CATALOGUE 2013/14 - Superlab · Syrris is the world leader in batch chemistry reactor systems and flow chemistry or microreactor systems. Syrris takes pride in creating extremely

C A T A L O G U E 2 0 1 3 / 1 4

Background

Syrris is the world leader in batch chemistry reactor systems and

flow chemistry or microreactor systems. Syrris takes pride in

creating extremely high quality, easy to use automated products

for chemists in areas such as the pharmaceutical industry,

academia, CROs, petrochemical industry, etc.

These versatile products cover a broad range of applications

from synthesis (automated or manual), process optimization and

reaction analysis to crystallization, calorimetry and scale-up.

Batch Chemistry Products

Our main batch chemistry reactor product families called Atlas,

Globe and Custom Reactor Systems are summarized on pages 4-5.

Our Service

Based in Royston (near Cambridge), UK, Syrris has subsidiary

offices in the USA, Japan, India and Brazil and over 35

distributors worldwide offering technical assistance and local

support. Syrris prides itself on providing excellent quality

service and comprehensive warranties.

As well as the range of batch reactor products in this

catalogue, Syrris offers a range of advanced flow chemistry

products called Asia and Africa. They enable cleaner, faster,

safer reactions and the integration of synthesis, work-up and

analysis.

Welcome to our 2013/14 batch chemistry reactors

catalogue.

As a synthetic organic chemist, I understand the

demand for reactors that offer exceptional quality,

flexibility, reliability and ease of use. Therefore these

principles are core to all Syrris products, whether it

be a jacketed reactor, syringe pump, calorimeter or

crystallization system.

By following these guiding principles we have grown

to become a global company. We now have hundreds

of satisfied customers worldwide, in over 45

countries. The positive feedback from our customers

gives us confidence in the excellence of the tools we

offer chemists. Recently, we were delighted when,

the strength of our product development team was

independently recognized, by an esteemed R&D100

award.

This catalogue features additions to our reactor

systems, Atlas and Globe, favoured by research and

development chemists the world over, as well as

more details of the capabilities of our custom reactor

systems. We take great pride in designing the highest

quality, easiest to use reactor systems in the world

and hope you enjoy them too.

Mike Hawes,

Chief Executive Officer

Syrris Ltd.

www.syrris.com2

Atlas Automated Synthesis System 6 - 56 Introduction to Atlas 6 - 8

Atlas Systems 6 - 20

Atlas Potassium 9

Atlas Volumetric Dosing 10

Atlas Gravimetric Dosing 10

Atlas Remote Mount 10

Atlas pH Monitoring and Control 11

Atlas Turbidity 11

Atlas Reaction Monitoring 12

Atlas Sonolab 12

Atlas FT-IR Spectrometer 13

Atlas Calorimeter 14

Atlas Lithium 15

Atlas Sodium 16

Orbit Systems 17

Atlas Sodium High Pressure 18

Atlas Potassium Pressure 19

Atlas Parallel Systems 20

Atlas Case Studies 21 - 23

Atlas Specific Parts 24 - 56

Modules 24

Syringe Pumps 30

Software 36

Sodium Pressure (200 bar) Parts 40

Atlas Orbit and Dry Bath 44

Accessories and Consumables 54

Contents

Globe Jacketed Reactor Platform 57 - 66 Introduction to Globe 57 - 58

Globe Systems 59 - 61

Globe 59

3 bar Globe 60

Automating Globe Systems 61

Globe Specific Parts 62 - 66

Modules 62

Accessories 65

Appendices 108 - 119 Compatibility Chart, System Specifications, Flow Chemistry, Services 108 - 119

Custom Reactor Systems 67 - 78 Introduction to Custom Reactor Systems 67 - 68

Automated High Pressure Reactors 69

Automated Atmospheric Pressure Reactors >5L 70

Case Studies 70 - 74

Automation of Existing Systems 75

Atlas and Globe Common Parts 79 - 107 Jacketed Vessels and Lids 80

Stirrers, Probes and Nodes 86

Circulators and 3rd Party Hardware 89

Pressure Parts 96

Accessories and Consumables 102

Communication Accessories 106

batch products

Syrris’ batch reactor product families are called Atlas, Globe and Custom Reactor Systems. See the table opposite and the brief descriptions to choose the system that meets your needs.

Visit www.syrris.com/videos to see videos of these products in action.

Atlas is a revolutionary range of modular products, which can form a wide range of lab reactors. Atlas

offers manual or automated control of one or many reactions at a time with volumes from 5 litres to

1ml in jacketed reactors, flasks or vials.

Designed specifically for ease of use, all Atlas chemical reactors can be scaled in 3 ways: by volume,

automation level (manual, automated control from the unit or full PC software control), and number

of reactions. All of the systems are highly chemically resistant and require no tools.

Atlas reactor applications include: reaction calorimetry, FT-IR analysis, crystallization control,

volumetric and gravimetric dosing, pH monitoring and control, high pressure reactions, parallel

synthesis etc.

For automated reactor systems with requirements outside of the Atlas range or to automate

systems already owned by customers, Syrris offer Custom Reactor Systems and the Reactor Master

respectively.

Syrris’ Custom Reactor Systems are designed and built to your specifications and tested at our

factory before installation at your facility. Complete systems from 100ml to 250 litres can be

configured using virtually any manufacturer’s apparatus. This can be entirely automated using the

Reactor Master PC Software.

Alternatively for the automation of a pre-existing jacketed reactor system already in your laboratory,

Syrris offer the Reactor Master and many related automated modules and software.

Key: •Ideal

O Possible

x Not Suitable

Atlas Globe Custom

Automated Jacketed Reactor

50ml to 5L, -80°C to +250°C, Vacuum to 3 bar • O x

Manual Jacketed Reactor

50ml to 5L, -80°C to +250°C, Vacuum to 3 bar O • x

Automated Jacketed Reactor

>5L, >250°C or >3 barx x •

Reaction Calorimeter

100ml to 2L, -40°C to +150°C, Vacuum to 3 bar • x x

Manual or Automated Round Bottom Flask/Vial Reactor

50ml to 2L, -40°C to +330°C, Vacuum to atmospheric • x x

Automated Pressure Reactor

100ml to 450ml, -40°C to +330°C, Vacuum to 200 bar • x x

globereactions

made easy

Globe is a jacketed chemical reactor system that saves time, money and space. The proprietary

technology allows vessels from 50ml to 5 litres to be changed in under a minute.

With a temperature range of -80°C to +250°C and pressure options from vacuum up to 3 bar, Globe

is the ideal process chemistry reactor.

Globe is manually controlled or can be upgraded to allow full automation.

globereactions

made easy

www.syrris.com6

Atlas is a modular and automated laboratory product designed specifically for research and development chemists. It is extremely easy to use and equally powerful, performing processes such as reactions in jacketed reactors, round bottom flasks, pressure reactors or vials.

Visit www.syrris.com/videos to watch the Atlas videos:

atlas

• Atlas Software

• Atlas for Controlling Round

Bottom Flasks, Reaction Tubes

and Vials

• Atlas Overview

• Atlas Calorimeter

• Atlas Jacketed Vessel Systems

from 50ml to 5 litres

Scan your smartphone infront of the QR Code opposite to be taken to the Atlas Overview video

or visit www.syrris.com/videos to see more.

What is Atlas?

Atlas simply does it all

Atlas is a high performance synthesis system that is flexible and truly easy to use. The intelligent base can be configured to control one or many reactions up to 5 litres in vials, flasks or jacketed reactors.

• Easy to use: Twist & click knob, large display and intuitive.

• Automated reactions without PC control: Set points, ramps or

sophisticated profiles are all possible for reaction temperature

and stirrer speed.

• Automatic data capture: All data such as temperatures and

stirrer speed are logged in a .csv file and can be downloaded

to a USB stick.

• Easy to upgrade to perform: Calorimetry, pH control,

gravimetric or volumetric reagent addition, crystallizations,

parallel reactions, etc.

• High performance stirring: 1200RPM magnetic or 800RPM

powerful overhead stirrer.

• Quick: Everything clicks together quickly and easily without

tools. Change vessels in under a minute.

Atlas Benefits

Modularity

Atlas is a highly modular chemistry platform. The illustrations on this

page highlight how the range of Atlas systems can be configured for

jacketed reactors, round bottom flasks or vials / reaction tubes.

When using the jacketed reactor configuration, modules can be added

to allow for applications such as crystallization, reaction calorimetry,

pH monitoring, high pressure and much more.

Left: Atlas Potassium, Above: Atlas Sodium, Below: Orbit Systems

Round bottom flasks50ml, 100ml, 250ml, 500ml and 1 litre

Hotplate/coldplateHotplate (to 280°C) or hot and coldplate (-40 to 160°C)

Parallel ChemistryDry baths are available for 3 round bottom flasks, 6 vials, 12 vials or custom arrangements

Optional Magnetic stirringUp to 1200RPM

Optional Overhead StirringStirring setup is easy, quick and aligned without any tools Wide range of sensors

Temperature probes, pH sensors, turbidity probes etc. with localized calibration

Automatic alignmentThe stirrer, flask, dry bath and hotplate are all automatically aligned

Safe Dry BathOutside remains safe to touch even when inside is hot

Quick ClampA single turn of the knob instantly clamps a range of neck sizes.

Round bottom flasks

Quick stirrer set upThe stirrer post clicks into the base in seconds

Powerful stirringCompact, auto aligning stirrer up to 800RPM

USB downloadDownload data to USB stick

Parallel chemistryMany bases can be controlled by one PC

Easy stirrer sealChemically resistant, auto aligning stirrer seal and guide

Wide range of sensorsTemperature probes, pH sensors, turbidity probes etc. with localized calibration

Quick clampNo tools required to change jacketed vessels in seconds

Wide range of stirrersDifferent styles and lengths available

Oil drain unitPress button to drain thermo fluid for leak free vessel changes

Jacketed vessels50ml, 100ml, 250ml, 500ml, 1 litre, 2 litre and custom profiles. 3 litre and 5 litre with Remote Mount

Simple controlTwist & click knob to change temperature / stirrer speed or edit and run automated experiments

Data loggingAll sensor data is logged automatically

Quick ConnectionsThermofluid connections made in seconds

Bottom outlet valveSpring loaded valve offers leak free sealing even at extremes of temperature and pressure

7 Port LidA wide range of port sizes in both vertical and compound angle configurations

Jacketed Reactors

Hotplate & ColdplateHotplate (to 280°C) or hot and cold plate (-40 to 160°C)

Magnetic stirringUp to 1200RPM

Parallel ChemistryAvailable with 6 x 45ml or 12 x 10ml tubes

Simple to useTwist & click lid seals all the reaction tubes simultaneously. All operations are tool-free.

Inert AtmosphereOne inert gas supply is distributed to all reaction tubes.

SafeCool wall surrounds heated area.

Vials and Reaction Tubes

Atlas simply does it all

What is Atlas?

Atlas is a unique laboratory reactor that can be scaled in 3 ways: by volume, automation level and number of reactions. Its unique design means it is fast and easy to change from one configuration to another without the need for tools.

Atlas Jacketed Reactor Systems

Jacketed vessels from 50ml to 5 litres can be controlled in a fully

automated fashion. They can be easily changed due to the quick

release Vessel Clamp (2101012), auto aligning stirrer, quick connect

fluid hoses and semi-automatic circulator fluid drain.

Without PC control, the intelligent base can control circulator or

reaction temperature, overhead stirrer speed and reagent addition

from a pump. Data from sensors such as thermocouples, pH sensors,

turbidity probes and stirrers are recorded by the base and can be

downloaded to a USB stick. All of the Atlas Jacketed Reactor Systems

are based on the Atlas Potassium System.

Specific jacketed reactor systems include the Atlas Calorimeter

System, Atlas Volumetric Dosing System, Atlas Gravimetric Dosing

System, pH Monitoring and Control systems, Atlas Turbidity and

Sonolab systems for crystallization, Atlas FTIR System and Atlas High

Pressure Systems.

Vial and Round Bottom Flask Systems

A variety of dry bath options fit onto the hotplate and magnetic stirrer

for single round bottom flasks or parallel flasks or vials. For cooled

reactions, the hotplate can be removed and a cold plate fitted.

At the centre of every Atlas system is the Atlas base. It contains

a powerful computer with chemically resistant mechanical and

electronic connections. The base can monitor sensors and control

process parameters such as temperatures, pressure, pH, turbidity,

stirrer speed and reagent addition.

Parameters can be defined as single setpoints or as sophisticated

profiles. The base automatically logs all set points and sensor data

which can then be downloaded in one file.

For more sophisticated reaction control, with real time graphs, Atlas

can be controlled by unique PC Software. Powerful and easy to use,

the Atlas Software can control and monitor other manufacturer’s

laboratory apparatus. It can even perform complete reaction

calorimetry with real time reaction power and enthalpy graphs.

Automation

By volume(1ml - 5 litres)

By automation level(manual to fully automated

laboratory reactor)

By number of reactions(single or parallel reactors)

Atlas is Scalable in 3 ways

The Stacking Atlas Dry Bath has concentric cups allowing round

bottom flasks from 50ml to 1 litre to be heated or cooled. A triple

dry bath is available for flasks from 50ml to 250ml and the Atlas Vial

Baths can conveniently heat or cool a wide range of reaction vials.

The Atlas Orbit can heat 6 or 12 reaction tubes under reflux in an inert

atmosphere. The base can automatically run reaction profiles and add

reagents.

Atlas Automated Synthesis System

Atlas Potassium is ideal for chemists who perform automated reactions in

jacketed reactors. The system can be supplied with interchangeable 50ml,

100ml, 250ml, 500ml, 1L and 2L* vessels and is suitable for pressures from

vacuum to 0.25 bar and circulator temperatures from -80°C to +250°C. With

an easy to use vessel clamping system and integral oil drain unit, vessels

and stirrers can be changed in under a minute, without tools. The range of

highly chemical resistant vessels in glass, stainless steel or hastelloy, have

an integrated bottom outlet valve to compensate for thermal expansion.

Compatible with circulators from virtually any manufacturer, Atlas Potassium

makes temperature control of the jacketed reactors safe and easy.

At the centre of the Atlas Potassium is the powerful Atlas Base (see page

24), which monitors sensors and controls processes. Parameters such

as circulator temperature and overhead stirrer speed can be changed by

simply turning the control knob. Alternatively, for automated synthesis, Atlas

Potassium can control and log temperatures, stirrer speed and other sensor

data, even without a PC, making multi step automated experiments easier than

ever before. All modes of operation enable data to be downloaded to a USB

stick.

Options

All Syrris’ range of Atlas jacketed reactor systems are based on the Atlas

Potassium, allowing Atlas to evolve with your changing chemistry requirements.

Simply add further modules to enable an extensive range of applications,

such as calorimetry and sonocrystallization. Other popular upgrades include:

Atlas PC Software for real time graphs and refined reaction control, Atlas

Remote Mount (for 5L vessels), Atlas Syringe Pumps (for intelligent and

highly chemically resistant volumetric dosing) and Atlas 3 bar pressure parts

(for automated control of reactions up to 3 bar). All upgrade parts are easily

installed by the user, without the need for tools.

A standard Atlas Potassium System contains:

Description Page Part Number

Base Unit 24 2101000

Scorpion Overhead Stirrer 25 2101004

Temperature Node 86 2101021

Node Extension 87 2101023

Triple Node Socket 87 2101024

Stirrer Seal and Guide 84 2101011

Jacketed Vessel Clamp 24 2101012

Oil Drain Unit 25 2101013

Jacketed Vessel 80 (various)

Jacketed Vessel Lid (UK, EU or US) 84 (various)

8mm Dia RTD Probe Holder 102 2101547

Oil Pipes from Reactor to Oil Drain Unit (Pack of 2) 54 2101014

Oil Pipes from Circulator to Oil Drain Unit (Pack of 2) 54 2101015

Reaction Vessel Drip Tray 54 2101039

Support Rods (Pack of 2) 54 2101009

Stirrer 85 (various)

RTD Probe 88 (various)

Base to Circulator Serial Cable (RJ11 to DB9 Male) 56 2400214

Reaction Vessel Seal (FFKM) 105 2101543

Circulator 89 (various)

Circulator Fluid 94 (various)

Atlas Potassium

Above: Optional Software

*2L Vacuum Jacketed Vessel requires the Remote Mount for

Jacketed Vessel Clamp (2101576)

www.syrris.com10


Based on an Atlas Potassium, the Atlas Volumetric Dosing System includes

an Atlas Syringe Pump (2200072) or Atlas Syringe Pump XL (2200376). The

Atlas Syringe Pump is a versatile volumetric dosing system that consists of two

syringes with valves and can be configured into 2 independent dosing pumps

or 1 continuous pump. When connected together, via a USB cable, the Base

Unit and Atlas Syringe Pump allow automated dosing without a PC. Profiles

of temperature, stirring speed and volume of reagent to be added can be run

automatically. The Atlas Syringe Pump automatically pauses if the temperature

exceeds a defined maximum. Add the Autosampler (2200196) and Autosampler

Probe (2200197) to automatically sample the reaction.

An Atlas Volumetric Dosing System contains:


Atlas Potassium 9

Atlas Syringe Pump / Atlas Syringe Pump XL 30 (various)

Atlas Volumetric Dosing

Atlas Gravimetric Dosing

Based on an Atlas Potassium, the Atlas Gravimetric Dosing System allows a

defined mass of reagent to be pumped from a balance to the reactor via a

controlled peristaltic pump. The mass flow rate can be defined, monitored and

adjusted by using the Atlas Software 1.

An Atlas Gravimetric Dosing System contains:


Atlas Potassium 9

Atlas Ports (2) 37 2101020

Atlas Software 1 36 2300102

Denver Summit Balance SI-4002 95 2200043

Watson Marlow Peristaltic Pump 323/DU/D 95 1802045

Atlas Remote Mount

Based on an Atlas Potassium System, the Atlas Remote Mount System enables

a jacketed reactor to be mounted on to laboratory scaffolding and become

remote from the Base Unit. The Remote Mount is connected to the Base Unit

using an umbilical cable which provides communications to devices such as

the Temperature Node (2101021) and Scorpion Overhead Stirrer (2101004).

When the Jacketed Vessel Clamp (2101012) is used with the Remote Mount, it is

compatible with vessels of up to 5 litres.

An Atlas Remote Mount System contains:


Atlas Potassium 9

Remote Mount for Jacketed Vessel Clamp 25 2101576

www.syrris.com 11


Atlas Turbidity

The Atlas Turbidity System is designed for crystallization control and analysis. It

allows turbidity to be examined and modified by controlling temperature and/or

additions to the vessel. Data is displayed using the Base Unit and can be plotted

and monitored using the Atlas Software 1. The Software will take actions

dependent on the turbidity value.

The Atlas Turbidity Probe (2200156) can be used with any Atlas reactor.

Volumetric dosing can be performed using the Atlas Syringe Pump (2200072)

or Atlas Syringe Pump XL (2200376). See also the Sonocrystallization system

(page 12).

An Atlas Turbidity System contains:


Atlas Potassium 9

Turbidity Probe - 400mm 88 2200156

Turbidity Node 86 2200157


Options



Atlas pH Monitoring and Control

The Atlas pH Monitoring and Control Systems are designed for people who

perform pH sensitive reactions.

The Atlas pH Monitoring System is based on the Atlas Potassium. It includes a

combined pH and Temperature Node (2200071) to allow Atlas to monitor both

reaction temperature and pH (note that this is included instead of the standard

Temperature Node). This system can be operated from the Base Unit or via the

Atlas Software 1.

The Atlas pH Control System also includes an Atlas Syringe Pump (2200072) or

Atlas Syringe Pump XL (2200376) and can therefore be configured to control

the pH of a reaction by adding either acid and/or base as necessary to maintain

a set pH value. This functionality is possible with or without Atlas Software 1.

An Atlas pH Monitoring System contains:


Atlas Potassium (minus the Temperature Node) 9

pH and Temperature Node 86 2200071

pH Probe - 400mm with Swivel Adaptor 88 2200029

An Atlas pH Control System contains:


Atlas Potassium (minus the Temperature Node) 9


pH and Temperature Node 86 2200071

pH Probe - 400mm with Swivel Adaptor 88 2200029

Above: Atlas pH Monitoring System

Above: Atlas pH Monitoring and Control System

www.syrris.com12


Atlas Reaction Monitoring

Based on an Atlas Potassium, the Atlas Reaction Monitoring System includes an

additional temperature node and RTD probe to monitor the jacket temperature.

The Atlas Reaction Monitoring System uses a combination of reaction

temperature and jacket temperature to accurately monitor both exothermic and

endothermic reaction processes. Tj-Tr is displayed and logged by the Base Unit.

Upgrades include Atlas Software 1 for PC control or for full calorimetry, see the

Atlas Calorimeter (page 14).

An Atlas Reaction Monitoring System contains:


Atlas Potassium 9



RTD Probe - Stainless Steel 100mm x 3mm 87 2101593

Atlas Sonolab

The Prosonix Sonolab is a high performance ultrasound module allowing full

control of crystallization processes. Using proprietary ultrasound technology,

the Sonolab allows control of particle size, shape, crystallinity and polymorph

in a completely automated and easy to use platform. Sonocrystallization also

offers process reproducibility and produces a narrow particle size distribution.

The Sonolab consists of a proprietary ultrasound flow cell and ultrasound

generator. This can be integrated with the Atlas Potassium system by the

addition of the Sonolab Accessories Pack (2200251) which includes a

circulating pump. The powerful Atlas Software (2300102) allows full control of

all the important parameters required for sonocrystallization and sonomilling

applications.

Sonocrystallization is the application of high intensity, low frequency ultrasound

to your process, resulting in acoustic cavitation of the solution. Controlled

cavitation allows extremely accurate control of nucleation, which in turn leads

to uniform and reproducible crystal growth.

An Atlas Sonolab System contains:


Atlas Potassium 9

Prosonix Sonolab SL10 Sonocrystallizer (230V/110V) 27 (various)

Sonocrystallizer Accessories Pack 27 2200251

Options

FBRM Software Integration Kit 39 2200408

Turbidity Probe - 400mm 88 2200156

Turbidity Node 86 2200157


Systems

www.syrris.com 13


Atlas FT-IR Spectrometer

Based on an Atlas Potassium, the Atlas FT-IR Spectrometer System includes a

Bruker Matrix-MF for online, real time IR analysis. This quantitative technique

is ideal for analyzing product yield, impurities, real time reaction kinetics,

mechanism and reaction end point. The Bruker Optics Matrix-MF OPUS

software allows easy set-up and data viewing. With the Syrris Atlas Software 1,

data such as integrated peak size (over a defined wavenumber range) can be

plotted on the same graph as other Atlas data e.g. reaction power, enthalpy, pH,

temperature and user added comments.

A diamond tipped, gold coated probe and industry leading optics allow for the

widest possible wave number range, accuracy and speed of analysis. The Atlas

FT-IR System is easy to upgrade to include calorimetry, pH control, gravimetric

or volumetric reagent addition, crystallizations, parallel reactions, etc.

For parallel analysis applications, up to 6 probes can be attached using the

Bruker Extension for Parallel Monitoring (RD2200604). To ensure that the MCT

does not require refilling with liquid nitrogen during very long experiments,

select the Bruker MCT Detector Mounted in Cryocooler (RD2200605).

An Atlas FT-IR Spectrometer contains:


Atlas Potassium 9

Bruker FTIR Spectrophotometer Matrix-MF 28 RD2200249

Bruker ATR Diamond Probe (MIR), 6mm x 300mm 28 RD2200600

Bruker OPUS Software Package 39 RD2200601

Bruker Atlas Software Drivers 39 RD2600005

Options

Bruker ATR Silicon Probe (MIR), 6mm x 300mm 28 RD2200602

Bruker Extension for Parallel Monitoring 28 RD2200604

Bruker MCT Detector Mounted in Cyrocooler 28 RD2200605

Systems

www.syrris.com14


The Atlas Calorimeter is a high performance system that can generate power

and enthalpy graphs quickly and easily. This, combined with the simple

configuration of reaction temperatures, dosing quantities and alarms provides

chemistry laboratories with an easy, safe and accurate calorimetry system.

The Atlas Calorimeter can be used for Heat Flow Calorimetry (HFC) or Power

Compensation Calorimetry (PCC). Based on the standard Atlas Potassium,

the Atlas Calorimeter also includes a power supply and the intelligent Atlas

Software that can create graphs within seconds.

The Atlas Software offers truly easy calorimetry operation. Configuration of

parameters such as reaction temperature, dosing quantities, expected power

level (e.g. moderate endotherm; strong exotherm) and alarms (with subsequent

actions) are defined in an easy to use wizard.

Reaction temperatures, reagent addition and pre/post run calibration, are

all controlled automatically, eliminating the need for user intervention.

Furthermore, the software automatically controls the operation of all

experimental parameters, providing highly accurate and efficient performance

with user friendly operation. The analysis package automatically accounts for

parameters such as the sensible heat of addition allowing the results to be

easily shown by the ‘single click’ plotting of power and enthalpy graphs.

Options

The Atlas Calorimeter can include many options including the Atlas Syringe

Pump (2200072) for volumetric dosing, or a balance (2200043) and peristaltic

pump (1802045) for gravimetric dosing.

General Calorimetry Specification for HFC and PCC

• Vessel options: 100ml, 250ml, 500ml, 1 litre and 2 litre* vacuum jacketed

reactors.

• Temperature range: -40°C to +150°C recommended for calorimetry (up to

200°C possible).

• Reaction power: 100W/litre maximum (50W for PCC).

• Sensitivity and accuracy: Typically better than 0.1W per kg and 1 to 5%

respectively (dependent on settling time and external conditions).

• Options include: Gravimetric dosing, pH, IR monitoring, turbidity, etc.

An Atlas Calorimeter System contains:


Atlas Potassium 9


Atlas Calorimetry Software Upgrade 39 2600003

Atlas Reporting Software 39 2600002

TTI Power Supply for Calorimetry 26 (various)

Heater Rod 55 (various)


Quick Response RTD Probe 55 (various)

RTD Probe - Stainless Steel 100mm x 3mm 87 2101593

Vacuum Jacketed Vessel 82 (various)

Velcro Oil Connector Insulator (pack of 2) 54 2200008

Atlas Port 37 2101020

Options


Atlas Calorimeter

*2L Vacuum Jacketed Vessel requires the Remote Mount for

Jacketed Vessel Clamp (2101576)

Systems

www.syrris.com 15


Atlas Lithium automates reactions in round bottom flasks or vials. The Atlas

Hotplate (max. 280°C) and Stacking Dry Bath can heat round bottom flasks

from 50ml to 1 litre giving excellent thermal transfer to the reaction whilst the

exterior surface remains safe to touch.

The Clamp holds a range of different vessel sizes securely and automatically

aligns flasks to the Dry Bath.

Turning the control knob changes the Hotplate temperature and the Magnetic

Stirrer speed (up to 1200RPM). Atlas Lithium also allows users to edit and run

profiles automatically from the Base Unit to control heating, cooling, stirring

and reagent addition.

Options

The Stacking Dry Bath can be substituted for any of the other Dry Baths or

Orbit Systems (see Dry Bath section, pages 44-52) and the Atlas Hotplate for a

Hot and Cold Plate (2200047).

The Hot and Cold Plate module is an easy and accurate way of heating and

cooling reactions in flasks and vials. Connected to the Base Unit via a bayonet

fitting and to a circulator, the Hot and Cold Plate can be heated up to +160°C

and down to -40°C. The circulator is controlled by the Base Unit.

The Atlas Lithium can also include the Atlas Syringe Pump (2200072) for

volumetric dosing. Controlled by the intuitive Base Unit, the versatile Atlas

Syringe Pump can be configured into two refilling flows, or one continuous flow.

A choice of dosing modes allows simple additions or intelligent active control

parameters including pH and temperature.

A standard Atlas Lithium System contains:



Hotplate 28 2101001

Magnetic Stirrer 29 2101002

Stacking Dry Bath 44 2101041

Clamp 29 2101040



RTD Probe - PTFE Coated 300mm x 8mm 88 2101583

Round Bottom Flask 56 (various)

Options

Hot and Cold Plate 28 2200047


Atlas Lithium

Above: Optional Atlas Syringe Pump

Systems

www.syrris.com16


Atlas Sodium

Atlas Sodium automates reactions in round bottom flasks. It is equipped with

a Magnetic Stirrer (up to 1200RPM) and a Scorpion Overhead Stirrer (up to

800RPM) for viscous reactions or reactions containing large quantities of solids.

The Stacking Dry Bath enables heating or cooling of round bottom flasks from

50ml to 1 litre (to 280°C hotplate temperature). Accurate reaction temperature

control is provided using an in-reaction RTD Probe and Temperature Node. The

Clamp holds a range of different vessel sizes securely and automatically aligns

flasks to the Dry Bath.

Turning the control knob changes the Hotplate temperature and the Magnetic

or Scorpion Overhead Stirrer speed. Atlas Sodium also allows users to edit and

run profiles automatically from the Base Unit to control heating, cooling, stirring

and reagent addition.

Options

The Stacking Dry Bath can be substituted for any of the other Dry Baths, or

Orbit Systems (see Dry Bath section, pages 44-48) and the Atlas Hotplate for a

Hot and Cold Plate (2200047).

The Hot and Cold Plate module is an easy and accurate way of heating and

cooling reactions in flasks and vials. Connected to the Base Unit via a bayonet

fitting and to a circulator, the Hot and Cold Plate can be heated up to +160°C

and down to -40°C. The circulator is controlled by the Base Unit.

The Atlas Sodium can also include the Atlas Syringe Pump (2200072) for

volumetric dosing. Controlled by the intuitive Base Unit, the versatile Atlas

Syringe Pump can be configured into two refilling flows, or one continuous flow.

A choice of dosing modes allows simple additions or intelligent active control

parameters including pH and temperature.

A standard Atlas Sodium System contains:



Hotplate 28 2101001

Magnetic Stirrer 29 2101002


Scorpion Overhead Stirrer Support (Sodium) 29 2101690



Clamp 29 2101040

Stacking Dry Bath 44 2101041

8mm Dia RTD Probe holder 102 2101547


Stirrer - PTFE 2 Blade Centrifugal 300mm 85 1802059

RTD Probe - PTFE Coated 300mm x 8mm 88 2101583

Stirrer Seal and Guide Release for Flasks (Sodium) 56 2200271

Round Bottom Flask 56 (various)

Options

Hot and Cold Plate 28 2200047


Above: Optional Hot and Cold Plate

Systems

www.syrris.com 17


The Orbit Parallel Reaction Stations are high performance parallel synthesis

systems for research and development chemistry. They fit conveniently on an

Atlas Hotplate (up to 280°C), Hot and Cold Plate (-40°C to +160°C) or regular

hotplate/stirrers (135mm diameter). The system allows 6 (24mm diameter,

45ml) or 12 (13mm diameter, 10ml) reaction tubes to be magnetically stirred

in an inert atmosphere and heated with reflux or cooled. It is possible to add

reagents under an inert atmosphere via the septa.

The Orbit 6 (2200033) or Orbit 12 (2200032) modules lift in and out of the

Orbit Reflux Unit (2200031), allowing the tubes to be freely transported as one

whilst the water and gas tubes remain connected to the Orbit Reflux Unit.

The Orbit 6 and Orbit 12 modules have twist and click lids which supply an

inert atmosphere to all the tubes. When the lid is removed, the tubes are

automatically re-sealed and are free to be transported individually.

The Orbit Reflux Unit requires an inert gas supply (if inert conditions are

required) and running cold water or recirculated coolant. Note that the

gas connection between the Orbit Reflux Unit and Orbit 6 or Orbit 12 is

automatically made and broken as the module is taken in and out. Syrris

recommends the Orbit Circulator (Julabo F250) (see page 53) if running water

is not available or not tolerated.

An Orbit 6 System contains:


Orbit 6 (24mm dia, 45ml tubes) 51 2200033

Orbit Reflux Unit 51 2200031

Orbit 6 Reaction Tubes (Pack of 6) 52 2200036

Orbit 6 Tube Caps (Pack of 6) 52 2200037

Orbit 6 Septa (Pack of 6) 52 2200038

Orbit 6 Stirrer Bars (Pack of 6) 52 2200040

Orbit Septa Opener (Pack of 6) 52 2200041

Orbit Gas Septa Ring (Pack of 5) 52 2200042

An Orbit 12 System contains:


Orbit 12 (13mm dia, 10ml tubes) 51 2200032

Orbit Reflux Unit 51 2200031

Orbit 12 Reaction Tubes (Pack of 12) 52 2200034

Orbit 12 Tube Caps with Septa (Pack of 12) 52 2200035

Orbit 12 Stirrer Bars (Pack of 6) 52 2200039

(2 Packs) Orbit Septa Opener (Pack of 6) 52 2200041

Orbit Gas Septa Ring (Pack of 5) 52 2200042

Orbit 6 and 12 System

The Orbit 6 and 12 System combines the benefits of the Orbit 12 and Orbit 6

Systems and so allows parallel reactions using 6 x 45ml tubes or 12 x 10ml tubes.

The Orbit Reflux Unit can be used with both Orbit 6 and Orbit 12 (see page 51

for more details).

Orbit Systems

Above: Optional Hot and Cold Plate

www.syrris.com18


The Atlas Sodium Pressure System is designed for applications where elevated

pressures (up to 200 bar) or temperatures (Hotplate temperatures up to

350°C†) are required e.g. hydrogenations, carbonylations, etc.

The easy to use modular pressure reactor system can be controlled manually or

automatically using the intuitive control knob and/or Atlas software. Available

in volumes of 100, 160, 300 and 450ml in stainless steel 316, hastelloy, titanium,

etc., the Atlas Sodium Pressure System offers heating and/or cooling, overhead

stirring (to 800RPM) or magnetic stirring (to 1200RPM).

The reactor (shown opposite) includes a dip tube for sampling, cooling coil,

thermowell, impellor, valves, manual pressure gauge and burst disc to ensure

safe operation.

The basic system allows automatic temperature and stirrer control and pressure

sensing. Upgrades include a pressure node and sensor for pressure logging,

Gas Selection Module, Pressure Control Module, gas flow meters and full PC

software control and automation.

Depending on the configuration, the following modes of operation are possible:

1) manual pressure control, 2) automatically maintain a desired pressure, 3)

pressure control with mass flow monitoring, 4) maintain a pressure and monitor

mass flow (ideal for gas uptake monitoring), 5) mass flow control and 6) off gas

monitoring. For more information, please contact Syrris.

An Atlas Sodium High Pressure System contains:



Hotplate 28 (various)

High Pressure Vessel 42 (various)

High Pressure Vessel Lid (in SS316, or Hastelloy) 41 (various)

Dry Bath for High Pressure Vessel 40 (various)





200 Bar System Starter Kit 42 RD2200670

Pressure Certification 43 (various)

Options

Pressure Node for 200 Bar System 43 2200707

Pressure Sensor for 200 Bar System 43 2200665

Gas Selection Module 97 2200375

200 Bar Gas Pressure Control Module* 40 2200388

Aalborg Mass Flow Meter 0-10L/min 101 2200354

Aalborg Mass Flow Controller 101 2200364


Port 37 2101020

Hotter Hotplate 40 (various)

Please see the Sodium Pressure (200 bar) Parts section for details on the use,

specifications and requirements of these modules

*(100 Bar with H2)

† Reaction temperatures in the Atlas Sodium High Pressure are dependent on the

modules chosen. Choices such as the High Pressure Vessel Lid and Hotplate selected

will influence the achievable temperature range.

Atlas Sodium High Pressure

Above: Optional Gas Selection Module

Above: Optional 200 Bar Gas Pressure Control Module


The Atlas Potassium Pressure System is a modular 3 bar pressure reactor

system that can be controlled automatically or manually. It is available with

reactors in volumes of 100ml, 250ml, 500ml, 1L, 2L or 3L (single or vacuum

jacketed†) that can be changed in under a minute without the need for tools.

The Atlas Potassium Pressure System is designed for applications where

elevated pressures are required (e.g. hydrogenations, carbonylations etc.) or

high vacuum applications. The basic system allows automatic temperature

control (-80°C to +200°C*), stirrer control (up to 800RPM or 2000RPM) and

pressure sensing. The data is also displayed and automatically logged by the

base. The system includes a burst disc and pressure relief valve.

Upgrades include the Gas Selection Module, Pressure Control Module, gas

flow meters/controllers and full PC software control. Depending on the

configuration, the following modes of operation are possible: 1) manual pressure

control, 2) automatically maintain a pressure, 3) pressure control with mass

flow monitoring, 4) maintain a pressure and monitor mass flow (ideal for gas

uptake monitoring), 5) mass flow control and 6) off gas monitoring. For more

information, please contact Syrris.

An Atlas Potassium Pressure System contains:





Pressure Sensor for 3 Bar System 99 2200370

Pressure Node for 3 Bar System 99 2200706

2 x Node Extensions 87 2101023

Triple Node Socket 87 2101024

Stirrer Seal and Guide (3 Bar System) 96 (various)

Jacketed Vessel Clamp (3 Bar System) 25 2200333

Oil Drain Unit 25 2101013

Jacketed Vessel (Rated to 3 Bar) 97 (various)

3 bar Jacketed Vessel Lid and Safety Manifold 98 2200664

6/8/9mm Probe Holder (3 Bar System) 100 (various)

Oil Pipes from Reactor to Oil Drain Unit (Pack of 2) 54 2101014

Oil Pipes from Circulator to Oil Drain Unit (Pack of 2) 54 2101015

Reaction Vessel Drip Tray 54 2101039


3 Bar Stirrer 100 (various)


Base to Circulator Serial Cable (RJ11 to DB9 Male) 56 2400214


3 Bar System Starter Kit 99 2200409

Atlas 3 Bar System Safety Enclosure 98 2200694

Circulator 89 (various)

Circulator Fluid 94 (various)

Options


3 Bar Gas Pressure Control Module 96 2200497


Port 37 2101020

Aalborg Mass Flow Controller 101 RD2200364

Aalborg Mass Flow Meter 0-10L/min 101 2200354


Atlas Potassium Pressure

Above: Optional 3 Bar Gas Pressure Control Module


*Range of temperatures can be dependent on the modules

chosen. +200°C is the maximum rated temperature for 3 bar

rated jacketed and vacuum jacketed vessels.

†2L and 3L Vacuum Jacketed Vessel require the Remote

Mount for Jacketed Vessel Clamp (2101576)

www.syrris.com20


Atlas Parallel Systems are multi-position reactor stations allowing any number

from 2 to 4 Atlas jacketed reactors or round bottom flasks, to be controlled

from one PC. They offer full, independent control and logging of all reaction

parameters such as temperature, stirrer speed, pH, dosing, heat flow, turbidity,

etc. and are therefore ideal for process optimization.

Atlas enables full parallel control of any of the systems already described

in this section by using Atlas Parallel Software (see page 37). The Atlas

Parallel Software allows many systems (up to 4) to be connected to one PC and

controlled in parallel e.g. up to 4 of the following systems:

• Atlas Potassium

• Atlas Volumetric Dosing

• Atlas Gravimetric Dosing

• Atlas Remote Mount

• Atlas pH Monitoring and Control

• Atlas Turbidity

• Atlas Reaction Monitoring

• Atlas Sonolab

• Atlas FT-IR Spectrometer

• Atlas Calorimeter

• Atlas Lithium

• Atlas Sodium

• Orbit Systems

• Atlas Sodium High Pressure

• Atlas Potassium Pressure

Atlas Parallel Software (see page 37) opens multiple instances of Atlas

Software 1 (2300102) or Atlas COM Port Software and defines the system to

which each piece of apparatus is assigned (such as Atlas Base Units or other

manufacturer’s apparatus connected by an Atlas Port). Data from all systems

can be viewed in the Run View of any instance of Atlas Software 1 and all can

be saved to one common .csv file.

The software provides whole system control, configuration and analysis. It

not only controls the Atlas hardware, but also virtually all RS232 controlled

apparatus or analogue sensor can be connected to the software. This allows

automation of any compatible laboratory apparatus with full recipe control.

Running reactions from the software allows all responses such as temperature,

stirrer speed, pH and mass flow to be continuously monitored and graphically

displayed in real time. Apparatus is configured using a simple “drag and drop”

interface and recipes can be created, changed and saved with the click of a

mouse.

Responses from sensors can also be used to control other parameters, trigger

alarms or take emergency action. Experiments can be modified “on-the-fly” and

all reaction data is continuously logged to .csv data files making analysis easy.

Atlas Parallel Systems

Text goes here...

applications

Atlas systems are used in hundreds of laboratories around the world in sectors such as the pharmaceutical industry, CROs, academia, petrochemical industry, fine chemical synthesis, nanoparticle synthesis and many more.

Applications include:

• Synthesis in Jacketed Reactors: Synthesis of APIs, fine chemicals, nanoparticles,

etc.

• Synthesis in Automated Jacketed Reactors:

Process development, process optimization,

design of experiment, etc.

• Calorimetry: Kinetic studies, scale-up, process safety, end

point detection, etc.

• Crystallization: Controlled API crystallization, purification,

polymorph control, API formulation, etc.

• Pressure Reactions: Polymer synthesis, hydrogenation,

carbonylation, etc.

• Synthesis in flasks, tubes and vials:

Process optimization, discovery, medicinal

chemistry, etc.

On the following pages you can read case studies demonstrating some of the ways Atlas is benefitting our customers' chemistry.

SystemsAtlas Automated Synthesis System Case Studies

An Atlas Calorimeter system, with a range of additional modules such as an

Atlas Syringe Pump, is used for academic research at the Centre of Materials

Technology. The system is used both with and without software automation.

Customer Application:

• Investigating polymerization reaction processes for commercially viable

low weight polymers.

• Saponification research and development to improve the physical

properties of the final product and improve efficiency.

• Reproducibly scale the production of sensitive cyclization reactions of 3D

Cage imines.

Case Study 1 - Calorimetry

"It has been shown that the Atlas Potassium has proven to be an

excellent reactor, which can be used to investigate polymerization

reaction processes for commercially viable low molecular weight

polymers."

Dr. Neil Campbell (Senior Experimental Officer, Centre for Materials

Discovery, Liverpool, UK)

4 high pressure Atlas Sodium reactors are run in parallel. 2 of the reactors have

overhead stirring and 2 have magnetic stirring. All of the reactors are 100ml and

are rated to 300°C and 200 bar. The reactors are heated using hotter hotplates

and a single circulator is connected to all 4 reactors to allow fast internal

cooling.


• Development and understanding of novel materials to create new

commercial products.

Case Study 3 - Parallel High Pressure

A system similar to this can be used for pressure applications such

as polymerization, gas insertion reactions, petrochemical reactions

supercritical fluids and many more.

An Atlas Calorimeter is used by process chemists at International Flavors and

Fragrances. The Atlas Calorimeter is used to generate power and enthalpy

graphs quickly and easily and can be used for Heat Flow Calorimetry (HFC) or

Power Compensation Calorimetry (PCC).


• Reproducing the same experiment in sites in Asia and Europe

simultaneously.

• Transferring experiment data from the research and development

laboratory to process and manufacturing laboratory.

• Validating new approaches and testing new reactions.

Case Study 2 - Calorimetry

“Before we had the Atlas system we used conventional labware and

oil baths, which required close monitoring. With the Atlas, we can

leave experiments running all night and get a good result the next

day, freeing up time to do other tasks. The system is easy to use and

reliable – we know that when we move from the Atlas system to the

large-scale plant we will get very similar results – and the software is

just beautiful.”

Onofre Casanova (Chemical Process Engineer, International Flavors

and Fragrances, Benicarlo, Spain)www.syrris.com22

Systems

23

2 Atlas systems are used by chemists working at petrochemical company,

PTT. The systems are regularly reconfigured so the chemists can utilize

Atlas' modularity. The system includes calorimetry, 3 bar pressure and

sonocrystallization modules and can be run in parallel. The Atlas can be

configured for use with triple jacketed vessels and round bottom flasks.

Includes full automation using the Atlas Software.


• Synthesize catalysts for the production of polyolefins such as polyethylene

and polypropylene.

• Test polymerization in slurry and gas phases.

Case Study 5 - 3 bar and sonocrystallization

"Our Atlas reactors are in use every working day, and the system is

very reliable. It offers great reproducibility, and its glass jacketed

reactors allow us to follow both the polymerization reaction and the

synthesis process."

Supabhorn Korboonsungserm (Researcher, Process Technology,

PTT, Thailand)

Case Studies Atlas Automated Synthesis System

An Atlas Sonolab system used by IICT for frontier research in chemical

engineering with the aim of developing technology for industrially important

products.


• Study of crystal growth for newly developed organic molecules and drugs.

• Catalyst recovery by measuring size, growth, effect of nucleation, and

yields.

• Inducing secondary nucleation by disrupting crystals or glomerates.

• Recovery of acetamide from aqueous solutions.

Case Study 4 - Sonocrystallization

"The Atlas Sonolab allows us to get data, very efficiently, from 3rd

party equipment such as circulators. I am thankful to Syrris for their

post sales support and quality of service. The Atlas system is very

modular and can be easily upgraded for high pressure reactions,

calorimetry, parallel synthesis and much more."

M Pradeep Kumar (Officer In Charge Pilot Plant, Senior Scientist,

Chemical Engineering, IICT, India)

A 3 bar pressure Atlas system, with pH Monitoring and control, is used by Siam

Research & Innovation Co. Ltd. to develop new compounds of grey cement

powder. The customer uses Atlas to log all set points and record all sensor data.


• Perform and control highly acidic and basic reactions and prepare

materials of different types and structures.

• Determine how additives affect physical and mechanical properties

of cement, and investigate the kinetics of cement hydration and the

interaction of admixtures.

Case Study 6 - pH Monitoring and Control

"We are confident that the Atlas system will grow with us, as we add

extra modules to meet our future requirements."

Wanjana Wannaphahoun (Researcher, Siam Research & Innovation

Co. Ltd., Thailand)

www.syrris.com24

The Base Unit is the centre of any Atlas system. The Base Unit can be

configured into a variety of different systems for different applications such as

discovery or process chemistry. In every case, the hardware clicks into place in

seconds without the need for tools and can be controlled in three ways:

1) Turn the control knob to change hotplate or circulator fluid temperature

and magnetic or overhead stirrer speed.

2) Edit and run profiles automatically from the Base Unit to control heating,

cooling, stirring and reagent addition.

Without PC control, the intelligent Base Unit can control circulator or reaction

temperature, overhead stirrer speed and reagent addition from a pump. Data

from sensors such as thermocouples, pH sensors, turbidity probes and stirrers

are recorded by the Base Unit and can be downloaded to a USB stick.

3) Use full PC software for complex recipe control, real time data plotting

and control of third party hardware. Connect many Base Units for parallel

chemistry.

The Base Unit has physical and electronic connections for other modules

such as the Scorpion Overhead Stirrer (2101004), Magnetic Stirrer (2101002),

Hotplate (2101001), Reaction Vessel Drip Tray (2101039), Temperature Node

(2101021) (or Triple Node Socket, 2101024) and Support Rods (2101009) for

mounting further apparatus.

• Supply voltage: 100 - 240V AC 50 - 60Hz

• Comms ports: 2 x USB A, 1 x USB B, 1 x RS232 RJ11

• Construction: Cast aluminium housing, epoxy powder coated (for high

chemical resistance)

• Dimensions: 23cm (9”) square

• Connection for Scorpion Overhead Stirrer

• Connection for Nodes (e.g. Temperature, pH, Turbidity)

• Connection for Atlas Hotplate or Hot and Cold Plate

• Connection for Magnetic Stirrer

2101000Base Unit

The Jacketed Vessel Clamp is a quick-release clamping mechanism for regular

(not 3 bar rated) Atlas jacketed reactors.

Designed to make changing reactors both quick and easy, the Jacketed Vessel

Clamp has a simple mechanism to clamp and release the reactor and lid

simultaneously. The reactor clamp fits onto the Support Rods (2101009) and

features supports for a Node Extension (2101023) and a further pair of Support

Rods. It is designed for used with the Jacketed Vessel Lids (not 3 bar rated),

please see the Jacketed Vessels and Lids section for more information.

Jacketed Vessel Clamp 2101012

Atlas Modules

Atlas Specific Parts Modules

Modules

www.syrris.com 25

The High Force Jacketed Vessel Clamp is an alternative to the regular Jacketed

Vessel Clamp (2101012). It is designed specifically for clamping regular Atlas

jacketed reactors (not 3 bar rated) in high torque applications. Designed to

make changing reactors both quick and easy, the High Force Vessel Clamp has

a simple mechanism to clamp and release the reactor and lid simultaneously.

The reactor clamp fits onto the Support Rods (2101009) that fit into the

Atlas Base. The clamp features a support for a Node Extension (2101023) and

threaded holes for a further pair of Support Rods. It is designed for used with

the Jacketed Vessel Lids (not 3 bar rated),

High Force Jacketed Vessel Clamp 2200505

Remote Mount for Jacketed Vessel Clamp 2101576

The Remote Mount allows a vessel assembly (including Jacketed Vessel,

Jacketed Vessel Clamp and Oil Drain Unit) to be located away from the Base

Unit (2101000). The Remote Mount can attach to standard laboratory

scaffolding and is connected to the Atlas system using an umbilical which

provides communications to devices such as the Temperature Node (2101021)

and the Scorpion Overhead Stirrer (2101004). When the Jacketed Vessel Clamp

is used with the Remote Mount, it is compatible with vessels of up to 5 litres.

The Oil Drain Unit provides the ability to drain oil from a Jacketed Reactor

Vessel back into a recirculator without exposure to the oil. It is connected to a

recirculator using Oil Pipes (2101015) with two M16 fittings and to a reaction

vessel with Oil Pipes (2101014) using quick release fittings.

The Oil Drain Unit fits over the Support Rods (2101009).

2101013Oil Drain Unit

Modules Atlas Specific Parts

Jacketed Vessel Clamp (3 Bar System) 2200333

The Jacketed Vessel Clamp for the 3 bar system is designed to accept any of

the Syrris Jacketed Vessel (Rated to 3 bar) and the Jacketed Vessel Lid (Rated

to 3 bar 2200664). It allows changing of vessels in under 1 minute and clamps

the lid and vessel by a torque knob therefore avoiding over or under tightening.

The Scorpion Overhead Stirrer provides auto aligning overhead stirring up to

800RPM for Atlas Potassium or Sodium type systems. Connecting directly to

the Base Unit, the Scorpion Overhead Stirrer includes a flexible arm and drive

head which can be instantly connected to either the regular Stirrer Seal and

Guide (2101011), 3 Bar Pressure Stirrer Seal and Guides (2200334 and 2200405)

or the 200 Bar Stirrer Seal and Guides (supplied in part numbers 2200294,

2200434, 2200671 and 2200673).

• Maximum speed: 800RPM

• Maximum torque: 11 Ncm

Scorpion Overhead Stirrer 2101004

www.syrris.com26


High Torque Stirrer Adaptor (for Heidolph Stirrers) 2200258

The High Torque Stirrer Adaptor (for Heidolph Stirrers), when used in

conjunction with a Heidolph Stirrer (see page 95) offers a high torque (with

torque feedback measurement) alternative to the Scorpion Overhead Stirrer

(2101004).

This adaptor kit includes the following components:

• Support Rods - These locate into the top of the Jacketed Vessel Clamp

• Support - This aligns the Heidolph Overhead Stirrer to the Stirrer Seal and

Guide (2101011)

• A quick adaptor between the Heidolph Stirrer and the Stirrer Seal and

Guide (factory fitted)

• A support post - This replaces the Scorpion Overhead Stirrer post

The Scorpion Drive Head is a replacement part for the Scorpion Overhead

Stirrer (2101004). It contains the motor for the Scorpion Overhead Stirrer and it

connects to the pole (with flexible arm).

2101120Scorpion Drive Head (without pole)

TTI Power Supply for Calorimetry (115V) 2200151

TTI Power Supply for Calorimetry (230V) 2200141

The TTI Power Supply is a key part of the Atlas Calorimeter, enabling Heat Flow

Calorimetry (HFC) and Power Compensation Calorimetry (PCC).

The TTI Power Supply is used with the Heater Rod (see page 55). The Power

Supply, controlled entirely by the Atlas Software 1 (2300102), delivers a known

power for calibrating HFC experiments or controls the temperature of the

reaction during PCC experiments.

The Scorpion Overhead Stirrer Pole (without Drive Head) is a replacement part

for the Scorpion Overhead Stirrer (2101004). It contains the pole with flexible

arm. It fits into the Atlas Base (2101000) and connects to the Scorpion Drive

Head (2101120).

Scorpion Overhead Stirrer Pole (without Drive Head) 2101110

www.syrris.com 27

Sonocrystallizer Accessories Pack 2200251

Prosonix Sonolab SL10 Sonocrystallizer (230V) 2200250

The Prosonix Sonolab is a high performance ultrasound module allowing full

control of crystallization processes. Using proprietary ultrasound technology,

the Sonolab allows control of particle size, shape, crystallinity and

polymorphism in a completely automated and easy to use platform.

Sonocrystallization also offers reproducibility and narrow particle size

distribution. The Sonolab consists of a proprietary ultrasound flow cell and

ultrasound generator.

Prosonix Sonolab SL10 Sonocrystallizer (110V) 2200574

Prosonix Sonolab Transformer (for 230V to 110V) 2200611

Sonolab Cell Standard Spares Pack 2200612

Sonolab Cell Superior Seals Pack 2200613

Sonolab Cell Ports and Adaptors Pack 2200614

The Sonocrystallizer Accessories Pack contains a peristaltic pump, tubing,

connectors and valves for recycling the reactor contents through the Sonolab

flow cell. The pack also contains ear defenders for convenience and stand to

hold the Sonolab flow cell close to the reactor.

Quartz Window for Sonolab SL10 Cell RD2200479

The Quartz Window for Sonolab SL10 Cell is a spare window for the Prosonix

Sonolab SL10 Sonocrystallizer (2200250).


The Sonolab Cell Standard Spares Pack contains additional spares such as:

• FEP coated silicone o-rings for main cell body (10)

• FEP coated silicon o-rings for sight glass (10)

• PTFE gaskets

• 2 additional sight glass windows

• Additional screws for cell body

The Sonolab Cell Superior Seals Pack contains accessories to provide higher

chemical resistance such as:

• FFKM o-rings for min cell body (5)

• FFKM o-rings for sight glass (5)

• PTFE gaskets

The Sonolab Cell Parts and Adaptors Pack contains a number of different

stainless steel adaptors for the cell including a sight glass blanking plate.

www.syrris.com28

2101001Hotplate (230V)

The Atlas Hotplate for the Base Unit connects via a bayonet fitting and is

automatically detected. The Atlas Hotplate includes a heater and an embedded

RTD for feedback of plate temperature and a thermal cut-out for safe

operation. The Atlas Hotplate can be controlled directly from the Base Unit

front panel to heat either to a set-point or a controlled profile. For use with the

Dry Baths and Orbit Systems.

• Maximum temperature: 280°C

• Cut-out temperature: 350°C

• Diameter: 135mm

2101005Hotplate (120V)


Bruker FTIR Spectrophotometer Matrix-MF RD2200249

The Atlas FT-IR Spectrometer System includes a Bruker Matrix-MF for real time

IR analysis. Data can be plotted by the Atlas Software 1 (2300102) as with other

sensors. A diamond tipped, gold ATR coated probe and industry leading optics

allow for the widest possible wave number, accuracy and speed of analysis.

• Source: MID IR

• Spectal range: 3,500 – 560cm-1

• Beam splitter: KBr

• MCT detector: Liquid N2 cooled (optional closed cycle MCT)

• Probe: Diamond ATR probe

• Temperature: -100°C to +180°C

• Probe head length: (290mm ±20mm) x 6mm diameter

Bruker ATR Diamond Probe (MIR), 6mm x 300mm RD2200600

Bruker ATR Silicon Probe (MIR), 6mm x 300mm RD2200602

Bruker Extension for Parallel Monitoring (up to 6) RD2200604

Bruker MCT Detector Mounted in Cryocooler RD2200605

Bruker ATR Micro Diamond Probe (MIR), 3.17 x 100mm RD2200603

This reduces the need for refilling with liq N2 during long experiments.

The Hot and Cold Plate connects to the Base Unit via a bayonet fitting and to a

circulator (see pages 89-94). The plate temperature (monitored by an

embedded RTD) or reaction temperature can be controlled directly from the

Base Unit front panel to heat or cool either to a set point or a controlled profile.

For use with Dry Baths and Orbit Systems.

• Minimum temperature: -40°C

• Maximum temperature: +160°C

• Diameter: 135mm

2200047Hot and Cold Plate

www.syrris.com 29

Triple Clamp 2101043

The Triple Clamp is a three position clamping mechanism designed to be used

with the Triple Dry Bath (2101042) and can hold up to three flasks which can be

different sizes. The Triple Clamp has a mechanism which holds a range of

different neck sizes in spring loaded jaws which can be locked into position. The

Triple Clamp is locked into position on the Support Rods (2101009) which holds

it aligned with the three positions of the Triple Dry Bath.

2101690Scorpion Overhead Stirrer Support (Sodium)

This module should be used to support the Stirrer Seal and Guide (2101011)

when using the Scorpion Overhead Stirrer (2101004) with round bottom flasks.

It connects to the Support Rods (2101009) and rests on top of the Clamp

(2101040) to allow the flask, stirrer and Stirrer Seal and Guide (2101011) to be

safely removed as one from the Stacking Dry Bath (2101041).

The Atlas Clamp is a quick-release clamping mechanism for round bottom

flasks and other devices. Flasks can be pushed into the spring loaded jaws

where they can be locked with a simple twist action. The Clamp is mounted

on Support Rods (2101009) on the rear of the Base Unit (2101000) and can

be quickly released or its height changed. The round bottomed flask always

remains aligned to the centre of the Base Unit and Stacking Dry Bath (2101041).

Clamp 2101040


The Magnetic Stirrer connects directly to the Base Unit using a bayonet fitting.

The stirrer is automatically detected by the Base Unit and stirring can be

controlled directly from the front panel with either set-points or profiles. In use,

the current stirring rate is shown along with the set-point on the LCD display.


2101002Magnetic Stirrer

Modules

www.syrris.com30

Atlas Syringe Pumps

The Atlas Syringe Pumps (regular up to 20ml/min or XL up to 200ml/min) are

versatile volumetric dosing and/or sampling systems. They allow 2 independent

refilling flows, one continuous flow, reaction sampling, intelligent control of pH

and temperature dependant dosing. An Atlas Syringe Pump or Atlas Syringe

Pump XL consists of two syringes and multi port valves and is controlled from

the front panel, by an Atlas Base Unit, Reactor Master or the Atlas or Reactor

Master PC software.

Both types of Atlas Syringe Pumps have 5 main modes of operation

(standalone modes shown by *):

1) Dual Dosing* allows independent control of each syringe (and associated

valve), e.g. dose with one syringe and autosample using the other.

Commands include: dose a volume, pump at a flow rate, dose one reagent

to many reactors, sophisticated profiles or autosampling (connect the

Autosampler and probe to enable automated sampling of up to 6 samples

with each syringe/valve)

2) pH control* (with an Atlas pH probe and node plugged in, dose an acid and/

or base to keep the pH within a defined range)

3) Continuous* (2 syringe pumps work together to produce 1 continuous flow,

i.e. one is refilling while the other is dispensing)

4) Atlas Base Control Mode (an Atlas Syringe Pump can be controlled from the

Atlas Base Unit or Reactor Master as part of an automated temperature and

stirrer speed profile)

5) PC Control Mode (PC software can control Dual Dosing, pH Control and

Continuous dosing in the same way as the Atlas Syringe Pump in standalone

mode)

During dosing commands a maximum temperature can be set to pause the

Atlas Syringe Pumps in the case of an exothermic reaction.

The valves are user changeable and are available in a number of different port

options. Each of the ports on each valve can be configured to be an input

or output, therefore, with a 6 port valve it is possible to pump from up to 5

sources to one reactor, etc. per syringe. The syringes are also user changeable

and come in a variety of sizes, corresponding to a variety of flow rate ranges.

Use the Atlas Pump Pressurized Input Store to enable an inert gas blanket over

the samples to be pumped and to minimize cavitation/bubbles.

Features common to the Atlas Syringe Pump and Atlas Syringe Pump XL:

• Chemical Resistance: All wetted parts made from glass, PTFE and PCFE

• Maximum Pressure: 6 bar

• Number of Syringes: 2

• Number of Valves: 2

Syringe Pumps and Accessories

Atlas Specific Parts Syringe Pumps

www.syrris.com 31

Syringe Pumps Atlas Specific Parts

Atlas Syringe Pump - without Valves or Syringes 2200100

The Atlas Syringe Pump (2200072) is supplied with two 4 port valves and two

2.5ml syringes by default. The Atlas Syringe Pump without Valves or Syringes

(2200100) allows valves and syringes to be purchased separately.

Atlas Syringe Pump Features:

•Options for Syringe Sizes: 50μl, 100μl, 250μl, 500μl, 1ml, 2.5ml or 5ml

•Options for Number of Ports per Valve: 2, 3, 4 or 6

•Minimum Flow Rate in Continuous Mode: 20% of syringe volume per

minute (e.g. 10μl/min when using 50μl syringes)

•Minimum Flow Rate in Dual Dosing Mode: 1% of syringe volume per

minute (e.g. 0.5μl/min using a 50μl syringe)

•Maximum Flow Rate in Continuous Mode: 400% of syringe volume (e.g.

20ml/min with 5ml). Note that much higher rates are possible with the

Atlas Pressurized Input Store.

•Maximum Flow Rate in Dual Dosing Mode: 400% of syringe volume (e.g.



Flow Rate range for the Atlas Syringe Pump (2200072) in μl:

Min Flow Rate μl/min Max Flow Rate μl/min

Syringe Size (μl)

ContinuousFlow

Dual DoseMode

ContinuousFlow

Dual DoseMode

50 10 0.5 200 200

100 20 1 400 400

250 50 2.5 1000 1000

500 100 5 2000 2000

1000 200 10 4000 4000

2500 500 25 10000 10000

5000 1000 50 20000 20000

2200072Atlas Syringe Pump

Modules

www.syrris.com32


2200376Atlas Syringe Pump XL

Atlas Syringe Pump XL - without Valves or Syringes 2200316

The Atlas Syringe Pump XL (2200376) is supplied with two 4 port valves and

two 25ml syringes by default. The Atlas Syringe Pump XL without Valves or

Syringes (2200316) allows valves and syringes to be purchased separately.

Atlas Syringe Pump XL Features:

• Options for Syringe Sizes: 0.5ml, 1ml, 2.5ml, 5ml, 10ml, 25ml or 50ml

• Options for Number of Ports per Valve: 3, 4, 6 or 8

•Minimum Flow Rate in Continuous Mode: 20% of syringe volume per

minute (e.g. 100μl/min when using 0.5ml syringes)

•Minimum Flow Rate in Dual Dosing Mode: 1% of syringe volume per

minute (e.g. 5μl/min using a 0.5ml syringe)

•Maximum Flow Rate in Continuous Mode: 400% of syringe volume (e.g.



•Maximum Flow Rate in Dual Dosing Mode: 400% of syringe volume (e.g.



Flow Rate range for the Atlas Syringe Pump XL (2200376) in ml:

Min Flow Rate ml/min Max Flow Rate ml/min

Syringe Size (ml)

ContinuousFlow

Dual DoseMode

ContinuousFlow

Dual DoseMode

0.5 0.1 0.005 2 2

1 0.2 0.01 4 4

2.5 0.5 0.025 10 10

5 1 0.05 20 20

10 2 0.1 40 40

25 5 0.25 100 100

50 10 0.5 200 200

Note that some combinations of valves and syringes on the Atlas XL Pump can make

up to 3 valve ports inaccessible. Please see the compatibility chart in the valves

section (see page 34).

www.syrris.com32

www.syrris.com 33www.syrris.com 33

Autosampler Probe (for Atlas Syringe Pumps) 2200197

The Autosampler Probe is designed for use with the Atlas Syringe Pump or

Atlas Syringe Pump XL and Autosampler Module (2200196) to aspirate up to

6 samples (when using 6 port valves) from a reactor into HPLC vials at user

defined intervals.

The Autosampler Probe consists of 6 PTFE pipes held in a chemically resistant

(PTFE and glass) sheath, which can be located in a Jacketed Vessel Lid port

using the probe holder included. Each of the PTFE pipes is connected to the

Autosampler Module during use.

Atlas Pump Pressurized Input Store 2200475

This module enables reagents pumped by the Atlas Syringe Pump (2200072) or

Atlas Syringe Pump XL (2200376) to be conveniently stored in up to 4 x 250ml

bottles under an inert gas blanket. The module accepts gas at pressures from

1 to 10 bar and automatically regulates the pressure inside the bottles to 1 bar.

This 1 bar pressure avoids a partial vacuum forming when the pump aspirates

and therefore allows higher flow rates, the use of more viscous solvents and

eliminates bubble formation, resulting in the most accurate pumping possible.

The pressurizable bottles include PTFE filters to prolong the life of the pump

valves and syringes and a septum in the cap to enable filling/emptying via a

canula.

PTFE Input filters for 5μm for 3.2mm diameter (pack of 5) 2200594

A pack of 5 PTFE filters that push on to 3.2mm OD pipe and are ideal for

fitting on the input pipes of the Atlas Syringe Pumps. Filtering out particles can

increase the life of the syringes and valves. Due to the flow restriction caused,

these filters are best used at low flow rates or with the Atlas Pump Pressurized

Input Store (2200475).

The Autosampler Module is designed for use with the Atlas Syringe Pump or

Atlas Syringe Pump XL and Autosampler Probe (2200197) to aspirate up to 6

samples (when using 6 port valves) from a reactor at user defined intervals.

The Autosampler Module, which can be mounted on the extra pair of Support

Rods provided, holds 6 x 2ml HPLC vials and is located, in a fluidic sense,

between the Atlas Syringe Pump and the Autosampler Probe. The Atlas Syringe

pumps can sequentially aspirate samples from the reactor into the vials (which

can contain a chemical quench if required).

Autosampler Module (for Atlas Syringe Pumps) 2200196


The Autosampler Probe Filter fits over the end of the Autosampler Probe

(2200197) and minimizes the likelihood of blocking the pipes when aspirating

samples. The filters are manufactured from PTFE and have a pore size of 10μm.

Autosampler Probe Filter (Cap and 5 Filters) 2200463

www.syrris.com34

Syringe for Atlas Pump - 50μl 2200093




3 Port Valve (PTFE/PCTFE) for Atlas XL Pump 2200384




Various valve types depending on number of inputs and outputs required for

Atlas Syringe Pump XL (2200376 and 2200316).

The following table highlights the compatibility between syringes and valves for

the Atlas XL pump:

3-Way 4-Way 6-Way 8-Way

500μl ü ü 1* 1*

1ml ü ü 1* 1*

2.5ml ü ü 1* 1*

5ml ü ü 1 1

10ml ü ü 1 1

25ml ü ü 1 1

50ml ü 2 1 3

Key

ü No Conflict

n*Number of port positions partially blocked (can be accessed with compact fitting pipe end fitting and gripper)

n Number of port positions totally blocked (no suitable fittings)

2 Port Valve (PTFE/PCTFE) for Atlas Pump 2200089




Various valve types depending on number of inputs and outputs required for

Atlas Syringe Pump (2200072 and 2200100).


www.syrris.com34


Syringe for Atlas XL Pump - 500μl 2200377

Syringe for Atlas XL Pump - 1.0ml 2200378

Syringe for Atlas XL Pump - 2.5ml 2200379

Syringe for Atlas XL Pump - 5ml 2200380




Various sized syringes for Atlas Syringe Pump XL (2200376 and 2200316).

Syringes are made from glass with PTFE plungers for excellent chemical

resistance.

Pipe End Fittings for Atlas Syringe Pump - Tefzel 3.2mm 2200199

A pack of 10 pairs of flangeless ferrules and ¼-28 fittings for either 1.6mm or

3.2mm pipe.

Pipe End Fittings for Atlas Syringe Pump - Tefzel 1.6mm 2200198

Syringe for Atlas Pump - 1ml 2200097

Syringe for Atlas Pump - 2.5ml 2200098

Syringe for Atlas Pump - 5ml 2200099

Various sized syringes for Atlas Syringe Pump (2200072 and 2200100).

Syringes are made from glass with PTFE plungers for excellent chemical

resistance.


PTFE Pipe 1.6mm OD x 0.5mm ID x 10m 2200301



www.syrris.com36

Atlas Software 1 2300102

Although the Base Unit (2101000) can control reaction profiles and log data,

Atlas Software 1 provides whole system control, configuration and analysis.

The intuitive PC-based application enables multiple systems such as stirrers,

circulators, pumps and balances to be intelligently combined using virtually any

manufacturers apparatus (see below).

The Atlas Software not only controls the Atlas hardware, but nearly all RS232

controlled apparatus and analogue sensors can be connected to the software

via a simple Port (2101020) which plugs into the computer’s USB connection.

This allows automation of any compatible laboratory apparatus with full recipe

control.

Running reactions from the Atlas Software 1 allows all responses such as

temperature, stirrer speed, pH and mass flow to be continuously monitored and

graphically displayed in real time. Apparatus is configured using a simple “drag

and drop” interface and recipes can be created, changed and saved with the

click of a mouse. Running reactions from the Atlas Software 1 allows responses

to be continuously monitored and graphed with easy to use alarms and

emergency control. Experiments can be modified “on-the-fly” and all reaction

data is continuously logged to .csv data files making analysis easy.

Virtually any RS232-enabled device with ASCII communications can be

configured, The current list of pre-configured devices is below:

Software

Atlas Specific Parts Software

BalancesDenver Pinnacle and Summit Series,

Mettler PG 5001 and PM series, Oxford

Top Pan, Sartorius CP and LP Series,

Kern PLS 2100-2, Ohaus Ranger

Count, A&D FX-iEP Series, Precisa XB

CirculatorsHuber Ministat, Nuevo, Unistat, etc.

Thermo Haake Phoenix II and DC50,

Julabo F series, Lauda Proline series,

Eyela PCC-7000

PumpsAtlas Syringe Pump,

Diaphragm: ProMinent gamma/I*,

Peristaltic: Cole Parmer Masterflex,

IKA, Watson Marlow 323Du & 520Du

Syrris FRX pump

Piston: Scilog Chemtec

Rotary/Piston: Ismatec MCP-CPF

Overhead StirrersIKA Eurostar, CAT R80D-PC, Heidolph

RZR Control, OptiChem Tempstir

FTIRBruker Matrix MF

RefractometersK-Patents PR-23

Pressure sensorsMensor series 6000 digital

Flow Meters and ControllersMeters: Aalborg GFM series*, Sierra

820 series*,

Controllers: Aalborg DFM, Cole Parmer

16 series, Ritter EDP 32 FP, Buchi BPC

pH metersAtlas pH and Temperature,

NodeDenver 215E and 215, Knick

Portamess 913, Mettler Toledo MPH

125 pH and SevenEasy pH meter

TurbidityAtlas Turbidity Probe, Mettler Toledo

Trb8300*

Vacuum ControllerVacuubrand CVC2000 & CVC3000

Temperature sensorsCole Parmer Digisense, J-Kem

Temperature monitor, Syrris 7033 Dual

channel RTD box

SonocrystallizationProsonix Sonolab SL10

Power supplyTTIEL302P

Powder doserLamda

*With RS232 to analogue converter

www.syrris.com36


Software Atlas Specific Parts

Atlas Parallel Software 1 (2 Bases) - Requires 2300102 2600006



The Atlas Parallel Software 1 allows many systems (up to 4) to be connected

to one PC and controlled in parallel. Atlas Parallel Software 1 opens multiple

instances of Atlas Software 1 (2300102) and defines the system to which each

piece of apparatus is assigned (such as Atlas Base Units or other manufacturer’s

apparatus connected by an Atlas Port). Data from all systems can be viewed

in the Run View of any instance of Atlas Software 1 and all can be saved to one

common .csv file.

Atlas Ports are an interface between RS232 devices and the Atlas Software 1

(2300102) or Reactor Master Software (2600004). Ports feature an LCD

display which displays the number of the port to make connections easy. RS232

devices such as pumps, balances, sensors, etc. can be added to the Atlas

system. Each RS232 device connected to the PC requires a separate Port. For

systems where 4 or more RS232 devices are to be used, please see the Atlas

COM Port Software (2600001).

Port 2101020

RS232 Device Supplied for Integration with PC s/w RD2600010

RS232 Device not Supplied for Integration with PC s/w RD2600009

Atlas Software (2300102 or 2600001) and Reactor Master Software (2600004

or RD2600023) can control apparatus from other manufacturers that have

ACSII RS232 communications. Although Syrris has already configured a wide

range of different apparatus types from many manufacturers it is also possible

to configure virtually any new RS232 controlled apparatus. However, due to

the relatively complex nature of this task, it is possible for Syrris to offer a

configuration service. If the apparatus is loaned to Syrris to assist with the

integration testing, please use part number RD2600010. If it is not available to

be loaned to Syrris for integration testing, please use part number RD2600009.

www.syrris.com38

COM port Parallel Software 1 (3 Bases) 2600021

COM port Parallel Software 1 (2 Bases) 2600020

The Atlas COM Port Parallel Software 1 allows many systems (up to 4) to be

connected to one PC and controlled in parallel. It is recommended in preference

to the regular parallel software when using RS232 controlled devices. Atlas COM

Port Parallel Software 1 opens multiple instances of Atlas COM Port Software 1

(2600001) and defines the system to which each piece of apparatus is assigned

(such as Atlas Base Units or other manufacturer's apparatus connected via

RS232). Data from all systems can be viewed in the Run View of any instance of

Atlas COM Port Software 1 and all can be saved to one common .csv file.

COM Port Parallel Software 1 (4 Bases) 2600022

Atlas Specific Parts Software

Atlas COM Port Software 2600001

Atlas COM Port Software 1 has the same functionality as Atlas Software 1

(2300102) with the exception that it uses RS232 connection directly to the

PC rather than via an Atlas Port (2101020). The Atlas COM Port Software 1 is

recommended for applications where more than 3 RS232 devices are to be

connected to one PC. Due to the nature of setting this up, it is recommended

that this is performed by Syrris engineers on a PC purchased from Syrris

(2200599). The Atlas COM Port Software is designed for use with the Ethernet

to 8 RS232 Ports for use with COM Port Software and Set Up (2200351).

Atlas Software

Atlas COM Port Software

Ease of set up? Easy Requires Syrris Engineer

Control of 1-3 RS232 Devices

Less Expensive More Expensive

Control of 4+ RS232 Devices

More Expensive Less Expensive

Set up of system using Atlas Software

Set up of system using Atlas COM Port Software

www.syrris.com 39

Bruker Atlas Software Drivers RD2600005

FBRM Software Integration Kit 2200408

The FBRM Software Integration Kit enables the integration of a third party

Focused Beam Reflectance Measurement device (not included) with the Atlas

Software 1 (2300102) or Atlas COM Port Software (2600001). FBRM is an ideal

technique for the real time, in-situ monitoring of crystal size or droplet size.

This part which includes software, a port, custom serial converters and cables

enables the plotting of up to 8 particle size ranges with other process data.

Bruker OPUS Software Package RD2200601

The Bruker OPUS Software Package contains the key OPUS software

components for use with the Bruker FTIR Matrix-MF (RD2200249).

The Bruker Atlas Software drivers allow data such as integrated peak size (over

a defined wavenumber range) to be imported from the OPUS software and

plotted on the same graph as other Atlas data e.g. reaction power, enthalpy, pH,

temperature and user added comments.

Atlas Reporting Software 2600002

The Atlas Reporting Software allows easy graphical analysis of log files

generated by either the Base Unit (2101000), Atlas Software 1 (2300102), or

Atlas Syringe Pump (2200072). Log files (in .csv format) are imported by

this wizard style software for the easiest possible graphing. Graphs are easily

customizable and can be exported as an image, PDF or .csv format. When a

calorimetry log file, generated by the Atlas Calorimetry Software Upgrade

(2600003) is imported, many other features are unlocked (see the Atlas

Calorimetry Software Upgrade description above).

Atlas Calorimetry Software Upgrade 2600003

The Atlas Calorimetry Software Upgrade allows the Atlas Software 1 (2300102)

or Atlas COM Port Software (2600001) to perform automated Heat Flow

Calorimetry (HFC) or Power Compensation Calorimetry (PCC). See the

Atlas Calorimetry System (page 14) for the associated, required hardware.

Calorimetry experiments can be created in seconds by wizard style actions

for PCC or HFC. User inputs such as reaction temperature, expected heat flux,

volume and flow rate of automated reagent addition allow the experiment to be

performed automatically.

Alarms and safety shutdown thresholds enable the system to shutdown safely

in the case of an unexpected event. When running, approximate power and

enthalpy data can be plotted in real time. For full data analysis, the Atlas

Calorimetry Software Upgrade also unlocks functionality in the Atlas Reporting

Software (2600002) that can generate calibrated power and enthalpy graphs

and correct for sensible heat of addition.

See the Atlas Calorimetry video at www.syrris.com/videos.

Software Atlas Specific Parts

www.syrris.com40

200 Bar Gas Pressure Control Module (100 Bar with H2) 2200388

This module automatically controls the dosing of gas into and out of the reactor

to control the pressure within the reactor. There are 3 modes:

1) Set Min. Pressure and Max. Pressure - In this mode the inlet valve is opened

if the pressure drops below the Min. Pressure and opens the outlet valve if

the pressure is above Max. Pressure. The Gas Pressure Control Module will

automatically maintain the pressure within the set range

2) Vent - This closes the inlet valve and opens the outlet valve.

3) Purge - This opens both the inlet and outlet valves.

The Pressure Control Module can be controlled from the twist and click knob

or can be connected to a PC via an Atlas Port and controlled by the Atlas or

Reactor Master Software. Valves are manufactured from 316L stainless steel.

The module is rated to 200 bar (100 bar with H2).

• Maximum input pressure: 200 Bar

• Maximum pressure read by the sensor: 200 Bar

• Maximum settable pressure: 200 Bar

•Pressure set to/displayed to increments of: 0.5 Bar

Atlas Sodium Pressure (200 bar) Parts

Atlas Specific Parts Atlas Sodium Pressure (200 bar) Parts

Drybath for 100ml High Pressure Vessel 2200203




Dry Bath for High Pressure Vessel

The drybaths for high pressure vessels fit onto the Hotplate (2101001) or Hotter

Hotplate and accept the stainless steel (2200433, 2200298 - 2200300), or

Hastelloy high pressure vessels (2200435 - 2200438).

The Atlas Hotter Hotplate for the Base Unit connects via a bayonet fitting

and is automatically detected. The Atlas Hotplate includes a heater and an

embedded RTD for feedback of plate temperature and a thermal cut-out for

safe operation. The Atlas Hotplate can be controlled directly from the Base Unit

front panel to heat either to a set-point or a controlled profile.

The Hotter Hotplate is designed to be used with the Sodium High Pressure

System and is fully compatible with Dry Baths for High Pressure Vessels.

When using the Hotter Hotplate with regular Dry Baths or Orbit Systems, the

maximum Hotter Hotplate temperature should be limited to +280°C.


• Cut-out temperature: +350°C

• Diameter: 135mm

2200401Hotter Hotplate (to 350°C) 240V

2200455Hotter Hotplate (to 350°C) 120V

www.syrris.com 41

Atlas Sodium Pressure (200 bar) Parts Atlas Specific Parts

High Pressure 275°C* Vessel Lid Hastelloy (Magnetic Stirring) 2200477

High Pressure 275°C* Vessel Lid T316SS (Magnetic Stirring) 2200476

These lids, available in 316 stainless steel or Hastelloy C276 are for use with

the Atlas Sodium Pressure System. Rather than housing a magnetic drive for

overhead stirring, the central port is simply blocked off, therefore lowering the

cost.

This part is used for applications using a magnetic stirrer (2101002) and

follower inside the vessel. It is compatible with the High Pressure Vessel C276,

available in 100ml, 160ml, 300ml and 450ml. The lid and vessel are for use with

the corresponding Dry Bath for High Pressure Vessel.

Lids rated to 275°C* have an FFKM seal, lids rated to 350°C* have a PTFE seal.

The lids come with a diptube, fine control needle valve, and gas Inlet with two

fine control needle valves for inlet regulation and venting. They also include a

pressure gauge, rupture disc, thermowell and cooling coil.

Note: The High Pressure Lid and High Pressure Vessel must be purchased together.

Note: The cooling coil is not supplied when the 100ml or 160ml vessel is ordered.* This is the maximum hotplate temperature when using the vessel lid

High Pressure 350°C* Vessel Lid T316SS (Magnetic Stirring) 2200672

High Pressure 350°C* Vessel Lid Hastelloy (Magnetic Stirring) 2200674

High Pressure 275°C* Vessel Lid T316SS (Overhead Stirring) 2200294

These lids, available in 316 stainless steel or Hastelloy C276 are for use with the

Atlas Sodium Pressure System and include a magnetic drive and stirrer adaptor

for overhead stirring. They are compatible with the High Pressure Vessels,

available in 100ml, 160ml, 300ml and 450ml. The lid and vessel are for use with

the corresponding Dry Bath for High Pressure Vessel.

Lids rated to 275°C* have an FFKM seal, lids rated to 350°C* have a PTFE seal.

The lids come with a diptube, fine control needle valve, and gas Inlet with two

fine control needle valves for inlet regulation and venting. They also include a

pressure gauge, rupture disc, thermowell and cooling coil.


Note: The cooling coil is not supplied when the 100ml or 160ml vessel is ordered.* This is the maximum hotplate temperature when using the vessel lid

High Pressure 275°C* Vessel Lid Hastelloy (Overhead Stirring) 2200434

High Pressure 350°C* Vessel Lid T316SS (Overhead Stirring) 2200671

High Pressure 350°C* Vessel Lid Hastelloy (Overhead Stirring) 2200673

Systems

www.syrris.com42

Modules

High Pressure Vessel T316SS and C276

Syrris offer a range of High Pressure Vessels for use with the High Pressure

Vessel Lids in the Atlas Sodium High Pressure system. These Vessels are made

of stainless steel or Hastelloy.

High Pressure Vessel T316SS 100ml 2200433




High Pressure Vessel Hastelloy C276 100ml 2200435




Atlas Specific Parts Atlas Sodium Pressure (200 bar) Parts

Stainless Steel RTD probe for 100ml and 160ml Vessels 2200686

These Stainless Steel RTD probes are for monitoring reaction temperature

in the Atlas 200 bar Sodium High Pressure Atlas systems. The lengths of the

probes are designed to suit the specified reaction vessel and all have a 3mm

diameter.

Stainless Steel RTD probe for 300ml Vessels 2200687

Stainless Steel RTD probe for 450ml Vessels 2200688

200 Bar System Starter Kit RD2200670

The 200 Bar System Starter Kit contains a selection of pipes and fittings that

are rated to at least 200 bar and allow gas connections between gas sources

and modules. The kit includes stainless steel tubing and a selection of Swagelok

fittings to make joints from the lid and the tubing.


Note: The cooling coil is not supplied when the 100ml or 160ml vessel is ordered.

Modules

www.syrris.com 43

Atlas Sodium Pressure (200 bar) Parts Atlas Specific Parts

ASME (American Society of Mechanical Engineers) Certification is the highest

level of Pressure Certification that Syrris can provide. ASME is a global standard

but is generally most applicable in US and Canada. It includes:

• Material Certificate (materials of construction)

• Hydrostatic Test Certificate

• Design Calculations of Vessels

In addition, and most importantly, the High Pressure Reactor is inspected by an

independent ASME inspector and stamped prior to leaving manufacturer.

High Pressure Vessel PED Certification 2200642

PED Certification is required for all Atlas Sodium High Pressure systems sold in

Europe (European Pressure Equipment Directive). In countries outside Europe,

PED certification may not be a full requirement but many customers will require

this level of certification. It includes:

• Material Certificate (materials of construction)

• Hydrostatic Test Certificate

• Design Calculations of Vessels

High Pressure Vessel ASME Certification 2200643

Pressure Node for 200 Bar System 2200707

The Pressure Node for 200 Bar System connects to the Atlas Base or Reactor

Master and when used with the Pressure Sensor for 200 Bar System (2200665)

allows the Atlas Base or Reactor Master to display pressure in real time on

the screen and log pressure data continuously. When used with the Reactor

Master or the Atlas Base with other nodes the Pressure Sensor requires a Node

Extension (2101023) and Triple Node Socket (2101024).

The Pressure Sensor for 200 Bar System connects to the Pressure Node for 200

Bar System to allow the Atlas Base or Reactor Master to display pressure in real

time on the screen and log pressure data continuously.

Pressure Sensor for 200 Bar System 2200665

www.syrris.com44

Stacking Dry Bath 2101041

The Stacking Dry Bath is an advanced way of heating round bottom flasks

without the issues associated with oil baths. The Stacking Dry Bath fits on a

regular 135mm diameter hotplate and has a series of concentric cups to hold

round bottom flasks from 50ml to 1 litre. The cups provide excellent thermal

transfer to optimize heating times. The exterior of the Dry Bath is safe to touch

even when the Dry Bath is hot.

The Stacking Dry Baths can safely operate with plate temperatures up to

+280°C and down to -80°C. The Stacking Dry Baths are light in comparison to

other Dry Baths, reducing the mass of the block to be heated, improving heat-

up and cool down times. The innovative design also means that the Stacking

Dry Bath can be used with 50, 100, 250, 500 and 1000ml round bottom flasks.

Use the Dry Bath with a Clamp (2101040) for quick alignment of flasks to the

correct position. The Stacking Dry Bath is compatible with most third party

stirrer hotplates (including IKA).

2 Litre Dry Bath 2200329

The 2 Litre Dry Bath is similar to the Stacking Dry Bath but accepts 2 Litre

round bottom flasks only. This part does not accept any inserts.

Stacking Dry Bath (to fit 150mm Hotplates) 2200290

This Stacking Dry Bath is identical to the regular Stacking Dry Bath (2101041)

except that the Dry Bath Base is designed to fit over a hotplate stirrer with a

diameter of 150mm (rather than the regular 135mm).

Japanese Stacking Dry Bath to fit 150mm Hotplate RD2200283

The Japanese Stacking Dry Baths are identical to the regular Stacking Dry

Baths except that the Japanese versions are designed to accept the JIS

(Japanese standard) size round bottom flasks and the Dry Bath Base is

designed to fit over a hotplate stirrer with a diameter of 150mm (rather than the

regular 135mm).

Japanese Stacking Dry Bath 2200241

The range of Japanese Stacking Dry Baths and inserts are identical to the

regular Stacking Dry Baths and inserts except that the Japanese versions are

designed to accept the JIS (Japanese standard) size round bottom flasks.

Atlas Orbit and Dry Baths

Atlas Specific Parts Orbit and Dry Baths

www.syrris.com 45

Orbit and Dry Baths Atlas Specific Parts

Triple Dry Bath 2101042

The Triple Dry Bath is a three position version of the Stacking Dry Bath. The

three positions each have inserts from 50ml to 250ml and each position can

hold a different volume Round Bottom Flask*. Use the Triple Dry Bath with the

Triple Clamp (2101043) to hold up to three flasks in the correct position.

The Triple Dry Bath is also compatible with other stirrer hotplates (including

IKA).

Large Vial Bath (6 x 28mm dia) 2200080

The Large Vial Bath is a safe, clean and quick way of heating or cooling up to

6 vials or reaction tubes of 28mm diameter. Each well is 30mm deep equating

to a directly heated volume of approximately 16ml. The Large Vial Bath is made

up of two parts (the Dry Bath Base and Large Vial Bath Insert) which allows

the insert to be changed to accept other vial sizes or round bottom flasks. The

vial bath contains a thermowell to accept an RTD Probe (2101593) and has an

insulated surround.

Small Vial Bath (12 x 17mm dia) 2200078

The Small Vial Bath will heat and cool up to 12 vials or reaction tubes of 17mm

diameter. Each well is 30mm deep equating to a directly heated volume of

approximately 5.5ml. The Small Vial Bath is made up of two parts (the Dry

Bath Base and Small Vial Bath Insert) which allows the insert to be changed

to accept other vial sizes or round bottom flasks. The vial bath contains a

thermowell to accept an RTD Probe (2101593) and has an insulated surround.

Custom Vial Bath 2200081

The Custom Vial Bath allows the needs of any vial size to be met. Simply state

the size of the vial or reaction tube to be heated or cooled and our engineers

will create a custom vial bath to fit.

Medium Vial Bath (8 x 20mm dia) 2200079

The Medium Vial Bath will heat and cool up to 8 vials or reaction tubes of

20mm diameter. Each well is 30mm deep equating to a directly heated volume

of approximately 9.5ml. The Medium Vial Bath is made up of two parts (the Dry

Bath Base and Medium Vial Bath Insert) which allows the insert to be changed

to accept other vial sizes or round bottom flasks. The vial bath contains a

thermowell to accept an RTD Probe (2101593) and has an insulated surround.

*The Triple Dry Bath is suitable for use with Round Bottom Flasks with Centre and 1

or 0 angled necks (see page 56)

www.syrris.com46

Dry Bath Base 2200060

The Dry Bath Base is used to heat or cool 1 litre round bottom flasks and also

accepts all the dry bath inserts for round bottom flasks (2200061 - 2200064)

and vials (2101607 - 2101609 and 2200053). The exterior of the Dry Bath is

insulated for safety and the unique design creates a natural convection current

to enable rapid cooling after switching off the hotplate.

The Dry Bath Base fits on the Atlas Hotplate (2101001), Hot and Cold Plate

(2200047) and most third party stirrer hotplates (with 135mm diameter). Note

that to use a flask insert, all the larger flask inserts must also be present.

Japanese Dry Bath Base to fit 150mm Hotplate RD2200284

The Japanese Dry Bath Base to fit 150mm Hotplate is identical to the Japanese

Dry Bath Base (2200246) except that it is designed to fit over hotplates of

150mm diameter (rather than 135mm).

Japanese Dry Bath Base 2200246

The Japanese Dry Bath Base is identical to the regular Stacking Dry Bath Base

except that it is designed to accept the JIS (Japanese standard) size 1 litre

round bottom flasks and the Japanese Dry Bath inserts.

Dry Bath Base to fit 150mm Hotplate 2200289

This Dry Bath Base is similar to the regular Dry Bath Base (2200060). The only

difference is that the Dry Bath Base is designed to fit over a hotplate stirrer with

a diameter of 150mm (rather than the regular 135mm).


www.syrris.com 47

Individual Dry Bath Inserts

The Dry Bath inserts fit into the Dry Bath Bases (2200060 and 2200290) and

can accept round bottom flasks or vials. As the round bottom flask inserts are

concentric, to use a particular size, all the larger sizes must also be present.

The vial bath inserts all fit directly into the Dry Bath Base. All the inserts have a

thermowell to accept an RTD Probe (2101593).

Dry Bath Insert 500ml 2200064




Large Vial Bath Insert (6 x 28mm dia) 2101609

Medium Vial Bath Insert (8 x 20mm dia) 2101608

Small Vial Bath Insert (12 x 17mm dia) 2101607

Vial Bath Insert - Custom 2200053

The range of Japanese Stacking Dry Bath inserts are identical to the regular

Stacking Dry Bath inserts except that they are designed to accept the JIS

(Japanese standard) size round bottom flasks. These inserts are for use with the

Japanese Dry Bath Base (2200246) or Japanese Dry Bath Base to fit 150mm

Hotplate (RD2200284).

Japanese Dry Bath Insert 50ml 2200242




Japanese Dry Bath Inserts


www.syrris.com48

Vials for Vial Baths

Syrris has identified a number of vials to work with the different size Vial Baths

available. Pack sizes are shown in brackets below. The large and small vials are

each packed with caps and PTFE faced silicone septa.

Large Vials (28mm dia, 20ml) With Caps and Septa (100) 2200069

Large Vials (28mm dia, 40ml) With Caps and Septa (100) 2200070

Small Vials (17mm dia, 8ml) With Caps and Septa (200) 2200066

PTFE Magnetic Stirrer Bars

Syrris recommend these PTFE coated magnetic stirrer bars for use with Atlas in

the above vials.

Cross (10 x 5mm) for large 28mm Vials (Pack of 10) 2200051

Oval (15 x 6mm) for large 28mm Vials (Pack of 10) 2200052

Round (12 x 3mm) for small 17mm Vials (Pack of 10) 2200049

Round (15 x 4.5mm) for large 28mm Vials (Pack of 10) 2200050


www.syrris.com 49

Orbit Systems

The Orbit Parallel Reaction Stations are high performance parallel synthesis

systems for research and development chemistry. They fit conveniently on the

Atlas Hotplate (2101001), Hot and Cold Plate (2200047) or regular hotplate

(135mm diameter). The system allows 6 (24mm diameter, 45ml) or 12 (13mm

diameter, 10ml) reaction tubes to be magnetically stirred in an inert atmosphere

and heated to +280°C* with reflux or cooled to –40°C. It is possible to add

reagents under an inert atmosphere via the septa.

The Orbit 6 (2200033) or Orbit 12 (2200032) modules lift in and out of the

Orbit Reflux Unit (2200031), allowing the tubes to be freely transported as one

whilst the water and gas tubes remain connected to the Orbit Reflux Unit. The

Orbit 6 and Orbit 12 modules have twist and click lids which supply an inert

atmosphere to all the tubes when in place. When the lid is removed, the tubes

are automatically re-sealed and are free to be transported individually.

The Orbit Reflux Unit requires an inert gas supply (if inert conditions are

required) and running cold water or re-circulated coolant. Note that the

gas connection between the Orbit Reflux Unit and Orbit 6 or Orbit 12 is

automatically made and broken as the module is taken in and out. Syrris

recommends the Orbit Circulator (Julabo F250, page 53) if running water is not

available or tolerated.

Orbit 6 System 2200076

The Orbit 6 System is a convenient combination of modules, accessories

and consumables to allow up to 6 parallel reactions to be stirred and heated

/ cooled under an inert atmosphere. The Orbit 6 System fits on the Atlas

Hotplate (2101001), Hot and Cold Plate (2200047) and most third party stirrer

hotplates. The Orbit 6 System contains the following modules, accessories and

consumables.

Description Part Number

Orbit 6 (24mm dia, 45ml tubes) 2200033

Orbit Reflux Unit 2200031

Orbit 6 Reaction Tubes (Pack of 6) 2200036

Orbit 6 Tube Caps (Pack of 6) 2200037

Orbit 6 Septa (Pack of 6) 2200038

Orbit 6 Stirrer Bars (Pack of 6) 2200040

Orbit Septa Opener (Pack of 6) 2200041

Orbit Gas Septa Ring (Pack of 5) 2200042


*+280°C is the hotplate temperature, the maximum temperatures inside the vials is

lower.

www.syrris.com50

Orbit 12 System 2200075

The Orbit 12 System is a convenient combination of modules, accessories and

consumables to allow up to 12 parallel reactions to be stirred and heated/

cooled under an inert atmosphere. The Orbit 12 System fits on the Atlas

Hotplate (2101001), Hot and Cold Plate (2200047) and most third party stirrer

hotplates. The Orbit 12 System contains the following modules, accessories and

consumables.





Orbit 12 Tube Caps with Septa (Pack of 12) 2200035




Orbit 6 and Orbit 12 System 2200077

The Orbit 6 and Orbit 12 System combines the benefits of the Orbit 12 and Orbit

6 Systems (above) and so allows parallel reactions using 6 x 45ml tubes or 12 x

10ml tubes. The Orbit Reflux Unit can be used with both the Orbit 6 and Orbit

12.






Orbit 6 Tube Caps (Pack of 6) 2200037









www.syrris.com 51


The Orbit 6 unit holds 6 reaction tubes (45ml, 24mm diameter) allowing the

bottom of the tube to be heated while the top is cooled to act in a similar

manner as a reflux condenser.

The Orbit 6 module lifts in and out of the Orbit Reflux Unit (2200031), allowing

the tubes to be freely transported as one whilst the water and gas tubes remain

connected to the Orbit Reflux Unit. The Orbit 6 module has a twist and click lid

which supplies an inert atmosphere to all the tubes when in place. When the lid

is removed, the tubes are automatically re-sealed and are free to be transported

individually.


The Orbit 12 unit holds 12 reaction tubes (10ml, 13mm diameter) allowing the

bottom of the tube to be heated while the top is cooled to act in a similar

manner as a reflux condenser.

The Orbit 12 module lifts in and out of the Orbit Reflux Unit (2200031), allowing

the tubes to be freely transported as one whilst the water and gas tubes remain

connected to the Orbit Reflux Unit. The Orbit 12 module has a twist and click lid

which supplies an inert atmosphere to all the tubes when in place. When the lid

is removed, the tubes are automatically re-sealed and are free to be transported

individually.


The Orbit Reflux Unit locates on to the Atlas Hotplate (2101001), Hot and Cold

Plate (2200047) and most third party stirrer hotplates. The Orbit 6 (2200033)

and Orbit 12 (2200032) fit into the Orbit Reflux Unit. The Orbit Reflux Unit

requires running cold water (or circulated coolant) to cool the condenser

efficiently and a nitrogen or argon supply to create the inert atmosphere for

the reaction tubes. As the Orbit 6 or Orbit 12 is lowered into the Orbit Reflux

Unit, the nitrogen/argon connection is automatically made and the condenser

section of the Orbit 6 or Orbit 12 is cooled.


www.syrris.com52


Pack of 6 reaction tubes (45ml, 24mm diameter) for Orbit 6 without caps or

septa.

Orbit 6 Reaction Tube Caps (Pack of 6) 2200037

Pack of 6 caps for Orbit 6 reaction tubes (without septa).


Pack of 6 PTFE faced silicone septa to fit Orbit 6 Reaction Tube Caps.


Pack of 12 reaction tubes (10ml, 13mm diameter) for Orbit 12 without caps or

septa.


Pack of 12 caps for Orbit 12 reaction tubes with PTFE faced silicone septa.


When the lid to the Orbit 6 or 12 is clicked into place, the Orbit Septa Openers

push open the split septa in the caps of the reaction tubes. This allows the inert

gas supply to flow into the reaction tube.


The Orbit Gas Septa Ring fits both the Orbit 6 (2200033) and Orbit 12

(2200032) and is a replaceable seal that allows reagent addition to or sample

removal from the reaction tubes via a hypodermic needle. The Orbit Gas Septa

Ring can be reused and rotationally repositioned to access previously

un-pierced sections.


Pack of 12 PTFE coated magnetic stirrer bars for Orbit 12 reaction tubes.


Pack of 6 PTFE coated magnetic stirrer bars for Orbit 6 reaction tubes.


www.syrris.com 53

2200059Orbit Circulator (Julabo F250) 240V / 50Hz

The Julabo F250 offers an environmentally friendly way of providing cooled

water for reflux systems (such as Orbit). The F250 is a low power cooling

recirculator (it does not offer any heating capacity) providing up to 210W of

cooling over a temperature range of 5 to 40°C. The small footprint makes this

ideal for bench-top operation whilst the maximum flow rate of 15 litres per

minute provides excellent cooling for a range of chemistry applications.

Orbit Circulator (Julabo F250) 115V / 60Hz 2200183



This module enables Atlas devices such as the Clamp (2101040) and

Autosampler Module (2200196) to be used with IKA hotplate stirrers. The holes

in the base plate locate the hotplate stirrer and the two support rods protrude

at the same distance from the IKA hotplate as they do the Atlas Hotplate. This

enables flasks to be automatically aligned with a Stacking Dry Bath placed on

the hotplate.

2200407Support Rods for IKA

This module fits on top of IKA Hotplates (or any other 135 diameter stirrer

plate) to enable cooling of reactions using a chiller or circulator. The top of

the module is 135mm in diameter to replicate the stirrer and the thin profile

maintains excellent magnetic coupling between the stirrer and the reactor.

• Fittings: M16 male

2200371Hot and Cold Plate for IKA Hotplate/Stirrer


www.syrris.com54

Oil Pipes from Circulator to Oil Drain Unit (Pack of 2) 2101015

Atlas Oil Pipes are insulated hoses and have M16 connections at each end. They

are designed to fit between a circulator and the Oil Drain Unit (2101013). 2m

length.

Oil Pipes from Reactor to Oil Drain Unit (Pack of 2) 2101014

Atlas Oil Pipes are insulated hoses and have M16 connections at one end and

a Connector - Oil Pipe to Jacketed Vessel (2200018) at the other. They are

designed to be used with a jacketed reactor and the Oil Drain Unit (2101013).

0.6m length.

Velcro Oil Connector Insulator (Pack of 2) 2200008

The flexible Velcro Oil Connector Insulators can be used to reduce condensation

or ice build-up at connections. Each insulator can be wrapped around a

connector and secured using the Velcro fastener. Two or more insulators can be

"daisy chained" together to surround larger diameter objects such as reactors.

Reaction Vessel Drip Tray 2101039

This 2 litre Reaction Vessel Drip Tray can be fitted into the central cavity of the

Atlas Base Unit (2101000) to catch any spills from a jacketed reactor.

Support Rods (Pack of 2) 2101009

A pair of Support Rods fit in the rear of the Atlas Base Unit (2101000). The

Oil Drain Unit (2101013), Clamp (2101040), Jacketed Vessel Clamp (2101012),

etc. are all held by the Support Rods. It is also possible to fit a further pair of

Support Rods to the top of the Jacketed Vessel Clamp to hold other apparatus.

Atlas Accessories and Consumables

Connector - Oil Pipe to Hot and Cold Plate (Pack of 2) 2200181

To enable quick connection and disconnection of oil pipes from the Atlas Hot

and Cold Plate (2200047), these connectors can be fitted to the Hot and Cold

Plate thus mimicking the same fittings found on Atlas jacketed vessels. This

requires the corresponding connector - Oil Pipe to Jacketed Vessel (Pack of 2)

2200018 to be fitted to the end of the oil pipes.

Atlas Specific Parts Accessories and Consumables

www.syrris.com 55

Accessories and Consumables Atlas Specific Parts

RTD Probe - FEP Coated SS Quick Response 300mm 2200144



The quick response RTDs connect to a Temperature Node (2101021) in the same

way as a regular RTD. The quick response RTDs have a thinner, chemically

resistant coating and are designed for use with the Atlas Calorimeter (see page

14). These RTDs come with a suitable probe holder.

RTD Probe - Hastelloy C-276 300mm 2200680



Oil Pipe Tidy 2200046

The Oil Pipe Tidy fits on the Jacketed Vessel Clamp (2101012) and is used to

seal the spare end of the Oil Pipes from Reactor to Oil Drain Unit (2101014)

when changing reactor, tidying them to an elevated position. This avoids

residual oil in the pipes dripping onto the fume cupboard floor and acts as a

safety feature should the circulator be switched on accidentally. There is also a

location to store the Scorpion Overhead Stirrer (2101004) when not in use.

Heater Rod for Calorimetry - 25W, 300mm FEP Coated 2200142

Heater Rod for Calorimetry - 50W, 500mm FEP Coated 2200143

These heater rods are designed for the Atlas Calorimeter. They are used for

Power Compensation Calorimetry (PCC) and for calibration in Heat Flow

Calorimetry (HFC). The Hastelloy versions are a more robust alternative to the

FEP coated Stainless Steel versions.

Heater Rod for Calorimetry - 25W, 300mm Hastelloy 2200683

Heater Rod for Calorimetry - 50W, 500mm Hastelloy 2200684

The quick response RTDs connect to a Temperature Node (2101021) in the same

way as a regular RTD. The quick response RTDs have a thinner, chemically

resistant coating and are designed for use with the Atlas Calorimeter (see page

14). These RTDs come with a suitable probe holder.

www.syrris.com56

When using the Stirrer Seal and Guide (2101011) with round bottom flasks, it is

possible to use this device to make the separation of the flask and the Stirrer

Seal and Guide easier. The two parts screw apart to assist in releasing the PTFE

Male B24 joint of the Stirrer Seal Guide from the ground glass female B24 joint

of the round bottom flask.

Stirrer Seal and Guide Release for Flasks (Sodium) 2200271

Base to Circulator Serial Cable (RJ11 to DB9 Male) 2400214

A 9 pin D-type to RJ11 cable for connecting Circulators to the Atlas Base Unit.

The corresponding RS232 or null modem cable required to connect from this

cable to a circulator will be supplied with the circulator if purchased from Syrris.

1 litre Round Bottom Flask - Centre and 2 Angled Neck 2101542

100ml Round Bottom Flask - Centre and 2 Angled Neck 2101539



Syrris produce a range of glassware specially designed for use with Atlas

Systems. A range of 3 neck flasks designed to be compatible with the Stacking

Dry Bath (2101041)* is available in volumes from 100ml to 1 litre. The centre port

is B24, compatible with the Stirrer Seal and Guide (2101011) and the side ports

are B19, compatible with the small and medium Jacketed Coil Condensers.

Round Bottom Flasks - Centre and 2 Angled Neck

Atlas Specific Parts Accessories and Consumables

50ml Round Bottom Flask 2101538



Syrris produce a range of glassware specially designed for use with Atlas

Systems. A range of 2 neck flasks designed to be compatible with the Triple

Dry Bath (2101042) is available in volumes from 50ml to 250ml. The centre port

is B24, compatible with the Stirrer Seal and Guide (2101011) and the side port

is B19, compatible with the small and medium Jacketed Coil Condensers. The

50ml flask has just one central joint.

Round Bottom Flasks

*The Centre and 2 Angled Neck Round Bottom Flasks are not suitable for use

with the Triple Dry Bath (2101042)

Text goes here...

systems

Globe is an innovative jacketed reactor platform from Syrris.

It has been designed by chemists to offer the ultimate ease of use and reaction flexibility. Globe is not automated by default but can be upgraded to include automation.

globe

SystemsWhat is Globe?

Globe's advanced technology allows vessels from 50ml to 5L to be compatible with just one clamp and one lid. Globe enables vessel changes in seconds and automatic stirrer alignment, plus the widest range of pressures and temperatures available.

Globe saves time, money and space

• More reactions in less time: The Globe oil drain unit and

quick clamp allow “single hand” vessel changes in

seconds

• Space saving: 50ml, 100ml, 250ml, 500ml, 1L, 2L, 3L or 5L

vessels, all use the same clamp, lid, circulator and

adjustable height Globe platform

• Easy to use: No tools, no fuss

• Maximum chemical resistance: All wetted parts are glass

or PTFE (stainless steel and Hastelloy options available)

• Wide temperature range: -80°C to +250°C

• Wide pressure range: Vacuum to 0.25 bar (or 3 bar with

pressure system)

• Leak free vessels: The spring loaded bottom outlet valve

eliminates leaks even at extremes of temperature and

pressure

• Upgrade to automation: Add the Globe Reactor Master or

PC software for total automation of reaction parameters

• Robust and reliable: Built on Syrris’ extensive experience,

the Globe reactor system is built to last

Globe Benefits

Globe saves time, money and space

Globe 3 Bar Systems

The regular Globe system is suited to atmospheric pressure or

vacuum processes. For pressure reactions, or for higher vacuum

applications, Syrris offer the Globe 3 Bar System.

Temperature Control

Globe is designed for accurate temperature control over a very

wide range of temperatures. The default temperature range is

-40°C to +200°C and this can be extended to -80°C or +250°C

with the low temperature or high temperature upgrade kits.

Globe’s range of proprietary technologies enable the fastest,

easiest and safest vessel change imaginable. The design saves

space and money by enabling vessels from 50ml to 5L to be

used with the same clamp, lid, circulator and stand.

Rapid oil drain: With the push of a button, the oil drain unit

quickly and safely drains oil from the jacketed reactor back

into the circulator.

Quick oil pipe connection and oil pipe tidy: These allow

quick and reliable connection of the oil pipes to the jacketed

vessel without the need for tools.

Quick vessel clamp and release: The Globe clamp can hold

the unclamped lid or vessel independently. A squeeze of the

lever seals the two together or releases. The vessel is removed

with a simple twist.

Easy to raise/lower motor and auto aligning stirrer: Pulling

the Globe handle raises the stirrer motor away from the Stirrer

Seal and Guide. A button on the Stirrer Seal and Guide allows

instant stirrer height adjustment.

www.syrris.com 59

Globe is designed for chemists who perform reactions in jacketed reactors.

Globe is a modular laboratory reactor. By default Globe is manually controlled

and includes a Frame Assembly (2200507) with inbuilt Jacketed Vessel Clamp,

which can be used with 50ml, 100ml, 250ml, 500ml, 1 litre, 2 litre, 3 litre and

5 litre† vessels. The system also includes a Jacketed Vessel Lid suitable for all

sizes of vessel. Globe uses exactly the same vessels as Atlas allowing total

interchangeability between Globe and Atlas systems.

Globe's thermo fluid connections allow it to be used with virtually any

circulator. The supplied RTD probe with LEMO connector is connected to a

circulator enabling process temperature control. By default the temperature

range of Globe is suitable for temperatures of -40°C to +200°C*, high and low

temperature upgrade kits are also available.

The auto aligning Stirrer Seal and Guide and easy lift stirrer motor offer ultimate

ease of use. A wide range of stirrer motor options are available for high speeds

(up to 2000RPM), high torque (up to 90Ncm), torque feedback, RS232 control

and digital display. Stirrers are also supplied in a wide variety of styles and

lengths.

Options

• High Temperature Upgrade Kit: allowing reactions to reach +250°C.

• Low Temperature Upgrade Kit: allowing reactions to reach -80°C.

• Globe Reactor Master: to allow all of the automation and data logging

functionality of Atlas.

• Globe Reactor Master PC Software: converts Globe into a totally

controlled laboratory reactor.

• Atlas Syringe Pump: for automated reagent dosing for reaction sampling,

intelligent control of pH and temperature dependent dosing.

A standard Globe System contains:


Globe Frame Assembly 62 2200507


Globe Stirrer Motor and Adaptor 63 (various)

Stirrer 85 (various)

Jacketed Vessel 80 (various)

Jacketed Vessel Lid (UK, EU or US) 84 (various)

Oil Pipes 65 (various)


RTD Probe with LEMO Connector 66 (various)

Probe Holder 102 (various)

Options

Jacketed Reactor High Temperature Upgrade Kit 84 2200330

Low Temperature Upgrade Kit

Globe Reactor Master 64 2200515

Globe Reactor Master PC Software 77 2600004

Atlas Syringe Pumps 30 (various)

*Globe's range of temperatures can be dependent on the modules chosen. Choices

such as circulator fluid, circulator, oil pipes and temperature upgrade kit will influence

the achievable temperature range. See these individual parts for their temperature

range.† Globe Offset Assembly required for 5L vessels.

Globe

Above: Optional upgrade to full automation

using the Globe Reactor Master Module

Systems Globe Jacketed Reactor Platform

www.syrris.com60

Globe 3 Bar System

The Globe 3 Bar System is a modular pressure reactor that is designed to be

controlled manually (by default). The Globe 3 Bar System has all of the benefits

of the standard Globe system but it is designed specifically for applications

where elevated pressures are required e.g. hydrogenations, carbonylations,

etc. Available in volumes from 100ml to 3 litres the Globe 3 Bar System offers

heating and/or cooling (-40°C to +200°C), overhead stirring (up to 800RPM or

2000RPM) and a variety of upgrade options.

The Globe 3 Bar System with an integrated Pressure Clamp is suitable for use

with 3 bar jacketed vessels available in 50ml, 100ml, 250ml, 500ml, 1 litre, 2 litre

and 3 litre volumes.

The Globe 3 Bar System is supplied with one lid which is compatible with all 3

bar vessels. The lid has a compatible safety manifold which includes a pressure

relief valve and a safety burst disc. The Globe 3 Bar System also includes a

safety enclosure, a selection of pipes and fittings and a compatible stirrer and

probe.

Options

• Gas Selection Module: allows 3 gases to be permanently connected to the

reactor at any one time.

• Pressure Control Module: automatically controls the dosing of gas into and

out of the reactor to control the pressure within the reactor.

• Gas Flow Meters: to monitor the amount of gas flowing to the reactor.

• Globe Reactor Master: to allow all of the automation and data logging

functionality of Atlas.

• Globe Reactor Master PC Software: converts Globe into a totally


A standard Globe System contains:


Globe 3 Bar Frame Assembly 62 2200508

Stirrer Seal and Guide (3 bar system) 96 (various)

Globe Stirrer Motor and Adaptor 63 (various)

3 Bar Stirrer 100 (various)

Jacketed Vessel (rated to 3 bar) 97 (various)

3 bar Jacketed Vessel Lid and Safety Manifold 98 2200664

Oil Pipes 65 (various)


RTD Probe with LEMO Connector 66 (various)

3 Bar Probe Holder 100 (various)

3 Bar System Starter Kit 99 2200409

Globe 3 Bar System Safety Enclosure 98 2200695

Options

Globe Reactor Master 64 2200515


Pressure Control Module 96 2200497

Gas Flow Meters 101 (various)

Globe Reactor Master PC Software 77 2600004


Above: Optional 3 Bar Pressure Control Module

Globe Jacketed Reactor Platform Systems

www.syrris.com 61

Systems Globe Jacketed Reactor Platform

Automating Globe

The Globe jacketed reactor system can be upgraded to perform automated

experiments, with or without a PC. Choose the Globe Reactor Master for full

automation and data logging or the Syringe Pumps for automated reagent

dosing. The Globe Reactor Master PC Software converts Globe into a fully


Globe Reactor Master

The Reactor Master automates Globe’s temperature, stirring speed, quantity

and timing of liquid additions. It can perform experiments of up to 99 steps

whilst logging all data. All of this is controlled by the twist and click knob. Data

can be viewed in real time and downloaded to a USB memory stick as a .csv file.

Please see the Reactor Master (page 64) for more details.

Syringe Pumps

The Atlas Syringe Pumps are versatile volumetric dosing and/or sampling

systems. They allow 2 independent refilling flows, one continuous flow, reaction

sampling, intelligent control of pH and temperature dependant dosing. They

consist of two syringes and multi port valves and can be controlled from

the front panel, by a Globe Reactor Master, or the Globe Reactor Master PC

software. See the Atlas Syringe Pumps (page 30) for more information.

Reactor Master Software

Reactor Master Software is an easy to use PC based application for control

and analysis of Globe experiments. Whole systems including stirrers,

circulators, RTDs, pumps, balances etc. can be configured using virtually any

manufacturer’s apparatus. The “drag and drop” interface means recipes can be

created, changed and saved with the click of a mouse. See the Reactor Master

Software (page 77) for more information.

Above: Optional upgrades for full automation

- Globe Reactor Master and Atlas Syringe Pump

Above: Optional upgrades for full automation

- Globe Reactor Master PC Software

www.syrris.com62

Globe Specific Parts Modules

The Globe Frame Assembly is the centre of any regular Globe system. The

sturdy stand holds the Jacketed Vessel Clamp, oil drain unit, drip tray and

mechanism for easy lifting/lowering of the stirrer motor.

The advanced Globe clamp technology allows vessels from 50ml to 5L to be

compatible with just one clamp and one lid. The clamp support the unclamped

lid or vessel independently. A squeeze of the lever seals the two together or

releases. This allows the vessel to be removed with a simple twist, enabling

vessel changes in seconds. The height of the Globe clamp is adjustable and can

be lowered (for use with ≤2L vessels) or raised (for use with ≥2L vessels).

The oil drain unit quickly and safely drains oil from the jacketed reactor back

into the circulator with the push of a button. The 5L drip tray locates in the base

of the stand and includes a convenient pouring spout and handle.

The Globe Frame Assembly includes a lever and mechanism to easily to raise/

lower the stirrer motor (not included). Pulling the Globe handle raises the stirrer

motor away from the Stirrer Seal and Guide.

Globe Frame Assembly 2200507

Globe 3 Bar Frame Assembly 2200508

The Globe 3 Bar Frame Assembly is the centre of any Globe 3 Bar Pressure

system (for use from vacuum to 3 barg). The sturdy stand holds the Jacketed

Vessel Clamp, oil drain unit, drip tray and mechanism for easy lifting/lowering of

the stirrer motor.

The advanced Globe clamp technology allows 3 bar pressure vessels from

100ml to 3L to be compatible with just one clamp and one 3 bar lid. The clamp

can support the unclamped lid or vessel independently. A turn of the knob seals

the two together or releases. This allows the vessel to be removed with a simple

twist, enabling vessel changes in seconds. The height of the globe clamp is

adjustable and can be lowered (for use with ≤2L vessels) or raised (for use with

up to 3L vessels).

The oil drain unit quickly and safely drains oil from the jacketed reactor back

into the circulator with the push of a button. The 5L drip tray locates in the base

of the stand and includes a convenient pouring spout and handle.

The 3 Bar Globe Frame Assembly includes a lever and mechanism to easily to

raise/lower the stirrer motor (not included). Pulling the Globe handle raises the

stirrer motor away from the Stirrer Seal and Guide.

Note: The 3 Bar Globe Frame Assembly is compatible with the 3 bar lid and 3

bar jacketed vessels only. It will not accept regular jacketed vessels.

Globe Modules

Globe High Force Globe Frame Assembly 2200628

The Globe High Force Globe Frame Assembly is an alternative to the regular

Globe Frame Assembly (2200507). It is identical except it designed specifically

for clamping jacketed reactors (not 3 bar) in high torque applications.

www.syrris.com 63

Modules Globe Specific Parts

2200577Globe Gold Stirrer (110V / US)

2200576Globe Gold Stirrer (230V / EU)

2200575Globe Gold Stirrer (230V / UK)

The Globe Gold Stirrer is capable of 20 to 700 RPM and 80Ncm of torque. This

stirrer motor features an LCD to display the actual stirrer speed and an RS232

communications port for use with the Globe Reactor Master or Reactor Master

PC software. It locates on the easy lift/lower mechanism of the Globe Frame

Assembly via a mount (included in this part number). When the mechanism is

lowered, the motor automatically aligns and connects to the Stirrer Seal and

Guide. The Globe Gold Stirrer features a pass-through hole in the stirrer body for

the stirrer shaft and therefore allows stirrer height adjustment.

Also see the Heidolph Stirrer section (see page 95) for higher torque or higher

speed applications.

Globe Bronze Stirrer (230V / EU) 2200582

Globe Bronze Stirrer (230V / UK) 2200581

The Globe Bronze Stirrer is the entry level stirrer motor for Globe, capable of 110

to 2000 RPM and 18Ncm of torque. It locates on the easy lift/lower mechanism of

the Globe Frame Assembly via a mount (included in this part number). When the

mechanism is lowered, the motor automatically aligns and connects to the Stirrer

Seal and Guide. The Globe Bronze Stirrer does not allow stirrer shaft height

adjustment and therefore requires an exact length stirrer.

Globe Bronze Stirrer (110V / US) 2200583

2200579Globe Silver Stirrer (230V / EU)

2200578Globe Silver Stirrer (230V / UK)

The Globe Silver Stirrer is capable of 50 to 1600 RPM and 50Ncm of torque. This

stirrer motor features an LCD to display the actual stirrer speed. It locates on the

easy lift/lower mechanism of the Globe Frame Assembly via a mount (included

in this part number). When the mechanism is lowered, the motor automatically

aligns and connects to the Stirrer Seal and Guide. The Globe Silver Stirrer features

a pass-through hole in the stirrer body for the stirrer shaft and therefore allows

stirrer height adjustment.

Globe Silver Stirrer (110V / US) 2200580

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Globe Reactor Master Basic (including stand) 2200515

Globe Reactor Master Pro (including stand) 2200516

The Globe Reactor Master automates Globe’s temperature, stirring speed

(when using the Globe Gold Stirrer or Heidolph Stirrers) and quantity and

timing of liquid additions (when using the Atlas Syringe Pump). It can perform

experiments of up to 99 steps whilst logging all process data. All of this is

controlled by the twist and click knob. Data can be viewed in real time on the

LCD and downloaded to a USB memory stick as a .csv file.

Globe Reactor Master Pro also offers:

• Connection of Atlas RTDs, pH and turbidity nodes and probes via a node

extension.

• Upgrade to full Reactor Master PC Software control (RD2600004).

FeatureReactor Master

BasicReactor Master

Pro

Data logging ü üData download to USB memory stick ü üCompatible with data analysis software ü üControl of thermoregulator temperature ü ü2 x Thermocouples sockets ü üPID control of reaction temperature û ü2 x RTD sockets û üUpgrade to full PC software control possible û üpH meter compatible û üTurbidity sensor compatible û ü

Compatible hardware:

Thermoregulators

• Huber

• Julabo

• Lauda

• Haake

Temperature Sensors

• K or T type thermocouple

• Syrris Atlas RTDs (Pt100)

• 2 and 4 wire RTDs

Overhead Stirrers

• Globe

• Heidolph

pH meters

• Syrris Atlas

Turbidity

• Syrris Atlas

Globe Specific Parts Modules

Globe Offset Assembly (factory fit) 2200636

As standard Globe is suitable for 50ml – 3L, the Globe Offset Assembly

expands the range so that 50ml - 5L vessels can be used. It enables the Stirrer,

Seal and Guide and Jacketed Vessel Clamp to be lifted a small distance further

up and away from the Globe frame, making it suitable for the larger vessel sizes.

The Globe Offset Assembly must be fitted by Syrris before installation on site.

www.syrris.com 65

Heidolph 2051/2052 Stirrer Mount for Globe 2200584

When using the Heidolph 2051 (22000254,267,26 ) or Heidolph 2052 (2200255,

268, 270) with a Globe system, this stirrer mount is required to fix the Heidolph

stirrer to the lift/lower mechanism of the Globe Frame Assembly (2200507 or

2200508).

Globe Accessories and Consumables

Globe Single Short Oil Pipe - Premium 1802037

A Globe Single Short Oil Pipe connects the top (oil output) fitting of a

jacketed vessel (via a jacketed Vessel Connector 2200018) to the Globe Frame

Assembly. This is from the Premium range and is suitable for temperatures

-80°C to +250°C. The length of this pipe is 0.6m.

Globe Single Long Oil Pipe - Premium - 2.5m 2200704

A 3m Globe Single Long Oil Pipe connects from the circulator to the bottom

(oil input) fitting of a jacketed reactor (via a Jacketed Vessel Connector

2200018). A 2.5m Globe Single Long Oil Pipe connects to the oil output on

the Globe Frame Assembly. This is from the Premium range and is suitable for

temperatures -80°C to +250°C.

Globe Oil Pipes Pack - Premium (-80°C to +250°C) 2200509

This premium pack with connectors contains 1 x Single Short Oil Pipe

(1802037), 1 x Single Long Oil Pipe 2.5m (2200704), 1 x Single Long Oil Pipe 3m

(2200705) and 1 set of Oil Pipe to Jacketed Vessel Connectors (2200018). This

constitutes all the pipes and fittings required to connect a circulator to a Globe

jacketed vessel.

Accessories and Consumables Globe Specific Parts

Globe Single Long Oil Pipe - Premium - 3m 2200705

Globe Oil Pipes Pack - Budget (-40°C to +120°C) 2200585

This budget pack with connectors contains 1 x Single Short Oil Pipe (2200513), 1

x Single Long Oil Pipe 2.5m (2200699), 1 x Single Long Oil Pipe 3m (2200700)

and 1 set of Oil Pipe to Jacketed Vessel Connectors (2200018). This constitutes

all the pipes and fittings required to connect a circulator to a Globe jacketed

vessel.

Globe Single Short Oil Pipe - Budget 2200513

A Globe Single Short Oil Pipe connects the top (oil output) fitting of a

jacketed vessel (via a jacketed Vessel Connector 2200018) to the Globe Frame

Assembly. This is from the Budget range and is suitable for temperatures -40°C

to +120°C. The length of this pipe is 0.6m.

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Globe Single Long Oil Pipe - Budget - 2.5m 2200699

A 3m Globe Single Long Oil Pipe connects from the circulator to the bottom (oil

input) fitting of a jacketed reactor (via a jacketed Vessel Connector 2200018). A

2.5m Globe Single Long Oil Pipe connects to the oil output on the Globe Frame

Assembly. This is from the Budget range and is suitable for temperatures -40°C

to +120°C.

Globe Reactor Master Stand 2200510

The Globe Reactor Master Stand clips onto the Globe Frame Assembly and

conveniently holds the Globe Reactor Master off the fume cupboard floor at a

convenient height.

A range of different size PTFE coated RTD Probes are available. These are fitted

with a specialist connector for connection directly to a circulator. Note that the

RTDs have various diameters and should be used with the corresponding probe

holder (see Atlas and Globe common parts). See the compatibility chart in this

catalogue to match reaction vessel with probe length.

RTD Probe PTFE Coated 200mm x 6mm - LEMO Connector 2200587





RTD Probes (PTFE Coated) - LEMO Connector

Globe Specific Parts Accessories and Consumables

Globe Drip Tray 2200634

This 5L Reaction Vessel Drip Tray can be fitted into the central cavity of a Globe

frame to catch any spills from a jacketed reactor.

Globe Single Long Oil Pipe - Budget - 3m 2200700

Systems

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custom reactor systems

Syrris’ Custom Reactor Systems are designed and built to your specifications. Complete systems including reactors, pressure reactors, stirrers, circulators, RTDs, pumps, sensors, etc. can be configured using virtually any manufacturer’s apparatus. Choose from automation of temperature, stirring and dosing via the Reactor Master or total automation using the Reactor Master PC Software.

What are Custom Reactor Systems?

For requirements outside of the Atlas and Globe product ranges Syrris offer Custom Reactor Systems. Ideal for applications requiring large vessels (>5L), elevated pressures (>3 bar) or high temperatures (>250°C), alongside automation and datalogging.

Customized products - flexible solutions

• Wide volume range: Reactors from 100ml to 250 litres in

glass, stainless steel or Hastelloy.

• Wide temperature and pressure range: Reactions can be

heated to 500°C and pressurized up to 200 bar.

• Safe: Warning alarms and emergency cut-off values or

actions can be defined.

• Control: High torque stirring including torque

measurement.

• Measured: Dosing of gas, liquid or powder, with fully

automated or manual control.

• Pressurized: Reactions such as fully controlled

hydrogenations and carbonylations can be performed.

• Integrated: Can provide integrated pH and liquid control.

• Flexible Control: Manual or fully automated for

unattended operation.

• Easy to use software: "Drag and drop" icons allow recipes

to be created, edited and run intuitively.

• Empowering: Virtually any manufacturer’s apparatus can

be configured into a system using the software.

• Powerful: Apparatus such as pumps and balances can be

combined in an intelligent fashion (e.g. enabling

gravimetric dosing or dosing to maintain a pH).

• Automatic data logging: All responses such as

temperature, stirrer speed, pH, mass flow, etc. can be

graphically displayed in real time and are continually

saved to one .csv file.

Complete systems can include reactors, stirrers, circulators,

temperature probes, pumps, balances, sensors, etc. and be

integrated with pH and/or liquid control. With manual operation

or complete automation via the Atlas PC software, Syrris’ custom

reactor service will provide a highly adaptable solution for any

chemistry laboratory.

With over 200 man years of combined experience, Syrris chemists

and engineers manufacture the highest quality customized

systems. They are assembled to your specification and rigorously

tested at our facility before installation at your laboratory.

Custom Reactor System Benefits Custom Reactor Systems

Pre-Configured Devices

Virtually any RS232 device with ASCII communications can be

configured. A selection of pre-configured devices includes:

BalancesDenver Pinnacle and Summit

Series, Mettler PG 5001 and

PM series, Oxford Top Pan,

Sartorius CP and LP Series,

Kern PLS 2100-2, Ohaus

Ranger Count, A&D FX-iEP

Series, Precisa XB

CirculatorsHuber Ministat, Nuevo, Unistat,

etc. Thermo Haake Phoenix

II and DC50, Julabo F series,

Lauda Proline series, Eyela

PCC-7000


Diaphragm: ProMinent

gamma/I*,

Peristaltic: Cole Parmer

Masterflex, IKA, Watson Marlow

323Du & 520Du

Syrris FRX pump


Rotary/Piston: Ismatec MCP-

CPF

Overhead StirrersIKA Eurostar, CAT R80D-

PC, Heidolph RZR Control,

OptiChem Tempstir



Flow Meters and ControllersMeters: Aalborg GFM series*,

Sierra 820 series*,

Controllers: Aalborg DFM, Cole

Parmer 16 series, Ritter EDP 32

FP, Buchi BPC


NodeDenver 215E and 215,

Knick Portamess 913, Mettler

Toledo MPH 125 pH and

SevenEasy pH meter

TurbidityAtlas Turbidity Probe, Mettler

Toledo Trb8300*

Vacuum ControllerVacuubrand CVC2000 &

CVC3000


Temperature monitor, Syrris

7033 Dual channel RTD box




Powder doserLamda


www.syrris.com 69

Automated High Pressure Reactors Custom Reactor Systems

For automated high pressure reactor requirements outside of the range of Atlas

Pressure Systems (3bar glass reactors, -80°C to +200°C up to 3 litres or 200

bar Stainless or Hastelloy reactors, -80°C to +300°C up to 450ml), Syrris offers

High Pressure Custom Reactor Systems.

The requirements of the system can be defined in detail by the customer.

Every system is assembled and tested at our factory before installation at the

customer's facility by one of our engineers or chemists. Our systems offer

unrivalled ease of use and sophisticated automation.

The High Pressure Customer Reactor Systems generally fall into one of two

categories:

Glass High Pressure Systems

• Vessel Volume: 100ml to 1.6 litres

• Temperature Range: -40°C to +200°C

• Automation / Logging: Via Reactor Master PC software and/or Syrris

Reactor Master series

• Pressure Range: Vacuum to +12.0 barg

Metal High Pressure Systems

• Vessel Volume: 100ml to 10 litres


• Automation / Logging: Device management and automation using Reactor

Master, Reactor Master PC Software or a combination of both

• Pressure Range: Vacuum to 60 bar

• Materials: Stainless steel, Hastelloy, titanium

Features common to both

• Heating / Cooling: Jacket utilizing re-circulator

• Lid Design: Wide range of port options to suit your application

• Agitation: Overhead stirring: 50 to 2000 RPM (optional torque

measurement)

• Agitator Types: Anchor, retreat curve, 4 blade impellor etc. in glass, PTFE,

stainless steel etc.

• Temperature Measurement: Reactor contents, jacket inlet temperature etc.

• Liquid Feed: Volumetric dosing, gravimetric dosing

• Gas Feed: Pressure control, gas dosing, gas uptake monitoring, etc.

• Other: Condensers, distillation assemblies, re-circulation, IR, pH

measurement and control, turbidity, conductivity, calorimetry, etc.

The following modes of operation are possible for both types of pressure

reactor systems:

• Automatically Maintain a Pressure: By using the Atlas Pressure Control

Module a consistent pressure to the reaction is maintained over the reaction

period.

• Pressure Control with Mass Flow Monitoring: Maintain a pressure and

monitor mass flow. Ideal for gas uptake monitoring.

• Mass Flow Control: Dose a known quantity of gas using the mass flow

controller.

• Off Gas Monitoring: Monitor off-gases with mass flow meters.

• Manual or Automated Gas Selection: All of the above modes of operation

are compatible with the Atlas Gas Selection Module.

Automated High Pressure Reactors

www.syrris.com70

Custom Reactor Systems Case Studies

For automated atmospheric pressure reactor requirements outside of the

range of Atlas Systems (50ml to 5 litres) Syrris offers Custom Reactor Systems.

These systems are fully customizable, i.e. they can be defined in detail by the

customer.

Each system is fully assembled and tested at our factory before installation at

the customer's facility by one of our engineers or chemists.

Automated Atmospheric Pressure Reactors >5L:

• Vessel Volume: 5 litres to 250 litres


• Automation / Logging: Device management and automation using Reactor

Master, Reactor Master PC Software or a combination of both

• Pressure Range: Vacuum to +0.5 bar

• Heating / Cooling: Jacket utilizing re-circulator (optional vacuum jacket)

• Agitation: Overhead stirring: 50 to 2000 RPM (optional torque

measurement)

• Lid Design: Wide range of port options to suit your application

• Agitator Types / Materials: Anchor, retreat curve, 4 blade impellor etc. in

glass, PTFE, stainless steel etc.

• Liquid Feed: Volumetric dosing, gravimetric dosing

• Outlet Valve: Temperature compensated zero dead volume rising stem

bottom outlet valve in chemically resistant PTFE

• Gas Feed: Low pressure purge, gas sparge, gas evolution monitoring, etc.

• Other: Condensers, distillation assemblies, re-circulation, IR, pH

measurement and control, turbidity, conductivity, calorimetry etc.

Automated Atmospheric Pressure Reactors >5L

An automated reactor system with two interchangeable reactors of 5 litre and

10 litre volumes. Designed for use in the flavours and fragrance industry.


• Data logging of speed and torque of overhead stirrer

• Temperature dependent automated gravimetric dosing

• One lid and stand to fit two interchangeable vessels

Case Study 1

www.syrris.com 71

Case Studies Custom Reactor Systems

20 litre automated synthesis system for the defense industry. This included

high torque stirring, volumetric liquid addition and temperature monitoring and

logging.


• Process requires exact temperature control (large scale/fast flow rate

quench on standby)

• Atmospheric glass reactor (up to 200°C)

• Twin head high flow Peristaltic Pump

• Level sensor to quench cool for safety reasons

• pH titration

• Baffles

Case Study 2

High pressure (200 bar) and high temperature (500°C) continuous flow reactor.

Features: 5 gas feeds (automatically selected), one liquid feed, mass flow meter,

take off for Gas Chromatography, catalyst bed, 4 optical probes (supplied by

customer), full data logging and automation.


• Use on-line UV spectroscopy (4 x probes) to monitor heterogeneous

catalyst mechanisms

• Catalyst performance and degradation levels monitored

• Catalysts were being developed for use in industrial hydrogenation,

alkylation and hydro-treating pilot-scale reactors

Case Study 3

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An automated, 100 litre single jacketed glass reaction system (-20°C to

+200°C) with temperature dependent gravimetric dosing. Features included full

data logging, automation and distillation condenser.


• 100 litre single jacketed reactor

• Process temperature from -20°C to +200°C

• Custom pH probe

• Liquid feed and pH control

• Automation and logging

Case Study 4

5 litre Stainless Steel Oil Jacketed Reactor - operating at pressures up to 40 bar

and at temperatures up to 250°C with high torque stirring.


• Distillation column and condenser

• Volumetric liquid dosing

• Pressure control with gas selection

• Gas mass flow meter

• Torque monitoring

• High performance circulator

Case Study 5

www.syrris.com 73

Case Studies Custom Reactor Systems

1.5 litre high pressure (60 bar) and high temperature (350°C) stainless steel

jacketed reactor system with calorimetry.

Features: Automated pressure control (using the Atlas Pressure Control

Module), high torque overhead stirring with torque feedback, mass flow meter,

power compensation calorimetry, heat flow calorimetry and high pressure liquid

dosing.


• Polymerizations under pressure

• Understanding kinetics and calorimetry of some polypropylene

polymerizations

Case Study 6

20 litre, vacuum jacketed reactor with interchangeable stirrer configurations.

The system includes high torque stirring and is for use in a pharmaceutical

industry pilot plant.

Features: High performance condenser and oil jacket temperature

measurement. Can be upgraded to full automation by adding a Reactor Master

and PC software.


• Reaction optimization

• Process development

Case Study 7

Systems

www.syrris.com74


300ml, stainless steel, oil jacketed reactor with operating temperature of up to

200°C and pressures up to 200 bar for the petrochemical industry. The system

has data logging and full PC-controlled automation.

Features: Coriolis flowmeter to measure mass, density and temperature.


• Measurement of deformation of polymer samples under supercritical

conditions

• Supercritical carbon dioxide work

Case Study 8

100ml, stainless steel, jacketed reactor, pressurized using high purity helium for

reactions up to 200 bar and 250°C for the petrochemical industry.

Features: Automated pressure control (using the Atlas Pressure Control

Module), dual liquid feeds, volumetric dosing, gas selection and a mass flow

meter.


• Removing hydrocarbons from water

• Addition of water to oil water mixtures

• Pressurization using an inert gas

Case Study 9

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Automating Existing Systems

The Reactor Master Basic automates jacketed reactor systems from other

manufacturers and logs data without the need for PC software. Circulators, (e.g.

Julabo, Huber, Haake, Lauda etc.) stirrers, (e.g. Heidolph, IKA, Chemglass etc.),

thermocouples and RTDs from virtually any manufacturer can be controlled by

the twist and click knob. Data can be viewed in real time and downloaded to a

USB memory stick as a .csv file.

The circulator, overhead stirrer and thermocouples are connected to the rear

of the Reactor Master Basic. The circulator temperature and stirrer speed can

be set using the twist and click knob and displayed on the LCD screen. It is also

possible to set stirring and temperature profiles to run in a totally automated

fashion. A Reactor Master Basic System contains:


Reactor Master Basic 2200247

Options

Circulator Cable (see page 106)

Stirrer Cable (see page 106)

Reactor Master Basic

Reactors already owned by customers can be upgraded to perform automated

experiments, even without a PC. Choose the Atlas Syringe Pump for automated

reagent dosing and/or the Reactor Master for automation and data logging of

temperature, stirring and reagent addition. The Reactor Master PC Software

converts existing reactors into a totally controlled laboratory reactor.


2200247

www.syrris.com76


The Reactor Master Pro retains all the benefits of the Reactor Master Basic but

also has the following additional benefits:

• Reaction temperature control (not just circulator temperature)

• Ability to use Atlas RTD sensors

• Ability to use Atlas Turbidity sensors

• Ability to use Atlas pH sensors

• Ability to use Atlas Pressure sensors

• Ability to upgrade to PC software (to control other manufacturer’s

apparatus)

A better reaction temperature is achieved by “closed loop” (PID) control of

the reactor temperature sensor and the set point of the circulator (rather than

simple “open loop” setting of a circulator bath temperature).

Connection of Atlas RTDs, pH and turbidity probes is possible via a node

extension.

FeatureReactor Master

BasicReactor Master

Pro

Data logging ü üData download to USB memory stick ü üCompatible with data analysis software ü üControl of thermoregulator temperature ü ü2 x Thermocouples sockets ü üPID control of reaction temperature û ü2 x RTD sockets û üUpgrade to full PC software control possible û üpH meter compatible û üTurbidity sensor compatible û ü A Reactor Master Pro System contains:


Reactor Master Pro 2200248

Options

Circulator Cable (see page 106)

Stirrer Cable (see page 106)

Reactor Master Software 2600004

Atlas Syringe Pump 2200072

Atlas Syringe Pump XL 2200376

Reactor Master Pro 2200248

Syringe Pump

The Atlas Syringe Pump is a versatile volumetric dosing and/or sampling

system. It allows 2 independent refilling flows, one continuous flow, reaction

sampling, intelligent control of pH and temperature dependant dosing. It

consists of 2 syringes and multi port valves and can be controlled from the front

panel, by a Reactor Master, or the Reactor Master PC software.

See the Atlas Syringe Pump and Syringe Pump XL (pages 30) for more

information.

2200072

Systems

www.syrris.com 77



Reactor Master Software is an easy to use PC based application for control and

analysis of experiments. Whole systems including stirrers, circulators, RTDs,

pumps, balances etc. can be configured using virtually any manufacturer’s

apparatus. The “drag and drop” interface means recipes can be created,

changed and saved with the click of a mouse.

The Reactor Master Pro (2200248) can control reaction profiles and log data.

The Reactor Master Software (which can operate with or without the Reactor

Master Pro) provides whole system control, configuration and analysis allowing

sophisticated experiments to be performed. Almost all RS232 controlled

apparatus and analogue sensors can be connected to the software via a simple

Port (2101020) which plugs into the computer’s USB connection. This allows

automation of any compatible laboratory apparatus with full recipe control.

Running reactions from the Reactor Master Software allows all responses such

as temperature, stirrer speed, pH and mass flow to be continuously monitored

and graphically displayed in real time. Data can also be used to trigger other

actions e.g. a pump and a balance can be combined to perform gravimetric

dosing. Apparatus is configured (including alarms and emergency control)

using a simple “drag and drop” interface. Recipes can be created, changed and

saved with the click of a mouse. Recipes can be run, paused or stopped and all

experimental parameters may be altered ‘on the fly’ during the experiment. All

reaction data is continuously logged to .csv data files making analysis easy.

Virtually any RS232-enabled device with ASCII communications can be

configured, the current list of pre-configured devices is below:

2600004

BalancesDenver Pinnacle and Summit Series,

Mettler PG 5001 and PM series, Oxford

Top Pan, Sartorius CP and LP Series,

Kern PLS 2100-2, Ohaus Ranger

Count, A&D FX-iEP Series, Precisa XB

CirculatorsHuber Ministat, Nuevo, Unistat, etc.

Thermo Haake Phoenix II and DC50,

Julabo F series, Lauda Proline series,

Eyela PCC-7000


Diaphragm: ProMinent gamma/I*,

Peristaltic: Cole Parmer Masterflex,

IKA, Watson Marlow 323Du & 520Du

Syrris FRX pump


Rotary/Piston: Ismatec MCP-CPF

Overhead StirrersIKA Eurostar, CAT R80D-PC, Heidolph

RZR Control, OptiChem Tempstir




Flow Meters and ControllersMeters: Aalborg GFM series*, Sierra

820 series*,

Controllers: Aalborg DFM, Cole Parmer

16 series, Ritter EDP 32 FP, Buchi BPC


NodeDenver 215E and 215, Knick

Portamess 913, Mettler Toledo MPH

125 pH and SevenEasy pH meter

TurbidityAtlas Turbidity Probe, Mettler Toledo

Trb8300*

Vacuum ControllerVacuubrand CVC2000 & CVC3000


Temperature monitor, Syrris 7033 Dual

channel RTD box



Powder doserLamda


Systems

www.syrris.com78


Reactor Master COM Port Software

The Reactor Master COM Port Software has the same functionality as Reactor

Master Software (2600004) with the exception that it uses RS232 connection

directly to the PC rather than via an Atlas Port (2101020). Although more

difficult to set-up, this is favoured (both technically and because it becomes

more cost effective) when 4 or more RS232 devices are required. Choose the

regular Reactor Master Software (2600004) when up to 3 RS232 devices are to

be used.

Due to the nature of setting up the Reactor Master COM Port Software, it is

recommended that this is performed by Syrris engineers on a PC purchased

from Syrris (2200599). The Reactor Master COM Port Software is designed for

use with the following part: Ethernet to 8 RS232 Ports for use with COM Port

Software and Set Up (2200351).


Reactor Master COM Port Software

Ease of set up?

Easy Requires Syrris Engineer

Control of 1-3 RS232 Devices

Less Expensive More Expensive

Control of 4+ RS232 Devices

More Expensive Less Expensive

RD2600023

Set up of system using Reactor Master Software

Set up of system using Reactor Master COM Port Software

Text goes here...

systems

Atlas and Globe are modular synthesis systems allowing parts to be quickly changed for different applications. Interchangeable modules can be configured into a wide range of systems, offering chemists ultimate reaction flexibility.

All of the parts in this section are compatible with both Atlas and Globe, allowing full interchange between these product families. A compatibility chart, showing which temperature probes and stirrers fit each reactor size is included for reference.

atlas and globecommon parts

Modules

www.syrris.com80

Atlas and Globe Common Parts Jacketed Vessels and Lids

Jacketed Vessels

Jacketed Vessels and Lids

Syrris' Jacketed Vessels have been designed with a number of features to

improve productivity and safety.

• Easy to use quick release oil connections.

• Chemically resistant zero dead volume bottom outlet.

• Easy to fit into the Jacketed Vessel Clamp, using lift and lock mechanism.

• Sprung bottom outlet valve offers leak free operation.

• The jacket height extends to cover the stated reactor volume.

• O-ring sealing groove for vacuum operations.

• Torispherical, dished, conical and round bottom profiles available.

Other designs such as split jacket and custom vessel profiles are available on

request.

• Jacket Temperature range: -40°C to +200°C by default. The temperature

range can be extended to -80°C with a low temperature upgrade kit or up

to +250°C with a high temperature upgrade kit.

• Wetted materials: Borosilicate 3.3 Glass, PTFE and FFKM

Most Syrris Jacketed Vessels fit both Atlas and Globe. Because of the unique

profile of some Syrris Jacketed Vessels they must be used with either an Atlas

Remote Mount or a Globe Offset Assembly. Please see the table below to

understand if these modules are required.

Part Numbers

Suitable for Atlas

Suitable for Globe

Suitable for Atlas with Remote Mount

Suitable for Globe with

Offset Assembly

Key

2200639

2200640

2200641

RD2200469

û û û ü Δ

2200253

2200074

2200048û û ü ü *

2200027 û ü ü ü

All other vessels

(not 3 bar)ü ü ü ü

Modules

www.syrris.com 81

Jacketed Vessels - Round Bottom

Round bottom vessels are traditionally used in most process development

laboratories and give excellent mixing when used with most stirrers.

100ml - Round Bottom 2101525



1 litre - Round Bottom 2101532



5 litre - Round Bottom* 2200253

This vessel has a high length to diameter ratio making it ideally compatible for

the Atlas Remote Mount. This vessel is suitable for use with Atlas (only using

the Remote Mount) and is suitable for use with Globe (only using the Globe

Offset Assembly). See 2200074 for smaller length to diameter ratio.

5 litre - Round Bottom Δ 2200639

This vessel has a low length to diameter ratio and are suitable for use with

Globe (the Globe Offset Assembly is required). Note this vessel cannot be used

with Atlas.

Suitable for Globe, Atlas with Remote Mount and Globe with Offset Assembly

* Suitable for Atlas with Remote Mount and Globe with Offset Assembly

Δ Suitable for Globe with Offset Assembly

www.syrris.com82


Jacketed Vessels - Vacuum Jacket

Vacuum Jacketed Vessels feature a dished bottom for mechanical strength

whilst the vacuum jacket provides insulation and prevents both fogging

and icing of the outer surface at low temperatures. Ideal for calorimetry

applications.

100ml - Vacuum Jacket - Dish Bottom 2200023



1 litre - Vacuum Jacket - Dish Bottom 2200026

2 litre - Vacuum Jacket - Dish Bottom 2200027

5 Litre - Torispherical Bottom Δ 2200640

These vessels have a low length to diameter ratio and are suitable for use with

Globe (the Globe Offset Assembly is required). Note these vessels cannot be

used with Atlas.

5 litre - Vacuum Jacket - Dish Bottom Δ 2200641

These vessels have a low length to diameter ratio and are suitable for use with

Globe (the Globe Offset Assembly is required). Note these vessels cannot be

used with Atlas.

Jacketed Vessels - Torispherical Bottom

Torispherical bottom vessels provide a good mimic to many pilot scale reactors

and are the ideal vessel for scale-up studies

50ml - Torispherical Bottom 2200184




1 litre - Torispherical Bottom 2200188

2 litre - Torispherical Bottom 2200189

Suitable for Globe, Atlas with Remote Mount and Globe

with Offset Assembly

* Suitable for Atlas with Remote Mount and Globe with

Offset Assembly


www.syrris.com 83

Jacketed Vessels - Conical Bottom

Conical bottom vessels allow low fill volumes to be used with good stirring.

250ml - Conical Bottom 2200019

500ml - Conical Bottom 2200020

1 litre - Conical Bottom 2200021

Jacketed Filtration Vessel 3 litre* 2200048

The Atlas Jacketed Filtration Vessel has a removable bottom with a glass

support to allow materials to be filtered through a filter paper, glass sinter or

solid bed. The vessel is plastic coated. Other sizes are available on request.

Jacketed Vessels and Lids Atlas and Globe Common Parts

Stainless Steel Jacketed Vessels - Torispherical Bottom

The stainless steel range of jacketed vessels, manufactured from 316 stainless

steel are designed to fit into the regular Jacketed Vessel Clamp (2101012), or

the Globe Frame Assembly (2200507) and be used with the regular Jacketed

Vessel Lids (2101030 or 2101594). These vessels are rated to 200°C but can be

used up to 250°C with the Atlas Jacketed Reactor High Temperature Upgrade

Kit (2200330).

100ml - Stainless Steel - Torispherical Bottom RD2200464



1 litre - Stainless Steel - Torispherical Bottom RD2200467

2 litre - Stainless Steel - Torispherical Bottom RD2200468

5 litre - Stainless Steel - Torispherical Bottom Δ RD2200469

Jacketed Vessel 5 Litre Dished Bottom* 2200074

Suitable for Globe, Atlas with Remote Mount and Globe

with Offset Assembly

* Suitable for Atlas with Remote Mount and Globe with

Offset Assembly


www.syrris.com84

Jacketed Vessel Lid (UK & EU) 2101030

The Vessel Lids fit all Jacketed Vessels and locate within the Jacketed Vessel

Clamp (2101012). They seal against the top of the Jacketed Vessels using a

Reaction Vessel Seal in FEP (2101016) or FFKM (2101543). The Jacketed Vessel

Lid (UK & EU) has 7 ports in total:

• 1 x vertical B24 centre port for the Stirrer Seal and Guide

• 3 x B19 ports designed for probes, sensors and condensers and are set

at an angle of 15° with a compound angle of 5° to avoid clashing with

items in other ports or the stirrer

• 1 x B29 port for larger probes, condensers or manual additions

• 2 x vertical GL18 ports designed to accept Atlas Jacketed Reactor

Baffles or other devices with suitable adaptors

Jacketed Vessel Lid (US) 2101594


Atlas Jacketed Reactor High Temperature Upgrade Kit 2200330

One pair of high temperature sidearm nuts enable jacket temperatures up to

250°C. Not suitable for use with 3 Bar Jacketed Vessels.

Custom Lid for Jacketed Vessel 2200006

If the fittings in the standard lid (above) do not match the requirements

of an application, custom lids, designed to individual specifications can be

manufactured. Contact Syrris for further details.

Stirrers

The Stirrer Seal and Guide holds a standard 8mm PTFE, or glass stirrer shaft

and gives a chemically resistant, vacuum tight seal onto a standard round

bottom flask or jacketed vessel lid. An auto-aligning, quick release mechanism

allows stirrers to be rapidly changed or adjusted for height as required.

The Stirrer Seal and Guide requires a Scorpion Overhead Stirrer (2101004), or

High Torque Stirrer.

2101011Stirrer Seal and Guide

The Vessel Lids fit all Jacketed Vessels and locate within the Jacketed Vessel

Clamp (2101012). They seal against the top of the Jacketed Vessels using a

Reaction Vessel Seal in FEP (2101016) or FFKM (2101543). The Jacketed Vessel

Lid (US) has 7 ports in total:

• 1 x vertical B24 centre port for the Stirrer Seal and Guide

• 1 x A19 port and 2 x A24 ports designed for probes, sensors and

condensers and are set at an angle of 15° with a compound angle of 5° to

avoid clashing with items in other ports or the stirrer.

• 1 x A29 port for larger probes, condensers or manual additions

• 2 x vertical GL18 ports designed to accept Atlas Jacketed Reactor

Baffles or other devices with suitable adaptors

www.syrris.com 85

Stirrer - PTFE 2 Blade Centrifugal 300mm 1802059

Stirrer - PTFE 4 Blade Propeller 300mm x 40mm dia 1802014



Stirrer - PTFE Anchor 300mm x 80mm dia 1802056



Stirrer - PTFE 3 Blade Retreat Impeller 400mm x 75mm dia 2101585



Stirrer - Glass 4 Blade Propeller 300mm x 27mm 2200285

Stirrer - Glass Anchor 300m x 36mm 2200286

Stirrer - Glass 3 Blade Retreat Impeller Cut Length x 45mm dia 2101523

Stirrer - Glass 3 Blade Retreat Impeller Cut Length x 75mm dia 2200085

Syrris' PTFE stirrers have steel shafts for strength and a thick PTFE coating for

chemical resistance. The maximum recommended stirring rate used for all glass

stirrers is 500rpm.

The glass stirrers are cut to length by Syrris before shipment (please specify

reaction vessel and desired stirring height from the bottom of the vessel when

placing an order). Glass stirrers are required for work under vacuum.

All stirrers are compatible with the Stirrer Seal and Guide (2101011). Custom

profile stirrers are available on request.

Stirrers Atlas and Globe Common Parts



www.syrris.com86

Temperature Node 2101021

The Temperature Node allows RTD probes to be connected as described above.

2200071pH and Temperature Node

The pH and Temperature Node allows pH and temperature probes to be

connected as described above. This module consists of a pH Node and a

Temperature Node and can be used to measure either pH or temperature, or

both. When used together, the pH is automatically temperature compensated.

The functionality of the Temperature Node is exactly the same as the

independent Temperature Node (2101021). The pH Node can measure pH values

from 0 to 14, has a 2 point user calibration and can read to better than 0.1 pH

accuracy, dependent upon calibration.

Probes and Nodes

The Syrris range of probes are designed for use with the Atlas Base, Reactor

Master or Atlas Syringe Pump. All probes must always be connected via their

corresponding node. When connected, the value detected by the probe (such

as temperature, pH, turbidity or pressure) is displayed on the front screen of the

module it is plugged into. The data is also logged by the module so that it can

be downloaded via a USB memory stick.

A single node can be connected to an Atlas base or up to 3 or 6 nodes can be

connected via node extensions using a Triple Node Socket or Six Way Node

Socket respectively.

Nodes must be connected to a Reactor Master or Atlas Syringe Pump using a

node extension. Up to 3 or 6 nodes can be connected via node extensions using

a Triple Node Socket or Six Way Node Socket respectively.

Multiple nodes of the same type connected to a single module (such as an Atlas

Base) can each be named to prevent confusion. If more than one node is being

used, they can be clipped to the Support Rods (2101009) using a Node Clip

(2200200).

Turbidity Node

The Turbidity Node allows the Turbidity Probe (2200156) to be connected

as described above. Turbidity is the cloudiness or haziness of a fluid caused

by individual particles and therefore this node in combination with the

corresponding probe is ideal for monitoring crystallization processes.

2200157

Atlas and Globe Common Parts Probes and Nodes

Probes & Nodes

www.syrris.com 87

Node Extension 2101023

The Node Extension allows nodes to be connected to a Triple Node Socket

(2101024), a Six Way Node Socket (2200259), Atlas Syringe Pumps or the

Reactor Master Pro. The Node Extension includes a clip to connect it to the

Support Rods (2101009).

The Triple Node Socket connects to the node port at the rear right of the Atlas

Base Unit (2101000) and can be used to connect up to three Nodes; i.e. one or

many temperature, pH and temperature, turbidity or pressure nodes up to a

combined total of 3 to the base via Node Extensions (2101023).

It can also be used to connect multiple nodes to an Atlas Syringe Pump or

Reactor Master Pro (via a node extension).

2101024Triple Node Socket

Node Clip 2200200

The Node Clip allows the Node Extension (2101023) sockets to be clipped to

the Support Rods (2101009). This is useful when using more than one node.

The Six Way Node Socket connects to the node port at the rear right of the

Atlas Base Unit (2101000) and can be used to connect up to six Nodes; i.e. one

or many temperature, pH and temperature, turbidity or pressure nodes up to a

combined total of 6 to the base via Node Extensions (2101023).

It can also be used to connect multiple nodes to an Atlas Syringe Pump or

Reactor Master Pro (via a node extension).

Six Way Node Socket 2200259

Probes and Nodes Atlas and Globe Common Parts

RTD Probe - Stainless Steel 100mm x 3mm for Dry Baths or Tj

The 100mm x 3mm Stainless Steel RTD probe can be used with the Stacking

Dry Bath (2101041), Triple Dry Bath (2101042) and Orbit Systems for accurate

temperature control. It can also be used with the Connector - Oil Pipe to

Jacketed Vessel (2200018) to monitor the temperature of circulator fluid as it

enters the reactor jacket (Tj). This is used in Heat Flow Calorimetry (HFC).

2101593

www.syrris.com88

A range of different size PTFE coated RTD Probes are available. These are fitted

with a specialist connector for connection to a Temperature Node (2101021).

Note that the RTDs have various diameters and should be used with the

corresponding probe holder. The 100mm probe (2101586) is ideal for use within

condensers or for headspace temperature measurement.

See the compatibility chart (see page 108) to match reaction vessel with

probe length.

RTD Probes - PTFE Coated

Atlas and Globe Common Parts Probes and Nodes

pH Probe - 400mm x 12mm with Swivel Adaptor 2200029

pH Probe - 200mm x 8mm with B19 Holder 2200054

These pH Probes connect to the pH and Temperature Node (2200071). The

swivel adaptor allows its angle to be adjusted within a jacketed reactor. These

combination probes have a AgCl reference, temperature range of 0°C to 70°C

and a pH range of 0 to 14. Response time of the probe is typically less than

45 seconds. For a pH probe compatible with 3 bar systems, please see the

Pressure Parts section.

Turbidity Probe - 400mm 2200156

The Turbidity Probe can be used as a simple crystallization point detector, or

in more complex studies involving metastable crystallization zones, secondary

nucleation and polymorphism issues. It requires a Turbidity Node (2200157)

and has a two point calibration. The stainless steel probe has a chemically-

protective borosilicate glass sheath, with a 7mm outside diameter. Suitable for

temperatures ranging from -50°C to + 250°C. Please note this is a reflection

probe for use in liquids. It is an IR Emitter operating at 950nm. For a Turbidity

probe compatible with 3 bar systems, please see the Pressure Parts section.

RTD Probe - PTFE Coated 100mm x 6mm 2101586






www.syrris.com 89

Heating Capacity: 3000w

Cooling Capacity: 250 200 100 0 -20 -40 -60 -75 °C

600 600 600 650 600 600 300 60 W

Flow Rate: 55 l/min

Temperature Range: -75°C to +250°C

Minimum Filling Volume (including Expansion Tank)*: 1.5 litres (2.8 litres)

Dimensions (W x L x H): 42.5 x 40 x 72cm

Huber Circulator - Unistat 705 (230V 1Ph 50Hz) 2200439

Huber Circulator - Unistat 705 (208V 2Ph 60Hz) 2200440

Huber Circulator - Unistat Tango Nuevo (230V 1Ph 50Hz) 2200441

Huber Circulator - Unistat Tango Nuevo (208V 2Ph 60Hz) 2200442


Cooling Capacity: 250 200 100 0 -20 -40 °C

700 700 700 700 400 60 W

Flow rate: 55 l/min


Minimum Filling Volume (including Expansion Tank)*: 1.5 litres (4.3 litres)

Dimensions (W x L x H): 42.5 x 27 x 63.6 cm

Circulators - Huber are Syrris' preferred circulator supplier

Huber Circulator - Unistat Petite Fleur (230V 1Ph 50Hz) 2200366




Cooling Capacity: 200 150 100 50 20 0 -20 -30 °C

480 480 480 480 480 450 270 160 W

Flow Rate: 33 l/min


Minimum Filling Volume* (including Expansion Tank): 1.5 litres (3.5 litres)

Dimensions (W x L x H): 26 x 45 x 50.4cm

Circulators Atlas and Globe Common Parts

*Note: A further 0.7 litres to 2.5 litres is required to fill the vessel jacket and pipes

(dependent on vessel size)

www.syrris.com90

Huber Circulator - CC510 (400V 3Ph 50Hz) 2200444



Cooling Capacity: 100 20 0 -20 -40 °C

2100 2100 2100 1000 400 W

Flow rate: 31 l/min


Filling Volume (including Expansion Tank)*: 18 litres (29 litres)

Dimensions (W x L x H): 45.5 x 51.5 x 101.4cm

Huber Circulator - CC505 (230V 1Ph 50Hz/60Hz) 2200446




1200 1200 1000 600 150 W

Flow rate: 33 l/min


Filling Volume*: 5 litres

Dimensions (W x L x H): 41 x 48 x 76.4cm

Atlas and Globe Common Parts Circulators

Huber Circulator - Ministat 240-cc-NR (230V 1Ph 50/60Hz) 2200448


Cooling Capacity: 100 20 0 -10 -20 -30 -40 °C

600 600 550 420 350 125 50 W

Flow Rate: 27 l/min


Minimum Filling Volume (Filling Volume)*: 4.5 litres (4.9 litres)

Filling Volume (including Expansion Tank)*: 7.3 litres

Dimensions (W x L x H): 30 x 46.5 x 51.6cm



Huber E-Grade Exclusive Upgrade for Ministat and CC 2200663

The Huber E-Grade upgrade enables the reaction temperature to be controlled

from the front panel of a Huber, when a temperature probe is connected

directly to the circulator. This is only required for ministats when used in a

manual system like Globe. Please order the Huber E-Grade upgrade for CC and

Ministat (2200663) with the Circulator.

www.syrris.com 91

Overflow Displacement Tank - Ministat 125 RD2200596



The Ministat Overflow Displacement Tanks allow easy draining of circulator

from the jacketed vessels on Atlas or Globe. When draining the circulator fluid

from the jacketed vessel using the Atlas or Globe oil drain units, the Overflow

Displacement Tank allows the circulator fluid to return to the circulator without

overfilling/overflowing the bath. The addition of a displacement tank will also

increase temperature performance as it reduces the overall volume of fluid

used.

Ministat Overflow Displacement Tanks


Huber Circulator - Ministat 230-cc (115V 1Ph 60Hz) 2200453


Cooling Capacity: 100 20 0 -10 -20 -40 °C

420 420 380 330 250 50 W

Flow Rate: 27 l/min


Minimum Filling Volume (Filling Volume)*: 2.8 litres (3.2 litres)

Filling Volume (including Expansion Tank): 4.5 litres

Dimensions (W x L x H): 25.5 x 45 x 47.6cm


Huber Circulator - Ministat 125-cc (100-115V 1Ph 50-60Hz) 2200454



300 300 210 150 50 W

Flow Rate: 27 l/min


Minimum Filling Volume (Filling Volume)*: 2 litres (2.75 litres)


Dimensions (W x L x H): 22.5 x 37 x 42.9cm




www.syrris.com92


Cooling Capacity: 200 20 0 -20 -40 -60 °C

1200 1200 1200 1100 1100 650 W

Flow Rate: 40 l/min



Dimensions (W x L x H): 43 x 65 x 126cm

Platinum Circulator (Presto A80) 230V / 50Hz 2200215

Platinum Circulator (Presto A80) 230V / 60Hz 2200216

Heating Capacity: 3000W

Cooling Capacity: 20 0 -20 -40 °C

2000 1500 1000 260 W

Flow Rate: 22-26 l/min



Dimensions (W x L x H): 46 x 55.1 x 89cm

Gold Cold Circulator (Julabo FP51-SL) 400V / 50Hz / 3Phase 2200013

2200003Gold Cold Circulator (Julabo FP51-SL) 230V / 60Hz / 3Phase

Gold Circulator (Julabo Presto A40) 230V 50/60Hz - UK 2200606

Gold Circulator (Julabo Presto A40) 230V 50/60Hz - EU 2200607

Gold Circulator (Julabo Presto A40) 208V 60Hz - US 2200608


Cooling Capacity: 200 100 20 0 -20 -30 -40 °C

1200 1200 1200 1100 500 300 100 W

Flow Rate: 16 - 40 l/min


Filling Volume (including Expansion Tank)*: 3.5 litres (6.2 litres)

Dimensions (W x L x H): 32.2 x 58.1 x 66cm




www.syrris.com 93

Heating Capacity: 2000w (1000w at 115V)


900 800 500 160 W

Flow rate: 22-26 l/min




2200499Silver Circulator (Julabo FP50-HL) 230V / 60Hz

2200498Silver Circulator (Julabo FP50-HL) 230V / 50Hz

Bronze Circulator (Julabo CF41) 115V / 60Hz 2200222



470 400 280 120 W

Flow Rate: 22 - 26 l/min


Filling Volume*: 5.5 litres


2200223Bronze Circulator (Julabo CF41) 230V / 50Hz

Bronze Circulator (Julabo CF41) 230V / 60Hz 2200500

Circulator (Julabo CF40) 115V / 60Hz 2200001

Circulator (Julabo CF40) 230V / 50Hz 2200011

2200191Circulator (Julabo CF40) 100V / 60Hz



470 400 280 120 W

Flow Rate: 15 l/min




2200501Circulator (Julabo CF40) 230V / 60Hz


www.syrris.com94

2200225Copper Circulator (Julabo CF30) 115V / 60Hz

Copper Circulator (Julabo CF30) 230V / 50Hz 2200226



Cooling Capacity: 20 0 -20 °C

320 250 150 W

Flow Rate: 15 l/min





Circulator Fluid

Syrris offers a range of circulator fluids for different temperature ranges, open

or closed bath circulators and Julabo or Huber circulators. Please contact Syrris

if your requirements are not met by the range of circulator fluids shown.

Julabo -40 to +250°C Closed Bath Presto, 10 Litres 2200483

Julabo -85 to +170°C Closed Bath Presto, 10 Litres 2200484

Huber -60 to +115°C for Open Baths, 10 Litres 2200485



Huber +20 to +275°C for Open Baths, 10 Litres 2200488

Huber DW-Therm (-90 to +200°C) for Closed Baths, 10 Litres 2200489

Julabo +20 to +250°C for Open Baths, 10 Litres 2200163

Julabo -50 to +105°C for Open Baths, 10 Litres 2200164

Julabo -20 to +180°C for Open Baths, 10 Litres 2200165




www.syrris.com 95

2200269Heidolph RZR 2051 Control Overhead Stirrer (110V / US)

Heidolph RZR 2052 Control Overhead Stirrer (230V / EU) 2200268

2200267Heidolph RZR 2051 Control Overhead Stirrer (230V / EU)

Heidolph RZR 2052 Control Overhead Stirrer (230V / UK) 2200255

Heidolph RZR 2051 Control Overhead Stirrer (230V / UK) 2200254

The Heidolph RZR Control Overhead Stirrer, offer a higher torque (with torque

measurement) alternative to the standard Atlas or Globe overhead stirrers.

With an Atlas system, the Heidolph Stirrers are used in conjunction with a High

Torque Stirrer Adaptor for Heidolph Stirrers (see page 26), and replace the

Scorpion Overhead Stirrer (see page 25). With a Globe system, the Heidolph

stirrers are used in conjunction with Heidolph 2051/2052 Stirrer Mount for

Globe (see page 65) and replace the Bronze, Silver or Gold Globe stirrers

(see page 63).

The Heidolph 2051 has a maximum speed of 2000 RPM and maximum torque

of 40 Ncm (peak overload) / 20 Ncm (continuous) with feedback. The Heidolph

2052 has a maximum speed of 1000 RPM and maximum torque of 180 Ncm

(peak overload) / 90 Ncm (continuous) with feedback. Control is possible via

the front panel of the stirrer, by the Atlas Software 1 (2300102) or Reactor

Master Software (2600004) using an Atlas Port (2101020) or from the Reactor

Master. Note that control is not possible from the Atlas Base Unit. For high

torque applications, please contact Syrris to confirm system specifications.

2200270Heidolph RZR 2052 Control Overhead Stirrer (110V / US)

Denver Summit Balance SI-4002 2200043

The Denver Summit Balance can be connected to the PC via a Port (2101020)

for control using the Atlas Software 1 (2300102) or Reactor Master Software

(2600004). It can be combined with the Watson Marlow Peristaltic Pump 323/

DU/D (see above) to enable gravimetric dosing of a reagent.

• Weighing capacity: 4000g

• Readability: 0.01g

Watson Marlow Peristaltic Pump 323/DU/D 1802045

The Watson Marlow Peristaltic Pump 323/DU/D can be connected to an Atlas

or Globe system to provide pumping of a wide range of liquids into any type

of vessel. The pump can provide pumping rates from rates from 1ml/min up to

2L/min depending on the tubing used. An extension module (1802046) can be

used to pump multiple liquids simultaneously (see page 96 for tubing).

3 Roller Extension Head for Watson Marlow 323/DU/D 1802046

Extension pump head for multi-channel pumping.

Other 3rd Party Hardware

3rd Party Hardware Atlas and Globe Common Parts

www.syrris.com96

Fluorinated Tubing 1.6mm bore (5m) 1802047



Syrris provides a range of tubing suitable for use in peristaltic pumps. This

chemically resistant tubing (contact Syrris for compatibility details) is available

in a range of sizes for different pumping requirements. This tubing is ideal for

use with Watson Marlow Pumps (1802045).

Transformer 3000W 2200367

This transformer may be used with third party apparatus e.g. Julabo or Huber

circulators where the voltage input on the apparatus is not compatible with the

laboratory supply. Please confirm compatibility of apparatus and supply with Syrris before purchase.

• Capacity: 3000 watts

• Input: 110/200/220/240 Volt

• Output: 110/220-240 Volt

• Dimensions (W x H x D): 19 x 16 x 25 cm

• Weight: 17Kg

Atlas and Globe Common Parts

3 Bar Gas Pressure Control Module 2200497

The Gas Pressure Control Module automatically manages the dosing of gas into

and out of the reactor to control the pressure within the reactor. There are 3

modes:

1) Set min. pressure and max. pressure - In this mode the inlet valve is opened

if the pressure drops below the min. pressure and opens the outlet valve if the

pressure is above max. pressure.

2) Vent - This closes the inlet valve and opens the outlet valve.

3) Purge - This opens both the inlet and outlet valves.

The Pressure Control Module can be controlled from the twist and click knob

or connected to a PC via an Atlas Port to be controlled by the Atlas or Reactor

Master Software. Valves are manufactured from 316L stainless steel. Rated to 3

bar.

• Maximum input pressure: 200 Bar

• Maximum pressure read by the sensor: 10 Bar

• Maximum settable pressure: 3 Bar

• Pressure set to/displayed to increments of: 0.1 Bar

Pressure Parts

Stirrer Seal and Guide Stainless Steel (3 Bar System) 2200334

The Stirrer Seal and Guide is rated to 3 bar and is designed for use with the

3 Bar Jacketed Vessel Lid (2200664). The material exposed to the reactor is

stainless steel 316. The top of the Stirrer Seal and Guide fits the Scorpion Stirrer

(or other stirrers such as Heidolph stirrers with the correct adaptor).



• Maximum 3 bar system temperature: +200°C

www.syrris.com 97

Pressure Parts Atlas and Globe Common Parts

Stirrer Seal and Guide PTFE (3 Bar System) 2200405

The Stirrer Seal and Guide is rated to 3 bar and is designed for use with the

3 Bar Jacketed Vessel Lid (2200664). The material exposed to the reactor is

PTFE for maximum chemical resistance. The top of the Stirrer Seal and Guide

fits the Scorpion Stirrer (or other stirrers such as Heidolph stirrers with the

correct adaptor).




Gas Selection Module 2200375

The Gas Selection Module allows 3 gases to be permanently connected to the

module yet only one gas connected to the reactor at any one time. It can be

controlled from the twist and click knob to select Gas 1, Gas 2, Gas 3 or None.

Alternatively it can be connected to a PC via an Atlas Port to be controlled by

the Atlas or Reactor Master Software.

Each gas has a flow regulator, the valves are constructed from 316L stainless

steel and the unit is rated to 200 bar. Note: when using with Hydrogen, the

maximum allowable pressure is limited to 100 bar.

Jacketed Vessel Round Bottom (Rated to 3 Bar)

There is a range of jacketed reactor vessels that are rated to 3 bar and are

designed for use with the 3 Bar Atlas Jacketed Vessel Clamp (2200333) or

Globe 3 Bar Frame Assembly (2200508) and 3 Bar Jacketed Vessel Lid and

Safety Manifold (2200664).

100ml - Round Bottom (Rated to 3 Bar) 2200411



1 Litre - Round Bottom (Rated to 3 Bar) 2200331



www.syrris.com98

Vacuum Jacketed Vessel Round Bottom (Rated to 3 Bar)

There is a range of jacketed reactor vessels that are rated to 3 bar and are

designed for use with the 3 Bar Atlas Jacketed Vessel Clamp (2200333) or

Globe 3 Bar Frame Assembly (2200508) and 3 Bar Jacketed Vessel Lid and

Safety Manifold (2200664).

100ml - Vacuum Jacket - Round Bottom (Rated to 3 Bar) 2200415



1 litre - Vacuum Jacket - Round Bottom (Rated to 3 Bar) 2200338

2 litre - Vacuum Jacket - Round Bottom (Rated to 3 Bar)* 2200416

3 litre - Vacuum Jacket - Round Bottom (Rated to 3 Bar)* 2200417

Atlas and Globe Common Parts Pressure Parts

Atlas 3 Bar System Safety Enclosure 2200694

Globe 3 Bar System Safety Enclosure 2200695

The safety enclosures for the Atlas and Globe 3 bar systems offer a compact

and safe shield when pressurizing vessels and facilitate easy access for

changing vessels between experiments. Essential for all 3 bar pressure systems.

SS 3 bar Jacketed Vessel Lid and Safety Manifold 2200664

The Jacketed Vessel Lid and Safety Manifold for the 3 bar system is designed

for use with the Jacketed Vessel Clamp for the 3 bar system (2200333) or

Globe 3 Bar Frame Assembly (2200508). The lid has 7 ports:

• 1 x vertical M30 centre port for the 3 bar Stirrer Seal and Guide

• 3 x GL18 ports designed for probes, sensors and condensers and are set at

an angle of 15° with a compound angle of 5° to avoid clashing with items in

other ports or the stirrer

• 1 x GL25 port for larger probes, condensers or manual additions

• 2 x vertical GL18 ports designed to accept Syrris probes

The lid and safety manifold, are manufactured from 316 stainless steel. The

safety manifold includes a pressure relief valve to gradually release gas in the

case of over-pressure and a safety burst disc that ruptures in the case of rapid

overpressure to protect the vessel and the user.

*Note: These vessels are only suitable an Atlas 3 bar system with the Remote Mount

or Globe 3 Bar Frame Assembly.

www.syrris.com 99

3 Bar Dip Tube for Autosampling 2200373

The 3 Bar Dip Tube for Autosampling consists of a PTFE pipe in a glass tube.

This can be located in one of the lid ports and allow samples to be sequentially

aspirated by the Atlas Syringe Pump (2200072) and dispensed to the

Autosampler Module (2200196). It can also be used for liquid or gas addition.

Pressure Node for 3 Bar System 2200706

The Pressure Node for 3 Bar System connects to the Atlas Base or Reactor

Master and when used with the Pressure Sensor for 3 Bar System (2200370)

allows the Atlas Base or Reactor Master to display pressure in real time on

the screen and log pressure data continuously. When used with the Reactor

Master or the Atlas Base with other nodes the Pressure Sensor requires a Node

Extension (2101023) and Triple Node Socket (2101024).

3 Bar System Starter Kit 2200409

The 3 Bar System Starter Kit contains a selection of pipes and fittings that are

rated to at least 3 bar and allow gas connections between gas sources and

modules. The kit includes ¼" OD PTFE tube, ¼" OD SS tube, ¼" push-fit to

threaded connections and a selection of Swagelok fittings to make joints from

the Jacketed Vessel Lid and Safety Manifold (2200664) and the ¼" tube.


Pressure Sensor for 3 Bar System 2200370

The Pressure Sensor for 3 Bar System connects to the Pressure Node for 3 Bar

System to allow the Atlas Base or Reactor Master to display pressure in real

time on the screen and log pressure data continuously.

www.syrris.com100

Probe Holders (3 Bar System)

The 3 Bar Probe Holders allow probes such as the PTFE RTD probes to be held

securely in a vessel by the 3 Bar Jacketed Vessel Lid (2200664). The holders

screw into the lid using a GL18 thread and provide a chemically resistant seal to

3 bar. The only wetted part is PTFE.

6mm Probe Holder (3 Bar System) 2200426



Quick Response RTD Probe Holder (3 Bar System) 2200429

Calorimetry Heater Probe Holder (3 Bar System) 2200430

3 Bar System Stirrers

Syrris offers a range of glass and PTFE stirrers for the Atlas Potassium 3 Bar

System in a variety of profiles. The maximum recommended stirring rate used

for all glass stirrers is 500rpm. As the 3 Bar System Stirrers cannot be height

adjusted due to the nature of the Stirrer Seal and Guides, each stirrer must be

cut to length by Syrris. Therefore, at the time of purchase please indicate the

vessel that the stirrer is to be used with.

4 Blade Propeller Stirrer PTFE 2200421

4 Blade Propeller Stirrer Glass 2200422

Retreat Curve Stirrer PTFE (500ml to 3 litre Vessels) 2200423

Anchor Stirrer PTFE (500ml to 3 litre Vessels) 2200418

Anchor Stirrer Glass (100ml to 250ml Vessels) 2200419

Anchor Stirrer Glass (500ml to 3 litre Vessels) 2200420

Retreat Curve Stirrer Glass (100ml to 250ml Vessels) 2200424

Retreat Curve Stirrer Glass (500ml to 3 litre Vessels) 2200425

Atlas and Globe Common Parts Pressure Parts

www.syrris.com 101

pH Probe - 200mm x 8mm with B19 Holder - 3 bar 2200697


Aalborg Mass Flow Controller 0-10L/min 2200364

The Aalborg Mass Flow Controller is for use with Atlas and Globe Pressure

Systems. It is ideal for applications such as dosing a controlled quantity of gas

into a reactor at an accurate rate.

Viewing data and programming is possible locally by the LCD and four button

keypad or remotely by the Atlas Software (via an Atlas Port and the unit's

RS232 interface). The materials in contact with the gas are 316 stainless steel

and Viton® O-rings. Please contact Syrris for flow rate ranges outside this

specification.

• Minimum set flow rate 200ml/min

• Accuracy: +/- 1% of full scale

Aalborg Mass Flow Meter 0-10L/min 2200354

Aalborg Mass Flow Meter 0-50L/min 2200355

The Aalborg Mass Flow Meters are for use with Atlas and Globe Pressure

Systems. They are ideal for applications such as understanding the total mass

of gas dosed into a reactor and gas uptake monitoring. Viewing data and

programming is possible locally by the LCD and four button keypad or remotely

by the Atlas Software (via an Atlas Port and the unit's RS232 interface). The

materials in contact with the gas are 316 stainless steel and Viton® O-rings.

• Accuracy: +/- 1% of full scale

Additional Calibration for Aalborg Mass Flow Meter 2200356

The Aalborg Mass Flow Meters are factory calibrated for use with Nitrogen. If

additional gases are to be used, specific calibrations are required. This part is

for the calibration of one additional gas. Please state the gas to be used at time

of purchase.

pH Probe - 400mm with Swivel Adaptor - 3 bar 2200696

This probe is identical to pH Probe - 400mm with Swivel Adaptor (2200029)

but is supplied with probe holder that is suitable for use with a 3 bar system.

Turbidity Probe - 400mm - 3 bar 2200698

This is the 3 bar pressure rated version of the PH probe – 200mm x 8mm with

B19 holder (2200054). The probe is pressure rated to 3 bar and it comes with a

GL18 3 bar rated swivel adaptor.

This probe is identical to Turbidity Probe - 400mm (2200156) but is supplied

with probe holder that is suitable for use with a 3 bar system.

www.syrris.com102

Condenser - Small Jacketed Coil B19 2101591

Jacketed coil condensers offer very good surface area for condensation. The

small condenser has a B19 connector, is 10cm long and has a surface area of

1.1x10-2m2. Suitable for vessels up to 250ml.

Condenser - Medium Jacketed Coil B19 2101590

Jacketed coil condensers offer very good surface area for condensation. The

medium condenser has a B19 connector, is 16cm long and has a surface area of

4x10-2m2. Suitable for vessels up to 1 litre.

Condenser - Large Jacketed Coil B29 2101589

The large jacketed coil condenser offers very good surface area for

condensation of 7x10-2m2. It has a B29 connector and features a bottom take-off

which can be rotated in to the solvent path for distillation or out of the solvent

path for reflux. Suitable for vessels up to 2 litres.

6mm Dia RTD Probe Holder (for B19 port) 2101546



The Probe Holder is fitted with an O-Ring to securely hold RTD probes in

place whilst providing a liquid and gas tight seal.

Accessories and Consumables

Connector - Oil Pipe to Jacketed Vessel (Pack of 2) 2200018

This part allows the quick connection and disconnection of Oil Pipes to

Jacketed Vessels. It also contains a thermowell enabling easy and accurate

measurement of the circulator fluid temperature at the input and/or output of

the jacketed reactor.

This connector screws onto an Oil Pipe using a regular M16 thread then

connects to an Atlas or Globe Jacketed Reactor without the need for tools. The

thermowell accepts the RTD Probe - Stainless Steel 100mm x 3mm (2101593).

Note that the M16 fitting and thermowell positions are interchangeable to

enable straight or 90° connection between the Jacketed Vessel and Oil Pipe.

This part is included in Oil Pipes from Reactor to Oil Drain Unit (2101014).

Atlas and Globe Common Parts Accessories and Consumables

8mm Dia RTD Probe Holder (for A24 port) 2200708

B19 (female) to A24 (male) Adapter 2200709

This adapter allows B19 Probe Holders to fit in A24 lid ports. Probe lengths may

need to be longer than specified on the compatibility chart.

www.syrris.com 103

Isolation Ball Valve for Circulator Pipe M16x1 1802039

An isolation valve for closing off oil pipes with M16 fittings.

Jacketed Vessel Earth Strap 2200201

This strap fits around Vacuum Jacketed Vessels to avoid static build up. This

part is included in all Vacuum Jacket Vessels

Baffles for 0.5 litre Torispherical Jacketed Vessel (Pack of 2) 2200171

Baffles for 1 litre Torispherical Jacketed Vessel (Pack of 2) 2200170

Baffles for 2 litre Torispherical Jacketed Vessel (Pack of 2) RD2200496

These baffles locate in the standard Jacketed Vessel Lids (2101030 and

2101594) and are designed to increase stirring efficiency within a large reactor

and mimic conditions found within pilot scale vessels.

Custom sizes and formats are available on request.

Baffles for 2 litre Round Bottom Jacketed Vessel (Pack of 2) 2101580

Sintered Dip Tube - Glass 450mm x 8mm No. 3 Sinter 2200202

Designed for bubbling gas into a jacketed reactor.

Liquid Feed Adaptor - B19 to Glass Tube 8mm x 200mm 2200158

GL14 Plastic Screw Cap with Aperture 2101517

GL18 Plastic Screw Cap with Aperture 2101516

Accessories and Consumables Atlas and Globe Common Parts

Baffles

www.syrris.com104

B29 Glass Stopper 1802066

B19 Glass Stopper 1802067

GL14 to B19 Joint - Glass Adaptor 2200177

GL18 to Male B19 Adaptor 2101519

GL18 PTFE Faced Silicone 6mm Sealing Ring 1802023



Set of Seals for Stirrer Seal and Guide 2101017

This part includes a full set of consumables and wearing parts for the Stirrer

Seal and Guide (2101011), including:

• 1 x PTFE Sprung Stirrer Shaft Seal

• 1 x Carbon filled PTFE Stirrer Shaft Seal Holder

• 1 x PEEK Static Seal

• 1 x Viton® O-ring for Static Seal

• 1 x Seal Spring

• 2 x FFKM Stirrer Guide O-ring

Stirrer Guide Replacement Seals (Pack of 5) 2200161

A set of five replacement FFKM O-rings for use at the base of the Stirrer Seal

and Guide (2101011).

Jacketed Vessel to Oil Pipe Seals (Pack of 2 Pairs) 2200107

Two pairs of replacement seals that fit inside the Connector - Oil Pipe to

Jacketed Vessel (2200018).

Atlas and Globe Common Parts Accessories and Consumables

www.syrris.com 105

Reaction Vessel Seal (FEP Coated Silicone) 2101016

A replacement FEP coated silicone O-ring for use with the Jacketed Reactor

and Lid (2101030 / 2101594).

Reaction Vessel Seal (FFKM) 2101543

A replacement FFKM coated silicone O-ring for use with the Jacketed Reactor

and Lid (2101030 / 2101594). Syrris recommends FFKM for the best seal with

high chemical resistance. Use this part for pressure or vacuum applications.

Bottom Outlet Valve Top Seal (FFKM) 1802042

Replacement FFKM O-ring for the upper seal of a jacketed vessel bottom outlet

valve. FFKM is the sealing material that offers the highest chemical resistance.

Bottom Outlet Valve Bottom Seal (FFKM) 1802152

Replacement FFKM O-ring for the lower seal of a jacketed vessel bottom outlet

valve. FFKM is the sealing material that offers the highest chemical resistance.

Bottom Outlet Valve - Sprung 9mm (Jacketed Vessels) 2200150

Bottom Outlet Valve - Sprung 9mm (Vacuum Jacketed) 2200193

Replacement PTFE Reaction Vessel Bottom Outlet Valves for use with Jacketed

Reactors. This valve comes complete with FFKM O-rings. The spring accounts

for thermal expansion and contraction, minimizing leaks.

Bottom Outlet Valve - Sprung 20mm (Jacketed Vessels) 2200276

For 3 litre and 5 litre jacketed vessels.

20mm Bottom Outlet Valve Top O-Ring 2200272

20mm Bottom Outlet Valve Bottom O-Ring 2200273

Accessories and Consumables Atlas and Globe Common Parts

www.syrris.com106

A range of comms cables are available for connecting RS232 controlled devices:

• to the Atlas or Reactor Master PC Software via Atlas Ports

• directly to a PC when using Atlas or Reactor Master COM Port Software

• directly to the Atlas Base Unit using an RJ11 to RS232 cable

• directly to the Reactor Master

Other cables are available on request.

Atlas and Globe Common Parts Communication Accessories

Communication Accessories

Comms Cables

RS232 Extension Cable - 5m 2200168

RS232 Null-Modem Cable - 5m 2200169

Comms Cable - Lauda Proline Circulator 2200135

Comms Cable - IKA / Chemglass Overhead Stirrer 2200167

Comms Cable - TTI Power Supply for Calorimetry 2200152

Comms Cable - Heidolph Overhead Stirrer 2200256

Comms Cable - CAT Overhead Stirrer 2200593

Comms Cable - IKA Eurostar Overhead Stirrer 2200125

Comms Cable - IKA Werke Peristaltic Pump 2200126

Comms Cable - Watson Marlow Peristaltic Pump 520Du 2200127

Comms Cable - Mettler SevenEasy pH Meter 2200128

Comms Cable - Julabo Circulator 2200129

Comms Cable - Watson Marlow Peristaltic Pump 323Du 2200133

Comms Cable - Haake DC50 Circulator 2200134

Comms Cable - Denver Summit Balance 2200160

Comms Cable - Huber Pilot One Controller 2200693

www.syrris.com 107

7 Port USB Powered Hub - UK 2200480

These USB hubs allow up to seven USB devices to be connected to one USB

port on a PC. An example of an application is the connection of multiple Atlas

Bases, Atlas Syringe pumps and/or Atlas Ports to one PC.

7 Port USB Powered Hub - US/EU 2200481

Ethernet to 8 RS232 Ports 2200351

This adaptor plugs into the ethernet port of a PC and allows up to 8 RS232

controlled devices to be connected. The price for this adaptor includes its

configuration into a PC. Note that the PC must be provided by Syrris or shipped

to Syrris at time of order. This adaptor is for use with the Atlas COM Port

Software 1 (2600001).

Atlas / Reactor Master PC (no control software) 2200599

Communication Accessories Atlas and Globe Common Parts

This computer is defined for use with the range of Atlas and Reactor Master

software packages. When purchased with a Syrris software application, the

software will be preinstalled on the computer. The following specification is the

minimum provided:

• CPU: 1.8Ghz+ Intel Pentium Dual Core processor

• Memory: 2GB

• OS: Windows XP Professional / Windows 7 Professional (32 bit)

• Hard Disk: 320GB

• Display Resolution: Super VGA 1024 x 768

• USB Ports: 4

Stirrers

Sti

rre

rs

PT

FE

2 B

lad

e C

en

trif

ug

al 3

00

mm

PT

FE

4 B

lad

e P

rop

elle

r 3

00

mm

x 4

0m

m d

ia

PT

FE

4 B

lad

e P

rop

elle

r 4

00

mm

x 4

0m

m d

ia

PT

FE

4 B

lad

e P

rop

elle

r 5

00

mm

x 5

0m

m d

ia

PT

FE

4 B

lad

e P

rop

ello

r 6

00

mm

x 6

0m

m d

ia

PT

FE

An

ch

or

40

0m

m x

80

mm

dia

PT

FE

An

ch

or

50

0m

m x

80

mm

dia

PT

FE

An

ch

or

60

0m

m x

80

mm

dia

PT

FE

3 B

lad

e R

etr

eat

Imp

elle

r 4

00

mm

x 7

5m

m d

ia

PT

FE

3 B

lad

e R

etr

eat

Imp

elle

r 5

00

mm

x 7

5m

m d

ia

PT

FE

3 B

lad

e R

etr

eat

Imp

elle

r 6

50

mm

x 7

5m

m d

ia

Gla

ss 4

Bla

de P

rop

elle

r 3

00

m x

27m

m

Gla

ss A

nch

or

30

0m

m x

36

mm

Gla

ss 3

Bla

de R

etr

eat

Imp

elle

r C

ut

Len

gth

x 4

5m

m

Gla

ss 3

Bla

de R

etr

eat

Imp

elle

r C

ut

Len

gth

x 7

5m

m

Reactors

Part Number

18

020

59

18

020

14

(220

04

21† )

18

020

15

(220

04

21† )

18

020

16

(220

04

21† )

220

06

68

18

020

57

(220

04

18† )

220

00

87

(220

04

18† )

220

06

67

210

158

5

(220

04

23

† )

220

012

4

(220

04

23

† )

220

017

6

(220

04

23

† )

220

028

5 (

220

04

22

† )

220

028

6 (

220

04

19† )

210

1523

(2

20

04

24

† )

220

00

85

(2

20

04

25

† )

Jacketed Vessel 100ml Round Bottom 2101525 (2200411†)



Jacketed Vessel 1 litre Round Bottom 2101532 (2200331†)



Jacketed Vessel 5 litre Round Bottom 2200253


Jacketed Vessel 50ml Torispherical Bottom 2200184




Jacketed Vessel 1 litre Torispherical Bottom 2200188


Jacketed Vessel 5 litre Torispherical 2200640

Jacketed Vessel 5 litre Dished Bottom 2200074

Jacketed Vessel 250ml Conical Bottom 2200019


Jacketed Vessel 1 litre Conical Bottom 2200021

Jacketed Vessel 100ml Vacuum Jacket 2200023 (2200415†)



Jacketed Vessel 1 litre Vacuum Jacket 2200026 (2200338†)


Jacketed Vessel 5 litre Vacuum Jacket 2200641

Jacketed Filtration Vessel 3 litre 2200048





1 litre Round Bottom Flask 2101542

Compatibility Chart

Ideally Suited

Suited

Not Suited

Part number is suitable for 3 bar pressure †

Key

Compatibility Chart

Probes and Heater Rods

RT

D P

rob

e -

PT

FE

Co

ate

d 1

00

mm

x 6

mm

RT

D P

rob

e -

PT

FE

Co

ate

d 2

00

mm

x 6

mm

RT

D P

rob

e -

PT

FE

Co

ate

d 3

00

mm

x 8

mm

RT

D P

rob

e -

PT

FE

Co

ate

d 4

00

mm

x 8

mm

RT

D P

rob

e -

PT

FE

Co

ate

d 5

00

mm

x 9

mm

RT

D P

rob

e -

PT

FE

Co

ate

d 6

00

mm

x 9

mm

RT

D P

rob

e -

Qu

ick R

esp

on

se 3

00

mm

RT

D P

rob

e -

Qu

ick R

esp

on

se 4

00

mm

RT

D P

rob

e -

Qu

ick R

esp

on

se 5

00

mm

pH

Pro

be -

40

0m

m w

ith

Sw

ivel A

dap

tor

pH

Pro

be -

20

0m

m x

8m

m w

ith

B19

Ho

lder

Tu

rbid

ity P

rob

e -

40

0m

m

Heate

r R

od

fo

r C

alo

rim

etr

y -

25

W, 3

00

mm

Heate

r R

od

fo

r C

alo

rim

etr

y -

50

W, 5

00

mm

Reactors

Part Number

210

158

6†

210

158

2† /

220

05

87

†♠

210

158

3† /

220

05

88

†♠

210

158

4† /

220

05

89

†♠

220

012

2† /

220

05

90

†♠

220

026

2† /

220

05

91†♠

220

014

4† *

/ 2

20

06

80

†♦

220

014

5† *

/ 220

06

81†♦

220

014

6† *

/ 220

06

82

†♦

220

00

29

/ 2

20

06

96

†

220

00

54

/ 2

20

06

97

†

220

015

6 /

220

06

98

†

220

014

2† *

/ 2

20

06

83

†♦

220

014

3† *

/ 2

20

06

84

†♦















Jacketed Vessel 5 litre Torispherical 2200640

Jacketed Vessel 5 litre Dished Bottom 2200074



Jacketed Vessel 1 litre Conical Bottom 2200021






Jacketed Vessel 5 litre Vacuum Jacket 2200641

Jacketed Filtration Vessel 3 litre 2200048





1 litre Round Bottom Flask 2101542

Headspace/Distillation

Ideally Suited

Suited

Not Suited

Part number is suitable for 3 bar pressure †

Part number with LEMO Connector ♠Material of construction Hasetelloy ♦Material of construction FEP Coated SS *

Key

Systems

www.syrris.com110

Batch Reactor Specifications

Atlas Potassium / Volumetric Dosing

System (see pages 9-13)*.

Dimensions

Height 98cm

Width 50cm/66cm*

Depth 30cm

Weights

Atlas Base Unit 4.8kg

Atlas Syringe Pump 6.75kg

Full System(inc. 100ml jacketed vessel)

17.5kg

Full System(inc. 2L jacketed vessel)

20.2kg

Max. Power Consumption

Atlas Base Unit 60W

Atlas Syringe Pump 60W

The Atlas Calorimeter (see page 14)

including power supply.

Dimensions

Height 98cm

Width 66cm

Depth 30cm

Weights


Atlas Syringe Pump 6.75kg

TTI Power Supply 4.1kg

Full System(inc. 100ml vacuum jacket)

22.4kg

Full System(inc. 2L vacuum jacket)

26.0kg


Atlas Base Unit 60W

Atlas Syringe Pump 60W

TTI Power Supply 50W

88

cm

23cm 50cm

98

cm

98

cm

66cm

The Atlas Sodium (see page 16) for

round bottom flask systems.

Dimensions

Height 88cm

Width 23cm

Depth 26cm

Weights


Full System 13.1kg


Atlas Base Unit 60W

With hotplate 660W

Atlas Sodium Atlas Potassium / Volumetric Dosing Atlas Calorimeter

*The pump fits within the footprint of a Potassium system (50cm wide) with vessel sizes of 1L or less. When the reactor volume is greater than or equal

to 2L, volumetric dosing systems are 66cm wide. Note: Due to the modularity of the Atlas system, data on this page should only be used as a guide.

Systems

www.syrris.com 111

Batch Reactor Specifications

approx. 60cm40cm

98

cm

(11

2cm

wit

h >

2L

Vess

el)

(See page 62).

Dimensions

Height (with >2L vessel) 98cm (112cm)

Width 40cm

Depth 52cm

Weights

Frame Assembly 12.85kg

A Globe system (see page 59)

includes oil pipes and a jacketed vessel.

Dimensions


Width 60cm

Depth 52cm

Weights


Full System(inc. 100ml jacketed vessel)

17.1kg


21.1kg


Overhead Stirrer 100W

A Globe system with automation

including the Reactor Master and Stand.

Dimensions


Width 70cm

Depth 52cm

Weights


Reactor Master & Stand 2.9kg

Full System (inc. 100ml jacketed vessel)

20kg


23.9kg


Overhead Stirrer 100W

Globe Reactor Master Pro 60W

98

cm

(11

2cm

wit

h >

2L

Vess

el)

98

cm

(11

2cm

wit

h >

2L

Vess

el)

approx. 70cm

Globe Frame Assembly 2200507 Globe with AutomationGlobe

Note: The measurements of Globe on this page include the system with the Bronze Stirrer (see page 63). Due to the modularity of Globe systems,

data on this page should only be used as a guide.

Chip Climate Controller This enables glass microreactors to be cooled or heated from -15°C to +150°C

Pressurized Input Store This enables the use of air sensitive reagents and eliminates bubble formation when pumping

Syringe Pump 2 Extremely chemically resistant continuous flow pumps. This can also be used as the “master” to control certain systems without a PC

Automated Collector This allows collection of multiple reactions in separate vials or vessels with waste automatically diverted

Heater (Tube Reactor Adaptor)This module has different reactor adaptors and enables temperatures up to 250°C

Reagent Injector 2 Extremely chemically resistant injection valves with sample loops

Sampler and DilutorThis enables on-line reaction analysis by automated sample extraction, dilution and transfer to an analytical system e.g. LCMS or UPLC

Asia Manager Software Easy to use for total ‘walk-away’ control of the Asia system

Pressure Controller Automatically pressurizes the reaction up to 20 bar (300psi)

FLLEX The FLLEX (Flow Liquid Liquid Extraction) module is the flow chemistry equivalent of separatory funnels

Flow chemistry offers faster, cleaner and safer chemical reactions by pumping them continuously through pipes or tubes. Asia is a revolutionary range of advanced flow chemistry products from Syrris.

It has been designed by chemists for chemists to enable the widest variety of chemical reactions and ultimate ease of use.

• Wider range of chemistries: Perform reactions that cannot be performed in batch and access new chemical space.

• Integration of synthesis, work-up and analysis: The Flow Liquid Liquid Extraction Module (FLLEX) enable two

immiscible phases to be mixed and separated in flow immediately following the reaction. Samples can be taken in

real time, diluted and injected into an LCMS / UPLC.

• Safer reactions: Only small amounts of material react at any time, minimizing exotherms and the quantity of any

hazardous intermediates.

• Cleaner Reactions: Reduced impurities via excellent, reproducible reaction control and optional use of solid phase

reagents/catalysts/scavengers.

• More reactions in less time: Multiple-step, multiple-day and difficult batch synthesis can be performed in one

process and shortened to a matter of minutes.

• Maximum chemical resistance: Glass and PTFE reactors allow a wide range of chemistry at a large range of

temperatures and pressures.

• Ideal for synthesis, rapid optimization and scale-up: Asia’s design allows successive experiments on a multitude of

scales, from milligrams to grams to kilograms, all on the same instrument.

• Robust and easy to use: Designed by chemists for chemists, the chemically resistant system can be controlled in 3

ways: manually, automated from the Asia Syringe Pump or automated from a computer.

Asia Benefits

Asia 330 System Configuration

www.syrris.com 113

The Future of Flow Chemistry

Asia 1-series flow chemistryAsia 1-series flow chemistry systems are operated manually.

This is ideal for chemists with lower budgets or those who prefer not to have automation.

asia 110 asia 120 asia 130

Asia 2-series flow chemistry Asia 2-series flow chemistry systems can automatically perform one experiment at a time.

Parameters such as reaction temperature, pressure, reagent injections and collection timings are all automated.These systems are ideal for introduction to the world of flow synthesis.


Asia 3-series flow chemistryAsia 3-series flow chemistry systems can automatically perform process optimization.

Parameters such as reaction time, temperature and ratio of reagents can be varied and each reaction collected and analyzed automatically.


Asia offers a variety of flow chemistry modules and systems making it ideal

for both beginners with modest budgets and experts who demand the utmost

functionality.

Asia has received an esteemed R&D 100 Award, a benchmark of excellence, with winners chosen by an independent panel of judges. This award recognizes Asia’s advanced functionalities, ease of use and applicability to an extremely wide range of chemistries. It also honours Syrris’ contribution to a technology that is enabling chemists to perform faster, safer and cleaner reactions.

Systems

www.syrris.com114

Services

Syrris support plans offer the peace of mind that you require when

purchasing new equipment for your laboratory.

All Syrris equipment is provided with a free of charge bronze support

plan valid for 12 months after the receipt of the equipment. This

comprehensive package offers you access to our team of Technical

Support Specialists who are available to assist you with the operation

and troubleshooting of our products, as well as answer any questions

you have regarding the application of the equipment to your

chemistry.

Support Plans

The cover provided by this free warranty can be upgraded, if desired,

to increase the level of support available. Once the initial warranty

period for the product has expired, it is important to maintain the

performance and serviceability of your equipment.

Syrris recommends one of three levels of cover to support your

systems:

Syrris offers a wide range of services and support for your products. Following the successful installation of your equipment, our dedicated team of Technical Support Specialists are available to ensure your equipment is kept in optimum condition at all times.

The Bronze Warranty guarantees telephone

support during office hours. In the unlikely

event you have a faulty part you will be

able to return it to Syrris for repair. Other

advantages of the Bronze warranty include

software upgrades to the latest releases.

Customers can upgrade and continue to

receive Bronze Warranty support after the

first 12 months.

Bronze Support Plan

Alongside all of the benefits of the Bronze

support plan, the silver support plan allows

access to on-site repairs provided by

qualified experts, with the added benefit of

inclusive parts and labour.

Silver Support Plan

Gold level care will reduce any unexpected

down time, increase the product life and

optimize the performance of your Syrris

equipment.

Gold Support Plan

Training & Workshops

Syrris offer free to attend Customer Workshops to ensure that you are getting the most out

of your equipment. Workshops are held for user groups worldwide. Please contact us if you

would like to attend one of our upcoming Customer Workshops.

We can also offer one-on-one practical assistance. This is charged at a daily rate plus travel

expenses. If you would like to have one of our experienced chemists visit your laboratory to

assist you with your application and get the most out of your system, please contact Syrris.

Support Plans Bronze Silver Gold

Telephone support (office hours) ü ü üChemistry application support (office hours) ü ü üSoftware and firmware updates ü ü üReplacement of faulty non-wetted parts ü ü üReturn unit to Syrris for repair ü ü üOn-site repair with our support scientist ü üAgreed on-site response time ü üPreventative maintenance visit ü12 Month Support Plan Order Numbers:

Atlas 2800009 2800010 2800011

Globe 2800012 2800013 2800014

For support contracts for Syrris flow chemistry and custom reactor systems please contact

[email protected] for more information.

To find out more, call us in the UK on +44 (0)1763 242 555 to speak to our support team

www.syrris.com 115

Testimonials

"Since investing in the Atlas from Syrris, we have been delighted

at the rapid uptake by our chemists and the high demand

that they have placed for available systems. We are also very

impressed with the speed and quality of the service and support."

Dr Phil Peach (Process CRD, Pfizer, UK)

“We have found Atlas to be extremely versatile and the ability

to re-configure the system as projects demand change is very

powerful. Applications such as turbidity, pH control, distillation

and calorimetry have been made easy with Atlas.

We have also received excellent post-sales support and technical

help from Syrris. We have been very impressed with the Atlas

software and find the ability to seamlessly integrate and control

3rd party equipment to be particularly important when designing

experiments.”

Ben Brockbank (Process Development, Syngenta Ltd)

"We purchased two Atlas systems, and are delighted with their

performance, ease of use and flexibility."

David Easson (VP Manufacturing and Process Dev., Epic

Therapeutics, Baxter Healthcare)

We are proud to have a large customer base that includes the vast majority of major pharmaceutical companies, academic institutions, CROs and biotechnology companies in over 40 countries worldwide. Read what our customers think:

"(Globe is) great for scaling up, in a safe and comfortable way!"

Freek Vrielynck (Senior Scientist, EcoSynth, Belgium)

"We work with zirconium compounds, which are ink additives for

the packing industry, and also perform drug discovery studies.

We use a range of vessels – from 100ml up to 2L – with our Atlas

Calorimeter which, like our 100L pilot system, has been tailored

to scale-up experiments and studies in support of this work. The

results obtained are fundamental to performing the technological

transfer of the procedures to the production plant.

We evaluated equivalent systems from a number of manufacturers

prior to purchasing the Atlas Calorimeter and 100L systems.

Syrris arranged a demonstration of one of its reactor systems in

our laboratory and explained its technological capabilities; this

was really important to us, as it allowed us to see and test the

product ourselves before we decided which system to buy.

The systems are well designed and the software is very functional,

efficient and easy to use, with a robust communication protocol.

User-friendly operation allows us to train staff rapidly. The

performance and reliability of both systems is really good, and

we are now considering purchasing an Asia flow system to

complement our existing Syrris equipment."

Valter Russo

(Director of R&D, Zirkon Industria e Comercio Ltda, Brazil)

“We at Torrent bought a Syrris Parallel Atlas jacketed reactor

system and found that the Atlas Reactor platform is extremely

flexible, powerful and user friendly system. This system has now

become core to our Chemical Research. We are continuing to

upgrade the Atlas systems with more functionality to perform

Reaction Calorimetry and Turbidity probes for crystallization

studies.

One key to our success with the Atlas system apart from the

strength of the product itself is the highly responsive nature of

Syrris as a company. Syrris has now developed new functionality

together with Torrent. In addition with Syrris now having an Indian

subsidiary, we also have a pool of highly knowledgeable people in

India who can resolve issues with us very quickly.

Torrent is very pleased with Syrris as a company and our

experience of the Atlas product line is very positive and we

sincerely believe that this would be a continuous and consistent

feature.”

Dr. Sunil S. Nadkarni (VP, Product Development Torrent, India)

Read more testimonials online at www.syrris.com/company/testimonials

www.syrris.com116

Index

Index

AAtlas Automated Synthesis System

Atlas Accessories and Consumables 54–56

Atlas Case Studies 21–23

Atlas Modules 24–29

Atlas Orbit and Dry Baths 44–53

Atlas Sodium Pressure (200 bar) Parts 40–43

Atlas Syringe Pumps 30–35

Atlas Systems 9–20

Introduction to Atlas 6–8

Software 36–39

Automation. See also Third Party Devices

Accessories7 Port USB Powered Hub 107Atlas / Reactor Master PC (no control software) 107Comms Cables 106Ethernet to 8 RS232 Ports 107

ModulesPort 37Reactor Master 75

SoftwareAtlas Calorimetry Software Upgrade 39Atlas COM Port Software 38Atlas Parallel Software 37Atlas Reporting Software 39Atlas Software 1 36COM port Parallel Software 38FBRM Software Integration Kit 39Reactor Master COM Port Software 78Reactor Master Software 77

SystemsAtlas Automated Synthesis System 9–20Automating Existing Systems 75–78Custom Reactor Systems 67–74

Autosampling

AccessoriesAutosampler Probe Filter (Cap and 5 Filters) 33

ModulesAtlas Syringe Pump 31Atlas Syringe Pump XL 32Autosampler Module (for Atlas Syringe Pumps) 33Autosampler Probe (for Atlas Syringe Pumps) 33

BBase Unit 24

CCalorimetry

AccessoriesCalorimetry Heater Probe Holder (3 Bar System) 100Comms Cable - TTI Power Supply for Calorimetry 106

ModulesJacketed Vessels - Vacuum Jacket 82TTI Power Supply for Calorimetry 26

Probes, Nodes and SensorsHeater Rod for Calorimetry 55RTD Probe - Stainless Steel 100mm x 3mm for Dry Baths or Tj 87

Software

Atlas Calorimetry Software Upgrade 39

SystemsAtlas Calorimeter 14

Circulators. See Heating and Cooling by Circulator

Clamps. See Vessels

Jacketed Vessel ClampsHigh Force Jacketed Vessel Clamp 25Jacketed Vessel Clamp 24Jacketed Vessel Clamp (3 Bar System) 25

Round Bottom Flask ClampsClamp 29Scorpion Overhead Stirrer Support (Sodium) 29Triple Clamp 29

Comms cables. See Automation

Cooling. See Heating and Cooling by Circulator

Crystallization

AccessoriesSonolab Accessories 27

ModulesProsonix Sonolab SL10 Sonocrystallizer 27

Probes, Nodes and SensorsTurbidity Node 86Turbidity Probe - 400mm 88

SystemsAtlas Sonolab 12Atlas Turbidity 11

Custom Reactor Systems 67–74

Automated Atmospheric Pressure Reactors >5L 70

Automated High Pressure Reactors 69

Case Studies 70–74

Introduction to Custom Reactor Systems 67–68

DDatalogging. See Automation

Dosing

Accessories3 Roller Extension Head for Watson Marlow 323/DU/D 95Pipe End Fittings for Atlas Syringe Pump 35PTFE Input filters for 5μm for 3.2mm diameter 33Syringes for Atlas Pump 34–35Valves (PTFE/PCTFE) for Atlas Pump 34

Modules3 Bar Gas Pressure Control Module 96Aalborg Mass Flow Controller 0-10L/min 101Atlas Pump Pressurized Input Store 33Atlas Syringe Pump 31Atlas Syringe Pump XL 32Denver Summit Balance SI-4002 95Watson Marlow Peristaltic Pump 323/DU/D 95

SystemsAtlas Gravimetric Dosing 10Atlas Volumetric Dosing 10Automated Atmospheric Pressure Reactors >5L 70Custom Reactor Systems - Case Study 6 73Custom Reator Systems - Case Study 1 70

Dry Baths. See also Round Bottom Flasks

ModulesIndividual Dry Bath Inserts 47Stacking Dry Baths 44Triple Dry Bath 45

Systems

www.syrris.com 117

Index

Atlas Lithium 15Atlas Sodium 16

FFlasks. See Dry Baths

FT-IR Spectrometer

AccessoriesFT-IR Accessories 28

ModulesBruker FTIR Spectrophotometer Matrix-MF 28

SoftwareBruker Atlas Software Drivers 39Bruker OPUS Software Package 39

SystemsAtlas FT-IR Spectrometer 13

GGas Dosing. See Dosing

Glassware. See Vessels

Globe Jacketed Reactor Platform 57–66

Globe Accessories and Consumables 65–66

Globe Modules 62–64

Globe Systems 59–61

Introduction to Globe 57–58

Gravimetiric Dosing. See Dosing

HHeat Flow Calorimetry. See Calorimetry

Heating and Cooling by Circulator

AccessoriesBase to Circulator Serial Cable (RJ11 to DB9 Male) 56Circulator Fluid 94Comms Cables 106Connector - Oil Pipe to Hot and Cold Plate (Pack of 2) 54Connector - Oil Pipe to Jacketed Vessel (Pack of 2) 102Globe Single Long Oil Pipe - Budget 66Globe Single Long Oil Pipe - Premium 65Globe Single Short Oil Pipe - Premium 65Isolation Ball Valve for Circulator Pipe M16x1 103Oil Pipes from Circulator to Oil Drain Unit (Pack of 2) 54Oil Pipes from Reactor to Oil Drain Unit (Pack of 2) 54Oil Pipe Tidy 55Velcro Oil Connector Insulator (Pack of 2) 54

ModulesCirculators 89–94Hot and Cold Plate 28Hot and Cold Plate for IKA Hotplate/Stirrer 53Oil Drain Unit 25

Heating (Electrical)

ModulesHotplate 28Hotter Hotplate (to 350°C) 40Support Rods for IKA 53

SystemsAtlas Lithium 15Atlas Sodium 16Atlas Sodium High Pressure 18

High Pressure Systems. See Pressure Systems

High Torque Stirring. See Stirring

Hotplates. See Heating (Electrical)

JJacketed Reactor Systems

Automated Jacketed Reactor Systems. See Atlas Automat-ed Synthesis System

Comparison Table 5

Jacketed Reactors. See Vessels

Manual Jacketed Reactors. See Globe Jacketed Reactor Platform

LLarger Scale Reactions

3L - 5L ModulesGlobe Offset Assembly (factory fit) 64

Jacketed Reactors. See VesselsRemote Mount for Jacketed Vessel Clamp 25

3L - 5L SystemsAtlas Remote Mount 10

>5L. See Custom Reactor Systems

MMagnetic Stirring. See Stirring

Manual Control. See Globe Jacketed Reactor Platform

Mass Flow Controllers. See Third Party Devices

Mass Flow Meters. See Third Party Devices

Monitoring Reactions. See Probes, Nodes and Sensors

OOrbit. See Tubes and Vials

PParallel Chemistry

Case StudiesParallel High Pressure 22

In Round Bottom Flasks. See Dry Baths

In Vials. See Tubes and Vials

SystemsAtlas Parallel Systems 20

PC Control. See Automation

Peristaltic Pump. See Dosing

pH Monitoring and Control

ModulesAtlas Syringe Pumps 30–35

Probes, Nodes and SensorspH and Temperature Node 86pH Probe 88

SystemsAtlas pH Monitoring and Control 11

Third Party pH Meter Control. See Third Party Devices

Pressure Reactions

ModulesGas Selection Module 97

Probes, Nodes and Sensors

www.syrris.com118

Index

pH Probe - 200mm x 8mm with B19 Holder - 3 bar 101pH Probe - 400mm with Swivel Adaptor - 3 bar 101Pressure Node for 3 Bar System 99Pressure Node for 200 Bar System 43Pressure Sensor for 3 Bar System 99Pressure Sensor for 200 Bar System 43Turbidity Probe - 400mm - 3 bar 101

Up to 3 bar

Jacketed Vessel. See VesselsModules

3 Bar Dip Tube for Autosampling 993 Bar Gas Pressure Control Module 963 Bar System Starter Kit 993 Bar System Stirrers 100Jacketed Vessel Clamp (3 Bar System) 25SS 3 bar Jacketed Vessel Lid and Safety Manifold 98Stirrer Seal and Guide PTFE (3 Bar System) 97Stirrer Seal and Guide Stainless Steel (3 Bar System) 96

SystemsAtlas Potassium Pressure 19Globe 3 Bar System 60

Up to 200 barModules

200 Bar System Starter Kit 42High Pressure Vessel 42High Pressure Vessel Lids 41Hotter Hotplate 40Stainless Steel RTD probe for High Pressure Vessels 42

Systems. See also Custom Reactor SystemsAtlas Sodium High Pressure 18

Probes, Nodes and Sensors

3 barpH Probe - 200mm x 8mm with B19 Holder - 3 bar 101pH Probe - 400mm with Swivel Adaptor - 3 bar 101Pressure Node for 3 Bar System 99Pressure Sensor for 3 Bar System 99Turbidity Probe - 400mm - 3 bar 101

200 barPressure Node for 200 Bar System 43Pressure Sensor for 200 Bar System 43

AccessoriesNode Clip 87Node Extension 87RTD Probe Holder 102Six Way Node Socket 87Triple Node Socket 87

NodespH and Temperature Node 86Pressure Node for 3 Bar System 99Pressure Node for 200 Bar System 43Temperature Node 86Turbidity Node 86

ProbesAutosampler Probe 33Bruker Probes for FT-IR Spectometer 28pH Probes 88RTD Probe - FEP Coated 55RTD Probes - PTFE Coated 66, 88RTD Probe - Stainless Steel 87Stainless Steel RTD probe for High Pressure Vessels 42Turbidity Probe 88

PTFE Pipe. See Dosing

Pumps. See Dosing

RReaction Calorimetry. See Calorimetry

Reaction Monitoring. See Probes, Nodes and Sensors

Reaction Tubes. See Tubes and Vials

Reactors. See Vessels

Reagent Addition. See Dosing

Remote Mount. See Larger Scale Reactions

Round Bottom Flasks. See also Dry Baths

50ml Round Bottom Flask - Centre Neck 56

100ml - 1 litre Round Bottom Flask - Centre and 2 Angled Neck 56

100ml - 250ml Round Bottom Flask - Centre and 1 Angled Neck 56

RS232. See Automation

SSampling. See Autosampling

Sensors. See Probes, Nodes and Sensors

Software. See Automation

Sonocrystallization. See Crystallization

Stainless Steel Reactor systems. See High Pressure Reactions >200 bar, Vessels

Stirring

High Torque StirringHeidolph 2051/2052 Stirrer Mount for Globe 65Heidolph Overhead Stirrers 95High Torque Stirrer Adaptor (for Heidolph Stirrers) 26

Magnetic StirringMagnetic Stirrer 29Orbit 6 Stirrer Bars 52Orbit 12 Stirrer Bars 52PTFE Magnetic Stirrer Bars 48

Overhead StirringAccessories

Stirrer Guide Replacement Seals (Pack of 5) 104Globe Bronze Stirrer 63Globe Gold Stirrer 63Globe Silver Stirrer 63Scorpion Drive Head (without pole) 26Scorpion Overhead Stirrer 25Scorpion Overhead Stirrer Pole (without Drive Head) 26Scorpion Overhead Stirrer Support (Sodium) 29Stirrer Bars 85Stirrer Seal and Guide 84Stirrer Seal and Guide Release for Flasks (Sodium) 56

Pressure Reaction Stirring3 Bar System Stirrers 100High Pressure Vessel Lid Magnetic Stirring 41High Pressure Vessel Lid Overhead Stirring 41Stirrer Seal and Guide PTFE (3 Bar System) 97Stirrer Seal and Guide Stainless Steel (3 Bar System) 96

Syringe Pumps. See Dosing

TThird Party Devices

SupportRS232 Device not Supplied for Integration with PC 37RS232 Device Supplied for Integration with PC 37

Tubes and Vials

Accessories (incl. vials) 52

Modules

www.syrris.com 119

Index

Custom Vial Bath 45Large Vial Bath (6 x 28mm dia) 45Medium Vial Bath (8 x 20mm dia) 45Orbit 6 (24mm dia, 45ml tubes) 51Orbit 12 (13mm dia, 10ml tubes) 51Orbit Reflux Unit 51Small Vial Bath (12 x 17mm dia) 45

SystemsOrbit 6 and Orbit 12 System 50Orbit 6 System 49Orbit 12 System 50

Turbidity. See Crystallization

VVessels. See also Round Bottom Flasks

Accessories. See also ClampsBaffles 103Bottom Outlet Valve - Sprung 105Custom Lid for Jacketed Vessel 84Jacketed Vessel Earth Strap 103Jacketed Vessel Lid 84Reaction Vessel Seals 105

Jacketed VesselsJacketed Filtration Vessel 3 litre 83Jacketed Vessels - Conical Bottom 83Jacketed Vessels - Round Bottom 81Jacketed Vessels - Torispherical Bottom 82Jacketed Vessels - Vacuum Jacket 82Stainless Steel Jacketed Vessels - Torispherical Bottom 83

Vials. See Tubes and Vials

Syrris is the world's most advanced provider of lab scale chemistry systems. Contact us now at: www.syrris.com

v2.0

Syrris Inc. (North America)156 Norwell Ave, Norwell,MA 02061

Syrris Japan, Inc.(Japan)SOHO Station 202, 24-8, Yamashita-cho, Naka-ku, Yokohama, Kanagawa

Syrris Scientific Equipment Pvt. Ltd.(India)420/421 Corporate Avenue, Sonawala Road, Goregaon (East), Mumbai, 400063

Syrris do Brasil Ltda.(Brazil)Rua Dr. Bacelar, 231 - cj 47 Vila Clementino, 04026-000 São Paulo - SP

Syrris Ltd. (Europe and Rest of World)27 Jarman Way, Royston, Hertfordshire,SG8 5HW, United Kingdom

T: +44 (0)1763 242555E: [email protected]: www.syrris.com

T: 617 848 1211E: [email protected]: www.syrris.com

T: +55 11 5083 4963E: [email protected]: www.syrris.com.br

T: +91 22 2686 4410E: [email protected]: www.syrris.com

T: 045 263 8211E: [email protected]: www.syrris.co.jp

Syrris Group Offices

QatarGulf Scientific GatewayDoha +974 4431 [email protected]

RussiaTirit LLCMoscow+7 (495) [email protected]

SingaporeAseptec PTE. LtdSingapore +65 6303 2425 [email protected]

SpainMTBMadrid+34 91 806 22 [email protected]

SwitzerlandStagroma AGReinach+41 61 71 78 717www.stagroma.com

TaiwanAnalytik Jena Taiwan Co., LtdSinjhuang City+886-2-85227886sales@analytik-jena.com.twwww.analytik-jena.com.tw

ThailandSujipuli Technology Co., LtdBangkok [email protected]

TurkeyBoyut Ltd.Istanbul +90 212 222 31 [email protected]

UK and IrelandGPE Scientific Limited.Leighton Buzzard

+44 (0)1525 [email protected]

AustraliaJohn Morris ScientificChatswood, NSW+61 2 9417 [email protected]

AustriaOmnichrom Handels gmbHWien+43 1 27 85 701www.ymc.de

ArgentinaLa Química Quirúrgica S.A.C.I.Ciudad Autónoma de Buenos Aires+54 (11) [email protected]

BelgiumBeun De Ronde Serlabo (BRS)Drogenbos+32 2 334 22 [email protected]

BrazilSuperlab Instrumentação AnalíticaSão Paulo+55 (11) [email protected]

ChinaUniversal Analytical & Testing Instruments Ltd. Shanghai +86 21 54170556 [email protected] www.uatil.com

CroatiaOhm Lab d.o.oZabok+385 (0) 49 221 580 [email protected] www.ohmlab.hr

Czech RepublicNeotec, spol. s r.o.Praha+420 257 289 511 [email protected] www.neotec.cz

FinlandMiliot SciencePorvoo+358 40 142 [email protected] www.miliot.com

FranceSerlabo TechnologiesEntraigues sur la Sorgue+33 4 9023 [email protected] www.serlabo.fr

GermanyYMC Europe GmbHDinslaken+49 2064 427 0www.ymc.de

GreeceMalva SAKifissia+30 210 800 0904www.malva.gr

Hong KongUniversal Analytical & Testing Instruments Ltd. Kowloon 852-36924581 [email protected] www.uatil.com

HungaryLab Services KftDabas+36 20 [email protected]

IndiaSyrris Scientific Equipment Pvt. Ltd.Goregaon +91 22 2686 [email protected]

IndonesiaP.T. Unitama Analitika PerkasaJakarta +62 21 53660541/[email protected]

IsraelIner-Tech [email protected] www.iner-tech.com

ItalySyrris Ltd.Herts, UK+44 (0)1763 242 555 [email protected]

JapanReifycs Analytical [email protected]

JapanAsahi Glassplant Inc.Kumamoto0968- 68 - [email protected]

KoreaUNa TradingSeoul [email protected] www.unatrading.com

LatviaArmgate SIARīgas raj.+371 67 976 782 [email protected]

LithuaniaArmgate, UABVilnius+370 5 278 95 [email protected] www.armgate.lt

MalaysiaAseptec SDN BHDSelangor+603 8941 5634 [email protected]

MexicoAureus Soluciones Integrales para Laboratorio S.A. de C.V.Mexico City+52 (55) 3300 [email protected]

New ZealandJohn Morris ScientificAuckland+64 366 [email protected]

NorwayNerliens Meszansky ASOslo+47 - 22 66 65 [email protected]

PolandMEGANTECHKatowice+48 32 250 65 [email protected]

PortugalMTBPorto +351 22 616 73 [email protected] www.mtbrandao.com

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CATALOGUE 2013/14 - Superlab · Syrris is the world leader in batch chemistry reactor systems and flow chemistry or microreactor systems. Syrris takes pride in creating extremely