Cetiol C5 An efficient Substitute for Cyclic Silicones

1

Cetiol® C5

An efficient Substitute for Cyclic Silicones

Silicon-free Formulations

Experience the nice sensorial Feel

BASF Personal Care2

Cetiol® C5

Market demand

Product description

Sensorial profile

Applications:

Skin Care

Decorative Cosmetics

Hair Care

BASF Personal Care3

Cetiol® C5

Market demand

Product description

Sensorial profile

Applications:

Skin Care


Hair Care

BASF Personal Care4

Cetiol® C5

Emollients Portfolio

Naturals

From 100% natural,

renewable

feedstocks; physically

purified by

water/alcohol or

energy

Natural

Modified

From 100%

natural, renewable

feedstocks;

chemically

processed,

catalyst or reaction

aids used

Ecohybrids

From natural,

renewable &

synthetic

feedstocks; natural

& synthetic building

blocks are

combined in a

chemical process.

Share natural C-

atoms > 70 %

Hybrids

From natural,

renewable &

synthetic

feedstocks; natural

& synthetic building

blocks are combined

in a chemical

process. Share

natural C-atoms <

70 %

Synthetics

From synthetic

feedstocks;

chemically

processed

Cegesoft® GPO

Cegesoft® PFO

Cegesoft® SB

Cetiol® C5

Cetiol® OE

Myritol® 331

Cegesoft® VP

Cegesoft® SH

Cetiol® PGL

Cetiol® V

Cetiol® SB 45

Eutanol® G

Fitoderm®

Cetiol® CC Cetiol® SenSoft

Cetiol® SN

Cetiol® B

Cetiol® AB

BASF Personal Care5

Cetiol® C5

Trend – Silicone-free

Products with silicone-free claims in the product

description increased significantly within the last

2 years in Europe.

Source: GNPD.com (2009 extrapolated)

BASF Personal Care6

Cetiol® C5

Market demand

Product description

Sensorial profile

Applications:

Skin Care


Hair Care

BASF Personal Care7

Cetiol® C5

INCI: Coco-Caprylate

From 100 % natural, renewable feedstocks

Skin compatibility: non irritant

Sensory feeling: cyclomethicone-like feel

Spreading value: 1300mm2 / 10min.

Easier handling in production than a volatile

substance, easier emulsification

BASF Personal Care8

Cetiol C5 Cyclic D5 Other

Alternatives

Origin 100 % vegetable synthetic mostly synthetic /

petro based

Skin compatibility + + -

Biodegradability + - -

Easy-to-emulsify + - -

Easy-to-handle + - -

Cetiol® C5

Coco-Caprylate

+ = good result, - = bad result

BASF Personal Care9

Cetiol® C5

Cetiol® C5 has good skin compatibility

To

tal ir

rita

tio

n S

co

re (

RS

S)

Irritant Moderate Non-irritant

(single 24hr occlusive

patchtest, 20% in EtOH,

Cetiol C5 undiluted, n=20)

Skin Compatibility of various light Emollients

BASF Personal Care10

Cetiol® C5

Market demand

Product description

Sensorial profile

Applications:

Skin Care


Hair Care


Cetiol® C5Skin distribution & adsorption: spreading value

Emollient INCI Spreading Value

[mm2/10 min]

Cyclomethicone > 190 high

Cetiol® Sensoft Propylheptyl Caprylate 1900

Cetiol® CC Dicaprylyl Carbonate 1600

Cetiol® OE Dicaprylyl Ether 1600

Cetiol® C5 Coco-Caprylate 1300

Cetiol® B Dibutyl Adipate 1000

Myritol® 331 Cocoglycerides 750 medium

Cetiol® PGL Hexyldecanol/Hexyldecyl Laurate 750

Eutanol® G 16 Hexyldecano 700

Myritol® 318 Caprylic/Capric Triglyceride 550

Cetiol® J 600 Oleyl Erucate 350 slow

Cegesoft® PS 6 Olus Oil (EU), Vegetable Oil 230

Almond Oil Prunus Dulcis 200


-1 -0,5 0 0,5 1

[low] [high] Spreadability

[slow] [fast] Distribution

[less] [muss] Cushion

[slow] [fast] Absorption I (1min.)

[slow] [fast] Absorption II (3min.)

[much] [less] Tackiness

[much] [less] Oiliness

[less] [much] Waxiness

[less] [much] Velvety

[less] [much] Powdery

[less] [much] Softness

[less] [much] Smoothness

[less] [much] Care feeling

Spreadability

Distribution

Cushion

Absorption I (1min.)

Absorption II (3min.)

Tackiness

Oiliness

Waxiness

Velvety

Powdery

Softness

Smoothness

Care feeling

Acceptance [low ] [high] Acceptance

Cetiol® C5

Cetiol® C5 matches Cyclomethicone in key skin sensory parameters

Sensorial profile of Cetiol® C5 vs Cyclomethicone

Line Zero = Cyclomethicone

n = 11

not significantSignificance ≥ 90% Significance ≥ 95% Significance ≥ 99%


Cetiol® C5

Ingredients INCI FR00827-404 -407

Emulgade® 165 Glyceryl Stearate (and) PEG-100 Stearate 3.0 3.0

Lanette® O Cetearyl Alcohol 2.0 2.0Cetiol® ININ Isononyl Isononanoate 5.0 5.0Myritol® 318 Caprylic/Capric Triglyceride 5.0 5.0DC 245 Cyclomethicone 5.0 ---Cetiol® C5 Coco-Caprylate --- 5.0Deionized water Water 76.1 76.1Glycerin Glycerin 3.0 3.0Elestab™ 50J Chlorphenesin (and)

Methylparaben (EU) 0.4 0.4

Rheocare™ C PLUS Carbomer 0.25 0.25NaOH (as 25%) Sodium Hydroxide 0.25 0.25

Viscosity mPa.s (Brookfield RVT, RT, Helipath TE, 4rpm) 166,000 131,000pH 6.22 6.20

Sensorial profile of Cetiol® C5 in emulsion– Test formulation


Cetiol® C5

Cetiol® C5 matches cyclomethicone in key sensory parameters

in formulations

Sensorial profile of Cetiol® C5 vs Cyclomethicone in emulsion

Line Zero = Cyclomethicone-formula

n = 11



INCI: Aqua, glycerin, petrolatum, dimethicone,

cyclopentasiloxane, stearic acid, caprylic/capric

triglyceride, glycol stearate, PEG-100 stearate,

dimethiconol, glyceryl stearate, cetyl alcohol, gelidium

cartilagineum extract, helianthus annuus (sunflower) seed

extract, octyldodecanol, tocopheryl acetate, hydrogenated

coco-glycerides, stearamide AMP, sodium hydroxide,

acrylates/C10-30 alkyl acrylate crosspolymer, carbomer,

propylene glycol, diethylhexanoate, disodium EDTA,

parfum, phenoxyethanol, methylparaben, propylparaben,

butylparaben, alpha-isomethyl ionone, benzyl alcohol,

benzyl salicylate, butylphenyl methylpropional, citronellol,

eugenol, hexyl cinnamal, hydroxyisohexyl 3-cyclohexene

carboxaldehyde, limonene, linalool, CI 77891....

Cetiol® C5

Sensory Benchmark Tests


Cetiol® C5Moisturizing Body Lotion

Ingredients INCI %

Eumulgin® Prisma Disodium Cetearyl Sulfosuccinate 1.00Lanette® O Cetearyl Alcohol 1.00Cutina® PES Pentaerythrityl Distearate 1.00Cutina® HVG Hydrogenated Vegetable Glycerides 0.50Cetiol® MM Myristyl Myristate 1.00 Cetiol® SB 45 Butyrospermum Parkii (Shea) Butter 0.50Cetiol® C5 Coco-Caprylate 6.00Cetiol® Sensoft Propylheptyl Caprylate 6.00Copherol® F 1300 C Tocopherol 0.50Cosmedia® SP Sodium Polyacrylate 0.30Keltrol CGT Xanthan Gum 0.20Glycerin Glycerin 5.00Cosmedia® SILC Silica 0.50Preservatives, Perfume q.s.Water Water 76.50

pH 6.2viscosity: ~ 12,000 mPas

SC-DE/09/197/6


Prototype formula with Cetiol® C5 matches benchmark

SC-DE/09/197/6 vs. Benchmark (zeroline)

n = 11


Cetiol® C5Moisturizing Body Lotion


Aqua/water, cyclohexasiloxane, glycerin, paraffinum liquidum/

mineral oil, myristyl/myristate, butyrospermum parkii butter/

shea butter, stearic acid, palmitic acid, PEG-100 stearate, cera

alba/ beeswax, glyceryl stearate, ethylhexyl

methoxycinnamate, PEG-20 stearate, drometrizole trisiloxane,

acrylamide/sodium acryloyldimethyltaurate copolymer, stearyl

alcohol, cetyl alcohol, isohexadecane, glycine soja

protein/soybean protein, methylparaben, acrylates copolymer,

triethanolamine, polysorbate 89, retinyl palmitate,

ethylparaben, acetyl trifluoromethylphenyl valylglycine,

disodium EDTA, helianthus annuus seed oil/ sunflower seed

oil, benzyl salicylate, chlorhexidine digluconate, benzyl

benzoate, linalool, benzyl alcohol, phenethyl alcohol, limonene,

hexyl cinnamal, citronellol, butylphenyl methylpropional,

geraniol, hydrolyzed soy protein, alpha-isomethyl ionone,

hydrolyzed elastin/ hydrolyzed elastin, amyl cinnamal, citral,

benzyl cinnamate, parfum/ fragrance, chlorphenesin.

F.I.L. B31930/1

Cetiol® C5



Cetiol® C5Moisturizing Day Cream

Ingredients INCI %

Eumulgin® Prisma Disodium Cetearyl Sulfosuccinate 0.25Cutina® PES Pentaerythrityl Distearate 1.00Cutina® HVG Hydrogenated Vegetable Glycerides 2.50Cetiol® SB 45 Butyrospermum Parkii (Shea) Butter 1.50Cetiol® C5 Coco-Caprylate 8.00Cetiol® PGL Hexyldecanol (and) Hexyldecyl Laurate 5.00Copherol® F 1300 C Tocopherol 0.50Cosmedia® SP Sodium Polyacrylate 0.80Eusolex OCR Octocrylene 2.00Parsol 1789 Butyl Methoxydibenzoylmethane 0.60Keltrol CGT Xanthan Gum 0.10Glycerin Glycerin 5.00Tapioca Starch Tapioca Starch 0.50Preservatives, Perfume q.s.Water Water 72.25

pH: 6.0Viscosity: ~175,000 mPas

SC-DE/09/201/3




n = 11

not siificant Significance ≥ 90% Significance ≥ 95% Significance ≥ 99%

Cetiol® C5Moisturizing Day Cream


Water, cyclomethicone, ethylhexyl salicylate, glycerin,

phenylbenzimidazole sulfonic acid, sucrose polystearate,

alcohol denat., dimethicone, methylpropanediol, aluminum

starch octenylsuccinate, mica, sine adipe lac, hydrolized

keratin, mangifera indica fruit juice, sodium stearoyl glutamate,

trideceth-9, hydrogenated polyisobutene, dimethiconol,

propylene glycol, ammonium acryloyldimethyltaurate/VP

copolymer, chondrus crispus, acrylates/C10-30 alkyl acrylate

crosspolymer, butyl methoxydibenzoylmethane, citric acid,

sodium carbomer, trisodium EDTA, phenoxyethanol, sodium

chloride, linalool, butylphenyl methylpropional, limonene,

citronellol, perfume,

CI 77891, CI 77491, CI 75470

Cetiol® C5



Cetiol® C5Tinted Day Cream

Ingredients INCI %

Emulgade® PL68/50 Cetearyl Glucoside (and) Cetearyl Alcohol 4.00Cutina® PES Pentaerythrityl Distearate 2.00Cetiol® SB 45 Butyrospermum Parkii (Shea) Butter 0.30Cetiol® C5 Coco-Caprylate 10.00Myritol® 312 Caprylic/Capric Tryglyceride 5.00Eutanol® G Octyldodecanol 0.50Copherol® F 1300 Tocopherol 0.50Keltrol CGT Xanthan Gum 0.05Glycerin Glycerin 3.00Tapioca Starch Tapioca Starch 0.50RonaTimiron Starluster MP-115 0.50Colorona Percious Fine Gold 0.30Rona Timiron Supersheen MP-1001 0.50Preservatives, Perfume q.s.Water Water 72.85

pH: 7.2viscosity: ~160,000 mPas

SC-DE/09/200/10




n = 11


Cetiol® C5

Tinted Day Cream


Cetiol® C5

Market demand

Product description

Sensorial profile

Applications:

Skin Care


Hair Care


Pleasure, Sensory and Performance

Cetiol® C5

Skin Care


Cetiol® C5Refreshing Protecting Gel Cream

Ingredients INCI %

I. Deionized water Water 76.10Glycerin Glycerin 3.00

II. Cosmedia® SP Sodium Polyacrylate 1.20 III. Cegesoft® PFO Passiflora Incarnata Seed Oil 2.00

Cegesoft® SBE Butyrospermum Parkii (Shea Butter) 1.50Eusolex 2292 Ethylhexyl Methoxycinnamate 2.00DC 200, 100 cs Dimethicone 2.00

IV. Cetiol® CC Dicaprylyl Carbonate 5.00Cetiol® C5 Coco-Caprylate 4.00Eusolex 4360 Benzophenone-3 0.10

V. Deionized water Aqua 5.00Osmhydran™ LS 8453 see data sheet 2.00

VI. Vegeseryl ™ LP LS 9058 Hydrolyzed Soy Protein 1.00Coviox® T 70 C Tocopherol 0.10Perfume, Preservatives q.s.

Viscosity mPas Brookfield RVT, RT, Helipath TE, speed 4): 89,000

pH: 5.5

FR00847.300


Cetiol® C5Delicious Night Cream

Ingredients INCI %

I. Deionized Water Water 61.95EDTA, 4Na Tetrasodium EDTA 0.05Elestab® 50J Chlorphenesin (and) Methylparaben 0.40Butylene Glycol Butylene Glycol 2.00Glycerin Glycerin 5.00

II. Cosmedia® SP Sodium Polyacrylate 0.50III. Emulgade® Sucro Sucrose Polystearate (and ) 5.00

Hydrogenated PolyisobuteneCutina® PES Pentaerythrityl Distearate 2.00Cetiol® CC Dicaprylyl Carbonate 5.00Cetiol® SN Cetearyl Isononanoate 3.00Cetiol® PGL Hexyldecanol (and) Hexyldecyl Laurate 3.00Cegesoft® PFO Passiflora Incarnata 2.00Cetiol® C5 Coco-Caprylate 4.00

IV. Cosmedia® PMMA V8 Polymethylmethacrylate 2.00V. Coviox® T 70 C Tocopherol 0.10

Perfume Perfume q.s.VI. Dulcemin™ LS 8594 see data sheet 4.00

Viscosity mPas (Brookfield RVT, RT, Helipath TE, speed 4): 148,700

pH: 6.3

FR00847.800


Cetiol® C5Fine comfortable Day Cream

Ingredients INCI %

I. Eumulgin® SG Sodium Stearoyl Glutamate 0.20Cutina® PES Pentaerythrityl Distearate 1.00Cutina® HVG Hydrogenated Vegetable Glycerides 1.50Cetiol® CC Dicaprylyl Carbonate 3.00Cetiol® PGL Hexyldecanol (and) Hexyldecyl Laurate 2.00Copherol® F 1300C Tocopherol 0.50Cegesoft® PFO Passiflora Incarnata 1.00Uvinul MC 80 Ethylhexyl Methoxycinnamate 2.00Parsol 1789 Butyl Methoxydibenzoylmethane 0.60Cosmedia® SP Sodium Polyacrylate 0.70Emulgade® Sucro Sucrose Polystearate (and ) 2.00

Hydrogenated PolyisobuteneCetiol® C5 Coco-Caprylate 2.00

II. Keltrol T Xanthan Gum 0.20III. Glycerin Glycerin 4,00

Deionized water Water 75.80IV. Indinyl™ CA LS 8998 see data sheet 2.50V. Phenonip XB Phenoxyethanol / Parabens 1.00

Perfume Perfume q.s.

Viscosity mPas (Brookfield RVT, RT, Helipath TE, speed 4): 214,000

pH: 6.5


Cetiol® C52-phase Make-up Remover

Ingredients INCI %

I. Cetiol® CC Dicaprylyl Carbonate 3.00Cetiol® C5 Coco-Caprylate 17.00Isohexadecane Isohexadecane 20.00

II. Hexylene Glycol Hexylene Glycol 1.00EDTA, 4 Na Tetrasodium EDTA 0.05Benzyl Alcohol Benzyl Alcohol 0.50NaCl Sodium Chloride 0.90Dipotassium Hydrogenphosphate Dipotassium Hydrogenphosphate 0.16Potassium Dihydrogenphosphate Potassium Dihydrogeophosphate 0.07Blue 1 (0.1 %) CI42090 0.25Deionized Water Water 57.07

Final pH 7,2

FR00847.2000


Cetiol® C5

Market demand

Product description

Sensorial profile

Applications:

Skin Care


Hair Care


Glamour, Sensory and Performance

Cetiol® C5



Cetiol® C5Mat finish Silicone-free Fluid Foundation O/W

Ingredients INCI %

I. Lameform® TGI Polyglyceryl-3 Disostearate 1.50Eumulgin® BA25 Beheneth-25 3.50Cetiol® CC Dicaprylyl Carbonate 4.90Cetiol® C5 Coco-Caprylate 4.00Cegesoft® VP s. data sheet 3.00 Cutina® PES Pentaerythrityl Distearate 1.00 Cegesoft® SH Shorea Stenoptera 1.00Phenonip XB Phenoxyethanol (and) Parabens 0.80Cegesoft® PS 6 Vegetable Oil 4.90Cetiol® SenSoft Propylheptyl Caprylate 3.00

II. Sun Croma C47-051 Titanium Dioxide 6.00SunPuro Yellow Iron Oxide C33-9001 Iron Oxide CI 77492 1.30 SunPuro Red Iron Oxide C33-8001 Iron Oxide CI 77491 0.60SunPuro Black Iron Oxide C33-7001 Iron Oxide CI 77499 0.20

III. Deionized Water Water 50.90Glycerin Glycerin 3.00Butylene Glycol Butylene Glycol 2.00

IV. Veegum Ultra Magnesium Aluminium Silicate 1.00Keltrol T Xanthan Gum 0.40

V. Cosmedia® Gel CC Dicaprylyl Carbonate (and) Stearalkonium Hectorite (and) Propylene Carbonate 3.00

VI. Cosmedia® PMMA V12 Polymethylmethacrylate 4.00 VII. Perfume Perfume q.s.

Viscosity mPas (Brook, RVT, spindle 3, speed 5) 8100mPas pH: 7.1

FR00829.1100


Cetiol® C5Anti-aging Concealer Silicon-free

Ingredients INCI %

I. Lanette® 22 Behenyl Alcohol 5.50Cutina® HR Hydrogenated Castor Oil 2.40Candelilla wax Candelilla Wax 4.00Cerauba T1 Carnauba Wax 1.60Myritol® 331 Cocoglycerides 10.00Cetiol® C5 Coco-Caprylate 15.00Myritol® 312 Caprylic/Capric Triglycerides 11.00Cegesoft® C24 Ethylhexyl Palmitate 20.70Lameform® TGI Polyglyceryl-3 Diisostearate 2.50

II. Sun Croma C47-051 Titanium Dioxide 6.00SunPuro Yellow Iron Oxide C33-9001 Iron Oxide CI 77492 1.30SunPuro Red Iron Oxide C33-8001 Iron Oxide CI 77491 0.60SunPuro Black Iron Oxide C33-7001 Iron Oxide CI 77499 0.20

III. Cosmedia® Cushion HDI/Trimethylol Hexyllactone Crosspolymer (and) Silica 4.00

Talc Talc 10.00IV. Active Powder Firmness™ LS 9689 Upon request 5.00

Perfume Perfume 0.2

FR00847.1603


Cetiol® C5Moisturizing Fluid Foundation Ecocert O/W

Ingredients INCI %

I. Eumulgin® SG Sodium Stearoyl Glutamate 0.75Dehymuls® PGPH Polyglyceryl-2 Dipolyhydroxystearate 1.75Cetiol® C5 Coco-Caprylate 4.00Myritol® 331 Cocoglycerides 4.00Cegesoft® VP s. data sheet 3.00 Cutina® HVG Hydrogenated Vegetable Glycerides 1.00Cegesoft® SH Shorea Stenoptera 1.00Cegesoft® PS 6 Vegetable Oil 3.00Vegetable Oil Amande Douce Prunus Amygdalus Dulcis Oil* 3.00Geogard 221 Dehydroacetic Acid (and) Benzyl Alcohol 0.80

II. Sun Croma C47-051 Titanium Dioxide 7.00SunPuro Yellow Iron Oxide C33-9001 Iron Oxide CI 77492 1.50 SunPuro Red Iron Oxide C33-8001 Iron Oxide CI 77491 0.50SunPuro Black Iron Oxide C33-7001 Iron Oxide CI 77499 0.20

III. Deionized Water Water 35.50Glycerin Glycerin 3.00Propylene Glycol Propylene Glycol 2.00

IV. Veegum Ultra Magnesium Aluminium Silicate 1.00Keltrol T Xanthan Gum 0.20

V. Cetiol® CC Dicaprylyl Carbonate 2.00Bentone EW Hectorite 0.80

VI. Sunsil 130 Silica 4.00 VII. Hamamelis HYD30006 Hamamelis Virginiana Distillate* 20.00 VIII. Perfume Perfume q.s.

Viscosity mPas Brook RVT, spindle 3, speed 5, 12,000 mPas pH: 5.8

FR00847.1100


Cetiol® C5Lip Gloss Silicone-free

Ingredients INCI %

I. Polybutene M100 Polybutene 53.50 Cetiol® SenSoft Propylheptyl Caprylate 10.00IPP Isopropyl Palmitate 15.00Cetiol® C5 Coco-Caprylate 5.00Cosmedia® DC Hydrogenated Dimer Dilinoleyl /

Dimethylcarbonate Copolymer 5.00Fitoderm® Squalane 5.0Red 28 Al Lake Red 28 Lake 0.05Perfume Perfume 0.3Coviox® T 70 C Tocopherol 0.10Nipasol M Propylparaben 0.50

II. Aerosil R972 Silica Dimethyl Silylate 5.30III. Ronastar Noble Spars Calcium Aluminium 0.25

Borosilicate (and) Silica (and) Titanium Dioxide

Viscosity (Brook. RVT, spindle 5, speed 10) 11,000 mPas

FR00829.100


Cetiol® C5

Market demand

Product description

Sensorial profile

Applications:

Skin Care


Hair Care


Cetiol® C5Natural Gloss Treatment Cream

Ingredients INCI %

I. Deionized Water Water 88.56Neolone 950 Methylisothiazolinone 0.10

II. Ultragel™ 300 Polyquaternium-37 0.30

III. Dehyquart® C 4046 Cetearyl Alcohol (and) Dipalmitoylethyl 5.00Hydroxyethylmonium Methosulfate (and) Ceteareth-20

IV. Cetiol® C5 Coco-Caprylate 4.00Perfume Perfume q.s.

V. Gluadin® WLM Benz Hydrolyzed Wheat Protein 2.00

VI. NaOH (sol. 50 %) Sodium Hydroxide 0.04

Final pH: 4.56Final viscosity: Brk, RVT (spindle 5, speed 10): 16,240 mPa.s

FR00847.702


This document, or any answers or information provided herein by BASF, does not constitute a legally

binding obligation of BASF. While the descriptions, designs, data and information contained herein are

presented in good faith and believed to be accurate, it is provided for your guidance only. Because many

factors may affect processing or application/use, we recommend that you make tests to determine the

suitability of a product for your particular purpose prior to use. It does not relieve our customers from the

obligation to perform a full inspection of the products upon delivery or any other obligation. The claims and

supporting data provided in this publication have not been evaluated for compliance with any jurisdiction’s

regulatory requirements and the results reported may not be generally true under other conditions or in

other matrices. Users must evaluate what claims and information are appropriate and comply with a

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Documents

Cetiol C5 An efficient Substitute for Cyclic Silicones