Effect of Backing Plate in Laser Treatment

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    Effect of backing plate on thermal cycles in laser surface

    treatment: Theoretical and Experimental study

    Thesis submitted to Indian Institute of Technology Kharagpur for the award of the

    degree of

    Master of Technology

    in

    Mechanical Engineering with Specialization in

    Manufacturing Science and Engineering

    by

    Mohit Goenka

    (10ME31001)

    Under the guidance of

    Prof. A. K. Nath

    Department of Mechanical Engineering

    Department of Mechanical Engineering

    Indian Institute of Technology Kharagpur

    2014-2015

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    INDIAN INSTITUTE OF TECHNOLOGY

    KHARAGPUR

    CERTIFICATE

    This is to certify that the thesis entitled, Effect of backing plate on thermal cycles

    in laser surface treatment: Theoretical and Experimental study submitted by

    Mr. Mohit Goenka (10ME31001) as a part of Master of Technology Project in

    Indian Institute of Technology, Kharagpur is a bonafide work completed under my

    supervision and guidance.

    He has been sincere, diligent and eager to grasp more knowledge in his field of work.

    I wish him good luck in his future endeavours.

    Date: May 31, 2015

    Prof. A.K Nath

    Place: IIT Kharagpur

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    CERTIFICATE OF EXAMINATION

    This is to certify that we have examined the thesis entitled Effect of backing plate

    on thermal cycles in laser surface treatment: Theoretical and Experimental

    study submitted by Mohit Goenka and hereby accord our approval of it as a work

    carried out and presented in a manner required for its partial fulfillment for the degree

    of Master of Technology in Manufacturing Sciences for which it has been submitted

    .This approval does not necessarily endorse to or accept every statement made,

    opinion expressed or conclusion as recorded in the thesis. It only signifies the

    acceptance of the thesis for the purpose for which it is submitted.

    External Examiner

    Date: May 2015

    Place: Kharagpur

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    DECLARATION

    I certify that

    a. The work contained in this report is original and has been done by me under

    the guidance of my supervisor.

    b. The work has not been submitted to any other Institute for any degree or

    diploma.

    c. I have followed the guidelines provided by the Institute in preparing the

    report.

    d. I have conformed to the norms and guidelines given in the Ethical Code of

    Conduct of the Institute.

    e. Whenever I have used materials (data, theoretical analysis, figures, and text)

    from other sources, I have given due credit to them by citing them in the text

    of the report and giving their details in the references. Further, I have taken

    permission from the copyright owners of the sources, whenever necessary.

    Mohit Goenka

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    v

    ABSTRACT

    An analytical solution for the variation in thermal cycles in a finite thickness

    workpiece, kept on different semi-infinite backing materials and irradiated by a

    stationary and moving laser beam has been derived. The effects of laser beam

    diameter, scan speed and backing material with heat sink compound in between on

    thermal cycles have been investigated experimentally. The thermal cycles are

    recorded using a non-contact type IR pyrometer. Mild steel, stainless steel and

    aluminium are used as backing materials, considering their heat conduction capacity.

    The effect of these backing materials on cooling rate, affected heat region and

    solidification time are studied. The cooling trend from analytical model and

    experiment has been compared. For experiment, a 1 mm finite AISI 1020 sheet has

    been used and it is irradiated with a stationary laser beam for 0.9 sec for stationary

    laser beam by varying spot diameters and keeping the power density constant. For

    moving laser beam, sample has been irradiated with 3 mm spot diameter by varying

    scan speed. The study shows that the cooling rate at surface i.e. at z=0, for a sample

    decreases with increase in laser spot diameter and this trend is maintained for all the

    six samples considered. Cooling is faster as the thermal conductivity of the backing

    material, with heat sink compound, increases but for a same backing material, without

    heat sink compound, it decreases. Cooling rate at z=0 for a finite mild steel sheet is

    minimum and for semi-infinite mild steel sheet it is maximum. Solidification time or

    melt pool life time follows the same trend as above, viz. for a given sample it

    decreases with the decrease in spot diameter. For a given spot diameter, with increase

    in thermal conductivity of backing plate it decreases. With increase in scan speed the

    effect of backing plate decreases viz. for higher scan speed value of 3500 mm/mincooling rate across all samples are nearly close by and consecutively the effect of

    backing plate is not observed. For a range of ~0.7-0.75 Crvalue thermal cycle plot

    from analytical model is in good agreement with the experimental graphs for a

    moving heat source at non-melting condition. All these have been demonstrated using

    thermal cycle plots, cooling rate bar plots, and heat affected region plots generated

    using experimental data.

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    vi

    ACKNOWLEDGEMENT

    I would like to express my deep sense of gratitude and profound thanks to Prof. A.K

    Nath, Department of Mechanical Engineering, IIT Kharagpur for providing me with

    this wonderful opportunity to work as a part of the team under his guidance. I am

    greatly thankful to him for encouraging us to come up with innovative solutions.

    I am also indebted to Mr Muvvala Gopinath for patiently mentoring and helping me

    out with project. I would like to credit Mr Shitanshu Shekhar Chakraborty for writing

    the MATLAB programme.

    Mohit Goenka

    10ME31001

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    vii

    LIST OF FIGURES

    Fig. No. Title Page No.

    3.1

    Schematic representation of an infinite sheet subjected to uniform

    heat flux at the top surface. 4

    3.2 Laser irradiation on a finite sheet of thickness h unit 5

    3.3 Schematic representation of heat partitioned at the z=0 interface 8

    3.4(i) Radial conduction for stationary laser beam, (ii) Radialconduction for moving laser source beam

    8

    4.1.1 2 kW Ybfiber laser used 9

    4.1.2 laser on time pulse for 0 sec input interaction time 10

    4.1.3 laser on time pulse for 0.5 sec input interaction time 10

    4.2.1

    (a) Schematic representation of a stationary laser beam falling on asemi-infinite mild steel plate for 0.9sec, (b) Schematic representationof a stationary laser beam falling on finite mild steel sheet placed ona backing material with heat sink compound applied

    12

    4.2.2

    (c) Schematic representation of a stationary laser beam falling onfinite mild steel sheet for 0.9sec, (b) Schematic representation of astationary laser beam falling on finite mild steel sheet placed on abacking material with no heat sink applied

    12

    4.3.1(a) Power meter, model-COMET-10K-V1 ROHS OPHIR make,accuracy 5% (b) Laser head (c) Pyrometer (d) Mild steel, AISI-1020 sample placed at an angle of 450with the vertical

    13

    4.3.2Reading for laser power absorptivity for AISI-1020 at varied laser

    powers 14

    5.1.1

    Thermal plot for top surface i.e. z-=0 for different samples on beingirradiated with a 2mm stationary laser spot diameter for 0.9sec fromAnalytical Model using MatLab

    15

    5.1.2

    Thermal plot for top surface i.e. z-=0 for different samples on beingirradiated with a 3mm stationary laser spot diameter for 0.9sec from

    Analytical Model using MatLab15

    5.2.1Experimental thermal cycle at z-=0 for samples on being irradiatedwith a 4mm laser spot diameter for 0.9sec 16

    5.2.2

    Cooling plot for top surface i.e. z-=0 for different samples on beingirradiated with a 2mm laser spot diameter for 0.9sec usingexperimental data

    16

    5.2.3

    Cooling plot for top surface i.e. z-=0 for different samples on beingirradiated with a 3mm laser spot diameter for 0.9sec usingexperimental data

    17

    5.2.4

    Cooling plot for top surface i.e. z-=0 for different samples on beingirradiated with a 4mm laser spot diameter for 0.9sec usingexperimental data

    17

    5.2.5Cooling rate for samples at z = 0 on irradiation with stationary source

    of different spot diameters 18

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    viii

    5.2.6

    (a) Intensity distribution for different spot radius (b) Olympus ModelSZ 1145TR PR zoom sterio microscope (c) 3X Magnification imageof affected region for 3mm spot on finite MS sheet

    20

    5.3.1

    (a) Heat affected region on the finite mild steel sheet for differentlaser spot diameter, (b) Affected region on the semi-infinite mild

    steel sheet for different laser spot diameter21

    5.3.2Plot of heat affected region on sample surface; 2mm spot diameter, P= 300W, V=0 and t= 0.9 sec 21

    5.3.3Plot of heat affected zone on sample surface; 3mm spot diameter, P =675W, V=0 and t= 0.9sec 22

    5.3.4Plot of heat affected zone on sample surface; 4mm spot diameter, P =1200W, V=0 and t = 0.9 sec 22

    5.4.1Cooling curve for different samples; 3mm spot diameter, P=675W,V=0(scan speed) and t = 0.9 sec 23

    5.4.2Cooling curve for different samples; 4mm laser spot dia, P=1200W,V=0(scan speed) and t = 0.9sec 23

    5.5.1Cooling trend at z=0 for semi-infinite mild steel sheet with differentlaser spot diameters 24

    5.5.2Cooling trend at z=0 for finite mild steel sheet with different laserspot diameters 24

    5.6.1Thermal cycle for 1mm MS plate at varying scan speed at z = 0, P =

    400W and 3 spot diameter 25

    5.6.2

    Thermal cycle for 1mm MS plate at varying scan speed at z = 0, P =

    600W and 3 spot diameter 25

    5.7.1Cooling cycle at z = 0 for various samples with P = 600W, 3 spotdiameter and 2000mm/min scan speed as laser parameter 26

    5.7.2Cooling cycle at z = 0 for various samples with P = 600W, 3 spotdiameter and 2500mm/min scan speed as laser parameter

    26

    5.7.3Cooling cycle at z = 0 for various samples with P = 600W, 3 spot

    diameter and 3000mm/min scan speed as laser parameter 27

    5.7.4Cooling cycle at z = 0 for various samples with P = 600W, 3 spotdiameter and 3500mm/min scan speed as laser parameter 27

    5.7.5Cooling rate for samples at z = 0 on irradiation with moving heatsource of different scan speed, P = 600W and 3mm spot diameter 28

    5.7.6Cooling cycle at z = 0 for various samples with P = 400W, 3 spotdiameter and 1000mm/min scan speed as laser parameter 30

    5.7.7Cooling cycle at z = 0 for various samples with P = 400W, 3 spot

    diameter and 1500mm/min scan speed as laser parameter 30

    5.7.8Cooling rate for samples at z = 0 on irradiation with moving heatsource of different scan speed, P = 400W and 3mm spot diameter 31

    5.8.1

    Cooling cycle at z = 0 from IR pyrometer for 1mm MS sheet, P =

    400W, 3 spot diameter and varying laser scan speed 32

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    ix

    LIST OF TABLES

    5.8.2Cooling cycle at z = 0 from Analytical model for 1mm MS sheet, P =400W, 3 spot diameter and varying laser scan speed, Cr= 0.7 32

    5.8.3Cooling cycle at z = 0 from IR pyrometer for 1mm MS sheet, P =

    600W, 3 spot diameter and varying laser scan speed 33

    5.8.4 Cooling cycle at z = 0 from Analytical model for 1mm MS sheet, P =600W, 3 spot diameter and varying laser scan speed, Cr= 0.7 33

    5.8.5Cooling cycle at z = 0 from Analytical model for 1mm MS sheet, P =600W, 3 spot diameter and varying laser scan speed, Cr= 1 34

    Table No. Title Page No.

    4.2.1 Laser parameters for stationary heat source, interaction time keptconstant at 0.9s

    11

    4.2.2Laser parameters for Moving heat source, laser spot diameter

    constant at 3mm 11

    4.2.3Materials used for the experiment and their properties. (source:

    EES and wikipidea)11

    4.3Reading for laser power absorptivity for AISI-1020 at varied laserpowers

    14

    5.2 Temperature at two fixed interval for different spot diameter 18

    5.3 Radius of the heat affected region on the samples surface 20

    5.7.1Temperature at two fixed interval for a given laser scan speed, P =

    600W28

    5.7.2Temperature at two fixed interval for a given laser scan speed, P =

    400W31

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    x

    TABLE OF CONTENTS

    ABSTRACT.............................................................................................................................. v

    ACKNOWLEDGEMENT...................................................................................................... vi

    LIST OF FIGURES............................................................................................................... vii

    LIST OF TABLES.................................................................................................................. ix

    1. INTRODUCTION................................................................................................................ 1

    2. LITERATURE SURVEY.................................................................................................... 2

    3. ANALYTICAL MODELLING.......................................................................................... 4

    4. EXPERIMENTAL DETAILS............................................................................................ 9

    4.1. Specifications of Laser used...................................................................................... 9

    4.2. Experiment Procedure and Laser Parameters.......................................................... 10

    4.3. Absorptivity of Mild Steel (AISI-1020):................................................................. 13

    5. RESULTS AND DISCUSSION.................................................................................... 15

    5.1. Thermal cycle plot from Analytical Modelling....................................................... 15

    5.2. Cooling plots of thermal cycle by IR sensor Stationary Heat Source................... 16

    5.3. Effect of laser spot diameters on affected region..................................................... 20

    5.4. Effect of backing on solidification time................................................................... 23

    5.5. Effect of laser spot diameter on solidification time................................................. 24

    5.6. Thermal Cycle for 1mm mild steel plate Moving Heat Source............................ 25

    5.7. Effect of backing plate on cooling rate Moving Heat Source............................... 26

    5.8. Cr, effective radial heat conduction: Moving Heat Source...................................... 32

    6. CONCLUSION.............................................................................................................. 35

    7. REFERENCES............................................................................................................... 36

    8. APPENDIX..................................................................................................................... 37

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    1

    1. INTRODUCTION

    Modification of surface properties over multiple length scales plays an important role

    in optimizing a materials performance for a given application. Lasers provide the

    ability to accurately deliver large amounts of energy into confined regions of a

    material in order to achieve a desired response. For opaque materials, this energy is

    absorbed near the surface, modifying surface chemistry, crystal structure, and/or

    multiscale morphology without altering the bulk.

    Cooling rate during laser treatment plays a crucial role in material surface properties.

    Cooling time for a finite mild steel sheet on irradiation with laser beam is slow as heat

    gets accumulated in it. So the study of backing plate and laser spot diameter effect on

    the cooling rate becomes useful to control the cooling trend. Analytical Modelling

    becomes important in such case to understand the process and control it. The target

    with modelling is:

    i. Semi quantitative understanding of the process mechanisms for the design of

    experiments and display of results dimensional analysis, order of magnitude

    calculations.

    ii.Parametric understanding for control purposes empirical and statistical charts,

    analytic models.

    iii.Detailed understanding to analyse the precise process mechanisms for the

    purpose of prediction, process improvement and the pursuit of knowledge

    analytic and numeric models.

    The analytical model for semi-infinite composite body considers both the body to be

    semi-infinite [1]. Later a partitioning function was established to take into account the

    laser treatment of finite sheet kept on a semi-infinite sheet [2]. It tries to quantify the

    fraction of heat flow from top body to the bottom body at the interface. Clearly it now

    helps to understand the cooling trend for a finite sheet irradiation by laser beam for

    parameters like spot diameter, scan speed, power, backing material etc.

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    2

    2. LITERATURE SURVEY

    Mathematical modelling is a tool to understanding and control of a process. There are

    many research papers depicting the shear importance of this tool to analyse a process

    undertaking certain assumptions. Steen and Mazumder [3]have discussed quite a few

    analytical models:

    i. Analytic models in 1-d heat flow.

    a. Assumption: Heat flows in 1 direction and there is no convection or heat

    generation. Equation:

    T(z, t) = 2Fo(t)0.5/K ierfc{z/2(t)0.5}, = thermal diffusivity, Fo = absorbed intensity, t = interaction timeii. Analytical models for a stationary point source.

    a. The instantaneous point source

    b. The continuous point source: Since heat is not a vector quantity the effects

    from different heat sources can be added [4].

    c. Source other than point source: By integrating point source solution over an

    area it is possible to calculate the heating from line sources, disc sources or

    Gaussian sources. Carslaw and Jaeger [1] discusses solutions for nearly anygeometry.

    iii. Analytical models for a moving point source: By integrating the point

    solution over time and moving it by making x= (xo+vt). Rosenthal [5]

    developed the well-known fundamental welding equations.

    iv. Analytical keyhole models-Line source solution: Assumed that energy is

    absorbed uniformly along a line in the depth direction.

    Carslaw and Jaeger [1] discussed the analytical modelling for semi-infinite

    composite solid. It considers that suppose the region x>0 is of one substance, K1,

    1, k1 and x0 and K1T1/x = K2T2/x , at x=0,

    t>0 where T1is for the temperature in the region x>0, and T2for that in the region

    x

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    3

    i. The initial temperature T, constant, in x>0 and zero in x 0 at the constant rate

    Foper unit time per unit area in the plane x=0. Solving gave:

    T2 = 2Fo(k1k2t)0.5K1k20.5 + K2k10.5 ierfc z , = 2k2t

    Both the above analytical model was derived assuming the composite body is of semi-

    infinite length.

    Duley [2]presented, in his book, the concept of partitioning function. The book

    discusses the effect of semi-infinite body on analytical model of finite thickness

    composite body; here the semi-infinite body act a base material for a finite body. It

    says that when a finite body with K1, 1, k1 is kept on a semi-infinite body with

    material property K2, 2and k2, where K, and k are thermal conductivity, density

    and thermal diffusivity of the respective bodies, the heat partitioned at the interface is

    given by a partitioning function:

    Pr = K1k2 K2k1K1k2 + K2k1

    Cooling rate plays an important role in deciding the microstructure of the material.

    The rate with which solidification occurs is equally important and controlling it by

    changing various parameters can be achieved. Laser surface processing has been a

    key element in a number of large-scale industrial manufacturing operations, yet at the

    same time it continues to reinvent it-self and find ever new uses in emerging areas.

    Matthew et al. [6] discusses some of the versatile capabilities of laser processing to

    modify the surface properties of materials in order to enhance their performance for a

    variety of applications.

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    4

    3. ANALYTICAL MODELLING

    For an infinitely thick sheet subjected to uniform heat flux at the entire top surface as

    shown in Fig. 3.1 solution of temperature field can be obtained by solving the

    following equation:

    Fig 3.1. Schematic representation of an infinite sheet subjected to uniform heat flux at the top

    surface.

    2T(z, t)z2 = 1K T(z, t)t , K Tzz=0 = H,T|z= = T0 T|t=0 = T0 z (3.1)

    Here, T, z, t, k, K, H and T0 denote temperature, depth from the top surface, time,

    thermal diffusivity, thermal conductivity, magnitude of heat flux and initial sheet

    temperature respectively. Now, a moving laser beam takes d/v time to move over a

    point on its scan path where the laser beam diameter is d and v is the scans peed. If

    the laser spot diameter d and the sheet thickness h are much larger than the thermal

    diffusion length, given by 2kd/v corresponding to the time, d/v the sheet can beconsidered to be semi-infinite and this heat transfer problem can be approximated to

    be similar to the situation depicted in Fig. 1. In that case the temperature as a function

    of z and t can be obtained as follows [3]:

    For t

    d/v (i.e during heating),

    T = T0 + HK ierfcz , = 2kd/vFor td/v (i.e during cooling), (3.2)T = T0 + H

    Kierfcz ierfc z , = 2k(t d/v)

    Here, H is taken as absorbed laser power intensity at the top surface (z = 0), 4 / (d2),

    A and P being absorptivity and laser power respectively. Considering semi-infinite

    sheet but adding a correction term for radial heat conduction loss the solution givenby Eq.(3.2) can be modified as the following [2]:

    H

    Z = 0

    Z

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    5

    For td/v (i.e during heating),T = T

    0+

    HK

    ierfc

    z

    ierfc

    z2 + (d2/4)1/2

    ,

    = 2

    kd/v

    For td/v (i.e during cooling), (3.3)T = T0 + H

    Kierfc z ierfcz2 + (d2/4)

    1/2

    ierfc z ierfcz2 + (d2/4)1/2

    , = 2k(t d/v)Considering the sheet to have finite thickness the solution of temperature field without

    radial heat conduction loss can be obtained as follows [4]:

    Fig 3.2. Laser irradiation on a finite sheet of thickness h unit

    For td/v (i.e during heating),T = T0 + H

    Kierfc|2(i 1) h+ z| + ierfc|2ih z| ni=1

    For td/v (i.e during cooling),(3.4)

    T = T0 +H

    Kierfc|2(i

    1) h+ z|

    + ierfc|2ih

    z|

    ni=1 ierfc|2(i 1) h+ z| + ierfc|2ih z| , = 2k(t d/v)

    Here, theoretically the value of n should be infinite but practically this solution

    converges rapidly with increasing value of n. Thus, combining the approaches used

    for obtaining Eqs. (3.3) and (3.4) a solution of temperature for finite sheet thickness

    with radial conduction loss can be arrived at as given by [7],

    2h-Z

    h

    Z = 0

    Z

    Laser beam

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    6

    For td/v (i.e during heating),T = T0 + HKierfc|2(i 1 )h+ z|

    ierfc(2(i 1)h+z)2 + (d2/4)1/2

    n

    i=1+ ierfc|2ih z| ierfc(2ih z)2 + (d2/4)1/2

    For td/v (i.e during cooling), (3.5)T = T

    0+

    H

    K

    ierfc |2(i 1)h+z| ierfc(2(i 1)h+z)2 + (d2/4)

    1/2 +ierfc |2ih z| ierfc

    (2ih

    z)

    2+ (d

    2/4)

    1/

    2

    n

    i=1

    ierfc |2(i 1)h+z| ierfc(2(i 1)h+z)2 + (d2/4)1/2 +ierfc |2ih z| ierfc(2ih z)2 + (d2/4)1/2

    A plate with finite thickness is kept over a substrate of semi-infinite length. (K1, k1, 1,

    Cp1) and (K2, k2, 2, Cp2) denotes the thermal conductivity, thermal diffusivity, densityand specific heat capacity of the top plate and substrate respectively.

    Now for material properties and scan speed such that the diffusion length > h ,where = 2k1d/v, h is the plate thickness, d is beam diameter and vis scan speed,a partitioning function Prcomes into equation 5 accounting for the heat partitioned by

    the substrate top surface.

    For t

    d/v (i.e during heating),

    T = T0 + HKPri ierfc|2(i 1) h+ z| ierfc(2(i 1)h + z)2 + (d2/4)

    1/2

    ni=0

    + ierfc|2ih z| ierfc(2ih z)2 + (d2/4)1/2

    For td/v (i.e during cooling), (3.6)

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    7

    T = T0 + HK Pri

    ierfc |2(i 1)h+z| ierfc(2(i 1)h + z)2 + (d2/4)1/2 +ierfc |2ih z| ierfc(2ih z)2 + (d2/4)1/2

    ni=0

    ierfc |2(i 1)h+z| ierfc(2(i 1)h+z)2 + (d2/4)1/

    2 +ierfc |2ih z| ierfc(2ih z)2 + (d2/4)1/2

    Where partitioning function is given as [2]:

    Pr = K1k2 K2k1K1k2 + K2k1

    During laser processing, for a stationary heat source, radial heat conduction takes

    place in all direction i.e. effectiveness of radial heat conduction Cr= 1. For a moving

    heat source Cr< 1 as radial heat conduction along the scan direction is negligible. So

    this factor Crwas multiplied to the radial part of the equation 3.6.

    For td/v (i.e during heating),T = T

    0+

    HK

    P

    ri

    ierfc

    |2(i 1 )h+ z|

    C

    r ierfc

    (2(i 1 )h+ z)2 + (d2/4)1/2

    n

    i=0+ ierfc|2ih z| Cr ierfc(2ih z)2 + (d2/4)1

    /2 For td/v (i.e during cooling), (3.7)T= T0

    +

    H

    KPri ierfc

    |2(i 1)h + z|

    Cr ierfc

    (2(i 1)h + z)2 + (d2/4)1/2

    +

    ierfc |2ih z| Cr ierfc(2ih z)2 + (d2/4)1/2

    ni=0

    ierfc |2(i 1) h+ z| Cr ierfc(2(i 1)h + z)2 + (d2/4)1/2 +ierfc |2ih z| Cr ierfc(2ih z)2 + (d2/4)1/2

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    8

    Fig 3.3. Schematic representation of heat partitioned at the z=0 interface

    Here in the above figure 3.3, heat gets partitioned at the interface of the two body at Z

    = 0. This partitioning is represented in the figure.

    E2 = Pr E1, where Pr = K1k2 K2k1K1k2 + K2k1

    Fig.3.4. (i) Radial conduction for stationary laser beam, (ii) Radial conduction for moving

    laser source beam

    The above figure 3.4 represents the schematic for radial heat conduction in two cases,

    i.e. for stationary heat source and moving heat source respectively. For stationary heat

    source since heat conduction is in all the direction Cr = 1is applied and for movingheat source since there is no conduction along the scan speed direction Crvalue has to

    be less than 1.

    Cr(i) = 1Cr(ii) < Cr(i)

    Z = 0

    ZE1

    E3

    E2

    Semi-infinite body

    K1, k

    1,

    1,C

    p1

    K2, k

    2,

    2, C

    p2

    Finite, h mm

    Laser beam

    V=0

    Scan Speed, V mm/min

    iii

    Laser beam

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    9

    4. EXPERIMENTAL DETAILS

    4.1.Specifications of Laser used

    The experiments were carried out with a 2 kW Ybfiber laser (IPG photonics, Model

    no. YLR - 2000) operating at 1.07 m wavelength. This can be operated in CW and

    pulsed-mode in 501000 Hz frequency range with 5100% duty cycle. The laser

    beam delivery system is mounted on a 5-axis CNC machine capable to move at

    speeds up to 20 m/min scan speed effectively.

    Fig. 4.1.1.2 kW Ybfiber laser

    The actual power of this laser is not same as the power set. This laser was capable of

    providing power upto 1280 W.

    During the experiments it was observed that the laser on time for 0.5 sec input on time

    was more than this. A diode oscilloscope setup was used to find the machines

    actual on time. It was found that the laser on time for 0 sec input laser interaction time

    was 0.9 sec and for 0.5 sec input time it was ~ 1.4 sec. Below fig. 4.1.2. and fig. 4.1.3.

    represents the pulse on time generated using oscilloscope. The extra 0.85 sec without

    any input on time is the time taken by the machine to read the programm lines. For fig

    4.1.2 each division represents 200ms and so total pulse on time is 4.5 times 200ms

    which is ~ 0.9 sec. Similarliy for fig 4.1.3 each division is 197ms and so total pulse on

    time is 7 times 197ms which is ~ 1.4 sec.

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    Fig. 4.1.2.laser on time pulse for 0 sec input interaction time

    Fig. 4.1.3.laser on time pulse for 0.5 sec input interaction time

    4.2.Experiment Procedure and Laser Parameters

    For a stationary heat source mild steel plate of finite thickness with various backing

    plates was irradiated with a staionary laser beam for 0.9sec. It was carried out to see

    the affect of thermal conductivity of the backing plates on temperature behavior or the

    cooling trend of the heat affected zone at Z=0 or in other words to observe the effect

    of partitioing fucniton used in the anlytical model of the same. Also, the affected

    region on the top surface of the mild steel due to laser irradiation gives us an idea

    about radial and vertical conduction of heat for different backing plates. For this 3

    different laser spot diameters were used and the laser power was changed accordingly

    to maintain effective power density constant.

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    For moving heat source case similar procedure was followed with keeping spot

    diameter constant at 3mm and changing the scan speed for a given power.

    Table 4.2.1.Laser parameters for stationary heat source, interaction time kept constant at 0.9s

    Laser Spot diameter (mm) 2 3 4

    Laser Power (W) 300 675 1200

    Table 4.2.2.Laser parameters for Moving heat source, laser spot diameter constant at 3mm

    Laser Scan Speed (mm/min)

    400W 1000 1500 2000 2500 3000

    600W 2000 2500 3000 3500 4000

    Table 4.2.3.Materials used for the experiment and their properties. (source: EES and wikipidea)

    Conductivity (W/m/K) Density (Kg/m3) Specific heat (J/kg/K)

    Mild Steel (AISI-1020) 43 7850 620

    Stainless Steel 16 7873 504.8

    Aluminum 205 2688 936.6

    Laser parameters are so selected such that the thermal diffusion length is always much

    greater than the thickness of the top mild teel plate. From above thermal diffusivity of

    mild steel is

    k = K/Cp, 8.810-6m2/s = 2kt, where t interaction time is ~0.9sec. Hence, the thermal diffusion lengthis 5.6mmwhich is much more than 1mmmild steel plate.Mild steel with finitte thickness was kept on different material of semi-inifinite

    thickness. In this experiment mild steel was irradiated with stationary laser beam for

    six different samples and for each sample three laser spot diameters were used.

    Inorder to improve the contact between the 2 plates, a heat sink compound was

    applied in between the plates. For moving heat source the case with mild steel

    backing without heat sink compound was not carried out. Below mentioned are the six

    samples:

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    Mild Steel of finite

    thickness (1mm)

    Semi-Infinite Mild Steel

    Plate

    Mild Steel (1mm) + Mild

    Steel backing (13mm)

    Mild Steel (1mm) + Heat

    Sink + Mild Steel backing

    (13mm)

    Mild Steel (1mm) + Heat

    Sink + Stainless Steel

    backing (10mm)

    Mild Steel (1mm) + Heat

    Sink + Aluminium backing

    (12.5mm)

    To avoid repetition in the paper, following short forms have been used ahead:

    MS: Mild Steel; SS: Stainless Steel; Al: Aluminium; HSC/HS: Heat Sink Compound

    Below schematics represent the laser irradiation on MS plate for different samples:

    (a) (b)

    Fig 4.2.1(a) Schematic representation of a stationary laser beam falling on a semi-infinite mild steel

    plate for 0.9sec, (b) Schematic representation of a stationary laser beam falling on finite mild steel

    sheet placed on a backing material with heat sink compound applied

    (c) (d)

    Fig 4.2.2. (c) Schematic representation of a stationary laser beam falling on finite mild steel sheet for

    0.9sec, (b) Schematic representation of a stationary laser beam falling on finite mild steel sheet placedon a backing material with no heat sink applied

    Z = 0

    Z

    Z = 0

    Z

    Al or SS or

    Z = 0

    Z

    Z = 0

    Z

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    Temperature was measured with the help of a non-contact infrared (IR) sensor

    (Micro-Epsilon make, model no. CTLM-2HCF3-C3H, temperature range=385 C to

    1600 C, response time=1ms) during the heating process of the workpiece. All the

    readings of the plots generated using pyrometer is to be multiplied with a calibration

    factor of 2.3. So for this experiment the minimum temperature measure was 885.5 C.

    4.3.Absorptivity of Mild Steel (AISI-1020):

    The absorptivity of the 1mm mild steel surface was estimated by measuring the

    incident and reflected laser powers from the surface with a laser power meter (model-

    COMET-10K-V1 ROHS OPHIR make, accuracy 5%). The power meter needs a

    continuous laser exposure of 10 s for each measurement. The average value of

    absorptivity was estimated to be ~75%. Below fig. 4.3 shows the instruments used to

    find the AISI-1020 absorptivity.

    Fig. 4.3.1.(a) Power meter, model-COMET-10K-V1 ROHS OPHIR make, accuracy 5%(b) Laser

    head (c) Pyrometer (d) Mild steel, AISI-1020 sample placed at an angle of 450with the vertical

    To find absorptivity of AISI-1020 laser power was increased from 200W to 600W insteps of 100W and resulting absorptivity value from each has been averaged.

    a

    b

    c

    d

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    Mild steel sample was kept at an angle of 45o with the vertical. For a given laser

    power and 16mm laser spot diameter 3 readings T1, T2and T3were taken. Table 4.3

    below shows the data from the experimental values obtained from the power meter.

    AISI-1020 was irradiated with laser beam and the reflected laser power was captured

    by the power meter.

    Both the average laser power reflected and % absorptivity has been depicted through

    Table 4.3 and fig 4.3.2 histogram plot below.

    Table 4.3.Reading for laser power absorptivity for AISI-1020 at varied laser powers

    Laser Power

    (W)

    Reflected Power (W)AVG.

    %

    AbsorptivityT1 T2 T3

    200 116.8 106.3 116.3 113.1333 43.43

    300 147 121.9 136 134.97 55.01

    400 98.6 95.8 102.1 98.83 75.3

    500 89.2 87.3 92 89.5 82.1

    600 86.4 83.2 89 86.2 85.63

    Fig. 4.3.2.Plots representing the laser power absorptivity for AISI-1020 for varied laser power ranging

    from 200W to 600W in steps of 100W

    0

    20

    40

    60

    80

    100

    200 300 400 500 600

    %A

    bsorptivity

    Laser Power (W)

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    5. RESULTS AND DISCUSSION

    Analytical plots for Stationary heat source:

    5.1.

    Thermal cycle plot from Analytical Modelling

    Fig. 5.1.1.Thermal plot for top surface viz. z-=0 for different samples on being irradiated with a 2mm

    stationary laser spot diameter for 0.9sec from Analytical Model using MatLab

    Fig. 5.1.2.Thermal plot for top surface viz. z-=0 for different samples on being irradiated with a 3mm

    stationary laser spot diameter for 0.9sec from Analytical Model using MatLab

    0

    200

    400

    600

    800

    1000

    1200

    1400

    1600

    1800

    0 0.5 1 1.5 2

    Temp(C)

    Time (sec)

    Analytical Model: Temp vs Time, stationary heat source of 2mm spot diamater,P=300W

    Finite MS sheet

    AL backingMS backing

    SS backing

    0

    200

    400

    600

    800

    1000

    1200

    1400

    1600

    1800

    2000

    2200

    2400

    2600

    0 0.5 1 1.5 2

    Tem

    p(C)

    Time (sec)

    Analytical Model: Temp vs Time, stationary heat source of 3mm spot diamater,P=675W

    Finite MS Sheet

    AL backing

    MS backing

    SS backing

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    Experimental plots for stationary heat source:

    5.2. Cooling plots of thermal cycle by IR sensor Stationary Heat Source

    Fig. 5.2.1.Experimental thermal cycle at z-=0 for samples on being irradiated with a 4mm laser spot

    diameter for 0.9sec

    Fig. 5.2.2.Cooling plot for top surface i.e. z-=0 for different samples on being irradiated with a 2mm

    laser spot diameter for 0.9sec using experimental data

    0 500 1000 1500 2000 2500

    400

    500

    600

    700

    800

    900

    1000

    Time (millisec)

    Temp(C)

    Finite MS Sheet

    Semi-Infinite Sheet

    Thermal cycle for stationary laser beam of 4mm spot diameter, P=1200W

    885

    1085

    1285

    1485

    1685

    1885

    2085

    2285

    0 50 100 150 200 250

    Temp(C)

    Time (millisec)

    Experiment: Stationary heat source, 2mm spot diameter, P=300W

    1mm MS

    Semi-Infinite MS

    12.5mm Al backing

    13mm MS backing

    10mm SS backing

    MS backing without Hsink

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    Fig. 5.2.3.Cooling plot for top surface i.e. z-=0 for different samples on being irradiated with a 3mm

    laser spot diameter for 0.9sec using experimental data.

    Fig. 5.2.4.Cooling plot for top surface i.e. z-=0 for different samples on being irradiated with a 4mm

    laser spot diameter for 0.9sec using experimental data.

    885

    1085

    1285

    1485

    1685

    1885

    2085

    0 200 400 600 800

    Temp(C)

    Time (millsec)

    Experiment: Stationary heat source, 3mm spot diameter, P=675W

    1mm MS

    Semi-infinite MS

    12.5mm Al backing

    13mm MS backing

    10mm SS backing

    MS backing without Hsink

    885

    1085

    1285

    1485

    1685

    1885

    2085

    2285

    0 500 1000 1500

    Temp(C)

    Time (millisec)

    Experiment: Stationary heat source, 4mm spot diameter, P=1200W

    1mm MS

    Semi-Infinite MS

    12.5mm Al backing

    13mm MS backing

    10mm SS backing

    MS backing without Hsink

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    From the above cooling plots from the experimental data, cooling rate trend is plotted

    to analyse the variation in the cooling rate within a sample for different laser spot

    diameters and also compare the cooling rates for a same spot diameter for different

    samples.

    Fig. 5.2.5.Cooling rate for samples at z = 0 on irradiation with stationary source of different spot

    diameters

    The above cooling rate bar graphs have been generated considering the time taken for

    different sample to cool down from a particular temperature to another at z=0.

    Suppose the temperature at time t1 is T1 C and at time t2 is T2 C where t2 > t1,

    cooling rate is given by (T1 T2)/(t2 t1)C/sec. For our calculation below are theT1and T2considered for plotting cooling rate bar graphs:

    Table 5.2.Temperature at two fixed interval for different spot diameter:

    Spot dia T1, C T2, C

    2mm 1345 885.5

    3mm 1345 885.5

    4mm 1288 885.5

    From both the plots i.e. cooling curves from experimental data fig. 5.2.2 - 5.2.4 and

    0

    2000

    4000

    6000

    8000

    10000

    12000

    14000

    16000

    Finite MSsheet

    MS backingwithout HS

    SS backing MS backing Al backing Semi-InfiniteMS sheet

    CoolingRate(C/sec)

    Cooling Rate of samples for different laser spot diameters at z=0

    2mm

    3mm

    4mm

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    cooling rate bar graph fig. 5.2.4, it is observed that:

    1. Cooling rate, at z=0, for a sample decreases with increase in laser spot diameter

    and this trend is maintained for all six samples. This may be due to the difference

    in temperature gradient for varying spot diameters. The radial temperature

    gradient decreases with increase in spot diameter. Now as radial conduction will

    be higher for higher temperature gradient hence cooling for 2mm spot diameter

    will be faster than the 3mm and 4mm spot diameters.

    2. Cooling rate, at z=0, for a given spot diameter is minimum for finite mild steel

    sheet, maximum for semi-infinite mild steel sheet and lies in between for rest

    samples.

    3.

    Cooling rate with Al backing, MS backing and SS backing were in decreasingorder respectively for a given spot diameter. Reason for such trend can be argued

    with their respective thermal conductivity which is also in decreasing order.

    4. Although theoretically cooling rate for sample with Al backing should have been

    higher than that of semi-infinite mild steel sheet but experimentally it didn't

    follow the trend. This shows that even the application of heat sink compound

    couldn't create a proper contact between mild steel and aluminium creating

    resistance.

    5. Cooling rate of mild steel backing with heat sink compound at z=0 is more than

    that of mild steel backing without heat sink compound because of the presence of

    air gap layer in the latter. Conductivity of air is very low and hence heat gets

    accumulated rather being conducted.

    Decrease in cooling rate with increase in laser spot diameter can be explained through

    the following reasoning:

    i.

    It is known that the thermal conduction is higher for high temperature

    gradient. Radial temperature gradient dT/dX decreases with increase in spot

    diameter, hence cooling for a 2mm laser spot is faster than a 3mm laser spot

    diameter and so on.

    ii. = L2/ k, where is thermal diffusion time, L is thermal diffusion length and

    kis thermal diffusivity. is defined as the time it takes for heat to travel over a

    distance L. Following this it is clear that energy travel in 2mm spot diameter is

    faster than 3mm and so on.

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    Fig. 5.2.6.(a) Intensity distribution for different spot radius (b) Olympus Model SZ 1145TR PR zoom

    sterio microscope (c) 3X Magnification image of affected region for 3mm spot on finite MS sheet

    5.3. Effect of laser spot diameters on affected region

    To have a better understanding of radial heat conduction vs heat conduction along the

    depth considering variation in laser spot diameters and 0.9 sec interaction time,

    circular plots of the affected region is generated for different samples.

    Fig. 5.3.1 shows the samples which are irradiated with a stationary laser beam varying

    the spot diameter as 2mm, 3mm and 4mm respectively keeping the power density

    constant. The above fig.5.2.6 (b) and (c) represents the images of those affected

    region on the material surface taken using a high resolution optical microscope. To

    plot the schematic of affected region, the images from optical microscope was

    measured using software ImageJ.

    Table 5.3.Radius of the heat affected zone on the samples surface:

    Radius of the affected region for different Laser spot diameters (mm)

    Samples For 2mm spot For 3mm spot For 4mm spot

    Finite MS sheet 2.718 3.875 5.264

    MS backing without HS 2.651 3.655 4.394

    SS backing 2.412 3.271 4.349

    MS backing 2.257 3.169 4.224

    Al backing 1.818 3.073 4.043

    Semi-Infinite MS sheet 1.526 2.306 3.132

    The above table 5.3 shows radius of the affected region on the sample surface for

    different laser spot diameter. All the measurements are in mm.

    r1=2mm

    r2=3mm

    r

    r2

    r1Spot dia 3mm, Finite

    MS sheet

    , 3X Magnification

    ab

    c

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    Fig. 5.3.1. (a) Heat affected region on the finite mild steel sheet for different laser spot diameter, (b)

    Affected region on the semi-infinite mild steel sheet for different laser spot diameter

    Fig. 5.3.2. Plot of heat affected region on sample surface; 2mm spot diameter, P = 300W, V=0 and t=

    0.9 sec, laser interaction time

    For all the three cases with different laser power and spot diameters such that the laser

    power intensity remains to be a constant, in MS plate with backing condition with

    heat sink the affected region radius increases as the thermal conductivity of the

    backing plate decreases. For finite MS sheet the radius is maximum as in this case

    radial heat conduction is maximum and heat gets accumulated. Comparing affected

    region for MS backing with and without heat sink, the backing condition with heat

    sink compound has smaller affected region as the heat sink compound creates a better

    contact improving the thermal conduction along the depth as compared to the other

    situation.

    4mm 3mm

    2mm

    (a) (b)

    mm

    mm

    -3 -2 -1 0 1 2 3

    2.5

    -2

    1.5

    -1

    0.5

    0

    0.5

    1

    1.5

    2

    2.5

    1mm MS

    Bulk MS

    AL backing

    MS backing

    SS backing

    MS without HS

    2mm spot dia

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    Fig. 5.3.3. Plot of heat affected zone on sample surface; 3mm spot diameter, P = 675W, V=0 and t=

    0.9sec, laser interaction time

    Fig. 5.3.4. Plot of heat affected zone on sample surface; 4mm spot diameter, P = 1200W, V=0 and t =

    0.9 sec, laser interaction time

    mm

    mm

    -4 -3 -2 -1 0 1 2 3 4

    -4

    -3

    -2

    -1

    0

    1

    2

    3

    4

    1mm MS

    Bulk MS

    AL backing

    MS backing

    SS backing

    MS without HS

    3mm spot dia

    mm

    mm

    -6 -4 -2 0 2 4 6

    -5

    -4

    -3

    -2

    -1

    0

    1

    2

    3

    4

    5

    1mm MS

    Bulk MSAL backing

    MS backing

    SS backing

    MS without HS

    4mm spot dia

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    5.4. Effect of backing on solidification time

    Fig. 5.4.1. Cooling curve for different samples; 3mm spot diameter, P=675W, V=0(scan speed) and t =

    0.9 sec, laser interaction time

    Fig. 5.4.2. Cooling curve for different samples; 4mm laser spot dia, P=1200W, V=0(scan speed) and t

    = 0.9sec laser interaction time

    In Fig. 5.4.1 and 5.4.2 the duration of horizontal trend during cooling or the durationbetween the changes in slopes depict the solidification time.

    885

    1085

    1285

    1485

    1685

    1885

    2085

    0 200 400 600 800 1000 1200

    Temp(C)

    Time (millisec)

    Cooling curve for staitionary heat source of 3mm spot diameter

    Finite MS sheet

    MS backing without HS

    10mm SS backing

    13mm MS backing

    12.5mm Al backing

    Semi-Infinte MS

    885

    1085

    1285

    1485

    1685

    1885

    2085

    2285

    0 400 800 1200 1600 2000

    Temp(C)

    Time (millisec)

    Cooling curve for staitionary heat source of 4mm spot diameter

    Finite MS sheet

    MS backing without HS

    10mm SS backing

    13mm MS backing

    12.5mm Al backing

    Semi-Infinte MS

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    5.5. Effect of laser spot diameter on solidification time

    Fig. 5.5.1. Cooling trend at z=0 for finite mild steel sheet with different laser spot diameters

    Fig. 5.5.2. Cooling trend at z=0 for semi-infinite mild steel sheet with different laser spot diameters

    In fig. 5.5.1 and 5.5.2 it can be observed that the solidification time increases with

    increase in spot diameter because the cooling rate decreases with spot diameter

    increment.

    885

    1085

    1285

    1485

    1685

    1885

    2085

    2285

    0 200 400 600 800 1000 1200

    Temp(C)

    Time (millisec)

    Cooling curve for stationary heat source on 1mm mild steel plate

    2mm Spot Dia

    3mm Spot Dia

    4mm Spot Dia

    885

    1085

    1285

    1485

    1685

    1885

    2085

    0 50 100 150 200 250

    Temp(C)

    Time (millisec)

    Cooling curve for stationary heat source on a semi-infinite MS plate

    2mm Spot Dia

    3mm Spot Dia

    4mm Spot Dia

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    5.6. Thermal Cycle for 1mm mild steel plate Moving Heat Source

    Experimental plots for Moving heat source:

    Fig. 5.6.1. Thermal cycle for 1mm MS plate at varying scan speed at z = 0, P = 400W and 3 spot

    diameter

    Fig. 5.6.2. Thermal cycle for 1mm MS plate at varying scan speed at z = 0, P = 600W and 3 spot

    diameter

    885

    1085

    1285

    1485

    1685

    1885

    2085

    0 100 200 300 400 500 600

    Temp

    (C)

    Time (millisec)

    Thermal cycle for 1mm MS plate, P=400W, 3mm spot diameter

    1000 mm/min

    1500 mm/min

    2000 mm/min

    2500 mm/min3000 mm/min

    885

    1085

    1285

    1485

    1685

    1885

    2085

    0 50 100 150 200 250

    T

    emp(C)

    Time (millisec)

    Thermal cycle for 1mm MS plate, P=600W, 3mm spot diameter

    2000 mm/min

    2500 mm/min

    3000 mm/min3500 mm/min

    4000 mm/min

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    5.7. Effect of backing plate on cooling rate Moving Heat Source

    Cooling plots for moving heat source, P = 600W, 3mm spot diameter:

    Fig. 5.7.1. Cooling cycle at z = 0 for various samples with P = 600W, 3 spot diameter and

    2000mm/min scan speed as laser parameter

    Fig. 5.7.2. Cooling cycle at z = 0 for various samples with P = 600W, 3 spot diameter and

    2500mm/min scan speed as laser parameter

    885

    985

    1085

    1185

    1285

    1385

    1485

    1585

    1685

    1785

    0 50 100 150 200

    Temp(C)

    Time (millisec)

    P = 600W, V = 2000mm/min and 3mm spot diameter

    1mm MS

    Al backing with HS

    MS backing with HS

    SS backing with HS

    Bulk MS

    885

    1085

    1285

    1485

    1685

    1885

    2085

    0 20 40 60 80 100

    Temp(C)

    Time (millisec)

    P = 600W, V = 2500mm/min and 3mm spot diameter

    1mm MS

    Al backing with HS

    MS backing with HS

    SS backing with HS

    Bulk MS

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    Fig. 5.7.3. Cooling cycle at z = 0 for various samples with P = 600W, 3 spot diameter and

    3000mm/min scan speed as laser parameter

    Fig. 5.7.4. Cooling cycle at z = 0 for various samples with P = 600W, 3 spot diameter and

    3500mm/min scan speed as laser parameter

    885

    985

    1085

    1185

    1285

    1385

    1485

    1585

    1685

    1785

    1885

    0 10 20 30 40

    Temp(C)

    Time (millisec)

    P = 600W, V = 3000mm/min and 3mm spot diameter

    1mm MS

    Al backing with HS

    MS backing with HS

    SS backing with HS

    Bulk MS

    885

    985

    1085

    1185

    1285

    1385

    1485

    1585

    1685

    0 10 20 30 40

    Temp(C)

    Time (millisec)

    P = 600W, V = 3500mm/min and 3mm spot diameter

    1mm MS

    Al backing with HS

    MS backing with HS

    SS backing with HS

    Bulk MS

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    From the above cooling plots from the experimental data, cooling rate trend is plotted

    to analyse the variation in the cooling rate within a sample for different laser scan

    speed and also compare the effect on cooling rates for a same scan speed for different

    samples.

    Fig. 5.7.5.Cooling rate for samples at z = 0 on irradiation with moving heat source of different scan

    speed, P = 600W and 3mm spot diameter

    The above cooling rate bar graphs have been generated considering the time taken for

    different sample to cool down from a particular temperature to another at z=0.

    Suppose the temperature at time t1 is T1 C and at time t2 is T2 C where t2 > t1,

    cooling rate is given by (T1 T2)/(t2 t1)C/sec. For our calculation below are theT1and T2considered for plotting cooling rate bar graphs:

    Table 5.7.1.Temperature at two fixed interval for a given laser scan speed, P = 600W:

    Scan Speed(mm/min) T1, C T2, C

    2000 1480 885.5

    2500 1400 885.5

    3000 1500 885.5

    3500 1400 885.5

    0

    5000

    10000

    15000

    20000

    25000

    30000

    1mm Sheet SS backing with

    HS

    MS backing with

    HS

    Al backing with

    HS

    Bulk MS

    Cooling

    Rate(C/sec)

    2000 mm/min 2500 mm/min 3000 mm/min 3500 mm/min

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    While plotting the above cooling rate histogram plots, for a given scan speed, T1C

    and T2 C temperature during the cooling cycle chosen was same across all the

    samples so as to compare the cooling rates.

    Observation:

    i. For a given laser scan speed cooling rate is least for 1mm mild steel sheet, it

    is maximum for bulk mild steel sheet and it ranges in between these two

    extremes for the backing conditions. Cooling rate for a given scan speed

    increases with the increase in thermal conductivity of the backing plate.

    Reasoning for this observation remains same as discussed earlier in the case

    of samples irradiation by a stationary heat source.

    ii.

    With the increase in laser scan speed the effect of backing plate decreases

    i.e. for higher scan speed value of 3500 mm/min the cooling rate across all

    samples are nearly close by and consecutively the effect of backing plate is

    not observed. This may be because with the increase in scan speed laser

    interaction time decreases and hence the thermal diffusion length also

    decreases. Due to this for higher scan speed, as for above case, thermal

    effect due to laser barely reaches the interface. As mentioned above the

    thickness of mild steel sheet is 1mm. Now considering the above scan

    speeds value, the theoretical thermal diffusion length = 2kd/vare:a) For 3500 mm/min, ~1.3mm

    b) For 3000 mm/min, ~ 1.45mmc) For 2500 mm/min, ~ 1.6mmd) & For 2000 mm/min, ~ 1.8mm

    Clearly for 2000mm/min,

    ~ 1.8mm is greater than the mild steel sheet

    thickness of 1mm as compared to laser scan speed of 3500 mm/min for

    which it is closer to the mild steel sheet thickness.

    iii. For a given sample with increase in laser scan speed cooling rate increases.

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    Cooling plots for moving heat source, P = 400W, 3mm spot diameter

    Fig. 5.7.6. Cooling cycle at z = 0 for various samples with P = 400W, 3 spot diameter and

    1000mm/min scan speed as laser parameter

    Fig. 5.7.7. Cooling cycle at z = 0 for various samples with P = 400W, 3 spot diameter and

    1500mm/min scan speed as laser parameter

    For both 600W and 400W cooling curves for varying scan speed at constant spot

    diameter the cooling rate trend is in match with the trend observed for stationary heat

    885

    985

    1085

    1185

    1285

    1385

    1485

    1585

    1685

    1785

    1885

    0 100 200 300 400

    Temp(C)

    Time (millisec)

    P = 400W, 3mm spot diameter and V = 1000 mm/min

    1mm MS

    Al backing with HS

    MS backing with HS

    SS backing with HS

    Bulk MS

    885

    1085

    1285

    1485

    1685

    1885

    2085

    0 10 20 30 40 50 60 70 80 90 100 110 120 130

    Temp(C)

    Time (millisec)

    P = 400W, 3mm spot diameter and V = 1500 mm/min

    1mm MS

    Al backing with HS

    MS backing with HS

    SS backing with HS

    Bulk MS

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    source i.e. with the increase in backing plate thermal conductivity cooling rate also

    increases.

    From the above cooling plots from the experimental data, cooling rate trend is plotted

    to analyse the variation in the cooling rate within a sample for different laser scan

    speed and also compare the effect on cooling rates for a same scan speed for different

    samples.

    Fig. 5.7.8.Cooling rate for samples at z = 0 on irradiation with moving heat source of different scan

    speed, P = 400W and 3mm spot diameter

    The above cooling rate bar graphs have been generated considering the time taken for

    different sample to cool down from a particular temperature to another at z=0.

    Suppose the temperature at time t1 is T1 C and at time t2 is T2 C where t2 > t1,

    cooling rate is given by (T1 T2)/(t2 t1)C/sec. For our calculation below are theT1and T2considered for plotting cooling rate bar graphs:

    Table 5.7.2.Temperature at two fixed interval for a given laser scan speed, P = 400W:

    Scan Speed(mm/min) T1, C T2, C

    1000 1500 885.5

    1500 1450 885.5

    1931.42

    5873.13

    2227.71

    6930.25

    3863.11

    7275.26

    4783.64

    8162.54

    5825.94

    9922.81

    0

    2000

    4000

    6000

    8000

    10000

    12000

    1000 mm/min 1500 mm/min

    CoolingRate(C/sec)

    Cooling Rate of samples for different laser Laser scan speed, P = 400W

    1mm Sheet

    SS backing with HS

    MS backing with HS

    Al backing with HS

    Bulk MS

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    5.8. Cr, effective radial heat conduction: Moving Heat Source

    Fig. 5.8.1. Cooling cycle at z = 0 from IR pyrometer for 1mm MS sheet, P = 400W, 3 spot diameter

    and varying laser scan speed

    Fig. 5.8.2. Cooling cycle at z = 0 from Analytical model for 1mm MS sheet, P = 400W, 3 spot diameter

    and varying laser scan speed, Cr= 0.7

    885

    935

    985

    1035

    1085

    1135

    1185

    1235

    1285

    1335

    0 20 40 60 80 100

    Temp(C)

    Time (millsec)

    Experimenatal: P=400 W and 3mm spot diameter

    2000 mm/min

    2500 mm/min

    885

    935

    985

    1035

    1085

    1135

    1185

    1235

    1285

    1335

    0 20 40 60 80 100

    T

    emp(C)

    Time (millisec)

    Analytical: P=400 W and 3mm spot diameter, Cr = 0.7

    2500 mm/min

    2000 mm/min

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    Fig. 5.8.3. Cooling cycle at z = 0 from IR pyrometer for 1mm MS sheet, P = 600W, 3 spot diameter

    and varying laser scan speed

    Fig. 5.8.4. Cooling cycle at z = 0 from Analytical model for 1mm MS sheet, P = 600W, 3 spot diameter

    and varying laser scan speed, Cr= 0.7

    885

    985

    1085

    1185

    1285

    1385

    1485

    1585

    1685

    0 20 40 60 80

    Temp(C)

    Time (millisec)

    Experimental: P=600 W and 3mm spot diameter

    3500 mm/min

    4000 mm/min

    4500 mm/min

    885

    985

    1085

    1185

    1285

    1385

    1485

    1585

    1685

    0 20 40 60 80

    Temp(C)

    Time (millisec)

    Analytical: P=600 W and 3mm spot diameter, Cr = 0.7

    3500 mm/min

    4000 mm/min

    4500 mm/min

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    Fig. 5.8.5. Cooling cycle at z = 0 from Analytical model for 1mm MS sheet, P = 600W, 3 spot diameter

    and varying laser scan speed, Cr= 1

    At 400W and 600W thermal cycle plots from both experimental and analytical

    modelling has been generated as shown in above fig 5.8.1 5.8.5. Laser spot diameter

    was kept at 3mm and the laser scan speed was varied for a given laser power such that

    the melting case do not occur. The analytical model developed earlier is based on non

    melting condition. To get a match for the thermal cycle with the experimental plot,

    parameters are such chosen so as to avoid melting. By keeping the laser absorptivity

    for AISI 1020 at ~75% and changing the Crvalue manually, thermal cycle plot was

    generated using MatLab programming.

    The value for Crwas manually fed from 0.5 1.

    Observation:

    i. It was observed that for a range of ~0.7-0.75 Crvalue and keeping all other

    parameters same, the thermal cycle plot from analytical model is in good

    agreement with the experimental graphs.

    ii. It is clearly seen from fig 5.8.5 that the C r= 1 incorporation to the analytical

    model under predicts and is not in good agreement with the experimental

    results observed in fig 5.8.3.

    885

    985

    1085

    1185

    1285

    1385

    1485

    1585

    1685

    0 20 40 60 80

    Temp(C)

    Time (millisec)

    Analytical: P=600 W and 3mm spot diameter, Cr = 1

    3500 mm/min

    4000 mm/min

    4500 mm/min

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    CONCLUSION

    1. Cooling rate, at z=0, for a sample decreases with increase in laser spot

    diameter and this trend is maintained for all the six samples considered.2. Cooling is faster as the thermal conductivity of the backing material, with heat

    sink compound, increases but for a same backing material, without heat sink

    compound, it decreases.

    3. Solidification time follows the same trend as above, viz. for a given sample it

    decreases with the decrease in spot diameter. For a given spot diameter, with

    increase in thermal conductivity of backing plate it decreases.

    4. Heat affected region for a given spot diameter decreases with increase in the

    conductivity of the backing plate with heat sink compound. It is maximum for

    finite MS sheet and minimum for semi-infinite MS sheet in the considered

    sample range.

    5. For a given laser scan speed cooling rate is least for 1mm mild steel sheet, it is

    maximum for bulk mild steel sheet and it ranges in between these two

    extremes for the backing conditions. Cooling rate for a given scan speed

    increases with the increase in thermal conductivity of the backing plate.

    6. With the increase in laser scan speed the effect of backing plate decreases viz.

    for higher scan speed value of 3500 mm/min cooling rate across all samples

    are nearly close by and consecutively the effect of backing plate is not

    observed.

    7. For a range of ~0.7-0.75 Crvalue thermal cycle plot from analytical model is

    in good agreement with the experimental graphs for a moving heat source at

    non-melting condition.

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    6. REFERENCES

    [1] Carslaw.H.S., Jaeger.J.C. "Conduction of Heat in Solids" 2nd Edition Oxford

    University Press, 1959.

    [2] Duley, W.W., 1983. Laser Processing and Analysis of Materials. Plenum

    Press, NewYork/London.

    [3] Steen, W.M., Mazumder, J., 2010. Laser Material Processing, 4th ed.

    Springer, London,pp. 256258.

    [4] McBride, R., Bardin, F., Gross, M., Hand, D.P., Jones, J.D.C., Moore, A.J.,

    2005. Modelling and calibration of bending strains for iterative laser forming.

    J. Appl. Phys. D:Appl. Phys. 38, 40274036.

    [5] Rosenthal. D. Trans ASME 849-866 1946.

    [6] Matthew S. Brown, Craig B. Arnold Fundamentals of Laser-Material

    Interaction and Application to Multiscale Surface Modification, 2010. 91-

    120.

    [7] Shitanshu Shekhar Chakraborty, Harshit More, Vikranth Racherla, Ashish

    Kumar Nath, Modification of bent angle of mechanically formed stainless

    steel sheets by laser forming, Journal of Materials Processing Technology,

    Volume 222, August 2015, Pages 128-141, ISSN 0924-0136.

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    7. APPENDIX

    Matlab code for the Analytical Model:

    % Funct i on t o comput e t emper ature vs t i me at Z = 0. % Anal yt i cal model used to comput e temper at ur e evol ut i on i n a f i ni t e% t hi ckness sheet , % wi t h a sheet at t he bott om at t ached, subj ect ed t o a st at i onar y heatsour ce of const ant wi dt h ( equal t o beamdi ameter) and% and uni f or m i nt ensi t y of magni t ude 4AP/ ( pi d 2) f or t i me d/ v( McBr i de et al . , 2006)

    % I NPUT PARAMETER%% A - - > Absor pt i vi t y% d - - > Di amet er of l aser beam i n mm% P - - > Laser power i n W

    % v - - > Scan speed i n m/ mi n% h - - > Sheet t hi ckness i n mm% zVec - - > Vect or cont ai ni ng di st ances f r om t op sur f ace i n mm wher et he t emper at ur e i s t o be est i mated. Fi r st poi nt shoul d be z=0% T0 - - > I ni t i al sheet t emper at ur e% n - - > No. of r ef l ect i ons consi der ed i n t he anal yt i cal expr essi onf or est i mat i on of t emper at ur e i n a f i ni t e thi ckness sheet % Tot al Ti me - - > Tot al t i me of anal yses i n seconds% Ti meI ncr ement - - > Ti me I ncr ement t o be used i n t he anal yses% TempRi seFor StepCal c - - > Temperature r i se f or t he St epTi mecal cul at i on% Cr - - > Ef f ect i veness of Radi al heat conduct i on, < or = 1% pr 1 - - > heat f l ow par t i t i oni ng i nt o subst r at e- 1 kept on a basemat er i al - 2

    cl ear al l A = 0. 75; d = 3; P = 400. 0; v = 1; h=1; zVec=0: 0. 05: 1; n=50; Cr = 0. 7; T0 = 27; Ti meI ncr ement= ( pi *d*60) / ( 4*v*1000*80) ; Tot al Ti me=2;TempRi seWi t hi nTi meI ncr ement=10; I nt ensi t yMul t i Fact or = 1; Tmeanguess=500; TPropMax1 = 1200; k2 = 205; r ho2 = 2688; cp2 = 936. 6; % k2, r ho2 and cp2 ar e conduct i vi t y, densi t y and speci f i c heat of t he% bot t om mat er i al i n SI uni t q = I nt ensi t yMul t i Fact or *( A*P*1e6) / ( pi *d 2/ 4) ; %Aver age i nt ensi t y i nW/ m 2zVec = zVec/ 1000; %Dept h i n mh = h/ 1000; %Sheet t hi ckness i n md = d/ 1000; %Beam di amet er i n mv = v/ 60; %Beam vel oci t y i n m/ sTcond1 = [ 0; 100; 200; 300; 400; 500; 600; 700; 800; 1000; 1200] ; %Temperat ur esat whi ch conducti vi t y i s speci f i edcond1 = [ 51. 9; 50. 7; 48. 2; 45. 6; 41. 9; 38. 1; 33. 9; 31. 1; 24. 7; 26. 8; 29. 7] ;%Conduct i vi t y at speci f i ed t emper at ur esTdens1 = [ 0; 100; 200; 300; 400; 500; 600; 700; 800; 1000; 1200] ; %Temperat ur esat whi ch densi t y i s speci f i eddens1 =[ 7700; 7700; 7700; 7700; 7700; 7700; 7700; 7700; 7700; 7700; 7700] ; %Densi t y atspeci f i ed t emper atur esTspht 1 = [ 0; 100; 200; 300; 400; 500; 600; 700; 800; 1000; 1200] ; %Temperat ur esat whi ch speci f i c heat i s speci f i ed

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    spht 1 = [ 486; 486; 550; 548; 586; 649; 708; 770; 624; 548; 548] ; %Speci f i c heatat speci f i ed t emper at ur es

    t p = d/ v; %Heat i ng t i me i n seconds

    zLength=l ength(zVec) ;

    %%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% ANALYSES FOR THE TOPSURFACE %%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%

    z=zVec( 1) ; count =1; Temp( 1, : ) =[ 0, T0] ; %I ni t i al i zi ng count and Temper at ur eT( 1, 1) =0; T( 1, 2: ( n+1) ) =T0;

    k=cond1( 1) ; r ho=dens1( 1) ; c=spht 1(1) ;

    di f f use=k/ ( r ho*c); del =2*sqr t ( di f f use*t p) ; TRi se1=q*del / ( k*sqr t ( pi ) ) ; Tmean =( T0+TRi se1) / 2;

    i f ( TRi se1>TPr opMax1) Tmean=TPr opMax1;

    end

    k1 = spl i ne( Tcond1, cond1, Tmean) ; %Thermal conduct i vi t y i n W/ m/ K atTmeanr ho1 = spl i ne( Tdens1, dens1, Tmean) ; %Densi t y i n kg/ m 3 at Tmeancp1 = spl i ne(Tspht 1, spht 1, Tmean) ; %Speci f i c heat i n J / kg/ K at Tmean

    di f f usi vi t y1 = k1/ ( r ho1*cp1) ; %Di f f usi vi t y i n m 2/ sec at Tmeandi f f usi vi t y2 = k2/ ( r ho2*cp2) ;

    pr 1=( ( k1/ sqr t ( di f f us i vi t y1) ) -(k2/ sqrt (di f f us i vi t y2) ) ) / ( (k1/ sqrt ( di f f us i vi t y1) ) +(k2/ sqrt ( di f f us i vi ty2)) ) ; pr1=1; %For wi t hout backi ng condi t i on

    f or t = Ti meI ncrement : Ti meI ncrement : Tot al Ti mecount =count +1; i f t

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    f 3 = 1/ exp( x3 2) / sqr t ( pi ) - x3*( 1- er f ( x3) ) ; f 4 = 1/ exp( x4 2) / sqr t ( pi ) - x4*( 1- er f ( x4) ) ;

    f 3=Cr *f 3; f 4=Cr *f 4;

    TempRi sez=TempRi sez+q*Di f f usi onLengt h1*( pr1 i ) *( f 1+f 2- f 3-f 4) / k1; %Temper at ur e ri se at dept h z t aki ng n r ef l ect i ons wi t h r adi alheat l oss

    T( count , i +1) = TempRi sez+T0; %Temper at ure est i mat ed at zt aki ng i r ef l ect i ons

    endx1 = z/ Di f f usi onLengt h1; x3 = sqr t ( z 2+d 2/ 4) / Di f f usi onLengt h1; f 1 = 1/ exp( x1 2) / sqr t ( pi ) - x1*( 1- er f ( x1) ) ; f 3 = 1/ exp( x3 2) / sqr t ( pi ) - x3*( 1- er f ( x3) ) ; f 3=Cr *f 3; TempRi sez1 = q*Di f f usi onLengt h1*( f 1- f 3) / k1;

    Temp( count , 1) =t ; Temp( count , 2) =T0+TempRi sez+TempRi sez1;

    el se %Bel ow i s t he t emperat ur e est i mat i on f or t he cool i ng per i od

    Di f f usi onLengt h1=2*sqr t ( di f f usi vi t y1*t ) ; Di f f usi onLengt h2=2*sqr t ( di f f usi vi t y2*t ) ; Di f f usi onLengt hCool i ng1 = 2*sqr t ( di f f usi vi t y1*( t - t p) ) ; Di f f usi onLengt hCool i ng2 = 2*sqr t ( di f f usi vi t y2*( t - t p) ) ;

    sum1=0; sum2=0;

    f or i =1: nx1 = ( 2*i *h+z) / Di f f usi onLengt h1; x2 = ( 2*i *h- z) / Di f f usi onLengt h1; x3 = sqr t ( ( 2*i *h+z) 2+d 2/ 4) / Di f f usi onLength1; x4 = sqrt ( ( 2*i *h- z) 2+d 2/ 4) / Di f f usi onLengt h1;

    f 1 = 1/ exp( x1 2) / sqr t ( pi ) - x1*( 1- er f ( x1) ) ; f 2 = 1/ exp( x2 2) / sqr t ( pi ) - x2*( 1- er f ( x2) ) ; f 3 = 1/ exp( x3 2) / sqr t ( pi ) - x3*( 1- er f ( x3) ) ; f 4 = 1/ exp( x4 2) / sqr t ( pi ) - x4*( 1- er f ( x4) ) ; f 3=Cr *f 3; f 4=Cr *f 4; sum1 = sum1+q*Di f f usi onLengt h1*( pr1 i ) *( f 1+f 2- f 3- f 4) / k1;

    x11 = ( 2*i *h+z) / Di f f usi onLengt hCool i ng1; x22 = ( 2*i *h- z) / Di f f usi onLengt hCool i ng1; x33 = sqr t ( ( 2*i *h+z) 2+d 2/ 4) / Di f f usi onLengt hCool i ng1; x44 = sqrt ( ( 2*i *h- z) 2+d 2/ 4) / Di f f usi onLengt hCool i ng1;

    f 11 = 1/ exp( x11 2) / sqr t ( pi ) - x11*( 1- er f ( x11) ) ; f 22 = 1/ exp( x22 2) / sqr t ( pi ) - x22*( 1- er f ( x22) ) ; f 33 = 1/ exp( x33 2) / sqr t ( pi ) - x33*( 1- er f ( x33) ) ;

    f 44 = 1/ exp( x44 2) / sqr t ( pi ) - x44*( 1- er f ( x44) ) ; f 33=Cr *f 33;

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    f 44=Cr *f 44;

    sum2 = sum2+q*Di f f usi onLengthCool i ng1*( pr1 i ) *( f 11+f 22-f 33- f 44) / k1;

    T( count , i +1) = sum1- sum2+T0; %Temper at ure est i mat ed at z

    t aki ng i r ef l ect i onsendTempRi sez= sum1- sum2;

    x1 = z/ Di f f usi onLengt h1; x3 = sqr t ( z 2+d 2/ 4) / Di f f usi onLengt h1; x11 = z/ Di f f usi onLengt hCool i ng1; x33 = sqr t ( z 2+d 2/ 4) / Di f f usi onLengthCool i ng1; f 1 = 1/ exp( x1 2) / sqr t ( pi ) - x1*( 1- er f ( x1) ) ; f 3 = 1/ exp( x3 2) / sqr t ( pi ) - x3*( 1- er f ( x3) ) ; f 11 = 1/ exp( x11 2) / sqr t ( pi ) - x11*( 1- er f ( x11) ) ; f 33 = 1/ exp( x33 2) / sqr t ( pi ) - x33*( 1- er f ( x33) ) ; f 3=Cr *f 3; f 33=Cr *f 33;

    sum1 = q*Di f f usi onLengt h1*( f 1- f 3) / k1; sum2 = q*Di f f usi onLengt hCool i ng1*( f 11- f 33) / k1; TempRi sez1= sum1- sum2;

    Temp( count , 1) =t ; Temp( count , 2) =T0+TempRi sez+TempRi sez1;

    endendcount Max=count ; TMax=max( Temp( : , 2) ) ; %Maxi mum t emper at ur e

    p = 1; TPrevi ous=T0; Resul t s( 1, 1) =0; Resul t s( 1, 2: ( zLengt h+1) ) =T0; f or i =1: count Max

    i f ( ( abs( Temp( i , 2) - TPr evi ous) >=TempRi seWi t hi nTi meI ncr ement ) | | ( Temp( i , 2) ==TMax) )

    p=p+1; Resul t s( p, 1) =i *Ti meI ncr ement ; Resul t s( p, 2) =Temp( i , 2) ; TPr evi ous=Temp( i , 2) ;

    end

    endp=p+1; Resul t s( p, 1)=countMax*Ti meI ncrement ; Resul t s( p, 2) =Temp( count Max, 2) ; pMax=p; del Tmax = max( abs( di f f ( Temp( : , 2) ) ) ) ;

    Fi gName=spr i nt f ( ' Temper at uresDat a. emf ' ) ; h=f i gur e; pl ot ( Resul ts ( : , 1) , Resul ts ( : , 2) , ' Li neWi dt h' ,2 ) ; xl abel ( ' Ti me ( s) ' ) ; yl abel ( ' Temper at ure ( Deg C) ' ) ;t i t l e( ' Temperatur es vs t i me' ) ;