INTERNATIONAL QUALITY ASSURANCE PROGRAMME (IQAP ...€¦ · The ICE programme is a UNODC mandated activity and is implemented through regular budget funds and through the UNODC Global

INTERNATIONAL QUALITY

ASSURANCE PROGRAMME (IQAP)

INTERNATIONAL COLLABORATIVE

EXERCISES (ICE)

Summary Report

SEIZED MATERIAL

2018/2

INTERNATIONAL QUALITY ASSURANCE PROGRAMME (IQAP) INTERNATIONAL COLLABORATIVE EXERCISES (ICE)

2018/2-SM Copyright (c) 2019 UNODC (2)

Table of contents Introduction Page 3

Comments from the International Panel of Forensic Experts

Page

3

NPS reported by ICE participants Page 5

Codes and Abbreviations Page 7

Sample 1 Analysis Page 8 Identified substances Page 8

Statement of findings Page 13

Identification methods Page 23

Summary Page 29

Z-Scores Page 30




Summary Page 55

Z-Scores Page 56




Summary Page 80

Z-Scores Page 81




Summary Page 105

Z-Scores Page 106

Test Samples Information

Samples Comments on samples

Sample 1 SM-1 was prepared from a seizure containing 22.7 % (w/w) Cocaine base. The test sample also contained lactose with methylecgonine, benzoylecgonine and cinnamoyl cocaine as minor components

Sample 2 SM-2 was prepared from a seizure containing 9.8 % (w/w) 3,4-methylenedioxypyrovalerone base. The test sample also contained lactose.

Sample 3 SM-3 was prepared from a seizure containing 19.6% (w/w) Metamfetamine base. The test sample also contained lactose

Sample 4 SM-4 was prepared from a seizure containing 7.1 % (w/w) Amfetamine base. The test sample also contained caffeine and lactose

Samples Substances Concentrations Comments on substances

Sample 1 Cocaine 22.7 %

Lactose -

Sample 2 3,4-Methylenedioxypyrovalerone 9.8 %

Lactose -

Sample 3 Lactose -

Metamfetamine 19.6 %

Sample 4 Amfetamine 7.1 %

Caffeine -

Lactose -



Introduction

An important element of the UNODC International Quality Assurance Programme (IQAP) is the implementation of the International Collaborative Exercises (ICE). The exercises allow laboratories, from both developing and developed countries to continuously monitor their performance in drug testing on a truly global scale. This report provides information on analytical results of laboratories participating in the Seized Materials (SM) group. In order to maintain confidentiality, the participating laboratories have been assigned random “Web Codes”, which change every round. The analytical results returned by laboratories participating in ICE are evaluated by UNODC and a confidential report is provided to each laboratory on its own performance. The overall analytical results are reviewed by the UNODC’s International Panel of Forensic Experts which oversees the implementation of these exercises, and offers guidance and support in addressing relevant quality issues. The exercises provide an overview of the performance and capacity of participating laboratories and enable UNODC to tailor technical support in the laboratory sector for greatest impact. The ICE programme is a UNODC mandated activity and is implemented through regular budget funds and through the UNODC Global Scientific and Forensic Programme – Support Project (GLOU54), which operationalizes the forensic aspects of the UNODC Thematic Programme on Research, Trend Analysis and Forensics"

Comments from the International Panel of Forensic Experts

Participation of Laboratories In the 2018/2 round of the ICE programme, results were submitted within both the Seized Materials (SM) and Biological Specimens (BS) test groups by 231 laboratories in 77 countries. Within the SM test group, there were 194 participating laboratories from 69 countries and within the BS test group, results were submitted by 82 laboratories from 46 countries. Qualitative Analysis Colour tests (53% of participants) were the most commonly used screening technique for test samples in the SM test group, while GC-MS (91% of participants) was the most commonly used technique for identification/confirmation of the components in the test samples followed by FTIR (43% of participants). The results for the qualitative identification of the controlled substances in the SM test group, the number of false positive/negative results and the analyses not performed are shown in the table 1.

Table 1. Performance of participants in the 2018/2 round of ICE.

Test sample SM-1

(Cocaine) SM-2

(MDPV) SM-3

(Metamfetamine) SM-4

(Amfetamine)

Correct identification by participants

100% 94.8% 98.4% 92.7%

Number of false positives

2 7 7 7

Number of false negatives

0 6 2 13

Number of Analyses not performed

0 4 1 1



With regard to false negative results reported, there were a total of 21 (6 for SM-2, 2 for SM-3 and 13 for SM-4). In total, there were 23 false positive results for controlled substances or new psychoactive substances. Compared to the previous round, the overall number of false positive/negative results reported by ICE participants has increased. Laboratories reporting false positive or false negative results should investigate the reasons for this and corrective actions should be taken as soon as possible in order to continuously improve performance. There were a total of 6 analyses not performed, majority for SM-2. ICE participants should note that test samples can contain any of the substances in the ICE menu and screening and identification carried out should take this into account. Quantitative Analysis The number of participants who carried out quantitative analysis, 141 (72%) for SM-1, 55 (28%) for SM-2, 111 (57%) for SM-3 and 95 (48%) for SM-4 continues to be encouraging. It is also encouraging that 151 (77%) of participants in the SM test group performed quantitation and of these, 113 (74%) quantified more than one substance, 92 (60%) quantified more than 2 substances and 46 (30%) quantitated all four test samples. It is understood that quantitative analysis of controlled substances is often governed by local legislation and the requirements of prosecution. With regard to the analytical techniques used by participants performing quantitation, 56% used GC-FID, 32 % used UPLC/HPLC-DAD and 19% used mass spectrometric methods (i.e. GC-MS, GC-MS-MS, LC-MS, LC-MS-MS). z-scores obtained by participants in quantification are shown in table 2 below.

Table 2. Quantitative performance of participants in the 2018/2 round of ICE.

z-score

Test sample

SM-1 (Cocaine)

SM-2 (MDPV)

SM-3 (Metamfetamine)

SM-4 (Amfetamine)

|z| < 2, satisfactory 77% 82% 80% 83%

2 ≤ |z| ≤ 3, questionable 10% 7% 5% 7%

|z| > 3, unsatisfactory 13% 11% 15% 10%

According to the recommendations in ISO 13528:2005, an unsatisfactory z-score is considered to give an action signal and a questionable z-score is considered to give a warning signal. A single action signal or warning signals in two successive rounds shall be taken that an anomaly has occurred that requires investigation. Participants with z-scores outside acceptable limits should review their quantification procedures as soon as possible. The following laboratories obtained a single action signal or warning signal in the two successive rounds of 2018/1 and 2018/2 and shall take this as an anomaly, which requires further investigation: 07RNYQ, 22YK4V, 2P2PU2, 4QMQQQ, 60XF00, 8TKCKC, 8XQEGQ, A8R888, AAPSTZ, CELGEE, ECOCCC, F9BYIQ, GU6GGK, HATVYH, HDYYZY, HRZZZ0, KOQ1NC, LC7LMZ, LLTO7L, NVWID3, PUTLIT, QMQ1QP, RPI8GV, T0PFVQ, WWWBLX and Y3XX1B. Of the 13 laboratories that obtained a single action or warning signal in ICE rounds 2017/2 and 2018/1 reported in the previous summary report, the following laboratories also obtained an action or warning signal in 2018/2: 07RNYQ, 2P2PU2, 4QMQQQ, 8TKCKC, AAPSTZ, HDYYZY, HRZZZ0, NVWID3, WWWBLX and Y3XX1B. Laboratories that need to perform quantitation routinely are encouraged to participate regularly in external proficiency testing or collaborative exercises such as the ICE programme. This will enable laboratories to assess the quality of their quantitative methods through the z-score values obtained. In addition to the use of z-scores as a measure of performance in quantitation, participants are encouraged to compare their results with the assigned values provided in individual quantification reports, to assess the accuracy of their quantitative performance. Laboratories reporting false positive or false negative results should investigate the root causes and corrective actions taken promptly in order to continuously improve performance. Participation in the ICE programme also helps in monitoring the effect of corrective actions. UNODC would like to acknowledge the valuable contribution of the Chemical Metrology Laboratory of the Health Sciences Authority, Singapore, for the provision of specific software used for the quantitative statistical calculations in the ICE programme.



New Psychoactive Substances (NPS) reported by laboratories participating in the 2018/2 round of the ICE programme During the 2018/2 round of ICE, participating laboratories provided information on NPS that had been identified in their laboratories. In total there were 175 reports of 116 substances. The most commonly reported substances were synthetic cannabinoids (35%) followed by synthetic cathinones as shown in figure 1.

Figure 1. NPS reported by ICE laboratories during the 2018/2 round of ICE

In terms of the mode of action of the NPS reported by ICE participants, the predominant substances reported were synthetic cannabinoid receptor agonists (SCRA) (35%), while 34% were stimulants as shown in figure 2.

Figure 2. Mode of action of NPS reported by ICE participants in the 2018/2 round of ICE

Synthetic

cannabinoids

35%

Synthetic

cathinones

26%

Other substances

22%

Phenethylamines

9%

Phencyclidine-type

substances

6%

Tryptamines

2%

Synthetic

cannabinoid

receptor agonists

35%

Stimulants

34%

Hallucinogens

10%

Opioids

8%

Dissociatives

5%

Sedatives/Hypnotics

5%

Others

3%



NPS most commonly reported by laboratories participating in ICE 2018/2 The substances most often reported by ICE participants was ketamine followed equally by the synthetic cannabinoid receptor agonists 5F-MDMB-PINACA (methyl 2-(1-(5-fluoropentyl)-1H-indazole-3-carboxamido)-3,3-dimethylbutanoate and 5F-MDMB-PICA (methyl 2-(1-(5-fluoropentyl)-1H-indole-3-carboxamido)-3,3-dimethylbutanoate. For further details on these substances and others reported to the UNODC Early Warning Advisory, ICE participants can log on to the UNODC ICE portal and select the icon for the Early Warning Advisory on New Psychoactive substances as shown below.



Codes and Abbreviations

(+) “positive”: Indicates that the analyte is identified; for presumptive tests (e.g. colour reactions), indicates that a positive reaction was obtained.

(-) “negative”: Indicates that the analyte is not identified.

(ANP): Analysis not performed.

Tech Code Name

140 Colorimetric reactions

141 Marquis reagent (sulphuric acid, formaldehyde)

142 Cobalt thiocyanate

150 Thin Layer Chromatography

160 High/Ultra High Performance Liquid Chromatography

161 High Performance Liquid Chromatography with diode array detection

170 Gas Chromatography NPD

171 Gas Chromatography FID

172 Gas Chromatography ECD

180 Gas Chromatography/Mass Spectrometry

190 Fourier Transform Infrared Spectrometry

200 Spectrophotometry (visible, UV)

210 Others (specify)

211 NMR

220 Microcrystal test

230 Liquid chromatography/mass spectrometry

231 Liquid chromatography/tandem mass spectrometry

250 Raman Spectroscopy



Sample 1 Analysis

Identified substances for Test Sample 1

Code Identified Substances

006FMT cocaine

02OWVV cocaina

07RNYQ Cocaíne Hydrochloride

0O73XC CLORHIDRATO DE COCAINA

14YQYB cocaine

1IIEIC Cocaine

1KOSTW Cocaine

1PSOP9 cocaine HCl

222A22 cocaine

22YK4V cocaine and its main metabolites

2333DY cocaine

2BSDEQ cocaine

2P2PU2 Cocaine

31933H cocaine

33Q3N2 Cocaine

3CUTP4 Cocaine

3EOHEE cocaine

3JJ2TA COCAINE

44N4AK cocaine

49LF34 Cocaine

4EF44P COCAINE

4FMLRF cocaine

4ITTTE cocaine

4QMQQQ Cocaine

4STTTT Cocaine

555HC5 Cocaine

55IZ55 cocaine

5BOT5R Cocaine

5W5519 COCAINE

60XF00 Cocaine HCl

64UHPY Cocaina

6C7TVN Cocaine

7HN7A7 Cocaine

7JGGMW cocaine

7P5A33 Cocaine

7S7SS2 Cocaine

7ULAFF Cocaine

7UN77R Cocaine Hydrochloride

7Z33IM cocaine

8288I1 Cocaine-Lactose




8828D8 Cocaine

8TKCKC cocaïne chlorhydrate

8XQEGQ Cocaine

9CKOOD Cocaine

9DKDUD cocaine

9LZ9YA Cocaïne

9N8FTT Cocaine

9ONAKN Cocaine

9QNQPB cocaine

9WFUHI Cocaine

9YN990 Cocaine

A8R888 Cocaine

AAPSTZ cocaine

ADPI7V cocaine

AEFKAT Cocaine

AGJ544 cocaine

AIQBL5 cocaine

AIW1Z2 Cocaine

ANAAAW Cocaine

AOZMSG COCAINE 22.7%

BEXBRB cocaine

BLBOCB Cocaine Hydrochloride

BSWNB0 cocaine

BUHHL2 Cocaine

BZZZIR Cocaine

C9QQGT Cocaine

CELGEE Cocaine

CLRNDG Cocaine

CMZFLS COCAINE HYDROCHLORIDE

CPBBXT Cocaine

CTRBHS Cocaine.

D3UIUC Cocaine

DIIBXI Cocaine Hydrochloride

DPAIVA cocaine

DYZ53I Cocaine hydrochloride

ECOCCC cocaïne

EDHZTN Cocaine

EQWWGJ Cocaine

ESWD79 Cocaine

F0000S Cocaine

F9BYIQ Cocaine

FD4JOW Cocaine

FPTIMV Test sample 2018/2/SM-1 contains cocaine

GCFWS5 cocain




GF7VNQ Cocaine

GFFGAC COCAINE

GKMCN5 Cocaine

GU6GGK Cocaine

H6MPDC Cocaine HCl + LACTOSE

H8G1O8 cocaïne

HATVYH Clorhidrato de Cocaina

HDYYZY cocaine

HEVEPB Cocaine and Lactose

HGGHOG cocaine

HHDUPI Cocaine

HI4WNN Cocaine + Cis-cinnamoylcocaine

HPIHHH cocaine hcl

HRFHJD Cocaine

HRZZZ0 Cocaine

HUAI9B Cocaine

ICZF4Z Cocaine

IL7F1S cocaine

IODUOV Cocaine

IXI4IQ Cocaine

JDZDJJ cocaine

JXQBZB cocaine

K59V35 Cocaine

K9O99N cocaine HCl

KHGLHU Cocaine

KILSPH Cocaine

KOQ1NC Cocaine

KSIKUP cocaine

KUVU4U cocaine

L9LV6L Cocaine

LC7LMZ Cocaine

LLTO7L Cocaine, Lactose

LTTTTQ Cocaine

MFE65O cocaine + lactose

MJMMJM cocaine

MR1LVU Cocaine Hydrochloride

MSFAND cocain

MSHBVG cocaine

N8BKMB Cocaine

NAK5A7 COCAINE

NCCCCR Cocaine

NPEUNW Cocaine

NSALLN COCAINE

NVWID3 COCAINE




OB929H cocaine

OKBALQ Cocaine

OLWSRI cocaine

ORPCAT cocaine

PCYCJC cocaine

PM7GBZ Cocaine hydrochloride

PMDM1U COCAINE

PMR0Q7 cocaine

PQIKKZ cocaine

PUTLIT Cocaine

QBF6VQ cocaine

QJJYGQ cocaina

QJOV22 Cocaine

QMQ1QP Cocaine

QORSXL Cocaine

QPXWKT Cocaine

QRCK2V cocaine

QRDRJ1 Cocaine + Lactose

QTQQQ1 cocaine

R2YIAE cocaine and cinnamoyl cocaine isomer

R7GREQ Cocaine

RCBIBN cocaine

RDRW1X cocaine

RPI8GV Cocaine

RRFXUO Cocaine

S919AS Cocaine

SBKWJS cocaine

SHIGZS cocaine, lactose

SRCKGX Cocaine

SUSSDP Cocaine

SV4SBQ Cocaine

SYLJNC cocaine

SYYY0F cocaine hydrochloride

SZVWV9 cocain

T0PFVQ Cocaine

TELOLF Cocaine

U3WKHW Cocaine

U479HU Cocaine

UHJIRN Cocaine

UNNSU8 Cocaine

USULOL Cocaine

UTTTWF Cocaine

V4HVM5 Cocaine

VBO7OP cocaine




W7K0RA cocaine

WEJJEJ Cocaine HCl

WMUWWC cocaine and metabolites

WPE9JA cocaine

WV88U8 COCAINE

WWWBLX Cocaine

XGLCLJ cocaine, allopseudococaine,norcocaine,cinnamoylcocaine,benzoylcocaine,ecgonine methyl ester

XLNP6X Cocaine

XUE0RE Cocaine

Y3XX1B cocaine

Y68SYY COCAINE

YMK92M cocaine

YQELRV cocaine

YQXDTM cocaine

YS66H6 cocaine

YSSSDR cocaine

YYONQA cocaine

Z00LTY Cocaine

Z7F75I COCAINE

Z7JWAE Cocaine Hydrochloride

ZJZZZ3 Cocaine



Statement of findings for Test Sample 1

Code Cocaine Lactose

006FMT + + MARQIUS REAGENT: negative result, COBALT THIOCYANATE: positive result, GC-MS: cocaine (compared with library MS spectrum of cocaine), FTIR: cocaine (compared with IR spectrum of cocaine), FTIR: lactose (spectrum of ethanol extract residue compared with IR spectrum lactose)

02OWVV + - 28.7 % de cocaína HCL

07RNYQ + ANP Powder contains cocaine - 21,8 % as hydrochloride

0O73XC + + PRUEBA DE SCREENING: TIOCIANATO DE COBALTO POSITIVO, PARA CLORUROS NITRATO DE PLATA PRECIPITADO POSITIVO (+) CROMATOGRAFIA EN CAPA FINA Rf CORRESPONDE A COCAINA, FTIR ESPESTRO PICOS ESPECIFICOS PARA COCAINA

14YQYB + ANP SM1 contains 19.9% cocaine.

1IIEIC + + This sample is cocaine.

1KOSTW + -

1PSOP9 + + 21,54 % cocaine base, (norcocaine, trans,cis - cinnamoylcocaine, methyl-ecgonidine), laktose,

222A22 + ANP also detected: anhydroecgonine methyl ester, benzoic acid

22YK4V + ANP tested by gc msd

2333DY + + laktóz

2BSDEQ + + White powder containing 21.6%w/w cocaine and lactose

2P2PU2 + + Cocaine was identified in SM1. Percentage as base is 25.75 %. In addition Ecgonidine and lactose were identified.

31933H + +

33Q3N2 + ANP Item 2018/2/SM-1 found to contain Cocaine.

3CUTP4 + + Lactose

3EOHEE + ANP cocaine

3JJ2TA + ANP

44N4AK + +

49LF34 + + The test sample 2018/2/SM-1 contains 21.22 % m/m cocaine base.

4EF44P + + LACTOSE




4FMLRF + + Cocaine in mixture with lactose and impurities

4ITTTE + + Also contains lactose

4QMQQQ + - Cocaine was found in the sample

4STTTT + ANP COCAINE is controlled by the Misuse of Drugs Act (as amended) as a Class A drug.

555HC5 + + Cocaine was identified by TLC and GC/MS ,quantified by GC.

55IZ55 + + cocaine was detected

5BOT5R + ANP

5W5519 + + LACTOSE

60XF00 + - contain Cocaine 21.14% as base

64UHPY + + Clorhidrato de Cocaina y lactosa

6C7TVN + + The test sample 2018/2/SM-1 was found to contain cocaine and lactose.

7HN7A7 + ANP In cobalt thoocyanate test, violet colour appears.We confirm with TLC and GCMS.

7JGGMW + + cocaine + lactose

7P5A33 + ANP

7S7SS2 + + The sample contains Cocaine

7ULAFF + ANP Test sample 2018/2/SM-1 was confirmed to contain cocaine, a DEA schedule II substance.

7UN77R + + The sample 2018/2/SM-1 was found to contain 224 milligrams of a white powder. This powder was found to contain a mixture of cocaine hydrochloride and lactose. The purity of cocaine was found to be 25% calculated as salt form.

7Z33IM + ANP It include cocaine, also minor components which benzoyl Ecgonine and Andhydroecgonine methyl ester.

8288I1 + +

8828D8 + + The sample contains cocaine which is listed as a controlled drug according to french order, appendix I of February 22nd 1990.

8TKCKC + + cocaïne chlorhydrate (22,9% as base) + lactose

8XQEGQ + + Lactose




9CKOOD + ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonine) calculated as the hydrochloride 23 % (w/w)

9DKDUD + + cocaine 24% base - Lactose

9LZ9YA + - 25%

9N8FTT + + Mass spectrometry profile correlation between sample and reference material certified

9ONAKN + ANP SM-1 was found to contain 21.3% cocaine

9QNQPB + + lactose

9WFUHI + - The powder was analysed and found to contain Cocaine. A further sample of the powder was analysed and found to contain 22% (weight for weight) Cocaine. Cocaine is a class A controlled drug within the provisions of the Misuse of Drugs Act 1971.

9YN990 + ANP Sample SM-1 found to contain Cocaine.

A8R888 + + SM 01 was found to contain cocaine Hcl and lactose

AAPSTZ + ANP

ADPI7V + + lactose

AEFKAT + + The sample contains Cocaine*HCl and Lactose, with 22.52% Cocaine base

AGJ544 + ANP

AIQBL5 + ANP

AIW1Z2 + ANP Controlled drug, Cocaine, present in sample. Concentration approx 22%

ANAAAW + + Sample 2018/2/SM-1 contains cocaine, lactose and cocaine derivates as minor components. Cocaine base concentration is (17,1 ± 0,2) %.

AOZMSG + -

BAYSRL + +

BEXBRB + ANP Examination of sample SM-1 revealed the presence of cocaine

BLBOCB + + the sample contains cocaine hydrochloride (22.3 +/- 0.4 % as cocaine free base) and lactose

BSWNB0 + ANP

BUHHL2 + ANP From screening test using (CT) and from confirmation test using (GC-MS), the sample was found to contain the controlled drug (Cocaine).




BZZZIR + ANP SM-1 contain Cocaine which is controlled under Malaysian Dangerous Drug Act 1952

C9QQGT + + Using the techniques CR, TLC, GC-MS and FT-IR sample was found to contain Cocaine and Lactose

CELGEE + ANP Sample tested positive for cocaine during screening with GC-MS. The latter was confirmed using GC-MS. The % purity by weight was 25.03%.

CLRNDG + + Sample contains %23 cocaine

CMZFLS + + A) One brown tinted glass container, labelled "2018/2/SM-1" "6, with attached black plastic lid that contained 209 milligrams of a white powder. This white powder was found to contain Cocaine Hydrochloride at an average purity of 23% in the salt form. Cocaine Hydrochloride is a Class A drug under the provisions of the Misuse of Drugs Act 1971 (as amended). Lactose is not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

CPBBXT + + We found a mixture of cocaine and lactose. The concentration of cocaine is 26.0% w/w.

CTRBHS + ANP This sample was found to contain Cocaine, which is a Class A controlled substance under the Misuse of Drugs Act 1971.

D3UIUC + ANP The sample contain cocaine

DIIBXI + + Item 2018/2/SM-1 was found to contain one glass vial which held 225 milligrams of white powder. This powder contained an average of 25% COCAINE HYDROCHLORIDE.

DPAIVA + + lactose

DYZ53I + +

ECOCCC + + SM1 contient de la cocaïne avec du lactose, de l'ecgoninemethylester et de la cinnamoylcocaïne.

EDHZTN + ANP One glass bottle containing 0.22 grammes of a powder containing 0.04 grammes of cocaine.

EQWWGJ + ANP In the sample 2018/2/SM1 was detected the presence of cocaine as base in percentage by weight of 22,7 %.

ESWD79 + + Also it was found as a diluent: lactose.

F0000S + ANP No

F9BYIQ + -

FD4JOW + + the sample contains cocaine and Lactose

FPTIMV + +

GCFWS5 + ANP




GF7VNQ + + Lactose is also present.

GFFGAC + + WAS FOUND COCAINE 20.8 (+/-) 1.4% AND LACTOSE

GKMCN5 + ANP The sample was found to contain 21.9% of cocaine (as base).

GU6GGK + ANP

H6MPDC + + The SCOTT test was able to observe a positive reaction to Cocaine (Blue color). Also used the MARQUIS test but without any reaction. What came to be confirmed after the application of TLC and FTIR tests. With FTIR, it was also possible to observe the presence of LACTOSE For TLC, a glass plate (20 × 20 cm) coated with silicon oxide was used. The solvent used was dichloromethane and the eluent used was methanol. Finally the plaque was observed using ultaviolet light the wavelength of approximately 254 nm and subsequently revealed using the developer of Dragendorf.

H8G1O8 + + Cocaïne is sheduled as illicit drug in France.

HATVYH + + Lactosa, Acido benzoico, Ecgonina Metil Ester, Norcocaina, Ecgonidina Metil Ester, Cis- Cinnamoilcocaina, Trans-Cinnamoilcocaina y Benzoilecgonina

HDYYZY + ANP

HEVEPB + + The Test sample 2018/2/SM-1 was analyzed by Thin Layer Chromatography technique and was found to contain Cocaine and Lactose.

HGGHOG + ANP

HHDUPI + ANP Cocaine is a Class A controlled drug subject to the provisions of the Misuse of Drugs Act 1971. The purity was ~22% expressed as base.

HI4WNN + ANP Substance routinely detected.

HPIHHH + + lactose

HRFHJD + + On analysis, I found the sample "SM-1" containing Cocaine and Lactose

HRZZZ0 + ANP -

HUAI9B + + The sample contained 22.6% (w/w) Cocaine (base) Lactose also detected in the sample.

ICZF4Z + + The sample contains 22.8% ± 1.4%. Also contain lactose

IL7F1S + + The sample contains 20,17±0,77 weight% cocaine-base. The sample also contains lactose.

IODUOV + ANP Powder containing cocaine




IXI4IQ + ANP

JDZDJJ + +

JXQBZB + + cocaine + lactose

K59V35 + + 2018/2/SM-1 contains Cocaine. It also contains anhydroecgonine methyl ester, ecgonine methyl ester, ecgonine, cinnamoylcociane isomers (cis and trans) and benzoylecgonine. It also contains lactose.

K9O99N + + lactose

KHGLHU + + Cocaine in lactose powder

KILSPH + ANP White powder and odorless

KOQ1NC + +

KSIKUP + + cocaine and lactose

KUVU4U + + In the analisys was obteined (cocaine), which controled substance and lactose which is uncontroled substance for Colombia

L9LV6L + ANP

LC7LMZ + + It has been detected the presence of cocaine in the sample.

LLTO7L + + This powder was found to contain cocaine together with the adulterant lactose

LTTTTQ + ANP Sample 2018/2/SM-1 was found to contain cocaine.

MFE65O + + The sample was analyze by GC-MS with differents solvents: Methanol, chloroform, ethanol and ethanol with internal standard.

MJMMJM + - The sample contains 20.5% cocaine as a free base

MR1LVU + + Sample 2018/2/SM-1 contained Cocaine Hydrochloride, at a concentration of 22% (calculated as base), together with the adulterant Lactose. Cocaine Hydrochloride is a Class A controlled drug under the provision of the Misuse of Drugs Act 1971 (as amended). Lactose is not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

MSFAND + - lactose

MSHBVG + + found cocaine with purity of 23 %

N8BKMB + ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule 1 2. (2) Cocaine (benzoylmethylecgonine) calculated as the hydrochloride 24 % (w/w)




NAK5A7 + ANP Sample 2018/2/SM-1 was found to contain cocaine.

NCCCCR + + SM-1 was contained cocaine base.The test sample also contained lactose, methylecgonidine

NPEUNW + + A composite was formed from 1 unit for testing of 1 unit received. Cocaine hydrochloride and lactose confirmed in the composite.

NSALLN + ANP TEST SAMPLE 2018/2/SM -1 CONTAIN COCAINE

NVWID3 + + After chemical analysis was performed the sample was contained COCAINE and Lactose .

OB929H + ANP

OKBALQ + ANP

OLWSRI + ANP It include only cocaine

ORPCAT + + Table 1 Schedule 1, Narcotic substances (not used by medicine)

PCYCJC + ANP cocaine is controlled by the Royal Decree of the 6th of september 2017

PM7GBZ + ANP The sample contains Cocaine hydrochloride and traces of caffeine and phenacetine. The purity of the sample is 26.16% as cocaine base.

PMDM1U + ANP White powder material that contains drug under international controle - COCAINE.

PMR0Q7 + + positive for illicit substance

PQIKKZ + ANP

PUTLIT + ANP The sample contains cocaine.

QBF6VQ + ANP cocaine

QJJYGQ + + cocaina clorhidrato y lactosa

QJOV22 + ANP It include only cocaine

QMQ1QP + + The sample contains cocaine and lactose as an adulterant. Cocaine as a psychoactive substance is controlled in Poland.

QORSXL + + Cocaine (21.1%) and lactose

QPXWKT + + Presence of cocaine hydrochloride and lactose was detected in the sample. The sample also contained multitude of trace level alkaloid impurities (cis/trans)cinnamoylcocaine, methyl ester ecgonine, benzoyl ecgonine.

QRCK2V + + lactose




QRDRJ1 + + In the 2018/2/SM-1 it was proved presence of Cocaine and Lactose, with a quantification as base of 22.7%. It was also proved the presence of ecgonidine methylester and cynnamoilcocaine

QTQQQ1 + ANP cocaine was detected by GC/MS and quantified by GC/FID

R2YIAE + - Examination and analyses performed on the solid in SM-1 showed it to contain cocaine hydrochloride (a central stimulant) and cinnamoyl cocaine isomer

R7GREQ + ANP Cocaine confirmed in SM-1.

RCBIBN + + cocaine

RDRW1X + ANP It include only cocaine

RPI8GV + + Identified by GCMS & LCMSMS technique and quantified by GC-FID technique.

RRFXUO + + Sample contained cocaine as hydrochloride and LACTOSE. Identification of cocaine by FTIR and GC/MS, quantification by GC/FID. Identification of LACTOSE by FTIR and Colorimetric Reactions (MolishTest).

S919AS + - Sample turned white to blue colour with Cobalt ThioCyanate test and Cocaine was found in GCMS analysis

SBKWJS + + ./.

SHIGZS + + The sample contains cocaine which is scheduled as illicit drug in France. The lactose is not scheduled as illicit drug in France. It's a cutting agent.

SRCKGX + + The sample contains cocaine. The content of cocaine is determined to 24 % (as cocainehydrochloride). Cocaine is a controlled substance in X.

SUSSDP + -

SV4SBQ + ANP Powder contains cocaine. Cocaine is a controlled drug under the Misuse of Drugs Acts, 1977 to 2016. The cocaine in this case is not exempt from control under subsection (1) of Section 3 of the Misuse of Drugs Act, 1977 under the terms of the Misuse of Drugs (Exemption) Order, 2017. The Exemption Order does not provide for an exemption in respect of Section 15 of the Misuse of Drugs Act, 1977. The cocaine content of the powder was found to be 21.6 percent.

SYLJNC + ANP The sample contains cocaine (23.4%)

SYYY0F + + White powder containing by weight 24.8%w/w cocaine expressed as free base

SZVWV9 + +

T0PFVQ + - The analysis confirmed that the SM-1 contains cocaine 19.3% w/w.

TELOLF + + In the sample SM-1 there is a cocaine. Cocaine is on the list of drugs.




U3WKHW + -

U479HU + - Cocaine

UHJIRN + -

UNNSU8 + ANP Based on the above analysis, the sample was found to contain cocaine

USULOL + ANP Satisfied with result obtained

UTTTWF + + Cocaine cut with lactose was identified

V4HVM5 + + The sample contained 19.6% cocaine (w/w base). The sample also contained lactose and cinnamoyl cocaine, norcocaine, methylecgonine and anhydroecgonine methyl ester as minor components.

VBO7OP + - Non addulterants

W7K0RA + ANP this finding was obtained with Cobalt thiocyanate test and thin layer chromatography

WEJJEJ + + Base Cocaine 21.80+-1.96% (w/w) and Lactose

WMUWWC + - cocaine ecgoninametilester benzoilecgonina

WPE9JA + + cocaine was detected by GC/MS, confirmed by FTIR and quantified by GC/FID

WV88U8 + + LACTOSE

WWWBLX + ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonine) calculated as the hydrochloride 19 % (w/w)

XGLCLJ + + The major compound we founded in sm-1 after GC/MS injection is cocaine, the overs compounds were in trace

XLNP6X + + Cocaine and Lactose

XUE0RE + + The sample contains 19.61 % of Cocaine and also contains Benzoylecgonine and Ecgonine methyl ester

Y3XX1B + + samle is mixture of cocaine and lactose

Y68SYY + ANP On analysis of a representative sample of the powder cocaine was detected with a purity of approximately 23% (calculated as base).

YMK92M + ANP In the test simple 2018/2/SM-1 was detected cocaine

YQELRV + + The sample contains cocaine. The concentration has not been determined.




YQXDTM + ANP White powder containing 23.8%w/w of cocaine

YS66H6 + ANP found cocaine 22.0%ww

YSSSDR + +

YYONQA + ANP White powder containing cocaine (24.5%w/w) wich is controlled by national law

Z00LTY + ANP 2018/2/SM-1 has been detected containing Cocaine.

Z7F75I + ANP ECGONIDINE, ECGONINE METHYL ESTER, CINNAMOYLCOCAINE

Z7JWAE + ANP The white powder was analysed and found to contain Cocaine Hydrochloride.

ZJZZZ3 + - Cocaine and sugar are found due to our analysis in the identification part. In the quantification part, the ratio of cocaine is found as 22.4 %



Identification methods for Test Sample 1

Analytical Technique Codes

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

006FMT S S S SI I

02OWVV SI SI I SI

07RNYQ SI I I

0O73XC S S I I

14YQYB SI SI SI S immunichromatography

1IIEIC S I I

1KOSTW I I

1PSOP9 SI I I

222A22 S I I

22YK4V SI I

2333DY I SI SI

2BSDEQ I SI I

2P2PU2 S S I I S Fast blue B test

31933H S S S SI I

33Q3N2 S I

3CUTP4 I SI I

3EOHEE SI

3JJ2TA S S S I

44N4AK S I I

49LF34 I SI

4EF44P SI I

4FMLRF I S I I S

4ITTTE I SI I

4QMQQQ S S SI

4STTTT S S I

555HC5 S I I

55IZ55 SI I

5BOT5R SI

5W5519 SI I

60XF00 S S I I I

64UHPY SI S S I I I

6C7TVN S S S SI I

7HN7A7 S S I I

7JGGMW SI SI

Legend: S ... used for Screening I ... used for Identification SI ... used for both



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

7P5A33 I I I SI Rapid test

7S7SS2 S I I

7ULAFF S S S I

7UN77R S S I I S Simons Reagent

7Z33IM SI SI I SI

8288I1 S S I I

8828D8 I I

8TKCKC I I

8XQEGQ S I I I

9CKOOD S I I GC-FTIR

9DKDUD SI

9LZ9YA S I

9N8FTT I I

9ONAKN S S I

9QNQPB I I SI I

9WFUHI S I

9YN990 S I

A8R888 S I SI S

AAPSTZ S S S I S

ADPI7V S I SI SI

AEFKAT S I

AGJ544 SI

AIQBL5 SI SI I

AIW1Z2 SI I GC-IRD

ANAAAW S S S I I

AOZMSG S SI SI

BAYSRL SI I

BEXBRB S I

BLBOCB S S S I I I I GC/MS/MS

BSWNB0 SI

BUHHL2 S S I S Negms

BZZZIR S S S I

C9QQGT S S S I I

CELGEE SI

CLRNDG S I I

CMZFLS S S I I S Simons Reagent

CPBBXT SI SI SI I I

CTRBHS S S I

D3UIUC SI ASAP-QTOF



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

DIIBXI S S S I I

DPAIVA I SI I

DYZ53I S I I I I

ECOCCC S I I I I HPLC/RID

EDHZTN S S I SI I

EQWWGJ S S I S TANRED

ESWD79 I SI

F0000S S S I I

F9BYIQ S I SI

FD4JOW S I I

FPTIMV SI I I

GCFWS5 S S I I

GF7VNQ I I S

GFFGAC S S I I

GKMCN5 I SI

GU6GGK SI

H6MPDC S S S I I

H8G1O8 I SI I

HATVYH S I I

HDYYZY I SI

HEVEPB S S SI S Fast Blue B Salt Test

HGGHOG S S I

HHDUPI S S I

HI4WNN S S I

HPIHHH SI I

HRFHJD S I I

HRZZZ0 SI

HUAI9B S S S I I I

ICZF4Z S I I

IL7F1S S I SI I

IODUOV S I I SI

IXI4IQ I

JDZDJJ I S

JXQBZB S I I

K59V35 I I I S I SI SI I I

K9O99N I SI

KHGLHU I SI I

KILSPH S S SI I

KOQ1NC S I I SI



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

KSIKUP I SI I

KUVU4U S S I I

L9LV6L S I

LC7LMZ SI S I

LLTO7L S S I I

LTTTTQ S S SI

MFE65O SI I

MJMMJM SI

MR1LVU S S I I

MSFAND SI

MSHBVG SI I

N8BKMB S I I I GC-FTIR

NAK5A7 I SI

NCCCCR I SI I

NPEUNW SI I

NSALLN S I

NVWID3 SI S I

OB929H SI SI SI I

OKBALQ SI I

OLWSRI S I SI SI

ORPCAT S S S I I I

PCYCJC I S

PM7GBZ S S S I

PMDM1U S S I

PMR0Q7 S S S I I

PQIKKZ SI

PUTLIT SI

QBF6VQ S S S I

QJJYGQ S S S I I I I

QJOV22 SI SI SI

QMQ1QP SI I Tollens reaction

QORSXL S I

QPXWKT S I I I S

QRCK2V I I SI I

QRDRJ1 I SI I I I

QTQQQ1 SI

R2YIAE S S S I I I

R7GREQ S S S I I

RCBIBN SI SI SI I SI I



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

RDRW1X S I S I I

RPI8GV I S S SI I I

RRFXUO I SI I

S919AS S S S I I

SBKWJS SI SI

SHIGZS S SI I I

SRCKGX I I

SUSSDP I S

SV4SBQ I I

SYLJNC S S S I I

SYYY0F I SI

SZVWV9 SI I

T0PFVQ S S S I I

TELOLF S S S I I I I

U3WKHW SI SI SI I

U479HU S S I

UHJIRN S S S I I

UNNSU8 S I

USULOL S I

UTTTWF S S I I

V4HVM5 I SI

VBO7OP I I I SI

W7K0RA S S I

WEJJEJ S S S I I I SI Duquenoise

WMUWW C

S S I I S S

WPE9JA SI I

WV88U8 S I

WWWBL X

S I I GC-FTIR

XGLCLJ I S

XLNP6X I SI I

XUE0RE I SI I

Y3XX1B SI I I I I

Y68SYY S S I I HRMS

YMK92M I

YQELRV I I S Raman

YQXDTM I SI

YS66H6 SI

YSSSDR SI



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

YYONQA I SI

Z00LTY SI I

Z7F75I S S S I I

Z7JWAE S I I

ZJZZZ3 SI I



RESPONSE SUMMARY FOR TEST SAMPLE 1

The response summary of all 194 participating laboratories for the identification of SM-1, frequency of use of

screening and identification techniques and false positives and negatives:

Correct identification of Test Sample-1:

Substance Name Number of laboratories

Cocaine 194

Lactose 101

False positives for Test Sample-1:

Round Code Substance Reported Tech Code

PM7GBZ Caffeine 180

WMUWWC Morphine 171, 180

False negatives for Test Sample-1 with respect to Cocaine (techniques(s) used):

There were no false negative results for SM-1

Analysis not performed for Test Sample-1 with respect to Cocaine:

All participating laboratories carried out analysis for Cocaine

Frequency of use of screening, identification and quantification techniques:

Response Summary

Participants 194

Technique 140 141 142 150 160 161 171 180 190 200 210 211 230 231 250

Screening (No.) 66 74 65 20 2 4 8 70 17 1 2 0 1 0 4

(%) 34.0 38.1 33.5 10.3 1.0 2.1 4.1 36.1 8.8 0.5 1.0 0.0 0.5 0.0 2.1

Identification (No.) 21 11 10 39 6 16 27 178 85 3 10 2 3 5 4

(%) 10.8 5.7 5.2 20.1 3.1 8.2 13.9 91.8 43.8 1.5 5.2 1.0 1.5 2.6 2.1

Quantification (No.) 0 0 0 1 12 24 77 21 1 0 2 0 1 1 0

(%) 0.0 0.0 0.0 0.7 8.5 17.0 54.6 14.9 0.7 0.0 1.4 0.0 0.7 0.7 0.0

Participants: 194


Z-Score Report per Sample per Substance: Round: 2018/2 Substance: SM-1; Cocaine

Z-scores can be interpreted by participants in line with ISO 13528:2005, section 7.4.2 and ISO/IEC guide43-1:1997(E) as follows:

IzI < 2 = satisfactory

2 ≤ IzI ≤ 3 = questionable

IzI > 3 = unsatisfactory

According to the recommendations in ISO 13528:2005, an unsatisfactory z-score is considered to give an action signal and a questionable z-score is

considered to give a warning signal. A single action signal or warning signal in two successive rounds shall be taken that an anomaly has occurred

that requires investigation.

Robust average: 22.4%

UNODC value: 22.7%



Z-Score Report per Sample per Substance:



Z-Scores for Test Sample 1

Code

Cocaine

Code

Cocaine

Concentration (mass%)

Deviation from

robust average

z-score Concentration (mass%)

Deviation from

robust average

z-score

7P5A33 7.2 -15.2 -12.8 MR1LVU 22.0 -0.4 -0.4 QMQ1QP 12.6 -9.8 -8.2 3JJ2TA 22.0 -0.4 -0.4 WWWBLX 16.6 -5.8 -4.9 31933H 22.0 -0.4 -0.4 ANAAAW 17.1 -5.3 -4.5 YMK92M 22.1 -0.3 -0.3 MFE65O 17.9 -4.5 -3.8 DPAIVA 22.1 -0.3 -0.3 SHIGZS 18.0 -4.4 -3.7 DIIBXI 22.2 -0.3 -0.3 T0PFVQ 19.3 -3.1 -2.6 SBKWJS 22.2 -0.2 -0.2 07RNYQ 19.4 -3.0 -2.6 DYZ53I 22.3 -0.1 -0.2 V4HVM5 19.6 -2.8 -2.4 HGGHOG 22.3 -0.1 -0.1 XUE0RE 19.6 -2.8 -2.4 AIQBL5 22.3 -0.1 -0.1 A8R888 19.8 -2.6 -2.3 UHJIRN 22.3 -0.1 -0.1 14YQYB 19.9 -2.5 -2.1 3CUTP4 22.3 -0.1 -0.1 LLTO7L 20.0 -2.4 -2.1 BLBOCB 22.3 -0.1 -0.1 IL7F1S 20.2 -2.2 -1.9 IXI4IQ 22.3 -0.1 -0.1 Y3XX1B 20.4 -2.0 -1.8 ZJZZZ3 22.4 0.0 -0.1 222A22 20.4 -2.0 -1.8 4FMLRF 22.4 0.0 -0.1 MJMMJM 20.5 -1.9 -1.6 RRFXUO 22.4 0.0 0.0 9CKOOD 20.6 -1.8 -1.6 7UN77R 22.5 0.1 0.0 GU6GGK 20.8 -1.6 -1.4 9N8FTT 22.5 0.1 0.0 GFFGAC 20.8 -1.6 -1.4 SZVWV9 22.5 0.1 0.0 EDHZTN 20.8 -1.6 -1.4 FPTIMV 22.5 0.1 0.0 CMZFLS 20.9 -1.5 -1.3 AEFKAT 22.5 0.1 0.0 YSSSDR 21.0 -1.4 -1.3 H8G1O8 22.6 0.2 0.1 HATVYH 21.0 -1.4 -1.2 AGJ544 22.6 0.2 0.1 4STTTT 21.0 -1.4 -1.2 OKBALQ 22.6 0.2 0.1 QORSXL 21.1 -1.3 -1.1 QTQQQ1 22.6 0.2 0.1 60XF00 21.1 -1.3 -1.1 QRCK2V 22.6 0.2 0.1 49LF34 21.2 -1.2 -1.0 HUAI9B 22.6 0.2 0.1 9ONAKN 21.3 -1.1 -1.0 HI4WNN 22.6 0.2 0.1 SRCKGX 21.3 -1.1 -0.9 QJOV22 22.6 0.2 0.1 1KOSTW 21.4 -1.0 -0.9 UTTTWF 22.7 0.3 0.2 1PSOP9 21.5 -0.9 -0.8 EQWWGJ 22.7 0.3 0.2 2BSDEQ 21.6 -0.8 -0.7 AOZMSG 22.7 0.3 0.2 F9BYIQ 21.6 -0.8 -0.7 QRDRJ1 22.7 0.3 0.2 SV4SBQ 21.6 -0.8 -0.7 MSFAND 22.7 0.3 0.2 N8BKMB 21.7 -0.7 -0.6 7S7SS2 22.8 0.4 0.3 AAPSTZ 21.8 -0.6 -0.6 8828D8 22.8 0.4 0.3 QJJYGQ 21.8 -0.6 -0.6 ICZF4Z 22.9 0.5 0.3 HHDUPI 21.8 -0.6 -0.6 5W5519 22.9 0.5 0.4 WEJJEJ 21.8 -0.6 -0.6 OLWSRI 22.9 0.5 0.4 TELOLF 21.8 -0.6 -0.5 8XQEGQ 22.9 0.5 0.4

U3WKHW 21.9 -0.5 -0.5 8TKCKC 22.9 0.5 0.4 9QNQPB 21.9 -0.5 -0.5 KHGLHU 22.9 0.5 0.4 C9QQGT 21.9 -0.5 -0.5 QPXWKT 23.0 0.6 0.4 GKMCN5 21.9 -0.5 -0.5 NPEUNW 23.0 0.6 0.4 VBO7OP 22.0 -0.4 -0.4 Y68SYY 23.0 0.6 0.4 YS66H6 22.0 -0.4 -0.4 BAYSRL 23.0 0.6 0.4 AIW1Z2 22.0 -0.4 -0.4 55IZ55 23.0 0.6 0.4 SUSSDP 22.0 -0.4 -0.4 CLRNDG 23.0 0.6 0.4 9WFUHI 22.0 -0.4 -0.4 MSHBVG 23.0 0.6 0.4 HPIHHH 22.0 -0.4 -0.4 QBF6VQ 23.0 0.6 0.4




Code

Cocaine


Deviation from robust

average z-score

RDRW1X 23.0 0.6 0.5 1IIEIC 23.0 0.6 0.5

WV88U8 23.1 0.7 0.5 OB929H 23.1 0.7 0.5 RPI8GV 23.1 0.7 0.5 7Z33IM 23.1 0.7 0.6 8288I1 23.2 0.8 0.6 PCYCJC 23.2 0.8 0.6 555HC5 23.3 0.9 0.7 RCBIBN 23.3 0.9 0.7 SYLJNC 23.4 1.0 0.8 YQXDTM 23.8 1.4 1.1 K9O99N 24.0 1.6 1.3 9DKDUD 24.0 1.6 1.3 ECOCCC 24.1 1.7 1.4 WPE9JA 24.2 1.8 1.5 4EF44P 24.3 1.9 1.5 CTRBHS 24.4 2.0 1.6 YYONQA 24.5 2.1 1.7 SYYY0F 24.8 2.4 2.0 KOQ1NC 24.9 2.5 2.0 9LZ9YA 25.0 2.6 2.1 CELGEE 25.0 2.6 2.1 HDYYZY 25.7 3.3 2.7 2P2PU2 25.8 3.4 2.7 CPBBXT 26.0 3.6 3.0 22YK4V 26.0 3.6 3.0 PM7GBZ 26.2 3.8 3.1 LC7LMZ 26.5 4.1 3.4 R2YIAE 26.6 4.2 3.4 02OWVV 28.7 6.3 5.2 7JGGMW 31.0 8.6 7.1 HRZZZ0 31.3 8.9 7.4 NVWID3 36.8 14.4 12.0 64UHPY 38.2 15.8 13.2 PUTLIT 38.9 16.5 13.8

4QMQQQ 52.0 29.6 24.7 BSWNB0 52.6 30.2 25.2 JDZDJJ 59.0 36.6 30.5



Sample 2 Analysis



006FMT MDPV

02OWVV 3,4-methylendioxypyrovalerona

07RNYQ MDPV

0O73XC MPDV, 3,4 METHYLENEDIOXYPYROVALERONE

14YQYB MDPV

1IIEIC MDPV

1KOSTW 3,4-MDPV

1PSOP9 3,4 - methylenedioxypyrovalerone HCl ( MDPV HCl)

222A22 MDPV

22YK4V 3,4 mdpv

2333DY MDPV

2BSDEQ MDPV

2P2PU2 MDPV (3,4-Methylenedioxypyrovalerone)

31933H MDPV

33Q3N2 Methyledioxypyrovalerone (MDPV)

3CUTP4 MDPV

3EOHEE 3,4 MDPV

44N4AK MDPV

49LF34 MDPV

4EF44P MDPV

4FMLRF 3,4-MDPV

4ITTTE 3,4-MDPV

4QMQQQ MDPV

4STTTT MDPV

555HC5 3,4 -methylenedioxypyrovalerone (MDPV)

55IZ55 MDPV

5BOT5R 3,4 MDPV

5W5519 MDPV (3,4-Methylenedioxypyrovalerone)

60XF00 3,4 Methylenedioxypyrovalerone HCl

64UHPY MDPV

6C7TVN MDPV

7HN7A7 MDPV

7JGGMW MDPV

7S7SS2 3,4-Methylenedioxypyrovalerone

7ULAFF 3,4-Methylenedioxypyrovalerone (MDPV)

7UN77R Methylenedioxypyrovalerone (MDPV)

7Z33IM 3,4-Methylenedioxypyrovalerone

8288I1 3,4-Methylenedioxypyrovalerone - Lactose

8828D8 3,4-Methylenedioxypyrovalerone

8TKCKC 3,4-MPDV chlorhydrate




8XQEGQ Methylendioxypyrovalerone(MDPV)

9CKOOD 3,4-Methylenedioxypyrovalerone

9DKDUD MDPV

9LZ9YA 3,4-MDPV

9N8FTT 3,4-Methylenedioxypyrovalerone

9ONAKN 3-4-Methylenedioxypyrovalerone

9QNQPB 3,4Methylenedioxypyrovalerone

9WFUHI Methylenedioxypyrovalerone (MDPV)

9YN990 3,4-Methylenedioxypyrovalerone

A8R888 MDPV

AAPSTZ MDPV

ADPI7V MDPV

AEFKAT MDPV

AGJ544 MDPV

AIQBL5 MDPV

AIW1Z2 3,4-Methylenedioxypyrovalerone

ANAAAW 3,4-Methylenedioxypyrovalerone (MDPV)

AOZMSG 3,4-METHYLENEDIOXYPYROVALERONE (MDPV)

BEXBRB MDPV

BLBOCB Methyledioxypyrovalerone Hydrochloride

BUHHL2 MDPV

BZZZIR 3,4–Methylenedioxypyrovalerone (MDPV)

C9QQGT Methylenedioxypyrovalerone (MDPV) and Lactose

CELGEE alpha-PVP

CLRNDG 3,4-methylenedioxypyrovalerone

CMZFLS METHYLENEDIOXY-PYROVALERONE (MDPV)

CPBBXT 3,4-Methylenedioxypyrovalerone

CTRBHS Methylenedioxypyrovalerone (MDPV).

D3UIUC 3,4-MDPV

DIIBXI Methylenedioxypyrovalerone

DPAIVA MDPV

DYZ53I MDPV

ECOCCC MDPV

EDHZTN Methylenedioxypyrovalerone

EQWWGJ 3,4-MDPV

ESWD79 MDPV

F0000S Methylendioxypyrovalerone (MDPV)

F9BYIQ 3,4-Methylenedioxypyrovalerone

FD4JOW 3,4-Methylenedioxypyrovalerone

FPTIMV Test sample 2018/2/SM-2 contains Methylendioxypyrovalerone (MDPV)

GCFWS5 MDPV

GF7VNQ 3,4-Methylenedioxypyrovalerone (MDPV)

GFFGAC 3,4 MDPV

GKMCN5 3,4-Methylenedioxypyrovalerone




GU6GGK MDPV

H6MPDC 3,4 - MDPV + LACTOSE

H8G1O8 3,4 MDPV

HATVYH Clorhidrato de 3,4-Metilendioxipirovalerona

HDYYZY MDPV

HEVEPB MDPV and Lactose

HGGHOG 3,4 Methylenedioxypyrovalerone

HHDUPI MDPV

HI4WNN 3,4-MDPV

HPIHHH MDPV

HRFHJD Methylenedixypyrovalerone

HRZZZ0 3,4-Methylenedioxypyrovalerone

ICZF4Z 3,4-Methylenedioxypyrovalerone

IL7F1S 3,4-MDPV

IODUOV MDPV

IXI4IQ MDPV

JDZDJJ MDPV

JXQBZB 3,4 Methylenedioxypyrovalerone

K59V35 MDPV (methylenedioxypyrovalerone)

K9O99N MDPV HCl

KHGLHU 3,4-Methylenedioxypyrovalerone

KILSPH MDPV

KOQ1NC MDPV

KSIKUP pyrovalerone

KUVU4U 3,4-methylenedixypyrovalerone (MDPV)

L9LV6L 3,4 Methylenedioxypyrovalerone

LC7LMZ 3,4-MDPV

LLTO7L MDPV, lactose

LTTTTQ 3,4-methylenedioxypyrovalerone (MDPV)

MFE65O 3,4-Methylenedioxypyrovalerone + lactose

MJMMJM 3,4-MDPV

MR1LVU Methylenedioxypyrovalerone (MDPV)

MSFAND MDPV

MSHBVG 3-4 3,4-Methylenedioxypyrovalerone

N8BKMB methylenedioxypyrovalerone

NAK5A7 3,4-METHYLENEDIOXYPYROVALERONE

NCCCCR 3,4-Methylenedioxypyrovalerone

NPEUNW 3,4-Methylenedioxypyrovalerone

NSALLN MDPV

OB929H MDPV

OKBALQ 3,4-Methylenedioxypyrovalerone

OLWSRI 3,4-Methylen edioxypyrovalerone

ORPCAT MDPV

PCYCJC MDPV




PM7GBZ 3,4-Methylenedioxypyrovalerone (MDPV)

PMDM1U MDPV

PMR0Q7 methyledioxypyrovalerona (MDPV)

PQIKKZ MDPV

PUTLIT 3,4-Methylenedioxypyrovalerone

QBF6VQ MDPV

QJJYGQ MDPV

QJOV22 3,4-Methylenedioxypyrovalerone

QMQ1QP 3,4-MDPV

QORSXL 3,4-MDPV

QPXWKT 3,4-methylenedioxypyrovalerone (MDPV)

QRCK2V 3,4-Methylenedioxypyrovalerone

QRDRJ1 Methylenedioxypyrovalerone (MDPV) + Lactose

QTQQQ1 MDPV

R2YIAE Methyledioxypyrovalerone and lactose

R7GREQ 3,4-Methylenedioxypyrovalerone

RCBIBN MDPV

RDRW1X 3,4-Methylenedioxypyrovalerone

RPI8GV Methylenedixypyrovalerone (MDPV)

RRFXUO MDPV

S919AS 3,4 Methylenedioxy pyrovalerone

SBKWJS MDPV

SHIGZS 3,4-Methylenedioxypyrovalerone, lactose

SRCKGX MDPV

SUSSDP MDPV

SV4SBQ 3,4-Methylenedioxypyrovalerone (MDPV)

SYLJNC 3,4-Methylenedioxypyrovalerone

SYYY0F MDPV

SZVWV9 mdpv

T0PFVQ MDPV

TELOLF MDPV

U3WKHW 3,4-methylenedioxypyrovalerone

U479HU 3,4-Methylenedioxypyrovalerone

UHJIRN 3,4-methylenedioxypyrovalerone

UNNSU8 Methyelenedioxypyrovalerone (MDPV)

USULOL 3,4-Methylenedioxypyrovalerone

UTTTWF 3,4-methylenedioxypirovalerone

V4HVM5 3,4-Methylenedioxypyrovalerone

VBO7OP Pyrovalerone

W7K0RA it was not detected

WEJJEJ MDPV HCl

WMUWWC 3,4-methyl metilene dioxy pirovalerone

WPE9JA DMPV

WV88U8 3,4 MDPV




WWWBLX Methylenedioxypyrovalerone (MDPV)

XGLCLJ MDPV

XLNP6X Pyrovalerone

XUE0RE MDPV

Y3XX1B MDPV

Y68SYY METHYLEDIOXYPYROVALERONE (MDPV)

YMK92M 3,4-methylendioxypyrovalerone

YQELRV MDPV

YQXDTM MDPV

YS66H6 MDPV

YSSSDR Pyrovalerone

YYONQA MDPV

Z00LTY MDPV

Z7F75I NO DRUGS FOUND

Z7JWAE Methlenedioxypyrovalerone

ZJZZZ3 MDPV




Code 3,4- Methylenedioxypyr ovalerone

Lactose

006FMT + + MARQUISE REAGENT: negative reaction, COBALT THIOCYANATE: negative reaction, GC-MS: MDPV (compared with library MS spectrum of MDPV), FTIR: MDPV (compared with IR spectrum of MDPV), FTIR: lactose (spectrum of ethanol ectract residue compared with IR spectrum of lactose)

02OWVV + - 3,4-methylendioxypyrovalerona identificado por GC/MS

07RNYQ + ANP Powder contains MDPV

0O73XC + + PRUEBA DE SCREENING: ZIMERMAN POSITIVO (AMARILLO), CRISTALES CARACTERISTICOS CON CLORURO DE MERCURIO, CROMATOGRAFIA EN CAPA FINA REVELADOR NINHIDRINA Rf CORRESPONDE (AZUL), FTIR ESPECTRO CORRESPONDE A MPDV BIBLIOTECA EQUIPO

14YQYB + ANP SM2 contains 16.96% MDPV.

1IIEIC + + This sample is MDPV.

1KOSTW + -

1PSOP9 + + 9,61 % MDPV base, laktose

222A22 + ANP

22YK4V + ANP comfirmed by gc msd

2333DY + + laktóz

2BSDEQ + + White powder containing 11.1%w/w MDPV and lactose

2P2PU2 + + Percentage of MDPV was 8.84 %. Additionally Lactose was identified.

31933H + +

33Q3N2 + ANP Item 2018/2/SM-2 found to contain Methyledioxypyrovalerone (MDPV).

3CUTP4 + + Lactose

3EOHEE + ANP 3,4 MDPV

3JJ2TA ANP ANP

44N4AK + +

49LF34 + + The test sample 2018/2/SM-2 contains 9.47 % m/m methylenedioxypyrovalerone (MDPV).

4EF44P + + LACTOSE




Lactose

4FMLRF + + 3,4-MDPV in mixture with lactose


4QMQQQ + + MDPV was found in the sample

4STTTT + ANP METHYLENEDIOXYPYROVALERONE is controlled under the Misuse of Drugs Act 1971 (as amended) as a Class B drug, by virtue of the fact that it is a compound structurally derived from 2- amino-1-phenyl-1-propanone by substitution in the phenyl ring with an alkylenedioxy substituent; substitution at the 3-position with an alkyl substituent; and by inclusion of the nitrogen atom in a cyclic structure.

555HC5 + + 3,4 -methylenedioxypyrovalerone (MDPV) was identified by TLC and GC/MS ,quantified by GC.

55IZ55 + + MDPV was detected

5BOT5R + ANP

5W5519 + + LACTOSE

60XF00 + + Contain 3,4 Methylenedioxypyrovalerone 7.28% as base and Lactose (not Quantitated)

64UHPY + + Metildioxipirovalerona y lactosa

6C7TVN + + The test sample 2018/2/SM-2 was found to contain methylenedixypyrovalerone (MDPV) and lactose.

7HN7A7 + ANP In GCMS,we found MDPV peak.

7JGGMW + + MDPV + lactose

7P5A33 ANP ANP

7S7SS2 + + The sample contains 3,4-Methylenedioxypyrovalerone

7ULAFF + ANP Test sample 2018/2/SM-2 was confirmed to contain 3,4-Methylenedioxypyrovalerone (MDPV), a DEA schedule I substance.

7UN77R + + The sample 2018/2/SM-2 was found to contain 229 milligrams of a white powder. This powder was found to contain a mixture of methylenedioxypyrovalerone (MDPV) and lactose.

7Z33IM + ANP It include only 3,4-Methylenedioxypyrovalerone, We are not detected amount. Because There is not standart reference materials our laboratory now.

8288I1 + +

8828D8 + + The sample contains 3,4-methylenedioxypyrovalerone which is listed as a controlled drug according to french order, appendix IV of February 22nd 1990.




Lactose

8TKCKC + + 3,4-MPDV chlorhydrate (9% as base) + lactose

8XQEGQ + + Lactose

9CKOOD + ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 17.1.. Methylenedioxypyrovalerone (MDPV)

9DKDUD + + Mdpv - Lactose

9LZ9YA + -


9ONAKN + ANP SM-2 was found to contain 3,4-Methylenedioxypyrovalerone

9QNQPB + + lactose

9WFUHI + - The powder was analysed and found to contain Methylenedioxypyrovalerone (MDPV). Methylenedioxypyrovalerone (MDPV) is a compound structurally derived from 2-amino-1-phenyl-1- propanone by substitution in the phenyl ring with an alkylenedioxy substituent; substitution at the 3- position with an alkyl substituent; and by inclusion of the nitrogen atom in a cyclic structure, and as such is a class B controlled drug within the provisions of the Misuse of Drugs Act 1971.

9YN990 + ANP Sample SM-2 found to contain 3,4-Methylenedioxypyrovalerone.

A8R888 + + SM 02 was found to contain Methylenedixypyrovalerone (MDPV) and lactose

AAPSTZ + ANP

ADPI7V + + lactose

AEFKAT + + The sample contains MDPV*HCl and Lactose, with 10.45% MDPV base

AGJ544 + ANP

AIQBL5 + ANP

AIW1Z2 + ANP Controlled drug, MDPV, present in sample. Concentration approx 9%

ANAAAW + + Sample 2018/2/SM-2 contains MDPV and lactose. MDPV was not quantified because our laboratory does not have reference standard. Tiocianate reaction was negative with this samples but Scott modificated reagent gives positive reaction.

AOZMSG + -

BAYSRL + +




Lactose

BEXBRB + ANP Examination of sample SM-2 revealed the presence of 3,4-methylenedioxypyrovalerone

BLBOCB + + the sample contains methyledioxypyrovalerone hydrochloride (10.3 +/- 0.1% as MDPV free base) and lactose

BSWNB0 ANP ANP

BUHHL2 + ANP From confirmation test using (GC-MS), the sample was found to contain the controlled drug (MDPV).

BZZZIR + ANP SM-2 contain 3,4–Methylenedioxypyrovalerone (MDPV) which is controlled under Malaysian Poisons Act 1952

C9QQGT + + Using the techniques CR, TLC, GC-MS and FT-IR sample was found to contain Methylenedioxypyrovalerone (MDPV) and Lactose

CELGEE + ANP Sample tested positive for alpha-PVP. The substance was confirmed using GC-MS. No quantification was done as the substance is not included in the list of validated quantifiable substances in our laboratory.

CLRNDG + +

CMZFLS + + B) One brown tinted glass container, labelled "2018/2/SM-2" "2, with attached black plastic lid that contained 216 milligrams of a white powder. This white powder was found to contain Methylenedioxypyrovalerone (MDPV). MDPV is a Class B drug under the provisions of the Misuse of Drugs Act 1971 (as amended). Lactose is not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

CPBBXT + + We found a mixture of 3,4-Methylenedioxypyrovalerone and lactose.

CTRBHS + ANP This sample was found to contain Methylenedioxypyrovalerone (MDPV), which is a Class B controlled substance under the Misuse of Drugs Act 1971.

D3UIUC + ANP The sample contain 3,4-MDPV

DIIBXI + + Item 2018/2/SM-2 was found to contain one glass vial which held 223 milligrams of white powder. This powder contained METHYLENEDIOXYPYROVALERONE (MDPV).

DPAIVA + + Lactose

DYZ53I + +

ECOCCC + + SM2 contient de la MDPV avec du lactose

EDHZTN + ANP One glass bottle containing 0.22 grammes of a powder containing 0.02 grammes of methylenedioxypyrovalerone, being a compound structurally derived from 2-amino-1-phenyl-1- propanone by substitution in the phenyl ring with an alkyenedioxy substituent and by substitution at the 3-position with an alkyl substituent and by inclusion of the nitrogen atom in a cyclic structure.

EQWWGJ + ANP 3,4-MDPV was identified in the sample 2018/2/SM2




Lactose


F0000S + ANP Methylendioxypyrovalerone (MDPV) is not controlled (scheduled) drug based on local (national) Law No.02/L-128

F9BYIQ + -

FD4JOW + + the sample contains 3,4-Methylenedioxypyrovalerone and Lactose

FPTIMV + +

GCFWS5 + ANP NPS


GFFGAC + + WAS FOUND 3,4 MDPV AND LACTOSE

GKMCN5 + ANP The sample was found to contain 3,4-methylenedioxypyrovalerone.

GU6GGK + ANP

H6MPDC + + In relation to the 2018/2/SM-2 sample, a blue staining was observed when the SCOTT test was applied. A yellow color was observed when the MARQUIS test was applied, which presupposes the presence of 3.4-MDPV. He came to confirm that it was after the 3.4-DMPV after the application of TLc and Ftir. With FTIR, it was also possible to observe the presence of LACTOSE.

H8G1O8 + + 3,4 MDPV is sheduled as illicit drug in France.

HATVYH + + Lactosa

HDYYZY + ANP

HEVEPB + + The Test sample 2018/2/SM-2 was analyzed by Thin Layer Chromatography technique and was found to contain MDPV and Lactose.

HGGHOG + ANP

HHDUPI + ANP MDPV is the common name for methylenedioxyprovalerone, a Class B drug subject to the provisions of the Misuse of Drugs Act 1971 (amendment) order 2010.

HI4WNN + ANP NPS

HPIHHH + + lactose

HRFHJD + + On analysis, I found the sample "SM-2" containing Methylenedixypyrovalerone and Lactose




Lactose

HRZZZ0 + ANP -

HUAI9B + + The sample contained 3-4-Methylenedioxypyrovalerone (MDPV) and Lactose.

ICZF4Z + + Also contain lactose.

IL7F1S + + The sample contains 9,61±0,54 weight% 3,4-MDPV-base (3,4-methylenedioxypyrovalerone-base). The sample also contains lactose.

IODUOV + ANP Powder containing MDPV

IXI4IQ + ANP

JDZDJJ + +

JXQBZB + + 3,4 MDPV+ LACTOSE

K59V35 + + 2018/2/SM-2 contains MDPV(methylenedioxypyrovalerone). It also contains lactose.

K9O99N + + lactose

KHGLHU + + 3,4-Methylenedioxypyrovalerone in lactose powder

KILSPH + ANP White powder and odorless

KOQ1NC + + new psychoactive substance

KSIKUP + + pyrovalerone and lactose

KUVU4U + + In the analisys was obteined (3,4-methylenedixypyrovalerone (MDPV)), which controled substance and lactose which is uncontroled substance for Colombia

L9LV6L + ANP

LC7LMZ + + It has been detected the presence of 3,4-Methylenedioxypyrovalerone in the sample.

LLTO7L + + This powder was found to contain MDPV together with the adulterant lactose

LTTTTQ + ANP Sample 2018/2/SM-2 was found to contain 3,4-methylenedioxypyrovalerone (MDPV).

MFE65O + + We analized the sample by FTIR and GC-MS. We could identify lactose by colourimetric test. The sample was analyze by GC-MS with differents solvents: Methanol, chloroform, ethanol and ethanol with internal standard.

MJMMJM + - The sample contains 10,8% 3,4-MDPV




Lactose

MR1LVU + + Sample 2018/2/SM-2 contained Methylenedioxypyrovalerone (MDPV) together with the adulterant Lactose. Methylenedioxypyrovalerone (MDPV) is a Class B controlled drug under the provision of the Misuse of Drugs Act 1971 (as amended). Lactose is not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

MSFAND - - LACTOSE

MSHBVG + + found sintetic cathynone 3,4-Methylenedioxypyrovalerone buth for lack of standard we cannot specify the purity %

N8BKMB + ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule 1 17.1. Methylenedioxypyrovalerone (MDPV)

NAK5A7 + ANP Sample 2018/2/SM-2 was found to contain 3,4-Methylenedioxypyrovalerone.

NCCCCR + + SM-2 was contained 3,4-Methylenedioxypyrovalerone base.The test sample also contained lactose

NPEUNW + + A composite was formed from 1 unit for testing of 1 unit received. 3,4-Methylenedioxypyrovalerone (salt form not determined) and lactose confirmed in the composite.

NSALLN + ANP TEST SAMPLE 2018/2/SM -2 CONTAIN MDVP

NVWID3 + + After chemical analysis was performed the sample was contained MDPV and Lactose.

OB929H + ANP

OKBALQ + ANP

OLWSRI + ANP It include only 3,4-Methylenedioxypyrovalerone

ORPCAT + + Table 1 Schedule 1, Narcotic substances (not used by medicine)

PCYCJC + ANP MDPV is controlled by the Royal Decree of the 6th of september 2017

PM7GBZ + ANP The sample contains 3,4-Methylenedioxypyrovalerone (MDPV). Quantitation was not performed because of the luck of standard.

PMDM1U + ANP White powder material that contains drug under international controle - MDPV.


PQIKKZ + ANP

PUTLIT + ANP The sample contains 3,4-Methylenedioxypyrovalerone.

QBF6VQ + ANP Lactose was found but the Communiqué 2018-086-CAL-QUI Report of uncontrolled substances and traces in Competency Tests indicate that sharp suttances are not reported or outside the scope of the procedures.




Lactose

QJJYGQ + + MDPV y Lactosa

QJOV22 + ANP It include only 3,4-Methylenedioxypyrovalerone

QMQ1QP + + The sample contains 3,4-MDPV and lactose as an adulterant. 3,4-MDPV is a cathinone derivative stimulant drug, one of the first designer drug emerged the NPS market. The substance is controlled in Poland.

QORSXL + + 3,4-MDPV (8.5% ) and lactose

QPXWKT + + Presence of 3,4-methylenedioxypyrovalerone hydrochloride and lactose was detected in the sample. The sample also contained multitude of trace level impurities.

QRCK2V + + lactose

QRDRJ1 + + In the 2018/2/SM-2 was proved the presence of Methylenedioxypyrovalerone (MDPV) and Lactose, with a quantification as base of 16.1%

QTQQQ1 + ANP MDPV was detected by GC/MS and quantified by GC/FID

R2YIAE + + Examination and analyses performed on the solid in SM-2 showed it to contain methyledioxypyrovalerone (a synthetic cathinone) and lactose

R7GREQ + ANP 3,4-Methylenedioxypyrovalerone confirmed in SM-2.

RCBIBN + + MDPV

RDRW1X + ANP It include only 3,4-Methylenedioxypyrovalerone


RRFXUO + + Sample contained MDPV as hydrochloride and LACTOSE. Identification of MDPV by FTIR and GC/MS, quantification by GC/FID. Identification of LACTOSE by FTIR and Colorimetric Reactions (Molish Test).

S919AS + - 3,4 MDPV was found in GCMS analysis

SBKWJS + + ./.

SHIGZS + + The sample contains 3,4-Methylenedioxypyrovalerone which is scheduled as illicit drug in France. The lactose is not scheduled as illicit drug in France. It's a cutting agent.

SRCKGX + + The sample contains MDPV (3,4-methylenedioxypyrovalerone). MDPV is a controlled substance in X.

SUSSDP + -




Lactose

SV4SBQ + ANP Powder contains 3,4-Methylenedioxypyrovalerone (MDPV). Methylenedioxypyrovalerone (MDPV) is a controlled drug under the Misuse of Drugs Act 1977 to 2016. This is because MDPV is structurally derived from 2-amino-1-phenyl-1-propanone by substitution in the phenyl ring with an alkylenedioxy group and by substitution at the 3-position of the propanone side-chain with an alkyl substituent and by inclusion of the nitrogen atom in a cyclic structure. (See paragraph 1A(b) of Schedule 1 to the Misuse of Drugs (Amendment) Act, 2015).

SYLJNC + ANP The sample contains 3,4-Methylenedioxypyrovalerone (not quantified)

SYYY0F + + White powder containing MDPV

SZVWV9 + +

T0PFVQ + - We detected MDPV in SM-2, but we are not able to give a quantitative result.

TELOLF + + In the sample SM-2 there is a MDPV. MDPV is on the list of drugs.

U3WKHW + - we can not quantify MDPV because we haven't got seized samples.

U479HU + - 3,4-Methylenedioxypyrovalerone

UHJIRN + - Not quantificated due to a lack of standard

UNNSU8 + ANP Based on the above analysis, the sample was found to contain Methyelenedioxypyrovalerone (MDPV)

USULOL + ANP Satisfied with result obtained

UTTTWF + + 3,4-methylenedioxypirovalerone cut with lactose was identified

V4HVM5 + + The sample contained 8.3% 3,4-MDPV and also lactose.

VBO7OP + - Non addullterants. Only qualitative results

W7K0RA ANP ANP in thin layer chromatography we could see the spot in SM-2 but because of we do not have all the drug standards we could not detect what was that?

WEJJEJ + + Base MDPV 9.65% and lactose

WMUWWC + - 3,4-methyl metilene dioxi pirovalerona

WPE9JA + + DMPV was detected by GC/MS and quantified by GC/FID

WV88U8 + + LACTOSE

WWWBLX + ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 17.1. Methylenedioxypyrovalerone (MDPV)




Lactose

XGLCLJ + + The major compound we founded in sm-2 after GC/MS injection is MDPV

XLNP6X - + Pyrovalerone and Lactose

XUE0RE + + The sample contains 9.68 % of MDPV and also contains MDPPP

Y3XX1B + + sample contains MDPV and lactose

Y68SYY + ANP On analysis of a representative sample of the powder Methyledioxypyrovalerone was detected.

YMK92M + ANP In the test simple 2018/2/SM-2 was detected 3,4 methylendioxypyrovalerone

YQELRV + + The sample contains MDPV. The concentration has not been determined.

YQXDTM + ANP White powder containing MDPV (not quantified)

YS66H6 + ANP

YSSSDR + +

YYONQA + ANP White powder containing MDPV (8.8%w/w) wich is controlled by national law

Z00LTY + ANP 2018/2/SM-2 has been detected containing 3,4-Methylenedioxypyrovalerone.

Z7F75I - ANP

Z7JWAE + + The white powder was analysed and found to contain Methylenedioxypyrovalerone (MDPV).

ZJZZZ3 + - MDPV and sugar are found due to our analysis during identification. But we hadn't got the reference material of MDPV and that's why we couldn't complete the quantification part.





Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

006FMT S S S SI I

02OWVV SI SI I SI

07RNYQ SI I I

0O73XC S S I I


1IIEIC S I I

1KOSTW I I

1PSOP9 SI I I

222A22 S I I

22YK4V SI I

2333DY I SI SI

2BSDEQ I SI I


31933H S S S SI I

33Q3N2 S I

3CUTP4 I SI I

3EOHEE SI

3JJ2TA S S S I

44N4AK S I I

49LF34 I SI

4EF44P SI I

4FMLRF I S I I S

4ITTTE I SI I

4QMQQQ S S SI

4STTTT S S I

555HC5 S I I

55IZ55 SI I

5BOT5R SI

5W5519 SI I

60XF00 S S I I I

64UHPY SI S S I I I

6C7TVN S S S SI I

7HN7A7 S S I I

7JGGMW SI SI




Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210


7S7SS2 S I I

7ULAFF S S S I


7Z33IM SI SI I SI

8288I1 S S I I

8828D8 I I

8TKCKC I I

8XQEGQ S I I I


9DKDUD SI

9LZ9YA S I

9N8FTT I I

9ONAKN S S I

9QNQPB I I SI I

9WFUHI S I

9YN990 S I

A8R888 S I SI S

AAPSTZ S S S I S

ADPI7V S I SI SI

AEFKAT S I

AGJ544 SI

AIQBL5 SI SI I

AIW1Z2 SI I GC-IRD

ANAAAW S S S I I

AOZMSG S SI SI

BAYSRL SI I

BEXBRB S I


BSWNB0 SI


BZZZIR S S S I

C9QQGT S S S I I

CELGEE SI

CLRNDG S I I


CPBBXT SI SI SI I I

CTRBHS S S I

D3UIUC SI ASAP-QTOF



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

DIIBXI S S S I I

DPAIVA I SI I

DYZ53I S I I I I


EDHZTN S S I SI I


ESWD79 I SI

F0000S S S I I

F9BYIQ S I SI

FD4JOW S I I

FPTIMV SI I I

GCFWS5 S S I I

GF7VNQ I I S

GFFGAC S S I I

GKMCN5 I SI

GU6GGK SI

H6MPDC S S S I I

H8G1O8 I SI I

HATVYH S I I

HDYYZY I SI


HGGHOG S S I

HHDUPI S S I

HI4WNN S S I

HPIHHH SI I

HRFHJD S I I

HRZZZ0 SI

HUAI9B S S S I I I

ICZF4Z S I I

IL7F1S S I SI I

IODUOV S I I SI

IXI4IQ I

JDZDJJ I S

JXQBZB S I I


K9O99N I SI

KHGLHU I SI I

KILSPH S S SI I

KOQ1NC S I I SI



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

KSIKUP I SI I

KUVU4U S S I I

L9LV6L S I

LC7LMZ SI S I

LLTO7L S S I I

LTTTTQ S S SI

MFE65O SI I

MJMMJM SI

MR1LVU S S I I

MSFAND SI

MSHBVG SI I


NAK5A7 I SI

NCCCCR I SI I

NPEUNW SI I

NSALLN S I

NVWID3 SI S I

OB929H SI SI SI I

OKBALQ SI I

OLWSRI S I SI SI

ORPCAT S S S I I I

PCYCJC I S

PM7GBZ S S S I

PMDM1U S S I

PMR0Q7 S S S I I

PQIKKZ SI

PUTLIT SI

QBF6VQ S S S I


QJOV22 SI SI SI


QORSXL S I

QPXWKT S I I I S

QRCK2V I I SI I

QRDRJ1 I SI I I I

QTQQQ1 SI

R2YIAE S S S I I I

R7GREQ S S S I I




Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

RDRW1X S I S I I

RPI8GV I S S SI I I

RRFXUO I SI I

S919AS S S S I I

SBKWJS SI SI

SHIGZS S SI I I

SRCKGX I I

SUSSDP I S

SV4SBQ I I

SYLJNC S S S I I

SYYY0F I SI

SZVWV9 SI I

T0PFVQ S S S I I


U3WKHW SI SI SI I

U479HU S S I

UHJIRN S S S I I

UNNSU8 S I

USULOL S I

UTTTWF S S I I

V4HVM5 I SI

VBO7OP I I I SI

W7K0RA S S I


WMUWW C

S S I I S S

WPE9JA SI I

WV88U8 S I

WWWBL X

S I I GC-FTIR

XGLCLJ I S

XLNP6X I SI I

XUE0RE I SI I

Y3XX1B SI I I I I

Y68SYY S S I I HRMS

YMK92M I

YQELRV I I S Raman

YQXDTM I SI

YS66H6 SI

YSSSDR SI



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

YYONQA I SI

Z00LTY SI I

Z7F75I S S S I I

Z7JWAE S I I

ZJZZZ3 SI I








MDPV 184

Lactose 105



CELGEE alpha-PVP 180

KSIKUP Caffeine, Pyrovalerone 180, 190

0O73XC Ketamine 150, 190

VBO7OP Pyrovalerone 141, 171

WMUWWC Paracetamol 171, 180

XLNP6X Pyrovalerone 180, 190

YSSSDR Pyrovalerone 180

False negatives for Test Sample-2 with respect to MDPV (techniques(s) used):

Round Code Tech Code

CELGEE 180

KSIKUP 180, 190

VBO7OP 141, 171

XLNP6X 180, 190

YSSSDR 180

Z7F75I 180

Analysis not performed for Test Sample-2 with respect to MDPV:

Round Code

3JJ2TA ANP

7P5A33 ANP

BSWNB0 ANP

W7K0RA ANP


Response Summary

Participants 194

Technique 140 141 142 150 160 161 171 180 190 200 210 211 230 231 250

Screening (No.) 66 74 65 20 2 4 8 70 17 1 2 0 1 0 4

(%) 34.0 38.1 33.5 10.3 1.0 2.1 4.1 36.1 8.8 0.5 1.0 0.0 0.5 0.0 2.1


(%) 10.8 5.7 5.2 20.1 3.1 8.2 13.9 91.8 43.8 1.5 5.2 1.0 1.5 2.6 2.1


(%) 0.0 0.0 0.0 0.0 3.6 23.6 49.1 12.7 1.8 0.0 1.8 5.5 0.0 1.8 0.0

Participants: 194


Z-Score Report per Sample per Substance: Round: 2018/2 Substance: SM-2; MDPV


UNODC value: 9.8%














Code

MDPV

Code

MDPV


Deviation from

robust average


Deviation from

robust average

z-score

60XF00 7.3 -2.5 -2.6 UTTTWF 9.9 0.1 0.0 NPEUNW 8.0 -1.8 -1.9 RRFXUO 10.0 0.1 0.1 RPI8GV 8.0 -1.8 -1.9 HRZZZ0 10.0 0.2 0.1 V4HVM5 8.3 -1.5 -1.6 1IIEIC 10.0 0.2 0.1 07RNYQ 8.4 -1.4 -1.5 5W5519 10.0 0.2 0.1 QORSXL 8.5 -1.3 -1.4 PUTLIT 10.0 0.2 0.2 QMQ1QP 8.6 -1.2 -1.3 WV88U8 10.1 0.3 0.2 YYONQA 8.8 -1.0 -1.1 YSSSDR 10.1 0.3 0.2 A8R888 8.8 -1.0 -1.1 222A22 10.1 0.3 0.2 2P2PU2 8.8 -1.0 -1.0 31933H 10.2 0.4 0.4 8TKCKC 9.0 -0.8 -0.9 BLBOCB 10.3 0.5 0.4 QPXWKT 9.2 -0.7 -0.7 AIQBL5 10.4 0.6 0.5 NVWID3 9.3 -0.5 -0.6 ECOCCC 10.4 0.6 0.5 AIW1Z2 9.3 -0.5 -0.6 AEFKAT 10.5 0.6 0.6 555HC5 9.4 -0.4 -0.5 MJMMJM 10.8 1.0 0.9 HI4WNN 9.4 -0.4 -0.4 DPAIVA 11.0 1.2 1.1 49LF34 9.5 -0.3 -0.4 2BSDEQ 11.1 1.3 1.2 RCBIBN 9.5 -0.3 -0.4 LC7LMZ 11.1 1.3 1.2 EDHZTN 9.5 -0.3 -0.4 8XQEGQ 12.0 2.2 2.2 OB929H 9.6 -0.2 -0.3 HDYYZY 12.1 2.3 2.3 IL7F1S 9.6 -0.2 -0.3 HATVYH 12.3 2.5 2.5 1PSOP9 9.6 -0.2 -0.3 QRDRJ1 16.1 6.3 6.3 WEJJEJ 9.7 -0.2 -0.2 14YQYB 17.0 7.2 7.2 XUE0RE 9.7 -0.1 -0.2 JDZDJJ 24.0 14.2 14.3 WPE9JA 9.7 -0.1 -0.2 QTQQQ1 29.6 19.8 20.0 BAYSRL 9.7 -0.1 -0.2 4QMQQQ 38.0 28.2 28.5 SZVWV9 9.7 -0.1 -0.2 Y3XX1B 49.0 39.2 39.6 4FMLRF 9.8 0.0 -0.1



Sample 3 Analysis



006FMT Metamfetamine

07RNYQ Methamphetamine

0O73XC METAMFETAMINA

14YQYB Methaphetamine

1IIEIC Methamphetamine.

1KOSTW Methamphetamine

1PSOP9 Metamfetamine HCl

222A22 metamphetamine

22YK4V methampetamine

2333DY methamphetamine

2BSDEQ metamphetamine

2P2PU2 Methamphetamine

31933H metamphetamine

33Q3N2 Metamfetamine

3CUTP4 Metamphetamine

3EOHEE METAMPHETAMINE

3JJ2TA METAMFETAMINE

44N4AK metamfetamine

49LF34 Metamfetamine

4EF44P Metamfetamine

4FMLRF Metamfetamine

4ITTTE Metamphetamine

4QMQQQ Methamphetamine

4STTTT Methylamphetamine

555HC5 Methamfetamine

55IZ55 Metamphetamine

5BOT5R Metamfetamine

5W5519 METAMPHETAMINE

60XF00 Methamphetamine HCl

64UHPY Metanfetamina

6C7TVN Methamfetamine

7HN7A7 Methamphetamine

7JGGMW methamphetamine

7P5A33 MDEA

7S7SS2 Metamfetamine

7ULAFF Methamphetamine

7UN77R Methylamphetamine Hydrochloride

7Z33IM Metamfetamine

8288I1 Metamfetamine, Lactose

8828D8 Metamfetamine




8TKCKC metamfetamine chlorhydrate

8XQEGQ Methamphetamine

9CKOOD Methamphetamine

9DKDUD Metamfetamine

9LZ9YA metamphetamine

9N8FTT Metamfetamine

9ONAKN Methamphetamine

9QNQPB Methamphetamine

9WFUHI Methylamphetamine

9YN990 Methamphetamine

A8R888 Metamfetamine

AAPSTZ methamphetamine

ADPI7V metamfetamine

AEFKAT Methamphetamine

AGJ544 Metanfetamine

AIQBL5 Metanfetamine

AIW1Z2 Metamfetamine

ANAAAW Methamphetamine

AOZMSG METAMFETAMINE 20.2 %

BEXBRB Methamphetamine

BLBOCB Methamphetamine Hydrochloride

BUHHL2 Methamphetamine

BZZZIR Methamphetamine

C9QQGT Methamphetamine

CELGEE Methamphetamine

CLRNDG methamphetamine

CMZFLS METHYLAMPHETAMINE HYDROCHLORIDE

CPBBXT Metamfetamine

CTRBHS Methamphetamine.

D3UIUC Metamphetamine

DIIBXI Methylamphetamine hydrochloride

DPAIVA METAMPHETAMINE

DYZ53I Methaphetamine hydrochloride

ECOCCC METHAMPHETAMINE

EDHZTN Methamphetamine

EQWWGJ Methamphetamine

ESWD79 Metamfetamine

F0000S Methamphetamine

F9BYIQ Metamfetamine

FD4JOW Metamfetamine

FPTIMV Test sample 2018/2/SM-3 contains Metamfetamine

GCFWS5 metamfetamine

GF7VNQ Metamfetamine

GFFGAC METHANPHETAMINE




GKMCN5 Methamphetamine

GU6GGK Metanphetamine

H6MPDC D- Methanphetamine +LACTOSE

H8G1O8 Methamphetamine

HATVYH Clorhidrato de Levo-Metanfetamina

HDYYZY MA

HEVEPB Metamfetamine and Lactose

HGGHOG Metamfetamine

HHDUPI Methylamphetamine

HI4WNN Metamphetamine

HPIHHH Metamfetamine hcl

HRFHJD Metamfetamine

HRZZZ0 Metamfetamine

HUAI9B Methamphetamine

ICZF4Z Metamfetamine

IL7F1S metamfetamine

IODUOV Methamphetamine

IXI4IQ Methanfetamine

JDZDJJ Méthamphétamine

JXQBZB METAMFETAMINE

K59V35 Methamphetamine

K9O99N metamphetamine HCl

KHGLHU Metamfetamine

KILSPH Methamphetamine

KOQ1NC Methamphetamine

KSIKUP Metamphetamine

KUVU4U Metamfetamine

L9LV6L Methamphetamine

LC7LMZ Metamfetamine

LLTO7L Methylamphetamine, lactose

LTTTTQ Metamfetamine

MFE65O Metamfetamine + lactose

MJMMJM methamphetamine

MR1LVU Methylamphetamine Hydrochloride

MSFAND METAMFETAMINE

MSHBVG Metamfetamine

N8BKMB methamphetamine

NAK5A7 METHAMPHETAMINE

NCCCCR Metamfetamine

NPEUNW Methamphetamine

NSALLN METANFETAMINE

NVWID3 Amfetamine

OB929H metanfetamina

OKBALQ Metamfetamine




OLWSRI Metamfetamine

ORPCAT Methamphetamine

PCYCJC metamphetamine

PM7GBZ Methamphetamine

PMDM1U METHAMPHETAMINE

PMR0Q7 metaphetamine

PQIKKZ metamfetamine

PUTLIT Metamfetamine

QBF6VQ Metamphetamine

QJJYGQ Metanfetamina

QJOV22 Metamfetamine

QMQ1QP Metamfetamine

QORSXL Methamphetamine

QPXWKT Metamphetamine

QRCK2V metamphetamine

QRDRJ1 Metamfetamine + Lactose

QTQQQ1 metamfetamine

R2YIAE Metamfetamine

R7GREQ Methamphetamine

RCBIBN metamphetamine

RDRW1X Metamfetamine

RPI8GV Metamfetamine

RRFXUO Metamfetamine

S919AS Methamphetamine

SBKWJS METAMFETAMINE

SHIGZS Metamfetamine, lactose

SRCKGX Methamphetamine

SUSSDP Methamphetamine

SV4SBQ Methylamphetamine

SYLJNC Metamfetamine

SYYY0F metamfetamine

SZVWV9 metamphetamine

T0PFVQ Metamphetamine

TELOLF metamphetamine

U3WKHW Methamphetamine

U479HU Methamphetamine

UHJIRN metamfetamine

UNNSU8 Metamfetamine

USULOL Metamfetamine

UTTTWF metamfetamine

V4HVM5 Methamphetamine

VBO7OP methamphetamine

W7K0RA metamfetamine

WEJJEJ Metamphetamine HCl




WMUWWC MDMA, metanfetamina

WPE9JA metamphetamine

WV88U8 METAMPHETAMINE

WWWBLX Methamphetamine

XGLCLJ Methamphetamine, dimethylamphetamine, N-Formylamphetamine

XLNP6X Metamfetamine

XUE0RE Methamphetamine

Y3XX1B metamfetamine

Y68SYY METHAMPHETAMINE

YMK92M methamphetamine

YQELRV metamphetamine

YQXDTM methamphetamine

YS66H6 metamfetamine

YSSSDR Metamfetamine

YYONQA metamfetamine

Z00LTY Methamphetamine

Z7F75I AMPHETAMINIC DERIVATIVES

Z7JWAE Methamphetamine

ZJZZZ3 Metamphetamine




Code Lactose Metamfetamine

006FMT + + MARQUISE REAGENT: positive result, COBALT THIOCYANATE: negative result, GC-MS: metamfetamine (compared with library MS spectrum of metamfetamine), FTIR: metamfetamine (compare with IR spectrum of metamfetamine), FTIR: lactose (spectrum of ethanol ectract residue compared with IR spectrum of lactose)

02OWVV - - no se pudo determinar por ningún método

07RNYQ ANP + Powder contains metahamphetamine - 17,92 % as base

0O73XC + + SCREENING: REACTIVO DE MARQUIS POSITIVO, REACCION DE ZIMON COLOR AZUL DIFERENCIA DE LA ANFETAMINA, CROMATOGRAFIA EN CAPA FINA Rf CORRESPONDE REVELADOR NINHIDRINA, FTIR ESPECTRO CORRESPONDE A METAMFETAMINA BIBLIOTECA EQUIPO

14YQYB ANP + SM3 contains 40.1% methamphetamine

1IIEIC + + This sample is methamphetamine.

1KOSTW - +

1PSOP9 + + 19,21 % metamfetamine base, laktose

222A22 ANP +

22YK4V ANP + confirmed by gc msd

2333DY + + laktóz

2BSDEQ + + White powder containing 20.0%w/w metamphetamine and lactose

2P2PU2 + + Percentage was 20.5 %. Additionally lactose was identified.

31933H + +

33Q3N2 ANP + Item 2018/2/SM-3 found to contain Metamfetamine.

3CUTP4 + + Lactose

3EOHEE ANP + METAMPHETAMINE

3JJ2TA ANP + We can´t cuantified due to we havent reference pattern

44N4AK + +

49LF34 + + The test sample 2018/2/SM-3 contains 19.54 % m/m metamfetamine.

4EF44P + + LACTOSE




4FMLRF + + Metamfetamine in mixture with lactose


4QMQQQ + + Methamphetamine was found in the sample

4STTTT ANP + Methylamphetamine controlled by the Misuse of Drugs Act 1971 (as amended) as a Class A drug.

555HC5 + + Methamfetamine was identified by TLC and GC/MS ,quantified by GC.

55IZ55 + + Metamphetamin was detected

5BOT5R ANP +

5W5519 + + LACTOSE

60XF00 - + Contain Methamphetamine 19.72% as base

64UHPY + - Metanafetamina y lactosa

6C7TVN + + The test sample 2018/2/SM-3 was found to contain metamfetamine and lactose.

7HN7A7 ANP + In marquis test,we found blue color.We confirm with TLC and GCMS.

7JGGMW - +

7P5A33 ANP -

7S7SS2 + + The sample contains Metamfetamine

7ULAFF ANP + Test sample 201/2/SM-3 was confirmed to contain methamphetamine, a DEA schedule II substance.

7UN77R + + The sample 2018/2/SM-3 was found to contain 225 milligrams of a white powder. This powder was found to contain a mixture of methylamphetamine hydrochlorise and lactose. The purity of methylamphetamine was found to be 24% calculated as salt form.

7Z33IM ANP + It include only Metamfetamine

8288I1 + +

8828D8 + + The sample contains metamfetamine which is listed as a controlled drug according to french order, appendix III of February 22nd 1990.

8TKCKC + + metamfetamine chlorhydrate (15,8% as base) + lactose

8XQEGQ + + Lactose




9CKOOD ANP + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 18. methamphetamine (N,a -dimethylbenzeneethanamine) calculated as the hydrochloride 24% (w/w)

9DKDUD + + Metamfetamine 19% base - Lactose

9LZ9YA - +


9ONAKN ANP + SM-3 was found to contain 19.4% Methamphetamine

9QNQPB + + lactose

9WFUHI - + The powder was analysed and found to contain Methylamphetamine. Methylamphetamine is a class A controlled drug within the provisions of the Misuse of Drugs Act 1971.

9YN990 ANP + Sample SM-3 found to contain Methamphetamine.

A8R888 + + SM 03 was found to contain Metamfetamine and lactose

AAPSTZ ANP +

ADPI7V + + lactose

AEFKAT + + The sample contains Methamphetamine*HCl and Lactose, with 17.80% Methamphetamine base

AGJ544 ANP +

AIQBL5 ANP +

AIW1Z2 ANP + Controlled drug, Metamfetamine, present in sample. Concentration approx 20%

ANAAAW + + Sample 2018/2/SM-3 contains methamphetamine and lactose. Methamphetamine base concentration is (15,2 ± 0,8) %.

AOZMSG - +

BAYSRL + +

BEXBRB ANP + Examination of sample SM-3 revealed the presence the metamphetamine

BLBOCB + + the sample contains methamphetamine hydrochloride (19.8 +/- 0.4% as methamphetamine free base) and lactose

BSWNB0 ANP ANP

BUHHL2 ANP + From screening test using (MR) and from confirmation test using (GC-MS), the sample was found to contain the controlled drug (Methamhetamine).




BZZZIR ANP + SM-3 contain Methamphetamine which is controlled under Malaysian Dangerous Drug Act 1952

C9QQGT + + Using the techniques CR, TLC, GC-MS and FT-IR sample was found to contain Methamphetamine and Lactose

CELGEE ANP + Sample tested positive for Methamphetamine. The substance was confirmed using GC-MS. No quantification was done as the substance is not included in the list of validated quantifiable substances in our laboratory.

CLRNDG + + Sample contains %19,7 methamphetamine.

CMZFLS + + C) One brown tinted glass container, labelled "2018/2/SM-3" "5, with attached black plastic lid that contained 211 milligrams of a white powder. This white powder was found to contain Methylamphetamine Hydrochloride at an average purity of 22% in the salt form. Methylamphetamine Hydrochloride is a Class A drug under the provisions of the Misuse of Drugs Act 1971 (as amended). Lactose is not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

CPBBXT + + We found a mixture of Metamfetamine and lactose. The concentration of Metamfetamine is 30.5% w/w.

CTRBHS ANP + This sample was found to contain Methamphetamine, which is a Class A controlled substance under the Misuse of Drugs Act 1971.

D3UIUC ANP + The sample contain methamphetamine

DIIBXI + + Item 2018/2/SM-3 was found to contain one glass vial which held 227 milligrams of white powder. This powder contained an average of 24% METHYLAMPHETAMINE HYDROCHLORIDE.

DPAIVA + + lactose

DYZ53I + +

ECOCCC + + SM3 contient de la METHAMPHETAMINE avec du lactose

EDHZTN ANP + One glass bottle containing 0.19 grammes of a powder containing 0.03 grammes of methamphetamine.

EQWWGJ ANP + Methamphetamine was identified in the sample 2018/2/SM3


F0000S ANP + No

F9BYIQ - +

FD4JOW + + the sample contains Metamfetamine and Lactose

FPTIMV + +




GCFWS5 ANP + +caffeine


GFFGAC + + WAS FOUND METHANPHETAMINE AND LACTOSE

GKMCN5 ANP + The sample was found to contain 19.4% of methamphetamine (as base).

GU6GGK ANP +

H6MPDC + + Regarding the sample 2018/2/SM-3, a very slow blue color was observed when the SCOTT test was applied to the sample and an orange color after the application of the MARQUIS test, which presupposes the presence of menhanphetamine or its derivatives. What came to be confirmed after the completion of TLc and FTIR. With FTIR, it was also possible to observe the presence of LACTOSE.

H8G1O8 + + Methamphetamine is sheduled as illicit drug in France.

HATVYH + + Lactosa

HDYYZY ANP +

HEVEPB + + The Test sample 2018/2/SM-3 was analyzed by Thin Layer Chromatography technique and was found to contain Metamfetamine and Lactose.

HGGHOG ANP +

HHDUPI ANP + Methylamphetamine is a Class A drug subject to the provisions of the Misuse of Drugs Act 1971.

HI4WNN ANP + Quite usual

HPIHHH + + lactose

HRFHJD + + On analysis, I found the sample "SM-3" containing Metamfetamine and Lactose

HRZZZ0 ANP + -

HUAI9B + + The sample contained 19.1% (w/w) Methamphetamine (base) Lactose also detected in the sample.

ICZF4Z + + Also contain lactose.

IL7F1S + + The sample contains19.9 ± 1.3 weight% metamfetamine-base. The sample also contains lactose.

IODUOV ANP + Powder containing methamphetamine

IXI4IQ ANP +




JDZDJJ + +

JXQBZB + + METAMFETAMINE + LACTOSE

K59V35 + + 2018/2/SM-3 contains Methamphetamine. It also contains lactose.

K9O99N + + lactose

KHGLHU + + Metamfetamine in lactose powder

KILSPH ANP + White powder and odorless

KOQ1NC + +

KSIKUP - + Metamphetamine

KUVU4U + + In the analisys was obteined (Metamfetamine), which controled substance and lactose which is uncontroled substance for Colombia

L9LV6L ANP +

LC7LMZ + + It has been detected the presence of Metamfetamine in the sample.

LLTO7L + + This powder was found to contain methylamphetamine together with the adulterant lactose

LTTTTQ ANP + Sample 2018/2/SM-3 was found to contain 17.6% metamfetamine

MFE65O + + The sample was analyze by GC-MS with differents solvents: Methanol, chloroform, ethanol and ethanol with internal standard.

MJMMJM - + The sample contains 18,8% methamphetamine as free base

MR1LVU + + Sample 2018/2/SM-3 contained Methylamphetamine Hydrochloride, at a concentration of 19% (calculated as base), together with the adulterant Lactose. Methylamphetamine Hydrochloride is a Class A controlled drug under the provision of the Misuse of Drugs Act 1971 (as amended). Lactose is not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

MSFAND - + LACTOSE

MSHBVG + + found Metamfetamine with purity of 18%

N8BKMB ANP + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 18. Methamphetamine (N, a-dimethylbenzeneethanamine) calculated as the hydrochloride 22% (w/w)

NAK5A7 ANP + Sample 2018/2/SM-3 was found to contain methamphetamine.

NCCCCR + + SM-3 was contained Metamfetamine base.The test sample also contained lactose




NPEUNW + + A composite was formed from 1 unit for testing of 1 unit received. Methamphetamine hydrochloride and lactose confirmed in the composite.

NSALLN ANP + TEST SAMPLE 2018/2/SM -3 CONTAIN METAMFETAMINE

NVWID3 - + After chemical analysis was performed the sample was contained AMFETAMINE TYPE STIMULANTS.

OB929H ANP +

OKBALQ ANP +

OLWSRI ANP + It include only Metamfetamine

ORPCAT + + Table 2 Schedule 2, Psychotropic substances (used by medicine)

PCYCJC ANP + metamphetamine is controlled by the Royal Decree of the 6th of september 2017

PM7GBZ ANP + The sample contains Methamphetamine hydrochloride. The purity of the sample is 20.36% as Methamphetamine base.

PMDM1U ANP + White powder material that contains cdrug under international controle - METHAMPHETAMINE.


PQIKKZ ANP +

PUTLIT ANP + The sample contains metamfetamine .

QBF6VQ ANP +

QJJYGQ + + Metanfetamina y lactosa

QJOV22 ANP + It include only Metamfetamine

QMQ1QP + + The sample contains metamfetamine and lactose as an adulterant.The substance is controlled in Poland.

QORSXL + + Methamphetamine (19.9%) and Lactose

QPXWKT + + Presence of metamphetamine hydrochloride and lactose was detected in the sample.

QRCK2V + + lactose

QRDRJ1 + + In the 201/2/SM-3 was proved the presence of metamfetamine and Lactose.

QTQQQ1 ANP + metamfetamine was detected by GC/MS and quantified by LC/MS/MS




R2YIAE - + Examination and analyses performed on the solid in SM-3 showed it to contain metamfetamine ( a central stimulant)

R7GREQ ANP + Methamphetamine confirmed in SM-3

RCBIBN + + metamphetamine

RDRW1X ANP + It include only Metamfetamine


RRFXUO + + Sample contained Metanfetamine as hydrochloride and LACTOSE. Identification of Metanfetamine by FTIR and GC/MS, quantification by GC/FID. Identification of LACTOSE by FTIR and Colorimetric Reactions (MolishTest).

S919AS - + Sample turned white to orange colour with Marquis test and methamphetamine was found in GCMS analysis

SBKWJS + + ./.

SHIGZS + + The sample contains Metamfetamine which is scheduled as illicit drug in France. The lactose is not scheduled as illicit drug in France. It's a cutting agent.

SRCKGX + + The sample contains methamphetamine. The content of methamphetamine is determined to 25 % (as methamphetaminesulphate). Methamphetamine is a controlled substance in X.

SUSSDP - +

SV4SBQ ANP + Powder contains Methylamphetamine (Metamfetamine). Methylamphetamine is a controlled drug under the Misuse of Drugs Acts, 1977 to 2016.

SYLJNC ANP + The sample contains Metamfetamine (19.7%)

SYYY0F + + White powder containing metamfetamine

SZVWV9 + +

T0PFVQ - + We detected metamphetamine in SM-3, but we are not able to give a quantitative result.

TELOLF + + In the sample SM-3 there is a metaphetamine. Metamphetamine is on the list of drugs.

U3WKHW - + we can not quantify methamphetamine because we haven't got seized samples.

U479HU - + Methamphetamine contain 19.12%

UHJIRN - +

UNNSU8 ANP + Based on the above analysis, the sample was found to contain metamfetamine




USULOL ANP + Satisfied with result obtained

UTTTWF + + Low amount of metamfetamine

V4HVM5 + + The sample contained 19.2% of methamphetamine and and also lactose.

VBO7OP - + Non addulterants

W7K0RA ANP + we detected a spot in SM-3 with metamfetamine Rf in thin layer chromatography

WEJJEJ + + Base Metamphetamine 18.57% and Lacose

WMUWWC - + MDMA metanfetamina

WPE9JA + + metamphetamine was detected by GC/MS and quantified by GC/FID

WV88U8 + + LACTOSE

WWWBLX ANP + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 18. Methamphetamine (N, alpha-dimethylbenzeneethanamine)

XGLCLJ + + The major compound we founded in sm-3 after GC/MS injection is dimethylamphetamine

XLNP6X + + Metamfetamine and Lactose

XUE0RE + + The sample contains 19.68 % of Methamphetamine

Y3XX1B + + sample contains metamfetamine and lactose

Y68SYY ANP + On analysis of a representative sample of the powder Methamphetamine was detected with a purity of approximately 24% (calculated as base).

YMK92M ANP + In the test simple 2018/2/SM-3 was detected methamphetamine

YQELRV + + The sample contains metamphetamine. The concentration has not been determined.

YQXDTM ANP + White powder containing methamphetamine (19.0%w/w)

YS66H6 ANP +

YSSSDR + +

YYONQA ANP + White powder containing metamfetamine(20.4%w/w) wich is controlled by national law

Z00LTY ANP + 2018/2/SM-3 has been detected containing 17.4% of Methamphetamine.

Z7F75I ANP + NO MORE FINDINGS




Z7JWAE + + The white powder was analysed and found to contain Methamphetamine.

ZJZZZ3 - + Metamphetamine and sugar are found due to our analysis in the identification part. In the quantification part, the ratio of metaphetamine is calculated as 19.5%.





Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

006FMT S S S SI I

02OWVV SI SI I SI

07RNYQ SI I I

0O73XC S S I I


1IIEIC S I I

1KOSTW I I

1PSOP9 SI I I

222A22 S I I

22YK4V SI I

2333DY I SI SI

2BSDEQ I SI I


31933H S S S SI I

33Q3N2 S I

3CUTP4 I SI I

3EOHEE SI

3JJ2TA S S S I

44N4AK S I I

49LF34 I SI

4EF44P SI I

4FMLRF I S I I S

4ITTTE I SI I

4QMQQQ S S SI

4STTTT S S I

555HC5 S I I

55IZ55 SI I

5BOT5R SI

5W5519 SI I

60XF00 S S I I I

64UHPY SI S S I I I

6C7TVN S S S SI I

7HN7A7 S S I I

7JGGMW SI SI




Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210


7S7SS2 S I I

7ULAFF S S S I


7Z33IM SI SI I SI

8288I1 S S I I

8828D8 I I

8TKCKC I I

8XQEGQ S I I I


9DKDUD SI

9LZ9YA S I

9N8FTT I I

9ONAKN S S I

9QNQPB I I SI I

9WFUHI S I

9YN990 S I

A8R888 S I SI S

AAPSTZ S S S I S

ADPI7V S I SI SI

AEFKAT S I

AGJ544 SI

AIQBL5 SI SI I

AIW1Z2 SI I GC-IRD

ANAAAW S S S I I

AOZMSG S SI SI

BAYSRL SI I

BEXBRB S I


BSWNB0 SI


BZZZIR S S S I

C9QQGT S S S I I

CELGEE SI

CLRNDG S I I


CPBBXT SI SI SI I I

CTRBHS S S I

D3UIUC SI ASAP-QTOF



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

DIIBXI S S S I I

DPAIVA I SI I

DYZ53I S I I I I


EDHZTN S S I SI I


ESWD79 I SI

F0000S S S I I

F9BYIQ S I SI

FD4JOW S I I

FPTIMV SI I I

GCFWS5 S S I I

GF7VNQ I I S

GFFGAC S S I I

GKMCN5 I SI

GU6GGK SI

H6MPDC S S S I I

H8G1O8 I SI I

HATVYH S I I

HDYYZY I SI


HGGHOG S S I

HHDUPI S S I

HI4WNN S S I

HPIHHH SI I

HRFHJD S I I

HRZZZ0 SI

HUAI9B S S S I I I

ICZF4Z S I I

IL7F1S S I SI I

IODUOV S I I SI

IXI4IQ I

JDZDJJ I S

JXQBZB S I I


K9O99N I SI

KHGLHU I SI I

KILSPH S S SI I

KOQ1NC S I I SI



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

KSIKUP I SI I

KUVU4U S S I I

L9LV6L S I

LC7LMZ SI S I

LLTO7L S S I I

LTTTTQ S S SI

MFE65O SI I

MJMMJM SI

MR1LVU S S I I

MSFAND SI

MSHBVG SI I


NAK5A7 I SI

NCCCCR I SI I

NPEUNW SI I

NSALLN S I

NVWID3 SI S I

OB929H SI SI SI I

OKBALQ SI I

OLWSRI S I SI SI

ORPCAT S S S I I I

PCYCJC I S

PM7GBZ S S S I

PMDM1U S S I

PMR0Q7 S S S I I

PQIKKZ SI

PUTLIT SI

QBF6VQ S S S I


QJOV22 SI SI SI


QORSXL S I

QPXWKT S I I I S

QRCK2V I I SI I

QRDRJ1 I SI I I I

QTQQQ1 SI

R2YIAE S S S I I I

R7GREQ S S S I I




Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

RDRW1X S I S I I

RPI8GV I S S SI I I

RRFXUO I SI I

S919AS S S S I I

SBKWJS SI SI

SHIGZS S SI I I

SRCKGX I I

SUSSDP I S

SV4SBQ I I

SYLJNC S S S I I

SYYY0F I SI

SZVWV9 SI I

T0PFVQ S S S I I


U3WKHW SI SI SI I

U479HU S S I

UHJIRN S S S I I

UNNSU8 S I

USULOL S I

UTTTWF S S I I

V4HVM5 I SI

VBO7OP I I I SI

W7K0RA S S I


WMUWW C

S S I I S S

WPE9JA SI I

WV88U8 S I

WWWBL X

S I I GC-FTIR

XGLCLJ I S

XLNP6X I SI I

XUE0RE I SI I

Y3XX1B SI I I I I

Y68SYY S S I I HRMS

YMK92M I

YQELRV I I S Raman

YQXDTM I SI

YS66H6 SI

YSSSDR SI



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

YYONQA I SI

Z00LTY SI I

Z7F75I S S S I I

Z7JWAE S I I

ZJZZZ3 SI I








Metamfetamine 191

Lactose 100


False negatives for Test Sample-3 with respect to Metamfetamine (techniques(s) used):

Analysis not performed for Test Sample-3 with respect to Metamfetamine:

Round Code

BSWNB0 ANP



64UHPY 3,4-Methylenedioxymetamfetamine (MDMA) 140, 180

7P5A33 N-Ethyl-methylenedioxyamphetamine (MDEA) 140, 161

GCFWS5 Caffeine 150, 180

NVWID3 Amfetamine 180

0O73XC 3,4-Methylenedioxymetamfetamine (MDMA) 150, 190

WMUWWC 3,4-Methylenedioxymetamfetamine (MDMA)

171, 180

XGLCLJ Dimethylamphetamine, N-formylamphetamine 180

Round Code Tech Code

7P5A33 140, 161

02OWVV 180

Response Summary

Participants 194

Technique 140 141 142 150 160 161 171 180 190 200 210 211 230 231 250

Screening (No.) 66 74 65 20 2 4 8 70 17 1 2 0 1 0 4

(%) 34.0 38.1 33.5 10.3 1.0 2.1 4.1 36.1 8.8 0.5 1.0 0.0 0.5 0.0 2.1


(%) 10.8 5.7 5.2 20.1 3.1 8.2 13.9 91.8 43.8 1.5 5.2 1.0 1.5 2.6 2.1


(%) 0.0 0.0 0.0 0.0 8.1 22.5 49.5 13.5 0.9 0.0 0.9 0.9 0.9 2.7 0.0

Participants: 194


Z-Score Report per Sample per Substance: Round: 2018/2 Substance: SM-3; Metamfetamine


UNODC value: 19.6%














Code

Metamfetamine

Code

Metamfetamine


Deviation from

robust average


Deviation from

robust average

z-score

F9BYIQ 3.9 -15.4 -13.6 GKMCN5 19.4 0.1 0.1 YSSSDR 6.8 -12.5 -11.1 9ONAKN 19.4 0.1 0.1 PUTLIT 11.6 -7.7 -6.8 ZJZZZ3 19.5 0.2 0.1

RDRW1X 14.5 -4.8 -4.3 5W5519 19.5 0.2 0.1 4STTTT 15.0 -4.3 -3.8 SZVWV9 19.5 0.2 0.1 8TKCKC 15.8 -3.5 -3.1 HPIHHH 19.5 0.2 0.1

4QMQQQ 16.0 -3.3 -3.0 49LF34 19.5 0.2 0.2 HDYYZY 16.2 -3.1 -2.8 UTTTWF 19.6 0.3 0.2 RPI8GV 17.0 -2.3 -2.1 WV88U8 19.6 0.3 0.3 QMQ1QP 17.2 -2.1 -1.9 DYZ53I 19.7 0.4 0.3 Z00LTY 17.4 -1.9 -1.7 XUE0RE 19.7 0.4 0.3 CMZFLS 17.5 -1.8 -1.6 SYLJNC 19.7 0.4 0.3 UHJIRN 17.6 -1.7 -1.5 CLRNDG 19.7 0.4 0.3 LTTTTQ 17.6 -1.7 -1.5 60XF00 19.7 0.4 0.3 AEFKAT 17.8 -1.5 -1.4 QRCK2V 19.8 0.5 0.4 07RNYQ 17.9 -1.4 -1.3 DPAIVA 19.8 0.5 0.4 YMK92M 18.0 -1.3 -1.2 BLBOCB 19.8 0.5 0.4 MSHBVG 18.0 -1.3 -1.2 FPTIMV 19.8 0.5 0.4 QJJYGQ 18.1 -1.2 -1.1 QORSXL 19.9 0.6 0.5 N8BKMB 18.1 -1.2 -1.1 IL7F1S 19.9 0.6 0.5 HATVYH 18.2 -1.1 -1.0 BZZZIR 19.9 0.6 0.5 ANAAAW 18.2 -1.1 -1.0 2BSDEQ 20.0 0.7 0.6 33Q3N2 18.4 -0.9 -0.8 AIW1Z2 20.0 0.7 0.6 TELOLF 18.5 -0.8 -0.8 3CUTP4 20.0 0.7 0.6 WPE9JA 18.5 -0.8 -0.7 55IZ55 20.0 0.7 0.6 WEJJEJ 18.6 -0.7 -0.7 9CKOOD 20.0 0.7 0.6

QTQQQ1 18.6 -0.7 -0.7 OLWSRI 20.0 0.7 0.6 RCBIBN 18.7 -0.6 -0.6 8XQEGQ 20.0 0.7 0.6 SRCKGX 18.7 -0.6 -0.6 9QNQPB 20.1 0.8 0.7 MJMMJM 18.8 -0.5 -0.5 HRZZZ0 20.2 0.9 0.7 1IIEIC 18.9 -0.4 -0.4 AOZMSG 20.2 0.9 0.8 8828D8 18.9 -0.4 -0.4 LC7LMZ 20.2 0.9 0.8 EDHZTN 18.9 -0.4 -0.4 PCYCJC 20.2 0.9 0.8 HRFHJD 18.9 -0.4 -0.4 RRFXUO 20.2 0.9 0.8 VBO7OP 18.9 -0.4 -0.4 PM7GBZ 20.4 1.1 0.9 YQXDTM 19.0 -0.3 -0.3 YYONQA 20.4 1.1 0.9 QPXWKT 19.0 -0.3 -0.3 USULOL 20.5 1.2 1.0 NPEUNW 19.0 -0.3 -0.3 2P2PU2 20.5 1.2 1.0 AIQBL5 19.0 -0.3 -0.3 QJOV22 20.5 1.2 1.0 LLTO7L 19.0 -0.3 -0.3 A8R888 20.9 1.6 1.4 HI4WNN 19.0 -0.3 -0.3 SHIGZS 21.0 1.7 1.5 K9O99N 19.0 -0.3 -0.3 GF7VNQ 21.4 2.1 1.8 MR1LVU 19.0 -0.3 -0.3 7Z33IM 21.9 2.6 2.2 9DKDUD 19.0 -0.3 -0.3 ECOCCC 22.1 2.8 2.4 31933H 19.0 -0.3 -0.3 AAPSTZ 22.2 2.9 2.6 KOQ1NC 19.1 -0.2 -0.2 Y3XX1B 23.2 3.9 3.4 HUAI9B 19.1 -0.2 -0.2 GU6GGK 23.4 4.1 3.6 4EF44P 19.1 -0.2 -0.2 Y68SYY 24.0 4.7 4.1 DIIBXI 19.1 -0.2 -0.2 IXI4IQ 25.2 5.9 5.2

U479HU 19.1 -0.2 -0.2 CPBBXT 30.5 11.2 9.9 7UN77R 19.1 -0.2 -0.2 JDZDJJ 33.0 13.7 12.1 V4HVM5 19.2 -0.1 -0.1 NVWID3 33.6 14.3 12.6 1PSOP9 19.2 -0.1 -0.1 14YQYB 40.1 20.8 18.3 BAYSRL 19.3 0.0 0.0 S919AS 41.9 22.6 19.9 4FMLRF 19.3 0.0 0.0 555HC5 58.6 39.3 34.7 KHGLHU 19.3 0.0 0.0



Sample 4 Analysis



006FMT Amfetamine

02OWVV cafeina

07RNYQ Amphetamine

0O73XC ANFETAMINA

14YQYB Amphetamine

1IIEIC Amphetamine

1KOSTW Amphetamine, Caffeine

1PSOP9 Amfetamine sulfate

222A22 amphetamine

22YK4V amphetamine

2333DY amphetamine

31933H amphetamine

33Q3N2 Amfetamine

3CUTP4 Amphetamine

3EOHEE AMPHETAMINE

3JJ2TA AMFETAMINE

44N4AK amfetamine

49LF34 Amfetamine

4EF44P AMFETAMINE

4FMLRF Amfetamine

4ITTTE amphetamine

4QMQQQ Amphetamine

4STTTT Amphetamine

555HC5 Amfetamine

55IZ55 Amphetamine

5BOT5R Amphetamine

5W5519 AMPHETAMINE

60XF00 Amphetamine Sulfate

64UHPY Anfetamina

6C7TVN Amfetamine

7HN7A7 Amphetamine and caffeine

7P5A33 Amfetamine

7S7SS2 Amfetamine

7ULAFF Amphetamine

7UN77R Amphetamine Sulphate

7Z33IM amfetamine

8288I1 Amfetamine

8828D8 Amfetamine

8TKCKC amfetamine sulfate

8XQEGQ Amphetamine




9CKOOD Amphetamine

9DKDUD amfetamine

9LZ9YA amphetamine

9N8FTT Amfetamine

9ONAKN Amphetamine

9QNQPB Amphetamine

9WFUHI Amphetamine

9YN990 Amphetamine

A8R888 Amfetamine

AAPSTZ amphetamine

ADPI7V amfetamine

AEFKAT Amphetamine

AGJ544 amfetamine

AIQBL5 Amfetamine

AIW1Z2 Amfetamine

ANAAAW Amphetamine

AOZMSG AMFETAMINE 6.6 % AND CAFFEINE

BEXBRB Amfetamine

BLBOCB Amphetamine Sulfate

BZZZIR Amphetamine and Caffeine

C9QQGT Amphetamine, Caffeine and Lactose

CELGEE Amphetamine

CLRNDG amphetamine

CMZFLS AMPHETAMINE

CPBBXT Amfetamine

CTRBHS Amphetamine.

D3UIUC Amphetamine, caffeine

DIIBXI Amphetamine

DPAIVA AMPHETAMINE

DYZ53I Amphetamine sulphate

ECOCCC AMPHETAMINE

EDHZTN Amfetamine

EQWWGJ Amphetamine

ESWD79 Amfetamine

F0000S Amphetamine

FD4JOW Amfetamine

FPTIMV Test sample 2018/2/SM-4 contains Amfetamine + minor Metamfetamine

GCFWS5 amfetamine

GF7VNQ Amfetamine

GFFGAC ANPHETAMINE

GKMCN5 Amphetamine

GU6GGK Amphetamine

H6MPDC Amphetamine + COCAINE + LACTOSE

H8G1O8 Amphetamine




HATVYH Sulfato de Anfetamina

HDYYZY A

HEVEPB Amfetamine, Caffeine and Lactose

HGGHOG Amfetamine

HHDUPI Amphetamine

HI4WNN Amphetamine + Caffeine

HPIHHH amfetamine SO4

HRFHJD Amfetamine

HRZZZ0 Amfetamine

HUAI9B Amphetamine

ICZF4Z Amfetamine

IL7F1S amfetamine

IODUOV Amphetamine

IXI4IQ Amfetamine

JXQBZB AMFETAMINE

K59V35 Amphetamine

K9O99N amphetamine sulphate

KHGLHU Amfetamine

KILSPH Amphetamine and Caffeine

KOQ1NC amphetamine

KSIKUP Amphetamine

KUVU4U Amfetamine

L9LV6L Amphetamine

LC7LMZ amfetamine

LLTO7L Amphetamine, Caffeine, Lactose

LTTTTQ Amfetamine and caffeine

MFE65O Amfetamine + lactose + caffeine

MJMMJM amphetamine

MR1LVU Amphetamine

MSFAND AMFETAMINE

MSHBVG Amfetamine

N8BKMB Amphetamine

NAK5A7 AMPHETAMINE

NCCCCR Amfetamine

NPEUNW Amphetamine

NSALLN AMFETAMINE

NVWID3 Amfetamine

OB929H anfetamina

OKBALQ Amfetamine

OLWSRI amfetamine

ORPCAT Amphetamine, Methamphetamine

PCYCJC amphetamine

PM7GBZ Amphetamine

PMDM1U AMPHETAMINE




PMR0Q7 amphetamine

PQIKKZ amfetamine

PUTLIT Amfetamine

QBF6VQ Amphetamine

QJOV22 Amfetamine

QMQ1QP Amfetamine

QORSXL Amphetamine

QPXWKT Amphetamine

QRCK2V amphetamine

QRDRJ1 Amfetamine + Caffeine + Lactose

QTQQQ1 amfetamine

R2YIAE Amfetamine, caffeine and lactose

R7GREQ Amphetamine & Caffeine

RCBIBN amphetamine

RDRW1X Amfetamine

RPI8GV Amfetamine

S919AS Amphetamine, Caffeine

SBKWJS AMFETAMINE

SHIGZS Amfetamine, caffeine, lactose

SRCKGX Amphetamine

SUSSDP Amphetamine

SV4SBQ Amphetamine

SYLJNC Amfetamine

SYYY0F amfetamine

SZVWV9 amphetamine

T0PFVQ Amphetamine (+ caffeine)

TELOLF amphetamine

U3WKHW Amphetamine

U479HU Amphetamine

UHJIRN amfetamine

UNNSU8 Amfetamine

USULOL Amfetamine and Caffeine

UTTTWF Amfetamine

V4HVM5 Amphetamine

VBO7OP Amphetamine

W7K0RA amfetamine

WEJJEJ Amphetamine sulphate

WMUWWC anfetamina, cafeina

WPE9JA amphetamine

WV88U8 AMPHETAMINE

WWWBLX Amphetamine

XGLCLJ Amphetamine, Formetamide

XLNP6X Caffeine

XUE0RE Amphetamine




Y3XX1B amfetamine

Y68SYY AMPHETAMINE

YMK92M amfetamine

YQELRV Amphetamine

YQXDTM N-methyliminopropylbenzene

YSSSDR Amfetamine

Z00LTY Amphetamine

Z7F75I METHAMPHETAMINE

Z7JWAE Amphetamine

ZJZZZ3 Amphetamine




Code Amfetamine Caffeine Lactose

006FMT + + + MARQUISE REAGENT: positive result, COBALT THIOCYANATE: negative result, GC-MS: amfetamine (compared with library MS spectrum of amfetamine + retention time of reference substance), GC-MS: caffeine (compared with library MS spectrum of caffeine + retention time of reference substance), FTIR: amfetamine (compared with IR spectrum of amfetamine), FTIR: lactose (spectrum of ethanol extract residue compared with IR spectrum of lactose), precipitation reaction with BaCl2: sulfate anions, GC-FID: 9,33% amfetamine sulphate (6,81% amfetamine as base)

02OWVV - + - identificado por GC/Ms

07RNYQ + + ANP Powder contains amphetamine - 6.13 % as base

0O73XC + ANP + SCREENING: REACTIVO DE MARQUIS POSITIVO, REACCION DE SIMON COLOR ROSADO A ROJO DIFERENCIA DE LA METAMFETAMINA, CROMATOGRAFIA EN CAPA FINA Rf CORRESPONDE REVELADOR NINHIRRINA, FTIR ESPECTRO CORRESPONDE A ANFETAMINA BIBLIOTECA NO ENCONTRADO

14YQYB + - ANP SM4 contains 26.2% amphetamine

1IIEIC + + + This sample is amphetamine.

1KOSTW + + -

1PSOP9 + + + 6,28 % amfetamine base, laktose, caffeine

222A22 + + ANP + caffeine

22YK4V + + ANP this sample also contains caffeine

2333DY + + + koffein, laktóz

2BSDEQ - + + White powder containing caffeine and lactose

2P2PU2 - + + Caffeine and Lactose were identified.

31933H + + +

33Q3N2 + ANP ANP Item 2018/2/SM-4 found to contain amfetamine.

3CUTP4 + + + Lactose and Caffeine

3EOHEE + - ANP AMPHETAMINE

3JJ2TA + ANP ANP

44N4AK + + +

49LF34 + + + The test sample 2018/2/SM-4 contains 5.87 % m/m amfetamine.




4EF44P + + + LACTOSE CAFEINE

4FMLRF + + + Amfetamine in mixture with lactose and caffeine

4ITTTE + + + Also contains lactose and coffeine

4QMQQQ + + - Amphetamine was found in the sample

4STTTT + + ANP Amphetamine is controlled by the Misuse of Drugs Act 1971 (as amended) as a Class B drug.

555HC5 + + + Amfetamine was identified by TLC and GC/MS ,quantified by GC.

55IZ55 + + + Amphetamine was detected

5BOT5R + + ANP

5W5519 + + + LACTOSE AND CAFFEIN

60XF00 + + - Contain Amphetamine 6.57% as base and Caffeine

64UHPY + + + anfetamina, cafeina y lactosa

6C7TVN + + - The test sample 2018/2/SM-4 was found to contain amfetamine and lactose.

7HN7A7 + + ANP In GCMS, we found Amphetamine and Caffeine peak.

7JGGMW - + + lactose

7P5A33 + ANP ANP

7S7SS2 + + + The sample contains Amfetamine and Caffeine

7ULAFF + + ANP Test sample 201/2/SM-4 was confirmed to contain amphetamine, a DEA schedule II substance. The sample was also found to contain caffeine.

7UN77R + + + The sample 2018/2/SM-4 was found to contain 228 milligrams of a white powder. This was found to contain a mixture of amphetamine sulphate, caffeine and lactose. The purity of the amphetamine was found to be 10% calculated as salt form.

7Z33IM + + ANP It includes Metamfetamine But it also includes low amounts Caffeine, My-Inositol and Mannitol by adulterants. It includes %2,8 caffeine

8288I1 + + +

8828D8 + + + The sample contains amfetamine which is listed as a controlled drug according to french order, appendix III of February 22nd 1990.

8TKCKC + + + amfetamine sulfate (no quantified) + lactose + cafeine




8XQEGQ + + + Caffeine, Lactose

9CKOOD + ANP ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 19. (1) (ii) Amphetamine (a -methylbenzeneethanamine)

9DKDUD + + + amfetamine 7% base - caffeine, lactose

9LZ9YA + - - Also caffeine

9N8FTT + + + Mass spectrometry profile correlation between sample and reference material certified

9ONAKN + + ANP SM-4 was found to contain amphetamine and caffeine

9QNQPB + ANP + lactose

9WFUHI + - - The powder was analysed and found to contain Amphetamine. A further sample of the powder was analysed and found to contain 6% (weight for weight) Amphetamine. Amphetamine is a class B controlled drug within the provisions of the Misuse of Drugs Act 1971.

9YN990 + + ANP Sample SM-4 found to contain Amphetamine and Caffeine

A8R888 + + + SM 04 was found to contain Amfetamine , caffeine and lactose

AAPSTZ + + ANP and also we have found caffeine

ADPI7V + + + lactose, coffeine

AEFKAT + + + The sample contains Amphetamine sulfate, Caffeine and Lactose, with 7.17% Amphetamine base

AGJ544 + + ANP Also contains caffein

AIQBL5 + + ANP

AIW1Z2 + + ANP Controlled drug, Amfetamine, present in sample. Concentration approx 7. Other substance found is caffeine

ANAAAW + + + Sample 2018/2/SM-4 contains amphetamine, caffeine and lactose. Amphetamine was not quantified because our laboratory does not have reference standard.

AOZMSG + + -

BAYSRL + + +

BEXBRB + ANP ANP Examination of sample SM-4 revealed the presence the amfetamine

BLBOCB + + + the sample contains amphetamine sulfate (7.1 +/- 0.2% as amphetamine free base), caffeine and lactose

BSWNB0 ANP ANP ANP




BUHHL2 - + ANP From confirmation test using (GC-MS), the sample was found to contain the adulterant/diluent caffeine.

BZZZIR + + ANP SM-4 contain Amphetamine which is controlled under Malaysian Dangerous Drug Act 1952 and Caffeine which is controlled under Malaysian Poisons Act 1952

C9QQGT + + + Using the techniques CR, TLC, GC-MS and FT-IR sample was found to contain Amphetamine, Caffeine and Lactose

CELGEE + + ANP Sample tested positive for Amphetamine, Caffeine was also detected in the sample. The substances were confirmed using GC-MS.

No quantification was done as the substance is not included in the list of validated quantifiable substances in our laboratory.

CLRNDG + + + Sample caontains %6,5 amphetamine

CMZFLS + + + D) One brown tinted glass container, labelled "2018/2/SM-4" "5, with attached black plastic lid that contained 226 milligrams of a brown powder. This brown powder was found to contain Amphetamine at an average purity of 9% in the sulphate salt form. Amphetamine is a Class B drug under the provisions of the Misuse of Drugs Act 1971 (as amended). Caffeine and Lactose are not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

CPBBXT + + + We found a mixture of Amfetamine, Caffeine and lactose.

CTRBHS + + ANP This sample was found to contain Amphetamine which is a Class B controlled substance under the Misuse of Drugs Act 1971. It was also found to contain Caffeine which is not controlled.

D3UIUC + + ANP The sample contain amphetamine and caffeine

DIIBXI + + + Item 2018/2/SM-4 was found to contain one glass vial which held 229 milligrams of white powder. This powder contained an average of 7% AMPHETAMINE.

DPAIVA + + + CAFFEINE,LACTOSE

DYZ53I + + +

ECOCCC + + + SM4 contient de l'AMPHETAMINE ,caféine avec du lactose

EDHZTN + + + One glass bottle containing 0.22 grammes of a powder containing 0.01 grammes of amfetamine.

EQWWGJ + + ANP The sample 2018/2/SM-4 was found to contain Amphetamine

ESWD79 + + + Also it was found as a diluents: lactose and caffeine.

F0000S + + ANP Amphetamine is mixed with Caffeine.

F9BYIQ - + -

FD4JOW + + + the sample contains Amfetamine, Caffeine and Lactose




FPTIMV + + +

GCFWS5 + + ANP + caffeine

GF7VNQ + + + Lactose and Caffeine are also present.

GFFGAC + + + WAS FOUND ANPHETAMINE, LACTOSE AND CAFFEINE

GKMCN5 + + ANP The sample was found to contain amphetamine.

GU6GGK + + ANP

H6MPDC + - + With regard to the sample 2018/2/SM-4, no reaction was observed with the SCOTT test but when the MARQUIS test was applied, a light brown color was observed, which may indicate the presence of amphetamine or also cafeine. With regard to the sample 2018/2/SM-4, no reaction was observed with the SCOTT test but when the MARQUIS test was applied, a light brown color was observed, which may indicate the presence of amphetamine or also cafeine. With the application of TLC it was possible to observe the presence of amphetamine and with FTIR there was the presence of amphetamine and possibly cocaine.

H8G1O8 + + + Amphetamine is sheduled as illicit drug in France.

HATVYH + + + Cafeina y Lactosa

HDYYZY + ANP ANP

HEVEPB + + + The Test sample 2018/2/SM-4 was analyzed by Thin Layer Chromatography technique and was found to contain Amfetamine, Caffeine and Lactose.

HGGHOG + - ANP

HHDUPI + - ANP Amphetamine is a Class B drug subject to the provisions of the Misuse of Drugs Act 1971.

HI4WNN + + ANP Quite usual. Typical adulterant.

HPIHHH + + + caffeine lactose

HRFHJD + - + On analysis, I found the sample "SM-4" containing Amfetamine, Lactose and Caffeine

HRZZZ0 + + ANP -

HUAI9B + + + The sample contained Amphetamine. Lactose and Caffeine also detected in the sample.

ICZF4Z + + + Also contain caffeine and lactose.




IL7F1S + + + The sample contains 6.43± 0.56 weight% amfetamine-base. The sample also contains caffeine and lactose.

IODUOV + + ANP Powder containing amphetamine

IXI4IQ + + ANP

JDZDJJ - - +

JXQBZB + + + AMFETAMINE + CAFFEINE+ LACTOSE

K59V35 + + + 2018/2/SM-4 contains Amphetamine. It also contains lactose and caffeine.

K9O99N + + + lactose, caffeine

KHGLHU + + + Amfetamine, caffeine and lactose

KILSPH + + ANP White powder and odorless

KOQ1NC + + +

KSIKUP + + + Amphetamine and coffeine and lactose

KUVU4U + + + In the analisys was obteined (Amfetamine), which controled substance and lactose and caffeine which are uncontroled substance for Colombia.

L9LV6L + + ANP Caffeine

LC7LMZ + + + It has been detected the presence of Amfetamine in the sample.

LLTO7L + + + This powder was found to contain amphetamine together with the adulterants caffeine and lactose

LTTTTQ + + ANP Sample 2018/2/SM-4 was found to contain amfetamine and caffeine.

MFE65O + + + The sample was analyze by GC-MS with differents solvents: Methanol, chloroform, ethanol and ethanol with internal standard.

MJMMJM + - - The sample contains 7.4% amphetamine as a free base

MR1LVU + + + Sample 2018/2/SM-4 contained Amphetamine, at a concentration of 7% (calculated as base), together with the adulterants Caffeine and Lactose. Amphetamine is a Class B controlled drug under the provision of the Misuse of Drugs Act 1971 (as amended). Caffeine and Lactose are not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

MSFAND + - - CAFEINE, LACTOSE

MSHBVG + + + found Amfetamine with purity of 6.5%




N8BKMB + + ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 19. (1) Amphetamine (a-methylbenzeneethanamine)

NAK5A7 + + ANP Sample 2018/2/SM-4 was found to contain amphetamine.The sample was also found to contain caffeine.

NCCCCR + + + SM-4 was contained Amfetamine base.The test sample also contained caffeine, lactose

NPEUNW + + + A composite was formed from 1 unit for testing of 1 unit received. Amphetamine (salt form and isomer not determined), caffeine, and lactose confirmed in the composite.

NSALLN + + ANP TEST SAMPLE 2018/2/SM -4 CONTAIN AMFETAMINE AND CAFFEINE

NVWID3 + + + After chemical analysis was performed the sample was contained AMFETAMINE, Lactose and Caffeine .

OB929H + ANP ANP

OKBALQ + + ANP Caffeine

OLWSRI + + ANP It include both amfetamine and Caffeine by adulterant

ORPCAT + + + Table 2 Schedule 2, Psychotropic substances (used by medicine)

PCYCJC + + ANP amphetamine is controlled by the Royal Decree of the 6th of september 2017

PM7GBZ + + ANP The sample contains Amphetamine sulphate. The purity of the sample is 6.52% as Amphetamine base.

PMDM1U + + ANP White powder material that contains caffeine and drug under international controle - AMPHETAMINE.

PMR0Q7 + + + positive for illicit substance

PQIKKZ + + ANP with Caffeine

PUTLIT + + ANP The sample contains amfetamine and caffeine.

QBF6VQ + + ANP Caffeine and Lactose was found, but the Lactose was found and the Communiqué 2018-086-CAL- QUI Report of uncontrolled substances and traces in Competency Tests indicate that sharp suttances are not reported or outside the scope of the procedures.

QJJYGQ - + + Cafeina y lactosa

QJOV22 + + ANP It include both amfetamine and Caffeine by adulterant

QMQ1QP + + - The sample contains amfetamine and caffeine as an adulterant.The substance is controlled in Poland.

QORSXL + + + Amphetamine (6.2%), cafeine and lactose




QPXWKT + + + Presence of amphetamine sulphate, caffeine and lactose was detected in the sample.

QRCK2V + + + lactose, caffeine

QRDRJ1 + + + In the 2018/2/SM-4 was proved the presence of Amfetamine, Caffeine and Lactose.

QTQQQ1 + + ANP amfetamine was detected by GC/MS and quantified by GC/FID

R2YIAE + + + Examination and analyses performed on the solid in SM-4 showed it to contain amfetamine ( a central stimulant), caffeine (a xanthine stimulant) and lactose

R7GREQ + + ANP Amphetamine and Caffeine confirmed in SM-4.

RCBIBN + + + amphetamine, caffeine

RDRW1X + + ANP It include both Metamfetamine by drug and Caffeine by adulterant.

RPI8GV + + + Identified by GCMS & LCMSMS technique and quantified by GC-FID technique.

RRFXUO + + + Sample contained Anfetamine as hydrochloride, Caffeine and Lactose. Identification of Anfetamine by GC/MS with Certified Reference Material of anfetamine, quantification by GC/FID. Identification of Caffeine by FTIR and GC/MS. Identification of LACTOSE by FTIR.

S919AS + + - Sample turned white to orange colour with Marquis test and Amphetamine and Caffeine were found in GCMS analysis

SBKWJS + + + ./.

SHIGZS + + + The sample contains Amfetamine which is scheduled as illicit drug in France. The lactose and the caffeine are not scheduled as illicit drug in France. They are cutting agent.

SRCKGX + + + The sample contains amphetamine. The content of amphetamine is determined to 9 % (as amphetaminesulphate). Amphetamine is a controlled substance in X.

SUSSDP + + -

SV4SBQ + + ANP Powder contains Amphetamine (Amfetamine). Amphetamine is a controlled drug under the Misuse of Drugs Acts, 1977 to 2016. The amphetamine content of the powder was found to be 6.3 percent.

SYLJNC + + ANP The sample contains Amfetamine (5.4%)

SYYY0F + + + White powder containing amfetamine

SZVWV9 + + +

T0PFVQ + + - We found both amphetamine and caffeine (non-controlled substance) in SM-4, but we are not able to give a quantitative result.

TELOLF + + + In the sample SM-4 there is a amphetamine. Amphetamine is on the list of drugs.




U3WKHW + + - Very low concentration

U479HU + + - Amphetamine

UHJIRN + + - Also caffeine found

UNNSU8 + ANP ANP Based on the above analysis, the sample was found to contain amfetamine

USULOL + + ANP Satisfied with result obtained

UTTTWF + + + Low amount of amfetamine

V4HVM5 + - + The sample contained 6.7% amphetamine and also caffeine and lactose.

VBO7OP + + - Addulterants: caffeine

W7K0RA + ANP ANP we detected two spots in thin layer chromatography for SM-4. one spot was in amfetamine Rf and the other one was in ephedrine Rf.

WEJJEJ + - + Base Amphetamine 6.43%, caffeine and lactose

WMUWWC + + - cafeina anfetamina

WPE9JA + + + amphetamine was detected by GC/MS but not quantified

WV88U8 + + + LACTOSE

WWWBLX + ANP ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 19. (1) Amphetamine (alpha-methylbenzeneethanamine)

XGLCLJ + + + we founded amphetamine in sm-4 after GC/MS injection

XLNP6X - + + Caffeine and Lactose

XUE0RE + + + The sample contains 6.79 % of Amphetamine and also contains Caffeine

Y3XX1B + + + sample contains amfetamine, caffeine and lactose

Y68SYY + + ANP On analysis of a representative sample of the powder Amphetamine was detected with a purity of approximately 7% (calculated as base). The presence of caffeine was also detected

YMK92M + + ANP In the test simple 2018/2/SM-4 was detected amfetamine

YQELRV + + + The sample contains amphetamine and caffeine. The concentration has not been determined.

YQXDTM - + ANP White powder containing N-methyliminopropylbenzene (not quantified) and caffeine (not quantified)

YS66H6 - + ANP




YSSSDR + - +

YYONQA - + ANP White powder containing caffeine

Z00LTY + + ANP 2018/2/SM-4 has been detected containing Amphetamine.

Z7F75I - + ANP CAFEINE

Z7JWAE + + + The white powder was analysed and found to contain Amphetamine.

ZJZZZ3 + - - In the identification part Amphetamine, sugar and cafeine are found. In the quantification part the ratio of amphetamine is calculated as 7%.





Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

006FMT S S S SI I

02OWVV SI SI I SI

07RNYQ SI I I

0O73XC S S I I


1IIEIC S I I

1KOSTW I I

1PSOP9 SI I I

222A22 S I I

22YK4V SI I

2333DY I SI SI

2BSDEQ I SI I


31933H S S S SI I

33Q3N2 S I

3CUTP4 I SI I

3EOHEE SI

3JJ2TA S S S I

44N4AK S I I

49LF34 I SI

4EF44P SI I

4FMLRF I S I I S

4ITTTE I SI I

4QMQQQ S S SI

4STTTT S S I

555HC5 S I I

55IZ55 SI I

5BOT5R SI

5W5519 SI I

60XF00 S S I I I

64UHPY SI S S I I I

6C7TVN S S S SI I

7HN7A7 S S I I

7JGGMW SI SI




Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210


7S7SS2 S I I

7ULAFF S S S I


7Z33IM SI SI I SI

8288I1 S S I I

8828D8 I I

8TKCKC I I

8XQEGQ S I I I


9DKDUD SI

9LZ9YA S I

9N8FTT I I

9ONAKN S S I

9QNQPB I I SI I

9WFUHI S I

9YN990 S I

A8R888 S I SI S

AAPSTZ S S S I S

ADPI7V S I SI SI

AEFKAT S I

AGJ544 SI

AIQBL5 SI SI I

AIW1Z2 SI I GC-IRD

ANAAAW S S S I I

AOZMSG S SI SI

BAYSRL SI I

BEXBRB S I


BSWNB0 SI


BZZZIR S S S I

C9QQGT S S S I I

CELGEE SI

CLRNDG S I I


CPBBXT SI SI SI I I

CTRBHS S S I

D3UIUC SI ASAP-QTOF



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

DIIBXI S S S I I

DPAIVA I SI I

DYZ53I S I I I I


EDHZTN S S I SI I


ESWD79 I SI

F0000S S S I I

F9BYIQ S I SI

FD4JOW S I I

FPTIMV SI I I

GCFWS5 S S I I

GF7VNQ I I S

GFFGAC S S I I

GKMCN5 I SI

GU6GGK SI

H6MPDC S S S I I

H8G1O8 I SI I

HATVYH S I I

HDYYZY I SI


HGGHOG S S I

HHDUPI S S I

HI4WNN S S I

HPIHHH SI I

HRFHJD S I I

HRZZZ0 SI

HUAI9B S S S I I I

ICZF4Z S I I

IL7F1S S I SI I

IODUOV S I I SI

IXI4IQ I

JDZDJJ I S

JXQBZB S I I


K9O99N I SI

KHGLHU I SI I

KILSPH S S SI I

KOQ1NC S I I SI



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

KSIKUP I SI I

KUVU4U S S I I

L9LV6L S I

LC7LMZ SI S I

LLTO7L S S I I

LTTTTQ S S SI

MFE65O SI I

MJMMJM SI

MR1LVU S S I I

MSFAND SI

MSHBVG SI I


NAK5A7 I SI

NCCCCR I SI I

NPEUNW SI I

NSALLN S I

NVWID3 SI S I

OB929H SI SI SI I

OKBALQ SI I

OLWSRI S I SI SI

ORPCAT S S S I I I

PCYCJC I S

PM7GBZ S S S I

PMDM1U S S I

PMR0Q7 S S S I I

PQIKKZ SI

PUTLIT SI

QBF6VQ S S S I


QJOV22 SI SI SI


QORSXL S I

QPXWKT S I I I S

QRCK2V I I SI I

QRDRJ1 I SI I I I

QTQQQ1 SI

R2YIAE S S S I I I

R7GREQ S S S I I




Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

RDRW1X S I S I I

RPI8GV I S S SI I I

RRFXUO I SI I

S919AS S S S I I

SBKWJS SI SI

SHIGZS S SI I I

SRCKGX I I

SUSSDP I S

SV4SBQ I I

SYLJNC S S S I I

SYYY0F I SI

SZVWV9 SI I

T0PFVQ S S S I I


U3WKHW SI SI SI I

U479HU S S I

UHJIRN S S S I I

UNNSU8 S I

USULOL S I

UTTTWF S S I I

V4HVM5 I SI

VBO7OP I I I SI

W7K0RA S S I


WMUWW C

S S I I S S

WPE9JA SI I

WV88U8 S I

WWWBL X

S I I GC-FTIR

XGLCLJ I S

XLNP6X I SI I

XUE0RE I SI I

Y3XX1B SI I I I I

Y68SYY S S I I HRMS

YMK92M I

YQELRV I I S Raman

YQXDTM I SI

YS66H6 SI

YSSSDR SI



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

YYONQA I SI

Z00LTY SI I

Z7F75I S S S I I

Z7JWAE S I I

ZJZZZ3 SI I








Amfetamine 180

Caffeine 166

Lactose 102



FPTIMV Metamfetamine (minor) 150, 180

H6MPDC Cocaine 150, 190

ORPCAT Metamfetamine 150, 180

W7K0RA Ephedrine 150

XGLCLJ Formetamide 180

YQXDTM N-methyliminopropylbenzene 180

Z7F75I Metamfetamine 180, 231

False negatives for Test Sample-4 with respect to Amfetamine (techniques(s) used):

Round Code Tech Code Round Code Tech Code

02OWVV 180 QJJYGQ 180, 190

2BSDEQ 171, 180 XLNP6X 180, 190

2P2PU2 150, 180 YQXDTM 180, 171

7JGGMW 180 YS66H6 180

BUHHL2 180 YYONQA 180, 171

F9BYIQ 171, 180 Z7F75I 180, 231

JDZDJJ 150

Analysis not performed for Test Sample-4 with respect to Amfetamine:

Round Code

BSWNB0 ANP


Response Summary

Participants 194

Technique 140 141 142 150 160 161 171 180 190 200 210 211 230 231 250

Screening (No.) 66 74 65 20 2 4 8 70 17 1 2 0 1 0 4

(%) 34.0 38.1 33.5 10.3 1.0 2.1 4.1 36.1 8.8 0.5 1.0 0.0 0.5 0.0 2.1


(%) 10.8 5.7 5.2 20.1 3.1 8.2 13.9 91.8 43.8 1.5 5.2 1.0 1.5 2.6 2.1


(%) 0.0 0.0 0.0 0.0 8.4 26.3 48.4 10.5 0.0 0.0 1.1 1.1 1.1 2.1 0.0

Participants: 194


Z-Score Report per Sample per Substance: Round: 2018/2 Substance: SM-4; Amfetamine


UNODC value: 7.1%














Code

Amfetamine

Code

Amfetamine


Deviation from

robust average


Deviation from

robust average

z-score

NVWID3 2.1 -4.5 -5.7 4FMLRF 6.7 0.1 0.1 ECOCCC 3.0 -3.6 -4.6 V4HVM5 6.7 0.1 0.1 7P5A33 3.0 -3.6 -4.6 EDHZTN 6.7 0.1 0.1 LC7LMZ 3.2 -3.4 -4.3 HPIHHH 6.7 0.1 0.1

U3WKHW 3.4 -3.2 -4.1 KOQ1NC 6.8 0.2 0.1 8XQEGQ 4.6 -2.0 -2.5 XUE0RE 6.8 0.2 0.2 4STTTT 5.0 -1.6 -2.1 KHGLHU 6.8 0.2 0.2 RDRW1X 5.0 -1.6 -2.0 RPI8GV 6.8 0.2 0.2 AAPSTZ 5.2 -1.4 -1.9 006FMT 6.8 0.2 0.2 QPXWKT 5.2 -1.4 -1.8 DIIBXI 6.9 0.3 0.3 YMK92M 5.3 -1.3 -1.7 CTRBHS 6.9 0.3 0.3 HATVYH 5.3 -1.3 -1.7 7UN77R 7.0 0.4 0.4 SYLJNC 5.4 -1.2 -1.6 TELOLF 7.0 0.4 0.4 3JJ2TA 5.5 -1.1 -1.4 NPEUNW 7.0 0.4 0.5

HI4WNN 5.5 -1.1 -1.4 AIW1Z2 7.0 0.4 0.5 QMQ1QP 5.6 -1.0 -1.3 Y68SYY 7.0 0.4 0.5 BAYSRL 5.8 -0.8 -1.1 ZJZZZ3 7.0 0.4 0.5 49LF34 5.9 -0.7 -1.0 SHIGZS 7.0 0.4 0.5 OLWSRI 5.9 -0.7 -0.9 MR1LVU 7.0 0.4 0.5 QJOV22 5.9 -0.7 -0.9 9DKDUD 7.0 0.4 0.5 9N8FTT 6.0 -0.6 -0.8 RRFXUO 7.1 0.5 0.5 VBO7OP 6.0 -0.6 -0.8 BLBOCB 7.1 0.5 0.6 LLTO7L 6.0 -0.6 -0.8 K9O99N 7.1 0.5 0.6 9WFUHI 6.0 -0.6 -0.8 SZVWV9 7.1 0.5 0.6 8828D8 6.0 -0.6 -0.8 AEFKAT 7.2 0.6 0.7 4EF44P 6.0 -0.6 -0.8 WV88U8 7.2 0.6 0.7 07RNYQ 6.1 -0.5 -0.6 HGGHOG 7.2 0.6 0.7 QORSXL 6.2 -0.4 -0.6 5W5519 7.2 0.6 0.7 1PSOP9 6.3 -0.3 -0.5 UTTTWF 7.3 0.7 0.8 SV4SBQ 6.3 -0.3 -0.4 9QNQPB 7.3 0.7 0.8 FPTIMV 6.4 -0.2 -0.3 DPAIVA 7.3 0.7 0.8 PUTLIT 6.4 -0.2 -0.3 1IIEIC 7.4 0.8 1.0 WEJJEJ 6.4 -0.2 -0.3 MJMMJM 7.4 0.8 1.0 IL7F1S 6.4 -0.2 -0.3 PCYCJC 7.4 0.8 1.0 CMZFLS 6.5 -0.1 -0.2 A8R888 7.4 0.8 1.0 SRCKGX 6.5 -0.1 -0.2 3CUTP4 7.5 0.9 1.1 CLRNDG 6.5 -0.1 -0.2 7Z33IM 7.6 1.0 1.2 MSHBVG 6.5 -0.1 -0.2 HRZZZ0 7.6 1.0 1.3 RCBIBN 6.5 -0.1 -0.2 HDYYZY 8.0 1.4 1.7 PM7GBZ 6.5 -0.1 -0.1 OB929H 8.3 1.7 2.1 60XF00 6.6 0.0 -0.1 UHJIRN 8.5 1.9 2.4 31933H 6.6 0.0 -0.1 555HC5 8.8 2.2 2.8 AOZMSG 6.6 0.0 0.0 IXI4IQ 8.9 2.3 2.9 AIQBL5 6.6 0.0 0.0 4QMQQQ 11.0 4.4 5.5 55IZ55 6.6 0.0 0.0 YSSSDR 11.7 5.1 6.4

QTQQQ1 6.6 0.0 0.0 14YQYB 26.2 19.6 24.8 DYZ53I 6.6 0.0 0.0 Y3XX1B 87.7 81.1 102.6 QRCK2V 6.7 0.1 0.1



Laboratory and Scientific Section UNODC, Vienna International Centre Wagramer Strasse 5, P.O. Box 500 A-1400, Vienna, AUSTRIA Email: [email protected]

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