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Design of SHPB specimens for the determination of mode I, mode II and mixed mode fracture toughness of structural adhesives Nunes, P.D.P. (INEGI, Porto, Portugal), Marques, E.A.S., Carbas, R., Akhavan-Safar, A., da Silva, L. F. M. Introduction Adhesives are increasingly being used in the automotive industry as an alternative to classical mechanical joining methods, as they improve strength to weight ratio and reduce the cost of the projected structure. In the automotive industry, it is crucial to ensure passengers' safety if a collision occurs, for that, the behaviour of the entire structure should be analysed under impact conditions, and this includes the adhesives. The present work to aims design and to define a strategy to validate novel Split Hopkinson Pressure Bar (SHPB) specimens in order to understand how the mechanical properties of structural adhesives vary as a function of strain rate, through the definition of fracture toughness envelopes. Figure 4 Strain rate along the crack length for DCB (a) and ENF (b) at 15 mm/s. Design approach The working principle of a SHPB, represented in Figure 1, consists in launching a striker at high velocity that impacts into a setup bar-specimen-bar generating a stress wave that will load the specimen. In order to achieve the objective proposed in this work, there is a couple of design directions that one must follow to accomplish the design of specimens able to be used in the determination of the energy release rate using a SHPB machine for different loading directions: due to the operating principle of SHPB machines, the geometry should be as close as possible to a cylinder in order to allow proper stress wave transmission to the specimen and the specimens should be designed with different bondline angles so that different mixed mode conditions can be evaluated. Figure 2 Representation of the substrates of the novel SHPB specimens for different mode configurations. References [1] Carvalho, UT et al., “Validation of pure tensile and shear cohesive laws obtained by the direct method with single-lap joints,” International Journal of Adhesion and Adhesives, vol. 77, pp. 41- 50, 2017. [2] Nunes, P.D et al., “Numerical assessment of strain rate in an adhesive layer throughout double cantilever beam and end notch flexure tests,” Proceedings of the Institution of Mechanical Engineers, Part E: Journal of Process Mechanical Engineering, p.0954408920916007, 2020. Acknowledgements The authors would like to thank FCT for funding this work through grant Nº 029839, POCI-01-0145-FEDER-029839. Figure 1 Scheme of a representation of an SHPB machine. Figure 3 Direct method applied to the tensile and shear cohesive law estimation [1]. The final design of the specimens consists in two similar substrates, presented in Figure 2, bonded together. As shown in the image for the pure mode II substrate, the geometry consists in a threaded connection, in order to assemble the specimen to the bar, the bonded area that is designed at an angle with the loading direction to induce different mode mixities and an insert that allows the alignment in the mould to guarantee maximum geometrical accuracy. To evaluate the newly designed SHPB specimens, the authors started by focusing on the pure mode I and mode II specimens. The objective is to validate the new specimens by testing both the new specimens and the uniformly accepted tests proposed in the literature, like DCB and ENF, at quasi-static and intermediate strain rates and by resorting to simulation tools, namely finite element models with cohesive elements. Due to the influence of the CZM law shape in the numerical predictions the authors opted by the use of the direct method based in the J-integral formulation since cohesive law for each mode can be estimated with a single test. For proper comparison, specimens must be tested at same strain rate. Nunes et al. [2] studied the evolution of the strain rate for both DCB and ENF as can be seen in Figure 2. Moreover they found that the evolution shown in the graphics approximately changes with the test speed in a proportional manner. Mixed-mode (22.5°) Mixed-mode (45°) Mixed-mode (72.5°) Mode II (90°) Mode I (0°) Threaded connection Bonded area Mould insert SHPB specimen validation 0 5 10 15 20 25 30 0 10 20 30 40 50 60 70 80 Strain rate (s -1 ) Crack length (mm) Engineering strain rate True strain rate 0 10 20 30 40 0 20 40 60 80 100 120 140 160 180 Strain rate (s -1 ) crack length (mm) Engineering strain rate True strain rate (a) (b) With the information in the graphics above and the equation of strain rate: = 0 , where is the velocity and 0 the reference distance, the table below shows the test speed for each test that must be ensured to allow for testing at equivalent strain rates. Strain rate Test Speed DCB SHPB mode I ENF SHPB mode II 3.33E-02 s -1 1 mm/min 0.4 mm/min 1.2 mm/min 0.4 mm/min 200 s -1 100 mm/s 40 mm/s 120 mm/s 40 mm/s

Design of SHPB specimens for the determination of mode I

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Page 1: Design of SHPB specimens for the determination of mode I

Design of SHPB specimens for the determination of mode I, mode II and mixed mode fracture toughness of structural adhesivesNunes, P.D.P.(INEGI, Porto, Portugal), Marques, E.A.S., Carbas, R., Akhavan-Safar, A., da Silva, L. F. M.

IntroductionAdhesives are increasingly being used in the automotiveindustry as an alternative to classical mechanical joiningmethods, as they improve strength to weight ratio and reducethe cost of the projected structure. In the automotive industry,it is crucial to ensure passengers' safety if a collision occurs,for that, the behaviour of the entire structure should beanalysed under impact conditions, and this includes theadhesives.The present work to aims design and to define a strategy tovalidate novel Split Hopkinson Pressure Bar (SHPB)specimens in order to understand how the mechanicalproperties of structural adhesives vary as a function of strainrate, through the definition of fracture toughness envelopes.

Figure 4 – Strain rate along the crack length for DCB (a) and ENF (b) at 15 mm/s.

Design approachThe working principle of a SHPB, represented in Figure 1,consists in launching a striker at high velocity that impactsinto a setup bar-specimen-bar generating a stress wave thatwill load the specimen. In order to achieve the objectiveproposed in this work, there is a couple of design directionsthat one must follow to accomplish the design of specimensable to be used in the determination of the energy release rateusing a SHPB machine for different loading directions: due tothe operating principle of SHPB machines, the geometryshould be as close as possible to a cylinder in order to allowproper stress wave transmission to the specimen and thespecimens should be designed with different bondline anglesso that different mixed mode conditions can be evaluated.

Figure 2 – Representation of the substrates of the novel SHPB specimens for different mode configurations.

References

[1] Carvalho, UT et al., “Validation of pure tensile and shear cohesivelaws obtained by the direct method with single-lap joints,”International Journal of Adhesion and Adhesives, vol. 77, pp. 41-50, 2017.

[2] Nunes, P.D et al., “Numerical assessment of strain rate in anadhesive layer throughout double cantilever beam and end notchflexure tests,” Proceedings of the Institution of MechanicalEngineers, Part E: Journal of Process Mechanical Engineering,p.0954408920916007, 2020.

Acknowledgements

The authors would like to thank FCT for funding this workthrough grant Nº 029839, POCI-01-0145-FEDER-029839.

Figure 1 – Scheme of a representation of an SHPB machine.

Figure 3 – Direct method applied to the tensile and shear cohesive law estimation [1].

The final design of the specimens consists in two similarsubstrates, presented in Figure 2, bonded together. As shownin the image for the pure mode II substrate, the geometryconsists in a threaded connection, in order to assemble thespecimen to the bar, the bonded area that is designed at anangle with the loading direction to induce different modemixities and an insert that allows the alignment in the mould toguarantee maximum geometrical accuracy.

To evaluate the newly designed SHPB specimens, the authorsstarted by focusing on the pure mode I and mode II specimens.The objective is to validate the new specimens by testing boththe new specimens and the uniformly accepted tests proposedin the literature, like DCB and ENF, at quasi-static andintermediate strain rates and by resorting to simulation tools,namely finite element models with cohesive elements.

Due to the influence of the CZM law shape in the numericalpredictions the authors opted by the use of the direct methodbased in the J-integral formulation since cohesive law for eachmode can be estimated with a single test.

For proper comparison, specimens must be tested at samestrain rate. Nunes et al. [2] studied the evolution of the strainrate for both DCB and ENF as can be seen in Figure 2.Moreover they found that the evolution shown in the graphicsapproximately changes with the test speed in a proportionalmanner.

Mixed-mode (22.5°) Mixed-mode (45°)

Mixed-mode (72.5°) Mode II (90°)

Mode I (0°)

Threaded connection

Bonded area

Mould insert

SHPB specimen validation

0

5

10

15

20

25

30

0 10 20 30 40 50 60 70 80

Str

ain r

ate

(s-1

)

Crack length (mm)

Engineering strain rate

True strain rate0

10

20

30

40

0 20 40 60 80 100 120 140 160 180

Str

ain r

ate

(s-1

)

crack length (mm)

Engineering strain

rateTrue strain rate

(a) (b)

With the information in the graphics above and the equation ofstrain rate: ሶ =

𝑣

𝐿0, where 𝑣 is the velocity and 𝐿0 the reference

distance, the table below shows the test speed for each testthat must be ensured to allow for testing at equivalent strainrates.

Strain rate Test Speed

DCB SHPB mode I ENF SHPB mode II3.33E-02 s-1 1 mm/min 0.4 mm/min 1.2 mm/min 0.4 mm/min

200 s-1 100 mm/s 40 mm/s 120 mm/s 40 mm/s