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VI. DAFTAR PUSTAKA
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88
Lampiran 1. Metode ekstraksi sodium alginat dari rumput laut.
Rumput laut kering
Perendaman dalam HCl 1% 1 jam (rumput laut: HCl 1: 30 b/v)
Pencucian dengan air bersih sampai pH netral
Ekstraksi dengan larutan Na2CO3 2% sebanyak 1:30 (w/v),
pada suhu 600C - 700C, selama 60 menit, digiling dan ekstraksi dilanjutkan selama 60 menit
Penyaringan hasil ekstraksi disaring dengan
vibrator 150- mesh
Pemucatan ditambahkan NaOCl 4% volume filtrat selama 30 menit
Pengendapan asam alginat filtrat di tambahkan HCl 10% sampai pH 2.8 3.2, endapan asam alginat dipisahkan dan dicuci bersih
Konversi menjadi natrium alginat dititrasi dengan Na2CO3 10% sampai pH 7
Pemisahan natrium alginat filtrat dituangkan sedikit demi sedikit ke dalam Isopropil alkohol (1:2 v/v)
sambil diaduk dan dibiarkan selama 30 menit
Pengeringan dan penggilingan serat alginat dikeringkan dibawah sinar matahari selama + 12 jam,
sampai kadar air 12%
digiling dengan ukuran 60 mesh
bubuk natrium alginat
89
Lampiran 2. Uji statistik bahan baku alginat
ANOVA
85.889 3 28.630 248.557 .000.921 8 .115
86.810 112719.711 3 906.570 11607.815 .000
.625 8 .0782720.336 11
417.769 3 139.256 1622.405 .000.687 8 .086
418.456 111.337 3 .446 59.208 .000
.060 8 .0081.397 11
.445 3 .148 30.402 .000
.039 8 .005
.484 11
.097 3 .032 6.175 .018
.042 8 .005
.138 11
.665 3 .222 26.223 .000
.068 8 .008
.733 11
Between GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotal
Kadar air
Kadar Abu
Bahan Tdk larut air
Residu Pb
Residu Arsen
Kadar Ca
M/G
Sum ofSquares df Mean Square F Sig.
Post Hoc Tests (0 = Sargassum sp, 1 = Turbinaria sp. 2 = Komersial Sigma 3 = komersial toko)
Multiple Comparisons
Dependent Variable: Kadar airLSD
-.5300 .27711 .092 -1.1690 .10906.2200* .27711 .000 5.5810 6.85902.6733* .27711 .000 2.0343 3.3123
.5300 .27711 .092 -.1090 1.16906.7500* .27711 .000 6.1110 7.38903.2033* .27711 .000 2.5643 3.8423
-6.2200* .27711 .000 -6.8590 -5.5810-6.7500* .27711 .000 -7.3890 -6.1110-3.5467* .27711 .000 -4.1857 -2.9077-2.6733* .27711 .000 -3.3123 -2.0343-3.2033* .27711 .000 -3.8423 -2.56433.5467* .27711 .000 2.9077 4.1857
(J) Jenis Alginat1.002.003.00.002.003.00.001.003.00.001.002.00
(I) Jenis Alginat.00
1.00
2.00
3.00
MeanDifference
(I-J) Std. Error Sig. Lower Bound Upper Bound95% Confidence Interval
The mean difference is significant at the .05 level.*.
90
Multiple Comparisons
Dependent Variable: Kadar AbuLSD
-1.7867* .22818 .000 -2.3129 -1.2605-3.3567* .22818 .000 -3.8829 -2.8305
-36.3733* .22818 .000 -36.8995 -35.84711.7867* .22818 .000 1.2605 2.3129
-1.5700* .22818 .000 -2.0962 -1.0438-34.5867* .22818 .000 -35.1129 -34.0605
3.3567* .22818 .000 2.8305 3.88291.5700* .22818 .000 1.0438 2.0962
-33.0167* .22818 .000 -33.5429 -32.490536.3733* .22818 .000 35.8471 36.899534.5867* .22818 .000 34.0605 35.112933.0167* .22818 .000 32.4905 33.5429
(J) Jenis Alginat1.002.003.00.002.003.00.001.003.00.001.002.00
(I) Jenis Alginat.00
1.00
2.00
3.00
MeanDifference
(I-J) Std. Error Sig. Lower Bound Upper Bound95% Confidence Interval
The mean difference is significant at the .05 level.*.
Multiple Comparisons
Dependent Variable: Bahan Tdk larut airLSD
-2.1567* .23921 .000 -2.7083 -1.605010.5933* .23921 .000 10.0417 11.145010.6533* .23921 .000 10.1017 11.2050
2.1567* .23921 .000 1.6050 2.708312.7500* .23921 .000 12.1984 13.301612.8100* .23921 .000 12.2584 13.3616
-10.5933* .23921 .000 -11.1450 -10.0417-12.7500* .23921 .000 -13.3016 -12.1984
.0600 .23921 .808 -.4916 .6116-10.6533* .23921 .000 -11.2050 -10.1017-12.8100* .23921 .000 -13.3616 -12.2584
-.0600 .23921 .808 -.6116 .4916
(J) Jenis Alginat1.002.003.00.002.003.00.001.003.00.001.002.00
(I) Jenis Alginat.00
1.00
2.00
3.00
MeanDifference
(I-J) Std. Error Sig. Lower Bound Upper Bound95% Confidence Interval
The mean difference is significant at the .05 level.*.
91
Multiple Comparisons
Dependent Variable: Residu PbLSD
-.2400* .07083 .010 -.4033 -.0767.5567* .07083 .000 .3933 .7200
-.2800* .07083 .004 -.4433 -.1167.2400* .07083 .010 .0767 .4033.7967* .07083 .000 .6333 .9600
-.0400 .07083 .588 -.2033 .1233-.5567* .07083 .000 -.7200 -.3933-.7967* .07083 .000 -.9600 -.6333-.8367* .07083 .000 -1.0000 -.6733.2800* .07083 .004 .1167 .4433.0400 .07083 .588 -.1233 .2033.8367* .07083 .000 .6733 1.0000
(J) Jenis Alginat1.002.003.00.002.003.00.001.003.00.001.002.00
(I) Jenis Alginat.00
1.00
2.00
3.00
MeanDifference
(I-J) Std. Error Sig. Lower Bound Upper Bound95% Confidence Interval
The mean difference is significant at the .05 level.*.
Multiple Comparisons
Dependent Variable: Residu ArsenLSD
-.3400* .05701 .000 -.4715 -.2085.1367* .05701 .043 .0052 .2681
-.2600* .05701 .002 -.3915 -.1285.3400* .05701 .000 .2085 .4715.4767* .05701 .000 .3452 .6081.0800 .05701 .198 -.0515 .2115
-.1367* .05701 .043 -.2681 -.0052-.4767* .05701 .000 -.6081 -.3452-.3967* .05701 .000 -.5281 -.2652.2600* .05701 .002 .1285 .3915
-.0800 .05701 .198 -.2115 .0515.3967* .05701 .000 .2652 .5281
(J) Jenis Alginat1.002.003.00.002.003.00.001.003.00.001.002.00
(I) Jenis Alginat.00
1.00
2.00
3.00
MeanDifference
(I-J) Std. Error Sig. Lower Bound Upper Bound95% Confidence Interval
The mean difference is significant at the .05 level.*.
92
Multiple Comparisons
Dependent Variable: Kadar CaLSD
.0533 .05897 .392 -.0827 .1893
.0733 .05897 .249 -.0627 .2093
.2400* .05897 .004 .1040 .3760-.0533 .05897 .392 -.1893 .0827.0200 .05897 .743 -.1160 .1560.1867* .05897 .013 .0507 .3227
-.0733 .05897 .249 -.2093 .0627-.0200 .05897 .743 -.1560 .1160.1667* .05897 .022 .0307 .3027
-.2400* .05897 .004 -.3760 -.1040-.1867* .05897 .013 -.3227 -.0507-.1667* .05897 .022 -.3027 -.0307
(J) Jenis Alginat1.002.003.00.002.003.00.001.003.00.001.002.00
(I) Jenis Alginat.00
1.00
2.00
3.00
MeanDifference
(I-J) Std. Error Sig. Lower Bound Upper Bound95% Confidence Interval
The mean difference is significant at the .05 level.*.
Multiple Comparisons
Dependent Variable: M/GLSD
.2367* .07509 .014 .0635 .4098-.4133* .07509 .001 -.5865 -.2402-.1433 .07509 .093 -.3165 .0298-.2367* .07509 .014 -.4098 -.0635-.6500* .07509 .000 -.8232 -.4768-.3800* .07509 .001 -.5532 -.2068.4133* .07509 .001 .2402 .5865.6500* .07509 .000 .4768 .8232.2700* .07509 .007 .0968 .4432.1433 .07509 .093 -.0298 .3165.3800* .07509 .001 .2068 .5532
-.2700* .07509 .007 -.4432 -.0968
(J) Jenis Alginat1.002.003.00.002.003.00.001.003.00.001.002.00
(I) Jenis Alginat.00
1.00
2.00
3.00
MeanDifference
(I-J) Std. Error Sig. Lower Bound Upper Bound95% Confidence Interval
The mean difference is significant at the .05 level.*.
93
Lampiran 3. Statistik Pengaruh CaCO3 terhadap karakteristik gel alginat
Between-Subjects Factors
272727
999999999
1.002.003.00
jenis alginat
2.505.007.5010.0012.5015.0020.0025.0030.00
konsentrasiCaCO3
N
Tests of Between-Subjects Effects
Dependent Variable: keteguhan gel
98881.105a 26 3803.119 1999.270 .000304754.295 1 304754.295 160206.9 .000
501.722 2 250.861 131.876 .00096856.247 8 12107.031 6364.570 .000
1523.135 16 95.196 50.044 .000102.722 54 1.902
403738.122 8198983.826 80
SourceCorrected ModelInterceptVAR00005VAR00001VAR00005 * VAR00001ErrorTotalCorrected Total
Type I Sumof Squares df Mean Square F Sig.
R Squared = .999 (Adjusted R Squared = .998)a.
Post Hoc Tests keteguhan gel
Duncana,b
27 59.411127 59.751527 64.8526
.369 1.000
jenis alginat2.003.001.00Sig.
N 1 2Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = 1.902.
Uses Harmonic Mean Sample Size = 27.000.a.
Alpha = .05.b.
Keterangan: 1 = Sargassum sp. 2 = Turbinaria sp. 3 = Komersial Sigma
94
jenis alginat * konsentrasi CaCO3
Dependent Variable: keteguhan gel
.000 .796 -1.596 1.596-1.78E-15 .796 -1.596 1.596
60.540 .796 58.944 62.13676.190 .796 74.594 77.78681.970 .796 80.374 83.56688.093 .796 86.497 89.69089.800 .796 88.204 91.39692.520 .796 90.924 94.11694.560 .796 92.964 96.156
1.776E-15 .796 -1.596 1.5961.776E-15 .796 -1.596 1.596
40.820 .796 39.224 42.41659.860 .796 58.264 61.45672.110 .796 70.514 73.70682.990 .796 81.394 84.58690.140 .796 88.544 91.73692.860 .796 91.264 94.45695.920 .796 94.324 97.516
-1.42E-14 .796 -1.596 1.596-1.42E-14 .796 -1.596 1.596
61.903 .796 60.307 63.50071.777 .796 70.180 73.37372.797 .796 71.200 74.39380.270 .796 78.674 81.86680.950 .796 79.354 82.54683.670 .796 82.074 85.26686.397 .796 84.800 87.993
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.00
jenis alginat1.00
2.00
3.00
Mean Std. Error Lower Bound Upper Bound95% Confidence Interval
82
keteguhan gel
Duncana,b
9 .00009 .00009 54.42119 69.27569 75.62569 83.78449 86.96339 89.68339 92.2922
1.000 1.000 1.000 1.000 1.000 1.000 1.000 1.000
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.00Sig.
N 1 2 3 4 5 6 7 8Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = 1.902.
Uses Harmonic Mean Sample Size = 9.000.a.
Alpha = .05.b.
Tests of Between-Subjects Effects
Dependent Variable: kekuatan gel
1237975.5a 26 47614.442 490.490 .0001369888.2 1 1369888.178 14111.603 .000
1405.342 2 702.671 7.238 .0021192779.2 8 149097.400 1535.894 .00043790.949 16 2736.934 28.194 .000
5242.067 54 97.0752613105.7 811243217.6 80
SourceCorrected ModelInterceptVAR00005VAR00001VAR00005 * VAR00001ErrorTotalCorrected Total
Type I Sumof Squares df Mean Square F Sig.
R Squared = .996 (Adjusted R Squared = .994)a.
82
jenis alginat * konsentrasi CaCO3
Dependent Variable: kekuatan gel
-9.95E-14 5.688 -11.405 11.405-4.26E-14 5.688 -11.405 11.405-2.84E-14 5.688 -11.405 11.405
53.367 5.688 41.962 64.77177.000 5.688 65.595 88.405
151.333 5.688 139.929 162.738223.800 5.688 212.395 235.205289.533 5.688 278.129 300.938349.500 5.688 338.095 360.905
-4.26E-14 5.688 -11.405 11.405.000 5.688 -11.405 11.405
4.263E-14 5.688 -11.405 11.40538.900 5.688 27.495 50.30547.233 5.688 35.829 58.638
111.533 5.688 100.129 122.938263.033 5.688 251.629 274.438315.300 5.688 303.895 326.705367.300 5.688 355.895 378.705
-5.68E-14 5.688 -11.405 11.405.000 5.688 -11.405 11.405
39.267 5.688 27.862 50.671104.333 5.688 92.929 115.738130.467 5.688 119.062 141.871172.500 5.688 161.095 183.905228.900 5.688 217.495 240.305266.400 5.688 254.995 277.805281.567 5.688 270.162 292.971
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.00
jenis alginat1.00
2.00
3.00
Mean Std. Error Lower Bound Upper Bound95% Confidence Interval
kekuatan gel
Duncana,b
27 127.033327 127.170427 135.9370
.959 1.000
jenis alginat2.001.003.00Sig.
N 1 2Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = 97.075.
Uses Harmonic Mean Sample Size = 27.000.a.
Alpha = .05.b.
Keterangan: 1 = Sargassum sp. 2 = Turbinaria sp. 3 = Komersial Sigma
82
kekuatan gel
Duncana,b
9 .00009 .00009 13.08899 65.53339 84.90009 145.12229 238.57789 290.41119 332.7889
1.000 1.000 1.000 1.000 1.000 1.000 1.000 1.000
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.00Sig.
N 1 2 3 4 5 6 7 8Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = 97.075.
Uses Harmonic Mean Sample Size = 9.000.a.
Alpha = .05.b.
Tests of Between-Subjects Effects
Dependent Variable: elastis
1927.660a 26 74.141 261.872 .0002707.930 1 2707.930 9564.653 .000
96.761 2 48.381 170.884 .0001766.963 8 220.870 780.134 .000
63.936 16 3.996 14.114 .00015.288 54 .283
4650.879 811942.948 80
SourceCorrected ModelInterceptVAR00005VAR00001VAR00005 * VAR00001ErrorTotalCorrected Total
Type I Sumof Squares df Mean Square F Sig.
R Squared = .992 (Adjusted R Squared = .988)a.
82
jenis alginat * konsentrasi CaCO3
Dependent Variable: elastis
-1.33E-15 .307 -.616 .6164.441E-16 .307 -.616 .6161.832E-15 .307 -.616 .616
3.677 .307 3.061 4.2934.733 .307 4.117 5.3498.207 .307 7.591 8.8239.760 .307 9.144 10.376
10.957 .307 10.341 11.57311.557 .307 10.941 12.173
-4.44E-15 .307 -.616 .616-2.22E-15 .307 -.616 .616-1.80E-15 .307 -.616 .616
1.310 .307 .694 1.9262.110 .307 1.494 2.7266.070 .307 5.454 6.686
10.450 .307 9.834 11.06611.000 .307 10.384 11.61610.937 .307 10.321 11.553
.000 .307 -.616 .6161.776E-15 .307 -.616 .616
2.313 .307 1.697 2.9296.970 .307 6.354 7.5868.107 .307 7.491 8.723
10.260 .307 9.644 10.87611.610 .307 10.994 12.22612.677 .307 12.061 13.29313.410 .307 12.794 14.026
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.00
jenis alginat1.00
2.00
3.00
Mean Std. Error Lower Bound Upper Bound95% Confidence Interval
elastis
Duncana,b
27 4.653027 5.432227 7.2607
1.000 1.000 1.000
jenis alginat2.001.003.00Sig.
N 1 2 3Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = .283.
Uses Harmonic Mean Sample Size = 27.000.a.
Alpha = .05.b.
Keterangan: 1 = Sargassum sp. 2 = Turbinaria sp. 3 = Komersial Sigma
82
elastis
Duncana,b
9 .00009 .00009 .77119 3.98569 4.98339 8.17899 10.60679 11.54449 11.9678
1.000 1.000 1.000 1.000 1.000 1.000 .097
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.00Sig.
N 1 2 3 4 5 6 7Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = .283.
Uses Harmonic Mean Sample Size = 9.000.a.
Alpha = .05.b.
Tests of Between-Subjects Effects
Dependent Variable: mod rig
7567.160a 26 291.045 446.760 .00010665.840 1 10665.840 16372.291 .000
55.021 2 27.511 42.229 .0007118.798 8 889.850 1365.938 .000
393.341 16 24.584 37.737 .00035.179 54 .651
18268.179 817602.338 80
SourceCorrected ModelInterceptVAR00005VAR00001VAR00005 * VAR00001ErrorTotalCorrected Total
Type I Sumof Squares df Mean Square F Sig.
R Squared = .995 (Adjusted R Squared = .993)a.
82
jenis alginat * konsentrasi CaCO3
Dependent Variable: mod rig
5.329E-15 .466 -.934 .934-3.55E-15 .466 -.934 .934-5.33E-15 .466 -.934 .934
6.550 .466 5.616 7.4849.667 .466 8.732 10.601
14.683 .466 13.749 15.61819.773 .466 18.839 20.70823.727 .466 22.792 24.66127.610 .466 26.676 28.544
1.066E-14 .466 -.934 .9341.776E-15 .466 -.934 .9345.329E-15 .466 -.934 .934
8.087 .466 7.152 9.02111.380 .466 10.446 12.31413.310 .466 12.376 14.24422.270 .466 21.336 23.20427.137 .466 26.202 28.07130.743 .466 29.809 31.678
3.553E-15 .466 -.934 .934-7.11E-15 .466 -.934 .934
3.643 .466 2.709 4.57810.590 .466 9.656 11.52412.367 .466 11.432 13.30113.833 .466 12.899 14.76817.097 .466 16.162 18.03118.607 .466 17.672 19.54118.753 .466 17.819 19.688
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.00
jenis alginat1.00
2.00
3.00
Mean Std. Error Lower Bound Upper Bound95% Confidence Interval
mod rig
Duncana,b
27 10.543327 11.334427 12.5474
1.000 1.000 1.000
jenis alginat3.001.002.00Sig.
N 1 2 3Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = .651.
Uses Harmonic Mean Sample Size = 27.000.a.
Alpha = .05.b.
82
mod rig
Duncana,b
9 .00009 .00009 1.21449 8.40899 11.13789 13.94229 19.71339 23.15679 25.7022
1.000 1.000 1.000 1.000 1.000 1.000 1.000 1.000
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.00Sig.
N 1 2 3 4 5 6 7 8Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = .651.
Uses Harmonic Mean Sample Size = 9.000.a.
Alpha = .05.b.
Tests of Between-Subjects Effects
Dependent Variable: sineresis
922.910a 26 35.497 97.244 .0001783.345 1 1783.345 4885.539 .000
164.737 2 82.369 225.652 .000663.106 8 82.888 227.075 .000
95.066 16 5.942 16.277 .00019.711 54 .365
2725.966 81942.621 80
SourceCorrected ModelInterceptVAR00005VAR00001VAR00005 * VAR00001ErrorTotalCorrected Total
Type I Sumof Squares df Mean Square F Sig.
R Squared = .979 (Adjusted R Squared = .969)a.
182
jenis alginat * konsentrasi CaCO3
Dependent Variable: sineresis
.000 .349 -.699 .6991.776E-15 .349 -.699 .699
4.962 .349 4.263 5.6624.897 .349 4.197 5.5965.667 .349 4.967 6.3666.180 .349 5.481 6.8797.950 .349 7.251 8.6498.400 .349 7.701 9.0998.523 .349 7.824 9.223
3.553E-15 .349 -.699 .6993.553E-15 .349 -.699 .699
4.100 .349 3.401 4.7995.233 .349 4.534 5.9335.683 .349 4.984 6.3838.443 .349 7.744 9.143
10.170 .349 9.471 10.86910.763 .349 10.064 11.46310.923 .349 10.224 11.623
-8.88E-16 .349 -.699 .699-8.88E-16 .349 -.699 .699
2.663 .349 1.964 3.3633.053 .349 2.354 3.7533.173 .349 2.474 3.8733.447 .349 2.747 4.1463.870 .349 3.171 4.5693.997 .349 3.297 4.6964.590 .349 3.891 5.289
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.002.505.007.5010.0012.5015.0020.0025.0030.00
jenis alginat1.00
2.00
3.00
Mean Std. Error Lower Bound Upper Bound95% Confidence Interval
sineresis
Duncana,b
27 2.754827 5.175427 6.1463
1.000 1.000 1.000
jenis alginat3.001.002.00Sig.
N 1 2 3Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = .365.
Uses Harmonic Mean Sample Size = 27.000.a.
Alpha = .05.b.
Keterangan: 1 = Sargassum sp. 2 = Turbinaria sp. 3 = Komersial Sigma
183
sineresis
Duncana,b
9 .00009 .00009 3.90869 4.3944 4.39449 4.84119 6.02339 7.33009 7.7200 7.72009 8.0122
1.000 .094 .123 1.000 .177 .309
konsentrasi CaCO32.505.007.5010.0012.5015.0020.0025.0030.00Sig.
N 1 2 3 4 5 6Subset
Means for groups in homogeneous subsets are displayed.Based on Type I Sum of SquaresThe error term is Mean Square(Error) = .365.
Uses Harmonic Mean Sample Size = 9.000.a.
Alpha = .05.b.
184
Lampiran 4. Uji statistik pengaruh penambaha CaCO3 terhadap karakteristik Viskositas
4.1 Pengaruh penambaha CaCO3 terhadap peningkatan viskositas laruan alginat
ANOVA
159228.3 3 53076.111 660.014 .000643.333 8 80.417
159871.7 1139547.583 3 13182.528 249.119 .000
423.333 8 52.91739970.917 11
Between GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotal
Sargassum sp
Turbinaria sp
Sum ofSquares df Mean Square F Sig.
Post Hoc Tests
Sargassum sp
3 102.66673 229.66673 274.00003 425.0000
1.000 1.000 1.000 1.000
konsentrasi karbonat.002.503.504.50Sig.
DuncanaN 1 2 3 4
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Turbinaria sp
3 66.33333 102.00003 111.33333 220.0000
1.000 .155 1.000
konsentrasi karbonat.002.503.504.50Sig.
DuncanaN 1 2 3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
ANOVA
Komersial Sigma
1141154 2 570577.000 1730.769 .0001978.000 6 329.6671143132 8
Between GroupsWithin GroupsTotal
Sum ofSquares df Mean Square F Sig.
185
Post Hoc Tests
Komersial Sigma
3 334.00003 617.00003 1190.0000
1.000 1.000 1.000
konsentrasi karbonat.002.503.50Sig.
DuncanaN 1 2 3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
4.2 Pengaruh penambahan CaCO3 terhadap stabilitas viskositas alginat
ANOVA
Penurunan Viskositas
1596.271 5 319.254 210.198 .00018.226 12 1.519
1614.497 17
Between GroupsWithin GroupsTotal
Sum ofSquares df Mean Square F Sig.
Post Hoc Tests
Penurunan Viskositas
Duncana
3 52.68383 63.23263 71.77683 75.60953 77.32663 79.9090
1.000 1.000 1.000 .114 1.000
Perlakuan4.002.006.005.001.003.00Sig.
N 1 2 3 4 5Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Keterangan: 1 = Sargassum sp tanpa Ca, 2 = Sargassum sp dengan Ca, 3 = Turbinaria sp tanpa Ca, 4 = Turbinaria sp dengan Ca, 5 = Komersial Sigma tanpa Ca, 6 = Komersial Sigma dengan Ca
186
Lampiran 5. Uji statistik penambahan LBG terhadap karakteristik gel alginat 9.1 keteguhan gel
ANOVA
49.991 5 9.998 4.796 .01225.017 12 2.08575.008 1744.715 5 8.943 4.417 .01624.295 12 2.02569.011 17
6.016 5 1.203 .096 .991149.938 12 12.495155.954 17
Between GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotal
Sargassum sp
Turbinaria sp
Komersial Sigma
Sum ofSquares df Mean Square F Sig.
Post Hoc Tests
Sargassum sp
3 85.71433 88.43543 88.43543 88.70753 90.47623 90.8163
1.000 .090
Konsentrasi LBG.0010.0020.0030.0040.0050.00Sig.
DuncanaN 1 2
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Turbinaria sp
3 89.11563 92.51703 92.51703 93.19733 93.53743 93.8776
1.000 .305
Konsentrasi LBG.0010.0020.0030.0040.0050.00Sig.
DuncanaN 1 2
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
187
Komersial Sigma
3 85.03403 85.03403 85.37413 85.71433 85.71433 86.7347
.601
Konsentrasi LBG40.0050.0020.00.0010.0030.00Sig.
DuncanaN 1
Subsetfor alpha
= .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
9.2 kekuatan gel
ANOVA
817.036 5 163.407 .360 .8665452.440 12 454.3706269.476 175574.964 5 1114.993 1.341 .3129977.360 12 831.447
15552.324 1715857.876 5 3171.575 20.956 .000
1816.127 12 151.34417674.003 17
Between GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotal
Sargassum sp
Turbinaria sp
Komersial Sigma
Sum ofSquares df Mean Square F Sig.
Sargassum sp
3 223.20003 225.96673 234.50003 234.76673 238.20003 242.7333
.328
Konsentrasi LBG50.0040.00.0020.0010.0030.00Sig.
DuncanaN 1
Subsetfor alpha
= .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
188
Turbinaria sp
3 162.00003 175.1000 175.10003 179.4333 179.43333 182.2333 182.23333 190.7000 190.70003 219.0667
.287 .114
Konsentrasi LBG.0050.0040.0010.0020.0030.00Sig.
DuncanaN 1 2
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Komersial Sigma
3 93.56673 106.0333 106.03333 107.4000 107.40003 110.2667 110.26673 126.70003 184.0667
.149 .080 1.000
Konsentrasi LBG50.0040.0020.0030.0010.00.00Sig.
DuncanaN 1 2 3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
9.3 elastisitas
ANOVA
.558 5 .112 1.345 .311
.995 12 .0831.553 174.703 5 .941 4.976 .0112.268 12 .1896.971 17
31.682 5 6.336 18.401 .0004.132 12 .344
35.814 17
Between GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotal
Sargassum sp
Turbinaria sp
Komersial Sigma
Sum ofSquares df Mean Square F Sig.
189
Sargassum sp
3 9.96933 10.09433 10.10573 10.27773 10.28133 10.5167
.057
Konsentrasi LBG.0050.0010.0020.0030.0040.00Sig.
DuncanaN 1
Subsetfor alpha
= .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Turbinaria sp
3 7.39973 8.25533 8.3163 8.31633 8.3993 8.39933 8.5677 8.56773 9.1277
1.000 .430 .055
Konsentrasi LBG.0040.0010.0020.0050.0030.00Sig.
DuncanaN 1 2 3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Komersial Sigma
3 6.80533 7.1490 7.14903 7.2017 7.20173 7.4087 7.40873 8.13803 10.7307
.266 .079 1.000
Konsentrasi LBG50.0040.0020.0030.0010.00.00Sig.
DuncanaN 1 2 3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
190
9.4 Modulus rigidity ANOVA
3.689 5 .738 .208 .95342.546 12 3.54546.235 1737.297 5 7.459 .843 .545
106.191 12 8.849143.488 17
42.383 5 8.477 17.828 .0005.706 12 .475
48.089 17
Between GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotal
Sargassum sp
Turbinaria sp
Komersial Sigma
Sum ofSquares df Mean Square F Sig.
Sargassum sp
3 19.33273 19.87833 20.36103 20.43233 20.49833 20.6533
.449
Konsentrasi LBG40.0020.0050.00.0010.0030.00Sig.
DuncanaN 1
Subsetfor alpha
= .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Turbinaria sp
3 16.13433 16.94773 18.21533 18.32733 18.90203 20.6673
.117
Konsentrasi LBG.0050.0010.0040.0020.0030.00Sig.
DuncanaN 1
Subsetfor alpha
= .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
191
Komersial Sigma
3 9.26603 10.58973 10.68703 10.78733 11.80073 14.2373
1.000 .069 1.000
Konsentrasi LBG50.0040.0020.0030.0010.00.00Sig.
DuncanaN 1 2 3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
9.5 Sineresis
ANOVA
15.130 5 3.026 39.780 .000.913 12 .076
16.042 1734.461 5 6.892 94.226 .000
.878 12 .07335.338 17
4.289 5 .858 2.402 .0994.285 12 .3578.574 17
Between GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotal
Sargassum sp
Turbinaria sp
Komersial Sigma
Sum ofSquares df Mean Square F Sig.
Sargassum sp
3 5.40003 6.12333 6.69673 7.41673 7.87003 7.8700
1.000 1.000 1.000 .079
Konsentrasi LBG50.0040.0030.0020.00.0010.00Sig.
DuncanaN 1 2 3 4
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
192
Turbinaria sp
3 6.20993 6.50233 7.12093 7.80243 8.49253 10.3208
.210 1.000 1.000 1.000 1.000
Konsentrasi LBG50.0040.0030.0020.0010.00.00Sig.
DuncanaN 1 2 3 4 5
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Komersial Sigma
3 3.00333 3.05673 3.3767 3.37673 3.4433 3.44333 3.6833 3.68333 4.4667
.227 .060
Konsentrasi LBG40.0050.0030.0020.0010.00.00Sig.
DuncanaN 1 2
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
193
Lampiran 6. Uji statistik pengaruh penambahan LBG terhadap karakteristik viskositas alginat
6.1 Uji statistik pengaruh penambahan LBG terhadap peningkatan viskositas
ANOVA
1509994 5 301998.856 513.749 .0007054.000 12 587.8331517048 17
337476.0 5 67495.200 386.423 .0002096.000 12 174.667339572.0 174615827 5 923165.422 602.217 .000
18395.333 12 1532.9444634222 17
Between GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotalBetween GroupsWithin GroupsTotal
Sargassum sp
Turbinaria sp
Komersial Sigma
Sum ofSquares df Mean Square F Sig.
Post Hoc Tests
Sargassum sp
Duncana
3 456.33333 603.00003 743.33333 901.00003 1008.00003 1348.6667
1.000 1.000 1.000 1.000 1.000 1.000
Konsentrasi LBG.0010.0020.0030.0040.0050.00Sig.
N 1 2 3 4 5 6Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
Turbinaria sp
Duncana
3 109.66673 126.66673 180.00003 238.00003 367.00003 492.6667
.141 1.000 1.000 1.000 1.000
Konsentrasi LBG.0010.0020.0030.0040.0050.00Sig.
N 1 2 3 4 5Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
194
Komersial Sigma
Duncana
3 1190.66673 1236.66673 1633.33333 2295.66673 2306.3333 2306.33333 2374.0000
.176 1.000 .744 .056
Konsentrasi LBG.0010.0020.0030.0040.0050.00Sig.
N 1 2 3 4Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
6.2 Uji statistik pengaruh penambahan LBG terhadap stabilitas viskositas
ANOVA
Penurunan Viskositas
2018.483 5 403.697 71.123 .00068.113 12 5.676
2086.595 17
Between GroupsWithin GroupsTotal
Sum ofSquares df Mean Square F Sig.
Post Hoc Tests
Penurunan Viskositas
Duncana
3 37.26673 52.68333 57.56333 59.6867 59.68673 63.23003 71.7800
1.000 1.000 .296 .094 1.000
Perlakuan4.003.002.006.001.005.00Sig.
N 1 2 3 4 5Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
keterangan : 1 = Sargassum sp tanpa LBG, 2 = Sargassum sp dengan LBG, 3 = Turbinaria sp tanpa LBG, 4 = Turbinaria sp dengan LBG, 5 = Komersial Sigma tanpa LBG, 6 = Komersial Sigma dengan LBG
195
6.3 Uji statistik pengaruh penambahan LBG terhadap recovery viskositas ANOVA
Recovery viskositas
11571.943 5 2314.389 2104.691 .00013.196 12 1.100
11585.138 17
Between GroupsWithin GroupsTotal
Sum ofSquares df Mean Square F Sig.
Post Hoc Tests
Recovery viskositas
Duncana
3 56.17003 62.17003 64.66673 80.45673 88.59333 131.6200
1.000 1.000 1.000 1.000 1.000 1.000
Perlakuan5.001.003.002.006.004.00Sig.
N 1 2 3 4 5 6Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.Uses Harmonic Mean Sample Size = 3.000.a.
keterangan : 1 = Sargassum sp tanpa LBG, 2 = Sargassum sp dengan LBG, 3 = Turbinaria sp tanpa LBG, 4 = Turbinaria sp dengan LBG, 5 = Komersial Sigma tanpa LBG, 6 = Komersial Sigma dengan LBG