f1R`f 25 ' 90 13 :34 14 LASER P . 2

CURMTCAL ANALYSI SR1 POW'

Log Number900441 2

To! EnviroLmenta.i unit DEPT/GROUP! 543-000 PHONE : 332-5311

FROM : SSPL Analytical ChemlztrY, TackeLib?e Div . UockteL1 International, D/5~9-1£9 . ext . 5827

aZFRRENCE : t.13 90 F 97 ; ND 1251, pages 161 - 174 REPORT DATE: 05/25/90

SAMPLE 1NFORKATION FOR 9004412

$ample Dcnarption : Sail, Sotithsltia pad 1, di6t4ace foo t

Reque[iter : Beatrice KephartRequested Ana,lynis : 'Metals

Neceived• 04/23/90 it 10 :15:00

Sampler : M. 13alversan Sampl r ID#: 042390Mf101 Sap lo Timer 9 :25:110

Sampled : 04/23/90

B4X . LEV1I

ANAL Y1'E RESULT UNIT CONTAMINATE METHOD/SQi3teCE

Antimony *** mg/kg DNA 6010, SW-84 6

Ansonia *sx 0 .1$ mg/kg l3NA 7060, SW-89 6

Barium *** 65 mg/kg DNA 7060, SW-84 6

Beryllium Us 0 .064 mg/kg DNA 6010, SW-84 6

Cadmium ** ma/kg DNA 6010, SW-84 6

Chromium 2 .1 mg/kg DNA 6010, Sod-44 8

Cobalt 1 .2 mg/kg ANA 6010, SS4-84 6

Copper 8 .7 mg/kg DNA 60ia, sir- R4 6

LIW *** -22 mg/kg DNA 6010, BW-84 6

Neroury ND<0 .042 mglkg DNA 7470, SW-84 3

tol ybdeti um ND<0 .53 mg/kg DNA 6010, SW-84 5

Nickel *** 3.2 mg/kg DNA 6010, SW-846

Selenium 44• 0<0 . 57 mg/kg DNA 6010, SR-64 6

Silver *** NIKQ.04 mg/kg DNA 6010, Sif-64 6

Thallium #* ND<p .04 mg/kg DNA 8010, SW-84 6

Vanadze m vat 0.91 mg/kg DNA 6010, SW-84 6

zinc *** 90 xg/kg DNA 6010, SH-84 6

------ --------------------

SPECIAL NOTES: B . KeDb.art Env . Eng . in charge of project . Deter , rain runoff conta l. So

etated limits . WET extract prior to analysis .

COMMENTS : *** For information only . sAmpio was extracted peer the NET Etraction procedure

(Title 225 ISri.or to anlay5i5 .ABBREVIATIONS

1) TR = Trace 2) ND !tone dctcoted 3) c s Lets than

4) > = Greater than 5 ) DNA = Does not apply 6) NS . Not Stated

7)K.* = icon-Certified result for indication purposer3 onl y

APPROVED.- 1. . .1L SIGNED ,mianager

liocketd"c S5 9L Analytical Cuero try

- ' ChemistRockeLdyne SSrL AnalYtical Chemistry

HDMSe0004668 8

DNA (Are a I Burn Pad for BCRA Part B Permit)

MAY Z:5 " 93 13 :35 1* LASER P . 3

C EM -i CAL ANAT.YS JX S

Log t+Imber900441 2

T0: Environmeoral Unit DEPT/( tUup

PROM : SSFL Analytical Chemiffitry, Roeketdyue Div .

BEFERENCB : LB 90 p 97, NB 1251, pages 161-174

543-000 PHONE : 992-581 $Rockwell International , D/539-169, ext . ff827

REPORT DATE : 05/25/90

SAIM LE INP0PMiATION FOR 900441 :

Sample 0aaerption : Soil . Westaide vad 1, distance 3 Pee t

Renueater : Beatrice Xephart2eguested Analynisa : Metals

Received: 04/23/90 at 10:16 :00Samp ler: N . I€s.lveraort Sampler ID4 ; 042390MH02sampled : 04/23/94

Sampic Time : 9:27 :00

A14ALYTia RESULT UNIT

W . LEVELCONTAMI NATE rye i'HOD/SOURC E

Antimony vox ND(0 01 mg/kg DNA 6010, SW-84 6

Arsenic **;a 0 .22 mg/kg DNA 7060 . SW-84 6

Barium** 38 meAg DNA 7060, SW-84 6

Eeryllium *** 0 .11 mg/k8 1)NA 6010 . BN-94 6

Cadmium *** 0 .37 mg/kg DNA 6010, SW-84 6

Chrumi um *** 0 .82 mg/kg DNA 6010 , SW-84 6

Cobalt xxx 1 .5 mg/kg DNA 6010, SW-846

Copper *** 3.6 mg/kg DNA 6010 , SW-84 6

Lead aw 14 mg/kg DNA . solo, SW-846

Mercury *** ND<U,U4v mg/kg DNA 7470, SW-84 6

Molybdenum * NDc0 .53 mg/kg DNA 6010 , SW-646

Nickel *** 0.73 mg/kg DNA 6010 , SW-846

Selenium xax NDr0.46 mg/kg DNA 6010, St-84 6

Silver *** ND<C .04 mg/kg DNA 6010 . SW-846

Thall ium mx* ND(n .n4 mg/kg DNA 6010, SW-846

Vanadium 0 . 47 mg/kg 6010 , SW-84 6

Zinc xxx 37 mg/kg DNA 6030, EW-84 6

--------------------

SPECIFICATION : DNA (Area I Burn Pui for &CRA Part B Permit )

SPECIAL NOTED : B . Kephart Bav . Eng. its charge of project . .Deter . rain n ,na rt contam . N

stated limite . WET oxtrart prior to ast alysis .

CO MENTS; *** For information only . Sample waz extracted per the WET Ext : tact

(Title 22 ) prior t.n analysis .A8ai2EVTATIONS

F71

t = Trace 2) ND = None do tceted

w Grantor than 5 ) DNA = Does roo r. apply 6) N

Mori-eertii' iad result for indication purpagzs onl y

APP€ZOVED: - h SIGNED

Rocketdyne SS `L Analytical Chemistry

Procedure

tf-sh thanNot Statod

z Jr ChemistRcu :Le1-.cLyue SSFL Analytical Chemiotr y

HDMSe00046689

P .490 13 :35 1* LASER.MAY 25

CHEMICAL ANALYSI SRE POR'i

Log NumbQi.900441 4

m Dtal Unit DEPT /GROUP : 543-000 PHONE : 932-5314O: >rnaron

FROM: 5SFL Analytical Chemistry, Rockt7tdyne Div . Rockwell Intornational , D/539-169, ext. 582

REPORT OATS : 05/25/00REFERENCE : LB 90 p 97 ; NB 2251, pages 161-174

SAMPLE INPOItMATION FOR 9004414

Samp l e y c rption : Soil, Ncrthside pad 1, distance - 1 Foot

Rcqucster . Beatrice 14phart

Requested Analysis: MItMt,

Received : 04/23/90 at l0 :I-5 :C 0

3nmp1*r : M. Ha. .l.verson Smiler IDs ; 042300MH03 Sanplo Time: 9, 29 .00

Sampled : 04/23/90 -

MAX. Y .FVE L

ANALYTE EESU LT UNIT CONTAMINATE KeUJOD/SOUac.

T

-

- - _ - - -Ant imorty N1}<O .011 aag/kg DNA 6010, Sw-246

Arsenic *** 0 .20 mg/kS DNA 7000, 3W-846

Barium ** :a 21 mg/kg DNA 1060 , SW-846

Beryllium *** 0.021 mg/kg DNA 6010, SW-846

Cadmium 0.1s mg/kg DNA 6010, sW-846

Chromium 0.15 mg/kg DNA 6010 , SR-846

Cobalt *** 1_2 Mac/kg DNA 6010 , SW-84 6

Copper *** 0.62 mg/ke DNA 6010 , SW-846

Lead * r.u 3 .1 mg/3:g DNA $010 , SW-846

Mercury.:,5iI ug/kg DNA 7470 , BY-846

Molybdenum NIX 0 .53 mg/k4 DNA 6010, Sw-846

Nickel *** 0 .46 mg/ke DNA 6010 . SW--840

Selenium NDt0,4A mg/kg DNA 6010, SW-846

Silver *** NDCO.04 gag/kg DNA 6alfi, SW-84 6

Thallium 92% NDC0 . fly. jag/kg DNA 6010 , SW-846

Vanadium 0.69 mg/kg DNA 6010 , SW-846

Zinc * 6 .3 mg/kg DHA 6010, SW-846

------------------

SPECIFICATION : DNA (Ar?vt I Brhrri Peed for BONA Part B Permit )

9PECIAE NOTES : B, Kephart Env. Eng . inoharga of project . Dater . rain runoff contain . N

stated limits . WET extract prior to analy6is .

COMMENTS : *** For information only . Sample was extracted pPr WET Extraction Procedur e

(Title 22) prier Lu analysis .ABBREU .d'I'1O S

1) 'fR = Trace 2) Nt = Mane detected 3 }

4} > = Greater th4Ye 5) DNA = DoeA not apply

7) *

4

* Ncrn-rurtified result for ind= cation 'purBones on3y

6} N

__)

AFPROVEl) : -

$ocketdyn

managerSFL Anslyticol ChcmintrY

Less thisNot States[

SIGNED : ~f.~Chetaaat

Rcck®tdyne 8.9Fr. Arauiytical Chesi6tr y

HDMSe00046690

MAY 2S '90 19:36 1* LASER P . S

CHEMICAL ANALY8I sREPOkt`1'

ELFERENCEt L 9 90 p 87 ; NB 1251 , Da: es 161-174 Rkl'OR DATE : 05/25/90FROM. : SSFL Analytical f1hemistry, Rockctd yne L)iv . Rocksfell international , D/533189, ext. 582 7

Log Number000441 6

T0 : Rnvirommdntal limit DEPT/GROUP : 543-000 PHONE 392-5314

SAMPLE INFOEMATtnN FOR 9004415Sample Desorption : Soil, Northsida ' pad 2, distance = I Foot

Requester : Beatrice Kepkxtrt.Ret ur~Led Analyfi s fietals

Reecivcd : 04/23/90 at 10 :15 : 0nSa PIr±L : bf . Balveroon Sampler ID# 042320,+4104Sampled: 04/23/90

3awy1e Time : 9 :32 :00

MAX . LEVE LANALYTE RESULT UNIT CONTAMINATE METHOD/ SOURCE------------------------

Antimony *** ND<0.01Arsenic *** 0.49Barium *** 30Eoryllium u4x 0 .042cadmium *** 0.40Chromium *** 2.1Cobalt ** 2 .1Cogger *** 5 .2Lead *;* 3.5mercury a*x '45 =.

Molybdenum **4 00, 53Nickel 9** 3.5Selenium ** ND<0 .46Silver *** ND(0.010Pha1l ium ** k ND<0 .04Vanadium *** 1 .0zinc *** 42

----------- --------------mg/kg DNA 6010, SW-846mg/kg DNA r 7060, SW-846

mg/4 DNA 7060, 39.846mg/kg DNA 6010 , SW-246mg/kg DNA 6010 , Sol-046mg/kg DNA .6010, Sw-846mg/kg DNA - 6010 . SW-846mg/kg DNA 6010, SW-846mg/lcg DNA 6010 , SW-846mg/kg DNA 7470 , SW-846

mg/kg DNA 6010 , $W-846mg/kg DNA 6010, SW-846mg/kg DNA 6010 , SW-846mg/k€I DNA 6010, SW-846mg/kg DNA 6010, SW-846mg/kg DNA 6010, SW-846mg/kg DNA 6010, SW-846

SPECIFICATION : DNA (Area. I Burn Pad for RCRA Part 8 Permit )SPECIAL NOTES D . Kephart Env. Eng . in ch .rke of project . Deter. rain runoff contem . No

stated 1iiitH. WET extract prior to analysin .CONNEN'.`t$ : *x* For Information Only. Sample waa extracted por the WET Procedure ('1'itIo 22)

Dr•ior to anatysaii .

ADDREVI .1) `f R - = Trace 2 ) ND = None datectad 2 } < Less than4) = Greater than 5) DNA = Does not apply 6) N .S, Not at 'tea7) eta a Non-certified result for indication purposes onl y

Rooketdyne BSPL Analytical Chemistry R~c :ic~rdyne SSFL Analytical Lh,)mistry

ANi4OVED : _ ~~ w! 1r~^-.-- SYrtaF.t1'

Manager

HDMSe00046691

MAY 25 '90 13 :36 I . LASE R

Itoeketdyno SSFL Analytical Cii i istty Rucketdyne SS1'L Analytical Chemistry

CHEM ICAL ANAL.-Y'S X SREPORT

r~ i r l Or,; t AEPT/GROUP: 542-000oTO E 'v' P90-4E : 392-531 4nm trI DI139-109 t 5$2 7

*)AM- SBFL Analytical Chemistry kocketdyno Date . &ocicwell Internxr.unn cx

REFERENM! Y.A 9d p 91; N8 1201, -pages 101-174 RbP{7I{1 MAlt . : 05/25/90

SAMPLE INFORMATION FOR 90D441 6

Sample Descrption; Soil, Eaataide pad 2 dietanoc = 1 root

Regx:esetar : Beatrice Kephart, 0

Requested Ana1Yeia : t4etalsReceived: 64/20/90 aL 10 :15 :0 0

Sampler : M1. 11al'versonSampled! 04/23/90

Sampler iU# : 0423904 05 ample Time: 9 :34 : 0

MAX . LEVEL

ANALYTE RESULT ; uRIT cONTAMINATF Mk7HOD/SOUR.CF

- - - - - - - - - - - - - - - - - - - - - - - - - - - - - -- - - - - - - - - - - - - - ----------- ---------------------- -

Antimony *x* W1X0 .01 mgfkg DNA 6010, SW-84 6

Arsenic **x 0 .45 mgA--o DNA 7060 . SW-84 6

Buriuii * .** 25 mG/Kg DNA 7060, SW-846

Bary11ium *xt 0 .063 mg/kg DNA 6010, SCI-84 6

Cadmium *x* 0.46 mg/kg DNA 6010, SW-84 6

Ghromium *A* 1 .1 mg/ke DNA 6010, SW-846

Cobalt 4* 1.4 rms/kg DNA 6010, SW-84 6

Copper axx 3.0 mg/kg DNA 6010, SW-846

Lead *Et* 3 .1 mg/kg DNA 6010, 3W-84 6

Mercury v** 1 79 mg/kg DNA 1410, SW-846

Molybdenum ND<O .53 mg/4 DNA 6010, SW-846

Nickel *x* 2.4 , mg/kg DNA 6010, SW-84 6

selenium * ND<0.46 [ ms/k9 DNA 6010, SW-946

Silver x** 0 .46 mg/kg DNA 6010, SW-84 6

Thallium ND<4 .044 mg/kg DNA 6010, SW-94 6

Vanadium **ffi 1.1 mg/kg DNA 8010, SW-846

Zinc *** 25 mglkg DNA 6010 , SW-846

--------------

(Tit1. 22) prior to analyeie .* ABBREVIATIONS

1) TR = Trace 3) RD None ttetoored

4) ) = Gre, AT.er than 5) DNA = Dopy not apulY

7) t** = .4on-cortified result for indication purposes onl y

SPECIAL, W. TFS : B. Kephart Env . Eng . in charge of project. Deter . rain runoff tontam . No

steed limits . WET extract prior to analysi s

COM.'.ik: NTS : ~d r* or Information Only . 4*rnp 1 a was extracted per bh WET extraction procedur e

SPECIFICATION : DNA (Area I Burn Pad far RCRA Pert B Permit )

APPPOVfD :

P. 6

s) ( , Li,azi6) N.B. = Not Stated

sTCNFD: ~ .

Manager Chemist

HDMSe00046692

MH r' c:5 '90 13:37 1* LRSER

CHEMI CAL ANALYS XEFlPtDRT

Log NumberSCIO441 1

TO: EnvironmentalUnit DEPT/GROUP. 543-000 PHDNE s92-531 4Fl't0M : 35FL Analytic-ml Chemistry , RocketdynoDiv . Roekaeil Intcrf4tional, D/539-169, ext. 5827RL ENCE: to 90 57 Np , B 1251 , pages 161-174 REPORT DATE: 05/25/90

SAMPLE INFORMATION FOR 90044178ansp3a- D* crrption : Sail , Wectsi.de pad 2, diotttt]o = 1 Foot

Requester : Deatrice Xephat-tRQtlltested Analysis : Mot&ls

Received ; 04/23190 at 10 .15 :00Sampler : M. Halvorson Samp.lcr ID# : 042390M1i06Sampled* 04/23!94

Sample Time : s :36 .0000

AWALYTR----------------------

Resuur UNITNAX LEVELCONTAMINATE METHOD/SOURCE

Antimony 44# NU<U .U1 mg/kg DNA 6010 SW-846Arsenic 0.44 mg/lcg DNA,

7060 SW-846Barium 44* 28 mg/kg DNA,

7060 SW-846Bcryflium *4 0 .062 mag/kg DNA

,SW-94 6601 0Cadmium #4 0.43 mg/kg DNA "

,6010 SW-846Chromium 0.69 mg/kg DNA

,6010 SW-84 6

Cobalt 4** 1 .6 tag/kg DNA .,

0010, SW-84 6Copper *** 2.7 m8/kg D3~A SW-84 66010L6ad a44

`2.7 Wks DNA

,6010, SW-946

Mercury ;**Y Nl)fl, Q4 mg/kg,

DNA 71770, SW-84 6Molybdenum N<0,53 mx/kg DNA 6010 Sid-948Nickel *** 1 .9 mg/kg DNA

,6010, BW-846Selenium **s NDr0.65 mg/kg DNA 6010, 314-194 6Silver *** MD<0 .04 mg/1{g I)NA 6010, 6W-84 6Thallium >i ND<0 .04 me/kg DNA 6010 , SW-846Vanadium ND< 0 .51 m /k DN AZinc *** 21

g gmg /kg DNA

6010, SW-8466010 , SW-846

----------------------- -------------

SPECISIC93'1oN : DNe4 Area I Burn Pad for RC11A Part B Permit )SPECIAL NOTES : B. Kephart. ISnv . Eng , in charge of project . Deter , rein runoff contaz .st t d la e imits . WWX extract prior to u ,3ysis .COMMENTS ; *** For Iufarmtstion only, sttmDle was extracted per

(Title 22) prior to analysis .ARRRRvIA

the WET extraction proccdur c

.ViLV, -11 TR = raa 2) ND None dotceted 3) c = Less than4) 5 = Greater than 5 ) DNA Dues not apply 6 ) N .S . = Not Stated7j # Non-certified resul t for indication purposee only

APPROVED - w SIGNED:Manager

Raeketdyne 3;FL Analytical CIre,.m i s;.2ry Eteclr.otdyne SSFL Aailytica1 Chemistry

HDMSe00046693