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March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Braided Packing
An Old technology With a Modern Twist
March 10, 2016
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
What is Compression Packing?
• A material made from soft, pliable ingredients that is cut or formed into rings and compressed in an annular cavity to seal around a moving shaft.
• Compression packings are contained and compressed within a cavity called a stuffing box by a packing gland.
• Applications include pumps, valves, mixers and other unique types of equipment.
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
An Old Technology Perception
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Motion Packing Seals
Reciprocating Motion
Helical Motion
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Types of Packing Constructions
• Braided
• Twisted
• Wrapped, Rolled and Folded
• Extruded
• Laminated
• Bulk
• Die Formed
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Braided Mechanical Packing
• Braided Mechanical Packing is a “system” made of – Fibers– Braid Style– Lubricants
• Break-in• Blocking• Corrosion Inhibitors
• Some general requirements for packing– Resilience– Chemical Resistance– Strength– Temperature Resistance
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Types of Braided Packing
• Square braided (plaited) • Usually soft
• Uses fewer, larger diameter diameter yarns
• Large percentage of of lubricants
• Used in high-speed rotary rotary service at low low pressures
• Used in old and worn worn equipment
• Used for small cross cross sections
2 -Track Structure
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Types of Braided Packing
• Inter-braided
• Even distribution of yarn density yarn density throughoutthroughout
• Uses more strands of smaller smaller diameter than square braid
3-Track Structure
4-Track Structure
March 10, 2016 - VMA Technical Seminar
Braid Design
• Different Braiding Machines and Styles
• Square Braid• 1/8” – 1/2” cross sections• Highest coating pick-up percentage
Interbraid
Square Braid
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Bulk Material
• Flexible graphite can be molded to make solid rings
• Other material are used in extrusion, die forming, or molding
• PTFE
• Elastomers• Buna-N
• Ethylene-Propylene
• Neoprene
• FKM
• Silicone
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Carbon or Graphite Fiber
Price
Cleanliness
Disadvantages
Temperature
Heat Transfer
Chemical Resistance
Low Friction
Advantages
Carbon and graphite fibers are inert to most
chemicals and have low frictional coefficients.
pH range 0- 14 except for strong oxidizers
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
ePTFE/Graphite Fiber
ePTFE/Graphite fiber is a fiber that combines the
properties of PTFE and graphite. It is limited only by the
temperature range of the PTFE - pH range 0 -14
Temperature RangeDisadvantages
Heat Transfer
Chemical Resistance
Low Friction
Good tensile strength
Advantages
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
The Main Properties of Flexible Graphite Material
• Density: Is light in weight and has compressibility &
recovery
• Purity: 98% to 99% purity
• High & Low temperature: From -245°C to 850°C
• Corrosion resistant: Chemically inert except strong
oxidizers
• Excellent thermal conductivity
• Low thermal expansion
• Impermeability
• Self lubricating
• Flexible
• High compressibility
• Resilient
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Exfoliated Natural Graphite Flake (Enlarged View)
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Braided Flexible Graphite
• Flexible Graphite by
itself does not have
enough tensile
strength to braid.
• To create a
braidable yarn,
manufacturers use
a carrier or
support to give the
material the
mechanical
strength that by
itself it lacks.
• Typically
March 10, 2016 - VMA Technical Seminar
Outer Jacket
• Graphite Tape Yarn Encapsulated in an Inconnel Wire Mesh
• 4532°F (2500°C) max temperature
• 0 to 14 pH range
• Low Friction
Core
Outer Jacket
Corners (x4)
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Metals
• Some metal wires are used for fiber reinforcement– Stainless steel– Inconel– Copper– Brass– Monel
• Some metals are used in foils– Lead– Aluminum– Copper
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Lubricants
Packing Lubricants
- Compression packings generally contain lubricants
- Lubricants provide resiliency that allows the packing to
deform and recover under slight mechanical deficiencies such as shaft movement or flexing. Some lubricants can also be called ‘blocking agents’.
- Many packing manufacturers offer blends of materials. As a result, limitations and properties vary.
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Lubricants
Materials- Colloidal Polytetrafluoroethylene
- Animal & Vegetable Lubricants
- Petroleum (Mineral) Lubricants, (petrolatum)
- Solid Lubricants: - Graphite powder or flake
- molybdenum disulfide
- Boron Nitride
- Silicone oil
- Bio-lubricants (environmental implications)
March 10, 2016 - VMA Technical Seminar
Coating Formulation
• Individual strands must be coated prior to braiding• Greatest challenge:
• Flexibility• Adhesion• Permeability
Sample Formulations
Flexibility Testing
March 10, 2016 - VMA Technical Seminar
Coating Application
• Wet-Braiding
• Coat the packing while it’s being braided
• Higher coating content between the strands
Wet-Braiding on
Inverted Braider
Machine
March 10, 2016 - VMA Technical Seminar
Valve Packing Characteristics
• Square-Braid Design • Small cross-sections• High coating content
• Outer Jacket• Anti-extrusion capabilities
• Core• Internal spring characteristics
• Wet-Braiding• High coating content
• Low permeability Coating• Emission capability
Coatings act as a
fluid barrier to
enhance sealing
March 10, 2016 - VMA Technical Seminar
Testing & Validation
API-622 Test
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Testing and Validation
• Testing of packing in a fixture such as that specified by API 622 is not a guarantee that the same emission level will be achieved in a given valve.
• Factors such as surface finishes, concentricity, tolerances on diameters, bolt stress, and deformation under load all affect emission results
• Tests must be done first to qualify the packing and then to qualify the valve with the packing
March 10, 2016 - VMA Technical Seminar
Testing & ValidationNo Longer an Old Technology
ISO 15848 and API-624 Testing
March 10, 2016 - VMA Technical Seminar
Packing Behavior Study
Typical case and assumptions
Packing Rings
Packing Ring Size
Bolt Lubricant
Packing Gland Bolt Torque Applied
Gland Stress Applied
5 Cut Rings
1.0”(ID) x 1.5”
(OD) x 0.25”(CS)
Sliding Paste
(0.18 nut factor)
40 ft.-lbs
8,575 psi
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Packing Behavior Study
• CONTEXT Increasing demand from the end-users
Reduction of fugitive emissions
Reduction of opening/closing forces
Need for the differentiation from different packing types
No standardized method for packing calculation nor packing full characterization (mechanical, friction, sealing performance vs. packing load,..)
Existing standards for bolted flange joints with gasket with EN1591 and EN13555
=> FSA and ESA joined with CETIM and its industrial partners to work on the creation of a packing design tool, based on the system developed for bolted flanges
March 10, 2016 - VMA Technical Seminar
Page 28
2015/03
March 10, 2016 - VMA Technical Seminar
• SEALING TEST CELL
Study Test Equipment
Stem movement
(translation or
rotation) generation
Stem movement
transmission equipped
with load sensor or torque
meter
Sealing test cell
(room temperature)
Compression press gland
load application
He
To spectrometer
March 10, 2016 - VMA Technical Seminar
Page 29
2015/03
March 10, 2016 - VMA Technical Seminar
Vacuum chamber -
(Stuffing box/gland sealing)
Pressurized chamber
(Stuffing box/stem sealing)
• SEALING TEST CELL
March 10, 2016 - VMA Technical Seminar
Page 31
2015/03
March 10, 2016 - VMA Technical Seminar
• Mechanical test cell
Stuffing
box
Gland
Strain
gauges
March 10, 2016 - VMA Technical Seminar
Test Equipment Design Verification
March 10, 2016 - VMA Technical Seminar
Page 33
2015/03
March 10, 2016 - VMA Technical Seminar
-2.00E-06
0.00E+00
2.00E-06
4.00E-06
6.00E-06
8.00E-06
1.00E-05
1.20E-05
0 20 40 60 80 100 120 140 160défo
rmat
ion
circ
onfé
rent
ielle
position suivant la hauteur (mm)
cas n°2
Stuffing box design:
Stuffing box thickness : 10 mm
Materials: 1.0481 – P295 GH (EN10028-2)
Load case2 (min stress)
P=10 MPa, Length= 3 mm, T=20°C
3mm
P=10 MPa
ResultsDeformation peak 1 E-05=> OK for
gauges => stuffing box thin enough
Test Equipment Design Verification
March 10, 2016 - VMA Technical Seminar
Page 34
2015/03
March 10, 2016 - VMA Technical Seminar
• Contact pressure on internal diameter vs. Circumferential deformation
– variable packing/stufing-box contact length (3 to 12 mm)
– Constant contact pressure of 1 MPa
Contact length [mm]
3mm
12mm
y = 3.074E-07x + 1.329E-07R² = 9.989E-01
0.00E+00
5.00E-07
1.00E-06
1.50E-06
2.00E-06
2.50E-06
3.00E-06
3.50E-06
4.00E-06
0 1 2 3 4 5 6 7 8 9 10 11 12 13
max def (1 MPa)
max def
Linéaire (max def)
-5.00E-07
0.00E+00
5.00E-07
1.00E-06
1.50E-06
2.00E-06
2.50E-06
3.00E-06
3.50E-06
4.00E-06
0 20 40 60 80 100 120 140 160
déf
orm
atio
n c
irco
nfé
ren
tiel
le
position suivant la hauteur (mm)
effort 3 mm
effort 5 mm
effort 8 mm
effort 10 mm
effort 12 mm
3mm
12mm
def
orm
atio
n
Proportionnal to contact length on internal diameter for a
given contact pressure level
Test Equipment Design Verification
March 10, 2016 - VMA Technical Seminar
Page 35
2015/03
March 10, 2016 - VMA Technical Seminar
• Check of distance between gages
– strain gage chain (10 gages at 1mm distance each)
– Load case2: P=10MPa over 3mm => signal « flat » enough for a 1mm grid
-2.0E-06
0.0E+00
2.0E-06
4.0E-06
6.0E-06
8.0E-06
1.0E-05
1.2E-05
55 60 65 70 75 80 85 90 95
défo
rmat
ion
circ
onfé
rent
ielle
position suivant la hauteur (mm)
maillage
Test Equipment Design Verification
March 10, 2016 - VMA Technical Seminar
Page 36
2015/03
March 10, 2016 - VMA Technical Seminar
• Experimental calibration using elastomeric rings
– Hypothesis: K=1
– Test on a dedicated compression press using the mechanical cell
Test Equipment Design Verification
March 10, 2016 - VMA Technical Seminar
Page 37
2015/03
March 10, 2016 - VMA Technical Seminar
• Experimental calibration using elastomeric rings
1 2
3 4
5 …
..10
A,B,C Gauges (position angle 120°), same axial position => good alignement
-50
0
50
100
150
200
250
0 20 40 60 80 100 120 140 160 180
µm ChA Jauge 01
µm ChB Jauge 01
µm ChC Jauge 01
Test Equipment Design Verification
March 10, 2016 - VMA Technical Seminar
Page 38
2015/03
March 10, 2016 - VMA Technical Seminar
• Experimental calibration using elastomeric rings
0
50
100
150
200
250
300
0 10000 20000 30000 40000 50000
max
de
form
atio
n[µe
]
Force de fond [N]
max deformation mesuré (µ€)
max deformation calculée (µe)pour H =9mm
max deformation calculée (µe)pour H =10mm
max deformation calculée (µe)pour H =11mm
max deformation calculée (µe)pour H =12mm
=> Good order of magnitude for measurmement and calculation (initial
uncompressed packing height 12.7 = 2*6.35mm
Test
Test Equipment Design Verification
March 10, 2016 - VMA Technical Seminar
Page 39
2015/03
March 10, 2016 - VMA Technical Seminar
• SEALING TEST PROCEDURE
– 1 Apply initial axial stress of 1 MPa (reference)
– 2 Apply (and maintain) an axial stress of QA
– 3 Apply M stem movements (translation or rotation) handling an axial stress of QA (M=30)
– 4 Connect He spectrometer (check of vacuum and leakage level without He)
– 5 Pressurize (and maintain) with Helium at pressure level P
– 6 Leakage measurement over 2 hours
– 7 Unload to stress level Q1
– 8 6 Leakage measurement over 2 hours
– 7 Unload to stress level Q2
– ….
Packing Behavior Study
March 10, 2016 - VMA Technical Seminar
Page 40
2015/03
March 10, 2016 - VMA Technical Seminar
• SEALING TEST CURVE EXAMPLE
1.0E-08
1.0E-07
1.0E-06
1.0E-05
1.0E-04
1.0E-03
1.0E-02
1.0E-01
1.0E+00
0
10
20
30
40
50
60
70
80
90
0 1 2 3 4 5 6 7 8 9 10 11 12 13
Axi
al
stre
ss [
MP
a]
-He
Pre
ssu
re [
ba
r]
Time [hr]
Sealing test curve example
(QA=80MPa, 4 graphite rings, 10 bar He, translation)
Stress [MPa]
Pressure [bar]
Leakage [atm.cm3/s]
He spectrometer
connection
Pressurization
Leakage
measurement @80MPa
Leakage
measurement @60MPa
Leakage
measurement @40MPa
Leakage
measurement @30MPa
Leakage
measurement @20MPa
Test Results
March 10, 2016 - VMA Technical Seminar
Page 41
2015/03
March 10, 2016 - VMA Technical Seminar
1.00E-07
1.00E-06
1.00E-05
1.00E-04
1.00E-03
1.00E-02
1.00E-01
1.00E+00
0 10 20 30 40 50 60 70 80 90 100
Leak
age
[m
g/s
/m o
f st
em
pe
rim
ete
r]
Packing axial stress [MPa]
Leakage diagram (4 graphite rings, 10 bar He, translation)
40MPa_10b_1
40MPa_10b_2
60MPa_10b_1
60MPa_10b_2
80MPa_10b_2
A
B
C
Initial packing stress QA [MPa]
TIGHTNESS CLASS
LEAKAGE [mg/s/m] 40 60 80
C 1.00E-02 20/- 27/31 26
B 1.00E-04 - - 36
A 1.00E-06 - - 53
Test Results
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
On-Going Work
• Testing continues
• Different packing formulations must be tested to determine their behavior
• Algorithms will need to be developed
• Standardization will be essential
March 10, 2016 - VMA Technical SeminarMarch 10, 2016 - VMA Technical Seminar
Conclusions
• The performance demands are higher than ever• The products have higher performance than ever• Compression Packing formulation, design, and
testing use some old technology but also state of the art engineering tools
• Parameters such as compressive loads and friction will no longer just be based on experience and occasional verification
• Compression packing emission sealing is a modern technology