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ICP Test Report Certification Packet
Company name : Littelfuse, Inc. Product Series: 3AB Cartridge Product #: 322xxxP Series Issue Date: December 19, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.
Issued by: [Global EHS Engineer]
(1) Parts, sub-materials and unit parts
This document covers the 3AB Cartridge RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used
Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1
Remarks: 12A and above are RoHS compliant but not Pb Free Element used in these amperages is the 275 Pico Fuse, please see the 275 ICP test report for further information.
Form 585-047 Rev. A 2/21/06
2
Table 1: List of Raw Materials covered by this report
Item No. Raw Material Part Number Raw Material Description Page(s) 1 910-005 Fuse Cap (Base & Plating) 3-10 2 909-165 Body-Ceramic 11-39 3 87244 Adhesive (HMA) 40-45
4 082xxx Wire-Ag plated Cu 46-50 5 082xxx Wire-5% weight Ag Clad Cu 51-54 6 692535-003 Solder 55-60 7 90142 Filler-Sand 61-67 8 425907 Ink- Green 68-78 9 909-448 Body-Ceramic 79-86 10 10-1185 (497xxx) Element – Cu Clad Fe 58 Ni Ag 87-91 11 692321 Solder 92-97 12 910-xxx (910-272/910-023) Cap & Lead Assembly 98-103 13 087229 HF Epoxy Green Powder Coating 104-114
Test Report. No. CANEC1317187402 Date: 12 Nov 2013. Page 1 of 4.
DONGGUAN XINHAI METAL PRODUCTS CO.,LTD.
HENGZENG ROAD ZENGTIAN CHANGAN TOWN DONGGUAN CITY GUANGDONG PROVINCE
CHINA.
.
The following sample(s) was/were submitted and identified on behalf of the clients as : FUSE CAP.
SGS Job No. : CP13-057503 - SZ.
Client Ref. Info. :. H65 ,Ni.
Date of Sample Received :. 06 Nov 2013.
Testing Period :. 06 Nov 2013 - 12 Nov 2013.
Test Requested :. Selected test(s) as requested by client..
Please refer to next page(s)..
Please refer to next page(s)..
Test Method :.
Test Results :.
Signed for and on behalf of
SGS-CSTC Ltd..
Merry Lv.
Approved Signatory.
Test Report. No. CANEC1317187402 Date: 12 Nov 2013. Page 2 of 4.
Test Results :.
Test Part Description :.
Specimen No.. SGS Sample ID. Description.
1. CAN13-171874.002 Silvery plating on metal.
Remarks :.
(1) 1 mg/kg = 1 ppm = 0.0001%.
(2) MDL = Method Detection Limit.
(3) ND = Not Detected ( < MDL ).
(4) "-" = Not Regulated.
Elementary Analysis.
Test Method :. (1)Determination of Cadmium and Lead by ICP-OES after application of modified surface etching
digestion based on IEC62321-5:2013
(2)Determination of Mercury by ICP-OES after application of modified surface etching digestion
based on IEC 62321-4:2013
(3)With reference to IEC 62321:2008, determination of Hexavalent Chromium by spot test /
Colorimetric Method using UV-Vis..
002.
Cadmium (Cd). mg/kg. 10 ND
Lead (Pb). mg/kg. 10 ND
Mercury (Hg). mg/kg. 10 ND
Hexavalent Chromium (CrVI). - ♢ Negative
Test Item(s). Unit. MDL.
Notes :.
(1)◇Spot-test:
Negative = Absence of CrVI coating, Positive = Presence of CrVI coating;
(The tested sample should be further verified by boiling-water-extraction method if the spot test result is
Negative or cannot be confirmed.)
◇Boiling-water-extraction:
Negative = Absence of CrVI coating
Positive = Presence of CrVI coating; the detected concentration in boiling-water-extraction solution is
equal or greater than 0.02 mg/kg with 50 cm2 sample surface area.
Information on storage conditions and production date of the tested sample is unavailable and thus results
of Cr(VI) represent status of the sample at the time of testing..
Test Report. No. CANEC1317187402 Date: 12 Nov 2013. Page 3 of 4.
ATTACHMENTS
Plating Pb/Cd/Hg/Cr6+Testing Flow Chart
1) Name of the person who made testing: Michael Tso 2) Name of the person in charge of testing: Adams Yu
Sample Preparation
Sample Measurement
Metallic material
Spot test
Boiling water extraction
Adding 1,5- diphenylcarbazide for color development
A red color indicates the presence of Cr6+. If necessary, confirm with UV-Vis.
DATA
Positive
Negative
Pb/Cd/Hg Cr6+
Acid washing of plating layer
Precisely weighing sample after acid washing
Filtration
ICP-OES/AAS
DATA
Test Report. No. CANEC1317187402 Date: 12 Nov 2013. Page 4 of 4.
Sample photo:.
CANEC1317187402
CAN13-171874.002.
SGS authenticate the photo on original report only.
*** End of Report ***.
Test Report. No. CANEC1317187401 Date: 12 Nov 2013. Page 1 of 4.
DONGGUAN XINHAI METAL PRODUCTS CO.,LTD.
HENGZENG ROAD ZENGTIAN CHANGAN TOWN DONGGUAN CITY GUANGDONG PROVINCE
CHINA.
.
The following sample(s) was/were submitted and identified on behalf of the clients as : FUSE CAP.
SGS Job No. : CP13-057503 - SZ.
Client Ref. Info. :. H65 ,Ni.
Date of Sample Received :. 06 Nov 2013.
Testing Period :. 06 Nov 2013 - 12 Nov 2013.
Test Requested :. Selected test(s) as requested by client..
Please refer to next page(s)..
Please refer to next page(s)..
Test Method :.
Test Results :.
Signed for and on behalf of
SGS-CSTC Ltd..
Merry Lv.
Approved Signatory.
Test Report. No. CANEC1317187401 Date: 12 Nov 2013. Page 2 of 4.
Test Results :.
Test Part Description :.
Specimen No.. SGS Sample ID. Description.
1. CAN13-171874.001 Silvery plated metal.
Remarks :.
(1) 1 mg/kg = 1 ppm = 0.0001%.
(2) MDL = Method Detection Limit.
(3) ND = Not Detected ( < MDL ).
(4) "-" = Not Regulated.
Elementary Analysis.
Test Method :. (1)With reference to IEC 62321-5:2013, determination of Cadmium by ICP-OES.
(2)With reference to IEC 62321-5:2013, determination of Lead by ICP-OES.
(3)With reference to IEC 62321-4:2013, determination of Mercury by ICP-OES.
(4)With reference to IEC 62321:2008, determination of Hexavalent Chromium by spot test /
Colorimetric Method using UV-Vis..
001.
Cadmium (Cd). mg/kg. 2 ND
Lead (Pb). mg/kg. 2 ND
Mercury (Hg). mg/kg. 2 ND
Hexavalent Chromium (CrVI). - ♢ Negative
Test Item(s). Unit. MDL.
Notes :.
(1)◇Spot-test:
Negative = Absence of CrVI coating, Positive = Presence of CrVI coating;
(The tested sample should be further verified by boiling-water-extraction method if the spot test result is
Negative or cannot be confirmed.)
◇Boiling-water-extraction:
Negative = Absence of CrVI coating
Positive = Presence of CrVI coating; the detected concentration in boiling-water-extraction solution is
equal or greater than 0.02 mg/kg with 50 cm2 sample surface area.
Information on storage conditions and production date of the tested sample is unavailable and thus results
of Cr(VI) represent status of the sample at the time of testing..
Test Report. No. CANEC1317187401 Date: 12 Nov 2013. Page 3 of 4.
ATTACHMENTS RoHS Testing Flow Chart
1) Name of the person who made testing: Michael Tso 2) Name of the person in charge of testing: Adams Yu 3) These samples were dissolved totally by pre-conditioning method according to below flow chart (Cr6+ test method excluded).
Sample Preparation
Sample Measurement
Acid digestion with microwave/ hotplate
Filtration
Solution Residue
1) Alkali Fusion / Dry Ashing
2) Acid to dissolve
ICP-OES/AAS
DATA
Nonmetallic material
Metallic material
Adding digestion reagent
Heating to 90~95℃ for extraction
Filtration and pH adjustment
Adding 1,5- diphenylcarbazide for color development
UV-Vis
DATA
Spot test
Boiling water extraction
Adding 1,5- diphenylcarbazide for color development
A red color indicates the presence of Cr6+. If necessary, confirm with UV-Vis.
DATA
Positive
Negative
Pb/Cd/Hg
Cr6+
Test Report. No. CANEC1317187401 Date: 12 Nov 2013. Page 4 of 4.
Sample photo:.
CANEC1317187401
CAN13-171874.001.
SGS authenticate the photo on original report only.
*** End of Report ***.
Test Report. No. SHAEC1219975401 Date: 19 Nov 2012 . Page 1 of 6.
3M CHINA LIMITED .
222# TIAN LIN ROAD, SHANGHAI (200233)
.
.
The following sample(s) was/were submitted and identified on behalf of the clients as : 3M 3779-PG .
SGS Job No. : SP12-033081 - SH .
Date of Sample Received : . 14 Nov 2012.
Testing Period : . 14 Nov 2012 - 19 Nov 2012 .
Test Requested : . Selected test(s) as requested by client. .
Please refer to next page(s). .
Please refer to next page(s). .
Test Method : .
Test Results : .
Signed for and on behalf of
SGS-CSTC Ltd. .
JJ Fan.
Approved Signatory .
0000883989
Test Report. No. SHAEC1219975401 Date: 19 Nov 2012 . Page 2 of 6.
Test Results : .
Test Part Description : .
Specimen No.. SGS Sample ID. Description.
1. SHA12-199754.001 Brown solid.
Remarks :.
(1) 1 mg/kg = 1 ppm = 0.0001% .
(2) MDL = Method Detection Limit .
(3) ND = Not Detected ( < MDL ) .
(4) "-" = Not Regulated .
Halogen.
Test Method : . With reference to EN 14582: 2007, analysis was performed by Ion Chromatograph (IC). .
Test Item(s). Unit. MDL. 001.
Fluorine (F). mg/kg. 50 ND
Chlorine (Cl). mg/kg. 50 ND
Bromine (Br). mg/kg. 50 ND
Iodine (I). mg/kg. 50 ND
0000883989
Test Report. No. SHAEC1219975401 Date: 19 Nov 2012 . Page 3 of 6.
ATTACHMENTS RoHS Testing Flow Chart
1) Name of the person who made testing: Jan Shi/Yoyo Wang/Allen Xiao/Gary Xu 2) Name of the person in charge of testing: Jeff Zhang/George Xu/ Linda Li
3) These samples were dissolved totally by pre-conditioning method according to below flow chart.
(Cr6+
and PBBs/PBDEs test method excluded)
Sample Preparation
Sample Measurement
Acid digestion with microwave/ hotplate
Filtration
Solution Residue
1) Alkali Fusion / Dry Ashing
2) Acid to dissolve
ICP-OES
DATA
Nonmetallic material
Metallic material
Adding digestion reagent
Heating to 90~95℃ for extraction
Filtration and pH adjustment
Adding 1,5- diphenylcarbazide
for color development
UV-Vis
DATA
Spot test
Boiling water extraction
Adding 1,5- diphenylcarbazid
e for color development
A red color indicates the
presence of Cr6+
. If necessary, confirm with
UV-Vis.
DATA
Positive
Negative
Pb/Cd/Hg
Cr6+
Sample solvent extraction
Nonmetallic material
Concentration/ Dilution of
extraction solution
Filtration
GC-MS
DATA DATA
PBBs/PBDEs
0000883989
Test Report. No. SHAEC1219975401 Date: 19 Nov 2012 . Page 4 of 6.
Phthalates Testing Flow Chart
1) Name of the person who made testing: Elyn Yao
2) Name of the person in charge of testing: Rachel Zhang
Sample cutting/preparation
Sample measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
0000883989
Test Report. No. SHAEC1219975401 Date: 19 Nov 2012 . Page 5 of 6.
HBCDD Testing Flow Chart
1) Name of the person who made testing: Gary Xu
2) Name of the person in charge of testing: Jessy Huang
Sample cutting/preparation
Sample measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
0000883989
Test Report. No. SHAEC1219975401 Date: 19 Nov 2012 . Page 6 of 6.
Sample photo: .
SHAEC1219975401
SHA12-199754.001 .
SGS authenticate the photo on original report only .
*** End of Report *** .
0000883989
Test Report Number: SHAH00362270
Authorized by: For intertek testing services Ltd., Shanghai
Jacob Lin General Manager
Page 1 Of 5 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Applicant: ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU Date: JAN 18, 2013 GMBH
GEWERBESTRASSE 87,D-98669 VEILSDORF, GERMANY
Sample Description: Two(2) pieces of submitted samples said to be : (1) Substrate. (2) Plating. Item Name : Wire With Plating. Item No. : 101.014-.---- sliver plated copper wire Cu,Ag --%. Country Of Origin : Germany.
************************************************************************************************************************************************************ Tests Conducted:
As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************
To be continued
Test Report Number: SHAH00362270
Tests Conducted
Page 2 Of 5 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(A) Test result of RoHS Directive: Result Testing item (1)
Cadmium (Cd) content (mg/kg) ND Lead (Pb) content (mg/kg) ND Mercury (Hg) content (mg/kg) ND Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) ND
Result Testing item (2)
Cadmium (Cd) content (mg/kg) / Plating ND Lead (Pb) content (mg/kg) / Plating ND Mercury (Hg) content (mg/kg) / Plating ND Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) / Plating ND
Remark:mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter ND = not detected (B) RoHS Requirement:
Restricted substances Limits Cadmium (Cd) 0.01% (100 mg/kg) Lead (Pb) 0.1% (1000 mg/kg) Mercury (Hg) 0.1% (1000 mg/kg) Chromium (VI) (Cr6+) 0.1% (1000 mg/kg)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(C) Test method: Testing item Testing method Reporting limit
Cadmium (Cd) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Lead (Pb) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Mercury (Hg) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Chromium (VI) (Cr6+) content (for metal)
With reference to IEC 62321 Edition 1.0: 2008, by boiling water extraction and determined by UV-VIS Spectrophotometer.
0.02mg/kg with 50cm2
(in testing solution)
Date sample received: Jan.14, 2013 Testing period: Jan.14, 2013 To Jan.17, 2013
************************************************************************************************************************************************************ To be continued
Test Report Number: SHAH00362270
Tests Conducted
Page 3 Of 5 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(D) Measurement flowchart:
Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents Reference standard: IEC 62321 Edition 1.0: 2008
Remarks: *1: list of appropriate acid:
Material Acid added for digestion Polymers HNO3,HCL,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
************************************************************************************************************************************************************ To be continued
Sampling/grinding or cutting
Weigh sample and for different material, digest
the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized waterand add diphenyl-carbazide
solution
Cr6+
Weigh sample andadd organic
solvent
Soxhlet extractionor
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved
No
Cool and filter the extract
Yes
Test Report Number: SHAH00362270
Tests Conducted
Page 4 Of 5 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
************************************************************************************************************************************************************
To be continued
Test Report Number: SHAH00362270
Tests Conducted
Page 5 Of 5 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
************************************************************************************************************************************************************
End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Test Report Number : TWNC00300508
Authorized by: On Behalf of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
*THJ0300508* Page 1 of 4
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Applicant: Littelfuse Philippines Inc. Date : Mar 06, 2013 LIMA Technology Center, Lipa City,
Malvar, Batangas
Sample Description: One (1) group of submitted samples said to be : Part Description : Element - (Silver clad Cu wire with 5% Ag) 082686 Part Number : 082xxx Date Sample Received : Feb 26, 2013 Date Test Started : Feb 26, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Number : TWNC00300508
Test Conducted
*THJ0300508* Page 2 of 4
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
(Ⅰ) Test Result Summary: Result
Test Item Unit Test Method Silvery metal wire
RL
Heavy Metal
Cadmium (Cd) content ppm
With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Lead (Pb) content ppm
With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Mercury (Hg) content ppm
With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Chromium VI (Cr6+) content mg/kg with 50 cm2
With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.
Negative 0.02
Remarks: ppm = parts per million based on weight of tested sample = mg/kg
ND = Not detected
RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not found at the time of Test.
Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Feb 26, 2013 Test Period : Feb 26, 2013 To Mar 01, 2013 (Ⅱ) Limit: RoHS Limit
Restricted Substances Limits
Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
Number : TWNC00300508
Test Conducted
*THJ0300508* Page 3 of 4
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
(Ⅲ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as
detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Sampling/grinding or cutting
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
Boiling water extraction
Metal Polymers / Electronics
Negative*2 Confirm the tested samples are totally dissolved
Number : TWNC00300508
Test Conducted
*THJ0300508* Page 4 of 4
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Photo
Test Report. No. SHAEC1317518845 Date: 06 Sep 2013 . Page 1 of 6.
ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTD .
XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE, CHINA
.
.
The following sample(s) was/were submitted and identified on behalf of the clients as : LEAD-FREE SOLDER
WIRE.
SGS Job No. : SP13-026309 - SH .
Model No. :. YTW108(692535-001、692535-003、693535-004).
Composition : . Sn3.0CuRE.
Date of Sample Received : . 03 Sep 2013.
Testing Period : . 03 Sep 2013 - 06 Sep 2013 .
Test Requested : . Selected test(s) as requested by client. .
Please refer to next page(s). .
Please refer to next page(s). .
Test Method : .
Test Results : .
Based on the performed tests on submitted samples, the results of Lead,
Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB),
Polybrominated diphenyl ethers (PBDE) comply with the limits as set by RoHS
Directive 2011/65/EU Annex II; recasting 2002/95/EC. .
Conclusion :.
Signed for and on behalf of
SGS-CSTC Ltd. .
JJ Fan.
Approved Signatory .
Test Report. No. SHAEC1317518845 Date: 06 Sep 2013 . Page 2 of 6.
Test Results : .
Test Part Description : .
Specimen No.. SGS Sample ID. Description.
1. SHA13-175188.038 Silvery metal wire .
Remarks :.
(1) 1 mg/kg = 1 ppm = 0.0001% .
(2) MDL = Method Detection Limit .
(3) ND = Not Detected ( < MDL ) .
(4) "-" = Not Regulated .
RoHS Directive 2011/65/EU.
Test Method : . (1) With reference to IEC 62321-5:2013, determination of Cadmium by ICP-OES.
(2) With reference to IEC 62321-5:2013, determination of Lead by ICP-OES.
(3) With reference to IEC 62321-4:2013, determination of Mercury by ICP-OES.
(4) With reference to IEC 62321:2008, determination of Hexavalent Chromium by spot test /
Colorimetric Method using UV-Vis.
(5) With reference to IEC 62321:2008, determination of PBBs and PBDEs by GC-MS. .
038.
Cadmium (Cd) . 100 mg/kg. 2 ND
Lead (Pb). 1000 mg/kg. 2 129
Mercury (Hg). 1000 mg/kg. 2 ND
Hexavalent Chromium (Cr(VI)) . - - ♢ Negative
Sum of PBBs. 1000 mg/kg. - ND
Monobromobiphenyl . - mg/kg. 5 ND
Dibromobiphenyl . - mg/kg. 5 ND
Tribromobiphenyl . - mg/kg. 5 ND
Tetrabromobiphenyl . - mg/kg. 5 ND
Pentabromobiphenyl . - mg/kg. 5 ND
Hexabromobiphenyl . - mg/kg. 5 ND
Heptabromobiphenyl . - mg/kg. 5 ND
Octabromobiphenyl . - mg/kg. 5 ND
Nonabromobiphenyl . - mg/kg. 5 ND
Decabromobiphenyl . - mg/kg. 5 ND
Sum of PBDEs. 1000 mg/kg. - ND
Monobromodiphenyl ether . - mg/kg. 5 ND
Test Item(s). Limit. Unit. MDL.
Test Report. No. SHAEC1317518845 Date: 06 Sep 2013 . Page 3 of 6.
Test Item(s). Limit. Unit. MDL. 038.
Dibromodiphenyl ether . - mg/kg. 5 ND
Tribromodiphenyl ether . - mg/kg. 5 ND
Tetrabromodiphenyl ether . - mg/kg. 5 ND
Pentabromodiphenyl ether . - mg/kg. 5 ND
Hexabromodiphenyl ether . - mg/kg. 5 ND
Heptabromodiphenyl ether . - mg/kg. 5 ND
Octabromodiphenyl ether . - mg/kg. 5 ND
Nonabromodiphenyl ether . - mg/kg. 5 ND
Decabromodiphenyl ether . - mg/kg. 5 ND
Notes :.
(1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II
(2) ◇Spot-test:
Negative = Absence of Cr(VI) coating, Positive = Presence of Cr(VI) coating;
(The tested sample should be further verified by boiling-water-extraction method if the spot test result
is Negative or cannot be confirmed.)
◇Boiling-water-extraction:
Negative = Absence of Cr(VI) coating
Positive = Presence of Cr(VI) coating; the detected concentration in boiling-water-extraction solution is
equal or greater than 0.02 mg/kg with 50 cm² sample surface area.
Information on storage conditions and production date of the tested sample is unavailable and thus
Cr(VI) results represent status of the sample at the time of testing. .
Halogen.
Test Method : . With reference to EN 14582: 2007, analysis was performed by Ion Chromatograph (IC). .
Test Item(s). Unit. MDL. 038.
Fluorine (F). mg/kg. 50 ND
Chlorine (Cl). mg/kg. 50 392
Bromine (Br). mg/kg. 50 ND
Iodine (I). mg/kg. 50 ND
Test Report. No. SHAEC1317518845 Date: 06 Sep 2013 . Page 4 of 6.
ATTACHMENTS
RoHS Testing Flow Chart
1) Name of the person who made testing: Jan Shi/Star Wang/Shara Wang/Gary Xu 2) Name of the person in charge of testing: Jeff Zhang/George Xu/ Jessy Huang 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr
6+
and PBBs/PBDEs test method excluded)
Cr6+
Adding 1,5- diphenylcarbazide
for color development
UV-Vis
Nonmetallic material
Metallic material
Adding digestion reagent
DATA
A red color indicates the
presence of Cr6+
. If necessary, confirm with
UV-Vis.
Sample Preparation
Sample Measurement
PBBs/PBDEs
Sample solvent extraction
Concentration/ Dilution of extraction
solution
Filtration
GC/MS
DATA
ICP-OES
Solution
Filtration
Residue
1) Alkali Fusion / Dry Ashing
2) Acid to dissolve
Pb/Cd/Hg
Acid digestion with microwave/ hotplate
DATA
Heating to 90~95℃ for extraction
Filtration and pH adjustment
Boiling water extraction
Adding 1,5- diphenylcarbazide
for color development
Spot test Positive
Negative
DATA
Test Report. No. SHAEC1317518845 Date: 06 Sep 2013 . Page 5 of 6.
Halogen Testing (oxygen bomb) Flow Chart
1) Name of the person who made testing: Sisily Yin
2) Name of the person in charge of testing: Linda Li
Sample cutting/preparation
Sample measurement
Combustion in oxygen bomb
Dissolved in an absorption
solution
Filtration
Analyzed by ion
chromatography. Double confirm
by other instruments, if
necessary
DATA
Test Report. No. SHAEC1317518845 Date: 06 Sep 2013 . Page 6 of 6.
Sample photo: .
SHAEC1317518845
SHA13-175188.038 .
SGS authenticate the photo on original report only .
*** End of Report *** .
Test Report Number: SHAH00372747
Authorized By: For Intertek Testing Services Ltd., Shanghai
Jacob Lin General Manager
Page 1 Of 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Applicant: LITTELFUSE,INC. Date: APR 03, 2013 800 E. NORTHWEST HWY Attn: A.DIVIETRO/D.UNTIEDT
Sample Description: One(1) submitted sample said to be Beige Sand. Item Name : Sand. Item No. : 090142.
************************************************************************************************************************************************************ Tests Conducted:
As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************
To Be Continued
Test Report Number: SHAH00372747
Tests Conducted
Page 2 Of 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
1 (Ⅰ) Test Result Summary: Testing Item Result (ppm)
Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Remarks:ppm = parts per million = mg/kg
ND = not detected Responsibility of Chemist: Dent Fang / Leaf Liu
(Ⅱ) RoHS Requirement:
Restricted substances Limits Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)
The above limits were quoted from RoHS Directive 2002/95/EC and amendment 2005/618/EC for homogeneous material.
************************************************************************************************************************************************************ To Be Continued
Test Report Number: SHAH00372747
Tests Conducted
Page 3 Of 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅲ) Test Method: Testing item Testing method Reporting limit
Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-VIS Spectrophotometer. 1 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Remark:Reporting limit = Quantitation limit of analyze in sample
************************************************************************************************************************************************************ To Be Continued
Test Report Number: SHAH00372747
Tests Conducted
Page 4 Of 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅳ) MEASUREMENT FLOWCHART: Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents Reference standard: IEC 62321 edition 1.0:2008
Remarks: *1: List Of Appropriate Acid:
MATERIAL ACID ADDED FOR DIGESTION Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4
*2: If The Result Of Spot Test Is Positive, Chromium (Vi) Would Be Determined As Detected. ************************************************************************************************************************************************************
To Be Continued
Sampling/grinding or cutting
Weigh sample and for different material,
digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add Diphenyl-
carbazide solution
Cr6+
Weigh sample and add organic
solvent
Soxhlet extractionor
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Negative*2
Confirm the tested samples are totally
dissolved
No
Cool and filter the extract
Yes
Test Report Number: SHAH00372747
Tests Conducted
Page 5 Of 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
2 Halogen content
(Ⅰ) Test result summary:
Testing item Result (ppm)
Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND
Remarks:ppm = parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of chemist:Leaf Liu
(Ⅱ) Test method:
Testing item Testing method Reporting limit
Halogen content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm
Remark:Reporting limit = quantitation limit of analyte in sample
************************************************************************************************************************************************************ To Be Continued
Test Report Number: SHAH00372747
Tests Conducted
Page 6 Of 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅲ) MEASUREMENT FLOWCHART:
Test for halogen content REFERENCE STANDARD:EN 14582
************************************************************************************************************************************************************
To Be Continued
Add absorbent in a combustion flask & place weighed sample in equipment
Fill the combustion flask with oxygen
Ignite then leave the flask at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
Test Report Number: SHAH00372747
Tests Conducted
Page 7 Of 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Picture Of Sample
Date Sample Received:Mar.28, 2013 Testing Period:Mar.28, 2013 To Apr.2, 2013
************************************************************************************************************************************************************ End Of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 1 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Applicant: LITTELFUSE, INC. Date: Oct. 29, 2013 800 E. NORTHWEST HWY
DES PLAINES, IL 60016 ATTN: J. CABILAN / A. CESISTA JR
Sample Description: One (1) submitted sample said to be: Green ink Part Description : INK - GREEN Part Number : 425907
***************************************************************************************************************************************************** Tests conducted:
As requested by the applicant, for details refer to attached page(s). ***************************************************************************************************************************************************** Conclusion:
Tested sample Standard Result Submitted sample With reference to test method of IEC 62321 Edition 1.0: 2008
and maximum concentration limits quoted from RoHS Directive 2011/65/EU
Pass
**************************************************************************************************************************************************** To be continued
Prepared and check by: For Intertek Testing Services Ltd., Shanghai
Authorized by:For Intertek testing services Ltd., Shanghai
Joy Zhou
Jonny Jing Manager
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 2 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted 1. RoHS testing and Halogen content (I) Test Result Summary:
Testing Item Result (ppm) Heavy Metal Cadmium (Cd) content ND
Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND Halogen Content Fluorine (F) ND Chlorine (Cl) 700 Bromine (Br) ND Iodine (I) ND
Remarks:ppm = parts per million = mg/kg
ND = not detected Responsibility of Chemist:Dent Fang / Leaf Liu
***************************************************************************************************************************************************** To be continued
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 3 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (II) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm)
Lead (Pb) Content 0.1% (1000ppm)
Mercury (Hg) Content 0.1% (1000ppm)
Chromium VI (Cr6+) Content 0.1% (1000ppm)
Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(III) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-VIS Spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by Ion Chromatography
50 ppm
Remark:Reporting limit = Quantitation Limit of Analyze in Sample
***************************************************************************************************************************************************** To be continued
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 4 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (IV) Measurement Flowchart:
Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs Contents Reference Standard: IEC 62321 Edition 1.0:2008
Remarks:
*1: List of appropriate acid:
MATERIAL ACID ADDED FOR DIGESTION Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4
*2: If the result of spot test is positive, Chromium (VI) would be determined as detected.
*****************************************************************************************************************************************************
To be continued
No
Yes
Sampling/grinding or cutting
Weigh sample and for different material, digest
the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add diphenyl-carbazide
solution
Cr6+
Weigh sample and add organic
solvent
Soxhlet extraction or
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved Cool and filter the extract
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 5 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (V) Measurement flowchart:
Test or Halogen content Reference standard: EN 14582
*****************************************************************************************************************************************************
To be continued
Add absorbent in a combustion
flask & place weighted sample
in equipment
Fill the combustion flask with Oxygen
Ignite then leave the flask at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by Ion Chromatography
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 6 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted 2. Phthalate content test
With reference to EN 14372 by Gas Chromatography-Mass Spectrometry (GC-MS) analysis.
Tested Compound Result (%,w/w) Client’ requirement (%, w/w) Di-butyl phthalate (DBP) ND - Di(2-ethyl hexyl) phthalate(DEHP) ND - Benzyl butyl phthalate (BBP) ND - Sum of three phthalates ND 0.1 Di-iso-butyl phthalate (DIBP) ND 0.1
Remark:Detection Limit = 0.01%(w/w)
ND = Not Detected *****************************************************************************************************************************************************
To be continued
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 7 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
Measurement flowchart: Test for phthalate content
****************************************************************************************************************************************************
To be continued
Weigh sample and place in a
thimble
Extracted by soxhlet extraction
with organic solvent
Concentrate the extract
Make up with organic solvent
Transfer the extract into a
volumetric flask
Analyze by GC-MS
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 8 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted 3. HBCDD content
(Ⅰ)Test result summary:
Testing item Result (ppm)
HBCDD (hexabromocyclododecane) ND
Remarks:ppm = parts per million = mg/kg
ND = Not detected
(Ⅱ) Test method:
Testing item Testing method Reporting limit
HBCDD (hexabromocyclododecane) With reference to US EPA 3540C, by solvent extraction and determined by GC-MS
10 ppm
****************************************************************************************************************************************************
To be continued
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 9 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
Measurement flowchart: Test for HBCDD (hexabromocyclododecane) content
****************************************************************************************************************************************************
To be continued
Weigh sample and place into a thimble
Soxhlet extraction with organic solvent
Concentrate the extract
Analyze by GC-MS
Make up with organic solvent
Transfer the extract into a volumetric flask
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 10 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted 4. Total Antimony (Sb) Content
As per client’s request, acid digestion method was used and total Antimony content was determined by Inductively Coupled Argon Plasma Spectrometry. Result: <10ppm Remark: ppm = parts per million = mg/kg Date sample received: Oct. 16, 2013 Testing period: Oct. 16, 2013 To Oct. 29, 2013
****************************************************************************************************************************************************
To be continued
Test Report Number: 131000457SHA-004
Intertek Testing Services Ltd., Shanghai Page 11 of 11 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
Picture was provided by applicant
**************************************************************************************************************************************************** End of report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to
the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations
either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful
basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of
our gross negligence or wilful misconduct.
Test Report Number : TWNC00330773
Authorized by: On Behalf of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
*THJ0330773* Page 1 of 8 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Applicant: Littelfuse Philippines Inc. Date : Sep 12, 2013 LIMA Technology Center, Lipa City,
Malvar, Batangas
Sample Description: One (1) group of submitted samples said to be : Part Description : Body Ceramic Part Number : 909-448 Date Sample Received : Sep 06, 2013 Date Test Started : Sep 06, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Test Report
Number: TWNC00330773 Test Conducted
*THJ0330773* Page 2 of 8 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test Result Summary:
Result Test Item Unit Test Method
White ceramic RL
Heavy Metal
Cadmium (Cd) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Lead (Pb) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Mercury (Hg) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Chromium VI (Cr6+) content ppm
With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer.
ND 1
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ppm ND 5
Dibrominated Biphenyls (DiBB) ppm ND 5
Tribrominated Biphenyls (TriBB) ppm ND 5
Tetrabrominated Biphenyls (TetraBB) ppm ND 5
Pentabrominated Biphenyls (PentaBB) ppm ND 5
Hexabrominated Biphenyls (HexaBB) ppm ND 5
Heptabrominated Biphenyls (HeptaBB) ppm ND 5
Octabrominated Biphenyls (OctaBB) ppm ND 5
Nonabrominated Biphenyls (NonaBB) ppm ND 5
Decabrominated Biphenyl (DecaBB) ppm
With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
ND 5
Test Report
Number: TWNC00330773 Test Conducted
*THJ0330773* Page 3 of 8 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Result
Test Item Unit Test Method White ceramic
RL
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ppm ND 5
Dibrominated Diphenyl Ethers (DiBDE) ppm ND 5
Tribrominated Diphenyl Ethers (TriBDE) ppm ND 5
Tetrabrominated Diphenyl Ethers (TetraBDE) ppm ND 5
Pentabrominated Diphenyl Ethers (PentaBDE) ppm ND 5
Hexabrominated Diphenyl Ethers (HexaBDE) ppm ND 5
Heptabrominated Diphenyl Ethers (HeptaBDE) ppm ND 5
Octabrominated Diphenyl Ethers (OctaBDE) ppm ND 5
Nonabrominated Diphenyl Ethers (NonaBDE) ppm ND 5
Decabrominated Diphenyl Ether (DecaBDE) ppm
With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
ND 5
Halogen Content Fluorine (F) ppm ND 50 Chlorine (Cl) ppm ND 50 Bromine (Br) ppm ND 50 Iodine (I) ppm
With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND 50
Remarks: ppm = parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Sep 06, 2013 Test Period : Sep 06, 2013 to Sep 10, 2013 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
Test Report
Number: TWNC00330773 Test Conducted
*THJ0330773* Page 4 of 8 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Method: IEC 62321 edition 1.0:2008 Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by GC-MS
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
Make up with deionized water and add diphenyl-carbazide
solution
Cr6+
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
By boiling water extraction
Negative *2
Substrate Plating
Weigh sample and add alkaline solution
Definite temp. extraction
Cool and filter the extract
Cr6+
For different material, digest the sample with
appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Confirm the tested samples are totally
dissolved
Test Report
Number: TWNC00330773 Test Conducted
*THJ0330773* Page 5 of 8 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Measurement Flowchart: Test for Halogen Contents Reference Method:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling
Analyzed by ion chromatography
Test Report
Number: TWNC00330773 Test Conducted
*THJ0330773* Page 6 of 8 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for anyparticular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and onlyaccepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes nowarranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conductthe Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Number: TWNC00330773
*THJ0330773* Page 7 of 8 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Number: TWNC00330773
*THJ0330773* Page 8 of 8 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test Report Number : TWNC00294417
Authorized by: On Behalf of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
*THJ0294417* Page 1 of 5
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Applicant: Littelfuse Philippines Inc. Date : Jan 17, 2013 LIMA Technology Center, Lipa City,
Malvar, Batangas
Sample Description:
One (1) group of submitted samples said to be : Part Description : Ni42Fe58MCuAg5% Element Part Number : 497226 (497xxx) Date Sample Received : Jan 11, 2013 Date Test Started : Jan 11, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Number : TWNC00294417
Test Conducted
*THJ0294417* Page 2 of 5
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
(Ⅰ) Test Result Summary: Result
Test Item Unit Test Method Silvery metal wire
RL
Heavy Metal
Cadmium (Cd) content ppm
With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Lead (Pb) content ppm
With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Mercury (Hg) content ppm
With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Chromium VI (Cr6+) content mg/kg with 50 cm2
With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.
Negative 0.02
Remarks: ppm = parts per million based on weight of tested sample = mg/kg
ND = Not detected
RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result.
Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 11, 2013 Test Period : Jan 11, 2013 To Jan 15, 2013 (Ⅱ) RoHS Limits: Restricted Substances Limits
Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
Number : TWNC00294417
Test Conducted
*THJ0294417* Page 3 of 5
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
(Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
Boiling water extraction
Metal Polymers / Electronics
Negative*2 Confirm the tested samples are totally dissolved
Number : TWNC00294417
Test Conducted
*THJ0294417* Page 4 of 5
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as
detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Number : TWNC00294417
Test Conducted
*THJ0294417* Page 5 of 5
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Photo
Test Report Number : TWNC00340077
Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director
*THJ0340077* Page 1 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Applicant: Littelfuse Philippines Inc. Date : Nov 07, 2013 LIMA Technology Center, Lipa City,
Malvar, Batangas
Sample Description: One (1) group of submitted samples said to be : Part Description : Solder Part Number : 692321 Date Sample Received : Oct 30, 2013 Date Test Started : Oct 31, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Test Report
Number: TWNC00340077 Test Conducted
*THJ0340077* Page 2 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test Result Summary:
Result Test Item Unit Test Method
Silvery metal RL
Heavy Metal
Cadmium (Cd) content ppm
With reference to IEC 62321-5: 2013, by microwave or acid digestion and determined by ICP-OES.
ND 2
Lead (Pb) content ppm
With reference to IEC 62321-5: 2013, by microwave or acid digestion and determined by ICP-OES.
880880 2
Mercury (Hg) content ppm
With reference to IEC 62321-4: 2013, by microwave or acid digestion and determined by ICP-OES.
ND 2
Chromium VI (Cr6+) content mg/kg with
50 cm2
With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.
Negative 0.02
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting Limit, quantitation limit of analyte in sample mg/kg with 50cm2 = Milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of test. Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Oct 30, 2013 Test Period : Oct 31, 2013 to Nov 07, 2013 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
Test Report
Number: TWNC00340077 Test Conducted
*THJ0340077* Page 3 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:Cd/Pb: IEC 62321-5:2013; Hg: IEC 62321-4:2013; Chromium (VI): IEC 62321:2008
Sampling
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
Boiling water extraction
MetalPolymers / Electronics
Negative*2 Confirm the tested samples are totally
dissolved
Test Report
Number: TWNC00340077 Test Conducted
*THJ0340077* Page 4 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for anyparticular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and onlyaccepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes nowarranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conductthe Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Number: TWNC00340077
*THJ0340077* Page 5 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Number: TWNC00340077
*THJ0340077* Page 6 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test Report Number : TWNC00316622
Authorized by: On Behalf of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
*THJ0316622* Page 1 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Applicant: Littelfuse Philippines Inc. Date : Jun 18, 2013 LIMA Technology Center, Lipa City,
Malvar, Batangas
Sample Description: One (1) group of submitted samples said to be : Part Description : Cap & Lead Assy Part Number : 910-272/910-274/910-276 Date Sample Received : Jun 05, 2013 Date Test Started : Jun 06, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Tested Components:
(1) Coppery metal substrate of body (2) Silvery plating layer of body (3) Coppery metal substrate of pin (4) Silvery plating layer of pin
Test Report
Number : TWNC00316622 Test Conducted
*THJ0316622* Page 2 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test Result Summary:
Result Test Item Unit Test Method
(1) (2) (3) (4) RL
Heavy Metal
Cadmium (Cd) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND ND ND ND 2
Lead (Pb) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND ND ND ND 2
Mercury (Hg) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND ND ND ND 2
Chromium VI (Cr6+) content
mg/kg with 50
cm2
With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.
Negative Negative Negative Negative 0.02
Remarks: ppm = parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of test. Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jun 05, 2013 Test Period : Jun 06, 2013 to Jun 11, 2013 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
Test Report
Number : TWNC00316622 Test Conducted
*THJ0316622* Page 3 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
For different material, digest the sample with
appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Confirm the tested samples are totally
dissolved
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cr6+
Make up with deionized water and add diphenyl-carbazide solution
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
By boiling water extraction
Negative *2
Substrate Plating
Test Report
Number : TWNC00316622 Test Conducted
*THJ0316622* Page 4 of 6 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Number: TWNC00316622
*THJ0316622* Page 5 of 6
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Number: TWNC00316622
*THJ0316622* Page 6 of 6
Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test Report Number : TWNC00330767
Authorized by: On Behalf of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
*THJ0330767* Page 1 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Applicant: Littelfuse Philippines Inc. Date : Sep 12, 2013 LIMA Technology Center, Lipa City,
Malvar, Batangas
Sample Description: One (1) group of submitted samples said to be : Part Description : Epoxy Power Part Number : 087229 Date Sample Received : Sep 06, 2013 Date Test Started : Sep 07, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Test Report
Number: TWNC00330767 Test Conducted
*THJ0330767* Page 2 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test Result Summary:
Result Test Item Unit Test Method
Green powder RL
Heavy Metal
Cadmium (Cd) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Lead (Pb) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Mercury (Hg) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.
ND 2
Chromium VI (Cr6+) content ppm
With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer.
ND 1
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ppm ND 5
Dibrominated Biphenyls (DiBB) ppm ND 5
Tribrominated Biphenyls (TriBB) ppm ND 5
Tetrabrominated Biphenyls (TetraBB) ppm ND 5
Pentabrominated Biphenyls (PentaBB) ppm ND 5
Hexabrominated Biphenyls (HexaBB) ppm ND 5
Heptabrominated Biphenyls (HeptaBB) ppm ND 5
Octabrominated Biphenyls (OctaBB) ppm ND 5
Nonabrominated Biphenyls (NonaBB) ppm ND 5
Decabrominated Biphenyl (DecaBB) ppm
With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
ND 5
Test Report
Number: TWNC00330767 Test Conducted
*THJ0330767* Page 3 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Result
Test Item Unit Test Method Green powder
RL
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ppm ND 5
Dibrominated Diphenyl Ethers (DiBDE) ppm ND 5
Tribrominated Diphenyl Ethers (TriBDE) ppm ND 5
Tetrabrominated Diphenyl Ethers (TetraBDE) ppm ND 5
Pentabrominated Diphenyl Ethers (PentaBDE) ppm ND 5
Hexabrominated Diphenyl Ethers (HexaBDE) ppm ND 5
Heptabrominated Diphenyl Ethers (HeptaBDE) ppm ND 5
Octabrominated Diphenyl Ethers (OctaBDE) ppm ND 5
Nonabrominated Diphenyl Ethers (NonaBDE) ppm ND 5
Decabrominated Diphenyl Ether (DecaBDE) ppm
With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
ND 5
Halogen Content Fluorine (F) ppm ND 50 Chlorine (Cl) ppm 419 50 Bromine (Br) ppm ND 50 Iodine (I) ppm
With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND 50
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ppm ND 10
Dibutyl Phthalate (DBP) ppm ND 10
Benzyl Butyl Phthalate (BBP) ppm
With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS.
ND 10
Others
Hexabromocyclododecane (HBCDD) ppm
With reference to USEPA 3540C, by solvent extraction and determined by GC-MS.
ND 10
Test Report
Number: TWNC00330767 Test Conducted
*THJ0330767* Page 4 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Remarks: ppm = parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Sep 06, 2013 Test Period : Sep 07, 2013 to Sep 11, 2013 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
Test Report
Number: TWNC00330767 Test Conducted
*THJ0330767* Page 5 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Method: IEC 62321 edition 1.0:2008 Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by GC-MS
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
Make up with deionized waterand add diphenyl-carbazide
solution
Cr6+
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
By boiling water extraction
Negative *2
Substrate Plating
Weigh sample and add alkaline solution
Definite temp. extraction
Cool and filter the extract
Cr6+
For different material, digest the sample with
appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Confirm the tested samples are totally
dissolved
Test Report
Number: TWNC00330767 Test Conducted
*THJ0330767* Page 6 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test for Halogen Contents Reference Method:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling
Analyzed by ion chromatography
Test Report
Number: TWNC00330767 Test Conducted
*THJ0330767* Page 7 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test for Phthalates Contents Reference Method: EN 14372: 2004
Sampling
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MS
Test Report
Number: TWNC00330767 Test Conducted
*THJ0330767* Page 8 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Test for Hexabromocyclododecane (HBCDD) Content Reference Method:USEPA 3540C
Sampling
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MS
Test Report
Number: TWNC00330767 Test Conducted
*THJ0330767* Page 9 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for anyparticular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and onlyaccepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes nowarranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conductthe Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Number: TWNC00330767
*THJ0330767* Page 10 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Number: TWNC00330767
*THJ0330767* Page 11 of 11 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410