CHAPTER 1-Distillation Column Design

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Distillation Column Design for Deethanizer

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CHAPTER 1: GENNERAL DESCRIPTION OF DEETHANIZER (A-502)Deethanizer column is designed purposely to separate between C2 Product (Ethane, Ethylene, Acetylene) as top product and C3+ (propane, propylene, 1-3, butadiene) as bottom. The feed is coming from the Demethanizer. Several advantages of distillation include its ability:1. To produce a product with high purity.2. To handle a wide range of throughput.3. To handle a wide range of feed concentrations.

By operating at pressure of --- kPa, the deethanizer (A-502) is operated at temperature of --- oC. Sieve tray method has been selected to design the distillation column. Based on the calculations results, there are --- trays overall in the column to achieved the desired product quality with the assumptions of ---% trays efficiency. Stainless steel is chosen as the designed and tray material due to the ability of corrosion resistance. Tray columns generally provide satisfactory operation over a wide range f liquid and vapor loadings. The vapor and liquid rates can vary independently over a broad range and the column can operate satisfactorily. The basic requirement of a sieve tray is that it should: 1. Provide good vapor-liquid contact2. Provide sufficient liquid holdup for good mass transfer.3. Have sufficient area and spacing to keep entrainment and pressure drop within acceptable limits.4. Have sufficient downcomer area for the liquid to flow freely from plate to plate.

CHAPTER 2: PROCESS DESIGN OF DEETHANIZER (A-502)2.1 Multi-Component DistillationDetailed process design of deethanizer, A-502 which includes determination of column operating parameters and sizing of column internals are shown on this section.Determination of Column Operating ConditionThe first assumptions made in order to determine the column operating condition are that nothing heavier than heavy key appears at distillate and nothing lighter than light key in bottom. The summary of component distribution is as below:Table 1: Distribution of ComponentComponentFeed flow (kmol/hr)Feed Fraction, xfDistillate flow (kmol/hr)Distillate Fraction, xdBottom flow (kmol/hr)BottomFraction, xb

Ethane4298.774254.4245.39

Ethylene5889.025890.500.01

Acetylene55.3655.280.08

Propane27.60027.60

Propylene103.080103.14

1-3, Butadiene255.550255.68

Total

For the distillation column, the heavy key (HK) component is --- while the light key (LK) component is the ---. The vapor pressure, P* for pure component can be obtained from extended Antoine Equation below:

Where the value of A, B, C, D and E constant obtained from the appendix C in Coulson & Richardson Chemical Engineering Volume 6 (Fourth Edition). The relative volatility of each component is calculated by using the formula.

Relative volatility,

ComponentABC

Ethane

Ethylene

Acetylene

Propane

Propylene

1-3, Butadiene6.84999930.546238.854

Total

Table 2: Distribution of ComponentComponentP*KRelative Volatility,

Ethane

Ethylene

Acetylene

Propane

Propylene

1-3, Butadiene

Total