3
Our Chromatography and GC-MS courses have been acknowledged as the leading training courses in South Africa. Many of the people that have successfully completed these courses are now in senior positions all over sub-Saharan Africa and even abroad. Between them, the lecturers share more than 50 years of experience ranging from the fundamentals of physics and chemistry to the analysis of trace impurities in high purity gases, general GC application support, clinical and environmental analysis to advanced GC method development, method validation and the design and building of multidimensional systems for specialised applications. Our course material has been developed by ourselves and the course handbooks are printed in colour for ease of use. The high quality of this material sets these courses apart from any other course in chromatography. We remain flexible in our approach and can accommodate some specific requirements that may be needed beyond the scope of the course. All these courses can be presented at a customer site with suitable infrastructure for practicals and lectures. We strongly recommend that out of town participants all stay at the same Bed & Breakfast, thereby simplifying transport arrangements. Revision is handled each morning before continuing with the course syllabus. All teas and lunches are included in the course fees. All courses notes and lectures are presented in English. l l l Chromatography Consultants cc. Chromatography Consultants c.c. Tel: Fax: E-mail: Website: can assist out of town visitors to find suitable accommodation and transport. Please indicate on the application form. Contact Eleanor for bookings. Postnet Suite 58 Private Bag X1006 Plettenberg Bay 6600 +27 (0)83 395 4609 +27 (0)44 533 5066 +27 (0)86 617 9285 [email protected] http://www.ssscc.co.za John Swinley worked for a number of years in isotope ratio determinations by Mass Spectrometry while studying at the University of the Witwatersrand. After graduation, he spent a year working in Germany and Switzerland in the development of mass spectrometers. For many years he worked in the analytical instrumentation market and one of his customers happened to be Piet de Coning, who had just started a laboratory at Medunsa. Together they developed a training course in Capillary Gas Chromatography which was present annually from 1995. Collaborative work undertaken by John and Piet led to three publications in Journal of Chromatography A covering different aspects of corrosive gas analysis. In 2003 they were nominated for the Peldev Chairman's Award for this work. In 2008 John was awarded the Shimadzu award as Chromatographer of the Year by ChromSA, a division of the South African Chemical Institute. John has presented courses in all major centres of South Africa as well as sub-Saharan Africa. These have been as varied as specialised courses for the brewing industry in Kenya and South Africa, to the optimisation of the GC-MS for forensic chemistry. Several courses have been presented on the analysis of gases in transformer oil as well as an in-house course for 21 Nigerian participants for refinery applications. In all, John and Piet have presented in excess of 50 courses and have seen many of their participants progress through their chosen industry. Piet de Coning graduated from Randse Afrikaanse Universiteit now University of Johannesburg as a biochemist. After working for a number of years in clinical chemistry applications of GC and GC-MS at Medunsa, he moved to Necsa where he developed methods and instrumentation for the analysis of fluorinated compounds and environmental samples. The work included the certification of electronic grade gases which had to be certified for export, in many cases down to sub-ppm concentrations levels of impurities When Piet joined Sasol R&D in 2007 one of his tasks was to establish a laboratory for Gas Analysis. Subsequently he also worked on methods using GCMS with a Supersonic Molecular Beam interface to analyse waxes and oils as well as applications for GC-MSMS in positive and negative ion chemical ionisation modes. Much of his work at Necsa and Sasol required method validation and uncertainty estimation and course participants have an opportunity to share some of this expertise. , . Courses 2015 - Background Courses 2015 - Background Certificate courses in gas chromatography and mass spectrometry Certificate courses in gas chromatography and mass spectrometry C 4 C 4 . . . . . . . .

Certificate courses in gas chromatography and mass ... 2015 Brochure.pdf · as applications for GC-MSMS in positive and negative ion chemicalionisationmodes. MuchofhisworkatNecsaand

Embed Size (px)

Citation preview

Our Chromatography and GC-MS courses have been

acknowledged as the leading training courses in South

Africa. Many of the people that have successfully

completed these courses are now in senior positions all

over sub-Saharan Africa and even abroad.

Between them, the lecturers share more than 50 years of

experience ranging from the fundamentals of physics and

chemistry to the analysis of trace impurities in high purity

gases, general GC application support, clinical and

environmental analysis to advanced GC method

development, method validation and the design and

building of multidimensional systems for specialised

applications.

Our course material has been developed by ourselves and

the course handbooks are printed in colour for ease of use.

The high quality of this material sets these courses apart

from any other course in chromatography.

We remain flexible in our approach and can accommodate

some specific requirements that may be needed beyond

the scope of the course. All these courses can be presented

at a customer site with suitable infrastructure for practicals

and lectures.

We strongly recommend that out of town participants all

stay at the same Bed & Breakfast, thereby simplifying

transport arrangements.

Revision is handled each morning before continuing

with the course syllabus.

All teas and lunches are included in the course fees.

All courses notes and lectures are presented in English.

l

l

l

Chromatography Consultants cc.

Chromatography Consultants c.c.

Tel:

Fax:

E-mail:

Website:

can assist out of

town visitors to find suitable accommodation and

transport.

Please indicate on the application form.

Contact Eleanor for bookings.

Postnet Suite 58

Private Bag X1006

Plettenberg Bay 6600

+27 (0)83 395 4609

+27 (0)44 533 5066

+27 (0)86 617 9285

[email protected]

http://www.ssscc.co.za

John Swinley worked for a number of years in isotope ratio

determinations by Mass Spectrometry while studying at

the University of the Witwatersrand. After graduation, he

spent a year working in Germany and Switzerland in the

development of mass spectrometers. For many years he

worked in the analytical instrumentation market and one of

his customers happened to be Piet de Coning, who had just

started a laboratory at Medunsa. Together they developed

a training course in Capillary Gas Chromatography which

was present annually from 1995.

Collaborative work undertaken by John and Piet led to

three publications in Journal of Chromatography A

covering different aspects of corrosive gas analysis. In 2003

they were nominated for the Peldev Chairman's Award for

this work. In 2008 John was awarded the Shimadzu award

as Chromatographer of the Year by ChromSA, a division of

the South African Chemical Institute.

John has presented courses in all major centres of South

Africa as well as sub-Saharan Africa. These have been as

varied as specialised courses for the brewing industry in

Kenya and South Africa, to the optimisation of the GC-MS

for forensic chemistry. Several courses have been

presented on the analysis of gases in transformer oil as well

as an in-house course for 21 Nigerian participants for

refinery applications. In all, John and Piet have presented

in excess of 50 courses and have seen many of their

participants progress through their chosen industry.

Piet de Coning graduated from Randse Afrikaanse

Universiteit – now University of Johannesburg as a

biochemist. After working for a number of years in clinical

chemistry applications of GC and GC-MS at Medunsa, he

moved to Necsa where he developed methods and

instrumentation for the analysis of fluorinated compounds

and environmental samples. The work included the

certification of electronic grade gases which had to be

certified for export, in many cases down to sub-ppm

concentrations levels of impurities

When Piet joined Sasol R&D in 2007 one of his tasks was to

establish a laboratory for Gas Analysis. Subsequently he

also worked on methods using GCMS with a Supersonic

Molecular Beam interface to analyse waxes and oils as well

as applications for GC-MSMS in positive and negative ion

chemical ionisation modes. Much of his work at Necsa and

Sasol required method validation and uncertainty

estimation and course participants have an opportunity to

share some of this expertise.

,

.

Courses 2015 - BackgroundCourses 2015 - Background

Certificate courses in gas chromatography

and mass spectrometry

Certificate courses in gas chromatography

and mass spectrometry C4C4....

.

.

.

.

A prerequisite for the GCMS

course is a thorough knowledge

of capillary GC or ideally atten-

dance of our capillary GC course.

Practical examples and computer

animations are used where

possible. Although, we felt that

the real priority was MS

interpretation, it is impossible to

make sense of a bunch of results

without fully understanding the

analytical technique.

This course has been designed to

cater for all users of mass

spectrometers as well as

potential users. Interactive

spectral interpretation

constitutes nearly half of this

course.

GC-MS Course

The course includes:

MS theory

The ion source

Mass analysers

MS detectors

Vacuum systems

Tandem mass spectrometry

Spectral manipulation

QC and troubleshooting

Tuning

Quantitation

Library searching

Chemistry

Atoms and isotopes

Ionisation

Initial inspection of the

spectrum

§

§

§

§

§

§

§

§

§

§

§

§

§

§

§

§

§

§

§

§

§

Identifying the molecular ion

Finding the molecular formula

The odd-even electron rule

Loss of the alkyl radical

Rearrangement reactions

Aromatic molecular ions

The Capillary GC course offers a very

“hands-on” approach because our

groups are limited to a maximum of 3

participants per instrument.

Recently the course was modernised

to include the most modern techni-

ques such as comprehensive GCxGC.

The course covers topics such as:

Chemical separations

History

The rate theory

Sampling

Chromatographic system

§

§

§

§

§

Capillary gas chromatography

§

§

§

§

§

§

§

§

§

§

§

Injectors

Sample introduction

Gas solid chromatography

Gas liquid chromatography

Capillary columns

GLC manufacturing, operation and

optimisation

The oven and temperature

programming

General properties of detectors

Mass flow detectors

Concentration detectors

Qualitative analysis

§

§

§

§

Quantitative analysis

Optimisation

Data processing

Troubleshooting

Capillary Gas Chromatography:

R 9,000.00

5 days from

11 - 15 May 2015

per person

excluding VAT

Gas Chromatography Mass Spectrometry:

R 8,300.00

4 days from

18 - 21 May 2015

per person

excluding VAT

Courses will be presented at Chemetrix, Midrand

Course Calendar 2013Course Calendar 2015