GROUNDWATER MONITORING WELL SAMPLING (SECOND …1130 ug/1 (NP/SDWS of 300 and 50 ug/1, respectively.) Sample 50-01 contained iron at a concentration of 12700 ug/1 (NP/SDWS of 300 ug/1)

8 9

Rollins

December 18, 1987

Mr. Russ HartProject ManagerCERCLA Enforcement SectionU.S. EPA Region V

| 230 S. Dearborn Street| Chicago, IL 60604

RE: Groundwater Monitoring Well Sampling (Second Round) at theMaster Disposal Service Landfill

Dear Mr. Hart:

j Rollins Environmental Services (FS), Inc. (RES-FS) will perform thesecond round of groundwater sampling as required by the MDSL Work

! Plan. We anticipate performing this activity during the next period of• low groundwater level conditions (refer to the site map, submittedj 11/24/87, for sampling locations).

RES-FS has evaluated the analytical data from the first round ofmonitoring well samples to determine the number of samples and type ofanalyses necessary for the second round of sampling. Table 1 lists thefirst round of monitoring well samples collected in September, 1987. Theorganic and inorganic partial data packages are included as AttachmentsA and B, respectively.

RES-FS' evaluation of the first round analytical data indicated thefollowing, with respect to organic compounds (see Table 2):

Sample 30-01 contained 1,1-dichloroethene at a concentration of 18ug/l (detection limit 5 ug/1).

Sample 32-01 contained chloroethane at a concentration of 43 ug/1(detection limit 10 ug/1) and acetone at a concentration of 39 ug/1(detection limit 10 ug/1).

Sample 33-01 contained chloroethane at a concentration of 13 ug/1(detection limit 10 ug/1); acetone at a concentration of 16 ug/1(detection limit 10 ug/1) and benzene at a concentration of 8 ug/1(detection limit 5 ug/1).

EPA Region 5 Records Ctr.

232493

Mr. Russ HartDecember 18, 1987Page 2

Sample 37-01 contained acetone at a concentration of 30 ug/1(detection limit 10 ug/1).


Sample 42-01 contained trans 1,2-dichloroethene at a concentrationof 11 ug/1 (detection limit 5 ug/1).




Sample 49-02 contained toluene at a concentration of 360 ug/1(detection limit 250 ug/1). It should be noted that the high (250ug/1) detection limit for this sample is a result of a 50-fold dilutionfactor required for analysis of the sample. Additionally, sample 49-02 was a duplicate sample of sample 49-01, which contained tolueneat a concentration of 15 ug/1, well below the detection limit of 250ug/1 associated with these samples.

One semi-volatile compound was detected in the first round ofmonitoring well samples. The compound; bis(2-ethylhexyl)phthalatewas found in sample 30-01 at a concentration of 26 ug/1, in sample43-01 at a concentration of 36 ug/1 and in sample 49-01 at aconcentration of 48 ug/1. The detection limit for these threesamples was 10 ug/1. No other semi-volatile compounds weredetected in any of the monitoring well samples.

No pesticide/PCB compounds were detected in any of the monitoringwell samples.

The review of the groundwater monitoring well analytical data indicatedthe following, relative to inorganic compounds identified in the samples(see Table 3):

Sample 30-01 contained iron at a concentration of 470 ug/1, inexcess of the National Primary/Secondary Drinking Water Standards(NP/SDWS) of 300 ug/1 and manganese at a concentration of 92 ug/1(NP/SDWS of 50 ug/1).

Sample 33-01 contained iron at a concentration of 12500 ug/1(NP/SDWS of 300 ug/1) and manganese at a concentration of 219ug/1 (NP/SDWS of 50 ug/1).


Sample 39-01 contained iron at a concentration of 1980 ug/1(NP/SDWS of 300 ug/1) and manganese at a concentration of 68 ug/1(NP/SDWS of 50 ug/1).

Sample 40-01 contained manganese at a concentration of 1320 ug/1(NP/SDWS of 50 ug/1).

Sample 42-01 contained the following inorganic compounds:

-barium at 1190 ug/1 (NP/SDWS of 1000 ug/1)-iron at 16500 ug/1 (NP/SDWS of 300 ug/1)-manganese at 82 ug/1 (NP/SDWS of 50 ug/1).



Sample 49-01 contained iron at a concentration of 26200 ug/1(NP/SDWS of 300 ug/1) and manganese at a concentration of 1140ug/1 (NP/SDWS of 50 ug/1).

Sample 49-02 (a duplicate sample of 49-01) contained iron at aconcentration of 11000 ug/1 and manganese at a concentration of1130 ug/1 (NP/SDWS of 300 and 50 ug/1, respectively.)

Sample 50-01 contained iron at a concentration of 12700 ug/1(NP/SDWS of 300 ug/1).

All groundwater monitoring well samples displayed Total Dissolved Solids(TDS) concentrations above the NP/SDWS of 500 mg/1 except thefollowing samples: 31-01, 34-01, 36-02, 43-01 and 46-01. (Refer to Tablethree for specific concentrations.)

RES-FS proposes to modify the sampling plan for the second round ofgroundwater monitoring well samples to exclude the analysis of all semi-volatile and PCB/Pesticide compounds.

The second round of sample collection and analysis therefore will includethe following parameters:

CLP Volatiles (including the target alcohols)CLP InorganicsConventional ParametersField measurements of; pH, Specific Conductance andTemperature.

The proposal to modify the sampling plan is based on the followingrationale:


The only semi-volatile compound identified in any of the first roundsamples was a phthalate, which are found in virtually all rubberand plastic products. Therefore, the presence of phthalates at thelow ug/1 (ppb) concentrations found in three of the MDSLgroundwater samples are probably attributed to field and/orlaboratory contamination.

No PCBs or pesticides were found in any of the samples.

If you have any questions, please do not hesitate to call.Sincerely,

ROLLINS ENVIRONMENTAL SERVICES (FS), INC.

Rick SmithAssistant National Technical Director

Jeffrey M. BakerProject Manager

Attachments

JMB:bc

cc: Dennis Kugle, WDNRMike McCauley, Quarles & BradyDr. Kim Anderson, A. O. Smith Corp. - w/o attachmentsAaron Hardt, Rexnord, Inc. - w/o attachmentsTom Rutkowski, Briggs & Stratton Corp. - w/o attachmentsDave Quast, A. O. Smith Corp. - w/o attachmentsErnest McClellan, Plast-O-Meric - w/o attachmentsNancy Peterson, Quarles & Brady - w/o attachments

TABLE 1

Master Disposal Service Landfill

Groundwater Monitoring Well Sample Summary

Sampling Series Number 1

SAMPLENUMBER

WELLNUMBER

AQUIFERSAMPLED

DATESAMPLED

GW-030-01GW-031-01GW-032-01GW-033-01GW-034-01GW-035-01GW-036-01GW-036-02GW-037-01GW-038-01GW-039-01GW-040-01GW-041-01GW-O42-01GW-O43-01GW-044-01GW-045-01GW-046-01GW-047-01GW-048-01GW-049-01GW-049-02GW-050-01

MW-44MW-46MW-45MW-31MW-49MW-05MW-50MW-50MW-51MW-43MW-47MW-53MW-48MW-01MW-56MW-55MW-54MW-42MW-41MW-40MW-10MW-10MW-09

A-lA-3A-2A-lA-2A-lA-2A-2A-3A-3A-2A-lA-3A-lA-3A-2A-lA-3A-2A-lA-lA-lA-2

9/25/879/25/879/25/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/27/879/27/879/27/879/27/879/27/879/27/879/27/879/27/879/27/87

Please refer to Site Map for well locations.

1ABLE JMASTfR DISPOSAL SERVICE LANDFILLINORGANIC A N A L Y T I C A L SUMMARYGRUUNDUATER SAMPLING(PAGE 1 OF 2)

SAMPLE IDENTIFICATION NUMBER (1)

PARAMETER 3001

ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUM 67400CHROMIUMCOBALTCOPPERIRON 470**LEADMAGNESIUM 37600MANGANESE 92**MERCURYNICKELPOTASSIUM 6420SELENIUMSILVER

SODIUM 35400THALLIUMVANADIUMZINC

DISSOLVED IRONRESIDUE, FILT. (TOS) (mg/l) 550"

3101 3201 3301

678

8.226200 69200 153000

15

12500**

23000 126000219"

138264000 64300

20000 195000 227000

22

141270 1200** 1800**

3401 3501 3601

16

43600 38000 25900

300 116

28900 40500 2140021

13800 12900 16600

380 1200** 1300**

DETECTION3602 3701 3801 3901 4001 4101 LIMIT (2)

266 2006010

215 2005

5.3 529100 35400 62800 90900 103000 276000 5000

13 1050255

125 1980** 1005

23700 31200 37200 37600 500068** 1320** 15

0.244 CO

18500 70800 5000510

16000 29500 19000 33700 18500 51200 50001050

62 20

100280 1400" 670** 580" 680** 650" 10

NOTE: ** DENOTES CONCENTRATION OF PARAMETER EXCEEDS PRIMARY/SECONDARY DRINKING WATER REGULATIONS STANDARDSUNITS ARE EXPRESSED AS ug/l UNLESS OTHERWISE NOTED

(1) ID NUMBER REPRESENTS LAST 5 DIGITS OF THE NOMENCLATURE NOL-GU OXX-XX(2) CONTRACT REQUIRED DETECTION LIMITS

UBLE 3MASTER DISPOSAL SERVICE LANDFILLINORGANIC ANALYTICAL SUMMARYGROUNDUATER SAMPLING(PAGE 2 OF 2)


PARAMETER

ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANUtNESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMVANADIUMZINC

DISSOLVED IRONRESIDUE. FILT. (TDS) (*a/l)

4201 4301 4401 4501

203 224

1190** 649

240000 55100 288000 8140013 27

16500**

157000 26700 3060082** 144**

588380 5810 418000

246000 9920 205000

24

1992100" 390 2000** 920**

4601 4701 4801 4901

652 359

•

99000 54900 101000 25700020

54253 26200**

40000 170000105** 1140**

10234200 63300 65600

67400 86100 6150 303000

66 421

370 600** 1600** 2400**

4902

300

9.725100018

11000"

1680001130"

10366500

304000

682

2400"

DETECTION5001 LIMIT (2)

654

7.1133000

12700**

11600028

426220

U2000

40

115UOO"

200601020055

500010502551005

5000150.24050005105000105020

10010

UNITS EXPRESSED AS ug/l UNLESS OTHERWISE NOTED(1) 10 NUMBER REPRESENTS LAST 5 DIGITS OF THE NOMENCLATURE MDL-GU OXX-XX(2) CONTRACT REQUIRED DETECTION LIMITS

TABLE 3HASTER DISPOSAL SERVICE LANDFILLORGANIC ANALYTICAL SUMMARYGROUND WATER MONITORING WELL SAMPLING(PAGE 1 OF 2)


PARAMETER 3001 3101 3201 3301 3401 3501 3601 3602 3701 3801

CHLOROETHANE 43 13

ACETONE 39 16 30

1.1 DICHLOROE THANE 18

BENZENE 8**

BIS(2 ETHYLHEXYDPHTHALATE 26

TABLE 2MASTER DISPOSAL SERVICE LANDFILLORGANIC ANALYTICAL SUMMARYGROUND WATER MONITORING WELL SAMPLING(PAGE 2 OF 2)

PARAMETER 4201 4301 4401 4501 4601 4701 4801 4901 4902 5001

ACETONE 43 76 49

T 1,2-DICHLOROETHENE 11

TOLUENE 360

BIS(2-ETHYLHEXYL)PHTHALATE 36 48

DETECTION3901 4001 4101 LIMIT (2)

10

41 10

5

5

10

DETECTIONLIMIT (2)

10

5

250 (3)

10

NOTE: * DENOTES COMPOUND DETECTED IN THE METHOD BLANK" DENOTES CONCENTRATION OF PARAMETER EXCEEDS PRIMARY/SECONDARY DRINKING WATER REGULATIONS STANDARDS

UNITS EXPRSSED AS ug/l UNLESS OTHERWISE NOTED

(1) ID NUMBER REPRESENTS LAST 5 DIGITS OF THE NOMENCLATURE MDL-GW OXX-XX(.') CONTRACT REQUIRED DETECTION LIMITS(3) DETECTION LIMIT FOR SAMPLE INCREASED TO 250 BECAUSE OF 50-FOLD DILUTION FACTOR (5 FOR UNDILUTED SAMPLES)

ATTACHMENT A

MASTER DISPOSAL SERVICE LANDFILL

PARTIAL ANALYTICAL DATA PACKAGE

ORGANIC COMPOUNDS

LABORATORY NAME: ETC/TOXICON

LAB SAMPLE 10 NO: 4184-181SAMPLE MATRIX: WATEROATA RELEASE AUTHORIZED BY

ORGANICS ANALYSIS DATA SHEET(PAGE 1)

CASE NO: 4184flC REPORT NO: 4184CONTRACT NO: 0\ \DATE SAMPLE RECEIVED

VOLATILE COMPOUNDS

•9/29/87

CONCENTRATION: LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: 18/43/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (NOT DECANTED)

PH

CAS NUMBER74-87-174-8J-*7S-81-47S-88-J75-89-247-44-175-15-875-35-47S-JS-J154-48-i47-44-3187-84-278-f J-J71-S5-454-23-5188-85-475-27-4

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEHETHYLENE CHLORIDE . . . .ACETONECARBON OlSULFIDC1. l-DICHLOROETHENE . . . .1.1-OZCHLOROETHANC . . . .

TRANS-1.2-OICHLOROETHENE .CHLOROFORM1.2-OICHLOROETHANE . . . .2-BUTANONE1. 1. 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEIROMOOICHLOROMETHANE . . .

UG/L181818181185S

ItS55185S185

UUUuJuuu

uuuf6uuuu

CAS NUMBER78-87-518861-82-471-81-4124-48-179-88-571-43-218841-81-S118-75-87S-25-2188-18-15*1-78-4127-18-479-34-5188-88-3188-98-7188-41-4188-42-5

UG/L1.2-OICHLOROPROPANE . . .TRANS-1.3-OICHLOROPKOENE .TRICHLOROETHENEOIBROMOCHLOROMETHANE . . .1,1,2-TPICHLOROETHANE . .BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .

BROHOFORH4-HETHYL-2-PENTANONE . . .2-HEXANONCTETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES

18S18

UUUuuuuuuuuuuuuuuu

8 - COMPOUND WAS DETECTED IN THE 8C BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED

VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.

SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA

REPORTING 8UALIFIERS.FORM I

4 1 8 4 3 0 3 4 9

Laboratory Name: ETCToxicon

Case No: 4184

Sample Number

Organics Analysis Data Sheet

CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butjl Alcohol

sec-Butyl Alcohol

ConcentrationILf/L

300U

200U

200U

U Tndir«t<-f rftrnpr^r^ w^ ynalyrpj fly frit aft <jfftftfd_ Pi-pnn rtv minimum Aftrt-tinn limit fnrlhe tample with the U(e.g. 10U) baled on necessary coaxmratioa'dihaioo action. (This is not necessarily the instrument detection limit)The footnote should read: U-Compotmd was analyzed for but not detected The number is me minimum attainabledetection limit for the sample.

J TnH>r«tM m <yim«t<^ vabe. This flaj U ued timer wbea »«rimMing a coQcentratioQ for tentatively identified compoundswhere a 1:1 rappmc it asmpfd or »bf" mf "ift» ipe^r»l <<»« inHirjit«l thg presence of« componad ttm meets me ideati-ficatkm criteria bm the ronlt is VM than the edlWdeteaiooliiM If limit of detection is10 (JLgft. and a ooncenraion of 3 u{/L is calculated, report as 3J.

4 1 8 4 30350

3 I - ' ' ' - I ! .

Organics Analysis Data Sheet(Page 2)

Semivolatile Compounds

_oncentration Q.OVV) Medium /Circle One)

Date Extracted 'Prepared

•ate Analyred

Conc/Dil Factor:

'ercent Moisture (Decanted).

GPC Cleanup DY«s DNo

Separaiory Funnel E*iraciion

Continuous Liquid - Liquid Extraction DYes

CASNumber

ug/for ug/Kg(CirctoOfM)

108 95-2UI-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-63-212O-82-191-2O-3106-47-887-68359-50791-57-677-47-488-06-29595-491-58-788 74-4131-11-3208 96-899 09 2

*henol6(S<-2-Crttoroe(nvf (Ether

2-Chlorophenol1. 3-Dichlorobenzene1 . 4-DtchtorobefueneBenzyl Alcohol1. 2-Dichforobcnzen*2-Methytph«noltx*(2 <hloroicopropv<tEth«r

4-M«thylpr»enoiN-Nitnno-Oi-n-Propy1»mir»«Heicachloro«trujntNitrobenzene(sophorone2-NHroohenoi

2. 4-Oim«tnytpn«nO<

Beruoic Acidbisf^-CnloroethoKYlMetftant2. 4-DKhloroph«nol1. 2. 4-Trichkxo6eozeneNapntn«(«ne4-Chlofo»nitin«S«ucMorobui»dt«n«4 • Chloro- 3 • Mcthylphenol2-Metfty<n«phthal«ntHe ucMorocyclopentadierw2. 4. 6-Trichloroprtenol2. 4. 5-Trtchtofophenol2-CMoron»phth«lertc2 NitroaniltrteDimethyl PhihalateAcenaphthylene3-Niiroamline

/Cu.//>&10 ttIn,,.10k/Ok(m-ir\uL(flulUUi\nuIOuIDuWK,I/]U

/(VWin

inu.'(I*IOu.If)*m*10*ffa/<vlUr-/OiA

ftu(CllA

SOU

IDu.IfilA

5m

CASNumber

606-20-284-66-2

86-73-7

86-30-6

3-32-91-28-500-02-732-64-921-14-2

005-77-3

00-01-634-52-1

01-S5-318-74-17-86-55-01-820-12-7

84-74-2206-44-029-00-0

15-687H-94-16-55-3

117^1-7218-01-9117-84-0205-99-2207-08-9J032-8193-39-553-703191-24-2

!. 4-Dinrtropr»«nol

4-NitropNenol

2. 4-D<n(trotolu«n«

!,.6-Oinhrotolu«ne

4 -Chlof oph«riy(-pn«ny««th*r

UNruoanilin*

Oiethylphtrujujte

Fluorcnt

N-Nitrocodipf>enyujmine (1)

Phenanthrtnc

Anthracene

3 atytb* rvrytph t K» late3. 3'BerucKilAnrtvaccne

ChryMoc

0<-n-Octy< Prttrujlate

. 2. 3-Cd>Pyren«

Oibenrd8«nio(g.

ug/I or ug/Kg(CircU One

$4*

fiuKM\fi\HI(Oit-

IOu.3bffiu.

ll

flu

Wtf.IC]\f-

(1 >-C»TX>1 b* i«p*r»t«d fr

FCH r^ I

4 1 8 485

' - • - "*::

^SF . ; - - •• :' . i ' .~ 'd ' : ' . f =, i":.4 ; = *

:it:'.f ''.iff'

i:-, A n a l y s i s D a t a Sheet(Paqe 3)Pestu ides/PCBs

[Lc»j Rpd;ui (Circle onei

Date Anaiy.-ed: 07-Dct-B7Conc/DiJ Factor;Percent Hoisture(decinted) HR

6PC Cleanup Ye; MSeparator Funnel Eitractior.Continuous Liquid-Liquid Extra:tisr

CAS [ug/L] or uNuiber

319-84-6 ftlphi-BHC 0.05 U319-85-7 Beti-BHC 0.05 U319-B6-6 Delti-BHC 0.05 U58-89-9 GaiH-BHC (Lindine) 0.05 U76-«4-8 Heptachlor 0.051)109-00-2 Aldrin 0.05 U1024-57-3 Heptichlor Epoiidr . 0.05 U959-98-8 Endosulfin I 0.05 U60-57-1 Jieldrin 0.1 U72-55-9 4,4'-DD£ 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfifi II 0.1 U72-54-B 4,4'-DDD 0.1 U1-31-07-B Endosulfin Sulfite 0.1 U50-29-3 4,4 ' -BDT 0.1 U72-43-5 Kethojychlor 0.5 U53494-70-5 Endrin Ketont 0.1 U57-74-9 CMordanc 0.5 U8001-35-2 Touphene 1U12674-11-2 ftroclor-1016 0.5 U11104-28-2 flroclor-1221 0.51)11141-16-5 Aroclor-1232 0.5 U',3469-21-9 Aroclor-1242 0.5 U12672-29-6 ArDclor- i :4B 0.5 U11097-69-1 Aroclor-1254 ID11096-82-5 Aroclor-1260 1U

Vi = Voluie of eitract injected tul)Vs = Voluie of utter eitracted (illMs - Meiqht of saiple extracted (g)Vt ; Vo'.uie of total e i t ract (ul)

Vs = 1000 or Ms Vt 100CO Vi - 3.0

Fori 1

4 1 8 4 3 0 3 5 2

Laboratory Name ETC/Toxic on

• No


Tentatively Identified Compounds

Sample

CASMumtwr Compouod N««TM Frwction

1.. _&[££_

15

•**v16..

6..

2O..

1..

«..

!7..

10

NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight

4 1 8 4 3 0 3 5 3

• . "EE

LABORATORY NAME. ETC/TOXICON

LAB SAMPLE 10 NO: 41B4-1«2SAMPLE MATRIX: WATER

DATA RELEASE AUTHORIZED BY

418*4184

ORGANICS ANALYSIS DATA SHEET

(PAGE 1)CASE NO:AC REPORT NO:CONTRACT NO:

DATE SAMPLE RECEIVED: •9/29/87

VOLATILE COMPOUNDS

CONCENTRATION: LOU

DATE EXTRACTED/PREPARED:DATE ANALYZED: l«/«3/«7

CONC/DIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)

PH

CAS NUMBER

74-S7-3 CHLOROMETHANE

74-11-9 BROMOHETHAME

7S-B1-4 VINYL CHLORIDE

78-••-3 CHLOROETHANE

7S-»»-2 HETHYLENE CHLORIDE . . .

47-44-1 ACETONE

7S-1S-* CARBON DISULFIDE . . . .7S-3S-4 1.1-OICHLOROETHENE . . .

7S-3S-3 1.1-OZCHLOROCTHANC . . .154-49-S TRANS-1.2-OICHLOROETHENE47-44-3 CHLOROFORM

l»7-«4-2 1.2-OICHLOROETHANE . . .7«-fl-l 2-BUTANOME

71-5S-* 1.1.1-TRICHLOROETHANE .

54-23-4 CARiON TETRACHLORIOC . .

i«8-«S-4 VINYL ACETATE

7S-27-* BROHOOICHLOROMETHAME . .

UG/L

!•!•!•119

1

!•

UUUUJUUUUUUU

UUU

CAS NUMBER7t-«7-S

1041-*2-4

124-4B-1

71-43-2

UG/L

7S-2S-2

S»l-7t-4

7t-34-S

•3*

1,2-OICHLOROPROPANE . . .TRANS-1,3-OICNLOROPROENE .

TRICHLOROETHENEOIBROP10CHLOROMETHANE . . .

1. 1.2-TRICHLOROETHANE . .BENZENECIS-1,3-OICHLOROPROPENE .

2-CHLOROETHYLVINVLETHER .

BROMOFORM4-HETHYL-2-PENTANONE . . .

2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANE

TOLUENECHLOROBENZENEETHYLBENZENESTYREMETOTAL XYLENES

UUUUUUUUUUUJUUUUUU

B - COWPOUND WAS DETECTED IN THE «C BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED


SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING QUALIFIERS.

FORM X

4 1 8 4 3 Q 3 6 9

Laboratory Name: ETC/Toxicon

rase No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentration|i|/L

300U

200U

200U

*n*\ym\ fnr V^t |y^ faV&t4 Rgpflrt ** minimum Aftrt-Ann limit finr rtie tamplf with the 11(e.j. 10U) bued on aaxssxy concentntjoo/dilntka actkm. (This it not necessarily the Instrument detection limit)The footnote tV»iM read: U-Compouad wts totlyzed for bat not dftMfd. The number is the minimum attainabledetection limit for the sample.

an «timatM vihie. Thii flag bused dflier when e«timwhere a 1:1 response it assumed or when me mass qxctral data indicated fcc prae vt fif a nxnrK^ml *!*** "<m *»» M«*»-ficatioo criteria bot me resali bless than me fpecified detection limit but greater than iero(&f. 101). If limit of detection is10 m^L and a concentration of 3 (ig/L u cakiilatcd , report a§ 3J.

4 1 8 4 3 0 3 7 0

t . « : • • , N.

Concentration

Date Extracted

Date Analyzed

Cone/Oil Factor

CASNumber

"- • , ' -

Organics Ana(P

Semivolat

(Lovv^) Medium (Circle One)

'Pn»par»»d "-.'/^/(fO

!

tf (Decanted)

ug/lorug/Kg(Circle One)

nenol

S<-2-ChloroethvHEther

-Chloropn«r>ol

. 3-0«chlorobe>u«ne

. 4-Dichlorobenzent

entyl Alcohol

. 2-Dichloroberuenc

-Methytph*nol

is(2 <htor oisopropyDEther

-Mriy«ph«nol

- Nitroso-Oi -n -Propyte mine

exacMoroethant

rtroberuene

tophoron*

-Nrtroohenol

. 4-Dimetriy<pn*nol

teruoic Acid

is( • 2 -CMoroethocylMcthan*

. 4-Dknlorophenol

. 2, 4-Trich(orobeoz0ne

Uphtnakn«

•Chloroanilirw

<« xachlorobat«di«n«

-Chloro-3-M«rty1prwnol

,-Metfiy(n«phth«len*

tecicMorocvclopemadienc

!. 4. 6-Trich>orophenol

!. 4. 5-Tricnloroprtenol

! -CMoronaphifxalene

-Nitroaniline

iimethyl Phth»l»ie

icenaphthylene

lOu./fib.

10 uta*.10uiot^lrn~/AM.IQuiGaIDlA

lOuiffuIC^.Ifik

lUb-wiA

inu.lOt*./On.iDtttfi\fiQlL

IUK

(Oit-iQp.

/Ou.ft(A

(OtA56(\

K)&(C)IA.

lysis Data Sheetage 2)

ile Compounds

GPC Cleanup QYes D

Separatory Funnel Ext

Continuous Liquid - Li

CASNumber

3-32-9

1-28-5

00-02-7

32-64-9

21-14-2

606-20-2

8446-2

7005->2-3

86-73-7

00-01-6

534-52-1

86-30-6

01-55-3

118-74-1

87-86-5

85-01-6

120-12-7

84-74-2

206-44-0

129-00-0

J5-687

• 1-94-1

i6-5S-3

117-61-7

218-01-9

117-84 -O

205-99-2

207-08-9

JO-32-8

193 39 S

>3 703

191 24 2

SB r-pl- S ,:M'~.r

/TiO^ i'v ; j / C /

No

raction QYes

quid Extraction DYes

ug/torug/Kg(Circle One

Acenaphthene

[. 4-Otnrtroprienol

4-Nrtropr«enol

>ibeniofuran

!.4.0initrotoluene

L.6-Oinitrotoluene

Oiethytphthalate

4 -Chlorophenyl-prtenYlether

Fluor erw

4-Nrtroarufioe

4. 6-Oiniiro-2-Methylpherx>l

N-Nrtro$od»phertyUmir»e (1 )

4-Bromoohenyl-phenyletNer

Kexachbxobenzene

Pentachtorophenol

PNenantKren*

AnthraceneDi-n-Buty(phta«Ut«:luoranthene

Pyrerw

Butytoeruylp^Ûte

3. 3°-0«taorob«ruid<ne

B«ruo(aVknthrac«ne

Cxs(2-Ethy{f>eKyt)Ptnrxal«ie

ChryMrw

Di-n-Octyl Phthalate

Ber\io(b)Fluor>ntfier>e

Benzo(k f 1 ixxant Sene

B*nto<i)PvTene

Inoenotl. 2. 3-cdJPyene

O.bcnaa h)Antfv«cene

B«n»o(g. h. iJPeivlene

/^k&*5*14.

\C)kinuIfiu.ibu(Ci(0*

fÂS4U

lUuiCi*.

(C/u.50t\

iC/ii(fluIQujfiu

iOlL

J&uJ0(j

/(Ju.IfitIfJtA.

10iC}\r

IfJl*ÎDiiLs'fnu.

lr,«.

(1) Cannot CM

4 1 8 4 30371

•I:'

0-ga-;:s Aralysis Data Sheet("age 3)Pesticides/PCBs

C;-:er.t'iti3r: [Leu] KedSite Ejfaitei'Presare::Sate Ar^rreJ: 07-Oct-E?Cone -'til factor:Fe-cent Hcistir

i Circle :ae)2'-Sep-B7

1

GPC Cleanup Yes [«]-NoSeparatary Fur.nel Eitraction Ves

us liquid-Liquid Eitrichon [ij Yes

CASNuiber

[ug/L] or ug/Cg

319-84-i Alph»-BHC ........................ 0.05 U319-85-7 Beti-BHC ........................ 0.05 U319-86-8 Delti-BHC ........................ 0.05 U58-69-9 Baiw-BHC (Lindint) ............. 0.05 U76-44-8 Heptachlor ...................... 0.05 U309-00-2 Aldnn .......................... 0.05 U1024-57-3 H«pt«hlor Epoiide ............... • 0.05 U959-98-8 Endosulfin I .................... 0.05 U60-57-1 Diildrin ........................ 0.1 U72-55-9 4,4'-DDE ........................ 0.1 U72-20-8 Endrin ........................ 0.1 U33213-65-9 Endosulfin II ................... 0.1 U72-54-8 4,4'-DBD ........................ 0.1 U1-11-07-8 Endosulfan Sulfite ............... 0.1 U50-29-3 4,4'-DDT ........................ 0.1 U72-43-5 Bethoxychlor .................... 0.5 U

53494-70-5 Endrin Ketone ................... 0.1 U57-74-9 Chlordwe ....................... 0.51)

8001-35-2 Touplwm ....................... 1U12674-11-2 ftroclor-1016 .................... 0.5 U11104-28-2 ftroclor-1221 .................... 0.5 U11141-16-5 Aroclor-1232 .................... 0.5 U53.469-21-9 Aroclor-1242 .................... 0.5 U12b^-29-6 Arcclor-1248 .................... 0.5 U110»?-69-l Araclor-1254 .................... 1 U11096-82-5 Aroclor-1260 .................... 1U

»i = Volutf of fitrtct injected (ul)Vs = Volute of »»ter eitricted (§1)Ms = Height of staple eitracted Iq)Vt - Voluie of total eitract (ul)

Vs = 1000 or Is Vt - 10000 Vi = 3.0

Fors 1

4 1 8 4 3 0 3 7 2

Lat>o. aio.y Name ETC/To* icon

e No



S»»nple Number

CASCompound Nam* Fr»ctkxt

1- VGA

4.

S.

I"

li:-•i.. 51U

£Jc»

14..

I,...

17..

2O..

26.

28.

29.

3O

NFA denotes no fraction analyzedNCF denotes no compound foundlink denotes unknownmw denotes probable molecular weight

4 1 8 4 3 0 3 7 5

SAMPLE NUMBERMDLGU932*!


LAB SAMPLE ID NO: 4184-11*SAMPLE MATRIX: MATERDATA RELEASE AUTHORIZED BY

ORGAN ICS ANALYSIS DATA SHEET

(PAGE 1>CASE NO.

REPORT NO:CONTRACT NO.DATE SAMPLE RECEIVED: 49/29/87: frx///K/>-^—^/Lv*-/L/

41844184

VOLATILE COMPOUNDS

CONCENTMATION: LOWDATE EXTRACTED/PREPARED:

DATE ANALYZED: l«/*S/«7

CONC/OIL FACTOR. 1.PERCENT MOISTURE: <NOT DECANTED)

PH

CAS NUMBER

74-87-J74-83-97S-81-4

7S-M-375-89-2

47-44-1

75-15-871-3S-4

75-35-3154-48-547-44-3

187-84-278-93-371-55-4

54-23-5188-85-47S-27-4

CHLOROHETHANEBROMOMETHANE

VINYL CHLORIDECHLOROETHANEHCTHYLENC CHLORIDE . . . .

ACETONE

CARBON DISULFIOE

1. 1-OICHLOROETHENE . . . .

1. 1-OICHLOROETHANE . . . .

TRANS-1.2-OICHLOROETHENE .CHLOROFORM

1,2-DICHLOROETHANE . . . .

2-BUTANONE

1. 1. 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEBROMOOICHLOROMETHANE . . .

UG/L!• U!• U!• U43S U39

UUUJUUJUU

18 US U

CAS NUMBER

78-87-518«41-«2-479-81-4

124-48-1

79-88-S

71-43-218841-81-S118-75-8

7S-25-2188-1*-!S91-78-4

127-18-4

79-34-S1*8-88-3

188-98-7188-41-4

148-42-S

ue/L1,2-OICHLOROPROPANE . . .TRANS-1.3-OICHLOROPROENE .TRICHLOROETHENEOUROMOCHLOROMETHANE . . .1,1,2-TRICHLOROETHANE . .BENZENCCIS-1.3-DICHLOROPROPENE .

2-CHLOROETHYLVINYLETHEM .

BROMOFORM4-METHYL-2-PENTANONE . . .

2-HEXANONC

TETRACHLOROETHENE . . . .1.1.2. 2-TETRACHLOROETHANE

TOLUENE

CHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES

UUUUUUUUUUUUUUUUUU

J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.

U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR

THE SAMPLE.

SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THEREPORTING aUALIFIERS.

DATA

FORM I

4 1 8 4 3 0 5 3 4

Labora to ry Name: ETC/Toxicon

Case No: 4184

Sample Numtxr


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropjl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationut/L

300U

200U

200U

U Tiviirant oompoood was analyzed for but oat detected. Report the minimum detection limit for the sample with the U(e.g. 10U) based on necessary concentntioo/dihttkm action. (TO* is oot necessarily the instrument detection limit)The footnote should read: U-Compound was analyzed for but oot detected. The number is the minimum attainabledetection limit for me sample.

value. This flag is used either when T^ ation for tentatively identified compoundswhere a 1: 1 response is assumed or when the mass spectral data indicated the presence of a compound dot meets the identi-fcation criteria but die result is less than the specified detection limit but greater than zero (e£. 101). If limit of detection is10 Hf/L and a concentration of 3 H£/L is calculated, report as 3J.

4 1 8 4 3 0 5 3 5

LABORATORY NAME

CASE NO

ETC/TOKICON

418*NUMBER

ORGANIC* ANALYSIS DATA SHEET

(PAGE 2)

SEMIVOLATILE COMPOUNDS

CONCENTRATION: LOW

DATE EXTRACTED/PREPARED: l*/17/87

DATE ANALYZED: It/28/87

CONC/OIL FACTO*: 1.PERCENT hOISTURE: <DECANTED)

GPC CLEANUP YES X NO

SEPARATORY FUNNEL EXTRACTION YES

CONTINUOUS LlaUIO-LIOUID EXTRACTION YES

CAS NUMBER

1*8-95-2 PHENOL

111-44-4 BIS<2-CHLORO€THYL)ETHER .

9S-57-S 2-CHLOROPHENOL$41-73-1 1.3-OICHLOROBENZENE . . .

1*4-44-7 1.4-OICHLOROBENZENE . . .

l**-Sl-4 BENZYL ALCOHOL

9S-S*-1 1,2-OICHLOROBENZENE . . .

95-48-7 2-METHYLPHENOL39438-32-9 •15<2-CHLOROI50PROPYL)ETHER

1*4-44-5 4-METHYLPMEMOL

421-44-7 N-NITROSO-DI-N-PROPYLAMINE

47-72-1 HEXACHLOROCTKANE

98-95-3 NITROiENZEMC

78-59-1 ISOPHOROME88-75-i 2-NITROPHEMOU

1*5-47-9 2. 4-01METHYLPHENOL . . . .

4S-8S-* IENZOIC ACID

111-91-1 ° BXS<2-CHLOROETHOXY)METHANE

;2*-83-Z 2. 4-OICHLOROPHENOL". . . .

128-82-1 1,2,4-TRICHLOROIENZENE . .

91-2*-3 NAPHTHALENE

1*4-47-8 4-CHLOROANILINC87-48-3 HEXACHV.OROBUTAOIENE . . .

S9-S8-7 4-CHLORO-3-METHYLPHENOL .

91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTAOIENE

88-*4-2 2.4, 4-TRICHLOROPHENOL . .

95-7S-4 2.4.S-TRICHLOROPHENOL . .

91-58-7 2-CHLORONAPHTHALEME . . .88-74-4 2-NITROANILINC

131-11-3 DIMETHYL PHTHALATC . . . .

2*8-94-8 ACCNAPHTHYLEME

99-«9-2 3-NXTROANILXNC

UG/I

1*181*1*1*1*1*

181*1*

181*18

181*1*

581*1*181*1*1*1*

1*1*1*

5*1*

581818

5*

UUUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

CAS NUMBER83-32-9

51-28-518*-*2-7

132-44-9

121-14-2

4*4-2*-2

84-44-2

7885-72-384-73-7

l*8-l*-4

534-52-1

84-3*-4

181-55-3

118-74-1

87-84-5

8S-*l-8

128-12-7

84-74-2

284-44-*

129-**-*

85-48-791-94-1

54-55-3117-81-7

218-*l-9117-84-*

2*5-99-2

2*7-*8-9

5*- 32-8193-39-S

5 3-7*- 3

191-24-2

ACENAPHTHENE

2. 4-OINITROPHENOL . . . .

4-NXTROPHENOLDliCNZOFURAN

2.4-DINXTROTOLUENE . . . .

2.4-DXNXTROTOLUENE . . . .

OIETHYLPHTHALATE

4-CHLOROPHENYL-PHENYLETHEMFLUORENE

4-NXTROANILINC

4. 4-OINZTRO-2-METHYLPHENOL

N-NXTROSOOXPHENYLAMINE <1>

4-BROMOPHENYL-PHENYLETHER

HEXACHLOROBENZENE . . . .

PENTACHLOROPHENOL . . . .

PHENANTHRENE

ANTHRACENEOI-N-BUTYLPHTHALATE . . .

FLUORANTHENE

PYRENEBUTYLBENZYLPHTHALATE . . .

3. 3'-DXCHLOROBENZIOINE . .

BENZO(A) ANTHRACENE . . . .B X S < 2-ETHYLHEXYL > PHTHAL ATE

CHRYSENEOI-N-OCTYL PHTHALATE . . .

BENZO(B>FLUORANTHENE .

BENZO<H>FLUORANTH£NE . . .

BENZO< A) PYRENEXNOENO<1'2. 3-CD>PYRENE . .

DXBENZ<A.H> ANTHRACENE . .

BENZO<6. H.DPERYLENE . . .

UG/l1*S*

• •1*1*1*1*1*1*5*5*1*1*1*5*1*1*1*1*1*1*2*1*1*1*1*1*1*

1*1*1*18

UUU

uuuuuuuuuuuuuuuuuuuuuuuuuuuuu

<1> - CANNOT BE SEPARATED FROM OIPHENYLAMXNEFORM X

4184 30536

s-r

A n a l y s i s Eiti(Page 31Pestiudes/PCBs

C:nceitrat:Dn: [Lou] ''ediLi (Circle one)[ate [it'a:l.ei,frepa'ed: 29-Sep-87Date fir-:,-red: 07-Cct-B?Cor-:/Dil factor: 1rercer,t "oistjreldeiJited; NR

BPC Cleanup Yes [«HoSeparatory Funnel Extraction YesContinuous Liquid-Liquid E«trir.tii?n [i] Yes

CAS [ug/L] or ug/Kq

319-B*-6 Alptu-BHC ........................ 0.05 U319-85-7 Beti-BHC ........................ 0.05 U319-B6-B Delti-BHC ........................ 0.05 U58-B9-9 Saiti-BHC (Lindinr) ............. 0.05 U7fc-M-B HepUchlor ...................... 0.05 U309-00-2 ftldrin .......................... 0.05 U1024-57-3 Heptichlor Epoiide ............... 0.05 U959-9B-8 Endosulfin I .................... 0.05 U60-57-1 Ditldrin ........................ ' 0.1 U72-55-9 4,4'-DOE ........................ 0.1 U72-20-8 Endrin ........................ 0.1 U33213-45-9 Endosulfin II ................... 0.1 U72-54-B 4,4'-ODD ........................ 0.1 U1-31-07-8 Endosulfin Sulfitf ............... 0.1 U50-29-3 4,4'-DOT ........................ 0.1 U72-43-5 Hethwychlor .................... 0.5 U53494-70-5 Endrin Kttoni ................... 0.1 U57-74-9 Chlordine ....................... 0.5 U8001-35-2 Toxiphene ....................... 1U12674-11-2 Aroclor-1016 .................... 0.5 U11104-28-2 Aroclor-1221 .................... 0.5 U11141-16-5 Aroclor-1232 .................... 0.5 U53469-21-9 Aroclor-1242 .................... 0.5 U12672-29-6 Aroclor-1248 .................... 0.5 U11097-t9-l Aroclor-1254 .................... 1 U1109t-B2-5 Aroclor-1260 .................... ID

Vi = Voiuie of titrtct injected (ul)Vs = VoluM of «it»r extracted (il)Ms - Height of saiple eitrie ted (g)Vt - Voluie of totil eitrict (ul)

Vs = 1000 or Ms - Vt = 10000 Vi = 3.0

Fon 1

4 1 8 4 3 0 5 3 7

I i t . , ' .1:. • •

Case No


-"]Tan ta lively ld«ntif««d Compounds

CASNumb** Compound Frvction

of cjg/kg)

,40..

11.. (foeIf* n£31

•14..

IS..

1(053/>«k \ /

li.

M.

,24..

'25..


4 1 8 4 3 0 5 3 8

LABORATORY NAME. ETC/TOXICON

LAB SAMPLE 10 NO: 4184-95

SAMPLE MATRIX: MATER

OATA RELEASE AUTHORIZED BY

»184

418*

OROANICS ANALYSIS OATA SHEET

(PAGE 1>

CASE NO.

\ . 8C REPORT NO.CONTRACT NO:DATE SAMPLE RECEIVED:

VOLATILE COMPOUNDS

•9/29/87

CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYZED. l*/*3/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (NOT DECANTED)

PH

CAS NUMBEI74-87-374-B3-975-81-475-88-375-89-247-44-175-15-875-35-475-35-3154-48-547-44-3187-84-278-93-371-55-454-23-5188-85-475-27-4

t IKCHLOROMETHAKE 14BROMOHETHANE . 14VINYL CHLORIDE 14CHLOROETHANE 13HETHYLENE CHLORIDE . . . . !ACETONE . 14CARBON DISULFIOE1. 1-OICHLOROETHENE . . . .1, 1-DICHLOROETHANC . . . .TRANS-1. 2-DXCHLOROETHENE .CHLOROFORM1.2-OICHLOROETHANE . . . .2-BUTANONE 11. 1. 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATE 1BROMOOICHLOROHETHANC .. . <

i/L

> U> U> U1\ uk

uuuuuu

/*uu

» ui u

CAS NUMBER78-87-S1*841-82-479-81-4124-48-179-88-571-43-2

18841-81-5118-75-875-25-2188-18-1591-78-4127-18-479-34-5188-88-3188-98-7188-41-4188-42-5

UG/L

1.2-OrCHLOROPROPANC . . .

TRANS-1,3-OICHLOROPROENE .

TRICHLOROETHENE

DIBROMOCHLOROMETHANE . . .

1.1.2-TRICHLOROETHANE . .

BENZENE

CIS-1,3-DICHLOROPROPENE .

2-CHLOROETHYLVINYLETHE* .

BROHOFORH

4-HETHYU-2-PENTANONE . . .

2-HEXANONC

TETRACHLOROETHENE . . . .

1,1.2.2-TETRACHLOROETHANE

TOLUENE

CHLOROBENZENE

ETHYLBENZENE

STYRENE

TOTAL XYLENES

1*5

UUuUu

uuuuuuuuuuuu

B - COMPOUND WAS DETECTED IN THE «C BLANK.

U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED

VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR

THE SAMPLE.

SEE PACE 1A FOR COMPLETE DEFINITIONS OF THE OATAREPORTING aUALIFIERS.

FORM I

4 1 8 4 3 0 2 1 1


Case No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropjl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentration«/L

300U

200U

200U

Tiviir-yti-^ compound wts analyzed for but not <V-*fft"^ Report me mmimnm detection limit for the sample with the U(e.g. 10U) based on necessary couccmiation/dfluDOC action. fTha is not necessarily me instrument detection limit)The footnote shook! read: U-Compoond wts analyxcd for bat not detected. The lumber is the minimum attainabledetection limit for me sample.

**«"«*<"£ • <^nv*ntr«ri«i far tentarivdy Mearificd eompopndl1:1 rcipontf ii ngnmrf qr «wn fte T»^H sffftt^ «<ia W8""*! **• i*" 1* rf« gnmMind tfat maâ the idgnri.

fication criteria but flie resabis lea than (be ipedfled detection limit bot|reaiermaniero(e4. 101). If limit of detection is10 \if/L and a concentntioa of 3 HJ/L is calcuUMd. report ax 3J.

4 1 8 4 3 0 2 1 2

LABORATORY NAMECASE NO

E T C / T O X I C O N4184

NL-HBER


SEHIVOLATXLE COMPOUNDS

CONCENTRATION: LOWDATE EXTRACTED/PREPARED: *9/3««/B7DATE ANALYZED: l*/*S/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: <DECANTEO>

GPC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIBUIO-LI9UIO EXTRACTION YES

CAS NUMBER1*8-95-2 PHENOL111-44-4 §IS<2-CHLOROETHYL>ETHER .9S-S7-8 2-CHLOROPHCNOL5*1-73-1 1.3-OICHLOROiENZENC . . .166-44-7 1.4-DICHLOROBENZENE . . .l**-51-4 BENZYL ALCOHOL9S-S*-l 1,2-OICHLOROBENZENE . . .95-48-7 2-hETHVLPHEHOL39638-32-9 BIS<2-CHLOROISOPROPYL>ETHER1*4-44-! 4-METHYLPHENOL421-44-7 N-NITROSO-DI-N-PROPYLAMINE47-72-1 HEXACHLOROETHANC

98-9S-J NITROBENZENE7B-59-1 ISOPHORONE•B-7J-§ 2-NITROPHENOL

16S-47-9 2.4-DIHETHYLPHENOL . . . .45-85-6 BENZOIC ACID111-91-1 BIS<2-CHLOROETHOXY>METHANE12*-83-2 2.4-OICHLOROPHENOL . . . .126-82-1 1.2,4-TRICHLOROBENZENE . .9l-2*-3 NAPHTHALENE . . '1*6-47-8 4-CHLOROANILINE

87-68-3 HEXACHLOROBUTADIENE . . .S9-S*-7 4-CHLORO-3-METHYLPHENOL .91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE88-*4-2 2. 4, 4-TRICHLOROPHENOL . .95-95-4 2,4,5-TRICHLOROPHENOL . .91-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NXTROANILINC131-11-3 DIMETHYL PHTHALATE . . . .2*8-94-8 ACENAPHTHYLENE99-*9-2 3-NITROANILINE

UG/L

!•1*!•1816!•18181816161616161616S6161616161616161616165616S616165*

UUUUUUUUUUUUUUUUUUUUUUUUUUUU

UU

UUU

CAS NUMBER83-32-951-28-51*8-82-7132-44-9121-14-2464-28-284-44-2766S-72-384-7J-71*6-16-4534-52-184-36-41*1-55-3118-74-187-84-18S-61-8126-12-784-74-2264-44-6129-66-68S-48-791-94-154-55-3117-81-7218-61-9117-84-62*5-99-22*7-*8-95*-32-B193-39-553-76-3191-24-2

ACENAPHTHENE2.4-DINITROPHENOL . . . .4-NITROPHENOLOIBENZOFURAN2,4-OINITROTOLUENE . . . .2.4-DXNXTROTOLUENE . . . .OIETHYLPHTHALATE4-CMLOROPHENYL-PHENYLETHCR

FLUORENC4-NITROANILINE4. 4-OINITMO-2-METHYLPHENOLN-NITROSOOIPHENYLAMINE <1>4-BROHOPHENYL-PHENYLETHERHtXACHLOROBENZENE . . . .PEKTACHLOROPHENOL . . . .PHENANTHRENEANTHRACENEDI-N-BUTYLPHTHALATE . . .FLUORANTHENEPYRENEBUTYLBENZYLPHTHALATE . . .3.3'-OICHLOROBENZIOINE . .8ENZO<A)ANTHRACENE . . . .BIS<2-ETHYLHEXYL> PHTHALATECHRYSENEOI-N-OCTYL PHTHALATE . . .BENZO(B>FLUORANTHENE . . .BENZOOOFLUORANTHENE . . .BENZO<A)PYRENEINOENO<1.2.3-CO>PYRENE . .DIBENZ<A.H>ANTHRACENE . .BENZCMG. H, DPERYLENE . . .

UG/L16 U

UU

56561616161616165*5*161616ft*16161616161626161616161*1*1*1*1*

UUUUUUUUUUUUUUUUUUUUUUUUUUUU

16 U

<1> - CANNOT BE SEPARATED FROM 01PHENYLAMINE

FORM X

4 1 8 4 3 0 2 1 3

tin dtr-Cd'.E NC

Festicides/F'i&s

Concentration: [Lou] llediut (Circle one)Date Extracted/Prepared: 2?-Sep-87Date Analyzed: 06-OCT-87Conc/Dil Factor: 5Percent Hoisturefdlecanted) NR

EPC Cleanup Ves (x]-NoSsparjtory Fu-nsl Extraction YesContinuous Liquid-Liquid Extraction [i] Yes

CAS [uq/L] or us/KgNuiber

319-84-6 Alphi-BHC 0.25 U319-85-7 Beti-BHC 0.25 U319-Bt-B Delta-rHC 0.25 U58-69-9 Gifu-BHC (Lindine) 0.25 U74-M-E Heptachlor 0.25 U309-00-2 flldnn 0.25 U1024-57-3 Heptachlor Epoiide 0.25 U959-98-8 Endosulfin I 0.25 U60-57-1 Oitldrin ''o.5U72-55-9 4,4'-DDE 0.5 U72-20-B Endrin 0.51)33213-65-9 Endosulfin II 0.5 U72-54-8 4,4'-DDD 0.5 U1-31-07-B Endosulfin Sulfile 0.5 U50-29-3 4,4'-DDT 0.5 U72-43-5 nethoxychlor 2. U53494-70-5 Endrin Ketone 0. U57-74-9 Chlordin* 2. U8001-35-2 Toxaphene U12674-11-2 Aroclor-1016 2. U11104-28-2 Aroclor-1221 2.5 U11141-16-5 Aroclor-1232 2.5 U53469-21-9 Aroclor-1242 2.5 U12i72-29-(- «roclor-124B 2.5 U11C97-69-1 flroclor-1254 5U11096-82-5 Aroclor-1260 5U

Vi = Voluie of extract injected (ul)Vs - Volute of niter extracted (illIK = Height of saiple extracted (g)Vt -- Voluie of total extract (ul)

Vs = 1000 or Ms - Vt = 50000 Vi - 3.0

Fora ]

4184 30214

o.r f lo. , N.,,nc _KI'-''J^ ; i ;''";; _

Case No


Sample fJ, j . r \ t>--


CASCompouod Nam* Fraction

RT of

(ug/jfor ug/Vg)

1..2-oC,

/r

tf*7V

•7..

I.UkkUnit

W

ILnLUnic

An u .IB

17.

/Xnk: A

121..

23..

24..

25..

26..

27..

29..

30..


4 1 8 4 3 0 2 1 5

MOLl-w? 34*1


LAS SAMPLE 10 NO: 4114-94SAMPLE MATRIX: WATER

DATA RELEASE AUTHORIZED •


(PAGE 1)

CASE NO:

8C REPORT NO:

CONTRACT NO:

DATE SAMPLE RECEIVED.4l41844184

•f/29/87

VOLATILE COMPOUNDS

CONCENTRATION: LOW

DATE EXTRACTED/PREPARED:

DATE ANALYZED: l«/*3/87

CONC/DIL FACTOR: 1.

PERCENT MOISTURE: (NOT DECANTED)

PH

CAS MUNICH

74-87-1 CHLOROMETHANE

74-83-9 BROHOMETHANE

71-4U-4 VINYL CHLORIDE

7S-88-J CHLOROETHANE

71-89-2 METHYLENE CHLORIDE . . .

67-44-1 ACETONE

7S-1S-* CARBON OISULFIDE . . . .

71-31-4 1.1-DICHLOROETHENt . . .

71-15-1 1.1-DICHLOROETHANE . . .

1S4-48-1 TRAM1-1.2-OKHLOROETHENE

47-44-1 CHLOROFORM

1*7-84-2 1.2-OICHLOROETHANC . . .

71-93-3 2-1UTANOWE71-S»-* 1,1,1-TRICHLOROETHANE .

14-23-1 CARBON TETRACHLORIOE . .

1*8-81-4 VINYL ACETATE

71-27-4 BROHODICHLOROHETHAME . .

CAS NUMBER

!•

18

18

1

18

1

18

1

UUUUUUUUUUUU

UUUU

79-81-4

124-48-1

71-43-218841-81-1

118-71-8

71-21-2

191-78-4

127-18-4

79-34-1

188-88-3

188-41-4

188-42-1

1.2-DICHLOROFROPANE . . .

TRAN1-1.1-DXCHLOROPROENE .

TRICHLOROETHENE

OIBROHOCHLOROMETHANE . . .


BENZENE

CIS-1,3-OICHLOROPROPENE .2-CHLOROETHYLVZNYLETHER .

BROMOrOMH4-HETHYL-2-FENTANONE . . .

2-HEXANONETETRACHLOROETHCNE . . . .

1.1.2.2-TCTRACHLOROETHANE

TOLUENE

CHLOROBENZENE

ETHYLBENZENE

STYRENC

TOTAL XYLENE1

UG/L1SsS11s

UUUUUUUUUUUUUUUUUU

8 - COMPOUND WAS DETECTED IN THE BC BLANK.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED



REPORTING B.UALIFIER1.FORM I

4184 30248


Case No: 4184

Sample Number

10 3o


CAS Number

67-63-0

71-36-3

78-92-2

Compound N>me

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationjif/L

300U

200U

200U

U Tnduf*»f romrrtnvl jygg analyzed fOT but <VM <Vtf"1*'l_ RCBOft me minimum ijf^p'tfffq Imiit f(jf (he f«^p^f with |he U(e.(. 10U) based on necesvy concentntioB/dlhitian acttoo. CThit U not neccsvilymeuistnuneatdetoctiooUinil)The footnote timid rod: U-Compoond was analyzed for but not detected. The number is the mimmom tftriubfe

tvahe, Thb flat Un^ richer when e«tinudnj a cooceai«k)n for tentatively identiWoCPC till ICSDOQ3C IS ftSSD^QfiQ Of WuCO ^DC ^DAU tDOCt^H ullft IPolCJtPo QIC DI QCOCC OK ft C^^-UHMtlQ t&flt ^ftOCO u9C lOCflO"ficaion oteia but the result it less than tb« g>edfled detoetioo limit but greater man rero (04.101). If limit of detection ii10 \iffL and a concentration of 3 u$/L is calnilitfrrt, report at 3J.

4 1 8 4 3 0 2 4 9

r, .t

Case Mo

Concentration: (Low") Medium

Date Extracted'Prepared

Date Analyzed: Icldrhl



(Circle One)

N'jrn be r

Cone/Oil Factor:

Percent Moisture (Decanted).

GPC Cleanup QYes ONo

Separatory Funnel Extraction QYes

Continuous Liquid • Liquid Extraction QYes

CASNumber

ug/torug/Kg(Cwcle One)

CASNumber

108 95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-212O-82-191-20-3106-47-887-68-3S9-SO-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3208 96-899-O9 2

Phenolois<-2 -CWoroeth/HEther2-CM<xoprvtrtol1. 3-Oichlorobenz«ne1. 4-OichlorobenzeneBenzyl Alcohol1. 2-Dicnforob*n»ne2-M^hylprwnolbi«(2-chloroisopropyl)EtrMr4-M*thy1ph«nolN-Nrtroso-Oi-n-PropylamineHexacMoroethaneNrtrobenzeneIsophoront2-Nitropnenol2. 4-DimethylphenolBeruoic Acidbis( • 2 -CMoroethoxYlMemant2. 4-OicriloropHenol1. 2, 4-TrichlorotenuneNaphtha l«n«4-CMoroaniline

He Kachtorobutadiene4-Chloro-3-M«thY<phenol2-Methy<naphthaltnt

2. 4. 6-Trichlorophenol2. 4. 5-Tnchkxophenol2 -Chloronaphthalent2-N<iroanilineDimethyl PhthalateAcenaphTtiyleoe3-Nilroaniline

/0U./Ok10 utoi,.10k10k.{nt~\F\VL(fluluaIDulOuIDu}£Hifiu/Qb-

WfA

/nu.feklOu.IDum±tOfilUt<Ity.10*/Ou

S'tu(CliA

56*ID*IQlA

s»*

ug/lorwg/Ke(Circle One

83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-316-73-7100-01-6534.52-186-30-6101-55-3118-74-117-86-StS-01-8120-12-784-74-2206-44-0129-OOX)15-68-711-94-1>6-55-3117-81-7218-01-9117-84-0iOS-99-2207-08-9J032-8193 39 5i3-703191 24-2

Acenaphthene!. 4-Dinhroph«nol

4-Nitrophenol>ibemofuran!.4-Oinitrotoluene

2..6-Oinitrotolu«n«Oiethylphthalate4-Chlorophenyl-phenytether:luor»ne4-NrtroanilirM4. 6-Oinhro-2-Methy(ph«nolN-NrtrosodiphenyUmine (1)

Hexachloroberu«n«PtntachlorophenolPhencnthreneAnthraceneOt-n-Butylphthalate:luorinthenePyreneBjtytt>eruY<phthat«te

3. 3''0tchlorober\tid4neB*<uo(i (Anthracenebu(2-Ethy«h«xYl)Prrtn*l«teChrysene0«-n-Octy< PhthafateBento(b)FluoranmeneBeniotk)Fluoranth«neBen«o(a)Pvr«neIndenotl. 2. 3<dlPyreneOcbenita h(Antht jceneB«nro(g. h. iJPerylene

IVlt'faStu

IfOkIfiu\hu./ham*-10*

fsKsou

IVutot*(flu.

Si*

IQ"[fiu

!QUnulOh

WuJeu

/(JU./QL\OtA-

IQu.mirId1*'//)tînu^mi*.fn«.

(l)-Cannoi b«

fO'4 1 8 4 3027S

a=e No: 4164

Orqanics flnalysis Data Sheet(Page 3)Pesticides/PCBs

Conce"trjt.jc'-: [Lou] fledju* (Circle one)Date Extracted/Prepared; 29-Sep-B7Date Analyzed: Oi-Oct-B7Conc'Dil Factor: 1Percent Hoisture(decanted) UR

BFC Clej-'.p Yes [0-MoSeparatory Funnel Extraction YesContinuous Liquid-Liquid Extraction [x] Yes

CAS [ug.'L] or ug/KgNuibtr

319-84-6 Alph»-BHC 0.05 U319-85-7 I»U-BHC 0.05 U319-86-8 OelU-BHC 0.05 U58-89-9 6a«u-BHC (Lindane) 0.05 U76-44-8 HepUchlor 0.05 U309-00-2 Aldrin 0.05 U1024-57-3 Heptichlor Epoxidi 0.05 U959-98-8 EndosultM I 0.05 U60-57-1 Dieldrin 0.1 U72-55-9 4,4'-DD€ 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfin II 0.1 U72-54-8 4,41-ODD 0.1 U1-31-07-8 Endosulfin Sulf»te 0.1 U50-29-3 4,4'-Dl>T 0.1 U72-43-5 Bethoiychlor 0.5 U53494-70-5 Endrin K«ton« 0.1 U57-74-9 Chlord»n« 0.5 U8001-35-2 To»»phM» ID12674-11-2 Aroclor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U534A9-21-9 Aroclor-1242 0.5 U12672-29-6 ftroclor-1248 0.5 U11097-69-1 Arodor-1254 I D11096-82-5 Aroclor-1260 1U

Vi = Volutt of extract injected (ul)Vi = Volute of »*ter extracted 111)N« - Mfiqht o< staple ext racted (g)Vt -- Voluw of total ex t rac t lull

Vs -- 1000 or Hs Vt = 10000 = 3.0

For§

4 1 8 4 3 0 2 5 1

Lai aio' y f ; . < : • • • . - I: • •_ ' '.'.

~ - - ;pNo

Organics Analysts Data Sheet(Page 4}

Sample


;ASCompound N«m« Fraction

RT«n < i tion

(fl/j/orog/kg)^

/. .

•- .

1O..

IV. 51*?

16..

19..

21..

I..

24..

i..

-5..

29

NFA denotes no fraction analyzedNCF denotes no compound found'nk denotes unknown.nw denotes probable nrxDlecular weight

4 1 8 4 3 0 2 5 2


LAB SAMPLE ID NO: 4184-112

SAMPLE MATRIX: HATERDATA RELEASE AUTHORIZED BY

418*4184

ORCANICS ANALYSIS OATA SHEET

(PAGE 1)

CASE NO:*C REPORT NO:CONTRACT NO:

DATE SAMPLE RECEIVED:

VOLATILE COMPOUNDS

•9/29/87

CONCENTRATION: LOW


DATE ANALYZED: l»/»S/87

CONC/DIL FACTOR: 1.


PH

CAS NUMBEI74-87-374-83-f75 -81-*

7S-88-375-89-247-44-17S-U-*7S-3S-*75-35-3154-48-547-44-3187-84-278-93-371-SS-4S4-23-I188-85-475 -27-*

I

CHLOROMETHANEiROHOMETHANEVINYL CHLORIDECHLOROETHANCMETHYLENE CHLORIDE . . . .ACETONECARBON OISULFIDE1. 1-OICHLOROETHENE . . . .1. 1-OICHLOROCTHANC . . . .TRAMS-1.2-OICHLOROETHEMC .CHLOROFORM1,2-OICHLOROETHANE . . . .2-BUTANONE1, 1, 1-TRICHLOROETHANE . .CARBON TETRACHLORIDE . . .VINYL ACETATEBROMOOICHLOROMETHANE . . .

UO

14

1114

14

1

14

1

1<

/L

1 U• U1 U) U> u» u

uuuuuuuuu

I U

K U

CAS NUMBER78-87-K!••& 1-82-479-81-4124-48-179-M-571-43-218841-Ol-f'118-75-87S-2S-2188-18-1591-78-4127-18-479-34-S1*8-88-3188-98-7188-41-4188-42-5

UO/L

1.2-DICHLOROPROPANE . . .TRAN5-1.3-DICHLOROPROENE .TRICHLOROETHENEOIBROMOCHLOROHETHANE . . .1.1,2-TRICHLOROETHANE . .BENZENE

CIS-1.3-DICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORN

4-MCTHYL-2-PENTANONE . . .2-HEXANONt

TETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENE

CHLOROBENZENCETHYLBENZENCSTYRENETOTAL XYLENCf

18S1*!•I10SS•SS

uuuuuuuuuuuuuuuuuu

U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.


REPORTING QUALIFIERS.FORM I

4 1 8 4 3 0 5 7 5


Case No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

ConcentrationHi/L

300U

200U

200U

U Tnrticata c^T^tld "$ "ulyr^ fnr Hit rift AnmtA Bqvwt die minimum detection limit fog the mnple with me U(e.f . 10U) based on necessary concenlratioo/dilutJoo action. (Tto u »ot necessarily me instromem detection limit)Tbt footnote sbookl read: U-Compouod was analyzed for but not detected. The amber u the minimum inainabtedetection limit for the sample.

an fttim*fA value. This flag U used either when »p«Mring s coocentratioa far tentatively identified compounds1:1 fSpOMf U Igynffi Or TOPI fcC man lp«?rrf 4at> i~«^*4 i*«> pn^mr^ rf • nnmpmnd

featioo criteria btttbercsott is less than the speared det^^ If limit of detection is10 H4/L and a concentntion of 3 U£/L is calculated, report as 3J.

4 1 8 4 3 0 5 7 6

_ase No

_:or>centration




Medium (Circle One)

S»mplo N

>ate Analy7ed (tin 1X1

Conc/Dil Factor:


GPC Cleanup OYes DNo

Separaiory Funnel Extraction QYes


CAS wQ/lorug/KgNumber (Circle One

106 95 2111-44-4

95 57-8

Ml -73-1

106-46-7

100-51-6

95-50-195-48-739636-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-29595-491 58-788-74-4131-11-3208 96 899-09 2

Phenolbis<-2-Chtoroethyl|Ether2-Chlorophenol1 . 3-Dichlorobentene1. 4-DtchloroberueneSeruyi Alcohol1 . 2-Dichloroberuene2-Methylph«nolbts(2-chloroiMpropy1|ElH«r4-Methy<ph«nolN-Nitroso-Di-n-PropvUmirteHexachloroethaneNitrobenzeneUophofooe2-NiuopSenol2. 4-Dimethy<phenolBenioic Acidbi«( • 2 -Chtef oetnoxylMetna ne2. 4.Qichlorophenol1. 2. 4-TricMorobenzeneNaphthalene4-CMoroenitineHecacMorobuiadierte4-Chloro-3-Methy1pl>enol2-Memyl naphthaleneHeuchtorocyclopentadien*2. 4. 6-Trichloropnenol2. 4. 5-Tr<hloropKenol2 -CMoronaphthalene2-Nitroan<lineDimethyl PhthalateAcen«Dhthytene

3-NiIfoanilir>«

/On.rf}*10 itIn*.10u

/Ot^/nt~/rttciQuJuu.lf)ulOulOuICîQuIQ^

Wttinu.feuiOu.ID*m±lf)U

lOu.lOif-Ifo/OlA.

rou(flu

5t><*IDlA.

I0t*5»i\

CAS ug/lorug/KgNumber (Circle One

83-32-951-28-5100-02-7132-64-9121-14-2606-20-28446-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-18746-585-01-8120-12-7W-74-2206-44-0129-00-0»5-68-7M-94-1>6-553117-81-7218-01-9117-84-0205-99-2207-08-9J032-819339553-70-3191-24-2

Acenaphtrtene2. 4-Dinhrophenol4-Nitrophenol>iber\zofuran!. 4-Oinmoioluene!. 6-Oinhrotoluene

Oiethytpnthatate4-Chlorophen)1-pnenyletherRuorene4-Nttroaniline4. 6-Oinhro-2-MethYlpnenolN-NitrosodiphenyUmine (1 )4-Bromapneny1-pn*nytetherHexachlorobenzenePentachtefophenol^wriantTifer eA nTflrar^tfi*

Ot-n-SutylpHthatateFluorinthenePyreneBurylbemytphtha late3. 3'-0«Morober\zidine

Be<uo(< (Anthracene

bt*2-Ethy!hexy<)Prrthalate

CNy»ene

Oi-n-Octy4 Phthatate

B«rua(b)Fluor«nthene

Benzo(V)Fluoranthe<%e

BennXalPYTArw

lr«Jeno(1.2. 3<d»Py^ne

Oib«rvi(a hJAnthracerie

6«nio(g. h. i)PeTY<eoe

IVlA.'fa

54 U\n\*.lf)u/PU./huin*-fOif

5^ A

ft 14jOu.faIfiu.

*>«On

ftiufQuIf) Li

((?'')buJ»a

lOu./fluHJISL

(Ou./ntrifltL,

Ifivinu.ip<~In*.

(1 r-Canr>oi be

F 0'

4 1 8 4 3 0 5 7 77 - 8 5

-I

late E:tra:tf;:;Frepa'?;: :5-Ee;-6?

Cnnc/Dil Factor:Percent M:r=tLreH!s:arls:J'

Njiber

'ralvs;s Data it-pet

6PC r.!eanuf Yes [i]-NoSeparator; Fur..iel Eitrjction YesI:"*:.'u:u5 Liqs;iiJ-Li5i;ii! Estraction [>} Yes

or

319-B5-7

"19-Bt-B5B-89-9

309-OC-21024-57-3959-98-860-57-1

72-55-972-20-9

33213-65-972-54-81-31-07-850-29-372-43-553494-70-5

57-74-98001-35-212674-11-211104-28-2

11141-16-55*469-21-9

I'l'^-ei-l11C96-B2-?

Beti-BHCDelU-BHC

HeptjcMor

AldrinHeptachlor Eponde

4, 4' -DDE

Erdosulfin II4,4'-JIDll ,.,

Endoiulftn Sulfite4,4'-D|)T

Endnn Ketone

Aroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242

ftroclor-1254

Arodor-1260

0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.5 U0.1 U0.5 UI D

0.5 U0.5 U0.5 U0.5 U0.5 U

1 U1 U

Vs =

Vi = Volui* of eitrict injected lul)Vs = Volute of «ater eitricted (il)Us : Height of saiple eitricted lq|Vt -- Volute of total eitract (ul)

1POO or Ms - Vt =

Fort I

10000 Vi = 3.0

4 1 8 4 3 0 5 7 8

Name ETC/Toxicon

e No

Organics Analysis Data Sheet{Page 4)


Sample t>

'?/Vk*)03>SQ

CASNumb** Compound N«ITM Fraction

Estimated

1..

5..

7..

O..531

1C,

17.

1ft

UFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmv denotes probable molecular weight

4 1 8 4 3 0 5 7 9

LABORATORY NAME: ETC/TOXICONLAB SAMPLE ID NO: 4184-9*

SAMPLE MATRIX: WATER

DATA RELEASE AUTHORIZED BY:

ORGANICS ANALYSIS DATA SHEET<PAGE 1>

CASE NO: 4194•C REPORT NO: 4184

CONTRACT NO: Q\ «-fDATE SAMPLE RECEIVED:

,

*9/:9/87

VOLATILE COMPOUNDS

CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYZED: l«/»3/67

CONC/OIL FACTOR: t.

PERCENT MOISTURE: <NOT DECANTED)PH

CAS NUMBEP

74-87-3

74-83-f7S-81-4

7S-»#-3

7S-tt-247-44-1

7S-1S-8

7S-3S-*

7S-3I-3

154-4*-S

47-44-3l»7-»*-2

78-»3-»

71-SS-*

S4-23-Sl*8-«S-4

7S-27-4

1

CHLOROMETHANE

BROMOMETHANE

VINYL CHLORIDE

CHLOROETHANE

METHYLENE CHLORIDE . . . .

ACETONECARBON OISULFIOE

1. 1-DICHLOROETHEME . . . .

1, i-OICHLOROETHANE . . . .

TRAN3-1,2-DZCHLOROETHENE .

CHLOROFORM

1.2-OICHLOROETHANE . . . .

2-BUTANONE1.1. 1-TRICHLOROETHANE . .

CARBON TETRACHLOMIDE . . .

VINYL ACETATE

•RQMOOICHLOROMETHANC . . .

uc14

14

14

14

1

11

1

1

!

i/L

1 U> U> Ui u

> u» u

uuuuuu06uu

> uI U

CAS NUMBER

7«-i7-S

1M41-82-4

7f-*l-4

124-48-1

79-M-S71-43-2

1««41~*1-S

llt-75-8

71 -25 -2

1M-1*-1

S»t-78-4

127-18-*79-34-S

1*6-88-318t-»»-7

14>«-41-4

l»*-42-S

U6/L1,2-DICHLOROPROPANC . . .TRANS-1.J-OICHLOROPROENE .

TRICHLOROETHENEDIBROHOCHLOROMETHANE . . .1.1.2-TRICHLOROETHANE . .

BENZENECIS-t.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORM

4-METHVL-2-PENTANONE . . .

2-HEXANONETETRACHLOROETHENE . . . .

1-1,2.2-TETRACHLOROETHANC

TOLUENECHLOROBENZENEETHYLBENZENESTYRENE

TOTAL XVLENES

S14

UUuuuuuuuuuuuuuuuu

B - COMPOUND WAS DETECTED IN THE 8C BLANK.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED


SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING BUALIFIERS.

FOR* Z

4184 30321


Case No: 4184

Sample Nurabtr


CAS Number

67-63-0 ,

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationut/L

300U

200U

200U

U Indicates compound was analyzed for but not 'Vifficil Report the minimntn detection limit for tbe sample with the U(e-t-lOU) based on necesory cotKcxumxrtdihitkn actioo. (This is not necessarily the instnuneat detection limit)The footnote should read: U-Compound was analyzed for bat not detected. Tbe namber U tbe minimum ctainabledetection limh for the «»mpi<»

J i*Atr***f tn xti""** value. This flag 1s used eits«- when *<m««<i a ooncentiation for tentatively identified compoundswhere a 1:1 response U assumed or wben (he mass spectnl data indicated (he prueace of a compound that meets the ideoti-fication criteria but the result is less man the specified detecdoe limb but greater than zero (ej. 1QJ). If limit of detection is10 nt/L and a cooceamrioo of 3 n«/L is calculated, report as 3J.

4 1 8 4 3 0 3 2 2

LdlMV

Case

r.:S a f ~M p I *

Concentration fLow) Medium

Date Ertracted'Prepared

Date Analyzed

Conc/Dil Factor:

Organics Analysis Data Sheet(Page 2}


(Circle One) GPC Cleanup OYes ONo

CASNumber

idoif^l

r-

r* (Oeci«ntff<l) . . .

ug/lor ug/Kg(Circle One)

•henol*s(-2-Chloroethyt)Ether

-Chlorophenol. 3-Dichlorobenzene. 4-Oichlorobenzenetetuyt Alcohol

. 2-Dichlorobenzene

-MethyJphenol

i«<2 -chloroisopropyt)Eirter-Methylphenol

1 • Nitroso-Oi -n-PropylaminetexachloroethaneJrtrobenzene

wphorone

!-Nitroph«nolt. 4-Oimethvlpnenolleruoic Acid

» j< • 2 -ChtoroethoxylMethane

1. 4-Dichlorophenol. 2. 4-Tf tchlofooeniene

Naphthalene

l-Chloroartiline

•feKachlorobutadiene

l-Chlofo-3-Metrtytph«no«

l-Methytnaphthalent•«« uchlorocyclopentadtene

2. 4. 6-Trichlorophenol2. 4. 5-Tr«chkxophenol2-Ch(<xon«phthalen«

2-NitroanilineDimethyl Phthalate

Acenaphthyiene

/OIL//)nID uIn*.10klOl/nt-10*.ID*lu*lf)i*lOu10*10kifltL

/Ok-

%tt

in*.10*ip*ID*

lf)tL10*to*.lup-in*.

ftu(fitA

J*MID*

Continuous Liquid - Liquid Extraction OYes

CAS ug/lor ug/KgNumber (Circle One3-32-91-28-50X3-02-7

32-64-921-14-2

606-20-284-66-2

005-72-386-73-7

00-01-6534-52-1

86-30-6

01-55-318-74-1

I7-66-S

85-01-8120-12-7

84-74-2

206-44-0129-00-055-687M-94-1

>6-55-3117-81-7

218-01-9117-84-0205-99-2207-08-9

5032-819339553-703191 24-2

Acenaphtherte!. 4-Oinhrophenol

4-NitropNeno(liberuofuran

:.4-Dinitrotoluene!..6-D«nitroiotLiene

OiethyiphthalateJ /U | t . » . .

Fluorene

4-Nhroaniline4. 6-Oinitro-2-MethY<pr)enolN-Niuosodipt>enYl*iT»ine (1 j

4-Bromopheny(-phenytether

KeucMocobenzenePentacMoropnenoi

PhenamhreneAnthraceneOt-n-8uty»phthaujte

FluoramhenePyreneBatytt>eriiYU>hthalate3. 3'-Oichkxoberu;id<ne

Benzo(( uxnthr ace nebij(2 -EthyJSe cyHPhtha late

ChryseneOi-n-Octyl Phthalate

Benzo(b)Fl uora nthene

BenzotkjFluorantheneBenzo(a)PyTene

lnderto(1 . 2. 3-cd)Pyf eneDibenfla huVnthraceoeB«n;o(g h ip«ryleoe

IQiL

'diA

54uJIOJ*.(flu\f)LLin*(Otf-(Ot*

?4*9fiA

I(Mk*fflu

x>«(OnffilL

I(~)LI/f)bL

(flittun

afrtl

to*.lOt^JfJu.(fami>-iflbL,Ifii 'ink. _Ipls-

in*. _

(11 -Cjn

4 1 8 4 3 0 3 2 5

Analysis Data Sheet(Page 3)Pestuides/PCBs

Cor,cer,tr»tian: [Lou] Hediui (Circle ore)Pate E«tra:ted/Frepared: 29-Sep-87Date A."iiv;ed: 07-Oct-B7Conc/Dil Factor: 1Percent Roistu^decanteiJ) "R

6PC Cleanup Yes [i]-HoSeparatery Funnel Extraction YesContinuous liquid-Liquid Eitractian [x] Yes

CASNuiber

319-84-6319-85-7J19-86-858-89-976-44-8309-00-21024-57-3959-98-B60-57-172-55-972-20-833213-65-972-54-81-31-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-6110*7-69-111096-B2-5

Alph»-BHCBeta-WCBelta-IHC£jiia-BHC (Lindint)

Aldrin

Endosulfin I

4I4'-00£

Endosulfin I]4)4'-DDD

4f4--DOTHethoiychlor

Aroclor-1016Uroc lor- 1221flroclor-1232Aroclor-1242Aroclor-1248Arorlor-1254Aroclor-1260

[uq/L] or ug/Kq

0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.5 U0.1 U0.5 U

1 U0.5 U0.5 U0.5 U0.5 U0.5 U

1 U1 U

Vi = Voluie of titnct injected (ul)Vs : Volui* of Mter e.tricted (illUs : Height of saiple eitracted (q)Vt -- Voluie of total extract lull

Vs - 1000 or Ms Vt = 10000 Vi = 3.0

Fon 1

4 1 8 4 3 0 3 2 4

L o' a io ' y

••-No



Ei

Sample Number

CASNumber

1

*-

I-

t

S

»

f

*a.

10

•is

>4

S--

1ft

7

.•

19

•0

>1

•?»-

•J

?*

«J«J7.

M

M

10

Compound N«m«

Wo/.

UM*

UlOt.

*

Fraction

^/«r/i£

5f^,t/f4

RT orTSon^^Numbjr/

51563^

E*tim«t*d^Cooc«ntntiofl(ug/yor ug/kg)

15i-l

NFA denotes no fraction analyzedNCF denotes no compound foundInk denotes unknownmw denotes probable molecular weight

4184 30325

_ - S E R


LAB SAMPLE ID NO. 4184-188SAMPLE MATRIX: WATERDATA RELEASE AUTHORIZED •'


CASE NO: 4184X fiC REPORT NO. 41B4

CONTRACT NO: Q)^DATE SAMPLE RECEIVED:

VOLATILE COMPOUNDS

CONCENTRATION: LOW


DATE ANALYZED: 18/83/87

CONC/OIL FACTOR: 1.


PH

CAS NUMiER

74-87-1 CHLOROMCTHANC

74-81-* IROMOHCTHANC

7S-81-4 VINYL CHLORIDE

75-88-3 CHLOROCTHANC

7S-8»-2 METHYLENE CHLORIDE . . .

47-44-1 ACETONC

75-15-8 CARBON OISULFIDE . . . .

7S-35-4 1.1-OICHLOROETHENE . . .

75-35-3 1,1-DICHLOROCTHANC . . .

1S4-48-S TRANS-1,2-DICHLOROETHENE

47-44-1 CHLOROFORM

1*7-84-2 1,2-OICHLOROETHANC . . .

78,-tl-l 2-tUTANQNE

71-55-4 1. I. 1-TRXCHLOROCTHAME .

54-23-5 CARtON TETRACHLORIOE . .

188-85-4 VINYL ACETATE

71-27-4 BROMODICHLOROMETHANE . .

UG

11

11

14

14

S

14

1

1

'

»/L

1 UI U> Ur u> 0

> uuuuuuufOuu

1 U

1 U

CAS NUMBER78-87-S18841-82-47»-8l-4124-48-17»-88-S71-43-218841-81-S118-75-87S-2S-2188-18-1Sfl-78-4127-18-471-34-S188-88-3188-98-7188-41-4188-42-5

UG/L1.2-OICHLOROPROPANC . . .

TRANS-1. 1-OICHLOROPROENE .

TRICHLOROETHENE

DIBROMOCHLOROHETHANE . . .1,1,2-TRICHLOROETHANC . .

BENZENE

CI5-1.3-DICHLOROPROPENE .

2-CHLOROETHYLVINYLETHER .

•ROMOFORN4-METHYL-2-PENTANONE . . .

2-HEXANONC

TETRACHLOROETHENE . . . .1,1.2.2-TETRACHLOROETHANE

TOLUENECHLOROBENZENC

ETHYLBENZENE

STYRENE

TOTAL XYLENES

18

f18

18

S18

UUUuuuuuuuuuuuuuuu

B - COMPOUND WAS DETECTED IN THE 8C BLANK.



THE SAMPLE.

SEE PACE 1A FOR COMPLETE DEFINITIONS OF THE DATA

REPORTING QUALIFIERS.

FORH I

4 1 8 4 3 0 3 3 5

Labora tory Name: ETC/Toxicon

Case No: 4184

Sample Numt>«r


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationm/L

300U

200U

200U

U TifrtVTt tnmpnpuA was analyzed for but *w* ^"^f'lrt Repot the mini mm detection i""** for the sample with tfae U(e.g. 10U) baaed on necessary coocattmJon/dflution action. CThis is not necessarily the insirument detection limit)The footnote should read: U-Compoand was snalyzed for bat not detected. The number is me minimum attainabledetection Hmit for tbe *<"n«**

J Indicates U estimated Vibe. ™f H«|t ^t Tf^* ^Îff •*•• »«ri'««*<«e • moontr^lnH for t«itarivriy M«irifWM mmpnnfK<«where a 1:1 response is assumed or when the man speed! data indicated me presence of a compound mat meets me ideial-fcation criteria but merenb bless than me spedfW detection limit bnt ideate than KTO (e.j. 1QJ). Iflimitofdetectioots10 m/L and a concentration of 3 uj/L is calculated, report as 3J.

4 1 8 4 30336

La!, . 'a : . , r, ,- ..

Case No V-.


(Page 2)


Sample

Concentration (Low) Medium (Circle One)^-^ .rA+A


Date Analyzed

Conc/Dd Factor.

Percent Moisture (Decanted).


Separatory Funnel Extraction QYes

Continuous Liquid - Liquid Extraction QYes

CASNumber

ug/lerug/Kfl CAS

106-95-2111-44-4

95-57-8541-73-1106-46-7

100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-1

98-95-378-59-188-75-5105-67-965-85-0

111-91-1120-83-2120-82-191-20-3106-47-887-68-3S9-SO-791-S7-677-47-4

88-06-295-95-4

91-58-7 j88 74.4

131-11-320896-899-09 2

Phenolbis< - 2 -Cnioroeth yOEtrter

2-CMorophenol1 . 3-Oich(oroberuene

1 . 4-OicMorobenzentBeruyl Alcohol1 . 2-Oichtorobtnzene2-M«thy10henol

bis(2-chloroisopropY<)Ether4-MethytphtnolN-Nitroso-Di-n-PropyUmirw

HcKachloroethanc

NitrobenzeneIsophoront2-Nrtrophtnol2. 4-Oimethy(phenolBenzok Acidbis< - 2 -Ch(oro«tnoxYlM«th«ne

2. 4-Oichlorophenol1. 2. 4-TrkhloroberueneN«phtK»krt«

4-O>loro«r«ilineHe ucniorobut»diene4-Chloro-3-Methy1p'*"0<2-M«tny<n«phthaltnc

H«uchlorocyctopent>diene2. 4. 6 Trichlorophenol2. 4. S-Trichkxopnenol2 - CMorooi (fvi l«ne2-NiUoanilineDimethyl Ptithalate

Acenaphthylene3 Niuoarnlirv*

/Ou.//)k10 u

tOt*.10ulot*.(rit-/OM.

IQuilf)ulOuIDu/^KifiuIO(>-

^ttinu.10/Ou.ID*m±in &10*Ito.IfofOa

ftu\CitA

&nlOlA.fOlA

SttA.

Number (Circle One83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-77-316-73-7100-01-8534-52-116-30-6101-55-3118-74-1

17-86-585-01 -8120-12-7

84-74-2206-44-0129-00-0(5-68-711-94-1

>6-55-3117-81-7

218-01-9117-84-0205-99-2207-08-9MX 32 -819339-553-70-3191-24-2

Acenaphthene:. 4-Dinitrophenol

4-NrtrophenolJibennfuran

!. 4-Dinhrotoluene2, 4-D<nctroTofueneDJethvlprrtfialate

Fluor ene4-NhroamTirw

4. 6-OMtro-2-M«thYtpheno<

N-Nttro«o*phenvUmine (1 )JO h 4 IS* 4**tt* ~ *** OT«OP"* cvyi -pn* n ywv\c*

PtnuchtorophtnolPhencmhr«n.i

^nirvwcwncOi-n-ButytphthalateFluonnthenePyrene8ury(benry(phtna(ate3. 3'-Ochloroberuidine

8«Mo(«)Ajntv«cenetw(2 -Ethytrtexy()Prnhataie

Chryien*0<-n-Octyl PruhaUte8«nn(b)FluorantheneBenttXk |FI uorantnene

Beozo(«)PyTenelndeno(1.2. 3-cd)PyreneDiberuta h)Antnracene

8en/o(g. h. iJPerylene

IVk£JtA

50 U

10k[Ob.lf)u.(hy.(Otf-(0^

to*SSU

10kftOj*fflu.

&*QL,

'faIQitIfiu

IP"WuJou

/OlA.

lf)U

lOi*.lOu.fay-

it)itstnu. _

In*

4 1 5 4

Or;ar, i :« A n a l y s i s D a t a Sheet

iFage 3)

Pes t i c ides /PCBs

CDrcentratiDn: [Lcm] Kediui ;[;r:i; or,?'

[a'.e E . t ' ac ' .e^ r reoared : :s-le:-z~

ji'.s A - a i , : ? d : O ' -Oc t -B?

C o n c ' D i i F a c t o r : ;

Fer;ent Hcusture;de:intei!i NR

6PC Cleanup Y»s [«]-Ho

Separatory Funnel [inaction Yes

Continuous Liquid-Liquid Eitract ion [i] Yes

CA5Nulter

[uq/L] or ug/Kg

I19-B4-6 Alphi-BHC ........................ 0.05 U

319-B5-7 Beta-BHC ........................ 0.05 U

Ii9-Bi-8 DelU-BHC ........................ 0.05 U

58-69-9 Gana-BHC (Lindane) ............. 0.05 U

76-44-8 Heptachlor ...................... 0.05 U

109-00-2 Aldrin .......................... 0.05 U

1C24-57-3 Heptachlor Eponde ............... 0.05 U

959-98-8 Endosulfan I .................... . 0.05 U

60-57-1 Dieldrin ........................ 0.1 U

72-55-9 4,4'-DOE ........................ 0.1 U

72-20-8 Endrin ........................ 0.1 U

33211-65-9 Endosulfui II ................... 0.1 U

72-54-B 4,4'-DDD ........................ 0.1 U

1-31-07-B Endosultan Sulfate ............... 0.1 U5C-29-3 4 ,4 ' -DDT ........................ 0.1 U

72-43-5 Nethoxychlor .................... 0.5 U

53494-70-5 Endrin Ketone ................... 0.1 U57-74-9 Chlordant ....................... 0.5 U

8001-35-2 Touphene ....................... 1 U

12674-11-2 ftroclor-1016 .................... 0.5 U

11104-2B-2 ftroclor-1221 .................... 0.5 U

11141-16-5 Arodor-1232 .................... 0.5 U

53469-21-9 Aroclor-1242 .................... 0.5 U

12672-29-t Aroclor-1248 .................... 0.5 U

KO'T-69-1 Aroclor-1254 .................... 1 U

11096-82-5 f t r c c l o r - 1 2 6 0 . . . . . . . . . . . . . . . . . . . . 1 U

Vi = Volute of eitratt injected lul)Vs ; Voluie of Mter extracted (•!)Ms - Height of saiple eitracted Ig)Vt = Volute of total eitract (ul)

Vs • 1000 or Vt 10000 Vi s 3.0

Fori I

4 1 8 4 3 0 3 3 8

La

«•- No


Sample Numf>«>r


CASNumber Compound N«m« Fraction

RT ( E*tim«t«dc«<ur«tionpf ug/kg)

2.

10..

51 fo n

16..

»..

3 .24..

5..

27..I

|».'TO.

NFA denotes no fraction analyzedNCF denotes no compound found;nk denotes unknownmw denotes probable molecular weight

4 1 8 4 30339


LAB SAMPLE ID NO. 4184-113SAMPLE MATRIX: WATER


ORGANICS ANALYSIS DATA SHEET(PAGE 1>

CASE NO: 4184

8C REPORT NO. 4184CONTRACT NO: O l4^

DATE SAMPLE RECEIVED: 89/29/87

VOLATILE COMPOUNDS

SAMPLE NUMBERMOLGW93701

3-s'/

CONCENTRATION: LOU


DATE ANALYZCO: 18/85/87

CONC/OIL FACTOR: 1.

PERCENT MOISTURE. (NOT DECANTED)

PH

CAS NURSE*


74-83-» BROMOHETHANE

75-81-* VJNYL CHLORIDE

75-88-3 CHLOROETHANE

75-89-2 HETHYLENC CHLORIDE . . .

47-44-1 ACETONE75-15-8 CARBON DISULFIOE . . . .

7S-3S-4 1.1-DICHLOROCTHENE . . .75-35-3 1-1-OICHLOROETHANE . . .

156-68-5 TRANS-1.2-OICHLOROETHENE47-44-3 CHLOROFORM

187-84-2 1.2-DICHLOROETHANC . . .78-93-3 2-BUTANONE

71-SS-A 1,1.1-TRICHLOROETHANE .56-23-5 CARBON TETRACHLORIDE . .188-85-4 VINYL ACETATE75-27-4 BROMODICHLOROHETHANE . .

Ufi

i«1114

11

1

3<

1

1

>/L

» U

• U

> U

> U

L J

>

U

U

U

U

U

U

U

U

U

» U

1 U

CAS NUMBER

7S-87-S

18861-82-*

79-81-4

124-48-1

71-88-S

71-43-218861-81-5

118-75-8

75-25-2

181-18-1

Stl-78-6

127-18-4

7f-34-S

188-88-3

188-98-7

188-41-4

188-42-5

UG/L1,2-DICHLOROPROPANE . . .

TRANS-1. 1-DICHLOROPROENE .TRICHLOROETHENEOIBROMOCHLOROftETHAME . . .

1.1,2-TRICHLOROETHANE . .

BENZENECIS-l,3-DICHLOROPROPENE .

2-CHLOROETHYLVINVLETHER .IROMOFORM

4-NETHYL-2-PENTANONE . . .

2-HEXANONETETRACMLOROETHENE . . . .

1.1,2.2-TETRACHLOROETHANE

TOLUENE

CHLOROBENZENEETHYLBENZENE

STYRENETOTAL XYLENES

1851818S185§55S

UUUUUUUUUUUUUUUUUU




REPORTING 8UALIFIERS.FORM I

30539


Case No: 4184

Sample N


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

ConcentrationHf/L

300U

200U

200U

U inîrat** compound was analyzed for but not detected. Report the minimum detection limit for the sample with the U(e.g. 10U) based on necessary concenntion/dihilioD action. (This is not necessarily the instrument detection limit)The footnote sbould read: U-Gompound was analyzed for but not detected. Tbe number is the minimum attamabledetection limit for the sample.

J itrfintr* an *~pima»H value. This flag is used either when *frim«fing a ooncentnboo for tentatively Jdeatified compoundswhere a 1:1 response is ««pi*«««< or Men the mass spectral data <ndw-a*^ (he presence of a compound that meets the identi-ffcation criteria but tbc result is tess than the specified detection limit but greater than zero (e.|. 101). If limit of detection is10 |igft. and a concentration of 3 iig/L is calculated, report as JJ.

4 1 8 4 3 0 5 9 0

alxr <•<:."

Jase No i .J



S« •••

Joncentration: fLovvj Medium

Oate Extracted'Prepared *' ^ -

Date Analyzed f.

(Circle One)

Cone/Oil Factor:


GPC Cleanup OYes QNo

Separaiory Funnel Extraction QYes

Continuous Liquid - Liquid Extraction DYes

CASNumber

ug/lorug/Kg CAS ug/lorug/Kg(Circle One) Number (Circle One

/(CV

/0*fV?i~70&10

/AM.

Atti/<%/ty/0«/tfk.//7fc)$:Wtt//7^*/?««•/&kID*Ift*IftfiIfa.10*10*-iO\A.

S~614[OlA

5tq10*ICltA

3-32-91-28-500-02-7

32-64-921-14-2

606-20-284-66-2

005-72-36-73-7

00-01-634-52-1

86-30-6

01-55-318-74-1

87-86-585-01-8

20-12-784-74-2206-44-0129-00-0J5-68791-94-1

.6-55-3117-81-7

218-01-9117-64-020599-2207X»-9»32 8

193 395

J3-70-3191-24-2

Acenaphthvne1. 4-OinKrophenol

4-Nitrophenot>iberuofu'an

!.4-Oinhrotoluene! , .6 -OinKrotoluene

Oiethyiphthalate> -Chlorophenyl-phenylether

Fluorene4-Nitroaninne4. 6-Oinitr9-2-MettTy(phenol

N-NitrocodiphenyUmine (1 )

4-BromopSenvf-phenv<ether

HeuchlorooenzentPentachlorophenolPrteramhreneAmhr»c*ne04-n-ButyIphttxalate

Fluor* nthenePyreneButvtt>«<VYV>tK«iate3. 3'-OtcMorobenzidine3eozo(i)Amtv«cen«

txX2 -Ethy1heKyl)PriTtvaliwChryseneOi-n-Octyl PttttxalateBenzo(b)Fluoranthene

Benzofk)Fiuorantt>eneBerucXatPyrene

IrxJenotV 2. 3-cd)PyeneOibcnili h)Anthracer>e

Benio(g. h. ()P«rY««r>e

IQiiSfa54 u

I/9K(hit.lf)u.(i)u(f)lt-

fOt*ft A

&<4IUlLhi*

(OutJ*f

JHulf>k

iQuf)u

'Id'1]0u.

JtutVu.jf)(jL

lUljL

\0u.(f}tfid'*']T)i*s(f?AtlUl*i n^ __

f O' m I

4 1 8 4 3 0 5 9 17/85

H e .

Concen t r a t io r : [ Lc» j Hediui i C i r r l e aD a t e Ex t . -ac te i ' f ' epare i ! : :?-Sep-B'"a te H?a ;» :ed : 0 7 - G c t - E "Canc/d i F a c t o r : 1Percen t Hc is tare lde:anted i HP

BP: Cleanup Yes [iHoSeparately Fan-el Eitract:;r. Yes[:•'.:•..c.s L iuu id -L iQu iS [ - . ; ract ;o- [x ] Yes

CAS [u5 /L ] o- ug /KcNuliier

319-B4-6 Alphi-BHC O.C5 U

319-85-7 Beti-BHC 0.05 U

319-86-8 DelU-BHC 0.05 U

58-89-9 GaiM-BHC (Lindine) 0.05 U

76-44-8 Heptachlor 0.05 U

309-00-2 ftldnn 0.05 U

1024-57-3 Heptachlor Epciide 0.05 U959-9B-B Endosulfan I . 0.05 U60-57-1 Dieldrin 0.1 U72-55-9 4.4'-OD€ 0.1 U72-20-B Endrin 0.1 U33213-65-9 Endosulfan II 0.1 U72-54-B 4,4'-DDD 0.1 U1-31-07-8 Endosulfan Sulfate 0.1 U50-29-3 4,4'-DDT 0.1 U72-43-5 Kethoxychlor 0.5 U53494-70-5 Endrin Ketone 0.1 U57-74-9 Chlordane 0.5 UB001-35-2 Toiaphene 1U12674-11-2 Arodor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U53469-21-9 Aroclor-1242 0.5 U12672-29-6 Aroclor-1248 0.5 U11097-69-1 Aroclor-i:54 1 U

11096-82-5 Aroclor-1260 1 U

Vi = Voluie of eitract in jected lullVs - Volute of viter extracted (•!)Us - Height of saiple eitricted (g)Vt - Volute of total ex t rac t lull

Vs = 1000 or Us = Vt = 10000 Vi = 3.0

Fori

4 1 8 4 3 0 5 9 2

abo ra io ry N a m e f c - T C / T u x i c o n

e No



Sample

Number Compound Nam*C(tim«t«d**&*ntr«tioo

(ug/rr ug/kg)

n

l«DiO K. 531 15

603 *5uioic

/OZT-

1C

ms/^nil- h/4? 11

la

ss

,».129.


4 1 8 4 3 0 5 9 3

' . i M - - fc E c

:•«.? 38*:


LAB SAMPLE 10 NO: 4184-1*3

SAMPLE MATRIX: WATERDATA RELEASE AUTHORIZED BY:


<PA&E 1)

CASE NO: «1B4

8C REPORT NO: 41B4

CONTRACT NO: 0/4*1DATE SAMPLE RECEIVED: »»/29/87

VOLATILE COMPOUNDS

CONCENTRATION: LOW


DATE ANALYZED: l*/«3/87

CONC/DIL FACTOR: 1.


PH

CAS NUMBER

74-87-374-83-»7S-81-47S-**-3

7S-*»-247-44-1

7S-1S-*7S-3S-4

7S-3S-3

154-49-S47-44-3

l*7-*4-278-»3-371-SS-4

S4-23-Sl*8-*S-4

78 -27-4

UC/L CAS NUMBERCHLOROMETHANE !• U 78-87-S

8ROHOMETHANE 1* U l**41-*2-4

VINYL CHLORIDE !• U 7f-«l-4CHLOROETHANE !• U 124-48-1METHYL ENE CHLORIDE . . . . 2 J 7»-**-S

ACETONE

CARBON1* U 71-43-2

DISULFIOE

1. 1-DICHLOROETHENE . . . .

1, 1-OICHLOROETHANE . . . .TRANf-1. 2-OXCHLOROETHENE .CHLOROFORM

1.2-OICHLOROETHANE . . . .

2-BUTANOME 14

U 1**41-*1-S

U ll*-7S-8U 7S-2S-2U 1*8-1*-1

U i«l-78-4

U 127-18-4

» jKl 7»-34-S1. 1, 1-TRICHLOROETHANE . . S U 1*8-88-3

CARBON TETRACHLORIDE ... S U l*8-9*-7

VINYL ACETATE 1* U 1M-41-4

BROHODICHLOROMETHAME ... i U 1M-42-S

UO/L

flifri

1,2-OICHLOROPROPANE . . .

TRANS-1, 3-OICHLOROPROENE .TRICHLOROETHENCDIBROMOCHLOROMETHANE . . .1.1.2-TRICHLOROETHANE . .

BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHCR .

BROMOFOM4-METHYL-2-PEHTANONC . . .

2-HEXANONETETRACHLOROCTHENE . . . .

1.1.2.2-TETRACHLOROETHANE

TOLUENE

CHLOROBENZENE

ETHYLBENZENE

STYREMETOTAL XVLENES

1*

U

U

U

U

U

U

U

U

U

UU

U

UU

U

U

U

U

8 - COMPOUND WAS DETECTED IN THE K BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED


SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING 8UALIFIERS.

FORM I

4 1 8 4 3 0 3 8 9


Case No: 4184

Samplf N u m b e r


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropjl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

ConcentrationILK/L

300U

200U

200U

U lnrfir-«<>^ compound was analyzed for tat not detected. Repot the minimum detection limit for the sample with die U(e.j. 10U) based on necessary concentration/dilution action. (Thisitnot necessarily the iimruinent detection limit)The footnote ibould read: U-Compound w« analyzed for but not detected. The amber U the minimum aoinibledetectioa ^mit for the sample.

j Indicates an estimated vitoe. Thk fig to uaed either when qrimariat' muxuuaioo for tenativdy identified compoundswhere a 1:1 response is assumed or when the mass Mfi U il 4f*\ iM^**^ the presence of a compound that meets the identi-ficatkn criteria bat the result is less than *e tpecifM dettctkn Umb tat greater than zoo (e . 101). If limuof detectioois10 \itfL and a concentration of 3 m/L U catailansd. report a§ U.

4 1 8 4 30390

Case f. :


Sa-MpL. •

rf.O _<:-. .

Concentration

Date Ertracted'Prepared

Date Analyzed

Conc/Dil Factor

Medium

Semivolatite Compounds

(Circle One) GPC Cleanup QYes ONo

CASNumber

i ° / t If!, ' ' 1r* (O»c^nt<»*l) .


nenol

i$<-2-Chloroethyl)£ther-Cnlorophenol. 3-Dicnlorobentene. 4-Oicnlorobenteneenzyl Alcohol, 2-Dichlorobentene-Methytphenot««(2-chlorotsopropy1|E(her•Metfiytphenol-Nitfoso-Oi-n-PropyUminelexachloroethant(itrotenzenecopnoron*-Nitrophenol. 4-Dimethylph*nolleruoic Acid•2-CMofoetnocylMetnene. 4-Oichloropnenol. 2. 4-Trichloroberuene<aphm*(«ae-Oil&roeniline

<e (Achlorobutftdienel-CMoro-3-Melhylprtenol-Memylnaphthalene

». 4. 6-TricMorophenol!. 4. 5-TricMoroprtenol!-Chloronaphthalen«!-NitroenilineJ.mcthyi Ptitnadie»ên»phtriy1«r%e

/Ok./flk.10 uIn^lOu)Ck./ni~If)*.IfiuIQUL

lOulOu1C*.I HitID*.

527Uinu,10*10*ID*Ifiiflf)H.lOu./Ul/~\ur-/On.

$i(AIfilA

50t\10*IfilA


CAS ug/lorug/KgNumber (Crcle One3-32-91-28-500-02 -732-64-921-14-2

606-20-284-66-27005-72-386-73-700-01-6

534-52-186-30-601-55-318-74-1

87-86-515-01 -8120-12-7M-74-2206-44-0129-00-0)5-687J1-94-1.6-55-3117-81-7218-01-9117-84-0205-99-2207-08-9>032-8193 39553-70-3191-24-2

Acenaphtftene2. 4-Dinrtroprienol4-NrtropNenol>ibenzo(uran

:. 4.0inrtroto(uene2. 6-OinhrotoloeneDiethylphthalftte

Fluor ene4-NrtroaniliM4. 6-Otohro-2-Wethv<pn«nolN-Nitrosodipneny(amine (1)4-Bromophenyf-phenvtetrterHeuchlorobenzertePentMhlorophenolPhenanthrentAnthnoeneOi-n-6utv<prithalateFluomnthenePyreneBut/ft* ruy(pritn«t«t«3. 3'-O<hioroberu«dineBeoiota lAnthracenetx*2 -Ethy<t>eKy<)PhttulateOvYieneDi-n-OctyH PhtnalateBemo(b|Fluor*nthene8«fUo(k|Fluorantt>ene8enzo(a)PvTeneIndenotV 2. 3-cdWerKOibeoflj. h)Anthr«cen«Bento(g. h. iJPeryleo*

I0uS"dt<Wu

in*(Huin*IUUL(f)t?.

(0(fUK

senjUuto*(flu.

SHifOn(fiu

10"fhu[Q\L

Wuyu

to*./n^'if (fi-lp*lOif-ffjf^/(/i*-în*.

In* ..

rxji be tep«r«i«d ff

( o< 4 1 8 4 3 0 3 9 17 85

L d Z Z r a ' 7 ' t

Cdse N-:inc.

analysis Cat* Sheet(Page 3)Peshcides/PCBs

Concentration: [Lo»] tediut (Circle one)Date E«tracteJ/?repa'BS: 29-5ep-B7Date Anal.red: 07-Dct-S7Conc'Dil Factor: 1Percent rlcusture'decanted! HR

6PC Cleanup Yes [.HoSeparatory Funnel Extraction YesContinuous Liquid-Liquid Extraction [i] Yes

CAS [ug/L] or ug/KgNufber

319-B4-4 Alphi-BHC 0.05 U319-85-7 Beti-BHC 0.05 U319-B6-B D*Hi-BHC 0.05 U5B-B9-9 Sa»ia-BHC (Lmdane) 0.05 U74-44-B Heptachlor 0.05 U309-00-2 Aldnn 0.05 U1024-57-3 Htptachlor Epoiide . 0.05 U959-98-6 Endosulfan 1 0.05 U40-57-1 Dieldrin 0.1 U72-55-9 4,4'-OM 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfw II 0.1 U72-54-B 4,4'-BDD 0.1 U1-31-07-B Endosulfan Sulfite 0.1 U50-29-3 4,4'-ODT 0.1 U72-43-5 Htthoxychlor 0.5 U53494-70-5 Endrin Ketone 0.1 U57-74-9 CMord»n« 0.5 U8001-35-2 Toiapheni IU12674-11-2 Aroclor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U53469-21-9 Aroclor-1242 0.5 U12672-29-6 ftroclor-1248 0.5 U11097-69-1 Arodor-1254 1 U11096-82-5 Aroclor-1260 IU

Vi = Volute of titract injected (ul)Vs * Volute of water eitracted (•!)Us - Height of saiple extracted (9)Vt -- Volute of total eitract (ul)

Vs = 1000 or Us ; Vt - 10000 Vi - 3.0

Fort I

4 1 8 4 3 0 3 9 2

_abo'aiofy Name

e No .

LTC/To.\ i c



Sample Ncxnl>er

CASCompound NMTM Fraction

[ug/rer ug/kg)

1..

3..

6..

7..

1O..

.*..

37

16..

16..

17..

16..

19..

21..

as

29.

JO.

NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmv denotes probable molecular weight

4 1 8 4 3 0 3 9 3

LABORATORY NAME: CTC/TOXICON

LAI SAMPLE ID NO: 4184-111SAMPLE MATRIX: WATER

CATA RELEASE AUTHORIZED IV

OftCANICS ANALYSIS OATA SHEET(PACE 1)

CASE NO. 4184BC REPORT NO: 4184

CONTRACT NO: 0) C\DATE SAMPLE RECEIVED

VOLATILE COMPOUNDS

99/29/87

CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYZED: 14/49/87CONC/DIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)

PH

CAS NUtltER

74-87-1 CHLOROMCTHAMC

74-81-9 BROHOHETHANE

7S-81-4 VINYL CHLORIDE


75-89-2 METHYLENE CHLORIDE . . .

47-44-1 ACETONE

75-15-8 CARBON OISULFIOE . . . .

75-35-4 1.1-OICHLOROETHENE . . .

75-35-3 1,1-DICHLOROETHAMC . . .154-48-5 TRAN5-1.2-OICHLOROETHENC47-44-3 CHLOROFORM

187-84-2 1.2-OICHLOROETHANC . . .7t-93-3 2-iUTANOHt71-SI-4 1.1.1-TRICMLOROETHANE .

54-23-5 CARBON TETRACHLORIOC . .188-85-4 VINYL ACETATE

75-27-4 BROMODICHLOROHETHANC . .

»/LUUUUUUUUUUUUUUUUU

CAS NUMBER78-87-B1884 1-82-4

79-81-4124-48-1

79-88-571-43-218841-81-5118-75-8

75-25-2188-18-1

591-78-4127-18-4

79-34-5188-88-3188-98-7188-41-4

188-42-5

UO/L1.2-DICHLOROPROPANC . . .TRANS-1.3-OICNLOROPROENE .TRICHLOROETHENEDIIROMOCHLOROHETHANC . . .

1.1,2-TRICHLOROETHANE . .BENZENECIS-1.3-OICHLOROPROPENE .

2-CHLOROETHYLVINYLETHER .BROMOFORH4-METHYL-2-PENTANONC . . .

2-HEXANONE


1.1.2,2-TETRACHLOROETHANETOLUENECHLOROBENZENE

ETHYLBENZENESTYRENE

TOTAL XYLENES

1*

UUUUUUUUUUUUUUUUUU




FORM I

4 1 8 4 305 62

laboratory Name: ETC/Toxicon

Tase No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropjl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

ConcentrationRt/L

300U

200U

200U

U Indicate pntnpnnnj w^ •tmljmM fnr Hit TV* AetrftrA Pepnrt thg minimnin (toegtjnn limit for the tample wilh the U(e,j. 10U) bond on necessary concamdoa/dHutioo actioa. (This U not necessarily the instrument detection limit)The footnote should read: U-Compoond was analyzed for but not detected. The number is the minimum attainabledetection i>mit for the sample.Tndir^»t «n ,-aim,*** valiy. Thq fl«g lt njrj fitter mAtm f^jntiri^ • mnrrntntvm fnr tentatively MenrififtH enmpninxl*

where • 1:1 response U assumed or when the mass spectral data indicated me presence of a compound that meets the identi-fcattan criteria but the result is less than the specified detection limit but greater than zero (e . 10J). Iflimitofdetectioais10 \i%L and a coocentration of 3 U£/L is calculated, report as 3J.

4 1 8 4 3 0 5 6 3

LABORATORY NAME ETC/TOXICOH

CASE NO *18»NUMBER

ORGANIC* ANALYSIS DATA SHEET

<PAGE 2>

SEHIVOLATILE COMPOUNDS

CONCENTRATION: LOUDATE EXTRACTED/PREPARED: lt/17/87

DATE ANALYZED: lt/28/B7CONC/DIL FACTOR: 1.PERCENT hOISTURE: (DECANTED)

GPC CLEANUP YES X NO

SEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LiaUID-LiaUID EXTRACTION YES

CAS NUMBERltB-»*-2 PHENOL111-44-4 BIS<2-CHLOROETHYL>ETHER .tS-§7-8 2-CHLOROPHENOL5*1-73-1 1,3-OICHLOROBENZENE . . .

186-46-7 1.4-OICHLOROBENZENC . . .

ltt-Sl-6 BENZYL ALCOHOL»S-St-l 1.2-OXCHLOROBENZENE . . .

95-48-7 2-HETHYLPHENOL39638-32-9 BI*<2-CHLOROISOPROPYL>ETHER

lt6-44-S 4-HETHYLPHEMOL621-64-7 W-NITROSO-D1-H-PROPYLAHINE47-72-1 HEXACHLOROETMAME98-TS-J MITROBEMZCME

78-S9-1 ISOPHORONC88-75-1 2-NITROPHCNOLltS-67-9 2.4-OIHETHYLPHENOL ....

65-8S-t iENZOIC ACID111-91-1 BIS<2-CHLOROETHOXY>HETHAMt

12t-B3-2 2.4-DICHLOROPHENOL . . . .

128-82-1 1.2. 4-TRICHLORO»EHZE*e . .91-2t-l NAPHTHALENEl«A-47-t 4-CHLOROANILINE

87-68-3 HEXACHLOROIUTAOIEHE . . .S»-S»-7 4-CHLORO-3-NETMYLPHENOL .

11-S7-6 2-METHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTAOIENE88-«6-2 2.4.A-TRICHLOROPHENOL .' .

»S-»S-4 2,4.S-TRICHUOROFHENOL . .

f1-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROAMILINE

131-11-3 OIHETHVU PHTHALATE . . . .

288-96-8 ACENAPHTHVLENC»*-«»-2 J-NITROANILINE

UG/L CAS NUMBER UG/L

it U 83-32-9 ACENAPHTHENE It U

it U 51-28-5 2.4-DINITROPHENOL . . . . St Uit U ltt-t2-7 4-NITROPHENOL St UIt U 132-64-9 OIBENZOFURAM It U

It U 121-14-2 2.4-OINITROTOLUENE . . . . It UIt U 6t6-2t-2 2.6-OINITROTOLUENE . . . . It U

it U 84-66-2 OIETHYLPHTHALATE It Uit U 7ttS-72-3 4-CHLOROPHENYL-PHENYLETHER It UIt U 86-73-7 FLUORENE It Uit U ltt-it-6 4-NITROANILINE 5t U

it U 534-52-1 4.6-DIN1TRO-2-NETHYLPHENOL St Uit U 86-3t-6 N-NITROSOOIPHCNYLAHINE <1> It Uit U ltl-SS-3 4-BROHOPHENYL-PHENYi.ETHER it U

it U 118-74-1 HEXACHLOROBENZENE . . . . It Uit U 87-86-5 PENTACHLOROPHENOL . . . . St U

it U 8S-tl-8 PHENANTHREME It USt U 12t-12-7 ANTHRACENE it Uit U 84-74-2 OI-N-BUTYLPHTHALATE ... It U

it U 2t6-44-t FLUORANTHCNC it UIt U 129-tt-t PYRENE It Uit U 8S-68-7 8UTYLBENZYLPHTHALATE ... It Uit U 91-94-1 3.3'-OICHLOROtENZIOINE . . 2t U

It U 56-55-3 BENZO(A)ANTHRACENE . . . . It Uit U 117-81-7 BIS(2-ETHYLHEXYL>PHTHALATE It UIt U 21B-tl-9 CHRYSENE It UIt U 117-8»-t OI-N-OCTYL PHTHALATE . . It UIt U 2tS~99-2 BENZO(B)FLUCRANTHENE . . It USt U 2t7-t8-9 BENZO<K>FLUORANTHENE ... It Uit U St-32-8 8ENZO(A)PYRENE It U

St U 193-39-5 INOENOd. 2. 3-CO) PYRENE . It Uit U S3-7t-3 OIBENZ(A,H)ANTHRACENE . . It U

It U 191-24-2 BENZO<O.H. DPERYLENE ... It U

St U

<1> - CANNOT BE SEPARATED FROM DIPHENYLAHINEFORM I

30564

3)PpsticidM/PCBs

[1.3*] Sediut (Circle one! 6PC Cleanup Y« [*]-No

''Prepared: T'-Sep-E? Separa'.ory Fjrre! Extraction IPS

•'J-t'E' Cr'ii.-jDus L;5t;d-Liquj(! Ext'ac'.ior [s] >'es

•: 1•e!i?:art;j) Nfi

CAS [ag/L] or uoHuiber

319-84-4 Alpha-BHC 0.05 U

319-85-7 B*tj-BHC 0.05 U

319-Bi-B Dflta-BHC 0.05 U

58-89-9 Sana-BHC (Lindant) 0.05 U

74-M-B Htptachlor 0.05 U

309-00-2 Aldrin 0.05 U

1024-57-3 HepticMor Epo«ide 0.05 U959-9B-B Endosulfan I 0.05 U40-57-1 Oitldrin 0.1 U

72-55-9 M'-DDE «.l U72-20-8 Endrin 0.1 U

33213-45-9 Endosulfifl H 0.1 U72-54-8 4,4'-ODD 0.1 U1-31-07-8 Endosulfin Sulfitt 0.1 U50-29-3 4,4'-DDT 0.1 U72-43-5 Bethoiychlor 0.5 U

53494-70-5 Endrin Kftmc 0.1 U57-74-9 Chlordan* 0.5 UB001-35-2 Toxaphmt 1U12474-11-2 Aroclor-1014 0.51)

11104-28-2 Aroclor-1221 0.5 U11141-14-5 Aroclor-1232 0.5 U53469-21-9 Aroctor-1242 0.5 U

12672-29-4 Aroclor-1248 0.5 U11C97-49-1 ftroclor-1254 1 U

r-S Aroclor-1240 1U

Vi : Vcluie of ritrict in;rcteil lul)Vs = Voluii of Mter tttricttd (•!)Ms - Nrjght of saipl? eitractfd (9)Vt ^ Volute of total extract (ul)

Vs - 1000 or Us = Vt - 10000 Vi - 3.0

Fori I

4 1 8 4 3 0 5 6 S

Laboraio.y

eNo


Simple Number


CAS

1

3

s

7

aft

10

._,19

,4

IS

1C

17

1*19

21

27.

23

28

„

28

24

in

Compound N«rTM

Wd^

^J^fS

•

Fraction

ttft

fX^ft

B^g

Estimated

(ug/tW ug/kg)v /

• -«...,

NFA denotes no fraction analyzedNCF denotes no compound foundlink denotes unknownmw denotes probable molecular weight

4 1 8 4 3 0 5 6 6

LABORATORY NAME: CTC/TOXICON

LAB SAMPLE 10 NO: 4184-93SAMPLE MATRIX: WATER

DATA RELEASE AUTHORIZED •Y:|c/4


CASE NO:•C REPORT NO:CONTRACT NO:DATE SAMPLE RECEIVED: 89/29/87

. - / * / /

• / jj

41B44164

VOLATILE COMPOUNDS

CONCENTRATION: LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: l«/*3/B7CONC/OIL FACTOR: 1.PERCENT MOISTURE: KNOT DECANTED)

CAS NUMBER74-87-374-83-975-81-475-88-375-89-247-44-175-15-875-35-475-35-3154-48-S47-44-3187-84-278-93-371-55-454-23-5188-85-475-27-4

CHLOROMETHANCBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDE . . . .ACETONECARBON OISULFIDE1,1-DICHLOROETHENE . . . .1, 1-DICHLOROETHANE . . . .TRANS-1. 2-DICHLOROETHENE .CHLOROFORM1,2-OICHLOROETHANE . . . .2-BUTANONE1, 1, 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEBROMOOICHLOROMETHANE . . .

UG/L18 U18 U18 U18 US U18 U

1

UUUUUU<tuuu

18 US U

CAS NUMBER78-87-518841-82-479-81-4124-48-179-88-S71-43-218841-81-5118-75-875-2S-2188-18-1S91-78-4127-lt-*79-34-S

188-88-3188-98-7188-41-4188-42-5

UG/L1.2-OICHLOROPROPANE . . .TRANS-1. 3-DICHLOROPROENE .TRICHLOROETHENEDIBROMOCHLOROMETHANE . . .1. 1,2-TRICHLOROETHANE . .BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORH4-HETHYL-2-PENTANONE . . .2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES

UUUUUUUUUUUUUUUUUU

B - COMPOUND WAS DETECTED IN THE «C BLANK.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED



FORM I

4 1 8 4 3 0 1 6 9


Case No: 4184

Sample Numb«r


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

ConcentrationM/L

300U

200U

200U

indicates compound was analyzed for but not detpctgL Report the minimum detection limit for me sample with me U(e.j. 10U) y*1 on necessary concentration/dilution action. (Tnis is oot necessarily me instrument detection limit)The footnote should read; U-Compouad was analyzed for but not detected. The number U me minimum attainabledetection limit for the sample.Indicates an estimated vtlue. This flag Is used either when estimating * ccwxttration for lentativtly klentified compoond*where a 1:1 response it assnmed or when the mass tpectnl data inrliratcd me presence of a compound mat meets tfaeidenti-fkatioo criteria but the result is less dun me spedfied detection limit bat greater man zero (e . 101). If limit of detection ii10 ng/L and a coocentratioa of 3 u^/L is calculated, report as 3J.

4 1 8 4 30170

LABORATORY NAME

CASE NO

ETC /TOXICON4184


(PAGE 2)


CONCENTRATION: LOWDATE EXTRACTED/PREPARED: 99/39/97DATE ANALYZED: 18/85/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (DECANTED)

GPC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIQUIO-LiaUIO EXTRACTION YES

CAS NUMBER188-95-2 PHENOL111-44-4 i!S<2-CHLOROETHYL>ETHER .95-57-8 2-CHLOROPHENOLS41-7J-1 1.3-DICHLOROBENZENC . . .184-44-7 1,4-OICHLOROBENZENE . . .188-S1-4 •CMZVL ALCOHOL9S-S8-1 1.2-OICHLOROBENZENE . . .95-48-7 2-HETHYLPHENOL39438-32-9 BIS<2-CHLOROISOPROPYL>ETHER184-44-5 4-HETHYLPHENOL421-44-7 N-NITROSO-OX-N-PROPYLAHINE47-72-1 HCXACHLOROETHANC98-9i-3 NITROtENZENC7i-§t-l ISOPHORONC•S-7S-S 2-NITROPHENOL185-47-9 2, 4-0IMETHYLPHENOL . . . .45-85-8 iENZOIC ACID111-91-1 •IS<2-CHLOROETHOXY)HETHANC12«-83-2 2.4-OICHLOROPHENOL . . . .128-82-1 1.2.4-TRXCHLOROBENZENE . .91-28-3 NAPHTHALENE1*4-47-1 4-CHLOROANILINE87-48-3 HEXACHLOROBUTADIENE . . .S9-S8-7 4-CHLORO-3-HETHYLPHENOL .91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTAOIENE88-84-2 2,4.4-TRICHLOROPHENOL . .9S-9S-4 2,4,5-TRICHLOROPHENOL . .11-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROANILINE131-11-3 OIHETHYL PHTHALATE . . . .288-94-8 ACENAPHTHYLEME99-89-2 3-NITROAMILIME

U6/L1*191919191918181818181818181818S8181818181818181818185818S81818• 8

UUUUUUUUUUUUUUUUUUUUUUUUUUU

UU

UUUU

CAS NUMBER83-32-9S1-2B-S188-82-71 32-44- V121-14-2484-28-284-44-27885-72-384-73-7188-18-4S34-S2-184-38-4181-55-3118-74-187-84-S85-81-8128-12-784-74-2284-44-8127-88-885-48-791-94-154-55-3117-81-7218-81-9117-84-82*5-99-22*7-«<e-958-32-8193-39-553-78-3191-24-2

UG/L

ACENAPHTHENE 18 U2.4-DINITROPHENOL . . . . 58 U4-NITROPHENOL 58 UDIBENZOFURAN 18 U2.4-OINITROTOLUENE . . . . 18 U2.4-DXNITROTOLUENE . . . . 18 UDIETHYLPHTHALATE 18 U4-CHLOROPHENYL-PHENYLETHER 18 UFLUORENE 18 U4-NITROANILINE 58 U4.4-DINITRO-2-HETHYLPHENOL 58 UN-NITROSOOIPHENYLAHINE (!) 18 U4-BROHOPHENYL-PHENYLETKEM 18 UHEXACHLOROBENZEME . . . . 18 UPENTACHLOROPHENOL . . . . 58 UPHENANTHRENE 18 UANTHRACENE 18 UDX-N-BUTYLPHTHALATE ... 18 UFLUORANTHENE 18 UPYRENE 18 UBUTYLBENZYLPHTHALATE ... 18 U3.3'-OICHLOROBENZIOINE . . 28 UBENZO<A)ANTHRACENE . . . . 18 UBIS<2-ETHYLHEXYL>PHTHALATE 18 UCHRYSENE 18 UOI-N-OCTYL PHTHALATE ... 18 UBENZO(t>FLUORANTHENE ... 18 UBENZO<K)FLUORANTHENE ... 18 UBENZO(A>PYRENE 18 UINOENO<1,2.3-CD)PYRENE . . 18 UOIIENZ(A,H)ANTHRACENE . . 18 UIENZCXO. H, DPERYLENE ... 18 U

(i) - CANNOT BE SEPARATED FROM OIPHENYLAHINEFORH I

4 1 8 4 30171

N::

Organic* Analysis Data Sheet(Pige 3)Peshcides/PCBs

[arcentritio": [Lo»] Sediui (CKcle one)Site E'tractei.'Prepared: 29-Sep-B7Date Analyred: 06-Oct-87Conc/Di! Factor: 1Percent Ncisture(decanted) MR

6FC Clejr.us Yes [«]-NoSeparjlcTy Funnel Extrjction YesContinuous Liquid-Liquid Eitractian [x] Yes

CASNutber

[ug/U or ug/Kg

31T-84-4 Alphi-BHC ........................ 0.05 U319-85-7 Beti-BHC ........................ 0.05 U319-B6-B Delt*-BHC ........................ 0.05 U58-89-9 SaiM-BHC (Lindine) ............. 0.05 U76-44-8 HepUchlor ...................... 0.05 U309-00-2 Aldrin .......................... 0.05 U1024-57-3 Heptichlor Epo>id« ............... 0.05 U959-98-fl Endosulfin I .................... 0.05 U60-57-1 Dieldrin ........................ 0.1 U72-55-9 4,4'-OK ........................ 0.1 U72-20-8 Endrin ........................ 0.1 U33213-65-9 Endosulfin II ................... 0.1 U72-54-B 4,4'-DDD ........................ 0.1 U1-31-07-8 Endosulf»n SulUte ............... 0.1 U50-29-3 4,4 -DOT ........................ 0.1 U72-43-5 BethoiycMor .................... 0.5 U53494-70-5 Endrin Ketont ................... 0.1 U57-74-9 Chlordint ....................... 0.5 U8001-35-2 Tosiphene . . . . . . . . . . . . . . . . . . . . . . . I D12674-11-2 Arodor-1016 .................... 0.5 U11104-28-2 Aroclor-1221 .................... 0.5 U11141-16-5 Arodor-1232 .................... 0.5 U?TSfc9-2l-9 Aroclor-1242 . . . . . . . . . . . . . . . . . . . . 0 .5112t72-29-6 R r c c l o r - 1 2 4 B .................... 0.5 U11097-69-1 Aroclor-1254 . . . . . . . . . . . . . . . . . . . . 1 U11096-82-5 Aroclor-1260 . . . . . . . . . . . . . . . . . . . . 1U

Vs -

Vi = Volu»e of eitrict injected |ul)Vs -- Volute of »Jter eitrtcted (il)Ms - Height of s»ple eitrtcted |g)Vt - Volute o1 total extract (ul)

1000 or Us - Vt -

Fon I

10000 Vi • 3.0

4 1 8 4 3 0 1 7 2

Labofaio.y Name


Sample


CASNumber Compouod N««n« Numbw

Etlirnat*dtration

ug/or ug/kg)

1C

5.

7.

^_ 5*1 /o

|16.

6.

I 2O.

ST.

to


4 1 8 4 3 0 1 7 5

LABORATORY NAME:

LAB SAMPLE 10 NO:SAMPLE MATRIX:

ETC/TOXICON

4184-94

WATER

ORGANICS ANALYSIS DATA SHEETIfAGE 1>

/ -


CASE NO: 4184

ac REPORT NO: 41B4

CONTRACT NO: C(4^


VOLATILE COMPOUNDS

CONCENTRATION: LOW


DATE ANALYZED: 18/83/87

CONC/OIL FACTOR: 1.

PERCENT MOISTURE: <NOT DECANTED)

PH

CAS NUMBER

74-87-3 CHLOROMETHANE74-83-9 BROMOHCTHANE

75-81-4 VINYL CHLORIDE75-88-3 CHLOROETHANE75-89-2 HETHYLENC CHLORIDE . . .

67-64-1 ACETONE75-15-8 CARBON DISULFIDE . . . .7S-3S-4 1, 1-DICHLOROETHEME . . .

7S-3S-3 1,1-OICHLOROETHANE . . .

1S6-68-S TRANS-1.2-OICHLOROETHENE67-44-3 CHLOROFORM

187-84-2 1.2-DICHLOROETHANE . . .71-93-3 2-BUTANONE71-SS-4 1.1,1-TRICHLOROETHANC .

54-23-5 CARBON TETRACHLOMIDE . .188-85-4 VINYL ACETATE

75-27-4 BROHOOICHLOROHETHANC . .

uc/18

18

18

18

f

41

18

5

5

18|

L

U

U

U

U

U

U

U

U

U

U

U

B\J

U

U

U

U

eft

CAS NUMBER

78-87-5

18861-82-4

79-81-4

124-48-1

79-88-5

71-43-2

18861-41-*

118-75-8

7S-2S-2

188-18-1

591-78-4

127-18-4

79-34-5

188-88-3

188-98-7

188-41-4

188-42-i

b1

1.2-OICHLOROPROPANE . . .

TRANS-1.3-DZCHLOROPROENE

TRICHLOROETHENEOIBROMOCHLOROHETHANE . . .

1.1.2-TRICHLOROETHANE . .BENZENECXS-1, 3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .•ROMOFORM

4-METHYL-2-PENTANONE . . .

2-HEXANONE


1. 1.2. 2-TETRACHLOROETHANE

TOLUENE

CHLOROBENZENE

ETHYLBCNZENE

STYRENETOTAL XYLENE4

UO/LSs5555518518

18

518

UUUUUUUUUUU

UUUUUUU

B - COMPOUND WAS DETECTED IN THE 8C BLANK.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED


SEE PACE 1A FOR COMPLETE DEFINITIONS OF THE DATA

REPORTING 8UAHFIERS.

FORM I

4 1 8 4 3 0 1 8 4

a b o r a t o r y Name: ETOToxicon

ase No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butjl Alcohol

sec-Butyl Alcohol

ConcentrationHf/L

300U

200U

200U

U Itviiratff compound was analyzed for but not detected. Report me mfaimntti detection i™** for the t*r*f with the U(e.g. 10U) based on necessary concentration/dilution action. (This is not necessarily the instrument detection limit)The footnote should read: U-Compound was analysed for bat not detected. The number is the minimum attainabledetection limit for the sample.

j Tndif^t^t m i>etim«t«< vame. This flag is used either when »y<m«tint a concentration for tencttivety identified compoundswhere a 1:1 response is «««imH or when me m»*i medial data <m*i^«t««i the presence of a compound that meets the identi-fcarioa criteria but the result is less man the tpedfleddelectkmu^nit bat greater than zero (e . 10J). Iflimitofdetoctioais10 \ig/L and a concentration of 3 )ig/L is c?ir"latH. report as U.

4 1 8 4 3 0 1 8 5

LA90BA*:R* NAME

CASE NO

ETC / TOXIC ON

4184

ORGANIC* ANALYSIS DATA SHEET(PACE 2)

/a-


CONCENTRATION: LOWDATE EXTRACTED/PREPARED: *9/3*/87DATE ANALYZED: l*/*5/87

CONC/OIL FACTOR: t.PERCENT MOISTURE: (DECANTED)

GPC CLEANUP VES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIBUlO-LiaUID EXTRACTION YES

CAS NUHIER1*8-95-2 PHENOL111-44-4 iIS<2-CHLOROETHYL>ETHER .9S-S7-B 2-CHLOROPHENOL541-73-1 I.3-DXCHLOROBENZENE . . .1*4-44-7 1,4-OXCHLORQBENZENE . . .l**-Sl-4 BENZYL ALCOHOL9S-S8-1 1.2-OICHLOROBENZENE . . .95-48-7 2-HETHYLPHENOL39438-32-9 BX5(2-CHLOROXSOPROPYL>ETHER184-44-5 4-HETHYLPHENOL621-44-7 N-NXTROSO-DX-N-PROPYLAHXNE47-72-1 HEXACHLOROCTHANC98-95-3 NITROBENZENE78-59-1 ISOPHORONE••-75-5 2-NITROPHENOL185-47-f 2,4-DIhETHYLPHENOL . . . .65-BS-8 BENZOIC ACID111-91-1 BI§<2-CHLOROETHOXY>METHANE128-83-2 2.4-OICHLOROPHENOC . . . .128-82-1 1,2.4-TRICHLOROBENZENE . .91-28-3 NAPHTHALENE1*4-47-8 4-CHLOROANILINE87-68-3 HEXACHLOR08UTAOIENC . . .S9-5*-7 4-CHLORO-3-PIETHYLPHENOL .91-S7-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE8B-«*-2 2.4,6-TRICHLOROPHENOL . .95-95-4 2. 4,5-TRICHLOROPHENOL . .91-S8-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROANXLINE131-11-3 DIMETHYL FHTHALATE . . . .2*8-96-8 ACCNAPHTHYLEMC99-*9-2 3-NITROANILINE

UG/L1*1*1*1*1*1*181*1*1*181*

1*1*1*1*5*1*18!•!•1818181*181*5*

185*18185*

U

UUUU4iHUUUU

UUUUUUUU

UUUUUUUUU

U

UUUUU

CAS NUMBER83-32-9Sl-28-5188-82-71 32-64- V

01*121-14-2WK-28-2•4-66-27885-72-3•6-73-7188-18-6S34-S2-184-38-61*1-55-3ll«-7»-l•7-86-585-* 1-8128-12-784-74-2286-44-8129-88-885-68-7•l-?4-l56-55-3117-81-721B-*l-9117-84-82*5-99-22*7-*8-9S*-32-8193-39-553-7*-3191-24-2

UC/LACENAPHTHENE 1* U2.4-OINITROPHENOL . . . . 58 U4-NITROPHENOC 5* UOIBENZOFURAN 1* U2.4-OINITROTOLUENE . . . . 1* U2.4-OINXTROTOLUCNE . . . . 1* UOIETHYLPHTHALATE 18 U4-CHLOROPHENYL-PHENYLETHER 18 UFLUORENE 18 U4-NXTROANXLINC 58 U4.6-OXN1TRO-2-HETKYLPHENOL 58 UN-NITROSOOIPHENYLAHINE <1) 18 U4-SROMOPHENYL-PHENYLETHER 18 UHEXACHLOKOBENZENE . . . . 18 UPENTACHLOROPHENOL . . . . 58 UPHENANTHRENC 18 UANTHRACENE 18 UOI-N-tUTYLPHTHALATE ... 18 UFLUORANTHENE 18 UPYRENC 18 UBUTVLBENZYLPHTHALATE ... 18 U3.3'-OICHLOROBENZIOINE . . 28 UBENZO<A>ANTHRACENE . . . . 18 UBXS(2-ETHYLHEXYL)PHTHALATE 18 UCHRYSENE 1* UOI-N-OCTYL PHTHALATE ... 18 UBENZO<B>FLUORANTHENE . . 18 UBCNZOOOFLUORANTHENE . . . 1 8 UBENZO(A)PYRENE 18 UINDENO<1.2. 3-CD)PYRENE . . 18 UDIBENZ(A.H)ANTHRACENE . . 18 UBENZO(G.N. DPERYLENE ... 18 U

(1) - CANNOT BE SEPARATED FROM OIPHENYLAHINEFORM X

4 1 8 4 3 0 1 8 6

. 3 . - a .

fipjiysis Pa

iPage 7)Pesticides/Fx&s

DateDate Analyred: Oi-Dct-B"Conc/Dil Factor:Percent Hoistjreldecar.tei)

r'-5ep-«7

NR

af; CleanLC Yes [»]-MoSffji-itcry Fuin?, EifiCtJO" YfSContinuous Liquid-Liquid Eitriction [x] Yes

CftS tug'L] ar uq/KqNuiber

319-84-b ftlphi-BHC 0.05031S-85-7 Btta-BHC 0.05 U319-86-8 Delti-BHC 0.05 U5B-B9-9 Bauj-BHC (Lindane) 0.05 U76-44-8 Heptachlor 0.05 U309-00-: Aldrin 0.05 U10?4-57-3 Heptichlor Epoxide 0.05 U959-98-8 Endosullan I 0.05 U60-57-1 Oieldrin 0. U72-55-9 4,4'-OOE 0. U72-20-8 Endrin 0. U33213-65-9 Endosulfan II 0. U72-54-8 4,4'-DDO 0. U1-31-07-8 Endosulfan Sulfate 0. U50-29-3 4,4'-DDT 0.1 U72-43-5 Bethoxychlor 0.5 U53494-70-5 Endrin Ketone 0.1 U

57-74-9 CMordane 0.5 U8001-35-2 Toiaphtni 1U12674-11-2 Rroclor-1016 0.5 U11104-2B-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U5:«69-2l-9 Aroclor-1242 0.5 U:267:-:9-t Aroclor-1248 C.5 U11097-69-1 Aroclor-1254 1 U11096-B2-5 Aroclor-1260 1U

vs :

Vi = VoluK of extract injected lullVs * Voluie of Mater extracted (il)Ms - Height of saiple eitricted Ig)Vt ; Voluie of total extract l u l l

1000 or Vt --

Fort I

10000 Vi - 3.0

41 84 3 0 1 8 7

I ».. .r - > r,

Co'^c No _.

Orvjanics Analysis Data Sheet(Page 4)


CASNumber Compound Nwn« Fraction

Ectim«t«dgac«fitrction

(ug/tfor ug/Vg)

~Tiri (6

3.

*•

6.

I..

>..

11.. II8

. frf-7 (138

//nt Ib16.. lit

5t)1353

/intI..

I..

6..

27..

9..

30..

NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecuJar weight

4 1 8 4 3 0 1 8 8

LABORATORY NAME

LAB SAMPLE 10 NO:SAMPLE MATRIX:

ETC/TOXICOH4184-1*6WATER

DATA RELEASE AUTHORIZED

41844184

ORGAN1CS ANALYSIS DATA SHEET(PAGE 1)

CASE NO.flC REPORT NO.CONTRACT NO:DATE SAMPLE RECEIVED:

VOLATILE COMPOUNDS

•9/29/B7

CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYSED: l»/»3/B7CONC/DIL FACTOR. 1.PERCENT MOISTURE: <NOT DECANTED)

PH

CAS NUMBER74-17-1 CHLOROMETHANE74-BJ-* •ROMOnETHANC7J-81-4 VINYL CHLORIDE75-M-3 CHLOROETHANE7S-«l-2 METHYLENE CHLORIDE . . .47-44-1 ACETONE7S-is-« CARBON DISULFIOE . . . .7S-3S-* 1.1-OICHLOROETHENE . . .7S-3S-3 1.1-01CHLOROETHANE . . .134-48-S TRANS-1,2-OICHLOROETHENE47-44-J CHLOROFORMl«7-«4-2 1,2-DICHLOROETHANE . . .78-13-1 2-iUTANONE71-SS-4 1.1.1-TRICHLOROETHANE .S4-23-S CARBON TETRACHLORIDC . .l«8-tS-4 VINYL ACETATE75-27-4 BROM001CHLOROMETHANE . .

UO/L CAS NUMBER181*!•!•2!•SSi11SI19SS18i

U 78-87-SU l**41-«2-4U 7f-»l-*U 124-48-1J 7f-0-SU 71-43-2U 1041-V1-SU ll«-7S-8

U 7S-2»-2IM-lt-l

U S»l-78-4U 127-18-4J&1 7T-34-1U !••-••- 1U l»8-f«-7U 1M-41-4U l**-42-S

"Ail*

UG/L1.2-DICHLOROPROPANE . . .

TRANS-1. 3-OICHLOROPROENE .TRICHLOROETHENEOUROMOCHLOROMETHANE . . .1. 1. 2-TRICHLOROETHANE . .•ENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORH

4-METHYL-2-PENTANONE . - .2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES

UUUUUUUUUUUUUUUUUU

I - COMPOUND WAS DETECTED IN THE «C BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED



FORM I

4 1 8 4 3 0 4 4 7


"ase No: 4184

Sample N u m b e r


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

ConcentrationHt/L

300U

200U

200U

U Indicates compound was analyzed for but not detected. Report me minimum detection limit for the sample with the U(e.g. 10U) based on necessary cooceatntioQ/dilutioo action. (This U cot necessarily the instrument detection limit)The footnote shook! read: U~Compound was analyzed for but not detected. The number is the minimum attainabledetection limit for the sample.

an »ttim«t«d vitnf Thfr flag U iM«d atha- «h«i i»«fini«riin i cnnceaftarioB for lentafivriy MamTied compound!where a 1:1 response is assumed or wtiea me mass spectral data indicated the presence of a compound mat meets me identi-fication criteria but the result is less than me specified detection limit but greater manxero(e^. 10J). If limit of detection is10 vffL and a concentiation of 3 u</L is calculated, report as 3J.

4 1 8 4 3 0 4 4 8

LABORATORY NAME

CASE NO

ETC/TOXICON

4184

ORGANICS ANALVS1S DATA SHEET<PAGE 2)


CONCENTRATION: LOW

DATE EXTRACTED/PREPARED: 89/38/B7DATE ANALYZED: 18/84/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (DECANTED)

GPC CLEANUP VES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIQUID-LIQUID EXTRACTION YES

CAS NUMBER188-95-2 PHENOL111-44-4 BIS<2-CHLO*OETHYL)ETHEB .95-57-8 2-CHLONOPHENOL541-73-1 1.3-OICHLOROIENZENE . . .184-44-7 1,4-DICHLOROBENZENE . . .188-51-4 BENZYL ALCOHOL95-58-1 1,2-OICHLOROBENZENE . . .95-48-7 2-HETHYLPHENOL39438-32-9 8IS<2-CHLOROISOPROPYL>ETHER1*6-44-5 4-METHYLPHENOL621-44-7 N-NITROSO-DI-N-PROPYLAHINE47-72-1 HEXACHLOROETHANE98-95-3 NITROBENZENE78-59-1 ISOPHORONE88-7S-S 2-NIT MO PHENOL185-47-9 2.4-OIHETHYLPHENOL . . . .45-85-8 BENZOIC ACID111-91-1 BIS<2-CHLO»OETHOXY>METHANE128-83-2 2.4-OICHLOROPHENOL . . . .129-82-1 1,2,4-TRICHLOROBENZENE . .91-28-3 NAPHTHALENE1*4-47-8 4-CHLOROANIL1NE87-48-3 HEXACHLOROBUTAOIENE . . .59-54-7 4-CHLORO-3-METHYLPHENOL .91-57-4 2-METHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE88-84-2 2.4.4-TRICHLOROPHENOL . .95-95-4 2.4,S-TRICHLOROPHENOL . .91-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROANILINE131-11-3 DIMETHYL PHTHALATE . . . .288-94-8 ACENAPHTHYLEME99-89-2 3-NITROANILXNE

UG/L1*1818181818181818181818181818185818181818181818181818581858181858

UUUUUUUUUUUUUUU

UUUUUUUUUUUUUUUUUU

CAS NUMBER83-32-9il-28-S188-82-7132-44-9121-14-2484-28-284-44-27885-72-384-73-7188-18-4534-52-184-38-4181-55-3118-74-187-84-585-81-8128-12-784-74-2284-44-8129-88-88S-48-791-94-154-55-3117-81-7

218-81-9

117-84-8

285-99-2

287-88-9

58-32-8193-39-553-78-3191-24-2

ACENAPHTHENE2,4-OINITROPHENOL . . . .

4-NITROPHENOLOIBENZOFURAN2.4-OINITROTOLUENE . . . .2.4-OINITROTOLUENE . . . .OIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETMERFLUORENE4-NITROANILINE4,4-DINITRO-2-METHYLPHENOLN-NITROSOOXPHENYLAMINE <1>4-BROMOPHENYL-PHENYLETHERHEXACHLOROBENZENE . . . .PENTACHLOROPHENOL . . . .PHENANTHRENCANTHRACENEOZ-N-BUTYLPHTHALATE . - .FLUORANTHENEPYRENEBUTYLiENZYLPHTHALATE . . .3.3'-DICHLOROBENZIOINE . .

BENZO(A)ANTHRACENE . . . .BIS<2-ETHYLHEXYL>PHTHALATE

CHRYSENEOI-N-OCTYL PHTHALATEBENZO<B>FLUORANTHENE . .BENZO(K>FLUORANTHENE . . .BENZO(A>PYRENEINOENOM-2. 3-CD> PYRENEDIBENZ<A.H)ANTHRACENE . .BENZO<G,H. DPERYLENE . .

UG/L18 U58581818181818185858

18

18

1858

18

1818

18

1818

28

18

18

18

1*18

18

18

18

18

UUUUU

UUUUUUU

UUUUU

UUU

UUU

U

U

U

U

U

U

U

18 U

<1> - CANNOT BE SEPARATED FROM OIPHENYLAMINE

FORM I

4184 30449

fi-.s Data sheet

ir«e 3iPest ic i ies /PCBs

trat ion: [Lo»] Redui ( C i r c l e one)

ilricWtPrepirei: 25-3ep-67lite A m a z e d : 0 7 - O c t - 6 7Conc/Di l Fac tor : 5Percent Hc is ture ldecante i i Nft

6PL Cifjnup Yes [«]-NoS e p a r a t o r y Funnel [ i t ract ionCor t inuous liquid-Liquid E i t rac t io r [ i)

CAS [ug/L] or uq/KgNuiber

I19-B4-6 fllphi-BHC 0.25 U319-B5-7 Beti-BHC 0.25 U319-86-8 Delti-BHC 0.25 U58-89-9 6uii-BHC (lindane) 0.25 U76-4<-B Heptachlor 0.25 U309-00-2 ftldrin 0.25 U1024-57-3 Heptithlor Epo«ide 0.25 U959-98-fl EndosuHan I 0.25 U60-57-1 Oieldnn 0.5 U72-55-9 4,4'-DDE 0.5 U72-20-B Endrin 0.5 U33213-65-9 Endosulfin II 0.5 U72-54-8 4,4'-DDD 0.5 U1-31-07-8 Endosulfan Sulfitt 0.5 U50-29-3 4,4 ' -DDT 0. U72-43-5 H»tho»ychlor 2. U53494-70-5 Endrin Kftont 0. U57-74-9 Chlordane 2. UB001-35-2 Touphtnt U12674-11-2 Aroclor-1016 2. U11104-28-2 Aroclor-1221 2.5 U11141-16-5 Aroclor-1232 2.5 U53469-21-9 Aroclor-1242 2.5 U12672-29-6 Aroclor-1248 2.5 U11097-6'-! Aroclor-1254 5U11096-B2-5 Aroclor-1260 5 U

Vs =

Vi : Volute of otract injected lul)Vs : Voluii of vatcr eitracted dl)Ms - Height of saiple eitracted (g)Vt = VoluM of total e.trict lul)

1000 or Us = Vt -

Fort I

50000 Vi • 3.0

4 1 8 4 3 0 4 5 0

• J1 ,: , \ j r ; , t -

No



I Sample Nurntxv I

yjuur^Jo ioi I


4 1 8 4 30451

E N •;_ 5 E -

" .r• < J 3


LAB SAMPLE ID NO: 4184-7*

SAMPLE MATRIX: WATEROATA RELEASE AUTHORIZED «Y


CASE NO: «18»

QC REPORT NO: 4184CONTRACT NO:

DATE SAMPLE RECEIVED: •7/23/87

VOLATILE COMPOUNDS

CONCENTRATION: LOWDATE EXTRACTED/PREPARED:

DATE ANALYZED: 18/82/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (NOT DECANTED)

PH

CAS NUMBER74-87-3 CHLOROMETHANE74-83-7 BROMOHETHANE

75-81-4 VINYL CHLORIDE75-88-J CHLOROETHANE75-87-2 MCTHYLENE CHLORIDE . . .47-44-1 ACETONE

75-15-9 CARiON DISULFIOC . . . .

75-35-4 1.t-OICHLOROCTHENC . . .

75-35-1 1.1-OICHLOROETHANC . . .154-48-5 TRANS-1.2-OICHLOROETHENE47-44-1 CHLOROFORM

l»7-»4-2 1.2-OICHLOROETHANC . . .

78-73-3 2-IUTANONC71-SS-4 I.1.i-TRICHLOROETHANE .

S4-23-5 CARION TETRACHLORIDC . .

l«e-«5-4 VINYL ACETATE75-27-4 IROMOOICHLORCMETHAWC . .

181818S

UG/L18 U

UUUUUUUUUUU

1

18

•

UUUuu

CAS NUMBER78-87-518841-82-4

77-81-4124-48-177-88-S71-43-2

UO/L

118-75-871-25-2188-18-1571-78-4

127-18-4

77-34-5188-88-3

188-78-7188-41-4188-42-1

1,2-OICHLOMOPROPANE . . .TRANS-1.3-OICHLOROPROENE .

TRICHLOROETHENEDIBROMOCHLOROMETHANE . . .1.1.2-TRICHLOROETHANC . .BENZENECIS-1.3-OICHLOROPROPENE .

2-CHLOROETHYLVINYLETHER .BROMOFORM4-METHYL-2-PENTANONE . . .

2-HEXANONETETRACHLOROETHENE . . . .1.1,2.2-TETRACHLOROETHANE

TOLUENECHLOROBENZENE

ETHYLBENZENE

STVRENETOTAL XYLENES

18f18

18

51855555

U

uuuuuuuuuuuuuuuuu


SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING 8UALXFIERS.

FORM I

4184 30103

L a b o r a t o r y Name: ETC/Toxicon

Case No: 4184

Sample Numb«r


40 -ir~)

CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationug/L

300U

200U

200U

U tivliryti*; compound WS$ analymd for but DOt 4t9&t4. RcpOTl DC minimntn detection litnit for the Sample with mt U(e.g. 10U) Nm^l on necesssy n»i»<fjiii<uyi/iiiiyfvy) icdoo. (Thjj U not necosjrfly me iostnuaent detectioQ limit)

I wts SDiIyzed for but not 4ficrtfi1 The number is me «"ini«num MQidbleThe footnote ihould read:detection limit for the ample.

viJoe. This flv U nwd eiflier wbco ffttm^tiy t cooceafaaioo for texiBdvtly identified compounds1-1 nH^rmtr If fyfamrA or »<Un ft>g m»q fpertrri <to» itntiftW«1 Ihe prMencg rf • componfld flat meett flie ideali-

rtcanoo criteria but the remit b less than the Kpecified detectioa limit but greater msn zero (e . 101). If limit of detection is10 U£/L aad a cooceatntioa of 3 ug/L is calculated, report « 31.

4 1 8 4 3 0 1 0 4

L A B O R A T O R Y NAHE E T C / T

CASE NO «18»

•* r _ E N _ - £ E R

ORGAMC5 ANALYSIS DATA SHEET<PAGE 2>


CONCENTRATION: LOW

DATE EXTRACTED/PREPARED: *9/3*/87DATE ANALYZED: l*/*5/87

CONC/DIL FACTOR: 1.

PERCENT MOISTURE: (DECANTED)

GPC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIQUID-LIQUID EXTRACTION YES

CAS NUN0ER1*8-95-2 PHENOL

111-44-* 8IS<2-CHLOROETHYL>ETHER .

95-57-8 2-CHLOROPHENOL

S41-73-1 1,3-OICHLOROBENZENE . . .1*4-44-7 1,4-DICHLOROBENZENE . . .

1*9-51-* iENZYL ALCOHOL95-59-1 1,2-DICHLOROBENZEME . . .

95-41-7 2-HETHYLPHENOL39438-32-9 BIS(2-CHLOROISOPROPYL)ETHER

1*4-44-5 4-METHYLPHENOL

421-44-7 N-NITROSO-OI-N-PROPYLAMINE47-72-1 HEXACHLOROETHANE

9B-9S-3 NITROBENZENE

71-59-1 XSOPHORONE88-75-5 2-NITROPHENOL

185-47-9 2,4-OIMETHYLPHENOL . . . .45-85-9 tENZOIC AC 10

111-91-1 BIS<Z-CHLOROETHOXY>METHANE129-«3-2 2,4-OICHLOROPHENOL . . . .129-82-1 1,2.4-TRICHLOROBENZENE . .

91-29-3 NAPHTHALENE

1*4-47-8 4-CHLOROANILINE

87-48-3 HEMACHLORQBUTADIENE . . .S9-S9-7 4-CHLORO-3-METHYLPHENOL .

91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCVCLOPENTAOIENE

68-94-2 2,4.4-TRICHLOROPHENOL . .7S-7S-4 2.4,5-TRICHLOROPHENOL . .91-S8-7 2-CHLORONAPHTHALENE . . .88-74-4. 2-NITROANILINE

131-11-3 DIMETHYT. PHTHALATE . . . .

2*8-94-8 ACENAPHTHYLENE99-*9-2 3-NITROANILINE

UG/L1*1*

1*

1*

1*1*

!•1*

1*

1*

18

1*

18i*1*

1*

5*1*

1*1*

1*

1*

1919

19

19

19S*19

59

19

19

59

U

U

U

U

UU

U

U

U

U

U

U

UU

U

UU

U

UU

U

U

U

U

U

U

UU

U

U

U

UU

CAS NUMBED

83-32-9

51-28-5199-92-7

132-44-9

121-14-2494-29-2•4-44-27995-72-384-73-7

199-19-4534-52-1

84-39-4

191-55-3118-74-1

87-84-5•5-91-8128-12-784-74-2

294-44-9129-99-985-48-791-94-1

54-55-3117-81-7218-81-9

117-84-9295-99-22*7-*B-9

59-32-8193-39-5

53-79-3191-24-2

ACENAPHTHENE2. 4-DINITROPHENOL . . . .4-NXTNOPHENOLOIBENZOFURAN2,4-OINITROTOLUENC . . . .2.4-OINITRQTOLUENE . . . .

DIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETHER

FLUORENE4-NITROANILINE

4. 4-OINITW-2-HETHYLPHENOLN-NITROSOOIPHENYLAMINE <1>4-BROMOPHENYL-PHENYLETHCR

HEXACHLOROBENZENC . . . .PENTACHLOROPHENOL . . . .PHENANTHRENE

ANTHRACENEDI-N-BUTYLPHTHALATE . . .

FLUORANTHENE

PYRENEBUTYLBENZYLPHTHALATE . . .3, 3'-OICHLO«OBENZIOINE . .BEN20(A>ANTHRACENE . . . .BIS(2-ETHYLMEXYL)PHTHALATECHRYSENEDI-N-OCTYL PHTHALATE . . .BENZO<B>FLUORANTHENE . . .BENZO(H)FLUORANTHENE . . .BENZO(A)PYRENE

INOENO<1.2. 3-CO)PYRENE . .OIBENZ<A.H>ANTHRACENE . .

BENZO<G. H, DPERYLENE . . .

UG/L19

59

59

1919

19

19

19

19

59

59

1919

19

59

1919

19

1919

19

2919

34

19

19

19

1*1*19

19

19

U

U

U

UU

U

UU

U

UU

U

U

UU

UU

UU

U

U

U

U

U

U

U

U

U

U

UU

<1> - CANNOT BE SEPARATED FROM 01PHENYLAMINE

FORM I

4184 30105

Ld'r'i';', Hit;: -.".':-.. ::r

Case No: 4;=4

r j'.r-ies. !n;.

Organ:cs Analysis Data Sheet(Page 3)Peshcides/PC&s

Concentration: [Lou] Mefliui (Cir:le eDate Eitracted/Preparefi: 2'-Sep-87Bite Rnaly:ed; 06-0ct-fl7Conc/Dil Factor: 1Percent Moistureldecantedj NR

6FC C'.ea-u: Yes («]-NoSeparator* Funnel tstrac'ion YesCcntinuoi.3 Liquid-Liquid Extractian [«] Yts

CASNuiber

[uq/L] or ug/Kg

319-84-6 Alphi-BHC 0.05 U319-B5-7 B»tJ-BHC 0.05 U319-B6-8 Ddti-BHC 0.05 U53-89-9 Saiii-BHC ILjndine) 0.05 U76-44-8 HepticMor 0.05 U309-00-2 Aldrin 0.05 U1074-57-3 HeptKhlor Epoiide . 0.05 U959-98-8 Endosulfin I 0.05 U60-57-1 Dieldrin 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfin 11 0.1 U72-54-8 4,4'-DDB 0.1 U1-31-07-8 Endosulfjn Sulfite 0.1 U50-29-3 4,4 ' -DDT 0.1 U

72-43-5 Hethoxychlor 0.5 U53494-70-5 Endrin Kftont 0.1 U57-74-9 Chlord»ne 0.5 U8001-35-2 Touphene 1U12674-11-2 flroclor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 Uf3U!?-:i-9 Aroclor-1242 0.5 U12672-29-6 flroclor-1248 C.5 U11097-69-1 Aroc!or -1254 1 U

11096-82-5 Aroclor-1260 1 U

Vi = Voluw of utract injected (ul)Vs - Voluie of Niter ext racted (•!)Ms - Weight of saiple e x t r a c t e d (q)Vt = Voluie of total eitract (ul)

Vs - 1000 or Ms - Vt = 10000 Vi = 3.0

Fori

4 1 8 4 3 0 1 0 6

NoSsr


i I

f I

CASNumber


Compound Fr»cl»ooCctim«t«d

np*"f"**<w*(ug/jf<x ug/kg)

1O.

Sorrai 13,3.

I.

L 35iftffe

24

27.

30


4 1 8 4 3 0 1 0 7r- - i

LABORATORY NAME: ETC/TOKICON

LAI SAMPLE ID NO. 4184-BV

SAMPLE MATRIX: HATER

DATA RELEASE AUTHORIZED BY\Jt.

ORCANICS ANALYSIS DATA SHEET

'<PAGE 1)

CASE NO: 4184

•C REPORT NO: 4184

CONTRACT NO: O}^^

DATE SAMPLE RECEIVED.

VOLATILE COMPOUNDS

»9/23/87

CONCENTRATION: LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: l»/»2/87

CONC/DIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)

PH

CAS NUMBER74-87-374-83-975-81-475-88-37S-*9-247-44-175-15-875-35-4

75-35-3156-68-567-64-3187-84-278-93-371-55-454-23-518B-8S-475-27-4

CHLOROMETHANEBROMOMETHANCVINYL CHLORIDECHLOROETHANEMETHYUENE CHLORIDE . . . .ACETONECARBON OISULFIOE1. 1-DICHLOROETHENE . . . .1. 1-OICHLOROETHANE . . . .TRANS-1.2-DICHLOROETHEME .CHLOROFORM1.2-OICHLOROETHANE . . . .2-BUTANONE1. 1, 1-TRICHLOROETHANC . .CARBON TETRACHLORIDE . . .VINYL ACETATE

BROMOOICHUOROMETHANC - . .

UG/L18 U18 U18 U18 U5 U43

1

UU

UUUUUUU

18 U• U

CAS NUMBER71-87-51*841-82-471-81-4124-48-17V-88-571-43-21*861-81-5118-75-875-2S-2181-18-1591-78-4127-11-479-34-51*8-88-3188-98-71*8-41-4188-42-5

UG/L1.2-OZCHLOROPROPANC . . .TRANS-1,3-OICHLOROPROENE .TRICHLOROETHENCOIBHOMOCHLOROHETHANE . . .1.1,2-TRICHLOROETHANE . .BENZENECIS-1.3-OICHLOROMOPENE .


IROMOFOdM

4-METHYL-2-PEMTANONE . . .2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES

51*

UUUUUUUUUUUUUUUUUU



FORM I

4 1 8 4 3 0 0 8 4


Case No: 4184

Sample Nurabtr

/o


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropjl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

ConcentrationHt/L

300U

200U

200U

U Tndif^t^ mtnpnufyj IM^ »TnlyTH fnr Ht ~^ AftrftrA Pgi«t **• minimum d*«Mtinn limit fnr th» tarn pig with thg II(e.g. 10U) based on necessary concentradoo/dihition action. (This is not necessarily die instrument detection limit)The footnote should real U-Compound was analyzed for but not detected. The number is the minnnnm attainabledetection limit for me sample.

J T«<<irat»« «n fft^mttfA vahw. This flag U used either when >t*im«t<n£ a conctntration for teutatively identified compoondiwhere a 1:1 response is assumed or when the mass spectral data indicated me presence of a compound that meets the ideod-fication criteria but the result is less than die specified detection limit but greater man tero (&g. 1QJ). If limit of detection U10 iig/L and a concentration of 3 U&/L is calculated, report at 3J.

4 1 8 4 3 0 0 8 5

LABORATORY NAME

CASC NO:

ETC/TOXICON

418*

OUGANICS ANALYSIS DATA SHEET(PAGE 2)

SEMIVOLATILE COHPOUNOS

CONCENTRATION: LOWDATE EXTRACTED/PREPARED: 89/38/87DATE ANALYZED: 18/85/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (DECANTED)

CPC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIQUID-LieUIO EXTRACTION YES

CAS NUMBER188-95-2 PHENOL111-44-4 BX5(2-CHLOROETHYL>ETHEK .9S-S7-8 2-CHLOROPHENOLS41-73-1 1.3-DICHLOROBENZENE . . .184-44-7 1.4-OICHLOROBENZENE . . .188-51-4 BENZYL ALCOHOL95-58-1 1.2-OXCHLOROBENZENE . . .95-48-7 2-hETHYLPHENOC39438-32-9 BIS(2-CHLOROISOPROPYL)ETHER186-44-5 4-METHYLPHENOL421-64-7 N-NITROSO-DI-N-PROPYLAMINE47-72-1 HEXACHLOROCTHANC98-95-3 NITROiENZEMC7S-S9-1 ISOPHOROMC88-75-S 2-NITROPHENOL185-47-9 2.4-OIMETHYLPHENOL . . . .45-85-8 KNZOIC ACID111-91-1 §IS(2-CHLOROETHOXY)METHANE

128-83-2 2. 4-OICHLOKOPHENOL . . . .

128-82-1 1.2.4-TKXCHLOROBENZENC . .

91-28-3 NAPHTHALENE184-47-8 4-CHLOROANILINE•7-48-3 HEXACHLOROBUTAOIENC . . .59-58-7 4-CHLOHO-3-HETHYLPHENOL .91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE88-86-2 2.4.4-TRICHLOROPHENOL . .95-95-4 2.4,S-TRICHLOROPHENOL . .91-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROANILINC131-11-3 DIMETHYL PHTHALATE . . . .298-94-8 ACENAPHTHYLENC99-89-2 3-NXTMOANILINC

UG/L

!•!•1*1*!•!•

!•

!•!•!•!•1*

!•!•!•!•S»!•1*181*!•1818!•!•185818S81818S8

UuUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

CAS NUMiER

83-32-9Sl-28-5188-82-7132-44-9121-14-2484-28-284-44-27885-72-384-73-7188-18-4534-52-184-38-4181-5S-3118-74-187-84-58S-81-8128-12-784-74-2284-44-8129-88-885-48-791-94-1S4-SS-3117-81-7218-81-9117-84-82*5-99-2287-«8-958-32-8193-39-553-78-3191-24-2

ACENAPHTHENE2.4-OINITROPHENOL . . . .4-NITROPHENOLDliENZOFURAN2.4-OINITROTOLUENE . . . .2.A-DINITROTOLUENC . . . .DIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETHERFLUORENC4-NITROANXLXNC4,6-OINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAHINt <1>

4-iROMOPHENYL-PHENYLETHERHEXACHLOROIENZENE . . . .PENTACHLOROPHENOL . . . .PHENANTHRENEANTHRACENEOX-N-BUTYLPHTHALATE . . .

FLUORANTHENEPYRENE•UTYL8ENZYLPHTHALATE . . .3.3--OICHLOROBENZIDINE . .BENZO<A>ANTHRACENE . . . .BIS(2-ETHYLHEXYL >PHTHALATECHRYSENEOI-N-OCTYL PHTHALATE . . .•EN20(B)FLUORANTHENE . . .BENZO(K)FLUORANTHENE . . .BENZO<A)PYRENEINOENOd, 2. 3-COPYRENE

OIIENZ<A,H>ANTHRACENE . .8ENZO(G.H. DPERYLENE . . .

UG/L

18 U

U

U

58

58

18

18

18

18

18

18

58

58

18

18

18

58

18

18

18

18

18

18

28

18

1818

18

18

18

18

18

18

U

U

U

U

U

U

uuuuuuuuuuuuuuuuuuuuuuu

<1> - CANNOT BE SEPARATED FROM DIPHENYLAHXNE

FORH X

4184 3C086

I r e .Case Nc: MB*

Organic* Analysis Data Sheet(Page 3)PestKjdes/PCBs

Co^ce^'ation: [Lo»] Kediui (Circle on?)Date Eitractei/rrepared: I^-Sep-B7Date Anal/red: OtrOct-B7Conc/DiI Factor: 1Percent Koisture(decanted) NR

Cleave fes [«Hot;', Fur.nel Extraction Yes

Continuous Liquid-Liquid Extraction [i] Yes

CASNuiber

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-B33213-65-972-54-81-31-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-5

11096-B2-5

[ug/l] or

Alphi-BHCBet»-BHCDelta-BHCGaiia-BHC (Lindane)Heptachlor

Heptachlor Epoiide.Endosulfan IDieldrin

EndrinEndosulfin II

Endosulfan Sulfate.4,4'-DOTflethoxychlorEndrin KetoneCMordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260

0.05 U0.05 U0.<K U0.05 U0.05 U0.05 U0.05 U0.05 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.5 U0.1 U0.5 U

1 U0.5 U0,5 U0.5 U0.5 U0.5 U

1 U1 U

Vi = VoIuM of (itract injected lullVs - Voluit of »ater extracted (il)Us : Height of saiple extracted (glVt - Volute of total extract l u l l

Vs - 1000 or Hs = Vt = 10000 Vi = 3.0

Fori I

4184 30087

Name CTC/ToxLicon

e No


S»mple Number


CASNumbw Compound N«m« Fraction

Ettirrva1*d

1..

UIOIC 5111/lJtC SI?

/ 1/ I

16..

»-

12


4184 3C088

H


LAt SAMPLE ID NO: 4184-188SAMPLE MATRIX: WATER


4184

4184

OftGANICS ANALYSIS DATA SHEET

(PAGE 1)

CASE NO:

8C REPORT NO:

CONTRACT NO:

OATE SAMPLE RECEIVED:

VOLATILE COMPOUNDS

•9/29/87

CONCENTRATION: LOUOATE EXTRACTED/PREPARED.

OATE ANALYZED: 18/03/87

CONC/OIL FACTOR: i.


PH

CAS NUMBER


74-83-9 BROMOHETHANE7S-81-4 VINYL CHLORIDE75-88-3 CHLOROETHANE

7S-89-2 METHYLENE CHLORIDE . . .

47-44-1 ACETONE

75-15-8 CARBON OISULFIOE . . . .

7S-3S-4 i.1-OICHLOROETHENE . . .

7S-3S-J 1.I-DICHLOROETHANE . . .

154-48-5 TRANS-1.2-OICHLOROETHEME

47-44-3 CHLOROFORM

l«7-«4-2 1,2-DICHLOROETHANE . . .

78-93-3 2-kUTANONC

71-55-4 1. I. 1-TRICHLOROETHANE .

54-23-5 CARBON TETKACHLORIOC . .l»B-»S-4 VINYL ACETATE7S-27-4 BROMOOICHLOROMETHANE . .

IK

14

14

14

14

i

14

1

1

i/L

> U

> U

» U

> U

L J

» U

U

U

U

U

U

U

jfoU

U

» U

1 U

CAS NUMBER

78-87-5

18841-82-4

79-81-4

124-48-1

79-88-5

71-43-2

18841-81-5118-75-8

7S-25-2

188-18-1

591-78-4

127-1B-4

79-34-S

188-88-3

188-98-7

188-41-4

188-42-5

UG/L1,2-OICHLOROPROPANE . . .

TRANS-1,3-OICHLOROPROENt .

TRICHLOROCTHENEOIBROMOCHLOROMETHANE . . .


BENZENE

CIS-1,3-DICHCOROPROPENE .2-CHLOROETHYLVINYLETHER .

8MOHOFOMH

4-t4ETHYL-2-PENTANONe . . .

2-HEXANONETETRACHLOROETHENE . . . .


TOLUENE

CHLOMOBENZENE

ETHYL BENZENE


18

S!•18S18

UUUUUUUUUUUUUUUUUU

8 - COMPOUND WAS DETECTED IN THE 8C BLANK.



THE SAMPLE.


FORM I

4 1 8 4 3 0 5 0 2

Labora to ry Name: ETC/To»icon

Case No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationat/L

300U

200U

200U

U Indira*** ryunpounj yg rulymf fry *•'* "<* **«rtrf- *q*»* ft"* minimnm (toeeriftn liiqtt fnr the «mplg with Ae U(e.g. 10U) bised on necessary conce&tntioo/dilntkja action. (This is not necessarily the instrument detection limit)The footnote ttould read: U-Compound was analyzed for but not detected. The number is the minimum atninibiedetection Emit for the ample,

"I *«n'm«t*H vfhifi Thtf fl«f It nttnl rifafr mtv-ti tim«rin£ « n.kfiHi Jlvai fnr b-ntafivriy Mgnrifiad eompoundlwhere a 1: 1 response is •««"""*< or when the mas* spectral data !»««'•»**«< me presence of a compound that meets the identi-ffcation criteria but the resnltb less man the jpedfied detection limit but greater than rero (e . 1QJ). If limit of detection is10 (if/L and a concentration of 3 n</L is calculated, report at 3J.

4 1 8 4 3 0 5 0 3

Case No


(Page 2)


Sample N

Coi-Kentranon: U-O" ) Medium (Circle One)

)ate Extracted'Prepared

Jate Analyzed

Conc/Dil Factor

GPC Cleanup DYes QNo

CASNumber

10 \ t > } % 7

\r* 'n*eAnt*d)


tienol

<s< • 2 -ChloroethyHEther

-Chloropnenol

. 3-Dtchlorobenzene

. 4-Dtcnlorobenzene

ienzyl Alcohol

. 2-Dichlorooerutnt

-Methylphenol

is(2 -cnloroisopropyOCtner

•Methytpnenoi

l-Nitroso-D«-n-Propytam«ne

(exacMoroethant

(itrobenztne(opnoron*

•Nhrgphenot

.. 4-Dimethy{pn*nol

lenzoic Acid

><s<-2-Ch<oroetnoxYlM«itujne

. 4-Dichlorophenol

. 2, 4-TrichkxoberueneNaphtha t«f>«

l-ChloroaiMline

He tachlorobutadtenc

l-Chloro-3-Methylpnenolt -M«tt\v4naphth«lent

4e xacMorocvclopentadient

I. 4. 6-Trichloropnenol

J. 4. S-Tochforopneno!

! -Chloronaphthalene

!-NitroanilineDimethyl Phthalite

B£Cnaphthy1«r>e

lOu./DM10 uIn,*.10k/Of^//o<-/Aw.lOu1$IDulOulOuIQl

mi*lyi.^(4

IDlA.

IQi*

ID*

I/)U

lOlt.{Dtfi-\u*-tOlA.

ftulf)lA

56*1lOu.


CAS ug/lorug/KgNumber (Circle One3-32-9

1-28-5

00-02-7

32-649

21-14-2

606-20-2

84-66-2

7005-72-306-73-7

00-01-6

534-52-1

86-30-6

01-55-3118-74-1

8746-5

85-01-6

120-12-7

84-74-2

206-44-0

129-00-0J5^87

M-94-1

>6-553

117-81-7 1

218-01-9

117-84-0

20599-2

207-08-9

>0-32-8

193 395

53-70-3

191-24-2

Aceaiphtheoe

!. 4-Dinhrophenol

4-NilropSenolJibenzofuran

2.4-Oinitroiolu«ne

t. £-Oinhroto<uene

Oiethytphthalate

4-Chloropnenyl-phenytethef

Fluor ene

4-Nhroanifine

4. 6-Oinhro-2-Wethy1pnenol

N-Nrtrosodiphenytamine (1 )

4-Bromopheny<-pheny(ether

Kexachlorobenzent

'entachlorophe not

Phenanthrene

AnthnKene

Di-n-ButytphthalateFluoranrnene

PyreneBurytt>«azy{phtKalate

3. 3'-DtcMoraberuid<ne

Benn(t>Anthr*cene

t>n(2-Ethy(h«Ky<)Pmhalate

ChryMne

Oi-n-Octyt Pntnalate

Berujofrfluoranthene

Beniotli)Fluoranth«ne

B«nzo(a)Pyrene

InderxXL 2. 3-cd)P¥'«n«Otbenfli hlAnihcacene8enio(g. h. i)Perylene

IVK.$4**>4u

//Ok(fluin*./flu(Ot*fO*

3*KS9(4

IV*Mb.

(flu.*>«

Qu(0k

Qu

hulQh -JOu

Jeu/OU.Iflu

]QlA.

lOu.(Hlr

lO1^

ID1*'

/fl^n)tIn*. .

4 1 6 4

,,-: Sc.

Analysis Data S'leet(Paqe 3]Peshudes/PCBs

!Lo«] Nediui (Circle one) Bc: Ciei-ur ves [«}-1oCi'f E»ti-ac>.e:;s'e;a''e(i: 29-Sep-fl7 Separator-, "uirel Extraction VesSite a-a!,:ei: C?-Dct-B7 Crrti-u:.Conr/Dil Factor: 1Percent 'ois'-jreideca'ted) NR

CflS [ua'L] or u»/Nuiber

319-B4-6 Alphi-BHC 0.05 U319-B5-7 Beti-BHC 0.05 U319-B6-8 D«lt«-BHC 0.05 U58-69-9 Eana-BHC (Lindanc) 0.05 U76-44-B Keptachlor 0.05 U309-00-2 Aldrin 0.05 U1024-57-3 Keptachlor Epoxide 0.05 U959-9B-B Endosulfan 1 0.05 U60-57-1 Diildrin 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfan II 0.1 U72-54-8 4,4'-DDO 0.1 U1-31-07-8 Endosulfan Sulfatt 0.1 U50-29-3 4,4'-DDT 0.1 U72-43-5 Bethoiychlor 0.5 U53494-70-5 Endrin Kftone 0.1 U57-74-9 Chlordane 0.5 UB001-35-2 Toiapheni 1 U

12674-11-2 Aroclor-lOU 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U53469-21-9 Aroclor-1242 0.5 U12672-29-6 Aroclor-1248 0.5 U11C97-69-1 Aroclor-1254 I l l11C96-82-5 Aroclor-1260 ID

Vi = Volute of extract injected (ul)Vs = VoluH of Hittr eitricted (illUs = Height of sa«ple eitracted (g)Vt = Voluit of total extract (ul)

Vs = 1000 or Ns * Vt = 10000 Vi = 3.0

Fon 1

4184 30505

abo'ato'y Name

e No


Sample Numt>e»


CASNumber Compound N«m« Fnjction

E»tim«t»dtr«tionug/hg)

5.

•..

7..

(3

i::::18.

*9 ._.

77.


4 1 8 4 3 0 5 0 6

LABORATORY NAME ETC/TOXICON

LAB SAMPLE XO NO: 4184-92

SAMPLE MATRIX: WATERDATA RELEASE AUTHORIZED BY


CASE NO. 4184flC REPORT NO: 4184

v, DATE SAMPLE RECEIVED: 89/29/87

VOLATILE COMPOUNDS

CONCENTRATION: LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: 18/83/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)

PH

CAS NUMBER74-17-374-83-975-81-475-88-375-89-247-44-175-15-875-35-475-35-3156-48-547-44-1187-84-271-93-371-55-4S4-23-S188-85-475-27-4

CHLOROMETHANEBROMOMETHANCVINYL CHLORIDECHLOROETHANEHETHYLENE CHLORIDE . . . .ACETONECARBON DISULFIOE1.1-DICHLOROETHENE . . . .1. t-OICHLOROETHANE . . . .TRANS-l-2-OICHLOROETHENE .CHLOROFORM1,2-OICHLOROETHANE . . . .2-BUTANONE1. 1. 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEBROMOOICHLOROMETHANC . . .

UG/L18 U18 U18 U18 U5 U74

1

UUUUUU

*>UU

18 US U

CAS NUMBER71-17-518*41-82-479-81-4124-41-179-88-571-43-218841-81-5118-75-175-25-2188-18-1591-71-4127-11-479-34-S188-18-3188-98-7188-41-4188-42-5

UG/L1,2-OICHLOROPROPANE . . .TRANS-1, 3-OICHLOROPROENC .TRICMLOROETHENEOIBROMOCHLOROMETHANE . . .1. 1. 2-TRICHLOROETHANE . .BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHE* .BROMOFORM4-METHYL-2-PENTANONE . . .2-HEXANONCTETRACHLOROETHEME . . . .1. 1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES

S18

UUUUUUUUUUUUUUUUUU

8 - COMPOUND WAS DETECTED IN THE «C BLANK.


THE SAMPLE.

SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING 9.UALIFIERS.

FORM I

4 1 8 4 3 0 1 4 5


Case No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationm/L

300U

200U

200U

U Tt>Mw-«f>^ compound was analyzed for but not tfrtTT*^- Report the minirnnm detection limit for tbe sample with tbe U(e.t> 10U) based on necessary concauratioo/dilution action. (This is not necessarily die instrument detection limit)The footnote should read: U-Gompound was analyzed for but not detected. Tbe number is the minimum attainabledetection i»mh for the *a*if^

J Ttirlirjfr!* an Mrim«t»rt vain* Thh fl«« U MM< ritVr mîen Mfimaring « concgntrarinn for tentarivdy ktenrifiad compoondtwhere a 1:1 re^ncmjf is assumed or wheo me *"••• iueclJil <*•*• iiv<ir«t<«j the presence of a compound that meets die ideoti-ficatioa oilcria but tbe result bless than the specified detection limit but greaier than zero (e^TlQI). If limit of detection is10 ug/L and a concentration of 3 jig/L is raimiatoii^ report as 31.

4 1 8 4 3 0 1 4 4

Case No: 4184

Organic? Arjlysis Data Sheet(Page 31Peshudes/PCBs

Cor-ceJ-tration: [Lo»] flediui (CircleDate Extracted/Prepared: 29-5ep-B7Date Analyzed: 06-Oct-87Con;/Di! Factor: 1Percent Roisture(decanted) NR

Gf'C Cleans Yes [x]-NoSerarat:ry Funnel titrac'.ior fesContinusus Liquid-Liquid Extrjcticn [s] Yes

CAS [ug/L] or u;/Nuiber

319-84-6 «!ph«-BHC 0.05 U319-85-7 Beta-BHC 0.05 U319-86-fl Oelta-BHC 0.05 U58-89-9 EaiH-BHC (Lindani) 0.05 U74-44-8 HepUchlor 0.05 U309-00-2 ftldrin 0.05 U1024-57-3 Heptachlor Epo«id« . 0.05 U959-98-8 Endosulf»n I 0.05 UiO-57-1 Dieldnn 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-45-9 Endosulf«n II 0.1 U72-54-8 4,4'-DDD 0.1 U1-31-07-8 Endosulfan Sulfjte 0.1 U50-29-3 4,4'-DDT 0.1 U

72-43-5 HtthoiycMor 0.5 U53494-70-5 Endrin Kttoot 0.1 U57-74-9 Chlordani 0.5 UB001-35-2 Toiaphen* 1 U

12674-11-2 flrodor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 ftroclor-1232 0.5 U53469-21-9 ftroclor-1242 0.5 Ul?672-29-6 «rcclor-i:48 0.5 U11097-69-1 flroclor-1254 1U11096-82-5 Aroclor-1260 Ill

Vi - VoluM of extract injected (ul)Vs = Voluit of Mter extracted [•!)Us - Keiqht of saiple extracted (q)Vt = Volute of total extract l u l l

Vs = 1000 or N$ Vt = 10000 Vi •- 3.0

For* I

4 1 8 4 3 0 1 4 5

ETC/Toxucon

eNo

Organic* Analysis Data Sheet(Page 4)

ample Numbcf I

X4WU001 I


ncAsNumber Compound Nam* Frvction Numbw

Ertirrutcd

6"

6..

|..

11:10.

**it /£>

19..

i;:::11

uwk. 3/032

/on ITfStr.-i.oit. lozi 11

tan M90

UlOC I2/15 12.


4 1 8 4 3 0 1 4 6



SAMPLE MATRIX: WATER


• 184

4184

OKGANICS ANALYSIS DATA SHEET

<PAGE 1)

CASE NO:

aC REPORT NO:

CONTRACT NO. (


VOLATILE COMPOUNDS

•9^23/87

CONCENTRATION: LOW


DATE ANALYZED: l*/*2/fl7

CONC/DIL FACTOR: 1. PH

PERCENT MOISTURE: <NOT DECANTED*

CAS NUMBER74-17-374-83-97S-81-475-88-375-89-247-44-17S-1S-87S-3S-47S-3S-3154-48-k47-44-3187-84-278-93-371-1S-454-23-f188-8S-'47S-27-4

CHLOROHETHANEBROHOHETHANCVINYL CHLORIDECHLOROETHANEHETHYLENE CHLORIDE . . . .ACETONECARBON OISULFIOE1.1-OICHLOROETHEME . . . .i. 1-OICHLOROETHANC . . . .TRANS-1.2-DICHLOROETKENE .CHLOROFORM1,2-OICHLOROETHANE . . . .2-BUTANONE1. 1. l-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEBROMOOICHLOROMETHANC . . .

U6/L18 U18 U18 U18 Ui U4V

1

UUUUUUUUU

18 US U

CAS NUMBER78-87-S18841-82-479-81-4124-48-179-88 -S71-43-218841-81-S118-7S-87S-25-2188-18-1S91-78-4127-18-479-34-S188-88-3188-98-7188-41-4188-42-5

UG/L

1.2-OICHLOROPROPANE . . .

TRANS-1.3-OICHLOROPROENE .

TRICHLOROETHENE

OIBROMOCHLOROMETHANE . . .


BENZENECIS-1,3-OICHLOROPROPENE .


BROHOFORH

4-METHYL-2-PENTANONE . . .

2-HEXANONC



TOLUENE

CHLOROBENZENE

ETHYLBCNZENE

STYRENE

TOTAL XYLENES

18

S18

1*S

18

UUUUUUUUUUUUUUUUUU



THE SAHPLE.


REPORTING 8UALIFIERS.

FORM I

4 1 8 4 30121


Case No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationut/L

300U

200U

200U

compound wit analyzed for bat not drtpcleiL Report me minimim detection limit for me sample with the U(e.g. 10U) based on necessity concentration/dilution action. (This is not necessarily the instrument detection limit)The footnote should read: U-Compooad was analyzed for but not detected. The number U me minimum attainabledetection limit for the ample.TnrficjtM M >tfim»^ v^hif T^jf flgg <f ny^ ^ftg «*X« i^nnritu • cnnegntnrinn fnr tentatively idgnrified componndawhere a 1:1 response U teamed or when (he mats spectral dati 1**'** me presence of a compound that meets the ideati-ffcatioQcriteria but the result Is less man the specified detection limit but greater than zero (e . IQJ). If limit of detection U10 w/L and a coocentratkc of 3 n^L is calailated, report as M.

4 1 8 4 3 0 1 2 2

LABORATORY NAHECASE NO

ETC/TOX1CON



CONCENTRATION: LOWDATE EXTRACTED/PREPARED: *9/3*/B7DATE ANALYZED: l*/*S/87CONC/DIL FACTOR: i.PERCENT MOISTURE: <DECANTED)

6PC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LiaUID-LIBUIO EXTRACTION YES

CAS NUMBER

1*8-95-2 PHENOL111-44-4 IIS(2-CHLOROETHYL)ETHER .95-57-8 2-CHLOROPHENOL541-73-1 1,3-OICHLOROBENZENE . . .1*4-44-7 1,4-DICHtOROBENZEWE . . .l**-51-4 BENZYL ALCOHOL9S-S*-1 1.2-OICHLOROBENZENE . . .95-48-7 2-METHYLPHENOL39438-32-9 BIS<2-CHLOROISOPROPYL>ETHER1*6-44-1 4-METHYLPHENOL421-44-7 N-NITROSO-OI-N-PROPYLAHINE47-72-1 HEXACHLOROETHANE98-9S-I NITROBENZENE78-59-1 ISOPHORONEB8-7S-S 2-NITROPHENOL

1*5-47-* 2. 4-OIHETHYLPHENOi. . . . .6S-BS-* BCNZOIC ACID111-91-1 BIS<2-CHLOROETHOXY>HETHANE124-83-2 2.4-OICHLOROPHENOC . . . .129-82-1 1-2.4-TRICHLOROBENZENC . .91-2*-3 NAPHTHALENE1*4-47-8 4-CHLOROANILINE87-48-1 HEXACHLOROBUTAOIENE . . .S9-S*-7 4-CHLORO-3-METHYLPHENOL .91-57-4 2-METHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE88-**-2 2.4.4-TRXCHLOROPHENOL . .95-95-4 2,4.5-TRICHLOROPHENOL . .91-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROAMILINE131-11-3 DIMETHYL PHTHALATE . . . .2*8-96-8 ACENAPHTHWENE99-*9-2 3-NITROANILINE

UG/L

1*

1*i*l*l*i*

l*l*l*l*l*l*l*1*l*l*

S*1*1*1*1*1*1*1*1*1*1*S*1*

S*1*1*I*

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

CAS NUMBER

•3-32-*

S 1-28-5

l**-*2-7132-44-*

121-14-2

4*4-2*-2

•4-44-2

7**5-72-3

•4-73-7

l**-l*-4534-52-1

•4-3*-4

1*1-55-3

118-74-1

•7-84-S

•$-•!-•

12*-12-7

•4-74-2

2*4-44-*

12*-**-*•1-48-7

*l-»4-l

54-55-3

117-81-7

218-*l-»

117-84-*

2*5-99-2

2*7-*8-9

S*-32-8

193-39-5

53-7*-3

191-24-2

ACENAPHTHENE2,4-OINITROPHENOL . . . .4-NITROPHENOLD1BENZOFURAN2,4-DINITROTOLUENE . . . .2.4-OINITROTOLUENE . . . .

DIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETHERFLUORENE4-NITROANILINE

4.4-OINITRO-2-METHYLPHENOLN-NXTRO&OOXPHENYLANXNE <1>4-BROMOPHENYL-PHENYLETHERHEXACHLOROBENZENE . . . .PENTACHLOROPHENOL . . . .PHENANTHRENEANTHRACENEOX-N-BUTYLPHTHALATE . . .FLUORANTHENEPYRENCBUTYLBENZYLPHTHALATE . . .3,3'-OICHLOROBENZIOINE . .8ENZO(A)ANTHRACENE . . . .BIS<2-ETHYLHEXYL>PHTHALATECHRYSENEOI-N-OCTYL PHTHALATE . . .•ENZO<B)FLUORANTHENE . . .BENZO<K>FLUORANTHENE . . .BENZO<A>PYRENEINOENOM.2. 3-CD>PYRENE . .DIBENZ(A.H)ANTHRACENE . .•ENZO<G.H, DPERYLENE . . .

UG/L1* U

UUU

5*5*1*1*1*1*1*1*5*S*1*1*1*5*1*1*1*1*1*1*2*1*1*1*1*1*1*1*1*1*1*

UUUUUUUU

UUUUUUUUUUUUUUU

U

UUUU

(!) - CANNOT BE SEPARATED FROM DIPHENYLANXNEFORM I

4184 30123

Case No: (IB*!r:.

Organics analysis Data Sheet

(Page 3)

Pesticides/PCBs

•itf'.f *<wl

ND.5*0*701

[Lo»] Hediui (Circle one)

Date Exacted/Prepared: 29-Sep-8?

Date Analy:ed: Ob-Oct-87

Conc/Dil Factor: 1

Percent M:isture;decanted) NR

6PC Cleanup Yes («]-Ko

Separatory Funnel Eitraction Yes

Continuous Liquid-Liquid Eitractior, [:] Yes

CAS [ug/L] or ug/KqNuiber

319-B4-6 Alph»-BHC 0.05 U319-85-7 BeU-BHC 0.05 U319-96-8 Delt»-BHC 0.05 U58-89-9 6a«a-BHC (Lindini) 0.05 U76-44-8 Heptichlor 0.05 U309-00-2 Aldrin 0.05 U1074-57-3 Htptichlor Epoiide . 0.05 U

959-98-8 Endosulfjn I 0.05 U

60-57-1 Ditldrin 0.1 U

72-55-9 4,4'-DDE 0.1 U

72-20-8 Endrin 0.1 U

33213-65-9 Endosulfan II 0.1 U

72-54-8 4,4'-DDB 0.1 U

1-31-07-8 Endosulfin Sulfttc 0.1 U50-29-3 4,4'-DOT 0.1 U72-43-5 Hethoiychlor 0.5 U53494-70-5 Endrin Ifetone 0.1 U57-74-9 Chlordini 0.5 U8001-35-2 Toiiphenc 1 U12674-11-2 Aroclor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U51*69-21-9 Aroclor-1242 0.5 U12672-29-6 Aroclor-1248 0.5 U11097-69-1 Aroclor-1254 1U11096-82-5 Aroclor-1260 1 U

Vi = VoluM of extract injected (ul)Vs = Voluie of uter otricttd (•!)Ms - Htiqht of suple eitracted (9)Vt = Vcluie of total ritract (ul)

Vs = 1000 or Us = Vt 10000 Vi * 3.0

Fori I

4 1 8 4 3 0 1 2 4

Laboraiory Name ETC/Toxicon

..NOOrganics Analysis Data Sheet

(Page 4)


Sample Number

CASNumber Compound NWTM Fraction

Ectim«t«dy*ntT»tion

ug/J or ofl/kg)

i/oAL.

I..

5.

7..

II

W..

33toai n

M65J2L5VO.

!;::= it/o

'*-

in

NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownnrw denotes probable molecular weight

4 1 8 4 3 0 1 2 5

SAMPLE HUM1CRMDLGU948*!


LAB SAMPLE 10 NO: 4184-1*9SAMPLE MATRIX: WATER

DATA RELEASE AUTHORIZED tv.

ORGANICS ANALYSIS DATA SHEET<PAGE 1)

CASE NO:

•C REPORT NO:CONTRACT

41*44184


VOLATILE COMPOUNDS

CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYZED: 14)/«S/87COMC/OIL FACTOR: 1.PERCENT MOISTURE: (NOT DECANTED)

CAS NUHVEI

74-S7-3

74-f3-f7i-»l-47S-60-37»-*t-2

47-44-175 -18-07S-3S-47S-3S-J.!S4-4*-S

47-44-)107-44-278-1J-3

71-SS-4

S4-23-Sl«8-«S-47S-27-4

1

CHLOROMETHANE

•ROMOMETHANC

VINYL CHLORIDECHLOROETHANE

METHVLENE CHLORIDE . . . .ACETONECARION OISULFIOC

1. 1-OICHLOROETHENE . . . .

1.1-OICHLOROETHANE . . . .TRANS-1.2-OICHLOROETHENE .CHLOROFORM

1.2-DICHLOROETHANE . . . .2-tUTANONE1. 1. 1-TRICHLOROETHANE . .

CARION TETRACHLORIOE . . .VINYL ACETATE•ROMODXCHLONOMETHANE . . .

uc111414141

14

1

1

i/L• U> U> U» UI U» U

UUUUUUUUU

1 Ui U

CAS NUHtER

71-D7-S!M41-«2-47f~4»l-A

124-4S-17f-0»-§

71-43-21««41-«1-S110-7S-*

7I-2S-21M-1«-1Sfl-71-4127-11-47T-34-J

1M-M-3

1M-M-7l»»-41-4

l«*-42-S

UO/L1.2-DICHLOROPROPANE . . .

TRANS-l.l-OICHLOROPROENC .TRICHLOROCTHENEDliROMOCHLOROMETHANE . . .1.1,2-TRICHLOROETHANE . .•ENZEMCCIS-1,X-OICHLOROPROPENE .

2-CHLOROETHYLVINYLETHER .•ROMOFORH4-METHYL-2-PCNTANONI . . .2-HCXANOf«TETRACH4.0ROETHENC . . . .1,1.2.2-TETRACHLOROETHANETOLUENECHLOROIENZENCETHYLBENZENE


UUUUUUUUUUUUUUUUUU

U - COMPOUND ANALYZED FOR IUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.


REPORTING CUALIFIERS.FORM I

4 1 8 4 30520


Case No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationut'L

300U

200U

200U

U TnHir^x ft^mpyii^ -^ -f j)y^ fnr t^rt ti« ArtrrtfA P>pn»t ih» minimum A^^tina limit for the tampla wtlh the U

(e.j.lOU) based on oeceisa^ conceatndon/dQntiao actioa. CTbis it not necesurily the imtraman detection limit)The footnote should read: U-Compouad was analyxed for but not detected. The number ii the minimum ttainibledetection limit for the sample.

I Indicates an estimated vatoe. Thii flat bmeddmerittenrtfimaing a concentration for tenadvery identified componndiwhere a 1:1 response is assumed or when me mass spectral data indicated the presence of a oompoond that meets me identi-fication criteria but the result fa le« than the ipecifWd^lectkwli^ 101). If limit of detection isIQpf/Land a concentration of 3ut/Liscalcul«cd.reportasU.

4 1 8 4 3 0 5 2 1

B

LABORATORY NAME:

CASE NO:

ETC/TOXICOH

418ftSAMPLE NUMBER

MDLGWC48*!


<PAGE 2)

SEHXVOLATILE COMPOUNDS

CONCENTRATION: LOW

DATE EXTRACTED/PREPARED: *9/3*/B7DATE ANALYZED: l*/*5/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (DECANTED)

GPC CLEANUP VE5 X NO

SEPARATOftY FUNNEL EXTRACTION YES

CONTINUOUS LIQUID-LIQUID EXTRACTION YES

CAS NUMiER

1*8-95-2 PHENOL

111-44-4 tIS<2-CHLOROETHYL)ETHER .

95-57-8 2-CHLOROPHENOL

541-73-1 i,3-OXCHLOROBENZENE . . .

1*4-44-7 1,4-OXCHLOROBENZENC . . .

l**-5l-4 IENZVL ALCOHOL

95-S*-l 1,2-DXCHLOROBENZENE . . .

9S-4S-7 2-METHYLPHENOL

39438-32-9 BXS<2-CHLOROXSOPROPYL>ETHER

1*4-44-1 4-METHYLPHENOL

421-44-7 N-NITROSO-OI-N-PROPYLAHINE

47-72-1 HEXACHLOROCTHANE

98-9S-3 NITR01ENZENE

78-59-1 ISOPHORONE

88-7S-* 2-NXTROPHEMOL

1*5-47-9 2.4-OIMETHYLPHEHOL . . . .

45-85-* BENZOXC ACXO

111-91-1 IIS<2-CHLOROETHOXY>METHANE

!2*-83-2 2.4-OICHLOROPHENOL . . . .

12*-82-l 1,2,4-TRXCHLOROBENZENE . .

91-2*-3 NAPHTHALENE

1*4-47-8 4-CHLOROANILINE

•7-41-3 HEXACMLOROBUTAOXENE . . .

S9-5*-7 4-CHLORO-3-P1ETHYLPHENOL .

91-57-4 2-METHYLNAPHTHALENE . . .

77-47-4 HEXACHLOROCYCLOPENTAOIENE

88-*4-2 2. 4. 4-TRICHLOROPHENOL . .

95-95-4 2, 4.S-TRICHLOROPHENOL . .

91-58-7 2-CHLORONAPHTHALENE . .

••-74-4 2-NITROAHILXNE

131-11-3 DIMETHYL PHTHALATE . . . .

2*8-94-8 ACENAPHTHYLENE

99-*9-2 3-NXTROANXLXNE

1*

It

UG/L

1* UUU

UUUUU

1* U1* U

1* U1* U

18 U1* U

1* U

1* U5* U1* U1* U

1* U

1* U1* U18 U

1* U1* U1* U1* U5* U

1* U5* U

1* U1* U5* U

CAS NUMBER

83-32-951-28-5

132-44-9121-14-24*4-2*-284-44-27**5-72-384-73-7

534-52-184-3*-41*1-55-3118-74-187-84-585-*l-812*-12-7

84-74-2

2*4-44-*

85-48-7

91-94-1

54-55-3

117-81-7

218-*l-9

117-84-*

2*5-99-2

297-9B-9

5*-32-8193-39-553-7*-3191-24-2

ACENAPHTHENE

2,4-DINITROPHENOL . . . .

4-NXTROPHENOL

OIBENZOFURAM

2,4-DINITROTOLUENE . . . .

2.4-OXNXTROTOLUENE . . . .

OXETHYLPHTHALATE

4-CHLOROPHENYL-PHENYLETHER

FLUORENE

4-NITROANXLINC

4.4-OXNITRO-2-HETHYLPHENOL

N-NXTROSODXPHENYLAHXNE <1>

4-•ROMO PHENYL-PHENYLETHER

HEXACHLOROBENZENE . . . .

PENTACHLOROPHENOL . . . .

PHENANTHRENE

ANTHRACENE

OI-N-BUTYLPHTHALATE . . .

FLUORANTHENE

PYRENE

BUTYLBENZYLPHTHALATE . . .

3. 3'-OICHLOROBENZIOINE . .

BENZO<A)ANTHRACENE . . . .

BIS < 2-ETHYLHEXYL > PHTHALATE

CHRYSENE

DI-N-OCTYL PHTHALATE . . .

BENZO(B)FLUORANTHENE . . .

BENZO<K)FLUORANTHENE . . .

BENZO(A>PYRENE

XNOENO<1.2.3-CD>PYRENE . .

DIBENZ<A.H)ANTHRACENE . .

SENZOCG.H,I>PERYLENE . . .

1*1*5*I*

UU

UG/L

1* U5* U

%• U1* U1* U1* U1* U

uuuu

1*1*1* U5* U1* U1* U1* U1* U1* U1* U2* U1* U1* U1*1*1*1*1*1*1*1*

<1> - CANNOT BE SEPARATED FROM OXPHENYLAHINEFORM X

9 9

i::

Or;anics Analysis Data(Page 3)Pestindes/PCBs

"cncert'aticn: [In] Rediui (Circle oneiDate f.rtra:'.ed.;Fr?pared: 29-5ep-B7'ate Sra;,:ed: 07-Oct-B7Conc'Dil Factor: 1Fer:eit toistureldecanted) NR

6PC Cleanup Yes [i]-MoSecaratory Funnel Ertractio* YesContinuous Liquid-Liquid Extraction [x] Yes

CAS [ug.'L] or ug/KqNuabcr

319-84-4 Alpha-BHC 0.05 U319-B5-7 Btta-BHC 0.05 U319-B6-B BelU-BHC 0.05 U5B-B9-9 6aMi-BHC (Lindane) 0.05 U76-44-8 Heptachlor 0.05 U309-00-2 Aldrin 0.05 U1024-57-3 HepUchlor Epoxide 0.05 U959-9B-B Endosulfan I 0.05 U60-57-1 Bieldr in 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfan II 0.1 U72-54-8 4,4>-ODD 0.1 U1-31-07-fl Endosulfan Sulfate 0.1 U50-29-3 4,4'-DDT 0.1 U72-43-5 Kethoxychlor 0.5 U53494-70-5 Endrin Keton* 0.1 U57-74-9 CMordane 0.5 U8001-35-2 Touphtne 1 U12674-11-2 Aroclor-1016 0.5 U11104-28-2 Arodor-1221 0.5 U

11141-16-5 Arodor-1232 0.5 U53469-21-9 Aroclor-1242 0.5 U

12672-29-6 Aroclor-1248 0.5 U11097-69-1 firoc'.or-1254 1 U11096-82-5 Aroclor-1260 1 U

Vi : Voluie of extract injected (ul)Vs * VoluH of Mter extracted (illKs - Height of saiple extracted (g)Vt * Volute of total extract (ul)

Vs = 1000 or Ms •- Vt = 10000 Vi = 3.0

fori

4 1 8 4 3 G 5 2 3

"_>f J ' -J' r ^ •

-.*> No



CASCompound Nam* Fraction

(ug/yof ug/kg)

1.2.

J.

4.

6.

9..

110..

ai

14..

rhe..17..

i;§,::20..

!«..12..

'":£W.

29

30


4 1 8 4 3 0 5 2 4



SAMPLE MATRIX: HATERDATA RELEASE AUTHORIZED §Y


CASE NO: 4184

BC REPORT NO: 4184CONTRACT NO: O'^ *1DATE SAMPLE RECEIVED.5K*fUs

VOLATILE COMPOUNDS

CONCENTRATION: LOWDATE EXTRACTED/PREPARED.

DATE ANALYZED: i«/*9/87

OIL FACTOR: 5«. •

PERCENT MOISTURE: (NOT DECANTED>PH

CAS NUMBER

74-87-J CHLOROMETHANE74-B3-f BROMOHETHANE

7S-H-4 VINYL CHLORIDE

7S-M-J CHLOROETHANE7S-M-2 HETHYUENE CHLORIDE . . .

47-44-1 ACETONE75-1S-* CARBON DISULFIOE . . . .75-55-4 1.1-OICHLOROETHENE . . .

75-35-3 1.1-OICHLOROETHANE . . .

154-48-S TRANS-1.2-OICHLOROETHCNE47-44-3 CHLOROFORMt«7-«4-2 1.2-OICHLOROETHANE . . .

7«-»3-3 2-8UTANONE71-55-4 i,1.1-TRXCHLOROETHANE .

54-23-5 CARBON TETRACHLORIOE . .l»8-»S-4 VINVL ACETATE75-27-4 BROMOOICHLOROMETHANE . .

UG/L

SM U

U

U

SM U25 • U

SM U

25 • U

25 • U

25 • U

25« U

2S* U

25*

SM

25 •

25 •

SM

25 • U

CAS NUMBER78-87-5 1.2-DICHLOROPROPANE . . .

1M41-42-4 TRANS-1. 3-OICHLOMOPROCNE .

7»-«l-4 TRICHLOROETHENE124-48-1 OIBROMOCHLOROMETHANE . . .

79-««-5 1,1.2-TRICHLOROETHANE . .

71-43-2 BENZENE1*«41-«1-S CIS-1, 3-OICHLOROPROPENE .llt-75-i 2-CHLOROETHYLVINYLETHER .

7S-2S-2 BROMOFORH

1»8-1»-1 4-KETHYL-2-PENTANONE . . .

5*1-78-4 2-HEXANONC127-18-4 TETRACHLOROETHENC . . . .77-34-5 1.1.2.2-TETRACHLOROETHANE1*8-88-3 TOLUENE

l«8-9«-7 CHLOROBENZENEl*«-41-4 ETHYL8ENZENEl»«-«2-S STYRENE

TOTAL XYLENES

UG/L

2St> U2S*

25 •25 •

25 •

254-

25 •

25 •

SM

25*

SM

IS25 •

25*25*

25 •

UUUUUUUUUUUUJU

UUU

J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED

.VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR

THE SAMPLE.


REPORTING BUAL1FIERS.FORM I

4 1 8 4 3 0 2 6 1


Case No: 4184

Sample Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

ConcentrationL.C/L

300U

200U

200U

Tnrtiratflfr compound wa$ analyzed fOf but "** 6ttKlt4L Report tbt tninimntn detection limit for die fatnplg wllb tfaC U(e, j. 10U) based on necessary concentration/dilution action. (Thia is not necessarily the instrument detection limit)The footnote chooki read: U-Compoond wta tnilyred for but not detected. The number is (be minimnm attainabledetection limit for the sample.Infirtff* an yytirmarf vahif Thlt fl«y tf nand rioter wtw-n <»«»Tma»iiig « nnnn<»nfrarinB fnr tMitativriy uJCTtifiad compnnilda

where a 1:1 response is «^"m*«< or wten the mas spectral data iiMratr* the presence of a compound that meets the ideoti-Vtr'nn trlfrii Hit rtr rrmlt h l*itt ftan thf ip^rV^ tfflpr'Vî1itT|h '* fn-xtn Aon ran (g t 1QJ). If limit of detection is10 H«/L and a concentration of 3 ug/L is calculated, report as 3J.

4 1 8 4 3 0 2 6 2

Caê NoSfl"ip!e

"oncentrat'On

Date Exifacte<

Date Analyze*

Conc/Dil Fact

Percent Moisi

CASNumber

108 95-2111-44-4

95-57-8

541-73-1

106-46-7

100-51-6

95-50-1

95-48-7

39638-32-9

106-44-5

621-64-7

67-72-1

9895-3

78-59-1

88-75-5

105-67-9

65-85-0

111-91-1

120-83-2

120-82-1

91-20-3

106-47-8

87-683

59-50-7

91-57-6

77-47-4

88-06-295 95-491-58 788 74-4131-11-3

208 96 899-O9 2

(Lov»Tj Medium (Circle One)

•)/Prp.par*»d

1

or-

Lire (Decant*ri)

uQ/lorug/Kg(Circfe On*

Phenol

DiS<-2-Cnforoetrty»)Ether

2-Chlofophenol1. S-Dicnlorobeniena

1 . 4-Dtcnk>robenzene

Benzyl Alcohol

1. 2-DicNorobeniene

2-M«thyfpN*nolbis(2-chlorotSooropv1)Etrwr

4-MethytphenoiN-Nitro«O-0(-n-PropY<«min«

He (jchloroetftant

Nrtrabvruene

IsopNoron*

2-Nivophenol2. 4-Oim«tt>y1pn«nQl

B«ruoic AcidSiftJ ? f*t\t (- , MI. |)L«™w fc-v 'WOcinOKyp"**' fcaiie2. 4-D«hloroph*nol

1. 2. 4-TrichJofobe'ueneNlpnt^«n«

4-Chlofojnilin*

Heuc torobutaditne

4-Chloro-3-Metr«ytph*nol

2-Mettiylnaphthatene

KecacMorocydopentadicna

2. 4. 6-Trichloropt*nol

2. 4. 5-TncMoropNenol

2-C^>lo'onaphthaiene

2-NitrMnitine

0>Ti«fhy( Phtrvilite

Acenaphthylen*

3 N.voan.l.ne

/Ou./{)&10 uIn**10klOk/nt~{hi/L/QulUlA

tfiiilOuIDuic\*.mu/Q*-

toftin\A.lOu.lOu.(dy,

/n±/flulOiAlUtf-lur*/OjA

$euMIA/On.miA

5m




Separatory Funnel E«traciion QYes


CASNumtw

606-20-2

86-73-7

534.52-1

JS-01-8

3-32-9

1-28-5

00-02-7

32-649

21-14-2

-66-2005-172-3

00-07 •«

6-30-6

01-55-3

18-74-1

7-66-5

20-12-7

W-74-2

206-44X)

29-OOO15-687

11-94-1

>6-55-3

218-01-9

117-84-0

205-99-2

207-08-9

W32-8

19339 5

3703

191-24-2

Acenaphthen*

!. 4-Dirutroph«no<

4-Nitroprtenol)ibenzofuran

:. 4-Qinitroioluerx

0>«thytphth«late

4-CMoroph«nv<-ptony<«th«r

4-Nitroaninn«

og/lofog/Kg(Circto Oo«

Si*

2.£-Oin(troiolu«ne

4. 6-Oinhro-2-M*thylph«(>olN-Nrtr«odip!>er>yUmirv« (1 )

Ptntaehtorophenol

Anthracene

)i-n-Butv<ptiinalaie

Fluoranthcne

3. S'

3enzo(t)Antnracei%e

0>-n-Octy1 Phthalat*

B«nzQ(t»Ftuoranihene8enzo(li|Fluorantr>en«

8«rvro(*)Pyr«ri«

8«nzo(g. h.

lOu.

54 UI/OkHu

SonfOu

JDu

n*

7

4 1 8 4 302^85

A - a ! v s i s O a t a S h el cage :iP e s t i c i d e s / P C B s

"o-'cr'.ri'.i:-: [Lo»] KeJ:ji Circle one! 6PC Cleanup Yes [i]-Ho[it? [-.'.•;:'.;: 'c'?po"i: I'-Sero1 Separator/ Fur.nel Ertraction Yes";•.? «'i',. :E;: !'~-lct-:~ Cor.t;r.jOyS Liq-id-Liq-ii Eitractior. [x] resi:n: [•;! Fac:or: «fer:i-\ PuistLreiiiecar.tei. NR

CAS [ug/L] or ug/Kg

319-84-6 Alphi-BHC 0.25 U319-85-7 BeU-BHC 0.25 U319-86-8 Delti-BHC 0.25 U5E-B9-9 6aiw-BHC (Lindinf) 0.25 U76-44-6 Heptichlor 0.251)309-00-2 Aldrin 0.25 U1024-57-3 HeptacMor Eponde 0.25 U959-98-8 Endosulfin I . 0.25 U60-57-1 Bieidrin 0.5 U72-55-9 4,4'-DDE 0.5 U72-20-8 Endrin 0.5 U33213-65-9 Erdcsulfjn II 0.5 U72-54-8 4,4'-DDD 0.5 U1-31-07-8 Endosulfin Sulfiti 0.5 U50-29-1 4 ,4 ' -DDT 0.5 U72-43-5 Hfthoiychlor 2.5 U53494-70-5 Endrin Ketoni 0.5 U57-74-9 Chlordane 2.5 U8001-35-2 Toupheni 5U12674-11-2 Aroclor-1016 2.5 U11104-28-2 Aroclor-1221 2.5 U11141-16-5 Aroclor-1232 2.5 U53469-21-9 Aroclor-1242 2.5 U12672-29-6 ftrodor-1248 2.5 Ui:C"''-6<'-l f t r c c l o r - 1 2 5 4 5 U11^6-62-5 A r o c l o r - 1 2 6 0 5 U

Vi = Voluw of utrict injected (ul)Vs -- Voluif of vitcr t«trjcted (illMs - Kfight of satple ritrjcted (q)Vt -- Voluw of totil titract (ul)

V5 = 1000 or Ms ' Vt * 50000 Vi = 3.0

fora I

4 1 8 4 3 0 2 6 4

N.imo

No


Sample


CASNumber Compouod Hum* Fraction

Cstirn*t*dH(-»ti<X»ug/Vg)

17

7..

10..

I**..SIH

312/can 60

|,7,

IS..

£:12TL

frUV*

II**2C..

17..

^2_

10 KMT

NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknov/nnrw donotec; probable molecular weight

4 1 8 4 3 0 2 6 5


LAI SAMPLE ID NO: 4184-91

SAMPLE MATRIX: MATER


oftSANicS ANALYSIS DATA SHEET(PAGE 1>

CASE MO 4184

•C REPORT NO: 4184

o -/ o

DATE SAMPLE RECEIVED: 89/29/87

VOLATILE COMPOUNDS

CONCENTRATION: LOU


DATE ANALYZED:OIL FACTOR: SB. •

PERCENT MOISTURE: <NOT DECANTED)

PM

CAS NUMBER

74-i7-l CHLOROMETHANt

74-iJ-» •ROMOHCTHANC

7S-B1-* VINYL CHLORIDE

7S-*»-l CHLOROETHAMC

7S-«f-2 METHYLEMC CHLORIDE . . .

47-44-1 ACETONE7S-H-* CARiON OISULFIDC . . . .

7S-3S-* 1.1-DICHLDROETHENt . . .

7S-1S-1 1.1-OICHLOROETHANC . . .

1S4-4B-S TRANS-1.2-DXCHLOROETHENC

47-44-1 CHLOROFORM

1B7-B4-2 1.2-OICHLOROETHANC . . .

78-*3-l 2-BUTANOHC

71-SS-* 1.1.1-TRICHLOROETHAME .S4-23-S CARIOM TETRACHLORIOC . .

1M-9S-4 VINYL ACETATC

75-27-4 IftOMOOICHLOROMETHAMC . .

2S*

UG/L

SM U

SM U

SM U

U

U

U

U

U

U

U

U

U

U

2S8 U

25 • U

SM U

2S8 U

2S»

21 •

CAS NUMBER

7I-C7-S 1.2-DICHLOROPROPANl . . .l**41-*2-4 TRANS-t.l-OICHLOROPROENC .

79-tl-4 TRICHLOROCTHENC

12«-4t-l OIIROMOCHLOROMETHAMC . . .

7?-M-S 1.1.2-7RICHLOROETHANE . .

71-43-2 BENZENE

1*«41-*1-S CIS-1,1-OICHLOROPROPENE .

ll»-7$-t 2-CHLOROETHYLVINYLETHER .

7S-2S-2 BROMOFDMH

1*S-1«-1 4-METHYL-2-PENTANONC . . .

SY1-7S-4 2-HCXANONE

127-1B-4 TETRACHLOROETHENC . . . .

79-34-S 1.1.2.2-TETRACHLOROETHANE

148-81-3 TOLUENE .,•"

148-t»-7^ CHLOROtENZENC

i«t-4i-*' 'ETHYLIENZENCl*«-42-S STYRENC

TOTAL XYLENE8

2S*25 •

UG/L

2S8 U2S» U

2SB U

U

U

U

U

SM U

2S8 U

SM U

SM U

2St U

SM U

348

2S« U

25* U

2S* U

21* U



THE SAMPLE.


REPORTING QUALIFIERS.

FORM I I'


Tase No: 4184

Sampl* Number


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butyl Alcohol

sec-Butyl Alcohol

Concentrationut/L

300U

200U

200U

TnHirat^t compound wts milyttd for but not df*rtpd Report (he minimum detection limit for the sample with the U(e.i. 10U) based on nectnaryccnxntratic^ctfulknactioa. (This U not necessarily the instrument detection limit)The footnote timid re«k U-Q»mpoond WM tnalyzed for but not detected. Tbe mmber is the minimum ttiuubledetection limit for the cample.Indir*t»i «n »pi-mat>rf wflnf. Thk »<f It in** «*«• «**» pfn'mariin m enncgntratioB for temarivdy identified compopndlwbert a Mrecpoiueiiusamedai•««»me mm q>ectnl dan indicated thepraeaceof • compound thai meets die identi-fkation criteria but the remit bless man the specified detection limit bat greater dan rero (04.10J). If limit of detection is10 \ig/L md a concemmion of 3 W/L it ciloilatrt. report as M.

4 1 8 4 3 0 3 0 0

LABORATORY NAME

CASE NO.ETC/TOXICON418*

SAMPLE NUMBEH

ORGANICS ANALVSIS DATA SHEET(PAGE 2)


CONCENTRATION: LOWDATE EXTRACTED/PREPARED. *9/3*/87DATE ANALYZED: 19/23/07CONC/OIL FACTOR: 1.PERCENT MOISTURE (DECANTED)

GPC CLEANUP VES X NOSEPAftATOftV FUNNEL EXTRACTION YESCONTINUOUS LiaUID-LIBUIO EXTRACTION VES

CAS NUMBER UO/U1*8-95-2 PHENOL 1*111-44-4 BIS<2-CHLOROETHYL)ETHER . 1895-57-8 2-CHLOROPHENOL 1*541-73-1 1.3-OICHLOROBENZENC ... 1*1*4-44-7 1.4-OICHLOROBENZENE ... 19l**-St-4 BENZYL ALCOHOL 1995-58-1 1.2-OICHLOROBENZENE ... 1995-48-7 2-HETHYLPHENOL 1*39438-32-9 BX5<2-CHLOROISOPROPYL)ETHER 1*1*4-44-5 4-METHYLPHENOL 19421-44-7 N-NITROSO-DI-N-PROPYLAMINE 1947-72-1 HEXACHLOROETHANE 1998-95-3 NITROBENZENE 1978-59-1 X50PHOROME 1*88-75-1 2-NITROPHENOC 181*5-47-9 2.4-OIMETHYLPHENOL . . . . 1945-85-4 BENZOIC ACIO 59111-91-1 BIS(2-CHLOROETHOXY)METHANE 1912*-83-2 2.4-OICHLOROPHENOL . . . . 1912*-82-l 1.2.4-TRICHLOROIENZENC . . 1991-29-3 NAPHTHALENE 191*4-47-8 4-CHLOROANILINE 1987-48-3 HEXACHLOROBUTADIENE ... 1959-5*-7 4-CHLORO-3-METHYLPHENOL . 1991-57-4 2-METHYLNAPHTHALENE ... 1977-47-4 HEXACHLOPOCYCLOPENTAOIENE 1988-»4-2 2,4.4-TRICHLOROPHENOL . . 1*9S-95-4 2.4.5-TRICHLOROPHENOL . . 5891-58-7 2-CHLORONAPHTHALENE ... 1988-74-4 2-NITRQANILINE 59131-11-3 DIMETHYL PHTHALATE . . . . 192*8-94-8 ACENAPHTHYLENE 1*99-*9-2 3-NITROANILINE 5*

Uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

CAS NUMBER83-32-951-28-51*9-92-7132-44-9121-14-24*4-2*-284-44-27*95-72-384-73-7199-19-4534-52-184-39-4191-55-3118-74-187-84-S85-91-8129-12-784-74-2294-44-9129-99-985-48-791-94-154-55-3117-81-7218-*l-9117-84-*2*5-99-22*7-*8-959- 32-8193-39-553-78-3191-24-2

ACENAPHTHENE2. 4-DINITROPHENOL . . . .4-NXTROPHENOLDIBENZOFURAN2. 4-DXNITROTOLUENE . . . .2. 4-OINITROTOLUENE . . . .OIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETHERFLUORENC4-NXTROANXLINE4. 4-OINITRO-2-HETHYLPHENOLN-NITROSODIPHENYLAHINE <1>4-BROMOPHENYL-PHENYLETHERHEXACHLOROBENZENE . . . .PENTACHLOROPKENOL . . . .PHENANTHRENEANTHRACENEOI-N-BUTYLPHTHALATE . . .FLUORANTHENEPYRENE8UTVL BENZYL PHTHALATE . . .3-3'-DICHLO»OBENZIOINE . .BENZO<A)ANTHRACENE . . . .BIS < 2-ETHYLHEXYL > PHTHALATECHRYSENEDI-N-OCTYL PHTHALATE . . .BENZO(B)FLUCRANTHENE . . .BENZO<K>FLUORANTHENE . . .BENZO<A> PYRENElNDeNO(1.2. 3-CD)PYRENE . .OIBENZ<A.H> ANTHRACENE . .

8ENZO<O.H. DPERYLENE . . .

UG/l1*585*19191*1*1*1*5959191919591*1*19191919291919191*1*1*1*1*1*19

UUU

uuuuuuuuuuuuuuuuuuuuuuuuuuuuu

<1> - CANNOT BE SEPARATED FROM DIPHENYLAHINEFORM I

4 1 8 4 3 0 3 0 1

V=E S;:

3)Pest iudes/PCBs

[Lo«jDate Ext'«tei/»'f; irei!: :9-;ep-6'

Da1.? Ara' . , :ei : C r - 3 c t - E 7

Conc/Di l f a c t o r : 1

Percent r1ois 'ure!decar, ted! Nft

6PC Cleanup Yes [i]-HoBejaratcry Funnel E»tract;on YesCc~t:".Lj:i5 Liqu;i-L!q.id E x t r a c t i o n Ji] Yes

CA3Nuiber

[ug/L] or

319-64-i Alohi-BHC 0.05 U

319-85-7 Beti-BHC 0.05 U

319-86-8 DelU-BHC 0.05 U

58-S9-9 6ana-BHC (Lindant) 0.05 U7t-«4-B Heptjchlor 0.05 U

309-00-2 Aldrin 0,05 U

1024-57-3 Heptachlor Epoiid* 0.05 U959-9B-8 Endosulfjn I . 0.05 U60-57-1 BiiUrin 0. U72-55-9 4,4'-DDE 0. U72-20-8 Endrin 0. U33213-65-9 Endosulfin II 0. U72-54-B 4,4'-DOD 0. U1-31-07-8 Endosulfin Sulfate 0. U50-29-3 4,4'-DDT 0.1 U72-43-5 Methojychlor 0.5 U53494-70-5 Endrin Kftone 0.1 U57-74-9 Chlordine 0.5 U8001-35-2 Toxaphene 1 U12674-11-2 Aroclor-1016 0.5 U11104-28-2 Aroclor-1721 0.5 U11141-16-5 Aroclor-1232 0.5 U?:469-21-9 Aroclor-1242 0.5 U12=72-29-6 Aroc'.or-1248 0.5 U;::."-t=-l »'ocls'--l?54 1 Uli:°6-3:-5 CrocIar-1260 1 U

Vi : Volaie of eitract injected l u l lVs * Volute of »ater extracted (il)(Ts - Veiqdt of sjiple extracted (q)Vt = Voluie of total eitract lull

Vs = 1000 or Us Vt = 10000 Vi * 3.0

For* 1

4 1 8 4 3 0 3 0 2

Laboraio.y Name ETC/Toxj con

Case NoSample Number



CASNumber Compound N«m* Fr»ct*on

E«tim«t*dOC*ntntion

(yfl/yof ug/fcg)

MOP

4.

6.

9..

1O._

m9W3Ly/9/4

15.

16..

17.-

18..

19..

20..

21. -

22..

24..

25..

26..

27..

28..

30..

I/OV /CO

NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmu denotes probable molecular weight

4^84 50305

"-"6ES

LABORATORY NAME: ETC/TOXICONLAB SAMPLE 10 NO: 4184-184SAMPLE MATRIX: WATERDATA RELEASE AUTHORIZED BY:

4184

4184

ORGANICS ANALYSIS DATA SHEET<PACE 1)

CASE NO:AC REPORT NO:CONTRACT NO:DATE SAMPLE RECEIVED:

VOLATILE COMPOUNDS

89/29/87

CONCENTRATION. LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: 18/83/87CONC/DIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)

PH

CAS NUHiER

74-87-1 CHLOROMETHANC

74-83-9 BROHOHETHANE

75-81-* VINYL CHLORIDE


75-89-2 HETHYLENE CHLORIOC . . .

47-44-1 ACETONE7S-1S-8 CARBON OISULFIOE . . . .7S-3S-4 I,l-OICHLOROETHENC . . .7S-3S-3 1.1-DICHLOROCTHANE . . .1S4-48-S TRANS-1.2-OICHLOROETHENE47-44-3 CHLOROFORM187-84-2 1,2-OICMLOROCTHAMC . . .78-93-3 2-BUTANONE71-IS-4 1.1.1-TRICHXOROETHAMC .S4-23-S CARiON TETRACHLORIOE . .188-85-4 VINYL ACETATE71-27-4 BROMOOICHLOROnETHAME . .

UG/L18 U18 U18 U18 U2 J18 U

1

UUUUUU40UU

18 Uf U

CAS NUMBER78-87-S18841-82-479-81-4124-48-179-88-S71-43-21*861-81-5118-71-87S-2S-2188-18-1591-78-*127-18-479-34-S188-88-3188-98-7188-41-4188-42-5

UO/L1.2-OXCHLOROPROPANE . . .TRANS-1. 3-OICHLOROPROENE .TRICHLOROETHENCOIIROMOCHLOROHETHANE . . .1. 1,2-TRZCHLOROETHANC . .BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORH4-METHYL-2-PENTANONE . . .

2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRAC HLO ROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES

18t18

18

S18

UUUUUUUUUUUUUJUUUU

• - COMPOUND WAS DETECTED IN THE 8C BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED



FORK I

4184 30404


Case No: 4184

Sample Numb«r


CAS Number

67-63-0

71-36-3

78-92-2

Compound Name

Isopropyl Alcohol

N-Butjl Alcohol

sec-Butyl Alcohol

ConcentrationHt/L

300U

200U

200U

U Indicates compound was analyzed for but not dftKlfiT Report the minimum detection limit for the i"np>* with the U(e.{. 10U) based on neceaary concentndoo/dOntioa actioa (This is not necessarily the instrument detection limit)The footnote thmiM read: U-Compound was analyzed for but not 4r<»ctfd. The number u the minimum attainabledetection limit fox me sample,

J TndK-^tff m »«rim«t«4 value. This flat 1s used cither when f^timtting a concentration for tentatively identified compoundswhere a 1:1 n»«pn«tf> t* *nm»^ & «&*» (hi» m*^ «p«etni A*t* imtu-^f^ (be presence of a compound that meets the identi-fication criteria but me result is lea than me sfjedfied detectkxi limit but greater flian zero (e^. 101). If limit of detection U10 \if/L and a coocentntkio of 3 tig/L U caloilarcd, report as 3J.

4 1 8 4 3 0 4 0 5

Caie No

Concentration (Low) Medium

Date Exacted 'Prepared L

Date Analyzed (C|6 / fr"?

Cone/Oil Factor

Organics Analysis Data Sh.(Page 2)

Semi volatile Compounds

(Circle One)

iPercent Moisture (Decanted).

CASNumtor

ug/lorug/Kg(CirctoOrw)

108 95-2111-44-4

95 57-8541-73-1106-46-7

100-51-695-50-195-48-7

3963832-9106-44-5621-64-7

67-72-19895-3

76-59-188-75-5105-67-9

65-85-0

111-91-1120-83-2120-82-191-20-3106-47-887-68 35950-791-57-677-47-4

88-06-29595-4

91-58-788-74-4

131-11-320896 B99-09 2

•henol

b«s(- 2 -Chloro«th vHEther2-Chloiophenol1. 3-0«chlorob«nzene

1. 4-DichtorobenteneBenzyl Alcohol1 . 2-0«chloroberuene

2-Mcthyfprwnolbis(2 -Chlofoisooropy1)£lh«r

4-Mclhy<phenotN-Nitro»0-Oi-n-Propy<«mir»e

HeuchforoethancMarobenzencIsopnoron*

2-Nnrophenol2. 4-Dim«thv10h«nolBemoic Acidbis( 2 -Chloro*thory1M«th«n«2. 4-0<hloroph«no(

V 2. 4-Tfich»<xob«'vi«r»eNdpht^t«r»€

4-ChlO'O«nilio«

He «*cM(xobut«Jt«fte

4 -Chlof o-3 Mathylphertol2-M*ttiyl naphthaleneHe K*chlorocyclooent«d«ttnt2. 4. 6-Trichlorophenol

2. 4. 5-Trtch(orOf>Neno(2 -Chlororxaphthal«ne2-Ni(ro«nilir%eDimethyl Phthatate

Acenaphttiylerx3-Nitfoarnline

IGu./flk10 uIn*.10k10k.(nt~inu.iQuIDuiIftulOu[Ou1C*.IfluIQb-

WftIHm.Wi^/Ou.ID*in±lf)H((M(Ot*-\U^/Ok

r*u(Ou

J*M

lOi*.ffilA

5 HA.

GPCC

Sep.v

Con;

CASNumber

83-32-951-28-5100-02-7132-649121-14-2

K06-20-2[84-66-27005-72-386-73-7

100-01-6534-52-186-30-6101-55-3118-74-1

B7-86-585-01-8120-12-7

184-74.2

1206-44-0|l 29 -00-0JBS-687J9 1-94-1

B6-55-31117-81-7

121 8-01 -9111 7-84 -0205-99 2

207 -06 9>0-32 8193 39 553-70 3191-24 :

A^;

-

-

*~,

£ -i

Fl.

f

4

V

t

H;

0.

,-x.

-.

"

•

-

i"

_r

•~

,

(

1:_l

Kg

(1)

Analysis Data SheetIFage I)Pesticides/PCBs

Date Ara'.y:e!J: 07-Oct-B7Conc/Dil Factor:

:-5?:-67

1HP.

6PC Cleanuc Ves [«I-NOSeparatory F-nne! Extraction VesContinuous Liquid-Liquii! Extraction [i] Yts

CAS [ug/L] or ug/KgNdiber

Il«!-B4-i ftlphi-IHC 0.05 U!:'-85-7 Beta-BHC 0.05 U319-B6-B Delta-BHC 0.05 U58-89-9 6)iia-BHC (Undine) 0.05 U76-M-B HepUchlor 0.05 U309-00-2 Aidnn 0.05 U1024-57-3 Heptachlor Epoxidf • 0.05 U959-98-8 Endosulfift I 0.05 U60-57-1 Diildrin 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfin II 0.1 U72-54-6 4,4'-BDJ 0.1 U1-31-07-8 Endosulfm Sulfit* 0.1 U50-29-3 4 ,4 ' -ODT 0.1 U72-43-5 Hethoxrchlor 0.5 U53494-70-5 Endrin Keton* 0.1 U57-74-9 Chlord»n» 0.5 UB001-35-2 Touphtne 1 U12674-11-2 Arodor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0,5 U?:»6"-21-9 Aroc lor -1242 0.5 U1:672-29-6 «roclor-1248 0.51)11097-69-1 Aroclor-1254 ID11096-32-5 Aroclor-1260 1U

Vi = Voluic of titract injected (ul)Vt = Voluie of Mtcr extracted dl)Us = Height of saiple ((traded (g)Vt ; Volute of total ex t rac t (ul)

Vs - 1COO or Us = Vt = 10000 Vi = 3.0

Fort i

4 1 3 4 3 0 4 0 7

Laboiato-y N J " • • _ .

e N o



Sample

CASCornpourwJ NirrM Fraction

Eitirn«l«dtntionog/kfl)

1. MA

B-

1-

0-

51S611

3. • (Ur tJloWt^ Jl-O^C - 13is _s_17..

10

91

r'2C.

27.

30


4 1 8 4 3 0 4 0 8

ATTACHMENT B

MASTER DISPOSAL SERVICE LANDFILL

PARTIAL ANALYTICAL DATA PACKAGE

INORGANIC COMPOUNDS AND CONVENTIONAL PARAMETERS

f o r m 1

INORGANIC ANALYSIS UAYA

ETC/Toxicon

|EHA Sample N o . _ J

I " I( /MPt-frvJQ icei (

uate OCT 3 0 1987

so.sow NO. 785

LAb SAMPLE It). NO.

Lab Keceipt Uate

QC REPORT NO.

Elements Identified and Measured

Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

Cbncatcatkn FlagDOiJdan Msthad Cbrcentcatknr «g/kg dry weight (Circle One)

r>iii»Hnn Mtthad

1. Aluminum C9tTl

'{.. Antimony H-,0 U

3. Arsenic 0 .3/9 U

4. Barium f/fSl

S. tferylliua /.^W

b. Cadmium f8C/

7. Calcium ^7f/00

«. Chromium f7.3l

V. Cobalt *f.2U

10. Copper TS.tn

11. Iron ^1O

12. Lead /,3 U

A/

A)

— -

£

£

pFF

P

P

?>P

P

p

P

P

p

14.

15.

16.

17.

Ib.

19.

20.

21.

22.

23.

Magnesium 374>00

Manganese 9Z

hsrcury. O.7.U

Nickel f/fl

Potassium bVZO

Selenium A// tJ

Silver .- jZ.Vt/

Sodium 3SVOO

Thalliua #&/£/

Vanadium [&/1

Zinc D 21

ft

A//^

^

P

P

P

P

F

P

P

Fp

E

Precent Solids U)

Cyanide

Footnotes: For reporting results to tPA, standard result qualifiers are used. as defined on Cover Page. Additional flags or footnotes explaining

results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

Coaoent/t: Water:ColorationArtifact(s):None

Lab Manager

4184 6C03057/M/Fl/W

Date OCT 3 0 W7

ETC/Toxicon

iMOKCAMC A.'AL'lilS UA'IA SMtt'l

CASt NO.

SOU NO. 785LAb SAMPLE II). NO.

Lab Keccipt liate 7 ' 2.1' &'/

QC REPORT NO.

tlecnents Idencified and Measured

Concent cat ion:

Matr ix : Water

Low

Soil

Medium

Sludge Other

Concentration Fl^> DLLJrim rfethodiag/kg dry weight (Circle One)

H.

U.

1. Aluminum

2. Antimony

J. Arsenic

H. bariun

5. tierylliua

b. Cadmium

7. Calcium

b. Chrooiium

V. Cobalt

10. Copper

11. Iron fao}

12. Lead

P

F

F

P

P

F

P

P

P

p

P

F

17.

Ib.

22.

2J.

Precenc Solids (1)

Cyanide

Magnesium

Manganese

f-tercury

Nickel

Potassiua

Selcniua

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Foocnoces: For report ing results to tPA, standard result q u a l i f i e r s arc usedas defined on Cover Pafce. Addit ional flags or footnotes explainingresults are encouraged. Def in i t ion of such f lags must be explicitand contained on Cover Cage, however.

Comoeots: Water :Coloration C oi.oK.Lfa Clarity

Artifact(s):None

THIS 7?fSt/iT SHetT is fo*. IRON

Lab Manager

57 /M/F1 /W

4 1 8 4 6 0 0 6 7

; a-, i

INORGANIC ANALYSIS JMVAETC/Toxicon

\ f - f f , Sample N o .

uate °CT 3 0 1987

CASE: NO.sou NO. 785

UU» SAMPLE ID. NO. - JflZ

Lab Receipt Uace

QC REPORT NO.


Concent ration:

Matrix: Water

Low

Soil

Medium

Sludge Other

Qrca *J Hrinn Fl^g DQudai tfettal Oi i vt 11 «Hor> Pl^g TMVi<-lon HîrHr mg/kg dry weight (Circle One)

I. Aluminum Ll^

2. Anciotony U, f f^

3. Arsenic ftffit/

4. Barium f^S]

5. Beryllium f.CU

b. Cadmium ?.&(J

?. Calcium 26>ZOO

«. Chromium Tfc.?!

9. Cobalt <i.2(J

10. Copper ZMi>

11. Iron f^^l

12. Lead A<3 6/

/V

A/

^^

z

pFP

P

P

frP

P

P

P

P

r

1*.

16.

17.

20.

21.

22.

23.

Magnesium 23OOO

Manganese £l3]

Hercury O-2.0

Nickel f/97

Potassium T2S^6\

Selenium I.Jlt/

Silver . ^.^f

Sodium 2.OOOO

Thallium 0.4 /£/

Vanadium /~3.3~1

Zinc r/2l

fit

fit

/Q

Z,

pp

ppF

P

P

F

PP

Precenc Solid* (Z)Cyanide

Footnotes: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or footnotes explaining


Comaents: Water:ColorationArtifact(s):Nbne

Lab Manager

4184 6003157/M/Fl/W

Lr'A

Uace OCT 3 0 1987

ANALYSIS IM'IAETC/Toxicon CASK NO.

sou NO. 785LAb SAMPLE 10. NO. 4/8*+ "

Lab Receipt Uace

QC REPORT HO.

~ g7

blements Identif ied and Measured

Concent cation:

Matrix: Uacer

Cyanide

Low

Soil

Medium

SLodge Other

Pag

1 . Aluminum

2. Antimony

1). Arsenic

H. barium

5. terylliuo

6. Cadmium

7. Calcium

6. Chromium

V. Cobalt

10. Copper

11. Iron £J7ff]

12. Lead

P

FF

P

P

F

P

P

P

P

P

F

Obnoenttatiai Flag EdJuticn Vettedng/kg dry ueighc (Circle One)

U.

14.

10.

17.

Ib.

IV.

2u.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Potassiuo

Selcniua

Silver

Sodium

Thalliua

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids _(_*)_

Foocnoces: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Uefinitioa of such flags must be explicitadd contained on Cover Cage, however.

Comoents: Water: Coloration ClarityArtifact(s):None

THIS 7?gSl/tT SHetT is fo* J/?OA/

Lab Manager

57/K/Fl/ lv

4 1 8 4 6 0 0 6 S

J L H A b^-p No.

ETC/Toxicon

suu NO. 785

LAb SAMPLE ID. NO.

3Ze/

Date OCT 2 Q 1987

A.«ALY:>IS DA'M 6Ht.fl

CASE NO.

Lab Keccipt Uate

QC REPORT NO.

-f 7

-40

blements Identified and Measured

Concentration:

Matrix: Water

Cbroe

Low

Soil

Medium

Sludge Other

1.

*..

J.

6.

7.

0.

10.

11.

12.

Aluminum

Antimony

Arsenic A

barium

Beryllium

Cadmium

Calcium

Chromium

Co bale

Copper

Iron

Lead V,

T I S6\U,ff(Ji&ffUr/33j

LOU

t-.zolelZOO

SMU¥.2U

E9.Z]L3& '3 U A/

jL%

Z

pFF

P

P

P

P

P

Pp

P

F

Figg niiii-im {feted Cbnoertcatdm Flag rn'ii*-jm tfetfod«£/kg dry weight (Circle One)

U.

14.

I*.

10.

17.

Ib.

21.

22.

23.

Magnesium \~Si]

Manganese L V. Oj

hercury Q. Zl)

Nickel 13 U

Potassium J?6Y000

Selenium I.UU

Silver 2.*+U

Sodium I 95" OOO

Thallium ^.^/^

Vanadium L$«OJ

Zinc T9. 57

NV ^

^

pp

ppF

P

P

F

PP

Precenc Solids (2)

Cyanide

Footnotes: For reporting results to tPA, standard result qual i f iers arc usedas defined on Cover Pa&e. Additional flags or footnotes explainingresults are encouraged. Definition of such flags must 'be explicitand contained on Cover Page, however.

Water:ColorationArtifact(s):None

Lab Manager

4 1 8 4 6 C 0 3 85 7 / M / F l / W /

I Lr'A '. in t> ].- s > . |

Date OCT 3 0 1987

INORGANIC A-tALtsis UA'IA sutt'i

ETC/Toxicon CASK NO.

sow NO. 785

LAb SAMPLE 10. NO. 418 I' HQ_

Lab Keccipt Uace

QC REPORT NO.

tletnents Ident i f ied and Measured

Concentration:

Matrix: Water

Lou

Soil

Medium

Sludge Other

Gbncentcaticn Flag KJuticn hfethod OoncBntiatianXjg/lXor rag/leg dry weight (Circle Oa«)

Dilnrim

1 . Aluminum

2. Antimony

J. Arsenic

H. Barium

5. beryllluo

to. Cadmium

7. Calcium

(5. Chromium

9. Cobalt

10. Copper

11. Iron ££#!

12. Lead

P

F

F

P

P

F

P

P

p

P

P

r

16.

17.

16.

IV.

20.

21.

22.

Magnesium

Manganese

hercury

Nickel

Potassiuo

Selcniua

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precenc Solids (2)

Cyanide

Footnotes: For report ing results to tPA, standard result qua l i f i e r s arc used. as defined on Cover Page. Additional flags or footnotes explaining

results are encouraged. Definit ion of such flags muse be explicitand contained on Cover Page, however.

«: Water:Coloration CoLo/tLess Clarity CLEARArtifact(s):None

THIS 'RESULT SHetT is fo* D/ssoivfP XRou OtiLY .

Lab Manager

5 7 / M / F l / W

4 1 8 4 6 0 0 7 5

^ o r r. I

INORGANIC ANALYSIS UA'IA

ETC/Toxicon

Sample No.

uate OCT 3 0 1987

CASE NO.

785sou NO.LAb SAMPLE ID. NO.

Lab Keceipt liate <?-2<?-g7

QC REPORT NO.


Concentration:

Matrix: Water

Low

Soil

Median

Sludfce Other

1.'L.

3.

M .

5.

6.

7.

«.

10.

L I .

12.

Aluminum

Antimony

Arsenic t

Barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead /.

r\is~]&.6U

HflI.OU

8.ZIS300O

lS

Ciulrs.n

IZZOO

tu

A/

A/

%,x

J$

pF

F

P

P/p

P

P

P

P

P

F

g / o r ing/kg dry weight (Circle One)

13.

14.

it).

L7.

Ib.

19.

21.

22.

23.

Precent Solids (I)

Cyanide

Magnesium I2.(,000

Manganese 2. 1^

ftercury O.7.0

Nickel ;3?

Potassium (o^30O

Selenium /,/ft/

Silver 2.^1)

Sodium 2Z100O

Tha 1 1 ium 0. *?/ L/

Vanadium (".231

Zinc 22

A/A/

/£?

/^

^

P

P

P

P

F

P

P

F

PE

Footnotes: For reporting results to tPA, standard result qual i f iers arc used. as defined on Cover Page. Additional f lags or footnotes explaining


Comoentc: Water : Coloration ClarityArtifact(s):None

Lab Manager

4 1 8 4 6 C 0 2 45 7 / M / F l / W

Uate OCT 3 0 1<W7

LAK

SOU NO.

ETC/Toxicon

IMORCAMO A N A L Y S I S UA'lA ilit.fl

CASt NO.

785

LAb SAMPLt ID. NO. - 95*

Lab Keccipt Uate

0^; REPORT NO.


Concentration:

Matrix: Water

Cyanide

Low

Soil

Medium

Sludge Other

Mttrrf Oonoentratim Flqg DUiAian Msdrdrag/kg dry weight (Circle One)

I . Aluminum

'i. Antimony

J. Arsenic

H. barium

5. beryllium

b. Cadmium

7. Calcium

b. Chromium

*. Cobalt

10. Copper

11. Iron Ml

12. Lead

P

F

F

P

P

F

P

P

p

P

P

F

14.

13.

10.

17.

lt>.

19.

20.

21.

22.

23.

Magnesium

Manganese

Mercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids (2)

Footnotes: For reporting results to tPA, standard result qualif iers arc used. as defined on Cover Pa&e. Addit ional flags or footnotes explaining

results are encouraged. Def ini t ion of such f lags must be explicitand contained on Cover Cage, however.

Comoents: WaterrColoration LititTBKovJtJ Clarity CLEARArtifact(s):None _

THIS "ResuLT SHctT is fo*. "5/ssotvtD Jô/v

Lab Manager

57/M/F1/W

4 1 8 4 6 0 0 6 1

Korm 1

ANALYSIS IMVA

LAt

sou no

ETC/Toxicon

Sample No.

uace OCT 3 0 1987

CASE NO.785

LAb SAMPLE ID. NO.

Lab Receipt tiate 9

QC REPORT NO. V//V

bile men cs Identified and Measured

Concentration:

Matrix: Water

Low

Soil

HediuB

Sludge Other

uimi-fnnm

1. Aluminum frl^f]2. Antimony/^. /? L/J

J. Arsenic Oj-,1/)

*-• barium £lOT$

5. Beryllluo /.OU

6. Cadmium */.8U

7. Calciua V34>OO

8. Chroaium £".4U

9. Cobalt V.2U

10. Copper Df.8]

11. Iron T?/7

12. Lead /,$ U

rjagL

^

A/

/v

B iinm jTlNor

2x

2,

2.

"nmrq umDanttanonitg/kg dry weight (Circle One)

p" 13. Magnesium 2. f^flO

F U. Manganese fjfl

F is. Hercury O.7.0

P 16. Nickel C/7l

P 17. PotassiuQr3340l

>F"P 16. Selcniua 1 .& I/

P IV. Silver . 2MU

P 20. Sodlua /380O

p 21. Thalliua 0 ,<f/ U

p 22. Vanadlu« E9.^

P 2J. Zloc fg.O]

nagu

(J

^

iiinm

/^7

^

Ml IXl

P

P

P

P

F

P

P

F

PE

F Precent Solids (I)Cyanide

Footnotes: For reporting results Co tPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or footnotes explaining


Comoeats: Water;ColorationArtifact(s):None

Lab Manager

4 1 8 4 6 C 0 2 S5 7 / K / F l / U

\ t f A j .1 •-., • 1

Uace OCT 3 0 1987

LAK :.A:IL

sou NO.

ETC/Toxlcon

ANALYSIS UAYA SHt.fl

CASK NO.

783LAb SAMPLt 10. NO.

Lab Keccipc Date

QC REPORT NO.


Concent cue ion:

Matrix: Water

Low

Soil

Medium

Sludge Other

Conoertrariai Flag Dilirim hfetfrd CbnoerTrarim Flag Dilirim MsthxiXig/L\or ng/kg dry weight (Circle One)

1 . Aluminum

2. Antimony

J. Arsenic

H. barium

5. tierylliua

b. Cadmium

7. Calcium

«. Chromium

<*. Cobalt

10. Copper

tl. Iron £?3l

12. Lead

P

F

F

P

P

F

P

P

p

P

P

F

13.

U.

I*.

16.

17.

Ib.

iy.2u.

21.

22.

2U.

Magnesium

Manganese

hercury

Nickel

Potassiua

Selcniuo

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids (Z)

Cyanide

Foocnoces: For reporting results to tPA, standard result qualif iers arc used. as defined on Cover Page. Addit ional flags or footnotes explaining


Coauae.its: Water: Coloration Coto*lf*s ClarityArtifact(s):None

THIS SHctT iS fo* J/?o/v OtJLY

Lab Manager

57 /M/F l /W

4 1 8 * 6 0 0 6 2

tr'A jaraji !»•

Oate OCT 3 0 1987

I

LAt

SOU NO.

EIC/Toxicon

ANALYSIS U A i A illt.fl

CASE NO.

785

LAb SAMPLE 10. NO.

Lab Kecelpt liate

QC REPORT NO.

tie a>ents Identified and Measured

Concentration:

Matrix: Water

tow

Soil

Medium

Sludge Other

Cbnootzation Fl g DUi±Jm hfethod Cbncentxatim FJflg Dilution£ug/C)or mg/kg dry weight (Circle One)

i.i.3.

H.

5.

to.

7.

(5.

<*.

10.

11.

12.

Aluminum T/ £"67

Antimony /J.J9 0

Arsenic /^

harlum f/907

Beryllium 100

Cadmium 4.8 U

Calcium 380 OQ

Chromium [8. Li

Cobalt T5.27

Copper T7.V7

Iron 3O^7

Lead L3U A/

^

^

^

PFF

P

P

P

P

P

p

P

P

F

13. Magnesium yoS~OO

14. Manganese 2. 1

15. Kercury O-20

lb. Nickel fiZffJ

17. Potasstuo 03lOl

lt>. Selenluo J ,& U

IV. Silver [2.11

2o. Sodium / Z9OO

21. Thallium ^^//y

22. Vanadium T9. 77

23. Zinc f / /7

A/A/

JL*

7^

PP

PPF

P

P

F

PP

Precent Solids (t)

Cyanide

Footnotes: For reporting results to tPA, standard result qua l i f ie r* arc usedas defined on Cover Page. Additional flags or footnotes explaining

' results are encouraged. Definition of sucU flags must"be explicitand contained on Cover Cage, however.

Comoeuts: Water;Coloration ClaritvArtifact(s):None

Lab Manager

4 1 8 4 6 C 0 4 057/M/Fl/W/

Uace OCT 3 0 1987

LAt

SOU NO.

ETC/Toxicon

INOKCAMC Ai iALtSLS UA'iA iHt.E'1

CASE NO.

785

LAb SAMPLE 10. NO. - //Z

Lab Receipt Dace 9 -

QC REPORT NO.

hllements Identified and Measured

DiSS

Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

FT^g Dilirim tfethod Cbn

1 . Aluminum

2, Antimony

J. Arsenic

<4 . barium

5. beryllium

6. Cadmium

7. Calcium

H. Chromium

V. Cobalt

10. Copper

11. Iron £$2]

12. Lead

P

F

F

P

P

F

P

P

P

P

P

F

•fixation Flgg Edluticn Ffethaing/kg dry weight (Circle One)

13.

14.

10.

17.

16.

21.

22.

21.

Magnesium

Manganese

hercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids (I)

Cyanide

Foocnoces: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Pa&e. Additional flags or tootnotes explaining


Comoe.\t«: Water: Coloration CoLo*.i-eis Clarity

Artif act (s): None

THIS 7?CSt/t.T SHctT iS fo* "D/sson/fP jT/?Q/v

Lab Manager

57 /M/F1 /W

4 1 8 4 6 0 0 7 7

toro 1

INORGANIC ANALYSIS DATAEDC/Toxicon

( E P A Saople No. |I " I

vJ03(oO< I

^ôate 0 0 7 3 0 1 9 8 7

NO. Ji/il.SOW NO. 785

LAb SAMPLE 10. NO.

Ub Kecelpt Date 9-,29-g?

QC REPORT NO.


Coo cent radon:

Matrix: Water

Low

Soil

Medium

Sludge Other

1. Aluminum L^fl

2. Antimony V-OU

3. Arsenic O.ÔU1* "

i. Barium l$3J

S. Beryllium 1.00

6. Cadmium 4»8U

7. Calcium dfftfCC

tf. Chromium •5".tfU

9. Cobalt V-.2U

10. Copper TV. 61

11. Iron //^

12. Lead /. 3 U

1

A/

-.,/\/

Mor

2Z

2

mg/kg dry weight (Circle One)

p • 13. Magnesium 2/¥OO

F • 14. Manganese ClO]

F 15. Mercury O.2U

p i6. Nickel r/<riP 17. Potassium TdZOOl

/*P lt>. Selenium / .Û

P 19. Silver J2/fU^

P 2O. Sodium* - IbffGO

p 21. Thallium O-9JU

p 22. Vanadium TV.6]

P 23. Zinc rS8l

p Preceat Solids (Z)

A/

^

10

Z

pp

ppF

P

P

F

PE

Cyanide

Footnotes: For reporting results Co tPA, standard result qualifiers are uced. as defined oo Cover Page. Additional flags or footnotes explaining


Consents: Water: Coloration ClarltvArtifact(8):Ndne

4 1 8 4 6 C 0 : 8

Dace OCT 3 0 1987

INORGANIC ANALYSIS DAI A

LAE ETC/Toxicon

NO. 785LAb SAMPLE ID. NO.

CASK NO.

Lab Receipt liate i ~ ~ -

QC R£PORT NO.

Elements Idencified and Measured

1>ISS

Concent ration:

Matrix: Water

Low

Soil

[•tedium

Sludge Other

Grcentratjm Flag rHIm-im hfedtdXig/lNor mg/kg dry weight (Circle One)

Dilitlcn Mstitxl

1. Aluminum

2. Antimony

3. Arsenic

<< . barium

3. tterylliuo

6. Cadmium

7. Calcium

8. Chromium

1. Cobalt

10. Copper

11. Iron f^5l

12. Lead

pF

F

P

P

F

P

P

P

P

P

F

13.

14.

li.

lo.

17.

20.

21.

22.

2J.

Magnesium

Manganese

tercury

Nickel

Potassiua

Selcniua

Sliver

Sodium

Thalllua

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precenc Solids (Z)

Cyanide

Footnotes: For reporting results Co tPA, standard result qual i f iers arc used. as defined on Cover Pa&e. Addi t ional f lags or footnotes explaining

results are encouraged. Defini t ion of such f lags oust be explicitand contained on Cover Page, however.

Coroeoc*: Water: Coloration C»Lo*Leu. ClarityÂrtifact(s):None

THIS 7?fStAT SHeiT is fo* ZRou

Lab Manager

57/M/F1/W

4 1 8 4 6 0 0 6 5

I- u r p.

( E r ' A Sample No. |

I ' I

Oace OCT 2 0 1987

LAfc r

SOU NO

I MORGAN 1C ANALYSIS UA'lA S*

ETC/Toxicon CASE NO.

785

LAb SAMPLE ID. NO.

Lab Ueceipt liace

QC REPORT NO.

Clements Identified and Measured

Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

QmaAxaUai Flag DilUJm tfethri OmatxaUm Flag DUitlcn Mattedig/lXor ng/kg dry weight (Circle One)

£ •

2.

3.

5.

6.

7.

».

10.

L I .

12.

p_ -nAluminum L a l J

Antimony fr.ff 0

Arsenic 0 .fo U

Barium f/Ofl

tie ry Ilium /.Of

CadBium 4 8ll

Calcium 29100

Chrooium S-'fl'

Cobalt 4.20

Copper f"3.n

Iron C?tf

Lead /,J ^/

V

A/

^~^

X2,

2,

pFF

PPj*fp

P

Ppp

P

f

13.

U.

13.

16.

17.

Ib.

2u.

21.

22.

23.

Magnesium 23700

Manganese f?.fl

Mercury. O.2.O

Nickel /3U

Potassiua fZ990l

Selenium /// Z/

Silver ... 2.4f

Sodium ILOOO

Thallium 0.4 JtJ

Vanadium £6>.7l

Zinc 4.8U

A///^

jL

PP

PPFP

P

Fp

B

Precenc Solids (I)

Cyanide

Footnotes: For reporting results Co tPA, standard result qualifiers arc usedas defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of such flags mist be explicitand contained on Cover Vage, however.

Contents:

Artifact(s):None

Lab Manager

4 1 8 4 6002957/M/Fl/W

uace OCT 3 0 1987INORGANIC A N A L Y S I S UAYA 6itt.fi


SOI. NO. 785

LAb SAMPLE 10. NO. - I

Lab Receipt Date

QC REPORT NO.

tlaments Ident i f ied and Measured

Concentration:

Matrix: Water

Low Medium

Soil Other

fl »•*«• raHm T>i1i<-im M^ttrj Cbmerttatiai Flqg Dili±ian bfethod«g/kg dry weight (Circle One)

1 . Aluminum

2. Antimony

3. Arsenic

H. barium

5. tterylliun

b. Cadmium

7. Calcium

ti . Chromium

V. Cobalt

10. Copper

11. Iron r/5l

12. Lead

p

F

F

P

P

F

P

P

p

P

P

F

Ib.

17.

16.

21.

Magnesium

Manganese

hercury

Nickel

PotassiuD

Seleniuo

Silver

Sodium

Thalliua

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Freceac Solids (2)

Cyanide

Footnotes: For reporting results to tPA, standard result qua l i f i e r s arc used. as defined on Cover Page. Additional flags or footnotes explaining

results are encouraged. Defini t ion of such flags muse be explicitand contained on Cover Cage, however.

Comoeocs: Water: Coloration C.cLoAt.eii ClarityArtif act (s): None

THIS SHctT is fo* DISSOLVCD

Lab Manager

57/M/F1/W

4 1 8 4 6 0 0 6 6

N o .

Uate OCT 3 0 19g/_

LAt ETC/Toxicon

J A.iALYilS UA'lA bhbtl

CASE NO.

NO. 785

LAb SAMPLE 10. NO.

Lab Keceipt Uace

QC REPORT NO.

Concent rat ion:

Matrix: Water

Cbn

t laments Identified and Measured

Low

Soil

Medium

Sludge Other

1. Aluminum / l<?2j

'L. Antimony fa.,01)

3. Arsenic O.^ff U

H. barium ISO]

5. beryllium ).OU

b. Cadmium ^8^

7. Calcium 35^00

b". Chromium /3

y. Cobalt V2U

10. Copper L 6.9j

11. Iron X25"

12. Lead /J(J ^

*.

A/

2_

^

^^^^^

pFF

P

P

P

P

P

pp

P

fCyanide

23.

Magnesium L*f20O]

Manganese C-S-81

Hercury 0. 2.U

Nickel f / f7

Potassium I85OO

Seleniua I ,UU

Sliver 2.*i(J

Sodium 23500

T**l.LiuaS,f/tS

Vanadium T/3l

Zinc T5-9J

A/

/I/

2

^_

P

P

P

P

F

P

P

F

PP

Precenc Solids (Z)

Footnotes: For reporting results to t'PA, standard result qua l i f i e r s arc usedas defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of such flags must*be explicitand contained on Cover Page, houever.

Comae uts: Water: Coloration <Lttf(L~is ClarityArtifact(s):None

Lab Manager

4 1 8 4 6 C 0 4 157/M/Fl /W/

Lr'A b.inpl

Uace OCT 30 1967

INOKCAMC ANALYSIS UAiA

LAt

SOU NO.

ETC/lexicon CASK NO.

785LAb SAMPLE 10. NO. Lj-/8'+- 113

Lab Kecoipt Date

QC REPORT NO.

tlements Identified and Measured

Concentration:

Matr ix: Water

Low

Soil

Medium

Sludge Other

Goroertzatim Flag Dilnrim hfethod Ocncentratian Flgg QilnHmr rag /kg dry weight (Circle One)

1 . Aluminum

2. Antimony

J. Arsenic

«. barium

5. tserylliun

b. Cadmium

7. Calcium

ti. Chromium

*. Cobalt

10. Copper

H. Iron ll*i]

12. Lead

P

F

F

P

P

F

P

P

p

P

P

F

14.

13.

Ib.

17.

16.

IV.

2u.

21.

22.

Magnesium

Manganese

hercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Freoent Solids (I)

Cyanide

Footnotes: For reporting results to KPA, standard result qualif iers arc usedas defined on Cover Pa&e. Additional flags or footnotes explainingresults are encouraged. Defini t ion of such flags must be explicitand contained on Cover fage, however.

Comoents: Water rColoration C.oi.t*.<.es± Claritv CLEARArtifact(s):None

THIS 7?fSiAT SA/wT is fo* T>/ssotvep .!/?<

iLab Manager

3A/ ^LY

P**iUN

t

1

ft}Mû\ jL-

' ^V)

57 /M/F1 /W

4 1 8 4 6 0 0 7 8

(Et'A Sample No.

LAU :.AME

SOW NO.

uate 30 1987

EIC/Toxlcon

INORGANIC ANALYSIS UA'lA SHtEl

CASE NO.

JZ85LAB SAMPLE ID. NO. - I O.3

Lab Kecelpt liate

0^: REPORT NO. <

blemencs Identified and Measured

Concent ration:

Matrix: Water

Low

Soil

Median

Sludge Other

Qxcertzadan Flag ULjdon Fbthod Oanoatratim FlfgIg/Côr ng/kg dry wight (Circle One)

1. Aluminum ["| ill

*. Antimony tl-ff U

J. Arsenic O.^ffU

H. Barium f/O3l

S. tterylllua 1. 00

b. Cadmium if-.gO

7. Calcium U2SOO

8. Chromium 5.4U

9. Cobalt +.2U

10. Copper &>.8l

11. Iron ftofl

12. Lead /, 3 U

^

ft

2.ZL

2,

ppF

P

P

/'P

P

P

P

P

F Precent Solids (I)

Cyanide

13. Magnesium 3IZOO

U. Manganese f/Oj

15. hercury O. 2 J

16. Nickel LZ£]

17. Potass luofv^/d

Ib. Selenium l.i+U

19. Silver . Z.Û

2u. Sodium /<?OOO

21. ThallluaZf ^//y

22. Vanadium 0?.?]

23. Zinc &Z

A//^ ^

^

pp

pppppppp

Footnotes: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or footnotes explaining

results are encouraged. Definition of such flags must be explicitand contained on Cover Cage, however.

WaterrColorationJuTtifact(s):Kone

Lab Manager

4184 6003257/M/Fl/W

uace OCT 3 0 1987

LAK

SOU f-O.

ETC/Toxicon

INOKCANIC A N A L Y S I S UA'iA Slttt'i

CASE NO.

785

LAb SAMPLE 10. NO. - I O3

Lab teccipt Date

QC REPORT NO.

tleoents Ident i f ied and Measured

Concentration:

Matr ix: Water

Low

Soil

Medium

Sludge Other

Cbnoentran'm Flag Dilirion tfethod Ctancenrrarim Flgg DOuticn tfethcdwg/kg dry weight (Circle One)

U.

14.

I . Aluminum

2. Antimony

J. Arsenic

A. barium

5. tterylliua

b. Cadmium

7. Calcium

ti. Chromium

9. Cobalt

10. Copper

11. Iron /"/ft! 1

12. Lead

P

F

F

P

P

F

P

P

P

P

P

F

It).

17.

16.

iy.2u.

21.

22.

Magnesium

Manganese

tercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids

Cyanide

Footnotes: For reporting results to tPA, s t andard result qua l i f i e r s arc used. as defined on Cover Page. A d d i t i o n a l f lags or footnotes explaining

results are encouraged. Defini t ion of such f lags must be explicitand contained on Cover Page, however.

Concents: Water :Coloration CouAUr*i Clarity r^ / f~ & &f_ *• C f t f \

Artifact(s):None

THIS -Resucr SHetT IS fo*. "D/SSOLV£D ZRON OfJLY

»-Lab Manaxe r ^dlJwu»v irfjU^^ L

5 7 / M / F 1 / W

4 1 8 4 6 0 0 6 9

li.itr.ple NO.

uate OCT 3 0 1987INORGANIC A.»AL*:>tb UA'IA

LAfc

sou

LAb SAMPLE ID. NO.


785- III

Lab Receipt Uace

QC REPORT NO.

Concentration:

Matrix: Water x

(rnpHBHtflCfl

1. Aluminum f/731

2. Antimony &.0 (J

3. Arsenic^. *f£U

•«. Barium £/&<2j

5. beryllium /.£>U

6. Cadmium </.#U

7. Calcium ?0?0O

«. Chromium f6.3"I

S». Cobalt 4.20

10. Copper f7.JZ"J

11. Iron /<?80 '

12. Lead 1,3 U


Low Medium

Soil Sludge

Flag Dilution Mated Cbrcentxatian^gTôr mg/kg dry weight (Circle One)

1 p 13. Magnesium 37ZOG

b

A/

2.ZL

3s

F 14. Manganese 65

F It), tercury O-2U

P 16. Nickel r25j

P 17. Potassiua/JyjZO/

P 16. Selenium I.U-U

P IV. Silver 2.^11

P 20. Sodium 3370O

p 21. Thallium 0 .&/ (/

P 22. Vanadium D£~]

P 23. Zinc 19, 77

Other

FlflgO

y

A/

itfrj-lm

&

2__

fc£**l_nsui

ppppF

P

P

Fp

P

F Precent Solids (1)

Cyanide

Footnotes: For reporting results to tPA, standard result quali tiers arc usedas defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Uefinition of such flags must'be explicitand contained on Cover Cage, however.

Comoent*: Water; Coloration ClarityArtifact(s):None

Lab Manager

4 1 8 4 6 C 0 3 957/M/Fl/W/

Date OCT 3 0 1987

INORGANIC A ^ A L Y ^ I S UA'IA

ETTC/Toxicon CASE NO.

SOU NO. 785

LAb SAMPLE ID. NO. ~ HI

Lab Keccipt bate

QC REPORT NO.


Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

Cbnffif tf'i.ftfôn

I. Aluminum

2. Antimony

3. Arsenic

H. bariujo

S. beryllium

6. Cadmium

7. Calciun

tt. Chromium

V. Cobalt

10. Copper

11. Iron T5#]

12. Lead

P

F

F

P

P

F

P

P

P

P

P

F

Dili rim tfethodfg/Lôr mg/kg dry weight (Circle One)

13.

Flag Eh"ii<-inn {fatted

li.

lb.

17.

lb.

iy.20.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Potassium

Selcniua

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids (Z)

Cyanide

Foocnoces: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Paê. Addi t iona l f lags or footnotes explaining

results are encouraged. Definition of such f lags must be explicitand contained on Cover Page, however.

Water:Coloration C.t>Lod(.es& ClarityArtifact(s):None

THIS T?£SuCT SHetT is fo* T>is<>oLveD IRON OfJLY

Lab Manager

57/M/Fi/ ; ;

4 1 8 4 6 0 0 7 6

l-ot m

| EPA Sample No.

Uate OCT 3 0 1967

ETC/Toxicon

INORGANIC ANALYSIS UA'lA SHfcE'l

CASE NO.

NO. 785

LAb SAMPLE ID. NO.

Lab Keccipc Dace

QC REPORT NO.

Klemencs Identified and Measured

Concent radon:

Matrix: Water

Low

Soil

Medium

Sludge Other

1.

3.

M .

5.

6.

7.

8.

10.

11.

12.

Aluminum

Antimony

Arsenic 6

barium

beryllium

Cadmium

Calcium

Chromium

Co bale

Copper

Iron

Lead A

nsfil^jO

i.'fffU{7s"o3

I .OU

5.3I03OOO

[<U1f/Q]C9.2]

nstt.?6V

A/

/v

2.

/*?

pFF

P

PJfp

P

P

pp

P

F

g/Lôr ng/kg dry weight (Circle One)

13.

14.

I*.

16.

17.

16.

IV.

20.

21.

22.

23.

Pre cent Solids (Z)

Cyanide

Magnesium 31<*OO

Manganese 1 32O

hercury O.20

Nickel yV

Potassium V^Sfd]

Selenium /.&£/

Silver . - f6.v7

Sodium llS'OO

Thallium <9.<f/U

Vanadium C/V7

Zinc f/3]

/vA/

£

£

pp

ppF

P

P

F

PP

Footnotes: for reporting results Co tPA, standard result qua lit tecs arc used. as defined on Cover Pa&e. Addlcional flags or foocnoces explaining

results are encouraged. Definition of such flags muse be explicitand contained on Cover Page, however.

Cooaaents: Water:Coloration ClarityArtifact(s):None

Lab Manager

4 1 8 4 6 C 0 2 25 7 / M / F l / W

Uace OCT 3 0 1987

LAK :.

SOU NO.

ETC/Toxicon

INORGANIC A.tAL'li lS U.VlA bHt.t'1

CASE .NO.

785

LAb SAMPLE 10. NO. 4/8 t' 33

Lab Keccipc Uate

QC R£HORT NO.

tlements Ident i f ied and Measured

DiSS

Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

Gonoentcatiai Flag rh"li<-im Mated CorcertzatiaiIg/Lôr mg/kg dry weight (Circle One)

U.

r>ili<-inn

I . Aluminum

i. Antimony

3. Arsenic

M. barium

5. Beryllium

6. Cadmium

7. Calcium

8. Chromium

9. Cobalc

10. Copper

11. Iron /~3&7

12. Lead

P

F

F

P

P

F

P

P

P

P

P

F

lo.

17.

Ib.

IV.

i\j.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precenc Solids (Z)

Cyanide

Footnotes: For reporting results to tPA, s tandard result qua l i f i e r s arc used. as defined on Cover Paê. Addi t iona l f lags or footnotes explaining

results are encouraged. Def ini t ion of such f lags must be explicitand contained on Cover Cage, however.

Comoents: .Water iColoration C_e>t-e>Kt.e&s. Clarity

Artifact(s) .-None

THIS ~R6$uCT /s foK T>/sso<-vfD J/?o/v ONLY

Lab Manager

4 1 8 4 6 0 0 5 95 7 / M / F l / W

^ o r cr. 1

j Er'A baraple No.

LAtbOV« NO.

ETC/Toxicon

Uace OCT 3 0 195?

INORGANIC ANALYSIS UA'lA SHtEl

_ CASE \o.

785

LAb SAMPLE ID. NO.

Lab Keccipt Uate

QC REPORT NO.


Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

QiuaMxaLicn Flqg niliflm Ifetfcd CbncotzatlGn FLqg Dtlut±n (fedrxijg/lNor mg/kg dry weight (Circle One)

1. Aluminum 2b(e>

i. Antimony l^.&U

J. Arsenic Gfiffl)

H. harium 2/5*

5. Berylliuo /.OO

to. Cadniua V.Û

7. Calciua 21(oOOO

(5. Chrood.ua £.4(J

9. Cobalt 4.2U

LO. Copper f/Sl

11. Iron f52~]

12. Lead j ,3 U

N

N

z.z,

10

10

pFF

P

P

AP

P

P

P

P

F

13. Magnesium iZ-Zî

I*. Manganese [83

15. hercury O."2.(J

16. Nickel I3U

17. Potassium 7&800

Ito. Selenium /, ^£/

IV. Silver . fV.Ol

20. Sodium 5/2.OO

21. Thalliua^,^/^/

22. Vanadium 0^1

23. Zinc i:%i)

V

A/

/L>

2_

pp

ppFppF

PE

Precenc Solids (Z)

Cyanide

Footnotes: For reporting results to tPA, standard result qualif iers arc used. as defined on Cover Page. Additional flags or footnotes explaining

results are encouraged. Definition of such flags must be explicitand contained on Cover Cage, houever.

Comnents: Water:Coloration ClarityArtifact(s):None

Lab Manager

4 1 5 4 6 C 0 2 35 7 / M / F l / W

ETC/Toxicon

SOU NO. 785

LAb SAMPLK ID. NO.

Date OCT 3 0 1987

A:<ALt:>lS IM'lA

CASK NO.

Lab Receipt Date

QC REPORT NO.

tletaencs Identified and Measured

Concentration:

Matrix: Water

Low

Soil

[-tedium

Sludge Other

Ccrcenrrarton Flag Dilirim rfethod Flag T>i"li*-ifT|

I. Aluminum

'i. Antimony

J. Arsenic

•i. barium

5. tferylliua

b. Cadmium

7. Calcium

b. Chromium

9. Cobalc

10. Copper

11. Iron ££&!

12. Lead

P

F

F

P

P

F

P

P

p

P

P

F


13.

U.

17.

Ib.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids (Z)

Cyanide

Footnotes: For reporting results to tPA, s tandard result qua l i f i e r s arc used. as def ined on Cover Page. Addit ional flags or footnotes explaining

results are encouraged. Def in i t ion of such flags must be explicitand contained on Cover Page, however.

Coroent*: Water: Coloration Clarity

Artifact(s):None

THIS 7?fSuiT SHttT is fo* OrtLY

Lab Manager

5 7 / M / F l / W

6 G Q 6 0

I

Date OCT 3 0 1987

LMOI&AMC ANALYSIS UAVA

LA£ T.AME

SOW NO.

EIC/Toxicon CASE NO.

785

LAB SAMPLE 10. HO.

Lab Receipt Gate

QC REPORT NO.

Eleaents Identified and Measured

CooGeneration:

Matrix: Water

Low

Soil

Kedluai

Sludge Other

Hag QmatmUon PIqg DQut±n Matted•g/kf dry weight (Circle One)

1. Aluminum 2^3

•/. Antlaony U.ffU

3. Arsenic 030U

4. barlua / /9O

S. eerylllua 1.00

6. Cadvlua 9.1

7. Calclua ^0,OOO

<J. Chroodua /4

9. Cobalt pTSl

10. Copper r/2l

11. Iron ILSOO12. Lead AJ ^/

AJ

.-

A/

X,

/^

•

pppppF

U.

IS.

16.

17.

16.

20.

21.

22.

23.

Magneslua l57,OOO

Manganese 82.

Mercury O.2U

Nickel SS

Potasslua 838O

Selenlua l>l±U

Sliver 2.HU -.

Sodlua ' '•'.& tyj D00

Thalllua S.f/t/

Vanadlua £.3 Ij

Zloc D 3]

A/

A/

10

JL

pp

pppppppE

Freceot Solids (Z)

Cyanide

Footnotes: For reporting results to tPA, standard result qualifiers are used. as defined oo Cover Paê. Additional flags or footnotes explaining

results arc encouraged. Definition of such flags aust be explicitand contained on Cover Page, however.

UateriColoratlonArtif act(s):None

4 1 8 4 6 0 0 3 S

uace OCT 3 0 1987

INORGANIC A. iALts lS UA'lA SllLt'1

LAK

SOU NO.

ETC/Toxlcon CASE NO. V/gV

785

LAb SAMPLE II). NO.

Lab Keccipc liace / "V?9" ff 7

QC REPORT NO.

Elements Identif ied and Measured

1HSS

Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

Cbnoentratiai Flgg piliirim hfediod Cbraentxatiaijg/lNor tug/kg dry ueight (Circle One)

rKli<-inn ^fetJtxi

1 . Aluminum

'i. Antimony

J. Arsenic

H. Barium

5. beryllium

t>. Cadmium

7. Calcium

tt. Chromium

<y. Cobalt

10. Copper

11. Iron /?9

12. Lead

P

F

F

P

P

F

P

P

P

P

P

F

u.[4.

1>.

10.

17.

15.

iy.20.

21.

22.

Magnesium

Manganese

Hercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precenc Solids (2)

Cyanide

Footnotes: For reporting results to tPA, standard result qualifiers arc used. as def ined on Cover Page. Addi t iona l flags or footnotes explaining

results are encouraged. Defini t ion of such flags must be explicitand contained on Cover Page, however.

Comoeuc*: Water:Coloratlon ClarityArtifact(s):None

THIS SHftT is fo* ~t>moLyet>

Lab Manager

57/M/F1/W

4 1 8 4 6 0 0 7 2

l-orr I

ANALYSIS UA'lA

LAt

SOU NO.

ETC/Toxicon CASt NO.

Sample No.

wo yjo/ I

OCT 3 Q mr

785 Ub Receipt Uate 9-29-87

LAb SAMPLE 10. NO. QC REPORT NO. y/gy


Matrix:

Cyanide

Footnotes:

ration: Low

Water x

ainum fi I3l

Lmony lk,$(J

snic CfyfO*)

Lum T& 8l

fllium ADD

ilum 4.8U

:ium £S\QO

>mium 5.4U

ilc ^.2iJ>er rs.n* f(.8li / ,3cV

Medium

Soil Sludge

Flqg DLIudcn!

A/

N

^>L

2.

fEPcn UTcerctaticnmg/kg dry weight (Circle One)

p 13. Magnesium 2_(*70C

F 14. Manganese [~7. 1

F IS. hercury O.ZU

P Ib. Nickel l3\J

P 17. Potassium .58/0

y^ Ib. Selenium .j.llU

P IV. Silver Z.4U

P 20. Sodium 'HZO

p 21. Thallium <$> ,*? I U

p 22. Vanadium f8.<TI

P 23. Zinc £&.£]

Other

Flag T>n»*-fan

VV

/£?

^

mA**4hnsD]

pp

ppF

P

P

Fp

E

F Precent Solids (Z)

For report ing results to tPA, s tandard result qual i f iers arc usedas defined on Cover Page. Additional f lags or footnotes explainingresults are encouraged. Ueflnltloa of such f lags must be explicitand contained on Cover Page, houever.

Comoents: Water: Coloration ClarityArtifact(s):None

Lab Manager

4 1 8 4 6 C 0 1 95 7 / M / F l / W

Uace OCT 3 0 19°7

LAtsou NO.

ETC/Toxicon

A N A L Y S I S UA'lA SHtE'l

CASt NO. V/gV785

LAb SAMPLE ID. NO. " 90

Lab Keccipt Uace

QC REPORT NO.


Con ce n C era c ion:

Matrix: Wacer

Low

Soil

tedium

Sludge Other

Gcnoantraticn Flag DOyCkn rfetiiod

1 . Aluminum

i. Antimony

J. Arsenic

•*. barium

3. Beryllium

6. Cadmium

7. Calcium

tt. Chromium

9. Cobalc

10. Copper

11. Iron Z /3

12. Lead

P

F

F

P

P

F

P

P

P

P

P

F

Xfg/lNor mg/kg dry weight (Circle One)

13.

14.

16.

17.

Ib.

iy.2U.

21.

22.

23.

Precenc Solids (Z>

Cyanide

Magnesium

Manganese

hercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Footnotes: For repor t ing results to tPA, standard result qua l i f i e r s arc used. as defined on Cover Page. Addit ional flags or footnotes explaining

results are encouraged. Definition of such flags must be explicitai\d contained on Cover Page, hoover.

Comae MM: Water: Coloration Claritv CLEARArtifact (s):None

THIS SHctT is foX. ~D/sso<-v«? IRON

Lab Manager

4 1 8 4 6 0 0 5 65 7 / M / r l / W

l -o rm I

INORGANIC ANALYSIS UA'lA

Sample Ho. \"

Oace OCT 3 0 198/I ^

LAt

SOU NO.


785LAb SAMPLK ID. NO. - 89

Lab Keccipt liate q-

<}C REPORT NO. f 184


Concent radon:

Matrix:

on : Low

iter X

<<£» zm

Soil

Uutim Mated/L\or rag/kg

P

Medium

Sludge Other

CbncsTtCBtdon Floe Qdry weight (Circle One)

13. Magnesium L^/J

Ilirlcn Mated

P1. Aluminum 22H

'£.. Antimony ff*.d I?

3. Arsenic 0.^6 U

H. Barium 6>49

5. Beryllium f.OU

o. Cadmium ^.8U

7. Calcium 2i?OOO

«. Chromium £7

V. Cobalt ^,2U

10. Copper f /Vl

U. Iron L.(*S~]

12. Lead /.3 ^

N

N

2,2.

10

to

pFF

P

P

t?FpPpppF

13. Magnesium L7/J

14. Manganese tS'tJ

IS. hercury O.2U16. Nickel /3U

17. Potassiua LjIfOOO

Ib. Selenium \M U

IV. Sliver -T(o.f[

l\j. Sodium 2O5000

21. Thallium ff.^jf/U

22. Vanadium ("/ f 7

23. Zinc T/¥7

A/

^

/o;&

^

pp

ppF

P

P

F

P£

Preoent Solids (I)

Cyanide

Footnotes: For reporting results to tPA, standard result qua lit lees arc used. as defined on Cover Pa e. Additional flags or Footnotes explainingresults are encouraged. Definition of such flags must be explicitand contained on Cover Cage, however.

Comaene$: Water:Coloration Clarity

Artifact(s):None

Lab Manager

4 1 6 4 6 C 0 1 8

f o r m I

\ E f f , Sample No. |

I

Date OCT 3 n 10Q7

INORGANIC ANALYSIS UA'iA

ETC/Toxicon CASK .so.

NO. 785

LAb SAMPLE ID. NO.

Lab Keceipt liate *f->

QC REPORT NO.


ISS

Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

n i*>ni 1'nrim

1. Aluminum

2. Antimony

J. Arsenic

H. Barium

5. berylliua

6. Cadniua

7. Calciua

b. Chromium

V. Cobalt

10. Copper

11. Iron Z"3/l

12. Lead

P

F

F

P

P

F

P

P

P

P

P

r

U.

14.

13.

16.

17.

Ib.

19.

20.

21.

22.

23.

\JS UnXaLlili

ight (Circle One)

Kagnesiua

Manganese

hercury

Nickel

Potassiuo

Seleniua

Silver

Sodiua

Thallluo

Vanadiua

Zinc

tiaûi iim-im ctau.ua

P

P

P

P

F

P

P

F

P

P

Preoenc Solids (Z)

Cyanide

Footnotes: For reporting results Co tPA, standard result qualif iers arc used. as defined on Cover Page. Additional flags or footnotes explaining

results are encouraged. Definition of such flags muse be explicitand contained on Cover Cage, however.

Comneots: Water .'Coloration ClarityArtifact (s): None

THIS "ReSuLT SHctT i$ fe* Dm PL VCD OtiLY

Lab Manager

4 1 8 4 6 C 0 5 55 7 / M / F l / W

[Et'A Sanple No. |

I - I

\ JofSc i I

Oate OCT 30 1987

LAK NAME _

SOW NO.

LAb SAMPLE ID. NO.

INORGANIC ANALYSIS UAIAETC/Toxicon CASE NO.

785- IPS

Lab Kecelpt Bate

QC REPORT NO.

Concent ration:

Matrix: Water


Low Medium _

SludgeSoil Other

n i » i-g •Tar-inn

1. Alumloum flLfD~l

2. Antimony & .0 (J

3. Arsenic 0,50U

H. barium .S^T]

5. Beryllium /. OU

6. Cadmium *+.%[)

7. Calcium 84IOO

«. Chromium £5.41

V. Cobalt V.2L/

10. Copper [7s"7

11. Iron C8£]

12. Lead /r5 ^/

tUKU

(uj

A/

•

/J

n nw-im ]

7t)or

.&

2,

TcUCu *'"*** *fi! it ii«g/k.g dry weight (Circle One)

p 13. Magnesium 20LOO

F 14. Manganese /^¥

F IS. hercury O ^jj

P 16. Nickel /3L>

P 17. Potassium FS^S"]

P 16. Seleniua 1 >H-U

P IV. Silver F3. 5l

P 2O. Sodium /^29VOT

p 21. Thallium 0,9/ L/

p 22. Vanadium £?. 77

P 23. Zinc 2V

F Preceat Solid* (Z)

nqgL

^

^

ina-im

^

^

rauuu

P

P

P

Cyanide

Footnotes: For reporting results Co tPA, standard result qualifiers arc ueedas defined on Cover Paê. Additional fla^s or footnotes explainingresults are encouraged. Definition of such flags must* be explicitand contained on Cover Cage, however.

Comnents: Jfater: Coloration <n*itArtif act (s): None

Lab Manager

4 1 8 4 6003657/M/n/W/

j K i' A 1.. i m; i 11 •

Dace OC7 3 0 1987

INORGANIC A N A L Y S I S UA'IA

ETC/Toxlcon CASt .\o.

NO. 785

LAb SAMPLE 10. NO. - /g 3

Lab Receipt liate ?- Z1-97

QC REPORT NO.

bleoencs Ident if ied and Measured

Concenccacion:

Matrix: Wacer

Low

Soil

Medium

Sludge Other

Cbrcantzatian Flgg pOm-im ffethd Gcrcentxatian Flfg TMIirimr rag/kg dry weight (Circle One)

1 . Aluminum

2. Antimony

3. Arsenic

H. barium

5. tterylliua

b. Cadmium

7. Calcium

b. Chromium

^. .Cobalt

10. Copper

1 1. Iron tZ*ll

12. Lead

•

P

FF

P

P

F

P

P

p

P

P

F

U.

15.

10.

17.

16.

iy.2u.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Pocassiua

Selcniua

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precenc Solids (Z)

Cyanide

Footnotes: For report ing results to tPA, s tandard result qua l i f i e r s arc used. as defined on Cover Page. Addi t ional f lags or tootnotes explaining


Comoeots: Water: Coloration &>u*L&s Clarity

Artifact(s):None

THIS SHftT fo* J/?OA/

Lab Manager

f o r m I

J E P A No.

OCT 3 0 1387

INORGANIC ANALYSES IM'IAETC/Toxicon CASE NO.

sou NO. 785

LAb SAMPLE ID. NO.

Ub Keccipc Uate

QC REPORT NO.


Con cent radon:

Matrix: Water

Low

Soil

Medium

Sludge Other

Cbroertxatlon FUg DLTuelcn rfathadjg/L\or mg/kg dry weight (Circle One)

1.'t.

3.

5.

b.

7.

a.

10.

u.12.

Aluminum (t>5Z

An t imony JJ*. $ 0

Arsenic Cbffr

harlum CY5]

Beryllium I.QU

Cadmium f.&O

Calcium QÔOO

Chromium ,5".mJ

Cobalt 1.2U

Copper fiSl

Iron LSQ

Le«d /..^ 6/

A/

A/

^

^

-^L

PFF

PP

^pP

Pp

p

PF

H.

14.

1*.

Ib.

17.

16.

21.

22.

23.

Preoent Solids (Z)

Cyanide

Magnesium LV^f

Manganese [*/ , V~I

hercury- O.2U

Nickel /3 U

Potassium 2HZOO

Seleniua . I'MtJ

Silver - - 2 A U

Sodium U I^QO

Thallium 0 rf/ U

Vanadium F/2^1

Zinc 4. \ U

A/

A/^

2.

P

P

P

P

F

P

P

F

PE

Footnotes: For reporting results to tPA, standard result qua l i f i e r s arc used. as defined on Cover Page. Additional f lags or footnotes explaining

results are encouraged. Definition of sued flags must be explicitand contained on Cover Page, however.

Comoeot*: Water: Coloration Clarity

Artif act (s): None

A.Lab Manager

^4 1 8 4 60021

5 7 / M / F l / W

K l ' A j.i rr. p 1 1-

Uacc OCT 3 0 1987

ANALYSIS UA'lA


NO. 783LAb SAMPLE ID. NO. - 92.

Lab Keccipt liate

QC REPORT NO.

b'letnencs Identified and Measured

DlSS

Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

n n

1. Aluminum

2. Antimony

3. Arsenic

H. barium

5. tterylliua

b. Cadmium

7. Calcium

b. Chromium

9. Cobalt

10. Copper

II. Iron Z"/Sl

12. Lead

p

F

F

P

P

F

P

P

p

P

P

f

^fc^^r^^ CbnDentcatacn Flag DUiticn bfethcdg/Lôr mg/kg dry weight (Circle One)

13.

16.

17.

20.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids (I)

Cyanide

Footnotes: For reporting results to tPA, s tandard result q u a l i f i e r s arc used. as defined on Cover Page. Additional flags or footnotes explaining

results are encouraged. Definition of such flags must be explicitand contained on Cover Hage, houever.

Water: Coloration ClarityArtifact(s):Nbne

T/y/S 7?gSt/tT SHctT is fo*

Lab Manager

4 1 8 4 6 0 0 5 85 7 / M / F l / W

i -orm 1

INORGANICLAt :.AME

SOW NO.

ETC/Toxicon

785LAb SAMPLE 10. NO. - < \ \

UAYA

(EPA Sample No.

Uate OCT 3 0 1987

CASK NO.

Lab Kecclpc Uate 9- 29-87

QC REPORT NO.


Concencration:

Matrix: Water

Low

Soil

Medium

Sludge Other

Cbnoentcatlcn Flgg DUition tettad GbnomtraCLon Flag Dilutim Mattedjg/Lôr mg/kg dry weight (Circle One)

13.

14.

15.

16.

17.

Ib.

19.

20.

21.

22.

23.

I.

'i.

3.

•i.

5.

6.

7.

tt.

9.

10.

U.

12.

Aluminum

Antioiony

Arsenic

barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead

DillV-.ou

0.9ouC7<fl

l.ouf«u

5V900

SÛ

^.iU2AU

C3fl

/ .3U

/V

A/

zz

/c

PFF

P

P

ftP

P

P

P

P

F

Magnesium [|O7j

Manganese £3.\]

hercury O.ZU

Nickel 13 U

Potass lua 6>33O^

Selenium / . V U

Silver .. - 2.</U

Sodium Z t f lOO

Thallium 0.9/ U

Vanadium CV.7U

Zinc 0?}

A/

Z

2

P

P

P

P

F

P

P

F

PP

Precent Solids

Cyanide

Footnotes: For reporting results to tPA, standard result qual i f iers arc used. as defined on Cover Page. Additional flags or footnotes explaining


Comoenta: Water: Coloration Clarity

Artifact(s):None

Lab Maoaêr

4 1 8 4 6 C 0 2 05 7 / M / F l / W

! L t 'A L_ 1-1,- i.

INORGANIC

ETC/lexicon

SOU NO. 785

LAb SAMPLE 10. NO. */AS"f -

Uace OCT 3 0

U.VIA

CASK NO.

Lab Keccipc Uace

QC REPORT NO.

tleraents Identif ied and Measured

THSS

Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Ocher

Ctaroenfntfjm Fkg Di.1i.fim tfediod Cbrcentiaricn Flag Dilirim tfethadrag/kg dry weight (Circle One)

U.1 . Aluminum

'(.. Antimony

J. Arsenic

•*. barium

5. tserylliuo

b. Cadmium

7. Calcium

8. Chrootium

9. Cobalc

10. Copper

11. Iron f?./l

12. Lead

P

F

F

P

P

F

P

P

P

P

P

F

Ib.

17.

Ib.

IV.

2o.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Potassiuo

Selcniuo

Silver

Sodium

Thalliua

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precenc Solids (I)

Cyanide

Footnotes: For report ing results Co tPA, s tandard result q u a l i f i e r s arc used. as def ined on Cover Page. Addit ional f lags or tootnotes explaining

results are encouraged. Definition of such flags must be explicitand contained on Cover Cage, however.

Comoencs: Water: Coloration ClarityArcifact(s):Norte

THIS ~R£$uCT SHctT iS foi? ZRon OfJLY

Lab

4 1 8 4 6 0 0 5 7T 7 / M / F 1 / W

INORGANIC ANALYSIS UAVALAt

SOVt NO.

ETC/Toxicon

L > j r r ; > L e N o -

uate OCT 3 Q 1987

CASE NO.

785

LAb SAMPLE IU. NO.

Lab Kcccipt liace 9-23-f 1

QC REPORT NO.


Concentration:

Matrix: Water

Low

Soil

Medium

Sludge Other

Fl g Dilution rfethod Ctnoertxatiai Dlluticn tferiulig/r)or a^/kg dry weight (Circle One)

1.t.

3.

H .

5.

6.

7.

45.

10.

11.

12.

Aluminum

Antimony fa

Arsenic &

barium j

teryllium

Cadmium

[/SOI1.0LJ30U~JSO]

1.00480

Calcium IOIOOO

Chromium

Cobalt

Copper

Iron

Lead y

fall¥.2054

2£3,3 U

A/

»

AV

^^

/^

pFF

P

P

P

P

P

p

P

P

F

15.

17.

£o.

1«».

20.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium i

Vanadium

Zinc

H-OOOO

/OS"

G.-LUr*3i

f/goo]l.bV[2.11bISO?.<//{/

C/31(*(*

fj

VZL

^

pp

ppF

P

P

F

PP

Precent Solids (1)

Cyanide

footnotes: For reporting results to tlPA, standard result qualifiers arc usedas defined on Cover Page. Additional f lags or footnotes explainingresults are encouraged. Definit ion of such flags must 'be explicitand contained on Cover fage, however.

Comoe.it*: Water:Coloration PjJtrdLt+' ClarityArtifact(s):None

.UAAlMx:^vLab Manager w

4 1 8 4 6 C 0 5 75 7 / M / F l / W /

LAKSOU NO.

EIC/Toxicon

785LAb SAMPLE 10. NO. <//o"f -

Uatc OCT 3 0 1937

A;.ALYiLb UAlA

CASt NO. V/gV

Lab Receipt Date

QC REPORT NO.

Elements Ident i f ied and Measured

Concencracion:

Matr ix: Water

Cyanide

Low

Soil

(tedium

Sludge Other

I . Aluminum

2. Antimony

J. Arsenic

A. Barium

5. tterylliun

6. Cadmium

7. Calcium

b. Chromium

9. Cobalt

10. Copper

11. Iron ft/]

12. Lead

P

F

F

P

P

F

P

P

P

P

P

r

Flag DUutJan rfetfaxi Cbnoatxataan Flag DUutim Mattedig/Lôr ng/dg dry weight (Circle One)

U.

10.

17.

Ib.

IV.

2o.

21.

22.

23.

Magnesium

Manganese

ftercury

Nickel

Potassiun

Selcniua

Silver

Sodium

Thallium

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids (Z)

Footnotes: For reporting results to tPA, s t andard result qua l i f i e r s arc used. as def ined on Cover Paê. Addi t iona l f lags or tootnotes explaining

rftsuics are encouraged. Def ini t ion of such f lags must be explicitand contained on Cover Cage, however.

Comneots: Water :Coloration CbiJXU&> ClarityArtifact(s):None

THIS 7?fSutT SHctT IS fo^ J.RON

Lab Manager

4 1 8 4 6 G 0 7 4

Ko r m 1

INORGANIC A*ALY:>IS UAYA

ETC/Toxlcon

j E t - A Sample No. _ j

Oace OCT 3 0 1987

CASt NO.

SOU NO. 785

LAb SAMPLE II). NO. ~ <??

Ub Kecelpt Late

QC REPORT NO.

9-29-87


Concent ration:

Matrix: Water

Low

Soil

Medium

Sludge Other

Flat DLTiJtLan terird OimlmLkn Flag DOitim Mathodr rag/kg dry weight (Circle One)

1. Aluminum 35?

't. Antimony &,0 U

3. Arsenic C& .(*)

A. barium j}83

5. tSerylliua / ,OU

6. Cadmium \S

7. Calcium ZS10OO

«. Chromium j20

9. Cobalt C/G

10. Copper [fl]

11. Iron >2tlOO

12. Lead /,3U

A/

AJ

2,2.

to

10

pFF

P

P

/*P

P

p

P

P

F

U. Magnesium I70OOO

U. Manganese //V-O

li. hercury ^).2U

16. Nickel /02.

17. Potassium <oS(*00

16. Selenium / . Jf. /S

IV. Silver . fV./7

2O. Sodium 3Q3OOO

21. Thallium 47 ^/^/

22. Vanadium f^^J

23. Zinc 121

fll

/V

/o

1

/O

&

P

P

P

P

F

P

P

F

PE

Precent Solids (I)

Cyanide

Footnotes: For reporting results to t'PA, standard result qual i f iers arc used. as defined on Cover Page. Additional flags or footnotes explaining

resales are encouraged. Definition of such flags Bust be explicitand contained on Cover Page, however.

Conoents: Water: Coloration

Artifact(s):NoneClarity

Lab Manager

4 1 8 4 6 0 0 2 65 7 / M ' F i / w

oate OCT 3 0 1987

INORGANIC A..ALt^li UA'IA

LAL

sou


785

LAb SAMPLE 10. NO. - 97

Lab Keccipt Uate

QC REPORT NO.

Elements Idencified and Measured

DiSS

Concentrat ion:

Matrix: Wacer

Cyanide

Low

Soil

Medium

Sludge Other

1 . Aluminum

'i. Antimony

3. Arsenic

•i. barium

5. tierylliua

to. Cadmium

7. Calcium

y. Chromium

9. Cobalt

10. Copper

11. Iron fV^] 1

12. Lead

P

FF

P

P

F

P

P

p

P

P

F

<Viym< mi-innng/kg dry weight (Circle One)

13.

14.

Pilit-inn

16.

17.

Ib.

22.

23.

Magnesium

Manganese

hercury

Nickel

Pocassiuo

Selcniua

Silver

Sodium

Thalliuo

Vanadium

Zinc

P

P

P

P

F

P

P

F

P

P

Precent Solids (Z)

Footnotes: For reporting results to tPA, s tandard result qual i f iers arc used. as def ined on Cover Paê. A d d i t i o n a l flags or footnotes explaining

results are encouraged. Def in i t ion of such flags must be explicitacid contained on Cover Page, however.

Comoeots: _Water:Coloration ClarityArt.lfact(s):None

THIS "ReûCT SHetT is fo* DISSOLVED

Lab Manager

5 7 / M . F 1 / W

4 1 8 4 6 0 0 6 ^

f o r m I

Sample No. j"

Uate OCT 3 0 1987

fc :.A,'tt ETC/Toxlcon

sou NO. 785

; ANALYSIS UA'lA ihttl

CASt NO.

LAb SAMPLE ID. NO.

Ub Receipt Uate <j-29-$7

QC REPORT NO.


Concent ration:

Matrix: Water

Low

Soil

Medium

Sludge Other

CbnDsntratian Flag

Cyanide

hfetftxi Cbncertxatixn Flqg Dthttcn tfethodQg/kg dry weight (Circle One)

1. Aluminum 3OO

L. Antinony U.0 U

J. Arsenic 0 30 U

i. Kariua F/53^

5. berylllua LOU

t>. Cadnlum 9.7

7. Calcium 25"IOOO

«. Chrooiua /S

V. Cobalt [9.3]

10. Copper f/21

11. Iron f IOOO

12. Lead j .3 U

t\

ti

?,2

/O

/^

p

FF

P

P

/'P

P

p

P

P

p

13.

14.

13.

16.

17.

16.

20.

21.

22.

Magnesium lb%OOO

Manganese / /3O

hercury 0. 2.0

Nickel }O3>

Potassiua (olf SOO

Seleniua 1 . k. U

Silver fS.Vl

Sodium 30V-OOO

Thalliua <?.*7/{/

Vanadium T.2?3

Zinc (e>$2-

A/

A/

10

1010ZL

pp

PpF

P

P

Fp

P

Precent Solids

Footnotes: For reporting results to tPA, standard result qua 11 tiers arc used. «* defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of sued flags must be explicitand contained on Cover Cage, however.

Comoents: Water; Coloration ClarityArtifact(s):N6ne

Lab Manager

4 1 8 4 6 0 0 2 757/y. /Fl/W

OCT 3 0 1987'

IMOKCANIC AI 'ALtSLS UA'tA

ETC/lexicon CASK .NO.

sou NO. 785

LAb SAMPLK II). NO. 4/8*+-

Lab Keccipt Uace

QC REPORT NO,

blements Ident i f ied and Measured

Concentration:

Matrix: Wacer

Low

x Soil

i it i >4frifn F13R T i li jm M*f j \y \

[•tedium

Sludge

/Vu-L L LltTUTCfint

Other


1 . Aluminum

2. Antimony

J. Arsenic

«. barium

5. tferylliuo

6. Cadmium

7. Calcium

tt. Chromium

*. Cobalt

10. Copper

IL. Iron fV97

12. Lead

P

F

F

P

P

F

P

P

P

P

P

F

13. Magnesium

14. Manganese

li. hercury

16. Nickel

17. Potassium

16. Selenium

lu. Silver

2o. Sodium

21. Thallium

22. Vanadium

23. Zinc

P

P

P

P

F

P

P

F

P

P

Precenc Solids (I)

Cyanide

Footnotes: For repor t ing results Co tPA, s t andard result q u a l i f i e r s arc used. as defined on Cover Pa&e. Additional flags or footnotes explaining

results are encouraged. Definit ion of such f lags must be explicitacid contained on Cover fage, however.

Comoencs: Water: Color at ion ClarityArtifact(s):None

THis ~R£Sut.~T SHetT is fo* ~Dis.Soi.vfD ZRon

Lab Manager

5 7 / M / F 1 / W

4 1 9 4 6 0 C 6 4

ETC/Toxicon

INOHCAMC AÂLYalS UA'iA SHfcEl

CASE NO.

baople No. |

I " II/*\ D L Q. UJ Q gC 01 I

Uate OC1" 3 0 1987

NO. 785

LAb SAMPLE 10. NO.

Lab Kecclpt Uate

QC REPORT NO.


Concent radon:

Matrix: Water

Low

Soil

Medium

Sludge Other

QiuatfHtlm Flag T>t1i rim tfethri Cbrcertmrlm Flag Ttilirinn MattedKg/kg dry weight (Circle One)

13.

14.

1 . Aluminum /"/ 75 1

'£. Antimony lL,0 (}

3. Arsenic £)30U

H. Barium d>£^

S. Beryllium / .OL>

fe. Cadmium 7.1

7. Calcium /33OOO

B. Chromium T^.^

i>. Cobalt V.ZU

10. Copper £7.Q]

11. Iron 72700

12. Lead / *3 V

A/

A/

r1^*

2,

10

pFF

P

P

^PP

P

pp

P

F

16.

17.

Ib.

IV.

20.

21.

22.

Hagneslua KfpOOO

Manganese 2%

hercury G.ZO

Nickel ¥2.

Potassluo 622^7

Selenlua /.>>^/

Sllv«r 24U

Sodium IV2.OOO

Thalllua j.tf/L'

Vanadium f/fl

Zinc ¥0

A/

A/

/0

/<P

.

P

P

P

P

F

P

P

F

PE

Precenc Solid* (2)

Cyanide

Footnotes: For reporting results to EPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or tootnotes explaining


Co Water rColorationArtifact(s):None

4 1 8 4 6 C 0 3 357/M/Fl/W

j LI' A. '_.inp If

OCT 3 0 1987

INORGANIC A N A L Y S I S UA'IA

LAKSOU NO.

ETC/Toxicon CASt \o.

785

LAb SAMPLE ID. NO.

Lab Keccipc Date ?'

QC REPORT HO. V/gV

Elements Identif ied and Measured

Concent rat ion:

Mat r ix : Water

Low

Soil

Medium

Sludge Other

CorcenrrTirim Flag DOurjcn ttedxri Cbnoertratam Flag Diliricn hfetfadjgTlNor «g/kg dry weight (Circle One)

1. Aluminum

L. Antimony

J. Arsenic

•i. barium

5. Berylliua

6. Cadmium

7. Calcium

b. Chromium

9. Cobalt

10. Copper

11. Iron //5

12. Lead

P

FF

P

P

F

P

P

P

P

P

F

U.

17.

16.

iy.20.

21.

22.

23.

Magnesium

Manganese

hercury

Nickel

Pocassiuo

Selcniua

Silver

Sodium

Thalliua

Vanadium

Zinc

P

P

P

P

F

P

P

F

PP

Precent Solids (Z)

Cyanide

Footnotes: For repor t ing results to tPA, s tandard result qua l i f ie rs arc usedas def ined on Cover Paê. Addi t ional f lags or footnotes explainingresults are encouraged. Definition of such f lags muse be explicitand contained on Cover Page, however.

Comoents: Water : Coloration Cet.o4.LeiS Clarity CLEAR __Artifact(s):None _ ___ _

THIS 7?fStAT SHctT iS fo* "D/sSQivfP OfJLY

Lab Manager

57/M/Fl /v :

4 1 P /I 6 7 C 7

CONVENTIONALS CHEMICAL PARAMETER ANALYTICAL DATA.

PTC/TOXICON IDENTIFICATIONCUF:Jsrr IDEKHFICATIONSAMPLE MATRIXDATE SAMPLED

PARAMETER UNITS

4184/84MDLSW00803

09/21/87

4184/89MDLGW04401Wxer09/27/87

4184/90MDLCW0430IWtier09/27/87

4184/91MDLGW0470IWater09/27/87

4184/92MDLGW0460IVJmer09/27/87

4184/93MDLGW0400IWater09/26/87

*.**-*- ^0&amAW5i--î ,-^-vi. r û - jAlluUiruty. Toul mg/LChemic*! O>ygen Demand (COD) mgfLCyanide, ToUl mg/L

NA<5.0<02

1600<5.0<.02

270<5.0<.02

400(9<.02

30049<.02

47054<.02

I ludnen. Total fflg/LResidue, FUienMe (TDS) mg/LResidue, Total Suspended (TSS) mg/L

25038038

3102,0005,300

2703903.000

1506005,100

25037013,000

44068011,000

NA denote* Not Analyzed.

oo

-OCDCDO

CONVENTIONAL^ CHEMICAL PARAMETER ANALYTICAL DATA.

CTC/TOXICON IDENTIFICATIONCUIT-NT IDENTIFICATIONSAMPLE MATRIXDATE SAMPLED

4184/94MDLGW04101Water09/26/87

4184/95MDLGW03301Water09/26/87

4184/96MDLGW03401Water09/26/87

4184/97MDLGW04901Water

4184/98MDLGW04902Water09/27/87

4184/99MDLGW03601Water09/26/87

t» *> 8 ~fOPARAMETER UNITS

Alkalimry. Toul mg/LChemical Oxygen Dcmmd (COD) mg/LCyanide, Total mg/L

640180<02

1600160<.02

300<5.0<.02

2,000310<.02

2,100370<.02

1,300<5.0<.02

R, Toul mg/LRendue, Filterable (TDS) mg/LResidue, Total Suspended (TSS) mg/L

7106507.100

9201,800950

2203802,900

1.3002,400150

1,3002,400140

2101,300860

NA denotes Not Analyzed.

^

CD

CD

CDCD


fTCYTOXICON IDENTIFICATIONCLIENT IDENTIFICATIONSAMPLE MATRIXDATE SAMPLED

4184/100MDLGW03602Water09/26/J7

4184/101MDLGWD3001Water09/25/S7

4184/102MDLCW03101Water09/25/17

4184/103MDLGW03801Water090647

4184/104MDLGW0500IWater09/27/87

4184/105MDLGWB00001WllCT09/75/87

PARAMETER UNITS

Alkalinity, TotalChemical Oxygen Demand (COD)Cyanide, Total

mg/Lmg/Lmg/L

290<50<.02

43028<.02

190<5.0<.02

190<50<.02

82066«.02

.44<50<.02

I ludnen, Toul mg/LResidue, Rllerable (TDS) mg/LResidue, Todl Suspended (TSS) mg/L

1702807,800

350550340

17027049

2906701.100

8601,400NA

<.200170<4.0

NA denotes Not Analyzed

-T>.._A

OO


ETC/TO X1CON IDENTIFICATIONCLIFJMT IDENTIFICATIONSAMPLE MATRIXDATCSAMJUD

4184/106MDLGW0420IWater09/26/87

4184/108MDLGWW501Water0*27/87

4184/109MDLGW04801Water09/27/87

4184/110MDLGW03201W*er09/26/17

4184/111MDLGW03901Waier09/76/87

4184/112MDLGW03501Water09/26/87

PARAMETER UNITS

Alkalinity. ToutChemical Oxygen Demand (COD)Cyanide. Total

mg/Lmg/Lmg/L

1.400180•c.02

42021<.02

37021<.02

100<5.0<.02

42026<.02

33047<.02

Hardnen. TouU mg/LResidue. Filterable (TDS) mg/LRetidue. Tocal Suapended (TSS) mg/L

1.2002.100NA

36092026.000

4701.60014,000

2001.200310

40058074

3401.20063.000

NA denote* Not Analyzed

00

CONVENT1ONALS CHEMICAL PARAMETER ANALYTICAL DATA.

CTC/TOXICON IDENTIFICATIONCLIENT IDENTIFICATIONSAMPLE MATRIXDATE SAMPLED

4184/113MDLGW03701Water09/26/87

EPAQCStandardIdentification

EPAQCStandardTtue Value

mg/L

EPAQCPereenlRecovery

PARAMETER UNITS CONCENTRATION

Alkalinity. ToUl mg/LChemical Oxygen Denund (COD) mg/LCyuude, Total mg/L

2.200<5.0<.02

WP3I4-2WP12M-2WP586

17.5145.300

9792

100

llardneu. Total mg/LResidue, filterable (TDS) mg/LResidue, Total Suipended (TSS) mg/L

1.2001.40020.000

WPJM-2WP1IS5-3WP1185-3

20.7140307

949388

NA denotes Not Analysed

-fc*

CO

oCD

Documents

GROUNDWATER MONITORING WELL SAMPLING (SECOND …1130 ug/1 (NP/SDWS of 300 and 50 ug/1, respectively.) Sample 50-01 contained iron at a concentration of 12700 ug/1 (NP/SDWS of 300 ug/1)