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NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Dairy for Clean LabelInnovations in Dairy Based Ingredients for
Clean Label SolutionsRohit Kapoor, Ph.D.VP-Product ResearchNational Dairy CouncilRosemont IL
2020 Clean Label ConferenceMarch 25-26 2020Itasca IL
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
DISCLAIMER
The use of brands and images of branded products is intended only to provide examples of concepts being discussed, and does not imply endorsement of any brand or product
2
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Summary
• Clean label discussion is evolving and dairy ingredients are well positioned to deliver.
• Milk’s unique composition provides dairy ingredients with diverse functional properties and versatility for the development of clean label food products.
• Dairy ingredients can help clean label formulations in 2 ways:• By using “off-the shelf” dairy ingredients and leveraging their unique composition
and inherent functionality• By “tailoring” dairy ingredients to achieve targeted solutions
3
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Agenda1. Implications for food Ingredients in clean label
2. How can dairy ingredients help?
1. Dairy Ingredients 101
2. Leveraging dairy ingredients inherent functionality1. Dairy protein ingredients functionality and flavor2. Milk fat Ingredients
3. Tailoring dairy ingredients to achieve “targeted solutions”
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Implications for Food Ingredients in Clean Label
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Role of Food Ingredients in Food Products
Ingredients
NutritionFunctionTaste
• Neutral Flavors• No off-notes• Complement• Enhance eating experience • Macro and Micro-Nutrients
• Enhance Nutrition/Claims
• Ease in processing• Texture• Enhance eating experience• Product Stability• Shelf Life (Enhancement)
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
How can Dairy Ingredients help?
• Leverage their unique composition and inherent functionality• Protein, Lactose, Fats, Minerals
• Take advantage of dairy’s “clean” image
By using “off-the shelf” dairy ingredients
• Casein and whey protein modifications• pH• Temperature• Mechanical (process modification)• Enzymatic/Catalytic
• Lactose bioconversion• Fermentation• Enzymatic• Catalytic
By tailoring dairy ingredients to achieve “targeted solutions”
7
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Dairy Ingredients 101
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Lets start from the basics…composition
Component Typical Composition, %
Water 87.5Proteins 3.4Lactose 4.8Fat 3.9Ash (Minerals) 0.8
Caseins 2.7 %Whey Proteins 0.8 %
Source: Dairy Processing Handbook 2nd edition, Tetra Pak 2003
Cow’s Milk
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Lets start from the basics…dairy unit operationsPA
STEU
RIZA
TIO
N
CREA
M S
EPAR
ATIO
N
Ferm
enta
tion
Evap
orat
ion
Mem
bran
e Fi
ltrat
ion Dry
ing
Icons: The noun project
Fluid Milk and CreamFluid MilkCreamButterButter Oil/AMF
CheeseYogurt
Evaporated MilkCondensed Milk
Whe
y
Milk Powders (WMP/SMP/NDM)
Milk Protein Ingredients (MPC, MPI, MCC, Specialty Milk Proteins)
Whey Protein Ingredients (WPC, WPI, Specialty Whey Proteins)
Whey Powders
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Milk Protein Ingredients
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Milk Powders SMP, NDM
MPC-70 MPC-80 MPI
Protein, % 34.0 – 37.0 69.5 (min) 79.5 (min) 89.5 (min, db)
Lactose, % 49.5 – 55.0 20.0 (max) 9.0 (max) 5.0 (max)
Fat, % 0.6 – 1.25 2.5 (max) 2.5 (max) 2.5 (max)
Minerals, % 8.2 – 8.6 10.0 (max) 8.0 (max) 8.0 (max)
Moisture, % 3.0 – 5.0 6.0 (max) 6.0 (max) 6.0 (max)
Sources: 1. http://www.thinkusadairy.org/products2. USDEC. 2017. Dairy Ingredients Functionality and Composition Reference Guide. http://www.thinkusadairy.org
Casein : Whey Protein = 80 : 20
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Whey Protein Ingredients
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WPC 34 WPC 80 WPI
Protein, % 34.0 – 36.0 80.0 - 82.0 (db) 90.0 – 92.0 (db)
Lactose, % 48.0 – 52.0 4.0 – 8.0 0.5 – 1.0
Fat, % 3.0 – 4.5 4.0 – 8.0 0.5 – 1.0Minerals, % 6.5 – 8.0 3.0 – 4.0 2.0 – 3.0
Moisture, % 3.0 – 4.5 3.5 – 4.5 4.0 – 6.0
Sources: 1. http://www.thinkusadairy.org/products2. USDEC. 2017. Dairy Ingredients Functionality and Composition Reference Guide. http://www.thinkusadairy.org
No Caseins
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Lactose Rich Ingredients
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Whey Powder Whey Permeate/
Dairy Product Solids
Lactose (Food Grade)
Protein, % 11.0 – 14.5 2.0 – 7.0 0.1
Lactose, % 63.0 – 75.0 76.0 – 88.0 99.0 (min)
Fat, % 1.0 – 1.5 0.0 – 1.5 ---Minerals, % 8.2 – 8.8 8.0 – 14.0 0.1 – 0.3
Moisture, % 3.5 – 5.0 3.0 – 5.0 4.5 – 5.5
Milk
Cheese (10%)
Whey (90%)
Whey Proteins (WPC/WPI)
Whey PowderPermeate/Dairy Product
Solids
Lactose Minerals
Sources: 1. http://www.thinkusadairy.org/products2. USDEC. 2017. Dairy Ingredients Functionality and Composition Reference Guide. http://www.thinkusadairy.org
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
How can Dairy Ingredients help?
• Leverage their unique composition and inherent functionality• Protein, Lactose, Fats, Minerals
• Take advantage of dairy’s “clean” image
By using “off-the shelf” dairy ingredients
• Casein and whey protein modifications• pH• Temperature• Mechanical (process modification)• Enzymatic/Catalytic
• Lactose bioconversion• Fermentation• Enzymatic• Catalytic
By tailoring dairy ingredients to achieve “targeted solutions”
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Quick Refresher: Functional Properties
(Damodaran and Paraf, 1997)
“Functional properties describes how ingredients behave during preparation and cooking, how they affect the finished food product in terms of how it looks, tastes, and feels.”
https://www.ifst.org/lovefoodlovescience/resources/functional-properties-food
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Quick Refresher: How do (dairy) proteins manifest varied functional properties?
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Protein Structure and Interactions
(Primary, Secondary, and
tertiary)
Response to extrinsic factors
(food formulation, processing,
cooking etc.)
Functional Properties
• Water / solvents• pH / Process• salt• Temperature (Freezing-heating)• Shear • Pressure• Chemical / Enzymatic• Inter and intra- molecular
interactions
Source: Patel and Patel. 2015. Understanding the role of dairy proteins in ingredient and product performance.http://www.thinkusadairy.org/resources-and-insights/resources-and-insights/application-and-technical-materials/technical-report-understanding-the-role-of-dairy-proteins-in-product-performance
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Properties of dairy proteins…Versatility!
17Source: Patel and Patel. 2015. Understanding the role of dairy proteins in ingredient and product performance.http://www.thinkusadairy.org/resources-and-insights/resources-and-insights/application-and-technical-materials/technical-report-understanding-the-role-of-dairy-proteins-in-product-performance
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Dairy proteins offer a gamut of functional properties to food products…Versatility!
Food Product Functions required for most products Functions required for some products
Beverages Solubility, colloidal stability, viscosity, heat stability Acid stability, emulsifying, water holding
Bakery Solubility, emulsifying, gelation, color and flavor development
Foaming, foam stability, water holding, gluten modification
Confectionery Foaming, solubility, color and flavor development Emulsifying, gelation
Frozen desserts Emulsifying, solubility, dispersibility Solubility, water holding, fat mimetic, gelation
Formed meat products and meat analogs Emulsification, water holding, color development Salt solubility, low viscosity, gelation, fat
mimetic
Sauces, soups, gravies Emulsification, water holding viscosity
‘Imitation’ dairy Emulsifying, colloid stability Solubility, foaming, foam stability
Salty snacks Solubility, heat stability Foaming, foam stability, gelation
Sources: 1. http://www.thinkusadairy.org/products2. USDEC. 2017. Dairy Ingredients Functionality and Composition Reference Guide. http://www.thinkusadairy.org 18
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Why Dairy Protein Ingredients for Clean Label Foods?
Clean Label Foods
Use of less ingredients
•Ability to replace:•Starches•Hydrocolloids•Flavor maskers
•No protein blending required for nutritional equivalency
Dairy Protein
Ingredients
•Excellent Functionality•Cleaner Flavor•Higher protein quality
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Functionality: How do they compare to other protein sources?Functional Property Results
Water Holding Capacity Milk ~ Soy ~ Pea > Whey ~ Potato ~ Rice
Viscosity Milk ~ Pea > Whey ~ Soy ~ Potato ~ Rice
Heat Stability (acidic conditions, pH 3) Whey > Plant > Milk
Heat Stability (neutral conditions, pH 7) Milk ~Whey > Plant
Emulsion ActivityEmulsion Stability
Milk ~Whey ~ Pea ~ Soy > Potato > RiceMilk>Whey~ Pea ~ Soy > Potato > Rice
Foam AbilityFoam Stability
Whey > Soy ~Potato > Milk > PeaWhey > Milk > Soy and > Pea > Rice
Gel Strength Whey > Potato~Pea~Soy
Dairy proteins are versatile and offer a comprehensive solution to end users.Sources: 1. USDEC. 2018. A New Era for Protein: Why U.S. Dairy Delivers in the Crowded Protein Marketplace.
www.thinkusadairy.org2. Kapoor et. al. 2017. Characterization of commercial food protein ingredients. International Whey Conference. Chicago IL
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Sensory Profile: How do they compare to other protein sources?
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Sources: 1. USDEC. 2018. A New Era for Protein: Why U.S. Dairy Delivers in the Crowded Protein Marketplace.
www.thinkusadairy.org2. Kapoor et. al. 2017. Characterization of commercial food protein ingredients. International Whey Conference. Chicago IL
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
CerealSulfurous
BeanyPyrazine/bell pepperEarthy/potting soil
FruitySour aromatic
Sour tasteUmami taste
Sweet aromaticMilky/cooked
SoapyAnimalTortilla
CardboardBrothy
Herbal/grassySalty tasteBitter tasteAstringency
Dairy ProteinsPlant Proteins
Flavor Differences between Plant and Dairy Proteins
Sources: 1. USDEC. 2018. A New Era for Protein: Why U.S. Dairy Delivers in the Crowded Protein Marketplace.
www.thinkusadairy.org2. Kapoor et. al. 2017. Characterization of commercial food protein ingredients. International Whey Conference.
Chicago IL
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Scenario 1: Choosing My Protein*
Desired Properties Milk Protein Soy Protein Pea Protein
Clean Taste ●
Good Solubility ●
Medium Viscosity ● ●Good Heat Stability at neutral pH ●
Low Foaming ● ●
Good fat emulsification ● ● ●
UHT beverages
* For Illustrative Purposes Only
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Model UHT Beverage Test at WI-CDR(neutral pH)
MPI MPC MCC NW WPI WPC Pea Soy1 Soy3 Rice
PlantDairy
Sources: Burrington KJ. 2018. Characterization Study of Dairy and Plant Proteins. IFT Annual Meeting. Chicago ILUSDEC. 2018. A New Era for Protein: Why U.S. Dairy Delivers in the Crowded Protein Marketplace. www.thinkusadairy.org
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Scenario 2: Choosing My Protein*
Desired Properties Whey Protein Soy Protein Pea Protein
Clean Taste ●
Good Solubility ●
Low Viscosity ● ●Good Heat Stability at acidic pH ●
Low Foaming ● ●
Clarity ●
Protein Waters
* For Illustrative Purposes Only
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Model High Acid Beverage Test at CDR(low pH)
Rice1 separated right after process. Pea3 separated after sitting in the fridge overnight.
NW1 WPI4 WPC2 Pop1 Soy1 Pea3 Rice
PlantDairy26
Sources: Burrington KJ. 2018. Characterization Study of Dairy and Plant Proteins. IFT Annual Meeting. Chicago ILUSDEC. 2018. A New Era for Protein: Why U.S. Dairy Delivers in the Crowded Protein Marketplace. www.thinkusadairy.org
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Nutrition implication: All proteins are not created equal
• Protein Quality: The ability of a food protein to meet the body’s metabolic demand for amino acids and nitrogen
• Food proteins vary in their protein quality based on: o Amino acid composition o Digestibility
• Animal based proteins >90%• Plant based proteins 45 – 80%
o Bioavailability• PDCAAS (Protein Digestibility Corrected
Amino Acid Score) is the current gold standard for assessing protein quality
Food PDCAAS
Milk Protein Concentrate 1.00
Whey Protein Isolate 1.00
Soy Protein Isolate 0.98
Pea Protein Concentrate 0.89
Rice Protein Concentrate 0.42
Whole milk 1.00
Chicken breast 1.00
Egg (hard boiled) 1.00
Cooked peas 0.60
Cooked rice 0.62
Almonds 0.39
Chickpeas 0.74
Tofu 0.56
PDCAAS for Selected Isolated Proteins and Foods
Table adapted from Phillips SM, Front. Nutr., 201727
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Summary: Why Dairy Protein Ingredients for Clean Label Foods?
Clean Label Foods
Use of less ingredients
•Ability to replace:•Starches•Hydrocolloids•Flavor maskers
•No protein blending required for nutritional equivalency
Dairy Protein
Ingredients
•Excellent Functionality•Cleaner Flavor•Higher protein quality
28
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Cream, Butter, and Other Fat Rich Dairy Ingredients• Major Milk Fat Ingredients
• Cream• Butter• Anhydrous Milk Fat
• Advantages for Clean Label FormulationsChanging nutritional/health perspectivesClean and unique flavor profileComplex melt profile and crystallization
behavior Unique mouthfeel Flavor release and sensory experience Shortening replacements Ability to be fractionated for targeted
applications
29Source: Gnanasambandam et al. 2017. Milkfat and Related Ingredients Serving Today’s Marketplace. www.thinkusadairy.org
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High fat dairy ingredients are in trend…
Source: https://www.fooddive.com/news/cleaning-up-a-product-label-can-be-a-challenging-endeavor/511566/
“…Nestle focused on ingredients in its Stouffer's Macaroni and Cheese commonly found in the home, such as freshly made pasta, cheddar cheese and skim milk. One part of the recipe overhaul included replacing margarine with butter.”
Source: https://www.naturalproductsinsider.com/herbs-botanicals/coffee-creamers-getting-clean-label-makeover
Source: https://www.eater.com/2015/9/1/9239019/mcdonalds-uses-real-butter-axes-margarine-shocker
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
How can Dairy Ingredients help?
• Leverage their unique composition and inherent functionality• Protein, Lactose, Fats, Minerals
• Take advantage of dairy’s “clean” image
By using “off-the shelf” dairy ingredients
• Casein and whey protein modifications• pH• Temperature• Mechanical (process modification)• Enzymatic/Catalytic
• Lactose bioconversion• Fermentation• Enzymatic• Catalytic
By tailoring dairy ingredients to achieve “targeted solutions”
31
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Tailoring dairy ingredients to achieve “targeted solutions”…
Clean Label Foods
• Solubility• Heat Stability• Viscosity• Emulsification• Gelation• Foaming• Bio-preservation
Tailored Ingredients
• pH• Temperature• Mechanical• Enzymatic/Catalytic• Fermentation
Dairy Ingredients
• Dairy Proteins• Lactose• Minerals
Com
pone
nt
Trea
tmen
t
Resu
lt
32
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Remove “phosphates” with dairy ingredients
Pandalaneni et al. 2018. J. Dairy Sci. 101:9714–9724Pandalaneni et al. 2019. J. Dairy Sci. 102:155–163
Shelf Stable RTD
beverages
• Heat Stability
Calcium Reduced
MPC
• pH
MPC
• Dairy Proteins (Caseins and Whey Proteins)
• Minerals (Calcium) Trea
tmen
t
Com
pone
nt
Resu
lt
33
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Remove “emulsifiers” with dairy ingredients
Dr. Varadhanabhuti, University of Missouri ColumbiaSources:Kotchabhakdi, A. 2019. Developing clean label emulsifier based on whey protein and pectin complexesWang, Y. 2018. Emulsification properties of heated whey protein-pectin formed at neutral pH
Salad Dressings
• Emulsification
WPI + Pectin
• Temperature• pH
WPI
• Whey Proteins
Com
pone
nt
Resu
lt
Trea
tmen
t
34
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Better foaming lattes using milk powders…
Ice Cream;Lattes
• Foaming
Milk Powder
• Mechanical: High Pressure Jet
Skim Milk
• Dairy Proteins
Trea
tmen
t
Com
pone
nt
Resu
lt
Hettiarachchi C.A. et al. 2019. J. Food Engg. 261: 1 35
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Replace “Na-Caseinate”
Coffee Creamers
• Emulsification
Micellar Casein
• Mechanical: Fractionation
Skim Milk
• Caseins
Trea
tmen
t
Com
pone
nt
Resu
lt
Merrill et al. 2016. Leprino. US Patent Application # US20160374360A1
36
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Lactose rich dairy ingredients provide sweetener solutions…
Clean label solutions for:
Artificial Sweeteners
• Sweetener solutions
Sweeteners
• Enzymatic/Catalytic
Lactose rich whey
ingredients
• Lactose
Trea
tmen
t
Com
pone
nt
Resu
lt
37
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Fermentation of lactose rich dairy ingredients for clean label solutions…
Clean label solutions for: Preservatives
TexturizersFlavors
• Bio-preservatives• Exo-polysaccharides• Reaction Flavors
Cultured milk
Cultured whey
• Fermentation
Lactose rich dairy milk and whey
ingredients
• Lactose
Trea
tmen
t
Com
pone
nt
Resu
lt
Vedamuthu. E. 2011. Functional Ingredients from Dairy Fermentations. In Book: Dairy Ingredients for Food Processing. Chandan R. and A. Kilara.Reis et al. 2012. Food Eng Rev 4:124–140Sadiq et al. 2019. Comp. Rev. Food Science and Food Safety. 18 (5): 1403-1436.King et al. 1999. DuPont. Patent # USOO.59896 12A
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Summary
• Clean label discussion is evolving and dairy ingredients are well positioned to deliver.
• Milk’s unique composition provides dairy ingredients with diverse functional properties and versatility for the development of clean label food products.
• Dairy ingredients can help clean label formulations in 2 ways:• By using “off-the shelf” dairy ingredients and leveraging their unique composition
and inherent functionality• By “tailoring” dairy ingredients to achieve targeted solutions
39
NationalDairyCouncil.org @NtlDairyCouncil #DairyNourishesLife
Thank You
Rohit Kapoor Ph.D.
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