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TREATMENT RECORD FOR RANDOLPH CEMETERY, PHASE 2,

CITY OF COLUMBIA, RICHLAND COUNTY, S.C.

Chicora Foundation, Inc. PO Box 8664 ��

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www.chicora.org

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RANDOLPH CEMETERY CONSERVATION TREATMENT RECORDCEMETERY MARKERS

Chicora Foundation, Inc. PO Box 8664 Columbia, SC 29202 803-787-6910

Location: Randolph Cemetery State: SC ID.: Stone No.: 31.07, Priscilla Thompson Photographs: Before: x During: After: x

Condition Report

Marble headstone with ground break; one fragment lying face up on surface, other fragment still below grade. Fragment in the ground has likely sunk and requires resetting (inscription on top fragment appears incomplete). Heavy biological growth and staining.

Treatment Report

1. Bottom half of stone was excavated from the soil, set on 2x4s and allowed to dry. 2. Holes were drilled for the insertion of two 3/8” diameter 316 threaded stainless steel rods about 8-inches in

length. Registration was checked and holes cleaned using compressed air and acetone. 3. Rods were set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. The stone was clamped,

registration rechecked, and epoxy was allowed to set for 24 hours. 4. The stone was reset in a bed of pea gravel to promote drainage of water away from the stone and still

provide some flexibility should it be impacted by landscape maintenance activities. 5. The break was infilled using Jahn M-120 marble mortar. This was misted for 48 hours during the curing. 6. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Recommendation: If a means of watering is available at the cemetery, we recommend reseeding around this stone in order to minimize splash-back, soiling, and erosion. Splash-back will dramatically increase soiling and the resulting soil erosion will “dish-out” the soil around the stone, creating a depression that collects rain water, increasing moisture up-take by the stone. Recorded By: N. Southerland/ M. Trinkley Treated By: NS/DH Date: 9/9/10

Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 38, Harriet Taylor Photographs: Before: x During: After: x

Condition Report

Marble headstone is severely tilted in the ground. Evidence of mower damage scar along front base. Heavy biological growth.

Treatment Report

1. The stone was reset in a bed of pea gravel to promote drainage of water away from the stone and still

provide some flexibility should it be impacted by landscape maintenance activities. 2. Stone was cleaned using D/2 Biological Solution and flushed with potable water. Cleaning has improved

legibility of the stone and reduced the visibility of the mower scar at the base. Recorded By: N. Southerland/ M. Trinkley Treated By: NS/DH Date: 9/9/2010

Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 41.02, John F. Barre Photographs: Before: x During: After: x

Condition Report

Marble die on base has been toppled. While footprint of the die is visible on the base, there is no evidence that it was pinned. There is no evidence of any remnant setting compound. Stone evidences heavy biological growth and staining.

Treatment Report

1. The base of the stone was excavated and releveled in a bed of pea gravel to promote drainage of water

away from the stone and still provide some flexibility should it be impacted by landscape maintenance activities.

2. The stone was drilled for the insertion of a single 5/8” 316 threaded stainless steel rod about 6-inches in length. This was set in the center of the die. Registration was checked and holes cleaned using compressed air and acetone.

3. The rod was set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. 4. The die was set on the base in a 1:2.5 mix of NHL3.5 and sand, braced, and allowed to set for 48 hours. 5. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Recorded By: N. Southerland/ M. Trinkley Treated By: NS/DH Date: 9/9/2010

Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 58, Rosena Palmer Photographs: Before: x During: x After: x

Condition Report

Marble tablet stone originally reported to be in two pieces; however, a third piece was found during excavation revealing the monument to have originally been a tab in socket. The socket could not be located and is presumed lost. The left corner/cap area is broken and missing. The stone evidences heavy biological growth and staining.

Treatment Report

1. Stone was excavated from the soil, set on 2x4s, and allowed to dry. 2. A hole was dug and a OPC socket was created below grade. This was allowed to cure for 72 hours. 3. Holes were drilled in the stone for the insertion of four ¼” diameter 316 threaded stainless steel rods, about

6-inches in length. Two were set joining the base and mid-section; two more were set joining the mid-section and top. Registration of the individual fragments was checked and the holes were holes cleaned using compressed air and acetone.

4. The rods were set with Sikadur 31, a hi-mod, moisture insensitive structural epoxy. The stone was clamped and allowed to set for 72 hours.

5. The stone was set into the socket using a 1:3 mix of NHL3.5 and sand. It was braced for 24 hours to allow the mortar to set.

6. Breaks were infilled using Jahn M-120 marble mortar. These were misted for 48 hours during the curing. The missing section in the upper left corner of the stone was also filled with Jahn M120, however, no attempt was made to recreate lettering. This infill was also misted during the curing process. No color matching was performed, but as the stone lightens, the Jahn will blend with the stone and become less noticeable.

7. The stone was washed with D/2 Biological Solution and flushed with potable water.


Before: During:

During: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 60, Catherine Simons + footstone Photographs: Before: x During: After: x

Condition Report

Marble headstone was in four pieces and covered with soil and vegetation. A number of other stone fragments were intermingled, probably being stacked in this location. The largest fragment of the headstone exhibits edge damage along the upper left. Among the fragments was the intact footstone. Heavy biological growth and staining overall. Footstone is out of the ground and also exhibits heavy biological growth and staining.

Treatment Report

Stone Treatment

1. Stone was excavated from the soil, placed on 2x4s, and allowed to dry. 2. Stone was drilled for the insertion of three 3/8” diameter 316 threaded stainless steel rods about 8-inches in

length. Registration was checked and holes cleaned using compressed air and acetone. 3. Rods were set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. The stone was clamped

and allowed to set for 24 hours. 4. The stone was reset in a bed of pea gravel to promoted drainage of water away from the stone and still

provide some flexibility should it be impacted by landscape maintenance activities. 5. Breaks were infilled using Jahn M120 marble mortar. 6. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Footstone Treatment

1. The footstone was reset in a bed of pea gravel to promote drainage away from the stone and still provide some flexibility should it be impacted by landscape maintenance activities.

2. The footstone was cleaned using D/2 Biological Solution and flushed with potable water. Recommendation: If a means of watering is available at the cemetery, we recommend reseeding around this stone in order to minimize splash-back, soiling, and erosion. Splash-back will dramatically increase soiling and the resulting soil erosion will “dish-out” the soil around the stone, creating a depression that collects rain water, increasing moisture up-take by the stone. Recorded By: N. Southerland/ M. Trinkley Treated By: NS/DH Date: 9/9/2010

Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 61.02, Nancy Pickens + footstone Photographs: Before: x During: After: x

Condition Report

Marble headstone is severely tilted in the ground. Evidences heavy biological growth and staining. In the process of resetting, the associated footstone was found. The footstone has suffered damage to the top basket arch area; it is also heavily soiled.

Treatment Report

Stone Treatment

1. The stone was excavated from the soil and reset in a bed of pea gravel to promote drainage and still provide some flexibility should it be impacted by landscape maintenance activities.

2. The stone was cleaned using D/2 Biological Solution and flushed with potable water. Footstone Treatment

1. The associated footstone was reset in a bed of pea gravel to promote drainage away from the stone. 2. The footstone was cleaned using D/2 Architectural Antimicrobial and flushed with potable water.


Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 61.03, Felix Torrence Photographs: Before: x During: After: x

Condition Report

Marble tab in socket memorial. The stone has fallen and is broken in three fragments, with the tab still firmly attached in the socket. The socket is not marble, but formed OPC. This may be original or represent an earlier repair. The base is no longer level. The broken portions, on the ground, are heavily soiled with heavy biologicals and staining. An “associated” footstone is engraved “L.W.” and does not belong at this grave. It evidences a ground break.

Treatment Report

1. The die fragments were removed from the ground, set on 2x4s, and allowed to dry. 2. The base was releveled in a bed of pea gravel to promote drainage of water away from the stone and still

provide some flexibility should it be impacted by landscape maintenance activities. 3. The stone was drilled for the insertion of two ½” diameter 316 threaded stainless steel rods about 8-inches

in length. Registration was checked and holes cleaned using compressed air and acetone. 4. The rods were set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. The stone was braced

and allowed to set for 48 hours. 5. Space around the tab and base was filled using a 1:2.5 mix of NHL3.5 and sand. 6. Breaks were infilled using Jahn M120 marble mortar. This was misted for 48 hours during the curing. 7. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Recommendations:

1. If a means of watering is available at the cemetery, we recommend reseeding around this stone in order to minimize splash-back, soiling, and erosion. Splash-back will dramatically increase soiling and the resulting soil erosion will “dish-out” the soil around the stone, creating a depression that collects rain water, increasing moisture up-take by the stone.

2. The footstone – and other “orphan” stones in the cemetery should be collected for safekeeping until their correct location for resetting can be determined. These stones should have the find location recorded.


Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 106.01, Clio Bulkley Photographs: Before: x During: After: x

Condition Report

Marble die on base. The base evidenced drill holes for pins. The die still contains two hollow brass pins set in lead. The base is no longer level. Stone and base evidence extensive biological growth. Several bricks were mixed with the stone.

Treatment Report

1. The base of the stone was releveled in a bed of pea gravel to promote drainage of water away from the

stone and still provide some flexibility should it be impacted by landscape maintenance activities. 2. The brass pins and lead were removed by hand. 3. The existing holes were drilled deeper for the insertion of two 3/8” diameter 316 threaded stainless steel

rods about 8-inches in length. Registration was checked and holes cleaned using compressed air and acetone.

4. The rods were set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. 5. The die was bedded on the base using a 1:2.5 of NHL3.5 and sand. 6. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Recorded By: N. Southerland Treated By: NS/DH Date: 9/10/2010

Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 106.02, James B. Carroll Photographs: Before: x During: After: x

Condition Report

Marble tab in socket is tilted in the ground. The base is a poor quality marble that is starting to exhibit wear or erosion along veins. Even in the temperate climate of SC these openings in the base can allow water penetration with resulting freeze-thaw damage during the winter. The tab has been set into the socket using a very hard mortar and is firmly attached. Some of this original mortar is missing, creating open pockets in the setting compound. The stone has biological growth.

Treatment Report

1. The stone was reset in a bed of pea gravel to promote drainage of water away from the stone and still

provide some flexibility should it be impacted by landscape maintenance activities. 2. Although the tab was not loose in the socket, a 1:2.5 mix of NHL3.5 and sand was added to fill in gaps to

prevent water intrusion into the socket. 3. The larger cracks in the base were infilled using Jahn M120 marble mortar. 4. Smaller cracks were filled using Jahn M30 micro injection grout. 5. The stone was cleaned with D/2 Biological Solution and flushed with potable water.

Recommendation: The stone should be monitored for additional stresses or cracks opening in the base yearly. If evidence is found of new cracks or losses, a conservator should further evaluate the base for infilling using either Jahn M120 or M30 as appropriate. Recorded By: N. Southerland/ M. Trinkley Treated By: NS/DH Date: 9/10/2010

Before: Before (close-up of veining in the socket showing losses; also opening at socket):

After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 106.03, Kattie Carroll Photographs: Before: x During: After: x

Condition Report

Marble die on base. The die has fallen off its two bases – a marble base and a granite sub base. The granite base was almost completely buried under ground. The stone had heavy biological growth and staining. A single hole is present in the die and marble base, but no pin is present.

Treatment Report

1. The granite sub base was excavated and reset/leveled on a bed of pea gravel to promote drainage of water

away from the stone and still provide some flexibility should it be impacted by landscape maintenance activities.

2. The existing hole was drilled deeper for the insertion of a single 5/8” diameter 316 threaded stainless steel rod about 12-inches in length. Registration was checked and the hole cleaned using compressed air and acetone. This rod connects the sub-base, base, and die, ensuring stability of the stone.

3. The rod was set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. 4. The upper base and die were bedded using a 1:2.5 mix of NHL3.5 and sand. 5. The stone was cleaned using D/2 Biological Solution and flushed with potable water.


Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 126.01, Louisa Reese Photographs: Before: x During: After: x

Condition Report

Marble tab has fallen from its granite socket, which is no longer level. Although intact, the tab is eroded. The socket is poorly carved and much larger in some areas than the fitting tab. The stone, which had been reset in front of the socket, was covered with climbing vegetation, heavy biological growth, and staining.

Treatment Report

1. The base was releveled in a bed of pea gravel to promote drainage of water away from the stone and still

provide some flexibility should it be impacted by landscape maintenance activities. 2. Because the tab no longer provided adequate support of the stone, holes were drilled in the die and socket

for the insertion of two ½” diameter 316 threaded stainless steel rods about 10-inches in length. Registration was checked and holes cleaned using compressed air and acetone.

3. The rods were set using Sikadur 31, a hi-mod moisture insensitive structural epoxy. The stone was oriented to match others in the immediate vicinity (it had been reversed when reset out of the socket).

4. The socket was filled with a 1:2.5 mix of NHL3.5 and sand. Because of the socket size, this does create a noticeable mortar joint in some areas.

5. The stone was cleaned using D/2 Biological Solution and flushed with potable water. Recorded By: N. Southerland/ M. Trinkley Treated By: NS/DH Date: 9/10/2010

Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 126.02, Alonzo Reese + footstone Photographs: Before: x During: After: x

Condition Report

Marble tab was severely leaning in the socket and was loose. The base was not level. The associated footstone was found during conservation work. The stone had heavy biological growth and staining.

Treatment Report

Stone Treatment:

1. The die was removed from the socket and set aside. The socket was cleaned of remnant mortar using hand tools and was blown out using compressed air.

2. The base was releveled in a bed of pea gravel to promote drainage of water away from the stone and still provide some flexibility should it be impacted by landscape maintenance activities.

3. The tab was replaced into the socket, bedded in a 1:2.5 mix of NHL3.5 and sand to prevent water intrusion. 4. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Footstone Treatment:

1. The associated footstone was reset in a bed of pea gravel to promote drainage of water away from the stone and still provide some flexibility should it be impacted by landscape maintenance activities.

2. The footstone was cleaned using D/2 Biological Solution and flushed with potable water. Recommendation:


2. Special care is required to prevent climbing vegetation from emerging between the adjacent brick coping and the socket.


Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 129, John T. Lee + footstone Photographs: Before: x During: After: x

Condition Report

Broken marble headstone is partially reset/partially leaning against a socket with a remnant die still in place. The headstone, however, is not the same width as the tab remaining in the socket. Although the bottom portion of the headstone is missing, it is unlikely that this headstone fits to the socket. A footstone that matches the initials of the die was found piled on an adjacent stone. The stone has heavy biological growth and staining.

Treatment Report

1. Since no other stone was found in the vicinity that matched the socket, the socket was removed and a new

socket was made below grade out of OPC to better fit the broken portion of the headstone. 2. The headstone was set in the socket with a 1:2.5 mix of NHL3.5 and sand. 3. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Recommendations:


2. The socket – and other “orphan” stones in the cemetery – should be collected for safekeeping until their correct location for resetting can be determined. These stones should have the find location recorded.


Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 130 Photographs: Before: x During: After: x

Condition Report

When initially encountered, this appeared to be a pile of marble pieces. When separated, the pile became an unlevel marble base that was broken into four pieces, part of a tabbed headstone with the top portion missing, two footstones that went with other headstones (one being #129, the second not identified), and a piece of marble that had no writing and did not fit to any of the monuments in the area. The stones are heavily stained and have biological growth.

Treatment Report

1. The base was leveled in a bed of pea gravel to promote drainage away from the stone and still provide

some flexibility should it be impacted by landscape maintenance activities. 2. The broken pieces of the base were secured using Sikadur 31, a hi-mod, moisture insensitive structural

epoxy. The stone was clamped and allowed to set for 72 hours. 3. The structural stability of the socket was compromised by the damaged, so both the die and socket were

drilled for the insertion of a single 3/8” diameter 316 threaded stainless steel rod about 8-inches in length. Registration was checked and holes cleaned using compressed air and acetone. This will assist in providing stability and reduce the load bearing requirement of the socket.

4. The rod was set using Sikadur 31. The stone was braced and allowed to set for 48 hours. 5. The stone was set into the socket using a 1:2.5 mix of NHL3.5 and sand. 6. Breaks were infilled using Jahn M120 marble mortar. This was misted for 48 hours during the curing. 7. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Recommendation: If a means of watering is available at the cemetery, we recommend reseeding around this stone in order to minimize splash-back, soiling, and erosion. Splash-back will dramatically increase soiling and the resulting soil erosion will “dish-out” the soil around the stone, creating a depression that collects rain water, increasing moisture up-take by the stone. Recorded By: N. Southerland/ M. Trinkley Treated By: NS/DH Date: 9/10/2010

Before: After: 0



Location: Randolph Cemetery State: SC ID.: Stone No.: 414, S.B. Stratford Photographs: Before: x During: After: x

Condition Report

Marble tab in socket stone; tab is broken with a portion of the stone missing, making the bottom of the stone unable to securely register to the top. The marble base was almost completely buried. Stone has biological growth and staining.

Treatment Report


provide some flexibility should it be impacted by landscape maintenance activities. 2. Holes were drilled for the insertion of two 3/8” diameter 316 threaded stainless steel rods about 6-inches in

length. Registration was checked and holes cleaned using compressed air and acetone. 3. The rods were set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. The stone was braced

for 48 hours. 4. The missing portions of the stone were infilled using Jahn M120 marble mortar. 5. The stone was cleaned using D/2 Biological Solution and flushed with potable water.


Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 415, John Pope Photographs: Before: x During: After: x

Condition Report

Marble tab in socket. The tab has broken and the die is lying face-up on the ground. The tab is still firmly held in the socket; the base is no longer level. Stone has heavy biological growth and staining.

Treatment Report


provide some flexibility should it be impacted by landscape maintenance activities. 1. The stone was drilled for the insertion of two 3/8” diameter 316 threaded stainless steel rods about 8-

inches in length. Registration was checked and holes cleaned using compressed air and acetone. 2. The rods were set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. The stone was braced

and allowed to set for 48 hours. 3. The breaks was infilled with Jahn M120 marble mortar. 4. Gaps between the tab and socket were filled with a 1:2.5 mix of NHL3.5 and sand. 5. The stone was cleaned using D/2 Biological Solution and flushed with potable water.


Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 442, Mary E. Rose Photographs: Before: x During: After: x

Condition Report

Marble tab in socket. The die is broken into three pieces with the bottom piece secure in the marble socket. The base is not level and the stone has heavy biological growth. There is minor recent damage to the upper left corner of the die, possibly representing mower impact.

Treatment Report

1. The base was leveled in a bed of pea gravel to promote drainage of water away from the stone and still

provide some flexibility should it be impacted by landscape maintenance activities. 2. Holes were drilled for the insertion of four 3/8” diameter 316 threaded stainless steel rods from 6 to 8-

inches in length. Registration was checked and holes cleaned using compressed air and acetone. 3. Rods were set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. The stone was braced

and allowed to set for 48 hours. 4. Breaks and gaps were infilled using Jahn M120 marble mortar. 5. Gaps between the tab and socket were filled using a 1:2.5 mix of NHL3.5 and sand. 6. The stone was cleaned using D/2 Biological Solution and flushed with potable water.


Before: After:



Location: Randolph Cemetery State: SC ID.: Stone No.: 1062.04, Louisa Barley +footstone Photographs: Before: x During: After: x

Condition Report

Marble tab in socket. The die has broken with the bottom portion still securely in the socket. The base is not level and the stone has heavy biological growth and staining. A footstone was discovered during the conservation treatment. Although worn, the footstone is intact.

Treatment Report

Stone

1. The base was leveled in a bed of pea gravel to promote drainage of water away from the stone and still provide some flexibility should it be impacted by landscape maintenance activities.

2. Holes were drilled for the insertion of two ½” diameter 316 threaded stainless steel rods about 8-inches in length. Registration was checked and holes cleaned using compressed air and acetone.

3. The rods were set using Sikadur 31, a hi-mod, moisture insensitive structural epoxy. The stone was braced and allowed to set for 48 hours.

4. Breaks were infilled using Jahn M120 marble mortar. 5. The gaps between the tab and socket were filled with a 1:2.5 mix of NHL3.5 and sand. 6. The stone was cleaned using D/2 Biological Solution and flushed with potable water.

Footstone

1. The footstone was set in a bed of pea gravel to promote drainage and still provide some flexibility should it be impacted by landscape maintenance activities.

2. The footstone was cleaned using D/2 Biological Solution and flushed with potable water. Recorded By: N. Southerland/ M. Trinkley Treated By: NS/DH Date: 9/10/2010

Before: After:

APPENDIX PRODUCT MATERIAL SAFETY DATA SHEETS

& TECHNICAL DATA SHEETS

COMPANY IDENTITY: PACKAGING SERVICE CO., INC. DATE: 11/06/08 PRODUCT IDENTITY: CROWN ACETONE PAGE 1 OF 5 NEW MSDS DATE: 11/06/2008

MATERIAL SAFETY DATA SHEET This Material Safety Data Sheet conforms to the requirements of ANSI Z400.1, using the International Chemical Safety Cards of the Global Harmonizing System. THIS MSDS COMPLIES WITH 29 CFR 1910.1200 (HAZARD COMMUNICATION STANDARD). IMPORTANT: Read this MSDS before handling & disposing of this product. Pass this information on to employees, customers, & users of this product.

SECTION 1: IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND COMPANY PRODUCT IDENTITY: CROWN ACETONE COMPANY IDENTITY: PACKAGING SERVICE CO., INC. COMPANY ADDRESS: 1904 MYKAWA ROAD COMPANY CITY: PEARLAND, TX 77581 COMPANY PHONE: 1-281-485-1458 CHEMTREC PHONE: 1-800-424-9300

SECTION 2. COMPOSITION/INFORMATION ON INGREDIENTS

CONTAINS:

99-100% ACETONE (67-64-1) [200-662-2] Number in parentheses is CAS #, number in brackets is European EC #. ACET01 SECTION 3. HAZARDS IDENTIFICATION RISK STATEMENTS: R36/37/38 Irritating to eyes, respiratory system and skin. R12 Extremely Flammable. R66 Repeated exposure may cause skin dryness or cracking. R67 Vapors may cause drowsiness and dizziness. SAFETY STATEMENTS: S9 Keep container in a well-ventilated place. S16 Keep away from sources of ignition. No smoking.

SECTION 4. FIRST AID MEASURES

EYE CONTACT: For eyes, flush with plenty of water for 15 minutes & get medical attention. SKIN CONTACT: In case of contact with skin immediately remove contaminated clothing. Wash thoroughly with soap & water. Wash contaminated clothing before reuse. INHALATION: After high vapor exposure, remove to fresh air. If breathing is difficult, give oxygen. If breathing has stopped, trained personnel should immediately begin artificial respiration. If the heart has stopped, trained personnel should immediately begin cardiopulmonary resuscitation (CPR). SWALLOWING: Rinse mouth. GET MEDICAL ATTENTION IMMEDIATELY. Do NOT give liquids to an unconscious or convulsing person.

SECTION 5. FIRE FIGHTING MEASURES FIRE & EXPLOSION PREVENTIVE MEASURES: NO open flames, NO sparks, & NO smoking. Use a closed system, ventilation, explosion-proof electrical equipment, and lighting. Do NOT use compressed air for filling, discharging, or handling. EXTINGUISHING MEDIA: Use dry powder, carbon dioxide.


SPECIAL FIRE FIGHTING PROCEDURES: Water spray may be ineffective on fire but can protect fire-fighters & cool closed containers. Use fog nozzles if water is used. Do not enter confined fire-space without full bunker gear. (Helmet with face shield, bunker coats, gloves & rubber boots). Use NIOSH approved positive-pressure self-contained breathing apparatus. UNUSUAL EXPLOSION AND FIRE PROCEDURES: EXTREMELY FLAMMABLE!! VAPORS CAN CAUSE FLASH FIRE Keep container tightly closed. Isolate from oxidizers, heat, sparks, electric equipment & open flame. Closed containers may explode if exposed to extreme heat. Applying to hot surfaces requires special precautions. Empty container very hazardous! Continue all label precautions!

SECTION 6. ACCIDENTAL RELEASE MEASURES PERSONAL PROTECTIVE MEASURES: Vapors may ignite explosively & spread long distances. Prevent vapor buildup. Keep unprotected personnel away. Ventilate spill area. Remove all ignition sources. Use self-contained breathing apparatus. CONTAINMENT AND CLEAN-UP MEASURES: Stop spill at source. Dike and contain. Collect leaking liquid in sealable containers. Absorb remaining liquid in sand or inert absorbent. Remove to safe place. Do NOT wash away into sewer.

SECTION 7. HANDLING AND STORAGE HANDLING: Isolate from oxidizers, heat, sparks, electric equipment & open flame. Use only with adequate ventilation. Avoid breathing of vapor or spray mist. Avoid contact with skin & eyes. Wear OSHA Standard goggles or face shield. Consult Safety Equipment Supplier. Wear gloves, apron & footwear impervious to this material. Wash clothing before reuse. Avoid free fall of liquid. Ground containers when transferring. Do not flame cut, saw, drill, braze, or weld. Empty container very hazardous! Continue all label precautions! STORAGE: Vapors may ignite explosively & spread long distances. Prevent vapor buildup. Put out pilot lights & turn off heaters, electric equipment & other ignition sources during use & until all vapors are gone. Keep away from strong oxidants. Do not store above 49 C/120 F. Keep container tightly closed & upright when not in use to prevent leakage. ACET01 SECTION 8. EXPOSURE CONTROLS/PERSONAL PROTECTION: RESPIRATORY EXPOSURE CONTROLS: A respiratory protection program that meets OSHA 29 CFR 1910.134 and ANSI Z86.2 requirements or European Standard EN 149 must be followed whenever workplace conditions warrant a respirator's use. VENTILATION: LOCAL EXHAUST: Necessary MECHANICAL (GENERAL): Acceptable SPECIAL: None OTHER: None Please refer to ACGIH document, "Industrial Ventilation, A Manual of Recommended Practices", most recent edition, for details. PERSONAL PROTECTIONS: Wear OSHA Standard goggles or face shield. Consult Safety Equipment Supplier. Wear gloves, apron & footwear impervious to this material. Wash clothing before reuse. WORK & HYGIENIC PRACTICES: Provide readily accessible eye wash stations & safety showers. Wash at end of each work shift & before eating, smoking or using the toilet. Promptly remove clothing that becomes contaminated. Destroy contaminated leather articles. Launder or discard contaminated clothing.


SECTION 9. PHYSICAL DATA

APPEARANCE: Liquid, Water-White ODOR: Ketone BOILING RANGE: 56 56 57 C / 133 134 135 F AUTO IGNITION TEMPERATURE: 537 C / 1000 F (Lowest Component) LOWER FLAMMABLE LIMIT IN AIR (% by vol): 2.6 FLASH POINT (TEST METHOD): -16 C / 2 F (TCC) FLAMMABILITY CLASSIFICATION: Class I B GRAVITY @ 68/68 F / 20/20 C : API: 47.2 SPECIFIC GRAVITY (Water=1): 0.792 POUNDS/GALLON: 6.597 VOC'S (>0.44 Lbs/Sq In): 100.0 Vol. % / 792.0 g/L / 6.597 Lbs/Gal TOTAL VOC'S (TVOC): 100.0 Vol. % / 792.0 g/L / 6.597 Lbs/Gal NONEXEMPT VOC'S (CVOC): 0.0 Vol. % / 0.0 g/L / 0.000 Lbs/Gal HAZARDOUS AIR POLLUTANTS (HAPS): 0.0 Wt. % / 0.0 g/L / 0.000 Lbs/Gal VAPOR PRESSURE (mm of Hg)@20 C 186.0 NONEXEMPT VOC PARTIAL PRESSURE (mm of Hg @ 20 C) 0.0 VAPOR DENSITY (air=1): 2.0 WATER ABSORPTION: Complete REFRACTIVE INDEX: 1.358

SECTION 10. STABILITY & REACTIVITY STABILITY: Stable under normal conditions. CONDITIONS TO AVOID: Isolate from oxidizers, heat, sparks, electric equipment & open flame. MATERIALS TO AVOID: Reacts with strong oxidants, causing fire & explosion hazard. HAZARDOUS DECOMPOSITION PRODUCTS: Carbon Monoxide, Carbon Dioxide from burning. HAZARDOUS POLYMERIZATION: Will not occur. ACET01 SECTION 11. TOXICOLOGICAL INFORMATION MATERIAL CAS # TWA (OSHA) TLV (ACGIH) HAP Acetone 67-64-1 1000 ppm 500 ppm A4 No This product contains no EPA Hazardous Air Pollutants (HAP) in amounts > 0.1%. MATERIAL CAS # CEILING STEL(OSHA/ACGIH)

Acetone 67-64-1 None Known 750 ppm ACUTE HAZARDS EYE & SKIN CONTACT: Primary irritation to skin, defatting, dermatitis. Primary irritation to eyes, redness, tearing, blurred vision. Liquid can cause eye irritation. Wash thoroughly after handling. INHALATION: Anesthetic. Irritates respiratory tract. Acute overexposure can cause serious nervous system depression. Vapor harmful.


SWALLOWING: Swallowing can cause abdominal irritation, nausea, vomiting & diarrhea. SUBCHRONIC HAZARDS/CONDITIONS AGGRAVATED: CONDITIONS AGGRAVATED: Persons with severe skin, liver or kidney problems should avoid use. CHRONIC HAZARDS CANCER, REPRODUCTIVE & OTHER CHRONIC HAZARDS: This product has no carcinogens listed by IARC, NTP, NIOSH, OSHA or ACGIH, as of this date, greater or equal to 0.1%.

SECTION 12. ECOLOGICAL INFORMATION MAMMALIAN INFORMATION: MATERIAL CAS # LOWEST KNOWN LETHAL DOSE DATA

LOWEST KNOWN LD50 (ORAL) Acetone 67-64-1 5340.0 mg/kg(Rabbits)

LOWEST KNOWN LC50 (VAPORS) Acetone 67-64-1 21000 ppm (Cats)

LOWEST KNOWN LD50 (SKIN) Acetone 67-64-1 20000.0 mg/kg (Rabbits) AQUATIC ANIMAL INFORMATION: The most sensitive known aquatic group to any component of this product is: Mosquito Fish 13000 ppm or mg/L (48 hour exposure). MOBILITY: This material is a mobile liquid. DEGRADABILITY: This product is completely biodegradable. ACCUMULATION: This product does not accumulate or biomagnify in the environment.

SECTION 13. DISPOSAL CONSIDERATIONS Processing, use or contamination may change the waste management options. Recycle / dispose of observing national, regional, state, provincial and local health, safety & pollution laws. If in doubt, contact appropriate agencies.

SECTION 14. TRANSPORT INFORMATION IF CONTAINER HAS > PRODUCT RQ (SEE SECTION 15) PUT "RQ," BEFORE SHIPPING NAME. DOT SHIPPING NAME: UN1090, Acetone, 3, PG-II DRUM LABEL: (FLAMMABLE LIQUID) IATA / ICAO: UN1090, Acetone, 3, PG-II IMO / IMDG: UN1090, Acetone, 3, PG-II EMERGENCY RESPONSE GUIDEBOOK NUMBER: 127 ACET01 SECTION 15. REGULATORY INFORMATION EPA REGULATION: SARA SECTION 311/312 HAZARDS: Acute Health, Fire All components of this product are on the TSCA list. This material contains no known products restricted under SARA Title III, Section 313 in amounts greater or equal to 1%. SARA TITLE III INGREDIENTS CAS# WT. % (REG. SECTION) RQ(LBS) Acetone 67-64-1 100 (311,312) 5000 > 5000 LB / 2272 KG OF THIS PRODUCT IN 1 CONTAINER EXCEEDS THE "RQ" OF ACETONE. Any release equal to or exceeding the RQ must be reported to the National Response Center (800-424-8802) and appropriate state and local regulatory agencies as described in 40 CFR 302.6 and 40 CFR 355.40 respectively. Failure to report may result in substantial civil and criminal penalties. State & local regulations may be more restrictive than federal regulations.


STATE REGULATIONS: THIS PRODUCT MEETS REQUIREMENTS OF SOUTHERN CALIFORNIA AQMD RULE 443.1 & SIMILAR REGULATIONS CALIFORNIA PROPOSITION 65: This product contains no chemicals known to the State of California to cause cancer & reproductive toxicity. INTERNATIONAL REGULATIONS: The components of this product are listed on the chemical inventories of the following countries: Australia, Canada, China, Europe (EINECS), Japan, Korea, United Kingdom. ACET01 SECTION 16. OTHER INFORMATION

HAZARD RATINGS: HEALTH (NFPA): 1, HEALTH (HMIS): 2, FLAMMABILITY: 3, REACTIVITY: 0 (Personal Protection Rating to be supplied by user based on use conditions.) This information is intended solely for the use of individuals trained in the NFPA & HMIS hazard rating systems. EMPLOYEE TRAINING: See Section 3 for Risk & Safety Statements. Employees should be made aware of all hazards of this material (as stated in this MSDS) before handling it. NOTICE: The supplier disclaims all expressed or implied warranties of merchantability or fitness for a specific use, with respect to the product or the information provided herein, except for conformation to contracted specifications. All information appearing herein is based upon data obtained from manufacturers and/or recognized technical sources. While the information is believed to be accurate, we make no representations as to its accuracy or sufficiency. Conditions of use are beyond our control, and therefore users are responsible for verifying the data under their own operating conditions to determine whether the product is suitable for their particular purposes and they assume all risks of their use, handling, and disposal of the product. Users also assume all risks in regards to the publication or use of, or reliance upon, information contained herein. This information relates only to the product designated herein, and does not relate to its use in combination with any other material or process. Unless updated, this Material Safety Data Sheet is valid until 11/06/2011.

Cathedral Stone®

Products, Inc. 7266 Park Circle Drive, Hanover Maryland 21076 (800) 684-0901 FAX: (410) 782-9155 WEBSITE: www.cathedralstone.com

D/2 Biological Solution is a safe, easy to use liquid that removes a broad spectrum of biological deposits from hard environmental surfaces. A contact time of only 1 to 2 minutes will loosen most fungal and algal deposits with manual scrubbing and is typically sufficient for excellent results.

Growth of bacteria, fungi, algae, lichens, and mosses contributes significantly to the degradation of many types of construction materials, and can be disfiguring. D/2 can be utilized to control this problem on outdoor sculpture, monuments, decorative fountains, gravestones, and tombs. Biological growth found on some individual building features (such as parapets and zones of ground contact) or materials (such as stucco) can also be treated with D/2, although it is not a general purpose architectural cleaner.

Features and Benefits • Fast Acting: 1 to 2 minute contact time for

great results.

• Keeps Surfaces Clean for a Minimum of 1 year

• Safe for Landscape Plantings and

Grass

• No Detrimental Effects on Masonry

• Non-Toxic and Biodegradable: No special precautions required for handling and storage.

Application Procedures No Scrub/No Rinse Method 1. Apply D/2 Biological Solution with a brush or pump sprayer to a dry surface. Do not pre-wet the surface. 2. Allow to dry. Repeat if there are heavy biological deposits. D/2 works with the elements and results occur within one week to one month depending on severity of growth and weather conditions. The surface will become cleaner over time as the subsurface biological growth dies and releases.

Immediate Result Method 1. Apply D/2 Biological Solution with a brush, roller or pump sprayer to a dry surface. Do not pre-wet the surface. 2. After waiting 2-5 minutes, scrub surface with a non-metallic, short bristle scrub brush. 3. Allow the undiluted D/2 to remain on the surface 5-10 minutes longer. 4. Apply additional D/2 to maintain a wet surface and continue scrubbing. 5. Rinse with clean water.

Heavy biological deposits should first be loosened using a low pressure washer (300 to 600 psi), or by mechanical scraping using wood or plastic tools. Follow removal with one or more applications of D/2 as stated above. The surface will become cleaner over time as the subsurface biological growth dies and releases. Light biological deposits may be removed with a D/2 dilution of water from 1:1 to 1:4 parts water by volume. Perform tests to determine effectiveness of various dilutions. Follow testing with application of D/2 as stated above.

Safety Information D/2 Biological Solution is non-mutagenic, and contains no carcinogenic compounds as defined by NTP, IARC, or OSHA. It is considered essentially non-toxic by swallowing, as it has an oral LD50 of greater than 5.0 g/kg of body weight. No special ventilation is required during use.

.

Packaging and Coverage D/2 Biological Solution is available in 32 ounce spray bottle, 1 gallon and 5 gallon containers, and 55 gallon drums.

The area that can be treated with one gallon of D/2 will vary considerably as a function of the nature and extent of biological deposits, as well as the physical characteristics of the surface.

Typical coverage to remove medium deposits will vary from 250 to 350 square feet per gallon.

D/2 Biological Solution

D/2 Biological Solution Page 2

Cathedral Stone®


Technical Data Physical Form . . . . . . . . . . . . . . . . Transparent,

low viscosity liquid Color . . . . . . . . . . . . . . . . . . . . Almost colorless pH . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9.5 Specific Gravity . . . . . . . . . . . . . . . . . 1.01g/cc Solubility in Water . . . . . . . . . . . . . . Complete Vapor Pressure . . . . . . . . . . 25 mm Hg @ 20°C Notice: The information contained herein is based on our own research and the research of others, and it is provided solely as a service to help users. It is believed to be accurate to the best of our knowledge. However, no guarantee of its accuracy can be made, and it is not intended to serve as the basis for determining this product's suitability in any particular situation. For this reason, purchasers are responsible to make their own tests and assume all risks associated with using this product. 11/2008

0

0

1

0

Material Safety Data Sheet: D/2 BIOLOGICAL SOLUTION

Version No. 24005 Date of Issue: March 2008 ANSI-Z400.1-2003 Format

Section 1: PRODUCT & COMPANY IDENTIFICATION

Product Name: D/2 Biological Solution

Exclusively Distributed By: Manufactured By:

Cathedral Stone®

Products, Inc.

7266 Park Circle Drive

Hanover, MD 21076

Sunshine Makers, Inc.

15922 Pacific Coast Highway

Huntington Harbour, CA 92649

Telephone: 410-782-9150 Telephone: 800-228-0709

Fax: 410-782-9155 Fax: 562-592-3830

Emergency Phone: Chem-Tel 24-Hour Emergency Service: 800-225-3924

Use of Product D/2 Biological Solution is an easy-to-use liquid that aids in the removal of a broad spectrum of soils.

It is designed for use on outdoor sculpture, monuments, decorative fountains, stone, brick, terra cotta,

concrete, stucco, and other architectural surfaces.

Section 2: HAZARDS IDENTIFICATION

D/2 Biological Solution is a colorless liquid with a very faint detergent-like odor. It is non-flammable, non-

combustible, non-explosive, and non-reactive.

Hazard Rating (NFPA/HMIS) Rating Scale

Health = 1* Reactivity = 0 0 = Minimal 1 = Slight 2 = Moderate

Fire = 0 Special = 0 3 = Serious 4 = Severe

* Mild eye irritant, non-mutagenic and non-carcinogenic

Eye Contact: Eye Irritant.

Skin Contact: Prolonged skin contact with D/2 Biological Solution may irritate the skin. Repeated daily application to the skin

without rinsing, or continuous contact of D/2 Biological Solution on the skin may lead to irritation.

Ingestion: Essentially non-toxic. May cause stomach or intestinal upset if swallowed.

Inhalation: No adverse effects expected under typical use conditions. Adequate ventilation should be present when using D/2

Biological Solution over a prolonged period of time. Open windows or ventilate via fan or other air-moving

equipment if necessary. Mucous membranes may become irritated by concentrate mist.

Carcinogens: No ingredients are listed by OSHA, IARC, or NTP as known or suspected carcinogens.

Medical Conditions: No medical conditions are known to be aggravated by exposure to D/2 Biological Solution.

Section 3: COMPOSITION/INFORMATION ON INGREDIENTS

Ingredients CAS Number OSHA PEL ACGIH TLV

Surfactants Proprietary None established

Wetting Agents Proprietary None established

Buffers Proprietary None established

Section 4: FIRST AID MEASURES

If in Eyes: Immediately rinse the eye with large quantities of cool water; if present, contact lenses should be removed after 5

minutes of rinsing; continue rinsing 10-15 minutes more. Both upper and lower lids should be lifted to facilitate

thorough rinsing.

If on Skin: Minimal effects, if any, from diluted product; rinse skin with water, rinse shoes and launder clothing before reuse. -

Reversible reddening may occur in some dermal-sensitive users; thoroughly rinse area.

If Inhaled: Use in well-ventilated area, or use adequate protection from inhaling mist during spray applications. Prolonged

exposure of workers to concentrate-mist during spray application may cause mild irritation of nasal passages or throat.

If this happens, relocate workers to fresh air.

If Ingested: Give several glasses of milk or water to dilute; do not induce vomiting. If stomach upset occurs, consult physician.

Pg 1 of 3




Section 5: FIRE FIGHTING MEASURES

Extinguishing Media: Not flammable/non-explosive. No special procedures required.

Special Fire Fighting Procedures: None required.

Section 6: ACCIDENTAL RELEASE MEASURES

Personal Precautions: Avoid contact with eyes. Do not rub eyes with hands during cleanup. No special precautions for dermal

contact are needed. Wash hands thoroughly after cleaning up spill or leak.

Procedure to follow in case of spill or leak: Evacuate area. Identify source of leak or spill and contain with sand, earth, or

containment bin. Then proceed to clean up spill or leak.

Method for cleaning up: Recover all usable material. Residual may be removed by wipe or wet mope. Rinse area with plenty of

water and mop to sanitary sewer.

Section 7: HANDLING AND STORAGE

No special handling is required. Keep in a closed plastic container. Store at ambient temperature. Avoid contact with eyes.

Wash hands thoroughly after handling. This product is non-hazardous for storage and transport according to the U.S.

Department of Transportation Regulations.

This material does not meet the definition of a hazardous material according to 49 CFR, ICAO, IMDG and the UN Orange

Book.

Section 8: EXPOSURE CONTROLS/PERSONAL PROTECTION

Precautionary measures: No special requirements under normal use conditions.

Exposure Limits: The D/2 Biological Solution formulation presents no health hazards to the user, other than mild eye

irritancy.

Eye protection: Caution, including reasonable eye protection, should always be used to avoid eye contact where

splashing may occur, such as during spray applications.

Respiratory Protection: No special precautions required.

Ventilation: No special ventilation is required during normal use.

Skin protection: No special precautions required; rinse completely from skin after contact.

General hygiene conditions: There are no known hazards associated with this material when used as recommended. The

following general hygiene considerations are recognized as common good industrial hygiene

practices:

- Avoid breathing vapor or mist.

- Avoid contact with eyes.

- Wash thoroughly after handling and before eating, drinking, or smoking.

Section 9: PHYSICAL AND CHEMICAL PROPERTIES

Appearance: Clear Liquid Freezing Point: -9oC (16

oF)

Odor: Very faint detergent-like odor Boiling Point: 98oC (209

oF)

pH: 9.5 Specific Gravity: 1.011

Evaporation Rate: 0.4 (butyl acetate = 1) Vapor Pressure: 20.7 mm Hg

Water Solubility: 100% Vapor Density: 1.3 (air = 1)

Section 10: STABILITY AND REACTIVITY

Stability: Stable.

Materials to Avoid: Contains ammoniated compounds – do not mix with bleach, tub & tile cleaner,

mold/mildew removers, or chlorinated compounds.

Hazardous Decomposition Products: None expected

Pg 2 of 3




Section 11: TOXICOLOGICAL INFORMATION

Toxicity Data: Available from relevant laboratory testing of ingredients or similar mixtures.

Acute Toxicity: Oral LD50: >2.0 g/kg body weight Dermal LD50: Not estimated

Eye Irritation: With or without rinsing with water, the irritation scores in rabbits at 24 hours did not exceed 17 (mild

irritant) on a scale of 110 (extremely irritating); all scores were normal at seven days.

Dermal Irritation: In a standard test on rabbits, mild irritation was found at 72 hours; well-defined reddening was observed at

7 and 14 days after exposure.

Dermal Sensitization: No allergic reactions occurred in guinea pigs treated with D/2 Biological Solution.

Carcinogenicity: D/2 Biological Solution contains no carcinogenic compounds as defined by the National Toxicology

Program (NTP), the international Agency for Research on Carcinogens (IARC), or the Occupational

Health and Safety Administration (OSHA).

Section 12: ECOLOGICAL INFORMATION

Biodegradability: All components are inherently biodegradable.

Ecotoxicity: Not Tested.

Section 13: DISPOSAL CONSIDERATIONS

Unused Product: * Dilute with water 1:10 (1 part D/2 Biological Solution to 10 parts water) and dispose by sanitary sewer.

Used Product: *Used product may be hazardous depending on the cleaning application and resulting contaminants.

Empty Containers: *Triple-rinse with water and offer for recycling if available. Otherwise, dispose as non-hazardous waste.

*Dispose of used or unused product, and empty containers in accordance with the local, State, Provincial, and Federal regulations for

your location. Never dispose of used degreasing rinsates into lakes, streams, and open bodies of water or storm drains.

Section 14: TRANSPORT INFORMATION

IATA Proper Shipping Name: Detergent solution Hazard Class: Non hazardous

Section 15: REGULATORY INFORMATION

*Reportable components: None. The U.S. Environmental Protection Agency (EPA) has determined that propylene glycol

ethers are not included within the listed category "glycol ethers" under either EPCRA §313 Toxic Release Inventory or

Clean Air Act §112 Hazardous Air Pollutants (both lists include only ethylene glycol ethers). Nor are propylene glycol

ethers included in the various EPA Resource Conservation and Recovery Act, and Clean Water Act lists, nor the California

Proposition 65 lists.

All components are listed on: EINECS and TSCA Inventory

No components listed under: Clean Air Act Section 112

RCRA Status: Not a hazardous waste. CERCLA Status: No components listed

TSCA TRI Reporting: Not required / Not listed CA PROP. 65 Status: No components listed

Section 16: OTHER INFORMATION

For Safety Information, Sales Applications and Availability contact:

CATHEDRAL STONE®

PRODUCTS, INC.

7266 Park Circle Drive, Hanover, MD 21076

Telephone: 410-782-9150 Fax: 410-782-9155

DISCLAIMER: All information appearing herein is based upon data obtained by the manufacturer and recognized technical sources.

Judgments as to the suitability of information herein for purchaser’s purposes are necessarily purchaser’s responsibility. Therefore,

although reasonable care has been taken in the preparation of this information, Sunshine Makers, Inc. or its distributors extends no

warranties, makes no representations and assumes no responsibility as to the suitability of such information for application to

purchaser’s intended purposes or for consequences of its use.

Pg 3 of 3


Cathedral Stone® Products, Inc. 7266 Park Circle Drive, Hanover, Maryland 21076

(800) 684-0901 FAX: (410) 782-9155 WEB: www.cathedralstone.com

JAHN M30 Micro Injection Grout • Concrete and hard stone - #31 • Brick and soft stone - #32

Jahn M30 contains no corrosive constituents, and achieves extraordinary flow capacity, penetration and strong adhesion. The M30 injection grout is offered in two formulations for varying substrates. To enhance penetration and bonding, a small amount of synthetic material is included. M30 can be applied via gravity feed or pressure injection into hairline cracks up to 3/16” (5.0 mm) in width. This product may be utilized in both non-structural simple void applications and structural load bearing situations, is available in two levels of compressive strength and can be customized through testing.

Features And Benefits • Single-Component: Easy to mix correctly,

thereby improving quality control at the point of injection.

• Tenacious Adhesion: Strong bonding capabilities.

• Factory Controlled: No field chemistry resulting in product variation.

• Low Viscosity: Deep, thorough penetration.

• Simple Application: Can be applied by pouring or by pumping.

• Water Based: Environmentally and user safe. No solvent clean up or disposal problems.

Application Procedures Preparation Wash the surface and interior of the crack using clean water to remove all dust, loose or deleterious material, which could prevent proper flow and/or adhesion.

Mixing The mixing ratio is approximately 1 part powder to 1 part water by volume. Mixing must be done with a high speed drill (3,000 RPM or higher) equipped with a Jiffler-type mixing paddle. After mixing, the grout should be poured into another clean container using a sieve. Additional or repeated agitation is necessary if the grout is allowed to sit prior to use.

Injection Procedures

Immediately before injection, moisten interior of the crack by flushing with water. If the crack is allowed to dry out before the grout is injected, this step must be repeated. This is very important.

Transverse Cracks

Drill a series of injection ports in the center of the crack. These ports should be drilled in a downward direction. Seal the crack with removable, non-staining clay, sealant, or caulk.

Inject grout into the lowest port and continue until it flows freely from this port and other ports at the same level. Seal ports using non-staining clay, sealant, or caulk and proceed in identical fashion until the crack is filled. Clean up overflow and runs immediately with clean water.

Lateral Cracks (Delaminating Layers)

Drill a series of injection ports in a square configuration (90° angles) on the face of the substrate to create a “drill frame”. Ports should be drilled in a downward direction. Wash the surface and interior of the crack using clean water to remove dust and loose. Any dust or debris remaining between the layers will impede the flow of the grout. If this is the case, more holes will be required to attempt to fill all hollow areas.

Inject grout into lower left port and proceed until it flows freely from this port and other ports at the same level. Seal ports using non-staining clay, sealant, or caulk. Inject grout into lower right port and proceed in identical fashion. The order of

Jahn M30 Page 2

Cathedral Stone® Products, Inc. 7266 Park Circle Drive, Hanover, Maryland 21076

(800) 684-0901 FAX: (410) 782-9155 WEB: www.cathedralstone.com

injection is lower left, lower right, upper left, and then upper right. Clean up overflow and runs immediately with clean water.

Removal of Sealant Let the grout dry (approximately 24 hours) and remove all sealant, caulk, or clay. After removing the sealant, repair the crack surface and injection holes with Jahn Mortar that matches the color and type of existing masonry.

Clean Up While injecting, continually check for grout runs and spills on the surface of the masonry, and clean the surface before the grout has time to set. This is normally done with a clean sponge and water, and may have to be repeated several times, rinsing the sponge with clean water. Remove uncured grout from tools and equipment with water as soon as possible. Cured grout many only be removed chemically or mechanically.

Safety Requirements It is recommended that safety goggles, gloves, and a dust mask equipped with P-2 filters (or equivalent) be worn for protection while mixing the grout. Limitations • Do not apply Jahn Micro Injection Grout to a

frozen or hot substrate. The applied grout must be protected from extreme heat, freezing, excessive wind, direct sunlight, and rain. Ambient temperature range should be 40° F to 90° F with low to average humidity.

• Do not add bonding agents to Jahn Micro Injection Grout or use them as surface preparation materials.

Packaging A two-gallon plastic pail contains approximately 15 lb. of material. Coverage will vary depending on the type of substrate and the size of the crack.

Storage And Shelf Life Store material in a dry area away from direct sunlight. Ambient storage conditions should be in the range of 40° F to 90° F with low to average humidity. Average shelf life is six months in original, unopened packaging. Technical Data

Jahn M30 – #31 Micro Injection Grout

Compressive strength

2 days approx. 3 days approx. 7 days approx. 28 days approx.

3600 psi 6400 psi 7400 psi 9000 psi

Tensile strength 28 days approx. 360 psi Concrete granular size

Smaller than 6.3E-04 inches

Viscosity direct 80 cps Specific gravity 1.77 Consumption

Ratio water/dry material: 45% of total weight

Application mixed product

Approx. 30 minutes (68ºF)

Jahn M30 – #32 Micro Injection Grout

Compressive strength

2 days approx. 3 days approx. 7 days approx. 28 days approx.

1264 psi 2243 psi 2591 psi 3160 psi

Tensile strength 28 days approx. 195 psi Concrete granular size

Smaller than 6.3E-04 inches

Viscosity direct 80 cps Specific gravity 1.77 Consumption

Ratio water/dry material: 45% of total weight

Application mixed product

Approx. 30 minutes (68ºF)

Warning Not for internal consumption. Keep out of reach of children and animals. Consult Material Safety Data Sheet (MSDS) for specific information. Notice: The information contained herein is based on our own research and the research of others, and it is provided solely as a service to help users. It is believed to be accurate to the best of our knowledge. However, no guarantee of its accuracy can be made, and it is not intended to serve as the basis for determining this product's suitability in any particular situation. For this reason, purchasers are responsible to make their own tests and assume all risks associated with using this product. 03/2010

Cathedral Stone®


JAHN M120 • Marble Repair Mortar

CERTIFIED INSTALLERS ONLY

This single-component, cementitious, mineral based mortar is designed for the restoration of marble. Jahn M120 is completely vapor permeable and contains no latex or acrylic bonding agents or additives. M120 is formulated for compatibility with the marble substrate and is available in Standard, Premium, and Custom Colors. M120 provides a permanent solution, which both restores and protects the beauty of the marble. (Only Certified Installers may purchase Jahn M120 Marble Repair Mortar.)

Features and Benefits • Single-Component: Mixes with water only,

improving quality control and consistency of application.

• Compatible Formulations: Compatibility of physical properties ensures that the mortar and natural substrate react to the environment in the same way.

• Contains No Latex or Acrylic Bonding Agents: It protects the substrate by allowing salts, water vapor, and liquid water to reach the surface, preventing failure due to salt expansion or freeze/thaw cycles.

• Tenacious Adhesion: Strong bonding capabilities without relying on synthetic bonding agents.

• Factory Controlled: No field chemistry resulting in product variation.

• Custom Colored Upon Request: Closely matches existing masonry. Choose from Standard or Custom Colors.

• Certified Installers: Only installers with certification from Cathedral Stone Products can purchase Jahn M120 Marble Repair Mortar.

Application Procedures Surface Preparation Surfaces to receive M120 must be sound and free of all dust, dirt, grease, laitance and/or any other coating or foreign substance which may prevent proper adhesion. Remove all loose and deteriorated masonry from the repair area using

manual or pneumatic cutting tools. The area to be repaired should be cut to provide a minimum of 1/2” depth. Do not install repairs that have a feathered edge (see diagram in the next column), incorrect installation will cause repairs to fail prematurely. Wash the prepared surface with clean water and a bristle brush to remove dust from the pores.

Section: Correct (Square Cut) Surface Preparation

Section: Incorrect (Feathered Edge) Surface Preparation

Exposed Ferrous Metals In the event that ferrous metal reinforcement (re-bar, threaded rod, etc.) is exposed within the repair area or repairs are adjacent to ferrous metal jambs, lintels, anchoring systems etc., the Coronado Surface Tolerant Mastic 113 Line must be applied to all properly prepared ferrous metal surfaces before repairs are made. Refer to the Technical Data Sheets within Cathedral Stone’s Product line for proper preparation and use of the Coronado Surface Tolerant Mastic 113 Line. Mixing The mixing ratio is approximately 4 1/2 - 5 parts powder to 1 part water by volume (or until material is easy to spread), depending on temperature and humidity. More water may be required as ambient temperature rises. The mixing may be done by hand, stirring until the mortar is thoroughly mixed. The mortar should be the consistency of damp sand. M120 may also be mixed using a slow speed drill (400 - 600 rpm) equipped with a Jiffler-type mixing paddle. For best results, add the powder to the water slowly. The working time will vary, depending upon wind, temperature, and humidity. Using excessive water in the mixture may affect the color of the repair.

Application

Jahn M120 Page 2

Cathedral Stone®


Moisten the substrate using clean water. Jahn Mortar should be applied to a glistening wet surface on vertical applications and a well-dampened surface (with no pooling water) on horizontal applications. If the surface is allowed to dry out before applying M120, this step must be repeated. This is very important.

The next step of the application is what CSP has termed the “Peanut Butter” coat. The Jahn mortar should be mixed with water to the consistency of wet putty. Apply the “Peanut Butter” coat to the glistening wet substrate approximately 1/8 inch thick. Important – To achieve proper bond, the “Peanut Butter” coat must not dry out prior to application of Jahn Mortar (4.5:1) mix!

Since the working consistency of M120 is somewhat wet, large repairs may require successive applications in order to avoid material slump. If this is necessary, be sure to remove the shiny cement skin that sometimes forms on the surface by scraping away 1/16” of material. This will open the pores before an additional layer of material is applied.

Build up material beyond the surface of the original stone. The waiting period before finishing will vary, depending upon wind, temperature, and humidity. After achieving initial set, scrape away excess mortar until the desired profile is reached.

Curing Periodically mist M120 repairs using clean water for at least a 72-hour period. The timing for initial misting will vary with ambient conditions. Hot, dry conditions may require misting in 30 to 60 minutes. Cooler, damp conditions may require waiting several hours before beginning the curing process. Mist several times a day. Should access to the repairs be impossible over a period of time, plastic may be used to cover them temporarily. The application of plastic, however, does not remove the need for normal curing techniques.

Clean Up Remove uncured mortar from the perimeter of the repair before it dries using clean water and a rubber sponge. Repeat several times with clean water to prevent a halo effect (staining of adjacent masonry). Cured mortar may only be removed chemically or mechanically.

Safety Requirements

It is recommended that safety goggles, gloves, and a dust mask equipped with P-2 filters (or equivalent) be worn for protection while mixing.

Limitations • Do not apply Jahn Mortar to frozen or

exceedingly hot substrate. The applied mortar must be protected from extreme heat, freezing, excessive wind, direct sunlight, and rain. Ambient temperature range should be 40° F to 90° F with low to average humidity.

• Do not add bonding agents to Jahn Mortar or use them as surface preparation materials.

• Minimum thickness of mortar application is � .

Packaging and Coverage A 5-gallon plastic pail contains approximately 44 lb. of material. This will cover 0.5 cubic feet (12 square feet at 1/2” thickness). Storage And Shelf Life Store material in a dry area away from direct sunlight. Ambient storage conditions should be in the range of 40°F to 90° F with low to average humidity. Average shelf life is 6 months in original, unopened packaging.

Technical Data Jahn M120 – Marble Repair Mortar

LIQUI / PLASTIC PHASE

Ratio of water/dry material 3 fl. oz. to 4.5 lb.

Volume per pound mixed mortar 12.0 fl. oz./lb

HARDENED PHASE

Compressive strength 4700 to 5000 psi

Tensile bending strength 650 psi

Tensile strength 150 psi Linear coefficient of thermal expansion

0.10E-06 to 0.2E-06 in inches ºF

Modulus of elasticity 1200 to 1540 ksi Open porosity (%) 4.2 to 16.5 Specific gravity 1.3

Warning

Jahn M120 Page 3 Not for internal consumption. Keep out of reach of children and animals. Consult Material Safety Data Sheet (MSDS) for specific information.

Notice: The information contained herein is based on our own research and the research of others, and it is provided solely as a service to help users. It is believed to be accurate to the best of our knowledge. However, no guarantee of its accuracy can be made, and it is not intended to serve as the basis for determining this product's suitability in any particular situation. For this reason, purchasers are responsible to make their own tests and assume all risks associated with using this product. 1/2010

MSDS – Jahn Mortars (M-Products) Page 1 of 2 1/18/2008

Cathedral Stone®

Products 7266 Park Circle Drive Hanover, Maryland 21076 (800) 684-0901 FAX: (410) 782-9155 www.cathedralstone.com

Jahn Restoration Mortar (Jahn M-Products)

Material Safety Data Sheet

Section I –Product and Company Identification

Trade Name: Jahn Restoration Mortar Date Prepared: 9/10/2008

Supplier: Cathedral Stone Products Manufacturer: Cathedral Stone Products

Address: 7266 Park Circle Drive Address: 7266 Park Circle Drive

Hanover, Maryland 21076, U. S. A. Hanover, Maryland 21076, U. S. A.

Emergency Number: Chemtrec (800) 424-9300 Customer Code: CDTS

Telephone Number: (410) 782-9150 Fax Number: (410) 782-9155

Section II –Composition/ Information on Ingredients Ingredient Names OSHA PEL ACGIH TLV NOISH (RTECS)#

Silicon Dioxide (Quartz) (CAS: 14808-60-7) See table Z3 0.1 mg/m� Rdust; 9293

VV7330000

Non-Hazardous Aggregate N/A N/A 1000314NH Tricalcium Silicate (CAS: 12168-85-3) N/A N/A 1004122TS Dicalcium Silicate N/A N/A 1004278DS Tricalcium Aluminate (CAS: 12042-78-3) N/A N/A 1004124TA Calcium Oxide (CAS: 1305-78-8) 5mg/m� 2mg/m� EW3100000 Non-Hazardous Ingredients: Inorganic pigments N/A N/A 10000314NH

Section III – Physical/Chemical Characteristics Boiling Point: N/A Specific Gravity: 1400/1700 kg/m3 Vapor Pressure: N/A Melting Point: N/A Vapor Density (Air=1): N/A Evaporation Rate: N/A Solubility in Water (20º C): Negligible Solubility in Other Solvents: N/A Color: White to Pastel Odor: No Odor

Section IV – Fire and Explosion Hazard Data

Flash Point: N/A

Extinguishing Media: Media Suitable for Surrounding Fire (FP N).

Special Fire Fighting Procedure: Wear NIOSH / MSHA Approved SCBA & Full Protective Equip. (FP N).

Unusual Fire and Explosion Hazards: Not Relevant

Section V – Reactivity Data Stability: Yes Conditions to Avoid Stable (Stability): N/A Incompatibility (Materials to Avoid): N/A Hazardous Polymerization: No

Conditions to Avoid (Hazardous Polymerization): Not Relevant

MSDS – Jahn Mortars (M-Products) Page 2 of 2 1/18/2008

Cathedral Stone Jahn Mortars Material Safety Data Sheet

Section VI – Health Hazard Data Primary Routes of Entry: Inhalation Ingestion

Health Hazard acute and Chronic: Eye and Skin Irritation, Removes Oil From Skin. Other Potential Health Risks: None Carciogenicity – NTP: Yes Carciogenicity – IARC: Yes

Carciogenicity – OSHA: No

Explanation Carciogenicity: Not Relevant Signs / Symptoms of Exposure: See Health Hazards Medical Condition Aggravated by Exposure: None Specified by Manufacturer. Contact with Eyes: IMMEDIATELY FLUSH WITH POTABLE WATER FOR A MINIMUM OF 15 MINUTES, SEEK ASSISTANCE FROM MD (FP N). INHALATION: REMOVE TO FRESH AIR. SUPPORT BREATHING (GIVE 0*2/ARTF RESP) (FP N). INGESTION: CALL MD IMMEDIATELY (FP N).

Section VII – Safe Handling and Use Information Steps to be Taken in Case Material is Released or Spilled: Normal Clean Up.

Neutralizing Agent: None Specified by Manufacturer.

Waste Disposal Method: If This Material as Provided by the Manufacturer, Becomes a Waste, It Doesn’t Meet the Criteria of a Hazardous Waste as Defined by the EPA Under Authority of the RCRA. Disposal Must be in Accordance With Federal, State, or Local Regulations (FP N). Precautions-Handling / Storage: Store Dry

Other Precautions: Avoid Contact Between Skin Surfaces and Wet Mortar, or Clothing Saturated With Wet Mortar. Wash Clothing in Clean Water.

Normal Use: Mix With Water and Use Within 30 Minutes. Do Not Use Under 5°C (41°F).

Section VIII – Control Measures

Protective Gloves: Impervious Gloves Recommended. Respiratory Protection: NIOSH / MSHA Approved Dust Respirator. Ventilation: N/A Eye Protection: Chemical Worker’s Goggles. Other Protective Equipment: None Specified by Manufacturer. Work Hygienic Practices: None Specified by Manufacturer. Suppl. Safety and Health Data: None Specified by Manufacturer.

Section IX – Label Data Label Required: Yes

Label Status: G

Common Name: Cementitious Mortar Special Hazard Precautions: Inhalation: Pulmonary Diseases. Dust Can Cause Inflammation of the Lining Tissue of the Interior of the Nose and Inflammation of the Cornea. Label Name: Cathedral Stone Products, Inc. Label Street: 7266 Park Circle Drive Label City: Hanover Label State: Maryland Label Zip Code: 21076 Label Emergency Number: (410)782-9150 Fax: (410)782-9155

Section XX – Transportation DOT Shipping: N/A DOT Hazard: N/A

Section XXI Disclaimer: Although reasonable care has been taken in preparation of this document, we extend no warrantees, and make no representations as to the accuracy or completeness of information Contained therein, and assume no responsibility regarding the suitability of this information for the user’s intended purposes or for the consequences of its use. Each individual should make a determination as to the suitability of the information for his or her particular purpose.

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Mix&GO�2.5/1�Masonry�Mortar�This�Mix&GO�is�the�perfect�choice�when�a�highly�workable,�easy�to�use�product�is�needed,�particularly�in�stonework.��Our�Standard�Mix&GO�2.5/1�Mortar�is�made�with�NHL�3.5W,�however�can�be�made�with�the�Natural�Hydraulic�Lime�of�your�choice.��This�durable�100%�Natural�Mortar�product�is�perfect�for�almost�any�masonry�application.��No�sourcing�sands,�no�dealing�with�color,�just�add�water�“Mix&GO”.��Available�Custom�Colored�and�in�our�range�of�40�standard�colors.��Mix&GO�2.5/1�Mortar�is�MADE�IN�THE�USA.�

Where�to�Use�This�Mix&GO�is�designed�to�work�in�the�following�applications.��Laying�Brick,�Stone,�&�Masonry�Units,�Repointing�Brick�&�Stonework.��Mix&GO�2.5/1�Masonry�Mortars�can�be�used�on�interior�and�exterior�masonry.�

��TECHNICAL�INFORMATION�Components�Mix&GO�2.5/1�is�a�lime�mortar�that�contains�lime,�(Natural�Hydraulic�Lime,�conforming�to�EN:459),�a�blend�of�natural�sands,�and�(in�colored�products),�synthetic�iron�oxide�pigments.��This�product�contains�no�cement,�latex,�or�acrylic�admixtures.��

Compressive�Strengths�(Approximate)��

Lime 7 Days 14 Days 28 Days 56 Days 91 Days 182 Days 365 Days 730 Days

NHL3.5� 34.81 94.27 168.24 242.21 292.98 366.96 440.91 515.88

�Aggregate�Sieve�Analysis�(Percent�Retained)�

#2� #4� #8� #16� #25 #50 #100 #200� PAN

0.000 0.000 0.024 4.642 20.770 53.480 18.386 1.638 0.240 �Preparation�For�Laying�or�Bedding�Masonry:��Protect�work�from�harsh�direct�sunlight,�wind�and�rain,�and�if�necessary�freezing�temperatures.��Protect�sills,�ledges,�windows,�doors,�and�projections�from�droppings�and�splatters.��Do�not�use�tape�or�adhesives�on�any�masonry�surface.��Prevent�mortar�from�staining�the�face�of�the�masonry�and�or�other�surfaces�to�be�left�exposed.��For�Masonry�Repointing:��Remove�all�existing�cement�mortar�by�hand.��Angle�Grinders�should�not�be�used�at�risk�of�damaging�historic�masonry.��If�grinding�is�deemed�necessary�only�craftspeople�demonstrating�skill�at�this�task�should�perform�this�work.��All�deteriorated�mortar�should�be�raked�out�to�sound�mortar,�leaving�a�clean�square�face�at�the�back�of�the�joint,�to�which�ever�depth�is�greatest�(1�inch,�1�½�times�the�width�of�the�mortar�joints,�or�until�cohesive�existing�mortar�is�encountered).��Care�should�be�taken�not�to�damage�historic�masonry�surfaces�and�masonry�joints�should�not�be�widened.��Debris�should�be�removed�by�hand�brushing,�vacuuming,�or�pressurized�air.�If�there�is�evidence�of�moisture�retention�or�rising�damp�it�may�be�necessary�to�allow�the�structure�to�“dry�out”.��If�this�process�is�not�done,�lime�leeching�may�occur,�causing�failure�or�the�placed�mortar�and�staining�of�the�masonry.��Control�Absorption�by�wetting�units�or�surfaces�prior�to�application.��Surfaces�and/or�units�should�be�cool�and�damp�but�not�glistening�or�“holding�water”�to�prevent�premature�drying�of�mortar�

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Mixing�Directions��Mix&GO�can�be�mixed�either�by�hand�or�in�a�mechanical�paddle�mixer.��Add�one�bag�(65�lbs)�of�Mix&GO�with�1.1�gallons�and�blend,�adding�additional�water�as�necessary�to�achieve�workability.��Mix�for�at�least�5�minutes.�Please�note�that�adding�too�much�water�can�cause�mortar�to�shrink,�crack,�and/or�change�color�while�curing.��

Application��Lay�a�bed�of�mortar�to�sufficiently�create�full�bed�(horizontal)�joints�and�“butter”�brick�ends�to�form�full�head�(vertical)�joints.�Do�not�move�or�adjust�units�after�the�commencement�of�set,�which�can�cause�loss�of�bond�between�mortar�and�masonry�units.��If�adjustments�are�deemed�necessary�remove�both�the�masonry�unit�and�the�bed,�and�re�lay�using�fresh�mortar.��For�Masonry�Repointing:��Pack�mortar�firmly�against�the�previously�placed�mortar�by�applying�firm�pressure�to�ensure�close�contact�between�the�lifts.��When�finishing�mortar�joints�it�is�often�preferable�to�match�the�original�joint�profile.��Reworking:��Standard�Mix&GO�can�be�reworked�for�up�to�3�hours.��If�a�different�Natural�Hydraulic�Lime�is�required,�reworking�times�may�be�different.��Please�view�corresponding�Natural�Hydraulic�Lime�Datasheets.��If�a�significant�amount�of�water�is�need�to�rework�the�mortar,�the�hydraulic�set�may�have�started�and�the�material�should�be�discarded.��Curing�Time:��Mortar�work�should�be�protected�from�sun,�wind,�and�rain�for�at�least�7�days.��Mortar�work�should�be�protected�from�freezing�temperatures�for�at�least�28�days.��In�some�cases�mortar�work�may�need�to�be�protected�from�freezing�temperatures�for�several�months.��Coverages�and�Consumption�(per�bag)�

�Clean�Up�Ensure�that�all�work�is�properly�protected�prior�to�cleaning.��Maintain�clean�surfaces�on�the�face,�sills,�ledges,�and�projections�of�masonry�on�a�daily�basis,�and�with�a�trowel,�strike�off�minor�dabs�of�adherent�mortar�from�masonry�faces.��After�mortar�has�achieved�thumbprint�hardness,�lightly�brush�masonry�to�remove�small�mortar�burrs�from�joints�and�masonry�edges.��Manual�cleaning�of�masonry�can�be�effective�by�using�water�and�soft�bristled�brushes�to�remove�mortar�smears.�Mortar�must�be�sufficiently�cured�before�light�pressurized�spray�(less�than�300�PSI)�can�be�used.��Caution�should�also�be�excercised�due�to�the�fact�that�over�saturation�of�the�masonry�could�lead�to�moisture�migration.��Virginia�Lime�Works�does�not�recommend�cleaning�with�masonry�detergents,�however,�if�such�measures�deem�detergents�necessary,�contact�detergent�manufacturer�for�protocol�when�cleaning�“PURE�LIME�MORTAR”�and�test�the�treatment�in�small�inconspicuous�areas�to�determine�its�effectiveness�and�to�ensure�no�damage�occurs�to�the�building�fabric.��Tools�can�be�cleaned�using�conventional�methods�and�properly�protect�any�unused�product�from�moisture�and�freezing.��Opened�bags�of�Mix&GO�can�be�stored�in�sealed�pails�for�up�to�6�months�from�date�of�purchase.��

Alternate�products�Mix&GO�2/1,�Natural�Hydraulic�Lime�(to�be�mixed�with�sand�on�site),�Lime�Putty�Mortar,�Hot�Lime�Mortar.��

Additional�References�Mix&GO�Material�Safety�Data�Sheet,�Guide�to�Traditional�Lime�Mortar,�Guide�to�Natural�Hydraulic�Limes,�Mortar�Classification�Chart,�Guide�to�Masonry�Repointing.��

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Yield�(Gallons)�

Yield�(cubic�feet)�

Bricklaying�4”�bed��½”�thick�

Stonework�4”�bed��½”�thick�

Repointing�Brick�½”�joint�–�¾”�thick�

Repointing�Stone½”�joint�–�¾”�thick�

Approx.�5�gallons� Approx.�0.75�ft3� 30�brick� 41.25�linear�ft� 75�ft2� 220�linear�ft�

P.O. Box 516 Monroe, VA 24574 www.virginialimeworks.com

434/929-8113 434/929-8114 fax

e-mail: [email protected]

MATERIAL�SAFETY�DATA�SHEET�(MSDS)�Mix&GO�Pre�Mixed�Natural�Hydraulic�Lime�Mortar�Prepared�August�31,�2007�

Manufacturer: Virginia Lime Works P.O. Box 516 Monroe, VA 24574

Emergency Telephone No: 434/929-8113 Information Telephone No: 434/929-8113

SECTION I- PRODUCT IDENTIFICATION

Product Types: Virginia Lime Works Natural Hydraulic Lime Pre-Mixed Masonry Products

Product Names:

Virginia Lime Works Mix&GO 2:1 Mortar Virginia Lime Works Mix&GO 2.5:1 Mortar Virginia Lime Works Mix&GO 1:1 Mortar (Butterjoint) Virginia Lime Works Mix&GO BaseCoat Virginia Lime Works Mix&GO RenderCoat Virginia Lime Works Mix&GO FinishCoat Virginia Lime Works Mix&GO FinishCoat Exterior

Also applies to any custom colored or special mixes

SECTION II– HAZARDOUS INGREDIENTS/IDENTITY INFORMATION

Components

Natural Sand* *Composition varies naturally-typically contains quartz (crystalline silica)

Silica Sand

Hydraulic Calcium Hydroxide (hydrated hydraulic lime)

Calcium Carbonate (calcite)

Calcium Oxide (fired limestone)

Iron Oxide Pigments

*Respirable fraction

CAS No.

None 14808-60-7

14808-60-7

1305-62-0

1317-65-3

10034-77-2

01309-37-1

PEL (OSHA)

10mg/m3

15mg/m3

15mg/m3

5mg/m3*5mg/m3*

5mg/m3*

TLV (ACGIH)

10mg/m3

10mg/m3

5mg/m3*2mg/m3*

5mg/m3*

SECTION III- PHYSICAL INFORMATION

Appearance and Odor: White to Gray Powder with coarse particles (sand) in its non-colored state. With pigments color will vary; No Odor

Solubility: Slight

SECTION IV- FIRE AND EXPLOSION HAZARD DATA

Flammability: Noncombustible and nonexplosive

SECTION V- REACTIVITY DATA

Stability: Stable Cautions to avoid: Hydrofluoric acid dissolves silica to produce the corrosive gas silicon

tetrafluoride. Acids react violently to produce heat. Hazardous polymerization: Will Not Occur

P.O. Box 516 Monroe, VA 24574 www.virginialimeworks.com

434/929-8113 434/929-8114 fax

e-mail: [email protected]

SECTION VI- HEALTH HAZARD DATA

Route of Entry: Inhalation, Skin, Ingestion

Effects of OverexposureInhalation: Inhalation of the dust may cause coughing, sneezing, irritation and inflammation of the

upper respiratory tract. Inhalation of free crystalline silica (SiO2) may cause silicosis, a dust disease with signs and symptoms of coughing, shortness of breath, wheezing and changes in chest x-ray. Silicosis is typically associated with chronic or long-term exposure to silica; the disease may continue to progress even after exposure is eliminated. Exposure to very high air concentrations of free silica can cause an acute form of silicosis that may occur within one year after exposure begins. This condition may be fatal.

Dermal Exposure: Not absorbed through the skin. Calcium hydroxide and calcium oxide are caustic and may cause irritation of skin.

Eye Irritation: May be irritating to the eyes, with burning, itching, or redness.

Carcinogenicity: The Sixth Annual Report on Carcinogens, 1991, U.S. Department of Health and Human Services, National Toxicology Program states: “There is sufficient evidence of the carcinogenicity of respirable crystalline silica in experimental animals.” However, an IARC Working Group has reported limited evidence of carcinogenicity in humans. NIOSH considers respirable silica to be a potential human carcinogen. OSHA and ACGIH have not identified respirable silica as a carcinogen.

Ingestion: Not considered a likely route of exposure.

Emergency & First Aid: In case of contact with eyes, immediately flush eyes with large quantities of clean water for at least 15 minutes. Call a physician if irritation persists. Or skin contact, flush with water. If swallowed, do not induce vomiting. If conscious, have victim drink large quantities of water and contact a physician.

SECTION VII- WASTE DISPOSAL & HANDLING

Sweep and place bulk material in containers and remove for disposal or usE if not contaminated or wet. Flush spill area with water. This product is not classified as a hazardous waste under RCRA or CERCLA, however it may be a characteristic hazardous waste due to its high pH. The final, cured product is not hazardous. Dispose of in a landfill in accordance with all governmental regulations.

SECTION VIII- PERSONAL PROTECTION

Protective Clothing: Coveralls and protective gloves are recommended to minimize contact with skin.

Eye Protection: Safety glasses are recommended to minimize eye contact.

MAKE ALL EMPLOYEES, USERS, AND CUSTOMERS AWARE OF THE HAZARDS ASSOCIATED WITH THIS PRODUCT AND THE REQUIRED OSHA PRECAUTIONS FOR ITS USE

Respiratory Protection: Special care should be taken to prevent dust from becoming airborne. The use of ventilation systems and wet-methods are recommended. If other methods are not sufficient to reduce the dust concentration below the OSHA permissible exposure lime, use a NIOSH approved respirator with particle filters.

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Sikadur® 31, Hi-Mod Gel (1:1 Mix Ratio)High-modulus, high-strength, structural, epoxy paste adhesive

Description Sikadur 31, Hi-Mod Gel, is a 2-component, 100% solids, solvent-free, moisture-tolerant, high-modulus, high-strength, structural epoxy paste adhesive. It conforms to the current ASTM C-881 and AASHTO M-235 specifica-tions.

Where to Use � Structural bonding of concrete, masonry, metals, wood, etc. to a maximum glue line of 1⁄8 in. (3 mm). � Grout bolts, dowels, and pins. � Seals cracks and around injection ports prior to pressure-injection grouting. � Interior, vertical, and overhead repair of concrete as an epoxy mortar binder. � As a pick-proof sealant around windows, doors, lock-ups etc. inside correctional facilities.Advantages � Meets physical requirements of ASTM C-881 Types I, II & IV, Grade 3, Classes B & C. � Suitable for potable water contact, meets NSF/ANSI Standard 61. � Excellent adhesion to concrete, masonry, metals, wood, and most structural materials. � Paste consistency ideal for vertical and overhead repair of concrete. � Fast-setting and strength-producing adhesive. � Convenient easy mix ratio A:B = 1:1 by volume.

Product Data Sheet

Edition 7.1.2008Identification no. 039003NSikadur 31, Hi-Mod Gel

Typical Data (Material and curing conditions @ 73°F (23°C) and 50% R.H.)

Shelf Life 2 years in original, unopened containersStorage Conditions Store dry at 40°-95°F (4°-35°C). Condition material to 65°-85°F (18°-29°C)

before using.

Color GrayMixing Ratio Component ‘A’ : Component ‘B’ = 1:1 by volumeConsistency Non-sag pastePot Life Approximately 60 minutes @ 73°F. (500 gram mass)Tack-Free Time 1.5 - 2.5 hours at 30 mils. thickTensile Properties (ASTM D-638) 7 day Tensile Strength 3,300 psi (22.7 MPa) Elongation at Break 0.9 %Flexural Properties (ASTM D-790) 7 day Flexural Strength (Modulus of Rupture) 6,100 psi (42.0 MPa) Tangent Modulus of Elasticity in Bending 1.67 X 106 psi (11,520 MPa)Shear Strength (ASTM D-732) 7 day Shear Strength 4,600 psi (31.7 MPa)Bond Strength (ASTM C-882) Hardened Concrete to Hardened Concrete: 2 day (dry cure) 2,200 psi (15.2 MPa) 2 day (moist cure) 2,400 psi (16.5 MPa) 14 day (moist cure) 2,900 psi (20.0 MPa) Hardened Concrete to Steel: 2 day (dry cure) 2,900 psi (20.0 MPa)Tensile Bond Strength (Pull-off Method, Dyna, ASTM C-1583-04)

2 day 420 psi (2.9 MPa) Heat Deflection Temperature (ASTM D-648) 7 day (Fiber Stress Loading = 264 psi) 135°F (57°C) Water Absorption (ASTM D-570) 24 hour 0.07%Compressive strength (ASTM D-695) psi (MPa) 40°F (4°C)* ** 73°F (23°C)* ** 90°F (32°C)* ** 2 hour - - 450 (3.1) 4 hour - 800 (5.5) 10,500 (72.4) 8 hour - 8,500 (58.6) 12,200 (84.1) 16 hour 700 (4.8) 10,500 (72.4) 13,000 (89.6) 1 day 6,000 (41.4) 13,000 (89.6) 15,000 (103.4) 3 day 11,000 (75.8) 14,000 (96.5) 16,000 (110.3) 7 day 12,900 (88.9) 15,000 (103.4) 16,000 (110.3) 14 day 13,500 (93.0) 15,400 (106.1) 16,000 (110.3) 28 day 14,000 (96.5) 16,000 (110.3) 16,000 (110.3)Compressive Modulus of Elasticity (ASTM D-695) 7 day 7.95 X 105 psi (5,485 MPa)

* Material cured and tested at temperatures indicated. ** See Limitations section for further information.

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Coverage 1 gal. yields 231 cu. in. (3,785 cm3) of epoxy paste adhesive. 1 gal. (3.8 L) mixed with 1 gal. (3.8 L) by loose volume of oven-dried aggregate yields approximately 346 cu. in. (5,670 cm3) of epoxy mortar.

Packaging 3 gal. (11.4 L) units.

How to UseSurface Preparation Surface must be clean and sound. It may be dry or damp, but free of standing water. Remove dust, laitance,

grease, curing compounds, impregnations, waxes, and any other contaminants. Preparation Work: Concrete - Should be cleaned and prepared to achieve a laitance and contaminant

free, open textured surface by blastcleaning or equivalent mechanical means. Steel - Should be cleaned and prepared thoroughly by blastcleaning.

Mixing Pre-mix each component. Proportion 1 part Component ‘B’ to 1 part Component ‘A’ by volume into a clean pail. Mix thoroughly for 3 minutes with Sika paddle on low-speed (400- 600 rpm) drill until uniform in color. Mix only that quantity which can be used within its pot life. Prior to mixing, material should be conditioned to 65°-85°F (18°-29°C). To prepare an epoxy mortar, slowly add up to 1 part, by loose volume of an oven-dried aggregate, to 1 part of the mixed Sikadur 31, Hi-Mod Gel, and mix until uniform in consistency.

Application As a structural adhesive - Apply the neat mixed Sikadur 31, Hi-Mod Gel to the prepared substrates. Work into the substrate for positive adhesion. Secure the bonded unit firmly into place until the adhesive has cured. Glue line should not exceed 1⁄8-in. (3 mm).

To seal cracks for injection grouting - Place the neat mixed material over the cracks to be pressure injected and around each injection port. Allow sufficient time to set before pressure injecting.

For interior vertical and overhead patching - Place the prepared mortar in void, working the material into the prepared substrate, filling the cavity. Strike off level. Lifts should not exceed 1-in (25 mm).

As a pick-proof sealant - Use automated or manual method. Apply an appropriate size bead of material around the area being sealed. Seal with neat Sikadur 31, Hi-Mod Gel.

Limitations � THE NTSB HAS STATED THAT THIS PRODUCT IS APPROVED FOR SHORT TERM LOADS ONLY AND SHOULD NOT BE USED IN SUSTAINED TENSILE LOAD ADHESIVE ANCHORING APPLICA-TIONS WHERE ADHESIVE FAILURE COULD RESULT IN A PUBLIC SAFETY RISK. CONSULT A

DESIGN PROFESSIONAL PRIOR TO USE.

� Components of original 2:1 mix ratio formulation of Sikadur 31, Hi-Mod Gel cannot be cross-mixed with components of Sikadur 31, Hi-Mod Gel (NEW 1:1 Mix Ratio) formulation.

� Minimum substrate and ambient temperature 40°F (4°C). � Do not thin. Solvents will prevent proper cure. � When preparing an epoxy mortar, use oven-dried aggregate only. � Maximum epoxy mortar thickness is 1 in. (25 mm) per lift. � Epoxy mortar is for interior use only. Material is a vapor barrier after cure. � Minimum age of concrete must be 21-28 days, depending upon curing and drying conditions, for mortar applications. � Porous substrates must be tested for moisture-vapor transmission prior to mortar applications. � Not for sealing cracks under hydrostatic pressure. � Not an aesthetic product. Color may alter due to variations in lighting and/or UV exposure.

WARNING Component ‘A’ - IRRITANT, SENSITIZER. Contains epoxy resin, silica, and calcium carbonate. Causes eye irritation. May cause skin/respiratory irritations. Prolonged and/or repeated contact with skin may cause allergic reaction/sensitization. Harmful if swallowed. Deliberate concentrations of vapors for purposes of

inhalation is harmful and can be fatal.

Component ‘B’ - CORROSIVE, SENSITIZER, IRRITANT. Contains Amines, silica quartz (sand), and calcium carbonate. Contact with skin and eyes causes severe burns. Causes eye/skin/respiratory irritation. Prolonged and/or repeated contact may cause allergic reaction/sensitization. Harmful if swallowed. Deliber-

ate concentrations of vapors for purposes of inhalation is harmful and can be fatal.

Cured material, if sanded, may result in exposure to a chemical known to the State of California to cause cancer.

First Aid Eyes - Hold eyelids apart and flush thoroughly with water for 15 minutes. Skin - Remove contaminated clothing. Wash skin thoroughly for 15 minutes with soap and water. Inhalation - Remove person to fresh air. Ingestion - Do not induce vomiting. Contact a physician. In all cases, contact a physician immediately if

symptoms persist.

Handling & Storage Avoid direct contact with eyes and skin. Wear chemical resistant gloves/goggles/clothing. Avoid breathing vapors. Use with adequate general and local exhaust ventilation. Use a properly fitted NIOSH approved respirator. Wash thoroughly after handling product. Remove contaminated clothing and launder before reuse. Store product in a closed container in a cool, dry place.

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Visit our website at www.sikaconstruction.com 1-800-933-SIKA NATIONWIDE

Regional Information and Sales Centers. For the location of your nearest Sika sales office, contact your regional center.Sika Corporation Sika Canada Inc. Sika Mexicana S.A. de C.V. 201 Polito Avenue 601 Delmar Avenue Carretera Libre Celaya Km. 8.5Lyndhurst, NJ 07071 Pointe Claire Fracc. Industrial BalvaneraPhone: 800-933-7452 Quebec H9R 4A9 Corregidora, QueretaroFax: 201-933-6225 Phone: 514-697-2610 C.P. 76920 Fax: 514-694-2792 Phone: 52 442 2385800

Fax: 52 442 2250537

KEEP CONTAINER TIGHTLY CLOSED • KEEP OUT OF REACH OF CHILDREN • NOT FOR INTERNAL CONSUMPTION • FOR INDUSTRIAL USE ONLY

All information provided by Sika Corporation (“Sika”) concerning Sika products, including but not limited to, any recommendations and advice relating to the application and use of Sika products, is given in good faith based on Sika’s current experience and knowledge of its products when properly stored, handled and applied under normal conditions in accordance with Sika’s instructions. In practice, the differences in materials, substrates, storage and handling condi-tions, actual site conditions and other factors outside of Sika’s control are such that Sika assumes no liability for the provision of such information, advice, recommendations or instructions related to its products, nor shall any legal relationship be created by or arise from the provision of such information, advice, recommendations or instructions related to its products. The user of the Sika product(s) must test the product(s) for suitability for the intended application and purpose before proceeding with the full application of the product(s). Sika reserves the right to change the properties of its products without notice. All sales of Sika product(s) are subject to its current terms and conditions of sale which are available at www.sikacorp.com or by calling 800-933-7452. Prior to each use of any Sika product, the user must always read and follow the warnings and instructions on the product’s most current Technical Data Sheet, product label and Material Safety Data Sheet which are available online at www.sikaconstruction.com or by calling Sika's Technical Service Department at 800-933-7452. Nothing contained in any Sika materials relieves the user of the obligation to read and follow the warnings and instruction for each Sika product as set forth in the current Technical Data Sheet, product label and Material Safety Data Sheet prior to product use.

LIMITED WARRANTY: Sika warrants this product for one year from date of installation to be free from manufacturing defects and to meet the technical properties on the current Technical Data Sheet if used as directed within shelf life. User determines suitability of product for intended use and assumes all risks. Buyer’s sole remedy shall be limited to the purchase price or replacement of product exclusive of labor or cost of labor. NO OTHER WARRANTIES EXPRESS OR IMPLIED SHALL APPLY INCLUDING ANY WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE. SIKA SHALL NOT BE LIABLE UNDER ANY LEGAL THEORY FOR SPECIAL OR CONSEQUENTIAL DAMAGES. SIKA SHALL NOT BE RESPONSIBLE FOR THE USE OF THIS PRODUCT IN A MANNER TO INFRINGE ON ANY PATENT OR ANY OTHER INTELLECTUAL PROPERTY RIGHTS HELD BY OTHERS.

Sika and Sikadur are registered trademarks. Made in USA. Printed in Canada.

Clean Up Avoid contact. Wear chemical resistant clothing/gloves/goggles. In absence of adequate ventilation, use a properly fitted NIOSH respirator. Uncured material can be removed with solvent. Follow solvent manufactur-er’s instructions for use and warnings. Cured material (when Component ‘A’ combined with Component ‘B’) can only be removed mechanically. In case of spill, ventilate area and contain spill. Collect with absorbent material. Dispose of in accordance with current, applicable local, state and federal regulations.

M A T E R I A L S A F E T Y D A T A S H E E T

Page 1 of 5

Sikadur 31, Hi Mod Gel - Part A

HMIS

HEALTH 2

FLAMMABILITY 1

REACTIVITY 0

PERSONAL PROTECTION C

1. Product And Company Identification

Supplier Manufacturer

Sika Corporation Sika Corporation

201 Polito Ave 201 Polito Ave

Lyndhurst, NJ 07071 Lyndhurst, NJ 07071

Company Contact: EHS Department Company Contact: EHS DepartmentTelephone Number: 201-933-8800 Telephone Number: 201-933-8800FAX Number: 201-933-9379 FAX Number: 201-933-9379Web Site: www.sikausa.com Web Site: www.sikausa.com

Supplier Emergency Contacts & Phone Number Manufacturer Emergency Contacts & Phone Number

CHEMTREC: 800-424-9300 CHEMTREC: 800-424-9300

INTERNATIONAL: 703-527-3887 INTERNATIONAL: 703-527-3887

Issue Date: 04/15/2003

Product Name: Sikadur 31, Hi Mod Gel - Part ACAS Number: Not EstablishedChemical Family: Modified Epoxy ResinMSDS Number: 2665Product Code: 0390130

2. Composition/Information On Ingredients

Ingredient CAS Percent OfName Number Total Weight

AROMATIC HYDROCARBON BLEND Trade Secret

CALCIUM CARBONATE 471-34-1

MODIFIED EPOXY RESIN Trade Secret

NONYLPHENOL 25154-52-3

SILICA, QUARTZ 14808-60-7

Note: Exposure to silica, quartz is applicable only if cured with Part "B" and sanded.

3. Hazards Identification

Eye Hazards

May cause eye irritation.

Skin Hazards

May cause skin irritation. May cause skin sensitization.


Page 2 of 5


3. Hazards Identification - Continued

Ingestion Hazards

Harmful if swallowed.

Inhalation Hazards

May cause nose, throat, and lung irritation.

4. First Aid Measures

Eye

Rinse eyes thoroughly with water for at least 15 minutes. Consult physician.

Skin

In case of contact, immediately flush skin with plenty of water for at least 15 minutes.

Ingestion

Dilute with water. If swallowed, do not induce vomiting unless directed to do so by medical personnel.

Inhalation

If not breathing, give artificial respiration, seek medical attention.

5. Fire Fighting Measures

Flash Point: >213 °F >101 °C

Fire And Explosion Hazards

None Known.

Extinguishing Media

In case of fire, use water spray (fog) foam, dry chemical, or CO2.

Fire Fighting Instructions

Firefighters should wear self-contained breathing apparatus and full protective gear.

6. Accidental Release Measures

Avoid release to the environment. Use appropriate personal protective equipment (PPE). Contain spill and collect withabsorbent material and transfer into suitable containers. Ventilate enclosed area.

7. Handling And Storage

Handling And Storage Precautions

Store in a cool area. Keep containers tightly closed. Keep awat from ignition sources. Protect from heat anddirect sunlight.

Work/Hygienic Practices

Wash thoroughly with soap and water after handling.

8. Exposure Controls/Personal Protection

Engineering Controls

Use with adequate general and local exhaust ventilation.

Eye/Face Protection

Safety glasses with side shields or goggles.

Skin Protection

Chemical-resistant gloves. Lab coat or other work clothing to prevent skin exposure. Launder before reuse.

Respiratory Protection

A respirator protection program that meets 29 CFR 1910.134 requirement must be followed whenever workplaceconditions warrant a respirator's use. In areas where the Permissible Expsoure Limits are exceeded, use a


Page 3 of 5


8. Exposure Controls/Personal Protection - Continued

Respiratory Protection - Continued

properly fitted NIOSH-approved respirator.

Other/General Protection

Wash thoroughly after handling.

Ingredient(s) - Exposure Limits

CALCIUM CARBONATE ACGIH TLV-TWA 10 mg/m3 OSHA PEL-TWA 15 mg/m3 OSHA PEL-TWA 5 mg/m3SILICA, QUARTZ ACGIH TLV-TWA 0.1 mg/m3 (Notice of Intended Change) ACGIH TLV-TWA 0.05 mg/m3 (Proposed) OSHA PEL-TWA 30/%SiO2+2 mg/m3 OSHA PEL-TWA 10/%SiO2+2 mg/m3 OSHA PEL-TWA 250/%SiO+5 mppcf

9. Physical And Chemical Properties

Appearance

Yellowish Liquid

Odor

Characteristic

Chemical Type: MixturePhysical State: LiquidPacking Density: 1.1 g/cm3S o l u b i l i t y : InsolubleEvaporation Rate: Slower than ether

10. Stability And Reactivity

S t a b i l i t y : StableHazardous Polymerization: Will not occur

Conditions To Avoid (Stability)

None known

Incompatible Materials

None when stored and handled according to prescribed instruction.

11. Toxicological Information

Eye Effects

Irritation

Skin Effects

Sensitization/allergic reaction possible.

Conditions Aggravated By Exposure

Eye disease, skin disorders and allergies, chronic respiratory disease

Ingredient(s) - Carginogenicity

SILICA, QUARTZ NTP - Listed On The National Toxicology Program Listed In The IARC Monographs


Page 4 of 5


12. Ecological Information

Do not allow to enter waste water drians, waterways, or soil.

13. Disposal Considerations

Dispose in accordance with applicable federal, state and local government regulations.

14. Transport Information

Proper Shipping Name

Not regulated by the USDOT.

15. Regulatory Information

U.S. Regulatory Information

All ingredients of this product are listed or are excluded from listing under the U.S. Toxic Substances Control Act(TSCA) Chemical Substance Inventory.

SARA Hazard Classes

Acute Health HazardChronic Health Hazard

SARA Section 313 Notification

This product does not contain any ingredients regulated under Section 313 of the Emergency Planning andCommunity Right-To-Know Act of 1986 or 40 CFR 372.

State Regulations

WARNING: This product contains a chemical known to the State of California to cause cancer, birth defects, orother reproductive harm.

Ingredient(s) - State Regulations

CALCIUM CARBONATE Pennsylvania - Workplace HazardNONYLPHENOL Pennsylvania - Workplace Hazard Massachusetts - Hazardous SubstanceSILICA, QUARTZ New Jersey - Workplace Hazard Pennsylvania - Workplace Hazard California - Proposition 65 Massachusetts - Hazardous Substance

16. Other Information

HMIS Rating

H e a l t h : 2F i r e : 1R e a c t i v i t y : 0P P E : C

Revision/Preparer Information

MSDS Preparer: EHS DepartmentThis MSDS Supercedes A Previous MSDS Dated: 04/15/2003


Page 5 of 5


Disclaimer

The data in this Material Safety Data Sheet relates only to the specific material herein and does not relate to usein combination with any other materialor in any process. The information set forth herein is based on technical data that Sika believes to be reliable as of the date hereof. Since conditions of use are outside our control, we makeno warranties, express or implied andassume no liability in connection with any use of this information. Nothingherein is to be taken as a license to operate under or a recommendation to infringe any patents.

SIKA CORPORATIONPrinted Using MSDS Generator™ 2000

M A T E R I A L S A F E T Y D A T A S H E E TPage 1 of 5

SIKADUR 31 SBA REGULAR SET 40-60F - PART B

HMIS

HEALTH 3

FLAMMABILITY 1

REACTIVITY 0

PERSONAL PROTECTION C

1. Product And Company Identification

Supplier Manufacturer

SIKA CORPORATION SIKA CORPORATION

201 Polito Ave 201 Polito Ave

Lyndhurst, NJ 07071 Lyndhurst, NJ 07071

Company Contact: Kristin Kelley Company Contact: Kristin KelleyTelephone Number: (201) 933-8800 Telephone Number: (201) 933-8800FAX Number: (201) 933-9379 FAX Number: (201) 933-9379Web Site: www.sikausa.com Web Site: www.sikausa.com

Supplier Emergency Contacts & Phone Number Manufacturer Emergency Contacts & Phone Number

CHEMTREC: 800-424-9300 CHEMTREC: 800-424-9300

INTERNATIONAL: 703-527-3887 INTERNATIONAL: 703-527-3887

Issue Date: 02/20/2003

Product Name: SIKADUR 31 SBA REGULAR SET 40-60F - PART BCAS Number: Not EstablishedChemical Family: AMINEMSDS Number: 2456Product Code: 0393-14O

2. Composition/Information On Ingredients

Ingredient CAS Percent OfName Number Total Weight

BLEND OF ALIPHATIC AMINES TradeSecret

CALCIUM CARBONATE 471-34-1

NONYL PHENOL 84852-15-3

SILICA, QUARTZ 14808-60-7

*EXPOSURE TO SILICA, QUARTZ IS APPLICABLE ONLY IF CURED WITH PART "A" AND SANDED.

3. Hazards Identification

Eye Hazards

MAY CAUSE SEVERE BURNS. MAY CAUSE VISUAL DISTURBANCES, CORNEA DAMAGE, DAMAGE TOTHE OPTIC NERVE OR BLINDNESS. REPEATED AND/OR PROLONGED EXPOSURE MAY RESULT INADVERSE EYE EFFECTS (SUCH AS CONJUNCTIVITIS OR CORNEAL DAMAGE).

Skin Hazards

CORROSIVE, CONTACT MAY CAUSE SEVERE IRRITATION AND PAIN AND MAY CAUSE BURNS,NECROSIS AND PERMANENT INJURY. PROLONGED AND/OR REPEATED CONTACT WITH SKIN MAYCAUSE AN ALLERGIC REACTION/SENSITIZATION.

M A T E R I A L S A F E T Y D A T A S H E E T Page 2 of 5


3. Hazards Identification - Continued

Ingestion Hazards

MAY CAUSE EFFECTS TO THE GI TRACT, SUCH AS IRRITATION, NAUSEA, GI DISORDERS, ULCERATION,DIARRHEA OR CONSTIPATION.

Inhalation Hazards

MAY CAUSE RESPIRATORY TRACT IRRITATION.

4. First Aid Measures

Eye

RINSE EYES THOROUGHLY WITH WATER FOR AT LEAST 15 MINUTES. CONSULT PHYSICIAN.

Skin

WASH SKIN THOROUGHLY WITH SOAP AND WATER. REMOVE CONTAMINATED CLOTHING.IF SYMPTOMS PERSIST CONSULT PHYSICIAN.

Ingestion

DO NOT INDUCE VOMITING. DILUTE WITH WATER. CONTACT PHYSICIAN.

Inhalation

REMOVE TO FRESH AIR. IF BREATHING HAS STOPPED, INSTITUTE ARTIFICIAL RESPIRATION. CONSULTWITH PHYSICIAN.

5. Fire Fighting Measures

Flash Point: >200 °FAutoignition Point: N/AV °F

Fire And Explosion Hazards

NONE KNOWN

Extinguishing Media

In case of fire, use water spray (fog) foam, dry chemical, or CO2.

Fire Fighting Instructions

Firefighters should wear self-contained breathing apparatus and full protective gear.

6. Accidental Release Measures

WEAR SUITABLE PROTECTIVE EQUIPMENT. CONTAIN SPILL AND COLLECT WITH ABSORBENT MATERIAL ANDTRANSFER INTO SUITABLE CONTAINERS. AVOID CONTACT.

7. Handling And Storage

Handling And Storage Precautions

STORE IN A COOL DRY AREA. KEEP CONTAINERS TIGHTLY CLOSED.

Work/Hygienic Practices

WASH THOROUGHLY AFTER USING PRODUCT.

8. Exposure Controls/Personal Protection

Engineering Controls

Use with adequate general and local exhaust ventilation.

Eye/Face Protection

Safety glasses with side shields or goggles.



8. Exposure Controls/Personal Protection - Continued

Skin Protection

AVOID SKIN CONTACT. WEAR LONG SLEEVE SHIRT AND LONG PANTS. NITRILE OR OTHER CHEMICALRESISTANT GLOVES.

Respiratory Protection

General room ventilation is normally adequate.

Other/General Protection

WASH THOROUGHLY AFTER HANDLING.

Ingredient(s) - Exposure Limits

CALCIUM CARBONATE ACGIH TLV-TWA 10 mg/m3 OSHA PEL-TWA 15 mg/m3 OSHA PEL-TWA 5 mg/m3SILICA, QUARTZ ACGIH TLV-TWA 0.1 mg/m3 (Notice of Intended Change) ACGIH TLV-TWA 0.05 mg/m3 (Proposed) OSHA PEL-TWA 30/%SiO2+2 mg/m3 OSHA PEL-TWA 10/%SiO2+2 mg/m3 OSHA PEL-TWA 250/%SiO+5 mppcf

9. Physical And Chemical Properties

Appearance

DARK GRAY PASTE

Odor

AMINE

Chemical Type: MixturePhysical State: SolidMelting Point: N/AV °FBoiling Point: N/AV °FSpecific Gravity: 1.80Percent Volatiles: N/AVPacking Density: 15.1 #/GALVapor Pressure: N/AVVapor Density: >AIRSolubility: N/AVEvaporation Rate: SLOWER THAN ETHER

10. Stability And Reactivity

Stability: STABLEHazardous Polymerization: WILL NOT OCCUR

Conditions To Avoid (Stability)

NONE KNOWN

Incompatible Materials

STRONG OXIDIZERS, ACIDS, BASES

Hazardous Decomposition Products

CO, CO2, OXIDES OF NITROGEN



11. Toxicological Information

Conditions Aggravated By Exposure

EYE DISEASE, SKIN DISORDERS AND ALLERGIES, CHRONIC RESPIRATORY CONDITIONS

Ingredient(s) - Carginogenicity

SILICA, QUARTZ NTP - Listed On The National Toxicology Program Listed In The IARC Monographs

12. Ecological Information

No Data Available...

13. Disposal Considerations

Dispose in accordance with applicable federal, state and local government regulations.

14. Transport Information

Proper Shipping Name

CORROSIVE SOLID, BASIC, ORGANIC, N.O.S. (ALIPHATIC AMINES)

Hazard Class

8 PGII

DOT Identification Number

UN3263

DOT Shipping Label

CORROSIVE

15. Regulatory Information

U.S. Regulatory Information

All ingredients of this product are listed or are excluded from listing under the U.S. Toxic Substances Control Act(TSCA) Chemical Substance Inventory.

SARA Hazard Classes

Acute Health HazardChronic Health Hazard

SARA Section 313 Notification

This product does not contain any ingredients regulated under Section 313 of the Emergency Planning andCommunity Right-To-Know Act of 1986 or 40 CFR 372.

State Regulations

WARNING: This product contains a chemical known to the State of California to cause cancer, birth defects, orother reproductive harm.

Ingredient(s) - State Regulations

CALCIUM CARBONATE Pennsylvania - Workplace HazardSILICA, QUARTZ New Jersey - Workplace Hazard Pennsylvania - Workplace Hazard California - Proposition 65 Massachusetts - Hazardous Substance



16. Other Information

HMIS Rating

Health: 3Fire: 1Reactivity: 0PPE: C

Revision/Preparer Information

MSDS Preparer: Kristin KelleyThis MSDS Supercedes A Previous MSDS Dated: 09/17/1996

Disclaimer

The data in this Material Safety Data Sheet relates only to the specific material herein and does not relate to use incombination with any other materialor in any process. The information set forth herein is based on technical da tathat Sika believes to be reliable as of the date hereof. Since conditions of use are outside our control, we make nowarranties, express or implied andassume no liability in connection with any use of this information. Nothing hereinis to be taken as a license to operate under or a recommendation to i nfringe any patents.

SIKA CORPORATIONPrinted Using MSDS Generator™ 2000

Cemetery Preservation Plans

Historical Research

Identification of Grave Locations and Mapping

Condition Assessments

Treatment of Stone and Ironwork

Chicora Foundation, Inc. PO Box 8664 � 861 Arbutus Drive Columbia, SC 29202-8664 Tel: 803-787-6910 Fax: 803-787-6910 www.chicora.org

Documents

CONSERVATION TREATMENT RECORDhistoricrandolphcemetery.org › documents › research › forms › ...TREATMENT RECORD FOR RANDOLPH CEMETERY, PHASE 2, CITY OF COLUMBIA, RICHLAND COUNTY,