AT&T Hall Ridge Work Plan 03-07-2016

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    CB&I500 Penn Center Blvd.

    Suite 1000Pittsburgh, PA 15235

    Tel: 412.372.7701Fax: 412.380.4091

    www.CBI.com

    March 7, 2016 Project No. 156319

    Mr. Geoffrey Brown Emergency Response Program Oregon Department of Environmental Quality Western Region – Eugene 165 E 7 th Ave, Suite 100 Eugene, OR 97401 ‐3049

    Re: Path to Closure Work Plan AT&T Hall Ridge Cell Tower National Response Center Report No. 1140291 Oregon Emergency Response System Report No. 2016 ‐0374 Detroit, Marion County, Oregon

    Dear Mr. Brown:

    CB&I on the behalf of AT&T, is pleased to present this Path to Closure Work Plan for the post excavation

    and characterization activities at the AT&T’s Hall Ridge, Detroit, Oregon, cell tower (Site). The

    emergency response team, which consisted of CB&I, NRC, NWFF, and SMAF, have completed the initial

    phase of the emergency response including the removal of impacted soil in the release area,

    containment of the downslope migration of fuel, characterization of the impacted soil, snow removal,

    and initial road repairs.

    On February 11, 2016, Barry Williams (AT&T) received notification of a release of diesel at the subject

    site. The initial investigation estimated the amount of fuel released from the tank system at 550 gallons.

    It appeared the fuel was pumped from the 800 ‐gallon main tank to the 220 ‐gallon day tank, which

    discharged from the vent located on the roof. Mr. Williams notified the National Response Center to

    report the spill at 1740 Eastern Standard Time (EST). The National Response Center assigned Report No. 1140291 to the spill. Mr. Williams also notified the Oregon Emergency Response System at 1750 EST to

    report the spill and was assigned Report No. 2016 ‐0374.

    This Work Plan was developed to provide guidance for the implementation of bio ‐stimulation treatment

    activities and post excavation and characterization monitoring.

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    Mr. Geoffrey Brown ‐ 2 ‐ March 7, 2016

    Background

    The site and surrounding area are located on the U.S. Geological Survey 7.5 ‐minute Detroit, Oregon,

    topographic quadrangle map. The site is located at approximately 44°43’09.7” north latitude,

    122°13’03.6” west longitude. A review of the quadrangle map shows the site at an elevation of approximately 4,400 feet above mean sea level (msl). The nearest surface water to the site is an

    unnamed tributary, which is approximately 600 feet northeast of the site. A site vicinity map is

    presented as Figure 1.

    According to the United States Geological Survey’s National Geologic Map Database, the site is located

    on the eastern flank of the Sardine Syncline and the Breitenbush Anticline is located to the east. Bedrock

    dips at a shallow angle to the west. Bedrock listed is the Sardine Series, which consists of series of

    Miocene age rhyolite, andesite, basalt, tuff, and breccia exposed on Sardine Mountain northwest of

    Detroit.

    Emergency Response Tasks Completed

    The following tasks have been completed under this emergency response:

    On February 12, 2016, crews were mobilized to inspect the site. The impacted area was assessed and absorbent booms and pads placed in strategic areas to capture the free phase diesel.

    From February 13 through February 19, 2016 – Road clearing continued with additional snow fall. Several impacted areas were hand excavated. Absorbent pads inspected and replaced. Waste was containerized and staged for disposal.

    On February 22, 2016, the ORDEQ and USFS provisionally approved the Sampling and Analysis Plan.

    On February 23, 2016, the USFS located and authorized NRC to collect water from a source near the site for the percolation test.

    On February 24 ‐25, 2016, the percolation test commenced over a two ‐day period using fluorescent dye (Bright Dyes® FLT Yellow ‐Green Powder) to recreate the flow paths of diesel fuel through bedrock.

    On February 26, 2016, soil samples were collected on a 20 ‐foot grid to delineate the extent of the diesel in the shallow soil downslope from the release.

    On Friday February 19, 2016, Sunday February 21, 2016, and Sunday February 28, 2016, four surface water samples were collected from the unnamed tributaries (SW‐01, SW‐02, SW‐03, and SW‐04) and SW‐05 on Thursday February 25, 2016. Daily inspections occur at the five surface water locations.

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    Mr. Geoffrey Brown ‐ 3 ‐ March 7, 2016

    Discussion of Soil Sample Results

    On February 26, 2016, soil samples were taken from 21 locations at the release area excavation and downslope areas. Sample locations were identified using an established downslope grid and biased

    where diesel fuel was visually observed (Figure 3). Soil samples were analyzed for diesel range organics

    by NWTPH‐Dx, RBDM VOCs by EPA 8260B, and PAHs by EPA 8270D SIM. The laboratory analytical results

    have been tabulated and presented in Table 1.

    The soil sample results were compared against ORDEQ risk‐based concentrations (RBCs) for two

    exposure pathways: soil ingestion, dermal contact, and inhalation (RBCSS), and soil leaching to

    groundwater (RBCSW). Three sample locations showed NWTPH‐Dx concentrations that exceed RBCs via

    either exposure pathway. These three “hot spot” locations (0C, 1C, and 2C) follow the centerline of the

    downslope grid, adjacent to the release area excavation.

    At sample location 0C, laboratory results show RBC exceedances for NWTPH‐Dx (9,430 milligrams per

    kilogram [mg/kg]), Benzene (0.161 mg/kg), Ethylbenzene (3.70 mg/kg), Naphthalene (2.15 mg/kg), and

    1,2,4 ‐Trimethylbenzene (19.9 mg/kg). At sample location 1C, results show RBC exceedance for NWTPH‐

    Dx (66,400 mg/kg). At sample location 2C, results show RBC exceedance for NWTPH‐Dx (96,800 mg/kg).

    NWTPH‐Dx concentrations were also observed at sample locations EW‐SIDEWALL‐E (184 mg/kg), 0B

    (1,090 mg/kg), 1B (44.6 mg/kg), 2B (70.2 mg/kg), and 3A (29.1 mg/kg). These locations are directly

    adjacent to the “hot spot” locations, with the exception of 3A. The NWTPH‐Dx concentrations at all

    other sample locations were non ‐detect. The laboratory analytical results are presented in Appendix A.

    Outcrop Source Removal

    Diesel has accumulated on top of a bedrock outcrop located approximately 40 feet down slope from the

    release area as indicated by soil analytical data, PID readings and site observation. Impacted soil on top

    of the rock outcrop will be excavated to provide mass removal and eliminate known potential source

    areas for future leaching of diesel. The limits of the excavation will extend approximately 4 feet upslope

    from the rock outcrop, approximately 10 feet across the width of the rock outcrop, and extend

    approximately 1 foot deep to bedrock. The limits of the excavation will be determined in the field using

    a PID and field observations. Due to the extreme site conditions, the impacted soil will be excavated by hand.

    Confirmation soil samples will be collected on the side walls of the excavation, estimated at two samples

    along the top wall and one sample on each side walls of the excavation. The floor and down slope wall

    of the excavation are anticipated to be bedrock; therefore, soil samples are not anticipated at these

    locations. Soil samples will be analyzed for diesel range organics by NWTPH‐Dx, RBDM VOCs by EPA

    8260B, and PAHs by EPA 8270D SIM.

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    Mr. Geoffrey Brown ‐ 4 ‐ March 7, 2016

    Bio‐stimulation

    AT&T proposes to use a combination of two bio ‐stimulation products to naturally degrade residual

    diesel at the Site. These products include Oil Spill Eaters International Corporation’s proprietary OSE II

    and Micro ‐Blaze® Non ‐Formulated. Micro ‐Blaze® Non ‐Formulated is a consortium of hydrocarbon degrading bacteria that will be applied to the individual release areas in a 10% solution following the

    application of OSE II. Micro ‐Blaze® Non ‐Formulated contains no surfactants or nutrients, just a

    consortium of known hydrocarbon degrading bacteria.

    AT&T proposes to use Oil Spill Eaters International Corporation’s proprietary OSE II amendment to

    breakdown residual diesel LNAPL in the subsurface. OSE II is a bio ‐catalyst that contains enzymes and

    nutrients designed to enhance the emulsification of LNAPL and stimulate hydrocarbon consuming

    bacteria to degrade hydrocarbons released in the environment. Nutrients within OSE II will increase the

    rate of biodegradation of the diesel ‐consuming bacteria present beneath the Site to remove the

    dissolved diesel. OSE II has been evaluated by the Environmental Protection Agency and is listed as an

    accepted remedial response technology for hydrocarbon releases (Environmental Protection Agency,

    2009). The California Department of Wildlife (formerly Department of Fish and Game) has licensed OSE

    II for oil spill treatment in California. Documentation of the OSE II is provided in Appendix B.

    The application of the OSE II and Micro ‐Blaze® Non ‐Formulated is proposed in three areas. The first

    application will be applied to a small trench excavated on the upgradient side of the AT&T

    communication building. This will be conducted to treat residual diesel in the base course beneath the

    building foundation. The second application will be in the release area excavation to introduce these

    solutions into the subsurface following a similar pathway as the original release. The third application will be a surface application of these solutions within the limits of the downslope excavation following

    the removal of impacted soil on top of the rock outcrop and the surface application of the soil between

    the release area and rock outcrop. Documentation of Micro ‐Blaze® Non ‐Formulated is provided in

    Appendix B. Each of these applications is discussed below.

    Building Foundation Application OSE II/Micro ‐Blaze® Non ‐Formulated will be applied hydraulically upgradient of the AT&T

    Communication building in an attempt to treat residual diesel residing in the base course beneath the

    building foundation. A small trench will be excavated along the north footing of the building for the

    application of the OSE II. The trench will be approximately 1 foot wide and 6 inches deep. Excavated material will be placed along the outside extent of the trench to form a berm. A licensed archeologist

    will be on ‐site during all ground disturbance activities. Approximately 300 gallons of the OSE II solution

    will be gravity fed into the trench at such a rate as to not overflow the trench, while maintaining a

    constant head in the trench. Absorbent pads will be placed adjacent to the exposed base course along

    the south side of the building to capture diesel that may be displaced during this procedure.

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    Mr. Geoffrey Brown ‐ 5 ‐ March 7, 2016

    Release Area Application OSE II will be applied within the limits of the release area in an effort to follow the same pathway as the

    diesel during the original release. Approximately 900 gallons of OSE II solution will be applied on top of

    the exposed bedrock in the release area excavation. The application rate will be consistent with the dye

    test conducted on February 23, 2016 to evaluate flow pathways and maintained at a rate as to not

    overflow the excavation. Absorbent pads located downslope of the excavation will be monitored and

    replaced as necessary during this task.

    Outcrop Excavation OSE II Application OSE II will be applied to the surface of the downslope outcrop excavation adjacent to the rock outcrop

    and surrounding soil. Approximately 100 gallons of OSE II solution will be applied on top of the soil in the

    area extending from the release area to the rock outcrop using a hose. The soil in this area is potentially

    impacted based on soil analytical data and site observations. The application rate should be monitored

    to prevent surface runoff, but sufficient to promote infiltration and near saturation. If the soil in the

    treatment area becomes saturated to the point surface runoff occurs, the application rate will be

    reduced. If surface water runoff continues to occur, the remaining volume of OSE II solution will be

    applied to the release area. Absorbent pads located downslope of the impacted soil area will be

    monitored and replaced as necessary during this task.

    Mixing Procedure Micro ‐Blaze® Non ‐Formulated will be mixed to a 10% solution using 5 gallons of Micro ‐Blaze to 50

    gallons of water. The water will be collected from the sample source used in the dye test, pending USFS

    approval.

    The OSE II application system will consist of a bulk mixing tank, one 55 gallon drum of OSE II, a circulation pump, and associated hoses, valves, and fittings. The application system will be powered by

    an existing onsite generator. Surface water from a nearby stream will be used to blend with the OSE II to

    make the 25:1 solution of water to OSE II, pending USFS approval. Approximately 1,375 gallons of the

    OSE II/surface water solution will be applied in and around the release area. It is anticipated that the

    OSE II/surface water solution will be prepared in 300 ‐gallon batches for application; therefore, 12

    gallons of OSE II will be mixed with 300 gallons of water to prepare the 25:1 solution.

    Surface Water Sampling

    Currently, CB&I performs a daily visual inspection of five unnamed tributaries (SW‐01, SW‐02, SW‐03, SW‐04, and SW‐05) and collects weekly surface water samples from these locations on a weekly basis.

    These surface water samples are analyzed for RBDM VOCs by EPA Method 8260B and PAHs by EPA

    Method 8270D SIM. No VOCs or PAHs have been detected in any of the surface water samples collected

    from the identified streams. The laboratory analytical results have been tabulated and presented in

    Table 2. Surface water sample locations are presented in Figure 4.

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    Mr. Geoffrey Brown ‐ 6 ‐ March 7, 2016

    Surface water samples will be collected 30 days, 90 days, and 180 days following the application of OSE

    II to monitor potential impact to the adjacent surface water streams. Surface water sampling will be

    discontinued following the 180 day sampling event if the analytical results remain below laboratory

    detection limits. Approval will be requested from ORDEQ and USFS to discontinue the sampling program

    if no VOCs or PAHs have been detected in the surface water following the 180 days of post bio ‐

    stimulation sampling.

    In the event that any RBDM VOCs and PAHs are detected in the surface water samples above the

    applicable standards, then the surface water sampling plan will be amended to collect samples further

    downstream and/or at the reservoir discharge locations. The new surface water locations and the

    number of collected samples will be approved by ORDEQ and USFS.

    Data from the sampling will be submitted to the ORDEQ and USFS in status reports. The status reports

    will provide a brief summary of the analytical results and confirm the future sampling frequency.

    Absorbent and Weir Maintenance

    After excavation of the source area, crews established a downslope catchment system including a weir

    and trenches containing absorbent booms, and absorbent pads interweaved across the exposed

    bedrock seepage areas. Crews are monitoring the absorbents daily and replacing them as needed.

    Saturated absorbents are containerized in Super Sacs and removed offsite to a landfill.

    Following application of the OSE II treatment, crews will continue to change out absorbent pads and/or

    booms along the downslope hillside on a weekly basis. In the event that no color change in the

    absorbents is observed for 30 days, then crews will remove absorbents and booms from the site and backfill the weir, trenches, and potholes. Crews will restore the site as close as possible to pre ‐

    disturbance drainage conditions.

    Site Restoration

    Release area The release area excavation and adjacent area will be restored to pre ‐excavation conditions following

    the bio ‐stimulation application. Approximately 4‐inch layer of peat moss will be applied adjacent to the

    exposed building footing and over the exposed bedrock with previously observed contact with diesel.

    The diesel readily binds with peat moss until it naturally biodegrades, preventing any residual diesel from migrating offsite. Sufficient gravel will be placed over the peat moss to restore the site to near pre ‐

    excavation grade. Clean gravel that was excavated during the initial response and temporarily

    stockpiled adjacent to the excavation will be used as fill material. Additional gravel from an offsite

    source consisting of 3/4 ‐inch minus will be applied to the excavation to restore the area to the original

    grade. Fill material will be applied in 6‐inch lifts and compacted by driving over the fill material with the

    equipment. The area will be graded to promote positive drainage away from the building.

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    Mr. Geoffrey Brown ‐ 7 ‐ March 7, 2016

    Outcrop Excavation The outcrop excavation and adjacent area will be restored to pre ‐excavation conditions following the

    bio ‐stimulation application. Approximately 4‐inch layer of peat moss will be applied adjacent to the exposed bedrock with previously observed contact with diesel. Top soil will be applied on top of the

    peat moss in 6‐inch lifts and hand compacted until the elevation of the fill material is consistent with the

    surrounding topography. Grass matting will be applied over the top soil to minimize erosion.

    Recommendation

    Please provide your written approval if this Work Plan is acceptable or let us know if you have any

    questions, comments, or revisions. If necessary, the Work Plan will be revised and resubmitted for your

    approval. Thank you for your time during our on ‐site meetings and for your responsiveness in working

    with us to develop this Plan.

    Please contact either of the undersigned if you have any questions concerning this report.

    Sincerely:

    Ronald Malec, P.G. Kent Roberts

    Incident Commander,

    Unit

    Chief

    Senior

    Operations

    Manager

    412 ‐380 ‐4484 321 ‐543 ‐1194 [email protected] [email protected]

    MF:KR:RM:lmk Attachments

    cc: Lauren Plunk (AT&T) Bryn Thoms (ORDEQ) Greg Aitken (ORDEQ) Grady McMahan (USFS) Darrin Neff (USFS) Jamie Sheahan Alonso (USFS) Penny Keen (USFS) Mark Finney (CB&I) Bryan Holmes (CB&I)

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    Tables

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    1A 1B 1C 2A 2B

    Contaminant (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)

    PID Reading (ppm) ‐‐‐ ‐‐‐ 5.4 6.4 397 2.7 1.9NWTPH‐Dx: Diesel 9,500 4,600 ND 44.6 66,400 ND 70.NWTPH‐Dx: Oil > Max 11,000 123 159 ND ND 312Benzene 0.10 300 ND ND ND ND N

    Toluene 310 28,000 ND ND ND ND N

    Ethylbenzene 0.94 1,700 ND ND ND ND N

    Xylenes 49 20,000 ND ND ND ND N

    Naphthalene 0.37 580 ND ND ND ND N

    MTBE 0.50 12,000 ND ND ND ND N

    Isopropylbenzene 280 27,000 ND ND ND ND N

    n‐Propylbenzene No Std. No Std. ND ND ND ND N1,2,4 ‐Trimethylbenzene 5.6 2,000 ND ND ND ND N1,3,5 ‐Trimethylbenzene 110 3,500 ND ND ND ND N1,2 ‐Dibromoethane (EDB) 0.00056 9 ND ND ND ND N1,2 ‐Dichloroethane (EDC) 0.013 200 ND ND ND ND N

    Table 1Soil Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐0374

    Soil Sample Analytical Results

    RBCss 2RBCsw

    1

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    Table 1Soil Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐0374

    1A 1B 1C 2A 2B

    Contaminant (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)

    Acenaphthene ‐‐‐ 21,000 ND ND NA ND NAcenaphthylene No Std. No Std. ND ND NA ND NAnthracene ‐‐‐ 110,000 ND ND NA ND NBenz(a)anthracene 2.3 24 ND ND NA ND N

    Benzo(a)pyrene 1.9 2.4 ND ND NA ND N

    Benzo(b)fluoranthene ‐‐‐ 24 ND ND NA ND NBenzo(k)fluoranthene ‐‐‐ 240 ND ND NA ND NBenzo(g,h,i)perylene No Std. No Std. ND ND NA ND NChrysene ‐‐‐ 2,400 ND ND NA ND NDibenz(a,h)anthracene ‐‐‐ 2.4 ND ND NA ND NDibenzofuran No Std. No Std. ND ND NA ND NFluoranthene ‐‐‐ 10,000 ND ND NA ND NFluorene ‐‐‐ 14,000 ND ND NA ND NIndeno(1,2,3 ‐cd)pyrene ‐‐‐ 24 ND ND NA ND N1‐Methylnaphthalene No Std. No Std. ND ND NA ND N2‐Methylnaphthalene No Std. No Std. ND ND NA ND NNaphthalene 0.37 580 ND ND NA ND N

    Phenanthrene No Std. No Std. ND ND NA ND NPyrene ‐‐‐ 7,500 ND ND NA ND N

    Soil Sample Analytical Results

    RBCss 2RBCsw

    1

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    Table 1Soil Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐0374

    3A 3B 3C 3D 4A

    Contaminant (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)

    PID Reading (ppm) ‐‐‐ ‐‐‐ 3.3 2.0 3.3 1.7 3.4NWTPH‐Dx: Diesel 9,500 4,600 29.1 ND ND ND NDNWTPH‐Dx: Oil > Max 11,000 116 ND 98.7 ND 117Benzene 0.10 300 ND ND ND ND N

    Toluene 310 28,000 ND ND ND ND N

    Ethylbenzene 0.94 1,700 ND ND ND ND N

    Xylenes 49 20,000 ND ND ND ND N

    Naphthalene 0.37 580 ND ND ND ND N

    MTBE 0.50 12,000 ND ND ND ND N

    Isopropylbenzene 280 27,000 ND ND ND ND N

    n‐Propylbenzene No Std. No Std. ND ND ND ND N1,2,4 ‐Trimethylbenzene 5.6 2,000 ND ND ND ND N1,3,5 ‐Trimethylbenzene 110 3,500 ND ND ND ND N1,2 ‐Dibromoethane (EDB) 0.00056 9 ND ND ND ND N1,2 ‐Dichloroethane (EDC) 0.013 200 ND ND ND ND N

    Soil Sample Analytical Results

    RBCss 2RBCsw

    1

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    Table 1Soil Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐0374

    3A 3B 3C 3D 4A

    Contaminant (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)

    Acenaphthene ‐‐‐ 21,000 ND ND ND ND NAcenaphthylene No Std. No Std. ND ND ND ND NAnthracene ‐‐‐ 110,000 ND ND ND ND NBenz(a)anthracene 2.3 24 ND ND ND ND N

    Benzo(a)pyrene 1.9 2.4 ND ND ND ND N

    Benzo(b)fluoranthene ‐‐‐ 24 ND ND ND ND NBenzo(k)fluoranthene ‐‐‐ 240 ND ND ND ND NBenzo(g,h,i)perylene No Std. No Std. ND ND ND ND NChrysene ‐‐‐ 2,400 ND ND ND ND NDibenz(a,h)anthracene ‐‐‐ 2.4 ND ND ND ND NDibenzofuran No Std. No Std. ND ND ND ND NFluoranthene ‐‐‐ 10,000 ND ND ND ND NFluorene ‐‐‐ 14,000 ND ND ND ND NIndeno(1,2,3 ‐cd)pyrene ‐‐‐ 24 ND ND ND ND N1‐Methylnaphthalene No Std. No Std. ND ND ND ND N2‐Methylnaphthalene No Std. No Std. ND ND ND ND NNaphthalene 0.37 580 ND ND ND ND N

    Phenanthrene No Std. No Std. ND ND ND ND NPyrene ‐‐‐ 7,500 ND ND ND ND N

    Soil Sample Analytical Results

    RBCss 2RBCsw

    1

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    Table 1Soil Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐0374

    Ex Side4D 0A 0B 0C S

    Contaminant (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)

    PID Reading (ppm) ‐‐‐ ‐‐‐ 1.2 0.9 10.5 36.8 5.0NWTPH‐Dx: Diesel 9,500 4,600 ND ND 1,090 9,430 NDNWTPH‐Dx: Oil > Max 11,000 ND ND ND ND NBenzene 0.10 300 ND ND ND 0.161 ND

    Toluene 310 28,000 ND ND 0.224 2.93 ND

    Ethylbenzene 0.94 1,700 ND ND 0.200 3.70 ND

    Xylenes 49 20,000 ND ND 1.04 20.6 ND

    Naphthalene 0.37 580 ND ND ND 2.15 ND

    MTBE 0.50 12,000 ND ND ND ND N

    Isopropylbenzene 280 27,000 ND ND ND 1.03 ND

    n‐Propylbenzene No Std. No Std. ND ND 0.162 3.82 ND1,2,4 ‐Trimethylbenzene 5.6 2,000 ND ND 0.755 19.9 ND1,3,5 ‐Trimethylbenzene 110 3,500 ND ND 0.264 6.59 ND1,2 ‐Dibromoethane (EDB) 0.00056 9 ND ND ND ND N1,2 ‐Dichloroethane (EDC) 0.013 200 ND ND ND ND N

    Soil Sample Analytical Results

    RBCss 2RBCsw

    1

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    Table 1Soil Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐0374

    Ex Side4D 0A 0B 0C S

    Contaminant (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)

    Acenaphthene ‐‐‐ 21,000 ND ND ND ND NAcenaphthylene No Std. No Std. ND ND ND ND NAnthracene ‐‐‐ 110,000 ND ND ND ND NBenz(a)anthracene 2.3 24 ND ND ND ND N

    Benzo(a)pyrene 1.9 2.4 ND ND ND ND N

    Benzo(b)fluoranthene ‐‐‐ 24 ND ND ND ND NBenzo(k)fluoranthene ‐‐‐ 240 ND ND ND ND NBenzo(g,h,i)perylene No Std. No Std. ND ND ND ND NChrysene ‐‐‐ 2,400 ND ND ND ND NDibenz(a,h)anthracene ‐‐‐ 2.4 ND ND ND ND NDibenzofuran No Std. No Std. ND ND 0.0620 0.376 NDFluoranthene ‐‐‐ 10,000 ND ND ND ND NFluorene ‐‐‐ 14,000 ND ND ND 0.454 NDIndeno(1,2,3 ‐cd)pyrene ‐‐‐ 24 ND ND ND ND N1‐Methylnaphthalene No Std. No Std. ND ND 0.114 3.29 ND2‐Methylnaphthalene No Std. No Std. ND ND 0.155 5.58 NDNaphthalene 0.37 580 ND ND ND 2.08 ND

    Phenanthrene No Std. No Std. ND ND 0.0489 0.740 NDPyrene ‐‐‐ 7,500 ND ND 0.0411 0.389 ND

    RBCsw 1

    Soil Sample Analytical Results

    RBCss 2

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    Table 1Soil Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐0374

    Notes:

    Bold = Soil Sample analytical results exceeded applicable standard.

    mg/kg = milligrams per kilogram.

    MTBE = Methyl tert ‐butyl ether

    No Std. = No standard listed in Risk Based Concentrations for Individual Chemicals State of Oregon Department of Environmental Q

    PID = Photoionization detector readings are reported in parts per million (ppm).

    Soil samples were collected on February 26, 2016.

    ND = Concentration not detected at the laboratory method detection limit.NA = Not Analyzed

    Analytical Results were compared to the Oregon standards for the Soils Leaching to Groundwater (RCBsw) Urban Residential and tDermal Contact and Inhulation (RCBss) Construction Worker. The lowere of the two values was selected for comparison to the ana

    ‐‐‐ = All RBC values for indirect pathways that exceed a limit (Csat, S, or Pv) are removed from the Risk‐Based Concentrations For In

    > Max = The constituent RBC for this pathway is calculated as greater than 1,000,000 mg/kg or 1,000,000 mg/L. Therefore, this subthis scenario.

    2 Risk‐Based Concentrations For Individual Chemicals (State of Oregon Department of Environmental Quality), Soils Leaching to SoiInhalation (RBCss), Construction Worker dated November 1, 2015.

    1 Risk‐Based Concentrations For Individual Chemicals (State of Oregon Department of Environmental Quality), Soils Leaching to Grdated November 1, 2015.

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    SW‐01 Unnamed Tributary SW ‐01 SW ‐01 SW ‐01 SW ‐01 SW ‐01

    02/19/16 02/21/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    NWTPH‐Dx: Diesel 100 ND NA NA ‐‐ ‐‐

    NWTPH‐Dx: Oil 300 ND NA NA ‐‐ ‐‐

    Benzene 2.0 ND ND ND ‐‐ ‐‐

    Toluene 4,400 ND ND ND ‐‐ ‐‐

    Ethylbenzene 6.7 ND ND ND ‐‐ ‐‐ Xylenes 710 ND ND ND ‐‐ ‐‐ Naphthalene 0.78 ND ND ND ‐‐ ‐‐

    MTBE 64 ND ND ND ‐‐ ‐‐

    Isopropylbenzene 1,800 ND ND ND ‐‐ ‐‐

    n ‐Propylbenzene No Std. ND ND ND ‐‐ ‐‐

    1,2,4 ‐Trimethylbenzene 54 ND ND ND ‐‐ ‐‐

    1,3,5 ‐Trimethylbenzene 500 ND ND ND ‐‐ ‐‐ 1,2 ‐Dibromoethane (EDB) 0.034 ND ND ND ‐‐ ‐‐

    1,2 ‐Dichloroethane (EDC) 0.78 ND ND ND ‐‐ ‐‐

    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    Water Sample Analytical Results

    RBCtw 1

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐01 Unnamed Tributary SW ‐01 SW ‐01 SW ‐01 SW ‐01 SW ‐01

    02/19/16 02/21/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    Acenaphthene 2,400 ND ND ND ‐‐ ‐‐

    Acenaphthylene No Std. ND ND ND ‐‐ ‐‐

    Anthracene ‐‐‐ ND ND ND ‐‐ ‐‐

    Benz(a)anthracene 0.043 ND ND ND ‐‐ ‐‐

    Benzo(a)pyrene 0.011 ND ND ND ‐‐ ‐‐ Benzo(b)fluoranthene 0.11 ND ND ND ‐‐ ‐‐ Benzo(k)fluoranthene ‐‐‐ ND ND ND ‐‐ ‐‐

    Benzo(g,h,i)perylene No Std. ND ND ND ‐‐ ‐‐

    Chrysene ‐‐‐ ND ND ND ‐‐ ‐‐

    Dibenz(a,h)anthracene 0.011 ND ND ND ‐‐ ‐‐

    Dibenzofuran No Std. ND ND ND ‐‐ ‐‐

    Fluoranthene ‐‐‐ ND ND ND ‐‐ ‐‐ Fluorene 1,400 ND ND ND ‐‐ ‐‐ Indeno(1,2,3 ‐cd)pyrene 0.11 ND ND ND ‐‐ ‐‐

    1‐Methylnaphthalene No Std. ND ND ND ‐‐ ‐‐

    2‐Methylnaphthalene No Std. ND ND ND ‐‐ ‐‐

    Naphthalene 0.78 ND ND ND ‐‐ ‐‐

    Phenanthrene No Std. ND ND ND ‐‐ ‐‐ Pyrene ‐‐‐ ND ND ND ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐02Unnamed Tributary SW ‐02 SW ‐02 SW ‐02 SW ‐02 SW ‐02

    02/19/16 02/21/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    NWTPH‐Dx: Diesel 100 ND NA NA ‐‐ ‐‐

    NWTPH‐Dx: Oil 300 ND NA NA ‐‐ ‐‐

    Benzene 2.0 ND ND ND ‐‐ ‐‐

    Toluene 4,400 ND ND ND ‐‐ ‐‐

    Ethylbenzene 6.7 ND ND ND ‐‐ ‐‐ Xylenes 710 ND ND ND ‐‐ ‐‐ Naphthalene 0.78 ND ND ND ‐‐ ‐‐

    MTBE 64 ND ND ND ‐‐ ‐‐

    Isopropylbenzene 1,800 ND ND ND ‐‐ ‐‐

    n ‐Propylbenzene No Std. ND ND ND ‐‐ ‐‐

    1,2,4 ‐Trimethylbenzene 54 ND ND ND ‐‐ ‐‐

    1,3,5 ‐Trimethylbenzene 500 ND ND ND ‐‐ ‐‐ 1,2 ‐Dibromoethane (EDB) 0.034 ND ND ND ‐‐ ‐‐

    1,2 ‐Dichloroethane (EDC) 0.78 ND ND ND ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐02Unnamed Tributary SW ‐02 SW ‐02 SW ‐02 SW ‐02 SW ‐02

    02/19/16 02/21/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    Acenaphthene 2,400 ND ND ND ‐‐ ‐‐

    Acenaphthylene No Std. ND ND ND ‐‐ ‐‐

    Anthracene ‐‐‐ ND ND ND ‐‐ ‐‐

    Benz(a)anthracene 0.043 ND ND ND ‐‐ ‐‐

    Benzo(a)pyrene 0.011 ND ND ND ‐‐ ‐‐ Benzo(b)fluoranthene 0.11 ND ND ND ‐‐ ‐‐ Benzo(k)fluoranthene ‐‐‐ ND ND ND ‐‐ ‐‐

    Benzo(g,h,i)perylene No Std. ND ND ND ‐‐ ‐‐

    Chrysene ‐‐‐ ND ND ND ‐‐ ‐‐

    Dibenz(a,h)anthracene 0.011 ND ND ND ‐‐ ‐‐

    Dibenzofuran No Std. ND ND ND ‐‐ ‐‐

    Fluoranthene ‐‐‐ ND ND ND ‐‐ ‐‐ Fluorene 1,400 ND ND ND ‐‐ ‐‐ Indeno(1,2,3 ‐cd)pyrene 0.11 ND ND ND ‐‐ ‐‐

    1‐Methylnaphthalene No Std. ND ND ND ‐‐ ‐‐

    2‐Methylnaphthalene No Std. ND ND ND ‐‐ ‐‐

    Naphthalene 0.78 ND ND ND ‐‐ ‐‐

    Phenanthrene No Std. ND ND ND ‐‐ ‐‐ Pyrene ‐‐‐ ND ND ND ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐03Unnamed Tributary SW ‐03 SW ‐03 SW ‐03 SW ‐03 SW ‐03

    02/19/16 02/21/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    NWTPH‐Dx: Diesel 100 ND NA NA ‐‐ ‐‐

    NWTPH‐Dx: Oil 300 ND NA NA ‐‐ ‐‐

    Benzene 2.0 ND ND ND ‐‐ ‐‐

    Toluene 4,400 ND ND ND ‐‐ ‐‐

    Ethylbenzene 6.7 ND ND ND ‐‐ ‐‐ Xylenes 710 ND ND ND ‐‐ ‐‐ Naphthalene 0.78 ND ND ND ‐‐ ‐‐

    MTBE 64 ND ND ND ‐‐ ‐‐

    Isopropylbenzene 1,800 ND ND ND ‐‐ ‐‐

    n ‐Propylbenzene No Std. ND ND ND ‐‐ ‐‐

    1,2,4 ‐Trimethylbenzene 54 ND ND ND ‐‐ ‐‐

    1,3,5 ‐Trimethylbenzene 500 ND ND ND ‐‐ ‐‐ 1,2 ‐Dibromoethane (EDB) 0.034 ND ND ND ‐‐ ‐‐

    1,2 ‐Dichloroethane (EDC) 0.78 ND ND ND ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐03Unnamed Tributary SW ‐03 SW ‐03 SW ‐03 SW ‐03 SW ‐03

    02/19/16 02/21/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    Acenaphthene 2,400 ND ND ND ‐‐ ‐‐

    Acenaphthylene No Std. ND ND ND ‐‐ ‐‐

    Anthracene ‐‐‐ ND ND ND ‐‐ ‐‐

    Benz(a)anthracene 0.043 ND ND ND ‐‐ ‐‐

    Benzo(a)pyrene 0.011 ND ND ND ‐‐ ‐‐ Benzo(b)fluoranthene 0.11 ND ND ND ‐‐ ‐‐ Benzo(k)fluoranthene ‐‐‐ ND ND ND ‐‐ ‐‐

    Benzo(g,h,i)perylene No Std. ND ND ND ‐‐ ‐‐

    Chrysene ‐‐‐ ND ND ND ‐‐ ‐‐

    Dibenz(a,h)anthracene 0.011 ND ND ND ‐‐ ‐‐

    Dibenzofuran No Std. ND ND ND ‐‐ ‐‐

    Fluoranthene ‐‐‐ ND ND ND ‐‐ ‐‐ Fluorene 1,400 ND ND ND ‐‐ ‐‐ Indeno(1,2,3 ‐cd)pyrene 0.11 ND ND ND ‐‐ ‐‐

    1‐Methylnaphthalene No Std. ND ND ND ‐‐ ‐‐

    2‐Methylnaphthalene No Std. ND ND ND ‐‐ ‐‐

    Naphthalene 0.78 ND ND ND ‐‐ ‐‐

    Phenanthrene No Std. ND ND ND ‐‐ ‐‐ Pyrene ‐‐‐ ND ND ND ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐04Unnamed Tributary SW ‐04 SW ‐04 SW ‐04 SW ‐04 SW ‐04

    02/19/16 02/21/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    NWTPH‐Dx: Diesel 100 ND NA NA ‐‐ ‐‐

    NWTPH‐Dx: Oil 300 ND NA NA ‐‐ ‐‐

    Benzene 2.0 ND ND ND ‐‐ ‐‐

    Toluene 4,400 ND ND ND ‐‐ ‐‐

    Ethylbenzene 6.7 ND ND ND ‐‐ ‐‐ Xylenes 710 ND ND ND ‐‐ ‐‐ Naphthalene 0.78 ND ND ND ‐‐ ‐‐

    MTBE 64 ND ND ND ‐‐ ‐‐

    Isopropylbenzene 1,800 ND ND ND ‐‐ ‐‐

    n ‐Propylbenzene No Std. ND ND ND ‐‐ ‐‐

    1,2,4 ‐Trimethylbenzene 54 ND ND ND ‐‐ ‐‐

    1,3,5 ‐Trimethylbenzene 500 ND ND ND ‐‐ ‐‐ 1,2 ‐Dibromoethane (EDB) 0.034 ND ND ND ‐‐ ‐‐

    1,2 ‐Dichloroethane (EDC) 0.78 ND ND ND ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐04Unnamed Tributary SW ‐04 SW ‐04 SW ‐04 SW ‐04 SW ‐04

    02/19/16 02/21/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    Acenaphthene 2,400 ND ND ND ‐‐ ‐‐

    Acenaphthylene No Std. ND ND ND ‐‐ ‐‐

    Anthracene ‐‐‐ ND ND ND ‐‐ ‐‐

    Benz(a)anthracene 0.043 ND ND ND ‐‐ ‐‐

    Benzo(a)pyrene 0.011 ND ND ND ‐‐ ‐‐ Benzo(b)fluoranthene 0.11 ND ND ND ‐‐ ‐‐ Benzo(k)fluoranthene ‐‐‐ ND ND ND ‐‐ ‐‐

    Benzo(g,h,i)perylene No Std. ND ND ND ‐‐ ‐‐

    Chrysene ‐‐‐ ND ND ND ‐‐ ‐‐

    Dibenz(a,h)anthracene 0.011 ND ND ND ‐‐ ‐‐

    Dibenzofuran No Std. ND ND ND ‐‐ ‐‐

    Fluoranthene ‐‐‐ ND ND ND ‐‐ ‐‐ Fluorene 1,400 ND ND ND ‐‐ ‐‐ Indeno(1,2,3 ‐cd)pyrene 0.11 ND ND ND ‐‐ ‐‐

    1‐Methylnaphthalene No Std. ND ND ND ‐‐ ‐‐

    2‐Methylnaphthalene No Std. ND ND ND ‐‐ ‐‐

    Naphthalene 0.78 ND ND ND ‐‐ ‐‐

    Phenanthrene No Std. ND ND ND ‐‐ ‐‐ Pyrene ‐‐‐ ND ND ND ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐05Unnamed Tributary SW ‐05 SW ‐05 SW ‐05 SW ‐05 SW ‐05

    02/25/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    Benzene 2.0 ND ND ‐‐ ‐‐ ‐‐

    Toluene 4,400 ND ND ‐‐ ‐‐ ‐‐

    Ethylbenzene 6.7 ND ND ‐‐ ‐‐ ‐‐

    Xylenes 710 ND ND ‐‐ ‐‐ ‐‐

    Naphthalene 0.78 ND ND ‐‐ ‐‐ ‐‐ MTBE 64 ND ND ‐‐ ‐‐ ‐‐ Isopropylbenzene 1,800 ND ND ‐‐ ‐‐ ‐‐

    n ‐Propylbenzene No Std. ND ND ‐‐ ‐‐ ‐‐

    1,2,4 ‐Trimethylbenzene 54 ND ND ‐‐ ‐‐ ‐‐

    1,3,5 ‐Trimethylbenzene 500 ND ND ‐‐ ‐‐ ‐‐

    1,2 ‐Dibromoethane (EDB) 0.034 ND ND ‐‐ ‐‐ ‐‐

    1,2 ‐Dichloroethane (EDC) 0.78 ND ND ‐‐ ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    SW‐05Unnamed Tributary SW ‐05 SW ‐05 SW ‐05 SW ‐05 SW ‐05

    02/25/16 02/28/16

    Contaminant (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L) (μ g/L)

    Acenaphthene 2,400 ND ND ‐‐ ‐‐ ‐‐

    Acenaphthylene No Std. ND ND ‐‐ ‐‐ ‐‐

    Anthracene ‐‐‐ ND ND ‐‐ ‐‐ ‐‐

    Benz(a)anthracene 0.043 ND ND ‐‐ ‐‐ ‐‐

    Benzo(a)pyrene 0.011 ND ND ‐‐ ‐‐ ‐‐ Benzo(b)fluoranthene 0.11 ND ND ‐‐ ‐‐ ‐‐ Benzo(k)fluoranthene ‐‐‐ ND ND ‐‐ ‐‐ ‐‐

    Benzo(g,h,i)perylene No Std. ND ND ‐‐ ‐‐ ‐‐

    Chrysene ‐‐‐ ND ND ‐‐ ‐‐ ‐‐

    Dibenz(a,h)anthracene 0.011 ND ND ‐‐ ‐‐ ‐‐

    Dibenzofuran No Std. ND ND ‐‐ ‐‐ ‐‐

    Fluoranthene ‐‐‐ ND ND ‐‐ ‐‐ ‐‐ Fluorene 1,400 ND ND ‐‐ ‐‐ ‐‐ Indeno(1,2,3 ‐cd)pyrene 0.11 ND ND ‐‐ ‐‐ ‐‐

    1‐Methylnaphthalene No Std. ND ND ‐‐ ‐‐ ‐‐

    2‐Methylnaphthalene No Std. ND ND ‐‐ ‐‐ ‐‐

    Naphthalene 0.78 ND ND ‐‐ ‐‐ ‐‐

    Phenanthrene No Std. ND ND ‐‐ ‐‐ ‐‐ Pyrene ‐‐‐ ND ND ‐‐ ‐‐ ‐‐

    Water Sample Analytical Results

    RBCtw

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    Table 2Water Sample Analytical Results

    AT&T Hall Ridge

    Willamette National ForestDetroit, Oregon

    Oregon Emergency Response System Report No. 2016 ‐ 0374

    Notes:

    (μ g/L) = micrograms per liter.

    MTBE = Methyl tert ‐butyl ether

    No Std. = No Standard Listed

    ND = Concentration not detected at the laboratory reporting limit.

    NA = Not Analyzed ‐‐‐ = All RBC values for indirect pathways that exceed a limit (Csat, S, or Pv) are removed from the Risk‐Based Concentrations Fo

    1 Risk‐Based Concentrations For Individual Chemicals (State of Oregon Department of Environmental Quality), Groundwater Ing

    (RBCtw), Urban Residential dated November 1, 2015.

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    Figures

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    Appendix A

    Draft Laboratory Analytical Results

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    12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Apex Labs

    NRC-CB&I

    RE: AT&T Hall Ridge / 156319

    Portland, OR 972176211 N Ensign St

    Ron Malec

    Enclosed are the results of analyses for work order A6B0900, which was received by the laboratory on2/27/2016 at 9:15:00AM.

    Thank you for using Apex Labs. We appreciate your business and strive to provide the highest qualityservices to the environmental industry.

    If you have any questions concerning this report or the services we offer , please feel free to contact me byemail at: [email protected], or by phone at 503-718-2323.

    Sunday, February 28, 2016

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    Diesel and/or Oil Hydrocarbons by NWTPH-Dx

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil1A (A6B0900-01) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 13:53 ND --- 28.6F-17Oil "" ""123 --- 57.2

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 88 %

    Matrix: Soil1B (A6B0900-02) Batch: 6020836

    F-17Diesel NWTPH-Dxmg/kg dry 02/27/16 14:33144.6 --- 32.2F-17Oil "" ""159 --- 64.3

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 90 %

    Matrix: Soil1C (A6B0900-03) Batch: 6020835

    Diesel NWTPH-Dxmg/kg dry 02/27/16 13:535066400 --- 2040

    "" "Oil " ND --- 4080

    S-01"Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: %

    Matrix: Soil2A (A6B0900-04) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 15:12 ND --- 26.1

    "" "Oil " ND --- 52.2

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 90 %

    Matrix: Soil2B (A6B0900-05) Batch: 6020836

    F-17Diesel NWTPH-Dxmg/kg dry 02/27/16 15:32170.2 --- 35.9F-17Oil "" ""312 --- 71.8

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 83 %

    Matrix: Soil2C (A6B0900-06) Batch: 6020835

    Diesel NWTPH-Dxmg/kg dry 02/27/16 14:335096800 --- 2490

    "" "Oil " ND --- 4970

    S-01"Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: %

    Matrix: Soil2D (A6B0900-07) Batch: 6020836

    NWTPH-Dxmg/kg dry 5Diesel 02/27/16 16:12 ND --- 180F-17Oil "" ""606 --- 360

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 84 %

    Matrix: Soil3A (A6B0900-08) Batch: 6020836

    F-17Diesel NWTPH-Dxmg/kg dry 02/27/16 16:32129.1 --- 27.2F-17Oil "" ""116 --- 54.4

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 90 %

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    Diesel and/or Oil Hydrocarbons by NWTPH-Dx

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil3B (A6B0900-09) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 17:12 ND --- 25.7

    "" "Oil " ND --- 51.5

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 92 %

    Matrix: Soil3C (A6B0900-10) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 17:31 ND --- 27.0F-17Oil "" ""98.7 --- 54.0

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 90 %

    Matrix: Soil3D (A6B0900-11) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 17:12 ND --- 27.6

    "" "Oil " ND --- 55.3

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 90 %

    Matrix: Soil4A (A6B0900-12) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 17:31 ND --- 29.8F-17Oil "" ""117 --- 59.6

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 91 %

    Matrix: Soil4B (A6B0900-13) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 14:52 ND --- 25.0

    "" "Oil " ND --- 50.0

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 94 %

    Matrix: Soil4C (A6B0900-14RE1) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 15:12 ND --- 28.9F-17Oil "" ""87.2 --- 57.7

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 95 %

    Matrix: Soil4D (A6B0900-15) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 15:32 ND --- 25.0

    "" "Oil " ND --- 50.0

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 94 %

    Matrix: Soil0A (A6B0900-16) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 12:29 ND --- 34.5

    "" "Oil " ND --- 69.1

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 90 %

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    Diesel and/or Oil Hydrocarbons by NWTPH-Dx

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil0B (A6B0900-17) Batch: 6020836

    Diesel NWTPH-Dxmg/kg dry 02/27/16 15:5211090 --- 33.4

    "" "Oil " ND --- 66.8

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 99 %

    Matrix: Soil0C (A6B0900-18) Batch: 6020836

    Diesel NWTPH-Dxmg/kg dry 02/27/16 16:3259430 --- 186"" "Oil " ND --- 372

    S-05"Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 137 %

    Matrix: SoilEx Sidewall S (A6B0900-19) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 12:49 ND --- 25.0

    "" "Oil " ND --- 50.0

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 95 %

    Matrix: SoilEx Sidewall W (A6B0900-20) Batch: 6020836

    NWTPH-Dxmg/kg dry 1Diesel 02/27/16 12:49 ND --- 26.7

    "" "Oil " ND --- 53.5

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 95 %

    Matrix: SoilEx Sidewall E (A6B0900-21) Batch: 6020836

    Diesel NWTPH-Dxmg/kg dry 02/27/16 16:521184 --- 25.0

    "" "Oil " ND --- 50.0

    "Surrogate: o-Terphenyl (Surr) Limits: 50-150 % "" Recovery: 94 %

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil1A (A6B0900-01) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 13:54 ND --- 0.0217

    "" "Toluene " ND --- 0.108

    "" "Ethylbenzene " ND --- 0.0542

    "" "Xylenes, total " ND --- 0.163

    "" " Naphthalene " ND --- 0.217

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.108

    "" "Isopropylbenzene " ND --- 0.108

    "" "n-Propylbenzene " ND --- 0.0542

    "" "1,2,4-Trimethylbenzene " ND --- 0.108

    "" "1,3,5-Trimethylbenzene " ND --- 0.108

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0542

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0542

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 106 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 103 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 100 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 97 %

    Matrix: Soil1B (A6B0900-02) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 14:51 ND --- 0.0272

    "" "Toluene " ND --- 0.136

    "" "Ethylbenzene " ND --- 0.0680

    "" "Xylenes, total " ND --- 0.204

    "" " Naphthalene " ND --- 0.272

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.136

    "" "Isopropylbenzene " ND --- 0.136

    "" "n-Propylbenzene " ND --- 0.0680

    "" "1,2,4-Trimethylbenzene " ND --- 0.136

    "" "1,3,5-Trimethylbenzene " ND --- 0.136

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0680

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0680

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 104 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 102 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 100 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 98 %

    Matrix: Soil2A (A6B0900-04) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 15:20 ND --- 0.0162

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil2A (A6B0900-04) Batch: 6020833

    5035/8260Bmg/kg dry 50Toluene " ND --- 0.0812

    "" "Ethylbenzene " ND --- 0.0406

    "" "Xylenes, total " ND --- 0.122

    "" " Naphthalene " ND --- 0.162

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0812

    "" "Isopropylbenzene " ND --- 0.0812

    "" "n-Propylbenzene " ND --- 0.0406

    "" "1,2,4-Trimethylbenzene " ND --- 0.0812

    "" "1,3,5-Trimethylbenzene " ND --- 0.0812

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0406

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0406

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 109 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 104 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 99 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 96 %

    Matrix: Soil2B (A6B0900-05) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 15:48 ND --- 0.0353

    "" "Toluene " ND --- 0.177

    "" "Ethylbenzene " ND --- 0.0883

    "" "Xylenes, total " ND --- 0.265

    "" " Naphthalene " ND --- 0.353

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.177

    "" "Isopropylbenzene " ND --- 0.177

    "" "n-Propylbenzene " ND --- 0.0883

    "" "1,2,4-Trimethylbenzene " ND --- 0.177

    "" "1,3,5-Trimethylbenzene " ND --- 0.177

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0883

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0883

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 105 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 102 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 99 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 95 %

    Matrix: Soil2D (A6B0900-07) Batch: 6020833

    Benzene 5035/8260Bmg/kg dry 02/27/16 16:16500.0449 --- 0.0391

    Toluene "" ""0.887 --- 0.195

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil2D (A6B0900-07) Batch: 6020833

    Ethylbenzene 5035/8260Bmg/kg dry "500.832 --- 0.0976

    Xylenes, total "" ""4.74 --- 0.293

    "" " Naphthalene " ND --- 0.391

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.195

    "" "Isopropylbenzene " ND --- 0.195

    n-Propylbenzene "" ""0.642 --- 0.09761,2,4-Trimethylbenzene "" ""3.53 --- 0.195

    1,3,5-Trimethylbenzene "" ""1.04 --- 0.195

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0976

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0976

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 108 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 103 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 93 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 96 %

    Matrix: Soil3A (A6B0900-08) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 16:45 ND --- 0.0216

    "" "Toluene " ND --- 0.108

    "" "Ethylbenzene " ND --- 0.0539

    "" "Xylenes, total " ND --- 0.162

    "" " Naphthalene " ND --- 0.216

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.108

    "" "Isopropylbenzene " ND --- 0.108

    "" "n-Propylbenzene " ND --- 0.0539

    "" "1,2,4-Trimethylbenzene " ND --- 0.108

    "" "1,3,5-Trimethylbenzene " ND --- 0.108

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0539

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0539

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 105 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 102 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 100 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 97 %

    Matrix: Soil3B (A6B0900-09) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 17:13 ND --- 0.0160

    "" "Toluene " ND --- 0.0801

    "" "Ethylbenzene " ND --- 0.0400

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil3B (A6B0900-09) Batch: 6020833

    5035/8260Bmg/kg dry 50Xylenes, total " ND --- 0.120

    "" " Naphthalene " ND --- 0.160

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0801

    "" "Isopropylbenzene " ND --- 0.0801

    "" "n-Propylbenzene " ND --- 0.0400

    "" "1,2,4-Trimethylbenzene " ND --- 0.0801

    "" "1,3,5-Trimethylbenzene " ND --- 0.0801

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0400

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0400

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 108 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 103 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 100 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 93 %

    Matrix: Soil3C (A6B0900-10) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 17:41 ND --- 0.0156

    "" "Toluene " ND --- 0.0782

    "" "Ethylbenzene " ND --- 0.0391

    "" "Xylenes, total " ND --- 0.117

    "" " Naphthalene " ND --- 0.156

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0782

    "" "Isopropylbenzene " ND --- 0.0782

    "" "n-Propylbenzene " ND --- 0.0391

    "" "1,2,4-Trimethylbenzene " ND --- 0.0782

    "" "1,3,5-Trimethylbenzene " ND --- 0.0782

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0391

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0391

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 106 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 103 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 101 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 93 %

    Matrix: Soil3D (A6B0900-11) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 18:10 ND --- 0.0199

    "" "Toluene " ND --- 0.0994

    "" "Ethylbenzene " ND --- 0.0497

    "" "Xylenes, total " ND --- 0.149

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil3D (A6B0900-11) Batch: 6020833

    5035/8260Bmg/kg dry 50 Naphthalene " ND --- 0.199

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0994

    "" "Isopropylbenzene " ND --- 0.0994

    "" "n-Propylbenzene " ND --- 0.0497

    "" "1,2,4-Trimethylbenzene " ND --- 0.0994

    "" "1,3,5-Trimethylbenzene " ND --- 0.0994

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0497

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0497

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 104 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 102 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 99 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 95 %

    Matrix: Soil4A (A6B0900-12) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 18:38 ND --- 0.0205

    "" "Toluene " ND --- 0.103

    "" "Ethylbenzene " ND --- 0.0513

    "" "Xylenes, total " ND --- 0.154

    "" " Naphthalene " ND --- 0.205

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.103

    "" "Isopropylbenzene " ND --- 0.103

    "" "n-Propylbenzene " ND --- 0.0513

    "" "1,2,4-Trimethylbenzene " ND --- 0.103

    "" "1,3,5-Trimethylbenzene " ND --- 0.103

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0513

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0513

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 105 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 102 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 101 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 96 %

    Matrix: Soil4B (A6B0900-13) Batch: 6020833

    5035/8260Bmg/kg dry 50Benzene 02/27/16 19:07 ND --- 0.0162

    "" "Toluene " ND --- 0.0809

    "" "Ethylbenzene " ND --- 0.0404

    "" "Xylenes, total " ND --- 0.121

    "" " Naphthalene " ND --- 0.162

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil4B (A6B0900-13) Batch: 6020833

    5035/8260Bmg/kg dry 50Methyl tert-butyl ether (MTBE) " ND --- 0.0809

    "" "Isopropylbenzene " ND --- 0.0809

    "" "n-Propylbenzene " ND --- 0.0404

    "" "1,2,4-Trimethylbenzene " ND --- 0.0809

    "" "1,3,5-Trimethylbenzene " ND --- 0.0809

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0404

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0404

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 107 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 102 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 100 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 98 %

    Matrix: Soil4C (A6B0900-14) Batch: 6020834

    5035/8260Bmg/kg dry 50Benzene 02/27/16 14:15 ND --- 0.0140

    "" "Toluene " ND --- 0.0702

    "" "Ethylbenzene " ND --- 0.0351

    "" "Xylenes, total " ND --- 0.105

    "" " Naphthalene " ND --- 0.140

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0702

    "" "Isopropylbenzene " ND --- 0.0702

    "" "n-Propylbenzene " ND --- 0.0351

    "" "1,2,4-Trimethylbenzene " ND --- 0.0702

    "" "1,3,5-Trimethylbenzene " ND --- 0.0702

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0351

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0351

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 97 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 93 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 97 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 97 %

    Matrix: Soil4D (A6B0900-15) Batch: 6020834

    5035/8260Bmg/kg dry 50Benzene 02/27/16 14:41 ND --- 0.00983

    "" "Toluene " ND --- 0.0491

    "" "Ethylbenzene " ND --- 0.0246

    "" "Xylenes, total " ND --- 0.0737

    "" " Naphthalene " ND --- 0.0983

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0491

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

    Page 11 of

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  • 8/19/2019 AT&T Hall Ridge Work Plan 03-07-2016

    45/187

    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil0B (A6B0900-17) Batch: 6020834

    n-Propylbenzene 5035/8260Bmg/kg dry "500.162 --- 0.0680

    1,2,4-Trimethylbenzene "" ""0.755 --- 0.136

    1,3,5-Trimethylbenzene "" ""0.264 --- 0.136

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0680

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0680

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 94 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 91 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 96 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 98 %

    Matrix: Soil0C (A6B0900-18) Batch: 6020834

    Benzene 5035/8260Bmg/kg dry 02/27/16 16:29500.161 --- 0.0336

    Toluene "" ""2.93 --- 0.168

    Ethylbenzene "" ""3.70 --- 0.0840

    Xylenes, total "" ""20.6 --- 0.252M-04Naphthalene "" ""2.15 --- 0.336

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.168

    Isopropylbenzene "" ""1.03 --- 0.168

    n-Propylbenzene "" ""3.82 --- 0.08401,2,4-Trimethylbenzene "" ""19.9 --- 0.168

    1,3,5-Trimethylbenzene "" ""6.59 --- 0.168

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0840

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0840

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 97 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 93 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 101 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 98 %

    Matrix: SoilEx Sidewall S (A6B0900-19) Batch: 6020834

    5035/8260Bmg/kg dry 50Benzene 02/27/16 16:56 ND --- 0.00773

    "" "Toluene " ND --- 0.0386

    "" "Ethylbenzene " ND --- 0.0193

    "" "Xylenes, total " ND --- 0.0580

    "" " Naphthalene " ND --- 0.0773

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0386

    "" "Isopropylbenzene " ND --- 0.0386

    "" "n-Propylbenzene " ND --- 0.0193

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: SoilEx Sidewall S (A6B0900-19) Batch: 6020834

    5035/8260Bmg/kg dry 501,2,4-Trimethylbenzene " ND --- 0.0386

    "" "1,3,5-Trimethylbenzene " ND --- 0.0386

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0193

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0193

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 94 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 91 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 96 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 97 %

    Matrix: SoilEx Sidewall W (A6B0900-20) Batch: 6020834

    5035/8260Bmg/kg dry 50Benzene 02/27/16 17:22 ND --- 0.0119

    "" "Toluene " ND --- 0.0594

    "" "Ethylbenzene " ND --- 0.0297

    "" "Xylenes, total " ND --- 0.0890

    "" " Naphthalene " ND --- 0.119

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0594

    "" "Isopropylbenzene " ND --- 0.0594

    "" "n-Propylbenzene " ND --- 0.0297

    "" "1,2,4-Trimethylbenzene " ND --- 0.0594

    "" "1,3,5-Trimethylbenzene " ND --- 0.0594

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0297

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0297

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 94 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 92 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 96 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 98 %

    Matrix: SoilEx Sidewall E (A6B0900-21) Batch: 6020834

    5035/8260Bmg/kg dry 50Benzene 02/27/16 17:49 ND --- 0.00717

    "" "Toluene " ND --- 0.0358

    "" "Ethylbenzene " ND --- 0.0179

    "" "Xylenes, total " ND --- 0.0538

    "" " Naphthalene " ND --- 0.0717

    "" "Methyl tert-butyl ether (MTBE) " ND --- 0.0358

    "" "Isopropylbenzene " ND --- 0.0358

    "" "n-Propylbenzene " ND --- 0.0179

    "" "1,2,4-Trimethylbenzene " ND --- 0.0358

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    RBDM Compounds (BTEX+) by EPA 8260B

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: SoilEx Sidewall E (A6B0900-21) Batch: 6020834

    5035/8260Bmg/kg dry 501,3,5-Trimethylbenzene " ND --- 0.0358

    "" "1,2-Dibromoethane (EDB) " ND --- 0.0179

    "" "1,2-Dichloroethane (EDC) " ND --- 0.0179

    "Surrogate: Dibromofluoromethane (Surr) Limits: 70-130 % "1 Recovery: 93 %

    " 1,4-Difluorobenzene (Surr) Limits: 70-130 % "" 91 %

    " Toluene-d8 (Surr) Limits: 70-130 % "" 97 %

    " 4-Bromofluorobenzene (Surr) Limits: 70-130 % "" 98 %

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil1A (A6B0900-01) Batch: 6020836

    EPA 8270D (SIM)mg/kg dry 1Acenaphthene 02/27/16 14:05 ND --- 0.0143

    "" "Acenaphthylene " ND --- 0.0143

    "" "Anthracene " ND --- 0.0143

    "" "Benz(a)anthracene " ND --- 0.0143

    "" "Benzo(a)pyrene " ND --- 0.0143

    "" "Benzo(b)fluoranthene " ND --- 0.0143

    "" "Benzo(k)fluoranthene " ND --- 0.0143

    "" "Benzo(g,h,i)perylene " ND --- 0.0143

    "" "Chrysene " ND --- 0.0143

    "" "Dibenz(a,h)anthracene " ND --- 0.0143

    "" "Dibenzofuran " ND --- 0.0143

    "" "Fluoranthene " ND --- 0.0143

    "" "Fluorene " ND --- 0.0143

    "" "Indeno(1,2,3-cd)pyrene " ND --- 0.0143

    "" "1-Methylnaphthalene " ND --- 0.0143

    "" "2-Methylnaphthalene " ND --- 0.0143

    "" " Naphthalene " ND --- 0.0143

    "" "Phenanthrene " ND --- 0.0143"" "Pyrene " ND --- 0.0143

    "Surrogate: 2-Fluorobiphenyl (Surr) Limits: 44-115 % "" Recovery: 87 %

    " p-Terphenyl-d14 (Surr) Limits: 54-127 % "" 105 %

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil1B (A6B0900-02) Batch: 6020836

    EPA 8270D (SIM)mg/kg dry 1Acenaphthene 02/27/16 14:59 ND --- 0.0161

    "" "Acenaphthylene " ND --- 0.0161

    "" "Anthracene " ND --- 0.0161

    "" "Benz(a)anthracene " ND --- 0.0161

    "" "Benzo(a)pyrene " ND --- 0.0161

    "" "Benzo(b)fluoranthene " ND --- 0.0161

    "" "Benzo(k)fluoranthene " ND --- 0.0161

    "" "Benzo(g,h,i)perylene " ND --- 0.0161

    "" "Chrysene " ND --- 0.0161

    "" "Dibenz(a,h)anthracene " ND --- 0.0161

    "" "Dibenzofuran " ND --- 0.0161

    "" "Fluoranthene " ND --- 0.0161

    "" "Fluorene " ND --- 0.0161

    "" "Indeno(1,2,3-cd)pyrene " ND --- 0.0161

    "" "1-Methylnaphthalene " ND --- 0.0161

    "" "2-Methylnaphthalene " ND --- 0.0161

    "" " Naphthalene " ND --- 0.0161

    "" "Phenanthrene " ND --- 0.0161"" "Pyrene " ND --- 0.0161

    "Surrogate: 2-Fluorobiphenyl (Surr) Limits: 44-115 % "" Recovery: 89 %

    " p-Terphenyl-d14 (Surr) Limits: 54-127 % "" 107 %

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil2A (A6B0900-04) Batch: 6020836

    EPA 8270D (SIM)mg/kg dry 1Acenaphthene 02/27/16 15:27 ND --- 0.0130

    "" "Acenaphthylene " ND --- 0.0130

    "" "Anthracene " ND --- 0.0130

    "" "Benz(a)anthracene " ND --- 0.0130

    "" "Benzo(a)pyrene " ND --- 0.0130

    "" "Benzo(b)fluoranthene " ND --- 0.0130

    "" "Benzo(k)fluoranthene " ND --- 0.0130

    "" "Benzo(g,h,i)perylene " ND --- 0.0130

    "" "Chrysene " ND --- 0.0130

    "" "Dibenz(a,h)anthracene " ND --- 0.0130

    "" "Dibenzofuran " ND --- 0.0130

    "" "Fluoranthene " ND --- 0.0130

    "" "Fluorene " ND --- 0.0130

    "" "Indeno(1,2,3-cd)pyrene " ND --- 0.0130

    "" "1-Methylnaphthalene " ND --- 0.0130

    "" "2-Methylnaphthalene " ND --- 0.0130

    "" " Naphthalene " ND --- 0.0130

    "" "Phenanthrene " ND --- 0.0130"" "Pyrene " ND --- 0.0130

    "Surrogate: 2-Fluorobiphenyl (Surr) Limits: 44-115 % "" Recovery: 86 %

    " p-Terphenyl-d14 (Surr) Limits: 54-127 % "" 102 %

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

    Page 18 of

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    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil2B (A6B0900-05) Batch: 6020836

    EPA 8270D (SIM)mg/kg dry 1Acenaphthene 02/27/16 15:54 ND --- 0.0180

    "" "Acenaphthylene " ND --- 0.0180

    "" "Anthracene " ND --- 0.0180

    "" "Benz(a)anthracene " ND --- 0.0180

    "" "Benzo(a)pyrene " ND --- 0.0180

    "" "Benzo(b)fluoranthene " ND --- 0.0180

    "" "Benzo(k)fluoranthene " ND --- 0.0180

    "" "Benzo(g,h,i)perylene " ND --- 0.0180

    "" "Chrysene " ND --- 0.0180

    "" "Dibenz(a,h)anthracene " ND --- 0.0180

    "" "Dibenzofuran " ND --- 0.0180

    "" "Fluoranthene " ND --- 0.0180

    "" "Fluorene " ND --- 0.0180

    "" "Indeno(1,2,3-cd)pyrene " ND --- 0.0180

    "" "1-Methylnaphthalene " ND --- 0.0180

    "" "2-Methylnaphthalene " ND --- 0.0180

    "" " Naphthalene " ND --- 0.0180

    "" "Phenanthrene " ND --- 0.0180"" "Pyrene " ND --- 0.0180

    "Surrogate: 2-Fluorobiphenyl (Surr) Limits: 44-115 % "" Recovery: 80 %

    " p-Terphenyl-d14 (Surr) Limits: 54-127 % "" 98 %

    DRAFT REPORT, DATA SUBJECT TO CHANGE

    DRAFT REPORT The results provided in this report are PRELIMINARY and are subject to change basedon subsequent analysis, QC validation or final data review. Please use these resultswith the understanding that they may have not been finalized by the laboratory

    Page 19 of

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  • 8/19/2019 AT&T Hall Ridge Work Plan 03-07-2016

    53/187

    Apex Labs12232 S.W. Garden PlaceTigard, OR 97223 503-718-2323 Phone 503-718-0333 Fax

    Portland, OR 97217 02/28/16 12:19Ron Malec

    6211 N Ensign St

    NRC-CB&I

    Reported:

    Project Manager:

    Project Number:

    AT&T Hall RidgeProject:

    156319

    ANALYTICAL SAMPLE RESULTS

    Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM

    ResultAnalyte LimitReporting

    Method NotesDilutionUnitsMDL Date Analyzed

    Matrix: Soil3A (A6B0900-08) Batch: 6020836

    EPA 8270D (SIM)mg/kg dry 1Acenaphthene 02/27/16 16:21 ND --- 0.0136

    "" "Acenaphthylene " ND --- 0.0136

    "" "Anthracene " ND --- 0.0136

    "" "Benz(a)anthracene " ND --- 0.0136

    "" "Benzo(a)pyrene " ND --- 0.0136

    "" "Benzo(b)fluoranthene " ND --- 0.0136

    "" "Benzo(k)fluoranthene " ND --- 0.0136

    "" "Benzo(g,