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DEVELOPMENT OF TEST METHODS FOR SMART TEXTILES June 26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle

DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Page 1: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

DEVELOPMENT OF TEST METHODS FOR

SMART TEXTILES

June 26, 2016

Justine Decaens, Olivier Vermeersch,

Patricia Dolez & Dominic Lachapelle

Page 2: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

www.gcttg.com

Laboratory testing services

Research, Development &

Innovation

Expertise

Our Group

Our Group

Page 3: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

www.gcttg.com 3

Textiles became SMART ....

Page 4: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

www.gcttg.com

AGENDA:

1. Overview of test methods developed at CTT Group

2. Example 1: Thermal performance of heating textiles

3. Example 2: Dewatering performance of electro-conductive

geosynthetics for mine tailings

4. Example 3: Linear electrical resistance of tracks

5. Initiatives all around the world

Page 5: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

www.gcttg.com

Overview of test methods developed at CTT Group

5

•Method GCTTG 4002-09 :

•Method GCTTG 4003-10 and GCTTG 4004-11 :

Measurement of the evolution of the

electrical characteristics as a function of the

elongation and abrasion of an electro-

conductive textile.

Measurement of electrical resistance of conductive fibers

Page 6: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

www.gcttg.com

Test methods developed at CTT Group (cont’d)

6

•Method GCTTG 4008-15:

Characterization of the piezo-resistive sensitivity

of membranes

•Method GCTTG 4009-15 and 4011-16 :

Measurement of thermal performance and

homogeneity of heating or cooling textiles

•Method GCTTG 4010-15 :

Evaluation of the durability of electro-conductive

textiles when exposed to liquids

Page 7: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Example 1: Thermal performance of heating textiles

•Geographical context : Canada ���� Cold winter, need for suitable clothing

•Current workwear issues:

•Bulky, heavy, not breathable enough

•Difficult to adapt to different physical activities

•Reduced mobility

•Advantage of heating clothing

•Controlled and adjustable thermal comfort

• Thinner layers

Context:

8

Source : www.msdsonline.com

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•Comparison between the performance of heating textiles and traditionnal

insulating layers

•Adaptation of an existing test method : Guarded Sweating Hot Plate –

ASTM F1868

•Formula :

Methodology:

9

Hc

ATaTsRct

*)( −

=

• Ts, temperature of the plate (°C) : 35°C

• Ta, temperature of the climatic chamber (°C) : 20°C

• A, surface of the plate (m²)

• Hc, power output (W)

Thermal performance of heating textiles (cont’d)

Page 9: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Technical constraints :

• Retroaction with temperature controller and thermocouple

• Set point value : 2°C higher than the temperature measured at rest

Regulation of the heating power :

• Non homogenous surface : hot points

• Interface : high thermal conductivity + electrically insulated

• Determination of the interface dimensions : representative, not impacting

Development of the interface :

• Copper surface coated with PU/PC

•Surface 9*9 cm

10

Thermal performance of heating textiles (cont’d)

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Results :

• Large differences between product performances : Product # P1 thermal insulation

increases by 90% while Product #P2 thermal insulation only by 25%

• Influence of the encapsulation medium

• Relation between the Clo value and the temperature of use

0

1

2

3

4

5

1 2 3

Clo

(m

².K

/W

Heating products

Heating performances – Heavy

insulated coat

Système actif

Système passif

0

1

2

3

4

5

1 2 3

Clo

(m

².K

/W)

Heating products

Heating performances – Light,

non-insulated coat

Système actif

Système passif

11

Thermal performance of heating textiles (cont’d)

Page 11: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

www.gcttg.com

Example 2: Dewatering performance of electro-

conductive geosynthetics for mine tailings

Context:

• Production of crude bitumen from oil sands

mining expected to double by 2020

• Production of 1 ton of synthetic crude oil

by open-pit mining

� Requires 12.3 tons of oil sands

� Generates 15.6 tons of tailings

���� Investigation of the effect of the tailings

composition on their dewatering using

electrokinetic geocomposite (eGCP)

50 km

13

Page 12: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Principle:• eGCP Prototype = Drain-tube planar

geocomposite + metal electrode

• Filtration of different formulations of

Mature Fine Tailings (MFT)

• Obtained from Canadian oil sands

producers (MFTR)

• Produced in the laboratory (MFTS)

Dewatering performance of electro-conductive

geosynthetics for mine tailings (Cont’d)

14

Active dewatering

Page 13: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Test setup & protocol:

• Laboratory Scale Dewatering Device : Simulate the entire path of water taking place in

real tailings disposal, i.e. under self-weight consolidation, consolidation under the

weight of overlying layers of tailings, electro-osmosis, and drainage

20 L

15

Dewatering performance of electro-conductive

geosynthetics for mine tailings (Cont’d)

Page 14: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Results:• Volume of filtrate expelled from

the tailings as a function of time

for the successive phases of the

dewatering treatment

• 50% volume reduction at the

end of the treatment

• Increase in the shear strength

from 0 to ~ 25 kPa (trafficable

surface)

• Different MFT formulations

required different treatment

durations to reach a 50%-volume

reduction

16

Dewatering performance of electro-conductive

geosynthetics for mine tailings (Cont’d)

Page 15: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Example 3: Linear electrical resistance of tracks

Context - Partnership:

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• European project SUSTASMART – Supporting Standardization for Smart Textiles

• Categorising Smart Textiles

• Evaluating the need for standardization

• Identifying the first applications to consider

• Two standards have been proposed :

• Evaluating the thermal effect of PCM

• Determining the linear electrical resistance of conductive tracks

• Draft submitted to CEN/TC 248/WG 31 N 163

Page 16: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Objective :

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• Determine the electrical resistance of :

• Yarns

• Knitted or woven bands, ribbons

• Characterize the length/width ratio : 10/1

Four points – Four wires Method :

• Conditionning for 24 h (20°C – 65%HR)

• Relaxing for 24h (EN 12127)

• 5 specimens of at least 50 cm long

• For each specimen, 2 independant series of 5 voltage measurements

Linear electrical resistance of tracks (Cont’d)

Page 17: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Nature Weight (g/m²) Stress applied

Yarns - 0.5 cN / tex

Not stretchable fabrics

< 200 2N

200-500 5N

> 500 10N

Stretchable fabrics - 0.5 N

Method principle:

• Four electrodes aligned

• Distance between the electrode = at least

50 cm or 10 times the width of the track

• Electrodes are flat with a good contact with

the tested material (glue, soldering, etc.)

• Tension applied on the textile element :

Linear electrical resistance of tracks (Cont’d)

Page 18: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

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Initiatives all around the world

22

Standardization organisations:

• CEN : Creation of the first task group in 2006

• ASTM : workshop sessions began in 2012

• AATCC : March 2016

Research groups:

• CTT Group

• Centexbel

• Ohmatex

• Aachen University

• Others …

Source : www.forbes.com

Page 19: DEVELOPME OF TEST METHODS FOR SMART …...DEVELOPME OF TEST METHODS FOR SMART TEXTILES June26, 2016 Justine Decaens, Olivier Vermeersch, Patricia Dolez & Dominic Lachapelle Laboratory

Questions ?

Justine Decaens, CTT Group

[email protected]