Dr M SHAHID PhD Brief Bio-data

3 Aisha Apartments Muzammil Complex Aligarh Mobile +91 9359264128 Ph 0571-2700920 (ext) 3350 E -Mail shahid81chemgmailcom

Educational Qualifications

PhD in OrganometallicCoordination Chemistry from AMU Aligarh in 2011 MSc in Synthetic amp Natural Organic Chemistry from CSJM Kanpur with first division and first position BSc in Chemistry (with Physics amp Maths) from CSJM Kanpur with First Division Intermediate (Maths) amp High Schooling from UPB both with First Divisions amp Distinctions JRF-NET organized by CSIR-UGC in 2009 Graduate Aptitude Test in Engineering (GATE) organized by IIT Kanpur in 2007

Selected Achievements amp Awards

Fast Track Young Scientist awarded by SERB-DST New Delhi 2012 Research Associate awarded by CSIR New Delhi 2012 Certificate of Appreciation in online competition of Keplerrsquos Mission NASA USA 2009

Teaching Experience

Guest Lecturer July 2010- March 2011 Assistant Professor Sep 2011- Oct 2011 Guest Lecturer Oct 2011- March 2012 Assistant Professor Aug 2012- Sep 2012 Guest Faculty Sep 2012 till date

Courses taught BSc - Organic and Inorganic Chemistry MSc - Ist semester-Inorganic Reaction Mechanism MSc - IIIrd Semester- Organometallic Chemistry

Fellowships availed

Junior Research Fellowship by UGC from Oct 2009 to July 2010 UGC fellowship for central Universities from 2007 to Sep 2009

Research Profile

Summary of PhD work

Title of Thesis Synthesis amp Physico-chemical Investigations of Binary and Ternary Complexes of Metal Ions Mentor Prof Zafar A Siddiqi Significant outcomes

The chemistry of functionalized polycarboxylic acid and their binary and ternary complexes of metal ions has been taken under investigation The coordination chemistry of functionalized polycarboxylic acid ligands viz pyridinedicarboxylic acid (H2pda) iminodiacetic acid (H2imda) oxydiacetic acid (H2oda) or nitrilotriacetic acid (H3nta) has attracted special focus of inorganic and bioinorganic chemists over the past decades These ligands are very important tridentate chelating agents The flexibility of these ligands makes them useful for the formation of the complexes differing in coordination numbers conformations and 3-D architectures It is well known that in binary and ternary mixed ligand metal carboxylate complexes the carboxylate ligands play an important role to construct novel metal-organic frame works (MOFs) and supramolecular frameworks

Fig (a) A supramolecular network of the complex [Cu(IDA)(Phen)H2O]2H2O constructed from H-bonding (b) Two layers of the complex showing πndashπ interactions between phenanthroline rings and forming a supramolecular framework [Eur J Med Chem 44 (2009) 2517ndash2522]

I during my PhD focused on the study and design of mixed-ligand ternary metal iminodiacetate

complexes and their possible structural diversities and to pursue in-vitro antimicrobial antitumoral and superoxide dismutase (SOD) activities Ternary complexes of iminodiacetate containing an α-diimine as auxiliary ligand have been widely used as models for several mono and polynuclear metal-enzymes and therefore I have concentrated on the synthesis characterization and the structure-activity correlations of the mixed ligand complexes of transition lanthanide and tin metal ions Moreover due to the flexible nature of iminodiacetic acid ligand we have investigated various H-bonding and π-π interactions existing in these complexes which result in

1D 2D and 3D supramolecular network These supramolecular networks have been characterized using X-ray crystallography

Fig Crystal structure of the novel organotin(IV) compound Fig Mossbauer Spectra of a bimetallic complex t RT amp LNT a potential antitumor agent isolated by Dr Shahid [J Organomet Chem 694 (2009) 3768ndash3774]

Fig Crystal structure of 1D coordination polymeric structure of [Cu(dipic)(4-picoline)]n isolated by us [Eur J Med Chem 45 (2010) 264ndash269]

Fig Crystal structure of the dinuclear complex Fig Crystal structure of 1D coordination polymeric structure of (colouring scheme by symmetry equivalence) isolated [Cu(2-pa)2]middot2H2On isolated by us [Eur J Med Chem 57(2012) 102] by us [Spectrochim Acta Part A 93 (2012) 280]

Current Research Interests

Currently I am involved in Designing and magnetic studies of Molecule Based MAGNETS called Single Molecule Magnets (SMMs) having High Spin and Large Anisotropy Such molecules show slow relaxation of magnetization amp also QTM and can be used for Data Storage and Quantum Computations

Current Research Project(s)

Currently working as a Principal Investigator in SERB-DST funded project of Rs 1835 Lacs in Deptt of Chemistry AMU (Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) International Publications

Published = 20 (Twenty) Communicated = 5 (five) 2013

1 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [H2dea = diethanolamine L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence (CoII

2-CoIII2) defect dicubane core Z A Siddiqi Armeen Siddique M Shahid Mohd Khalid

Anjuli Prashant K Sharma Musheer Ahmad Sarvendra Kumar Yanhua Lan Annie K Powell Dalton Trans (RSC) 2013 (accepted)

2 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-benzimidazole derived ligands Zafar A Siddiqi Anjuli M Shahid Mohd Khalid Prashant K Sharma Armeen Siddique J Mol Structure 1037 (2013) 402-411

3 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Zafar A Siddiqi Armeen Siddique M Shahid Prashant K Sharma Anjuli Mohd Khalid J Mol Structure 1036 (2013) 209-215

4 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD

mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

5 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem (2012) (Accepted)

6 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

7 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

8 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique micro2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

9 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

10 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

11 Spectral and Physico-chemical investigations of novel homo-bimetallic di- 2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

12 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

13 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

14 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

15 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

16 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide

macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

17 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid M

Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

18 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

19 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

20 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

New J Chem (2013) Inorg Chem (2013) J Photochem Photobiol B Biology (2013) J Mol Structure (2013) Polyherdon (2013)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Seminar on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb at Department of

Chemistry AMU Aligarh (Poster) Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis

Moumlssbauer and EPR spectral characterization

5 International Satellite Meeting on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 4-6 March 2011 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

Dr M Shahid

ldquoGreatest pleasure in life is doing what people say you canrsquot dordquo

Research Profile

Summary of PhD work

Title of Thesis Synthesis amp Physico-chemical Investigations of Binary and Ternary Complexes of Metal Ions Mentor Prof Zafar A Siddiqi Significant outcomes

The chemistry of functionalized polycarboxylic acid and their binary and ternary complexes of metal ions has been taken under investigation The coordination chemistry of functionalized polycarboxylic acid ligands viz pyridinedicarboxylic acid (H2pda) iminodiacetic acid (H2imda) oxydiacetic acid (H2oda) or nitrilotriacetic acid (H3nta) has attracted special focus of inorganic and bioinorganic chemists over the past decades These ligands are very important tridentate chelating agents The flexibility of these ligands makes them useful for the formation of the complexes differing in coordination numbers conformations and 3-D architectures It is well known that in binary and ternary mixed ligand metal carboxylate complexes the carboxylate ligands play an important role to construct novel metal-organic frame works (MOFs) and supramolecular frameworks

Fig (a) A supramolecular network of the complex [Cu(IDA)(Phen)H2O]2H2O constructed from H-bonding (b) Two layers of the complex showing πndashπ interactions between phenanthroline rings and forming a supramolecular framework [Eur J Med Chem 44 (2009) 2517ndash2522]

I during my PhD focused on the study and design of mixed-ligand ternary metal iminodiacetate

complexes and their possible structural diversities and to pursue in-vitro antimicrobial antitumoral and superoxide dismutase (SOD) activities Ternary complexes of iminodiacetate containing an α-diimine as auxiliary ligand have been widely used as models for several mono and polynuclear metal-enzymes and therefore I have concentrated on the synthesis characterization and the structure-activity correlations of the mixed ligand complexes of transition lanthanide and tin metal ions Moreover due to the flexible nature of iminodiacetic acid ligand we have investigated various H-bonding and π-π interactions existing in these complexes which result in

1D 2D and 3D supramolecular network These supramolecular networks have been characterized using X-ray crystallography

Fig Crystal structure of the novel organotin(IV) compound Fig Mossbauer Spectra of a bimetallic complex t RT amp LNT a potential antitumor agent isolated by Dr Shahid [J Organomet Chem 694 (2009) 3768ndash3774]

Fig Crystal structure of 1D coordination polymeric structure of [Cu(dipic)(4-picoline)]n isolated by us [Eur J Med Chem 45 (2010) 264ndash269]

Fig Crystal structure of the dinuclear complex Fig Crystal structure of 1D coordination polymeric structure of (colouring scheme by symmetry equivalence) isolated [Cu(2-pa)2]middot2H2On isolated by us [Eur J Med Chem 57(2012) 102] by us [Spectrochim Acta Part A 93 (2012) 280]

Current Research Interests

Currently I am involved in Designing and magnetic studies of Molecule Based MAGNETS called Single Molecule Magnets (SMMs) having High Spin and Large Anisotropy Such molecules show slow relaxation of magnetization amp also QTM and can be used for Data Storage and Quantum Computations

Current Research Project(s)

Currently working as a Principal Investigator in SERB-DST funded project of Rs 1835 Lacs in Deptt of Chemistry AMU (Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) International Publications

Published = 20 (Twenty) Communicated = 5 (five) 2013

1 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [H2dea = diethanolamine L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence (CoII

2-CoIII2) defect dicubane core Z A Siddiqi Armeen Siddique M Shahid Mohd Khalid

Anjuli Prashant K Sharma Musheer Ahmad Sarvendra Kumar Yanhua Lan Annie K Powell Dalton Trans (RSC) 2013 (accepted)

2 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-benzimidazole derived ligands Zafar A Siddiqi Anjuli M Shahid Mohd Khalid Prashant K Sharma Armeen Siddique J Mol Structure 1037 (2013) 402-411

3 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Zafar A Siddiqi Armeen Siddique M Shahid Prashant K Sharma Anjuli Mohd Khalid J Mol Structure 1036 (2013) 209-215

4 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD

mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

5 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem (2012) (Accepted)

6 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

7 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

8 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique micro2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

9 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

10 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

11 Spectral and Physico-chemical investigations of novel homo-bimetallic di- 2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

12 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

13 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

14 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

15 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

16 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide

macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

17 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid M

Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

18 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

19 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

20 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

New J Chem (2013) Inorg Chem (2013) J Photochem Photobiol B Biology (2013) J Mol Structure (2013) Polyherdon (2013)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Seminar on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb at Department of

Chemistry AMU Aligarh (Poster) Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis

Moumlssbauer and EPR spectral characterization

5 International Satellite Meeting on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 4-6 March 2011 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

Dr M Shahid

ldquoGreatest pleasure in life is doing what people say you canrsquot dordquo

1D 2D and 3D supramolecular network These supramolecular networks have been characterized using X-ray crystallography

Fig Crystal structure of the novel organotin(IV) compound Fig Mossbauer Spectra of a bimetallic complex t RT amp LNT a potential antitumor agent isolated by Dr Shahid [J Organomet Chem 694 (2009) 3768ndash3774]

Fig Crystal structure of 1D coordination polymeric structure of [Cu(dipic)(4-picoline)]n isolated by us [Eur J Med Chem 45 (2010) 264ndash269]

Fig Crystal structure of the dinuclear complex Fig Crystal structure of 1D coordination polymeric structure of (colouring scheme by symmetry equivalence) isolated [Cu(2-pa)2]middot2H2On isolated by us [Eur J Med Chem 57(2012) 102] by us [Spectrochim Acta Part A 93 (2012) 280]

Current Research Interests

Currently I am involved in Designing and magnetic studies of Molecule Based MAGNETS called Single Molecule Magnets (SMMs) having High Spin and Large Anisotropy Such molecules show slow relaxation of magnetization amp also QTM and can be used for Data Storage and Quantum Computations

Current Research Project(s)

Currently working as a Principal Investigator in SERB-DST funded project of Rs 1835 Lacs in Deptt of Chemistry AMU (Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) International Publications

Published = 20 (Twenty) Communicated = 5 (five) 2013

1 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [H2dea = diethanolamine L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence (CoII

2-CoIII2) defect dicubane core Z A Siddiqi Armeen Siddique M Shahid Mohd Khalid

Anjuli Prashant K Sharma Musheer Ahmad Sarvendra Kumar Yanhua Lan Annie K Powell Dalton Trans (RSC) 2013 (accepted)

2 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-benzimidazole derived ligands Zafar A Siddiqi Anjuli M Shahid Mohd Khalid Prashant K Sharma Armeen Siddique J Mol Structure 1037 (2013) 402-411

3 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Zafar A Siddiqi Armeen Siddique M Shahid Prashant K Sharma Anjuli Mohd Khalid J Mol Structure 1036 (2013) 209-215

4 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD

mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

5 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem (2012) (Accepted)

6 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

7 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

8 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique micro2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

9 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

10 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

11 Spectral and Physico-chemical investigations of novel homo-bimetallic di- 2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

12 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

13 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

14 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

15 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

16 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide

macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

17 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid M

Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

18 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

19 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

20 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

New J Chem (2013) Inorg Chem (2013) J Photochem Photobiol B Biology (2013) J Mol Structure (2013) Polyherdon (2013)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Seminar on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb at Department of

Chemistry AMU Aligarh (Poster) Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis

Moumlssbauer and EPR spectral characterization

5 International Satellite Meeting on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 4-6 March 2011 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

Dr M Shahid

ldquoGreatest pleasure in life is doing what people say you canrsquot dordquo

Current Research Interests

Currently I am involved in Designing and magnetic studies of Molecule Based MAGNETS called Single Molecule Magnets (SMMs) having High Spin and Large Anisotropy Such molecules show slow relaxation of magnetization amp also QTM and can be used for Data Storage and Quantum Computations

Current Research Project(s)

Currently working as a Principal Investigator in SERB-DST funded project of Rs 1835 Lacs in Deptt of Chemistry AMU (Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) International Publications

Published = 20 (Twenty) Communicated = 5 (five) 2013

1 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [H2dea = diethanolamine L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence (CoII

2-CoIII2) defect dicubane core Z A Siddiqi Armeen Siddique M Shahid Mohd Khalid

Anjuli Prashant K Sharma Musheer Ahmad Sarvendra Kumar Yanhua Lan Annie K Powell Dalton Trans (RSC) 2013 (accepted)

2 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-benzimidazole derived ligands Zafar A Siddiqi Anjuli M Shahid Mohd Khalid Prashant K Sharma Armeen Siddique J Mol Structure 1037 (2013) 402-411

3 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Zafar A Siddiqi Armeen Siddique M Shahid Prashant K Sharma Anjuli Mohd Khalid J Mol Structure 1036 (2013) 209-215

4 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD

mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

5 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem (2012) (Accepted)

6 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

7 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

8 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique micro2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

9 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

10 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

11 Spectral and Physico-chemical investigations of novel homo-bimetallic di- 2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

12 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

13 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

14 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

15 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

16 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide

macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

17 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid M

Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

18 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

19 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

20 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

New J Chem (2013) Inorg Chem (2013) J Photochem Photobiol B Biology (2013) J Mol Structure (2013) Polyherdon (2013)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Seminar on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb at Department of

Chemistry AMU Aligarh (Poster) Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis

Moumlssbauer and EPR spectral characterization

5 International Satellite Meeting on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 4-6 March 2011 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

Dr M Shahid

ldquoGreatest pleasure in life is doing what people say you canrsquot dordquo

4 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD

mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

5 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem (2012) (Accepted)

6 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

7 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

8 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique micro2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

9 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

10 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

11 Spectral and Physico-chemical investigations of novel homo-bimetallic di- 2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

12 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

13 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

14 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

15 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

16 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide

macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

17 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid M

Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

18 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

19 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

20 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

New J Chem (2013) Inorg Chem (2013) J Photochem Photobiol B Biology (2013) J Mol Structure (2013) Polyherdon (2013)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Seminar on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb at Department of

Chemistry AMU Aligarh (Poster) Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis

Moumlssbauer and EPR spectral characterization

5 International Satellite Meeting on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 4-6 March 2011 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

Dr M Shahid

ldquoGreatest pleasure in life is doing what people say you canrsquot dordquo

2009

14 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

15 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

16 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide

macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

17 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid M

Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

18 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

19 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

20 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

New J Chem (2013) Inorg Chem (2013) J Photochem Photobiol B Biology (2013) J Mol Structure (2013) Polyherdon (2013)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Seminar on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb at Department of

Chemistry AMU Aligarh (Poster) Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis

Moumlssbauer and EPR spectral characterization

5 International Satellite Meeting on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 4-6 March 2011 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

Dr M Shahid

ldquoGreatest pleasure in life is doing what people say you canrsquot dordquo

4 National Seminar on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb at Department of

Chemistry AMU Aligarh (Poster) Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis

Moumlssbauer and EPR spectral characterization

5 International Satellite Meeting on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 4-6 March 2011 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains and 3D supramolecular networks

Dr M Shahid

ldquoGreatest pleasure in life is doing what people say you canrsquot dordquo