) for the Tremont Landfill