Upload
others
View
3
Download
0
Embed Size (px)
Citation preview
Reporting Limit 10 ppm *Total CBD = CBD + CBDA x 0.877 N/D - Not Detected, B/LOQ - Below Limit of Quantification
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 67995Order Name: CBD HempExtractBatch#: 3232020NOHE12Received: 12/28/2020Completed: 01/07/2021
Upstate Elevator Supply Co.388 Pine St. Suite 2Burlington VT, 05401(888) [email protected]
Sample
2.709% D9-THC
68.945% Total CBD
Cannabinoids TestSHIMADZU INTEGRATED UPLC-PDAGSL SOP 400 UPLOADED: 12/30/2020 12:23:20 Cannabinoids LOQ weight(%) mg/gD9-THC 10 PPM 2.709% 27.089THCA 10 PPM 0.057% 0.568CBD 10 PPM 68.807% 688.071CBDA 20 PPM 0.157% 1.567CBDV 20 PPM 0.358% 3.578CBC 10 PPM 2.894% 28.941CBN 10 PPM 0.065% 0.652CBG 10 PPM 1.283% 12.830CBGA 20 PPM N/D N/DD8-THC 10 PPM N/D N/DTHCV 10 PPM 0.140% 1.397
TOTAL D9-THC 2.709% 2.709%TOTAL CBD* 68.945% 689.445TOTAL CANNABINOIDS 76.470% 764.693
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
PESTICIDE ANALYSIS:GSL SOP 401 PREPARED: 12/29/2020 16:28:57 UPLOADED: 12/30/2020 15:31:11
N/D = Not Detected, A/LOQ = Above LOQ Level, B/LOQ = Below LOQ Level, B/LOD = Below LOD Level
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 67995Order Name: CBD HempExtractBatch#: 3232020NOHE12Received: 12/28/2020Completed: 01/07/2021
Upstate Elevator Supply Co.388 Pine St. Suite 2Burlington VT, 05401(888) [email protected]
GCMS-MS - Shimadzu GCMS-TQ8040
Pesticide Action Level(ppm)Results(ppm)
LOQ(ppm)
LOD(ppm)
CAPTAN 0.700 N/D 0.003 0.001CHLORDANE 0.100 N/D 0.003 0.001CHLORFENAPYR 0.100 N/D 0.003 0.001COUMAPHOS 0.100 N/D 0.003 0.001
Pesticide Action Level(ppm)Results(ppm)
LOQ(ppm)
LOD(ppm)
CYFLUTHRIN 2.000 N/D 0.003 0.001CYPERMETHRIN 1.000 N/D 0.003 0.001PARATHION-METHYL 0.100 N/D 0.003 0.001PENTACHLORONITROBENZENE 0.100 N/D 0.003 0.001
LCMS-MS - Shimadzu LCMS-8060
Pesticide Action Level(ppm)Results(ppm)
LOQ(ppm)
LOD(ppm)
ABAMECTIN B1A 0.100 N/D 0.005 0.001ACEPHATE 0.100 N/D 0.001 0.001ACEQUINOCYL 0.100 N/D 0.001 0.001ACETAMIPRID 0.100 N/D 0.005 0.001ALDICARB 0.100 N/D 0.005 0.001AZOXYSTROBIN 0.100 N/D 0.001 0.001BIFENAZATE 0.100 N/D 0.005 0.001BIFENTHRIN 3.000 N/D 0.005 0.001BOSCALID 0.100 N/D 0.005 0.001CARBARYL 0.500 N/D 0.003 0.001CARBOFURAN 0.100 N/D 0.001 0.001CHLORANTRANILIPROLE 10.000 N/D 0.005 0.005CHLORPYRIFOS 0.100 N/D 0.001 0.001CLOFENTEZINE 0.100 N/D 0.001 0.001DAMINOZIDE 0.100 N/D 0.005 0.001DIAZINON 0.100 N/D 0.001 0.001DICHLORVOS 0.100 N/D 0.005 0.001DIMETHOATE 0.100 N/D 0.001 0.001DIMETHOMORPH 2.000 N/D 0.005 0.001ETHOPROPHOS 0.100 N/D 0.001 0.001ETOFENPROX 0.100 N/D 0.001 0.001ETOXAZOLE 0.100 N/D 0.010 0.005FENHEXAMID 0.100 N/D 0.005 0.001FENOXYCARB 0.100 N/D 0.005 0.001FENPYROXIMATE 0.100 N/D 0.001 0.001FIPRONIL 0.100 N/D 0.003 0.001FLONICAMID 0.100 N/D 0.025 0.010FLUDIOXONIL 0.100 N/D 0.003 0.001HEXYTHIAZOX 0.100 N/D 0.005 0.001IMAZALIL 0.100 N/D 0.005 0.001
Pesticide Action Level(ppm)Results(ppm)
LOQ(ppm)
LOD(ppm)
IMIDACLOPRID 5.000 N/D 0.005 0.001KRESOXIM-METHYL 0.100 N/D 0.010 0.005MALATHION 0.500 N/D 0.005 0.001METALAXYL 2.000 N/D 0.001 0.001METHIOCARB 0.100 N/D 0.005 0.001METHOMYL 1.000 N/D 0.001 0.001MEVINPHOS 0.100 N/D 0.001 0.001MYCLOBUTANIL 0.100 N/D 0.005 0.001NALED 0.100 N/D 0.005 0.001OXAMYL 0.500 N/D 0.001 0.001PACLOBUTRAZOL 0.100 N/D 0.005 0.001PERMETHRINS 0.500 N/D 0.005 0.001PHOSMET 0.100 N/D 0.005 0.001PIPERONYLBUTOXIDE
3.000 N/D 0.001 0.001
PRALLETHRIN 0.100 N/D 0.005 0.005PROPICONAZOLE 0.100 N/D 0.010 0.005PROPOXUR 0.100 N/D 0.001 0.001PYRETHRINS(PYRETHRIN I)
0.500 N/D 0.005 0.005
PYRIDABEN 0.100 N/D 0.005 0.001SPINETORAM 0.100 N/D 0.001 0.001SPINOSAD 0.100 N/D 0.001 0.001SPIROMESIFEN 0.100 N/D 0.005 0.001SPIROTETRAMAT 0.100 N/D 0.001 0.001SPIROXAMINE 0.100 N/D 0.001 0.001TEBUCONAZOLE 0.100 N/D 0.005 0.001THIACLOPRID 0.100 N/D 0.001 0.001THIAMETHOXAM 5.000 N/D 0.001 0.001TRIFLOXYSTROBIN 0.100 N/D 0.001 0.001
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
fa
† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella run as Multiplex ** CFU/g Calculation based on MIP/Extract matrix *** Flavus = 2 Copies of DNA / Fumigatis = 2 Copies of DNA Niger = 20 Copies of DNA / Terrus = 10 copies of DNA
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 67995Order Name: CBD HempExtractBatch#: 3232020NOHE12Received: 12/28/2020Completed: 01/07/2021
Upstate Elevator Supply Co.388 Pine St. Suite 2Burlington VT, 05401(888) [email protected]
Microbial Analysis:PCR - Agilent AriaMX
Microbial Analysis GSL SOP 406 Uploaded: 01/05/2021 11:42:04
MICROBIAL ANALYSIS:
Test SOP Test Method Device Used LOD AllowableCriteria Actual Result Pass/Fail
ASPERGILLUS FUMIGATUS*** 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
ASPERGILLUS TERREUS*** 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
ASPERGILLUS FLAVUS*** 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
ASPERGILLUS NIGER*** 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
STEC E. COLI* 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
SALMONELLA* 406.01 USP 61/62† ARIAMX PCR 1 CFU/G**DETECT/NOTDETECTED
NOT DETECTED PASS
TOTAL YEAST AND MOLD 406.01 USP 61/62† ARIAMX PCRCFU/G BYSAMPLETYPE**
1,000 CFU/G NOT DETECTED PASS
AEROBIC BACTERIA COUNT 406.01 USP 61/62† ARIAMX PCRCFU/G BYSAMPLETYPE**
10,000 CFU/G NOT DETECTED PASS
ENTEROBACTERIACEAE 406.01 USP 61/62† ARIAMX PCRCFU/G BYSAMPLETYPE**
100 CFU/G NOT DETECTED PASS
COLIFORM 406.01 USP 61/62† ARIAMX PCRCFU/G BYSAMPLETYPE**
100 CFU/G NOT DETECTED PASS
PCR - Agilent AriaMX
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104
Order #: 67995Order Name: CBD HempExtractBatch#: 3232020NOHE12Received: 12/28/2020Completed: 01/07/2021
Upstate Elevator Supply Co.388 Pine St. Suite 2Burlington VT, 05401(888) [email protected]
Mycotoxin Analysis:LC-MS - Shimadzu LCMS-8060GSL SOP 401 Uploaded: 12/30/2020 15:31:03
Analyte Action Lvl (ppb) Results (ppb)AFLATOXIN B1 20 N/DAFLATOXIN B2 20 N/DAFLATOXIN G1 20 N/DAFLATOXIN G2 20 N/DOCHRATOXIN A 20 N/D
LOQ is 1ppb, LOD is 1ppb
Heavy Metals Analysis:ICP-MS - Shimadzu ICPMS-2030GSL SOP 403 Uploaded: 01/07/2021 08:10:32
Metal Action Level (ppb) Result (ppb)ARSENIC (AS) 200 B/LOQCADMIUM (CD) 200 B/LOQMERCURY (HG) 100 B/LOQLEAD (PB) 500 135
Lower Limit of Quantitation (LOQ) is 75 ppb
Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director
Green Scientific [email protected]
1-833 TEST CBD
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.