12
65 10 BZ Ԡ ( ݧIII-1) 10.1 ݴඇઢܗͳݱͱԿͰΖɻԽԠΛʹڍΔͱɺҰԠͷΑʹԠͷফඅͱͱʹ୯ ७ʹԠͳΑͳԠͰͳɺԠݮΛ܁ΓฦΓɺతʹෆ࿈ଓʹ ߦΔԠΛΕΑɻԠೱ pH ʹΑΓେҟͳΔʹͷΑͳݱ ىΔͰΖɻ·ɺԽԠʹݶΒɺͷճΓʹɺنଇਖ਼ϦζϜΛΉݱҙ֎ʹଟɻ ͱɺΧοϓʹೖΕίʔώʔΛஔΔͱɺৠΔͱʹڞҰఆͷͰઢΧοϓͷଆʹɻ ಈͷ৺υΩυΩΔͷɺपظతͳݱͱଊΔͱͰΔɻͷΑʹɺඇฏߧঢ়ଶͰΔʹ ΘΒੜΔɺతΔతʹنଇతͳݱߏͷͱΛɺগՊͷݴ༿Ͱ ʰҳߏʱͱɻ ݧͰԽԠͷҳߏʹߟΔɻBelousov-Zhabotinsky Ԡ (BZ Ԡ) ҳߏΛ ݱͱΑΒΕɺӷͷ৭ͱͱʹৼಈΔݱ؍ଌͰΔɻBZ ԠଐԘΛ৮ ഔͱɺΧϧϘϯ (ϚϩϯͳͲ) ΛषૉԘʹΑΓषૉԽΔԽԠͰΓɺܥʹଘΔ ͷೱपظతʹมԽΔΊɺΕʹ߹Θӷͷ৭มԽΔɻϚϩϯʹΔԠҎԼͷ ͱΓͰΔɻ 5HOOCCH 2 COOH + 3BrO 3 + 3H + 3HOOCCHBrCOOH + 2HCOOH + 4CO 2 + 5H 2 O ͳɺมԽΔ৭༻ΔଐԘͷ৭ʹΑΓҟͳΓɺηϦϜԘͰແ৭ͱԫ৭ʹɺຊݧͰ༻Δ ϑΣϩΠϯͰͱ੨ͷ৭ʹมԽΔɻ ݧΛ௨ɺBZ ԠͱڵຯԠΛཧղΔ΄ɺͷӷͷ߅ٵڧΛʹࡍఆΔख๏ΛߟɺݱΛཧతʹཧղΔΊͷज़ʹΔɻ 10.2 ༧श ݧͰɺLabView ͱϓϩάϥϛϯάޠݴΛ༻ɺಈଌఆϓϩάϥϜΛΔɻͰ ΔϓϩάϥϜɺʰͰߦݧʢܭଌʣΛɺʹثػߦΒΊʹΔͷʱͰ ΔͱΑɻͷΑͳଌఆϓϩάϥϜΛߏஙΔʹࡍɺ·ͲͷΑͳݧͷ ɺͲͷΑͳσʔλऩΛͳΕͳΒͳΛϋοΩϦͳΕͳΒͳɻຊݧͰ BZ ԠʹΔ৭ͷมԽʹҐଌఆΛ௨هΔͷɺΕΛखಈͰ (PC ΛΘʹ) ܭଌΔͱΒɺͲͷΑͳۀ࡞ΛΔΖɻݧલʹϑϩʔνϟʔτΛߟΈΑɻڭՊ ॻʹهΕϓϩάϥϜ (܅ͷ༧ਖ਼Εɾɾɾ) ͷϑϩʔνϟʔτͷ௨Γͷखॱͱͳ ΔͳͷͰɺݟൺΈΔͱΑɻೖͷஈ֊ͰςΩετʹ฿ϓϩάϥϜΛΔͱͱͳΔ (ͿͷৗखஈͰΔ) ɺʠͳͷΑʹॻΕΔʡΛߟɺͷϊϋΛशಘ ͱେͰΔɻΕͰΦϦδφϧͷϓϩάϥϜΛͰΔΑʹͳΒɻ

BZ S î g III-1) - 国立大学法人信州大学science.shinshu-u.ac.jp/~tiiyama/wp-content/uploads/2015/... · 2015-12-11 · 68 H10 ·BZ S ( î gIII-1) Ä*1 U r w O s ¯ Ë m T

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Page 1: BZ S î g III-1) - 国立大学法人信州大学science.shinshu-u.ac.jp/~tiiyama/wp-content/uploads/2015/... · 2015-12-11 · 68 H10 ·BZ S ( î gIII-1) Ä*1 U r w O s ¯ Ë m T

65

10

BZ ( III-1)

10.1

pH

Belousov-Zhabotinsky (BZ )

BZ

( )

5HOOCCH2COOH+ 3BrO−3 + 3H+ → 3HOOCCHBrCOOH+ 2HCOOH+ 4CO2 + 5H2O

BZ

10.2

LabView

BZ (PC )

( )

( )

Page 2: BZ S î g III-1) - 国立大学法人信州大学science.shinshu-u.ac.jp/~tiiyama/wp-content/uploads/2015/... · 2015-12-11 · 68 H10 ·BZ S ( î gIII-1) Ä*1 U r w O s ¯ Ë m T

66 10 BZ ( III-1)

10.3

4 ( ) (Mw: 150.89) (Mw:

104.06) (Mw: 102.89)

10.4

10.4.1

1. 67 ml 2 ml 5 g

2. 1 g / 10 ml 10 ml 1 g / 10 ml 5 ml 1.

(

)

3. 2. 50 ml 0.4 ml

10.4.2

650 nm

( 10.1

)

� �

� �

10.1

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10.5 67

10.4.3

10.7

PC

( 10.2 )

10.2

10.5

( ) (TEXIO 2040G)

”LabVIEW”

LabVIEW

10.1

PC GPIB(IEEE-488.2)

USB LAN

2

1. PC GPIB

2. PC PC

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68 10 BZ ( III-1)

*1

10.1 TEXIO 2040G

:IDN?

CONF:RES

CONF:VOLT:DC

CONF:VOLT:AC

CONF:CURR:DC

CONF:CURR:AC

READ?,@1

10.6 LabVIEW

LabVIEW

2

(

)

10.6.1

*1 segment;

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10.6 LabVIEW 69

10.6.2

( )

( )

10.6.3

( ) 2

[ ] ( ) ( )

[ ][ ]

Page 6: BZ S î g III-1) - 国立大学法人信州大学science.shinshu-u.ac.jp/~tiiyama/wp-content/uploads/2015/... · 2015-12-11 · 68 H10 ·BZ S ( î gIII-1) Ä*1 U r w O s ¯ Ë m T

70 10 BZ ( III-1)

10.6.4 While

While

10.6.5

*2

[ ]-[ ]

*2 / [ ] -[ ]-[ ]( )-[

]-[ / ]

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10.7 71

10.7

1.

[VISA ]*3 [VISA ]*4 [

]

[VISA ] PC

VISA � (TEXIO DL-2040)

*5

[ ]

CONF:VOLT:DC [ ]

LabView ( , )

( )

(

)

(⇒)

*3 VISA [ ] -[ ]-[ I/O]-[VISA]-[VISA ]*4 VISA [VISA ] [VISA ] -[ ]-[ ]*5 PC USB

Page 8: BZ S î g III-1) - 国立大学法人信州大学science.shinshu-u.ac.jp/~tiiyama/wp-content/uploads/2015/... · 2015-12-11 · 68 H10 ·BZ S ( î gIII-1) Ä*1 U r w O s ¯ Ë m T

72 10 BZ ( III-1)

2. [ ]

READ?,@1

[ ]*6

1 ( ) ( ) *7

[ ] *8

(READ?,@1) 100 ms

[VISA ] 15

[ ] *9 [ ]

[ ]-[ ]

[VISA ] [ ] [1] [ ] [ ]

[ ] [ ]

[ ] [ ]

[ ]

*6 [ / ]-[Express]-[ ]-[

]*7 [ ] -[ ]*8 [ / ]-[ ]-[ ]-[ ]-[ ]*9 [ / ]-[ ]-[ ]-[ ]-[ / ]-[ /

]

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10.7 73

3.

( vi)

[While ]*10 [While ]

[i]

(0 )

[TRUE] [ ] [?]

[i] [=0]

*11 [i] 0 [=0] (TRUE)

[TRUE] [ ]

[ ]

[i] 0 2 [=0] (FALSE)

[FALSE] [

] FALSE FALSE

2

( ; 10.6.3 )

[–] *12

*10 While [ / ]-[Express]-[ ]-[While ]*11 0 ? [ / ]-[ ]-[Express]-[ & ]-[Express ]-[0 ?]*12 [ / ]-[ ]-[Express]-[ & ]-[Express ]-[ ]

Page 10: BZ S î g III-1) - 国立大学法人信州大学science.shinshu-u.ac.jp/~tiiyama/wp-content/uploads/2015/... · 2015-12-11 · 68 H10 ·BZ S ( î gIII-1) Ä*1 U r w O s ¯ Ë m T

74 10 BZ ( III-1)

4.

[ ]

1. [ ]-[ ]-[ & ]-[ ]

( )

2. [ ]-[Express]-[ ]

(

3.

4. ( )

[ ] *13

[ ] ( )

*13 [ / ]-[ ]-[ ]-[ ]-[ ]

[ / ]-[ ]-[ ]-[ ]-[ / ]-[

]

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10.7 75

5.

X

Y *14

*14 XY [ / ]-[ ]-[ ]-[ ]-[XY ]

[ / ]-[ ]-[ ]-[ I/O]-[

]

%.6f ( )

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76 10 BZ ( III-1)

– –

(2015/12/10 )