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Caps
Screw Caps
• Open hole design, seal holds firmly while allowing the
autosamper needle to penetrate
• Usually made from polypropylene
Crimp Caps
• Open hole design
• Lacquered aluminum, or steel magnetic caps
Plug Caps, Polyethylene
• For shell vials
• Sampling needle pierces the cap directly
Screw Thread Measurements: Screw thread dimensions are
designated by a two part number, for example 8/425. The first
number indicates the diameter of the threads across the mouth of
the vial, here 8mm. The second number is a standardized specifi-
cation for thread styles, set by the Glass Packaging Institute (GPI)
and are uniform among American manufacturers.
Seals
Seal Thickness: Seal and facing thickness are listed in millime-
ters in this catalog. Some references express thickness in mils
(thousands of an inch). In general, thicker facings on the seal are
better since thicker materials are less permeable to volatile com-
pounds. One tradeoff, however, is that thicker facings are more
difficult to pierce with an autosampler syring needle.
Standard Seal
• Synthetic rubber, faced with 0.03 mm layer of PTFE
• Total thickness is 1 mm
• Resealable for short term sample storage
• For crimp caps
Seal ST
• High grade resealable seal
• Made from silicone faced on one side with 0.08 mm PTFE
• 1.5 mm thickness
• Available for screw tops only
TruSealTM
• High quality silicone seal
• Coated with 0.08 mm pure PTFE
• Reduced permeability and lower bleed than natural rubber
• For crimp and screw caps
Seal TT
• Premium grade, resealable
• Made from silicone faced on both sides with 0.08 mm PTFE
• Minimizes coring and the subsequent plugging of column
inlets
• Especially recommended for HPLC users
122 Chromatography Research Supplies, Inc.
Vials
Introduction to Autosampler Vials
Vial Selection Process
Most GC and HPLC Autosamplers Use One of Three Size Vials:
• 8 x 30 mm (0.8 mL)
• 12 x 32 mm (1.8 mL)
• 15 x 45 mm (4 mL)
These vials are available in:
• Screw Top
• Crimp Top
• Snap Top
• Shell Styles
Inserts can be used in vials when only a small amount of sample is available or
needed. Small springs are sometimes used to support the insert.
In addition, a one-piece reduced volume vial with the same external volume of the
stadard vial and the “Sleeve System” of supporting micro vials in plastic sleeves
can also be used with small volume samples. The sleeves have the same outer
dimensions as the standard vials and fit many popular autosamplers.
Headspace Autosamplers: Vials come in four sizes, 23 x 38 mm (6mL), 23 x 46
(10mL), 23 x 75 mm (20mL) and 30 x60 mm (27 mL)
Vial Diagrams, pp. 124, 125
Vial / Instrument Cross Reference, pp. 126, 127
www.chromres.com 123
Vials
Introduction to Autosampler VialsSeal PTFE
• Not resealable
• Low cost and recommended for one time use in autosamplers
• Soft and easy to penetrate
• Disks of pure 0.25 mm thick PTFE and cut to the correct
cap diameter
Polyethylene Plug Seal
• Low cost with good chemical resistance
• Seal is pierced directly by the autosampler syringe
• Not resealable
Materials Used in Vial Manufacture
Type 1 Borosilicate Glass
• Includes Type A and Type B glasses specified in ASTM E438
“Glasses in Laboratory Apparatus”
• 33-expansion glass has a coefficient of expansion of 33 x 10-7
cm/cmo C and is a commonly used Type A glass. It is sold
under trademarks Pyrex, Kimax and Duran
• 51-expansion glass is a Type B glass which is popular in
many laboratory applications
• CRS uses only Type 1 borosilicate glass in our autosampler,
EPA and headspace vials
Type II Glass
• Lower grade glass, also known as flint or soda-lime glass
• Has a lower softening point than borosilicate glass
• Inexpensive to make, but less suitable than borosilicate
glass for analytical techniques that requires high sensitivity
Importance of Glass Type:
Water is one of the most severe solvents frequently used in glass
vials. It can slowly dissolve traces of silica and other constituents
from the vials’ wall, altering the pH and potentially causing
increased surface area on which analytes may adsorb. In a com-
parison test between soda-lime glass and borosilicate glass, how-
ever, it has been shown that there is approximately thrity times
less leachables by weight over time from borosilicate glass, with
water as the solvent.
There is very little difference in extractables between Type 1
Class A and B borosilicate glass.
Polypropylene
• Used for disposable autosampler vials because of its
good chemical resistance, physical toughness and low cost
• Recommended for ion chromatography because of its
extremely low metal content and excellent cleanability with
dilute acid followed by deionized water rinse
• Translucent and autoclavable
• Continuous use temperature limit is 105 oC
TPX (Polymethylpentene)
• Popular plastic for vials and general laboratory use because
it is nearly as clear as glass
• Chemical resistance approaches that of polypropylene,
except with some aromatics and chlorinated hydrocarbons
which causes it to soften over time
• Withstands repeated autoclaving to 150 oC
• Fairly brittle at room temperature and may crack or break if
dropped
Chemical Properties of Seal Materials
FEP Fluorinated Ethylene Propylene
• A fluorocarbon with inertness similar to PTFE
• Clear and more flexible than PTFE, thus making an ideal
sealing material
PTFE Polytetrafluoroethylene
• Extremely inert
• Excellent sealing material and has good cleanability for
metals
Silicone
• Outstanding thermal stability, resilience and flexibility
• Allows the material to seal repeatedly after needle penetra-
tion
Rubber
• For most seals used today, it is a blend of natural and
synthetic materials
• Good low cost seal material with moderate re-sealing capa-
bilities
Chlorobutyl Rubber
• Synthetic rubber that offers excellent resistance to most
solvents
• High puncture tolerance and resists coring
• Usable temperature range is -40 oC to 125 oC
1.5 mL, 1.8 mL,
or 2.0 mL Vials?
Different manufacturers rate the capacity of their 12 x 32 mm
vials differently, due to different choices of volume at which a
vial is considered full. However, the dimensions of the vials are
the same. You can buy autosampler vials from CRS with confi-
dence; simply check the vial / autosampler cross-reference
chart on pages 126 - 127 to get the right vial for your instrument.
124 Chromatography Research Supplies, Inc.
Vials - Actual Size
12x32 mm Standard Mouth Vials Standard Mouth Vial Inserts
12x32 mm Wide Mouth Vials Wide Mouth Inserts
Misc. Vials Conical / Limited Volume Vials
Small Volume Crimp Vials
15x45 mm Vials and Inserts
123201 123205 123251 123255
123101 123341 1234060
53
10
1
05
31
59
05
31
51
05
31
61
05
31
71
06
31
01
06
30
11
06
31
51
06
31
81
06
31
71
06
31
61
124001 123248
123281
154655
154645 123153
123321
123353
123175
123161
154505
08
42
01
06
39
71063
95
1
063
551
08
40
51
08
40
01
07
4011
08
3002
074
06
1
0632
51
07
325
1
0632
01
083
061
06
39
61
www.chromres.com 125
Vials - Actual Size
Sample Vials Shell Vials
Reaction Vials
Headspace Vials
Beveled Top
Round Bottom
217003
196503
176005
271406
279515
275705
237504
224604
223801
237501
306001
224601
15454115456212
33
32
08
42
42
08
42
61
08
30
42
099450
099440
099430
0994200
99410
EPA Vials
Beveled Top
Flat Bottom
099400
126 Chromatography Research Supplies, Inc.
Vials
Autosampler Manufacturer/Vial Cross Reference
0.7 / 0.8 mL 0.8 mL 1.8 mL 1.8 mL 4 mL
Crimp Top Crimp Top Crimp Top Screw Top Screw Top
7x40 mm 8x30 mm 12x32 mm 12x32 mm 15x45 mm
Autosampler Std / Wide Std / Wide
Manufacturer Model p. 129 p. 129 p. 132 / p. 134 p. 140 / p.138, 143 p. 148
Agilent 8042,1050,1084,1090 (LC) •/•6850ALS •/• •/• •7670A,7671A •/• •/•7672, 1042, 1080, •/• •/•7673 A/B, 7683 see pages 138 */•
A.I.M. CPS-100 •/• •/•A.I. 42 Vial Tray •/•
60 Vial Tray •Alcott 738 •/•Beckman 501,507 •/• •/•
504 •Brucker LC51 •Chrompack, see Varian •/•CMA, see page 128
CTC Analytics LC PAL, HTS PAL •/• •/•HTC PAL1, GC PAL1 • •/• •/•Combi PAL1 • •/• •/•
Dani ALS 1000 •/•Finnigan A200S •CE Instruments / AS-V 42, AS 105 •/•Fisons AS-V 60 •
AS-800, see page 139
8000 •/•A200S •
Gilson 232-401,231-401 • •/• •/•Asted • •/• •/•Aspec •/• •/•
Hitachi AS-2000, -4000, -6000 2/•S6551 •/•
ICI •Kontron MSI 660 •/• •
360 •/• •/•LDC Marathon •/• •/•
Promis •/• •/• •713 •
LEAP LC PAL, HTS PAL •/• •/•HTC PAL1, GC PAL1 • •/• •/•Combi PAL1 • •/• •/•
Micromeritics
PerkinElmer Autosystem1 •/• •/• •AI-1, Integral 40001 •/•Clarus 500 •/• •/•ISS 100, ISS-200 •/• •/•LC600 (60), AS100 •LC600 42 Tray •/•420/B, 4900 •/•AS100B, AS300, AS2000 •LC30, 2000, B2000 •
* Agilent recommends wide-mouth vials, though standard-mouth vials are useable.1 These also use headspace vials; see Autosampler / Headspace Vial Cross-Reference Chart.2 Use 8 mm wide-lip screw cap.
www.chromres.com 127
Vials
Autosampler Manufacturer/Vial Cross Reference
0.7 / 1 mL 1.8 mL 1.8 mL 4 mL
Crimp Top Crimp Top Screw Top Screw Top
8x30 mm 12x32 mm 12x32 mm 15x45 mm
Autosampler Std / Wide Std / Wide
Manufacturer Model p. 129 p. 132 / p. 134 p. 140 / p. 138, 143 p. 148
Pharmacia LKB 2157-020, see page 139
Shimadzu AOC-8B/9, SIL-6A •/•AOC-14/1400 •/• •/• •SIL-2AS •SIL-6B, SIL-9A •/• •/•ASI-5000, Auto Inject, see page 151
Spark SPH 125 •/•Marathon •/• •/•Promis •/• •/• •
Spectra-Physics 8875 •/• •/•8880 •/• •/•
Tosoh TSK-6080, AS-8010 •/• •/• •Tekmar, see Headspace
Cross-Reference
ThermoElectron AS-2000 • •/• •/•Tracor 770,771,772 •/•Varian 8100, 8035, 8000 Series •/• •
8100/9100/90XX •/• •/•Vista •/•CP-8400, Marathon •/• •/•Combi PAL1 • •/• •/•
Waters 48-Position •96-Posn., see page 131
Alliance •/• •/•
Autosampler Autosampler 6 mL 10 mL 20 mL 27 mL
Manufacturer Model or Type p. 152 p. 152 / p. 155 p. 152 / p. 155 p. 152
Agilent G1888 / 7694E • •A.I. Headspace • •Carlo Erba/Fisons HS 500, HS 700 •CTC Analytics HTC PAL, GC PAL • •
Combi PAL • •Dani HSS 39.50, HSS 86.50 • •
SPT 37.50 •L.E.A.P. Technologies HS 500 •
HTC PAL, GC PAL • •Combi PAL • •
PerkinElmer TurboMatrix HS-16, -40, -110 • •40XL • •Integral 4000 • •
Shimadzu HSS-2B •AOC 5000; ASI-5000 see p. 151 • •
Tekmar 7000HT/7050 • •ThermoElectron AS-2000 •
HS-2000 • •Varian Genesis • • •
Combi PAL • •Prostar 410 •Prostar 420 • •
Headspace Autosampler/Vial Cross Reference
128 Chromatography Research Supplies, Inc.
Vials
6-7 mm Crimp Vials
Description Qty. Item No.
0.3 mL Crimp Top Vial 100/pk 063211
Combo-Pack 0.3 100/pk 063231
(0.3 mL Vial , Cap & Std Seal)
6 x 32 mm Vials 0.3 mL Capacity
• Fits CMA autosamplers, others...
• Uses 8 mm crimp caps and seals listed below.
• Type 1 borosilicate glass.
Description Qty. Item No.
0.6 mL Amber Crimp Vial 100/pk 083061
Combo Pack (Vial, Cap and Std Seal) 100/pk 083081
Support Sleeves, PTFE 50/pk 303001
7x 30 mm Crimp Vials
7 x 30 mm Amber Crimp-Top Vial 0.6 mL Capacity
• Tapered design allows withdrawal of almost all the sample.
• Vial uses 8 mm crimp caps and seals listed below.
• Type 1 borosilicate glass.
Support Sleeves: These are 8 mm wide to mimic standard 8 x 30 mm vials. Support sleeves
are required for proper positioning in autosampler trays that have a depression in the center
of each vial position. They are made from PTFE and are reusable.
Description Material Qty. Item No.
8 mm Cap and Std. Seal PTFE/Rubber 100/pk 308001
8 mm Cap and Seal S PTFE/Silicone 100/pk 308201
8 mm Cap and Seal TT PTFE/Silicone/PTFE 100/pk 308401
8 mm Cap and TruSeal™ PTFE/Silicone 100/pk 308231
8 mm Cap and Seal T PTFE 100/pk 308801
8 mm Crimp Caps and Seals for 6-8 mm Vials
• Caps are made from lacquered aluminum and have an open-hole design.
• Pre-stuffed with seals listed below.
Standard Seal - Good for routine use; self-sealing.
Seal S - A better-quality PTFE/silicone seal.
Seal TT - Premium-grade seal with two layers of PTFE. Coring is virtually eliminated.
TruSeal™ - A silicone/PTFE seal for pennies more than rubber. These offer lower permeabili-
ty and bleed than natural rubber, and resist degradation to 250°C. Because the TruSeal is
soft, lower crimping force is recommended. PTFE layer is 0.08 mm thick; total thickness 1.1 mm.
Seal T - Pure PTFE. Recommended for single use only.
308001
308801
308231
063211
www.chromres.com 129
Vials
7-8 mm Crimp Vials
8 x 30 mm Crimp-Top Vials 0.8 mL Capacity
• Fit many autosamplers.
• Vials use standard 8 mm crimp caps and seals listed on previous page.
• Type 1 borosilicate glass.
Description Qty. Item No.
0.8 mL Clear Vial 200/pk 083002
Combo Pack 200/pk 083022(Clear Vial, Cap and Standard Seal)
0.8 mL Amber Vial 200/pk 083012
Description Qty. Item No.
0.8 mL Amber Crimp Vial 500/pk 074011
Combo-Pack 0.8 500/pk 074031(0.8 mL Vial, Cap & Std Seal)
0.7 mL Amber Crimp Vial 100/pk 074061
Combo-Pack 0.7 100/pk 074081(0.7 mL Vial , Cap & Std Seal)
8 x 30 mm Shell Vials 0.8 mL Capacity
• A handy alternative to crimp-top vials.
• Comes complete with polyethylene plug cap; just push in to seal.
• Cap has 0.5 mm thickness in needle penetration zone for easy piercing.
• Not for use with autosamplers that pressurize the vial.
• Type 1 borosilicate glass.
Description Qty. Item No.
8 x 30 mm Shell Vial & Polyethylene Plug 200/pk 083042
074011 074061
7 x 40 mm Crimp-Top Vials 0.8 mL and 0.7 mL Capacity
• Amber for protection of light-sensitive materials.
• Flat bottom, or tapered bottom for microsampling work.
• Vials use standard 8 mm crimp caps and seals; page 128.
• Type 1 borosilicate glass.
083042
083012083002
130 Chromatography Research Supplies, Inc.
Vials
6-8 mm Crimp Vials; Sci-Vi® System
The Sci-Vi® System for Microsampling
• Unique method of microsampling for virtually all autosamplers.
• Vials fit in PTFE sleeve designed for your instrument.
• Round bottom (0.3 mL) or tapered-bottom (0.2 mL) vials are made from Type 1 borosilicate glass. 6 x 32 mm.
Sleeves - Made from PTFE or glass; reusable. Quantities are as shown below.
8 mm Crimp Caps and Seals for 6-8 mm Vials - Caps are made from lacquered aluminum
and have an open-hole design. Caps are pre-stuffed with seals listed below.
• Standard Seal - PTFE/rubber. Good for routine use; self-sealing.
• Seal TT - PTFE/silicone/PTFE. Coring is reduced, to guard against inlet plugging.
Description Qty. Item No.
Vials and Caps
0.3 mL Crimp Top Vial 100/pk 063201
0.2 mL Crimp Taper Vial 100/pk 063251
8 mm Cap & Std Seal 100/pk 308001
8 mm Cap & Seal TT 100/pk 308401
Combo-Pack 0.3 100/pk 063221
(0.3 mL Vial, Cap and Std Seal)
Combo-Pack 0.2 100/pk 063271
(0.2 mL Vial, Cap and Std Seal)
Sleeves
Sleeve 1. Replaces 1.8 mL Crimp Vials. 50/pk 300001
12x29 mm PTFE.
Sleeve 2. Replaces 0.8 mL Crimp Vials. 50/pk 3000028x27 mm PTFE.
Sleeve 11. Replaces 1.8 mL Crimp Vials 25/pk 300011
in the Agilent 7673A, PE Integral 4000,
and others. PTFE.
Borosilicate Glass version of 25/pk 300021
Sleeve 11. Re-usable.
PTFE Sleeves for the Sci-Vi® System
Sci-Vi Vials in Sleeve 11
063251 063201300011(Sleeve)
www.chromres.com 131
Vials
HPLC Vials
Description Qty. Item No.
1.2 mL Shell Vial with Polyethylene Cap 200 084242
200 µl Insert, Type 1 borosilicate glass 200 053852
1.0 mL PP Tapered Shell Vial with PP Cap 100 084261
Description Material Qty. Item No.
1.2 mL Crimp Top Vial 100/pk 084001
1.0 mL Tapered Crimp Top Vial 100/pk 084051
8 mm Crimp Cap & Std Seal PTFE/Rubber 100/pk 308001
8 mm Crimp Cap & Seal TT PTFE/Sil./PTFE 100/pk 308401
Combo-Pack 1.2 100/pk 084021
(1.2 mL Vial, Cap & Std Seal)
Combo-Pack 1.2P 100/pk 084041
(1.2 mL Vial and PE Plug Cap)
Combo-Pack 1.0 100/pk 084071
(1.0 mL Vial, Cap & Std Seal)
Combo-Pack 1.0P 100/pk 084091(1.0 mL Vial and PE Plug Cap)
Plug Cap for 8 mm Vials Polyethylene 100/pk 308021
Shell Vial and Cap for
Waters; Vial with Insert
Waters 96 Style Shell Vial 1.2 mL Capacity
• Matches the Waters® vial design; 8 x 40 mm (8 x 45 mm with cap, included).
• Made from Type 1 borosilicate glass.
• Polyethylene cap is pre-scored in a star design for easier syringe penetration.
• Insert available for small-volume sampling; fits into the cap.
Tapered-bottom Polypropylene Shell Vial 1.0 mL Capacity
• Has the same 8 x 40 mm external dimensions as the glass vial above
• Comes with pre-scored polyethylene cap.
• Type 1 borosilicate glass.
8 x 40 mm Crimp-Top Vials 1.2 mL, 1.0 mL Capacity
• For Waters 96 Vial Tray
• Flat bottom, or tapered bottom for microsampling work.
• Use standard 8 mm aluminum crimp caps or polyethylene plug caps.
• Vials are made from Type 1 borosilicate glass.
• For cap and seal descriptions see page 128.
084242 053852(Insert)
084261
308001
084001 084051
132 Chromatography Research Supplies, Inc.
Vials
12 x 32 mm Crimp Vials, Standard Mouth
1.8 mL Crimp-Top Vials
• Compatible with most GC and HPLC autosamplers using 12 x 32 mm (1.8 mL) vials
• Standard-width mouth.
• All vials are made from Type 1 borosilicate glass.
Description Qty. Item No.
Clear Crimp Vial 100/pk 123201
Combo-Pack 100/pk 123221
(Clear Vial, Cap & Std Seal)
Combo-Pack TT 100/pk 123231
(Clear Vial, Cap & Seal TT)
Amber Crimp Vial 100/pk 123211
Combo-Pack A 100/pk 123131
(Amber Vial, Cap and Std Seal)
Clear Labeled Crimp Vial 100/pk 123411
Combo-Pack L 100/pk 123491
(Clear Labeled Vial, Cap & Std Seal)
Amber Labeled Crimp Vial 100/pk 123212L
Clear Graduated Crimp Vial 100/pk 123202
Amber Graduated Crimp Vial 100/pk 123203
Description Material Qty. Item No.
11 mm Crimp Cap & Std Seal PTFE/Rubber 100/pk 311001
11 mm Crimp Cap & Seal S PTFE/Silicone 100/pk 311201
11 mm Crimp Cap & TruSeal PTFE/Silicone 100/pk 311231
11 mm Crimp Cap & Seal TT PTFE/Sil./PTFE 100/pk 311401
123201 123411 123212L
311001
311201
311401
311231
123211
11 mm Crimp Caps and Seals for 1.8 mL Vials
• Caps are made from lacquered aluminum and have an open-hole design.
• Pre-stuffed with seals listed below.
Standard Seal - Good for routine use; self-sealing.
Seal S - The better-quality seal.
Seal TT - Premium-grade seal reduces coring, to guard against inlet plugging.
TruSeal™ - A silicone/PTFE seal for pennies more than rubber. These offer lower permeabili-
ty and bleed than natural rubber, and resist degradation to 250° C. Soft, so lower crimping
force is recommended. The PTFE layer is 0.08 mm thick; total thickness is 1.1 mm.
123202 123203
www.chromres.com 133
Vials
12 x 32 mm Crimp, Standard Mouth
Description Qty. Item No.
250 µl Insert for 1.8 mL Vials 100/pk 053101
100 µl Insert, pulled point 100/pk 053159
100 µl Insert, mandrel point 100/pk 053151
100 µl TriSpring Insert 100/pk 053161
100 µl TriSpring Insert, Polypropylene 100/pk 053171
Inserts
• Allows use of microliter-size samples.
• Fit inside standard-mouth 12 x 32 mm, 1.8 mL vials.
• Mandrel- or pulled-point tip available; see box p. 145 for explanation of tip styles.
• Inserts measure 5 x 31 mm except TriSpring inserts, 5 x 29 mm.
• TriSpring inserts have a plastic spring already attached, to center the insert and
absorb shocks to minimize needle damage.
• Type 1 borosilicate glass except as noted.
A) 053101 B) 053159 C) 053151
D) 053161 E) 053171
A B C D E
Tapered-Bottom Vial 1.1 mL / 0.9 mL Capacity
• Microsample and analyze in one vial.
• Unique shape lets you concentrate samples into the tip by solvent evaporation.
• Tapered bottom allows maximum sample recovery.
• Standard mouth design.
• Type 1 borosilicate glass.
Please note: The 0.9 mL Univial is recommended for use with the Agilent 7673 / 7683.
Support Sleeves For use in autosampler trays that offer little lateral (sideways) support.
Sleeves are made from PTFE for repeated use.
Description Qty. Item No.
1.1 mL Tapered-Bottom Vial 100/pk 123251
0.9 mL Tapered-Bottom Vial 100/pk 103201
Combo-Pack 100/pk 1232711.1 mL Univial, Cap & PTFE/rubber Seal
Std Sleeves for 1.1 mL 50/pk 303121
Sleeves for 0.9 mL, for Agilent instruments 50/pk 303131
123251 123251303121
134 Chromatography Research Supplies, Inc.
Vials
12 x 32 mm Crimp, Wide Mouth
Snap / Crimp Wide-Mouth Vials 1.8 mL Capacity
• Easy to use - just snap on the cap.
• Recommended for short-term sample storage; the seal is not as tight as with
crimp or screw caps.
• Type 1 borosilicate glass.
Caps for Snap / Crimp Vials Polyethylene caps, available with a variety of septum materials.
Description Material Qty. Item No.
1.8 mL Snap/Crimp Clear Vial 100/pk 123341
1.8 mL Snap/Crimp Amber Vial 100/pk 123343
1.8 mL Snap/Crimp Clear Vial with Label 100/pk 123371
1.8 mL Snap/Crimp Clear Vial with Label, 100/pk 123344with Pre-inserted 250 µL Insert
Snap Cap for Snap/Crimp Vial PTFE seal 100/pk 311251
Snap Cap for Snap/Crimp Vial PTFE/Rubber seal 100/pk 311261
Snap Cap for Snap/Crimp Vial PTFE/Silicone seal 100/pk 311271
Snap Cap for Snap/Crimp Vial Polyethylene seal 100/pk 311281
123341 123343 123344
311251
311271
1.8 mL Crimp-Top Vials
• Wider opening minimizes bent autosampler needles, especially when using with
inserts.
• All vials are made from Type 1 borosilicate glass.
Caps and Seals Wide-mouth vials use the same caps and seals as our standard mouth vials
on page 132.
Description Qty. Item No.
Clear Wide Crimp Vial 100/pk 123101
Combo-Pack 100/pk 123121(Wide-Mouth Vial, Cap and Standard Seal)
Combo-Pack TT 100/pk 123111(Wide-Mouth Vial, Cap and Seal TT)
Amber Wide Crimp Vial 100/pk 123211A
Amber Wide Labeled Crimp 100/pk 123211L
Clear Graduated Wide Crimp 100/pk 123222
Amber Graduated Wide Crimp 100/pk 123224
123101 123211A 123211L 123222 123224
311261
www.chromres.com 135
Vials
12 x 32 mm Crimp, Wide Mouth
Description Qty. Item No.
Pre-Inserted Clear Vial 100/pk 123281
Pre-Inserted Clear Vial with Label 100/pk 123284
Pre-Inserted Amber Vial with Label 100/pk 123286
Pre-Inserted Crimp Vial 0.25mL Capacity
• Unique one-piece design for easy microsampling in your autosampler.
• Recommended for the Agilent 7673 A/B; 7683 A/B.
• Vials have a mini vial pre-inserted and permanently attached.
• Wide mouth design; uses 11 mm crimp caps and seals.
• Type 1 borosilicate glass.
EvapoVial 1.5mL Capacity
• Allows concentration and micro-volume delivery in the same vial, at a low price.
• The special tapered-ID bottom allows withdrawal of virtually all the sample.
• Wide mouth design.
• May be used with the 6 Port Mini-Vap for easy sample preparation.
• The screw-top EvapoVial comes complete with cap and seal.
• Vials are made from Type 1 borosilicate glass.
Description Qty. Item No.
1.5 mL Clear Crimp EvapoVial 100/pk 123153
11 mm Crimp Cap & PTFE/Rubber Seal 100/pk 311001
1.5 mL Clear Screw EvapoVial 100/pk 123157With Cap and PTFE/Rubber Seal
123281
123153 123157
Inserts
• For use with microliter-sized samples.
• Fits in wide-mouth 1.8 mL, 12 x 32 mm vials.
• Available with pulled-point or mandrel tip, see page 145 for explanation.
• Inserts measure 6 x 31 mm except TriSpring inserts, 6 x 29 mm.
• TriSpring inserts have a plastic spring already attached, to center the insert and
absorb shocks to minimize needle damage.
• Inserts are made from Type 1 borosilicate glass except as noted.
Description Qty. Item No.
350 µl Flat Bottom Insert 100/pk 063101
250 µl Tapered Insert, pulled point 100/pk 063011
250 µl Tapered Insert, mandrel point 100/pk 063151
250 µl TriSpring Insert 100/pk 063161
250 µl TriSpring Insert, Polypropylene 100/pk 063171
250 µl Tapered Hanging Insert 100/pk 063181
A) 063101 B) 063011 C) 063151 D) 063161
E) 063171 F) 063181
A B C D E F
Wide-mouth vial with
Hanging Insert 063181
123284 123286
136 Chromatography Research Supplies, Inc.
Vials
CRS Electronic Crimpers and Decappers
Description Item No.
Electronic Crimper, 8 mm, Complete Kit* 308900
Electronic Crimper, 11 mm, Complete Kit* 311900
Electronic Crimper, 13 mm, Complete Kit* 313900
Electronic Crimper, 20 mm, Complete Kit* 320900
Electronic Decapper, 11 mm, Complete Kit* 311940
Electronic Decapper, 13 mm, Complete Kit* 313940
Electronic Decapper, 20 mm, Complete Kit* 320940
Accessories
Replacement VersaPak® Gold (NiMH) Battery 300905
The Electronic Crimper is designed to fit
around vials placed in standard autosampler
trays. The adjustable setting provides a pre-
cision crimp, vial after vial.
Decapping 20 mm caps is now easy.
11 mm Electronic
Decapper
The cycle of these
tools are controlled
precisely with an
internal counter.
Adjustment
buttons for
precise control.
Hand-held Rechargeable Crimpers and Decappers
• Precision, rechargeable crimpers and decappers for 8, 11, 13 & 20 mm caps.
• Easy to use; comfortable grip.
• Hundreds of reproducible crimps from one charge.
• Adjustable crimping force.
• Includes standard Black & Decker VersaPak® Gold battery and charger.
one
two
three!
* Complete kit includes tool, one battery and battery charger.Please note: Specify country of use when ordering.
The CRS electronic crimping tools are powered by a standard Black and Decker VersaPak® bat-
tery and will cycle hundreds of times on a single charge. The cycle of all of these tools is con-
trolled precisely with an internal counter and is adjusted with two buttons on the side of the case.
The tools fit comfortably in the hand and weigh about 600 grams. When used in a seated position
the jaws can be positioned easily around closely-spaced vials in standard autosampler trays.
The complete tool comes with a VersaPak® Gold rechargeable battery, which uses environmental-
ly friendly NiMH technology, and a charger. Recharging generally takes 6-9 hours.The CRS elec-
tronic crimping tools are available in versions for most countries.
Crimp headspace vials
with the push of a button.
www.chromres.com 137
Vials
CRS Electronic Crimpers and Decappers
HD Crimper - For Heavy-Duty Use, Steel Crimp Caps
• Precision electronic Crimping System.
• Powerful 15v dc supply.
• Fits interchangeable jaw sets in a variety of sizes and styles.
• Multiple programs can be stored to accommodate different jaw sets.
• LCD display shows settings and verifies tool performance.
• Ideal for high-volume crimping.
The HD Crimper is designed to take on tasks that exceed the capability of the battery-pow-
ered electronic crimper. The HD Crimper controller box contains a universal 150 watt dc
power supply that can be plugged into the ac line (120/230volt 50/60 hz).
The motor is powerful enough to crimp and remove magnetic steel crimp caps used in
autosamplers with magnetic pickup arms. Even these caps can be crimped in approximately
1.5 seconds.
The portable tool portion of the HD crimper is connected to the controller box with a flexible
cable. It can be mounted in a support bracket that is attached to the rear of the case, or it
can be used as a portable tool when working with vials in racks.
The crimp cycle can also be started with an optional foot pedal.
Description Item No.
HD Crimper Controller and Power Supply 300900
11mm Jaw Set - Crimping 300911
11mm Jaw Set - Decapping 300912
20mm Jaw Set - Crimping 300920
20mm Jaw Set - Decapping 300921
20mm Jaw Set - Flip Off /Tear Off 300923
Foot Pedal activator for HD Crimper 300995
HD Crimper
Interchangeable jaw sets allow use with all
11 mm and 20 mm crimp caps and seals.
138 Chromatography Research Supplies, Inc.
Vials
CRS Vials for Robotic-Arm Autosamplers
• May be used with almost all autosamplers using 1.8 mL, 12 x 32 mm vials.
• Compatible with robotic autosamplers such as the 7673, 7683 A/B.
• Cap has the same shape as a crimp top seal.
• 40% Larger neck opening than standard-mouth vials.
• Type 1 borosilicate glass.
• Available with a 250 µL insert pre-assembled and permanently attached.
Pre-Stuffed Caps for CRS Robotic-Arm Vials
• Fit CRS robotic-arm type vials.
• Caps available pre-stuffed with several seal materials.
Description Qty. Item No.
CRS Robotic-Arm Clear Vial 100/pk 123242
Combo-Pack 100/pk 123243
(Clear Vial, Cap and PTFE/rubber Seal)
Combo-Pack ST 100/pk 123244
(Clear Vial, Cap and PTFE/Silicone Seal)
Combo-Pack TT 100/pk 123247
(Clear Vial, Cap and PTFE/Silicone/PTFE seal)
CRS Robotic-Arm Clear Vial with Label 100/pk 123248
Combo-Pack ST 100/pk 123250
(Clear Labeled Vial, Cap and PTFE/Silicone Seal)
Combo-Pack Slit Seal 100/pk 123252
(Clear Labeled Vial, Cap and Pre-slit PTFE/Silicone seal)
CRS Robotic-Arm Amber Vial with Label 100/pk 123253
Combo-Pack 100/pk 123254
(Amber Labeled Vial, Cap and Standard Seal)
Combo-Pack ST 100/pk 123256
(Amber Labeled Vial, Cap and PTFE/Silicone Seal)
Combo-Pack TT 100/pk 123258
(Amber Labeled Vial, Cap and PTFE/Silicone/PTFE seal)
Combo-Pack, Clear Pre-Inserted Labeled Vial, 100/pk 123268
Cap and PTFE/Silicone Seal
Combo-Pack, Amber Pre-Inserted Labeled Vial, 100/pk 123273
Cap and PTFE/Silicone Seal
Description Material Qty. Item No.
CRS Pre-Stuffed Caps PTFE 100/pk 309041
for Robotic-Arm Vials PTFE/rubber 100/pk 309042
PTFE/silicone 100/pk 309043
PTFE/Pre-slit silicone 100/pk 309044
PTFE/silicone/PTFE 100/pk 309045
123253 309043
309043
123242
123268
(Combo-
Pack)
123273
(Combo-
Pack)
www.chromres.com 139
Vials
12 x 32 mm, 12 x 40 mm Crimp Vials
Description Qty. Item No.
0.1 mL Polypropylene Crimp Vial 100/pk 123161
Combo-Pack Poly 100/pk 123181
(Polypropylene Vial/Cap/Std Seal)
0.1 mL TPX Crimp Vial 100/pk 123171
0.1 mL Glass Crimp Vial 12/pk 123351
Conical Vials 0.1 mL Capacity
• For microsampling without inserts, simply place in your autosampler.
• External dimensions are the same as regular 12 x 32 mm crimp-top vials.
• Standard-mouth design.
• Type 1 borosilicate glass.
Plastic
• Economical alternative to solid glass vials; disposable.
• Polypropylene is translucent white in color.
• TPX (polymethylpentene) has properties similar to polypropylene, but with
transparency close to that of glass.
Special Purpose Crimp Vials - Use caps and seals on page 132.
Description Qty. Item No.
0.8 mL Snap/Crimp Vial 100/pk 123321
Polypropylene Snap Ring Vial 0.8 mL Capacity
• The highest capacity of any of our plastic 12 x 32 mm vials.
• Vial uses snap caps, page 134, or standard aluminum crimp caps and seals,
page 132.
Description Qty. Item No.
2.5 mL Clear Crimp Vial 100/pk 124001
12 x 40 mm Vial 2.5 mL Capacity
• Fits ThermoFinnigan (Fisons) AS 800, ICI LC1600, Pharmacia LKB 2157-020
• Uses standard 11 mm crimp caps and seals.
• Type 1 borosilicate glass.
123351 123161 123171
123321
124001
140 Chromatography Research Supplies, Inc.
Vials
12 x 32 mm Screw-Top Vials, Standard Mouth
8 mm Seals: ST, TT,
PTFE
309715
1.8 mL Screw-Top Vials• Compatible with most GC and HPLC autosamplers
requiring 1.8 mL, 12 x 32 mm vials (12 x 35 mm with cap).
• Vials use 8 mm, 8-425 Caps.
• Combo Packs include the vial, and cap pre-stuffed with a
PTFE/silicone seal.
• Type 1 borosilicate glass.
Description Material Qty. Item No.
8 mm Black Screw Cap Polypropylene 100/pk 308115
8 mm Wide-Lip Screw Cap Black Polypropylene 100/pk 309115
8 mm Wide-Lip Screw Cap White Polypropylene 100/pk 309415
8 mm Silicone Seal ST PTFE/Silicone 100/pk 308515
8 mm Seal TT PTFE/Silicone/PTFE 100/pk 308715
8 mm Slit Seal PTFE/Silicone 100/pk 309715
8 mm TruSeal™ PTFE/Silicone 100/pk 308565
Pre-Assembled Open-Hole Screw Caps
8 mm (8-425) Cap/Seal ST PP/PTFE/Silicone 100/pk 309525
8 mm (8-425) Cap/Seal TT PP/PTFE/Sil./PTFE 100/pk 309585
8 mm Pierceable Screw Cap Polypropylene/Poly Seal 100/pk 309915
Caps and Seals
• Caps have open hole design; 8-425 threads.
• Available individually, or pre-stuffed with seals to save time and effort.
• Pierceable screw caps are for single-time use. They have a 0.25 mm thick
polypropylene seal molded into the cap, so it can’t fall out.
Note: Shimadzu, Hitachi and Jasco autosamplers require a special wide-lip cap, listed below.
(Or use wide-mouth vials with these autosamplers, listed on page 143.)
Silicone Seal ST Total thickness is 1.5 mm.
Seal TT Double layer of PTFE minimizes coring and inlet plugging.
TruSeal™ These offer reduced permeability and lower bleed than natural rubber, yet cost only
slightly more per seal.
Slit Seal is recommended for Hitachi, Jasco and Shimadzu autosamplers. Prescored for easy
needle penetration. Use with standard-mouth vials and wide-lip caps.
123205 123215
123225
308115
309525
309115
Pierceable ScrewCaps
Description Qty. Item No.
Clear Screw Vial 100/pk 123205
Combo-Pack 100/pk 123225
(Clear Vial, Cap and PTFE/Silicone Seal)
Amber Screw Vial 100/pk 123215
Combo-Pack A 100/pk 123135
(Amber Vial, Cap and PTFE/Silicone Seal)
www.chromres.com 141
Vials
12 x 32 mm Screw-Top Vials, Standard Mouth
Description Qty. Item No.
Clear Labeled Screw Vial 100/pk 123315
Amber Labeled Screw Vial 100/pk 123215L
Combo-Pack L 100/pk 123385
(Labeled Vial, Cap and PTFE/silicone seal)
Clear Graduated Screw Vial 100/pk 123340
Amber Graduated Screw Vial 100/pk 123342
Screw-Top Vials With Label 1.8 mL Capacity
• Mark vials with an ordinary pen or pencil on permanent ceramic patch.
• Graduated-label vials show the approximate volume of contents.
• 8-425 threads
• Type 1 borosilicate glass.
Description Qty. Item No.
250 µl Insert for 1.8mL Vials 100/pk 053101
100 µl Insert, pulled point 100/pk 053159
100 µl Insert, mandrel point 100/pk 053151
100 µl TriSpring Insert 100/pk 053161
100 µl TriSpring Insert,Polypropylene 100/pk 053171
A B C D E
123340 123342
123215L123315
Inserts
• Allows use of microliter-size samples.
• Fit inside standard-mouth 12 x 32 mm, 1.8 mL vials.
• Mandrel- or pulled-point tip available; see box p. 145 for explanation of tip styles.
• Inserts measure 5 x 31 mm except TriSpring inserts, 5 x 29 mm.
• TriSpring inserts have a plastic spring already attached, to center the insert and
absorb shocks to minimize needle damage.
• Type 1 borosilicate glass, except as noted.
A) 053101 B) 053159 C) 053151
D) 053161 E) 053171
142 Chromatography Research Supplies, Inc.
Vials
12 x 32 mm Screw-Top Vials, Standard Mouth
1.1mL Univial in cut-away Sleeve
Description Qty. Item No.
0.1 mL Poly Screw Top Vial 100/pk 123165
0.1 mL TPX Screw Top Vial 100/pk 123175
0.1 mL Clear Glass Vial 12/pk 123353
Description Qty. Item No.
1.1 mL Screw-Top Tapered Vial 100/pk 123255
Combo-Pack 100/pk 123275
(1.1 mL Vial, Cap & PTFE/Silicone Seal)
Standard Sleeves 50/pk 303121
Tapered-Bottom Vial 1.1 mL Capacity
• Microsampling and analysis with one vial.
• Tapered bottom lets you concentrate samples into the tip by solvent evaporation.
• Standard mouth design; 8-425 threads.
• Type 1 borosilicate glass.
Support Sleeves
• For use in autosampler trays that offer little sideways (lateral) support.
• Made from PTFE for repeated use.
Conical Vials 0.1 mL Capacity
• Standard dimensions of 12 x 32 mm, yet 100 µL capacity for small sample sizes.
• Standard mouth design with 8-425 threads.
• Type 1 borosilicate glass.
• Use standard 8-425 thread screw caps and seals (not included).
Plastic Vials
• Economical alternative to solid glass vials; disposable.
• Polypropylene is translucent white in color.
• TPX (polymethylpentene) has properties similar to polypropylene, but with trans-
parency close to that of glass.
123353 123165 123175
123255 123255303121
Description Qty. Item No.
1.8 mL Preassembled Vial ST 100/pk 123425
(Clear Std. Screw Vial, Cap and PTFE/Silicone Seal)
1.8 mL Preassembled Vial TT 100/pk 123435
(Clear Std. Screw Vial, Cap and PTFE/Silicone/PTFE seal)
Pre-assembled Screw-Top Vials 1.8 mL Capacity
• Completely pre-assembled with PTFE/silicone seal and open-hole screw cap.
• Cap is made from polypropylene.
• Vial is made from Type 1 borosilicate glass.
123425
www.chromres.com 143
Vials
12 x 32 mm Screw-Top Vials, Wide Mouth
1.8 mL Screw Top Vials
• 40% larger opening than our standard vial
• Minimizes risk of bent needles; especially when using small-volume inserts.
• Compatible with most GC/HPLC autosamplers requiring 1.8 mL, 12 x 32 mm vials
• Type 1 borosilicate glass.
Description Qty. Item No.
1.8 mL Clear Screw Vial 100/pk 123405
Combo-Pack 100/pk 123415
(Clear Vial, Cap and PTFE/Silicone Seal)
1.8 mL Amber Screw Vial 100/pk 123406
9 mm Seals: ST, TT,
PTFE
Description Material Qty. Item No.
10 mm Black Screw Cap Polypropylene 100/pk 310115
9 mm Silicone Seal ST PTFE/Silicone 100/pk 310515
9 mm Seal TT PTFE/Silicone/PTFE 100/pk 310615
9 mm Seal PTFE PTFE 100/pk 310005
9 mm Slit Seal PTFE/Silicone 100/pk 310815
Cap and Seals
• 10 mm, 10-425 thread cap fits the thread dimensions of 1.8 mL wide-mouth vials.
• Made from polypropylene; open-hole design.
• Wide-mouth vials are recommended for use with autosamplers that require it to
be suspended by the cap, including Shimadzu, Hitachi and Jasco. (Not recom-
mended for the Agilent 7673 or 7683 A/B.)
• Cap uses 9 mm seals.
Silicone Seal ST is made from white silicone rubber faced with a 0.08 mm PTFE layer. Total
thickness of 1.5 mm; resealable.
Seal TT is made from silicone faced on both sides with a 0.08 mm layer of PTFE, to reduce
coring and inlet plugging. Resealable.
Seal PTFE is a disk of pure PTFE, 0.25 mm thick. It is not resealable.
Slit Seal Recommended for Shimadzu, Hitachi and Jasco autosamplers. It is pre-scored for
easy sample needle penetration. The slit seal is made from PTFE layered on pure silicone. It
can also be used with other autosamplers, when lower sampling-needle force is desired.
123405 123406
310115
310815
144 Chromatography Research Supplies, Inc.
Vials
12 x 32 mm Screw-Top Vials, Wide Mouth
Description Qty. Item No.
Graduated Screw Vial 100/pk 123408
Amber Graduated Screw Vial 100/pk 123409
Vials With Graduated Label 1.8 mL Capacity
• Mark vials with an ordinary pen or pencil; ceramic patch is permanently attached.
• Graduated-label vials show the approximate volume of contents.
• Wide-mouth design with 10-425 threads
• Type 1 borosilicate glass.
123409123408
9 mm Seals: ST, TT,
PTFE
Description Material Qty. Item No.
10 mm Black Screw Cap Polypropylene 100/pk 310115
9 mm Silicone Seal ST PTFE/Silicone 100/pk 310515
9 mm Seal TT PTFE/Silicone/PTFE 100/pk 310615
Cap and Seals
• 10 mm, 10-425 thread cap fits the thread dimensions of 1.8 mL wide-mouth vials.
• Made from polypropylene; open-hole design.
• Cap uses 9 mm seals.
Silicone Seal ST is made from white silicone rubber faced with a 0.08 mm PTFE layer. Total
thickness of 1.5 mm; resealable.
Seal TT is made from silicone faced on both sides with a 0.08 mm layer of PTFE, to reduce
coring and inlet plugging. Resealable.
310115
www.chromres.com 145
Vials
Inserts for 12 x 32 mm Vials
Description Qty. Item No.
Inserts for Std. Mouth 1.8 mL Vials, Type 1 Borosilicate Glass
250 µl Flat Bottom Insert 100/pk 053101
100 µl Tapered Insert, pulled point 100/pk 053159
100 µl Tapered Insert, mandrel point 100/pk 053151
100 µl TriSpring Insert 100/pk 053161
Inserts for Std. Mouth 1.8 mL Vials, Polypropylene
100 µl TriSpring Insert 100/pk 053171
Inserts for Wide Mouth 1.8 mL Vials, Type 1 Borosilicate Glass
350 µl Flat Bottom Insert 100/pk 063101
250 µl Tapered Insert, pulled point 100/pk 063011
250 µl Tapered Insert, mandrel point 100/pk 063151
250 µl TriSpring Insert 100/pk 063161
250 µl Tapered Hanging Insert 100/pk 063181
Inserts for Wide Mouth 1.8 mL Vials, Polypropylene
250 µl TriSpring Insert 100/pk 063171
For use when you have only a small amount of sample available for analysis.
• Available in a variety of styles, to fit both standard-mouth and wide-mouth 1.8 mL,
12 x 32 mm vials.
• Inserts for standard-mouth vials measure 5 mm in diameter, while wide-mouth
inserts measure 6 mm in diameter. Inserts measure 31 mm in length, except for
TriSpring inserts, 29 mm.
Flat-bottom inserts have the largest capacity and are generally lowest in cost. They are
placed directly in the host vial.
Tapered-bottom inserts allow sampling of just microliters of liquid, with nearly complete with-
drawal from the tip. They are also set directly into the host vial. The tips are either drawn dur-
ing manufacture (“pulled points”) or formed (“mandrel points”).
TriSpring Inserts These handy inserts have a plastic spring already attached to the tapered
bottom. The spring centers the insert in the host vial and acts as a shock absorber if the insert
is touched by the autosampler needle.
Hanging Insert has a lip that rests on top of a wide-mouth crimp or screw top vial. The sep-
tum seals directly and positively against the insert, reducing the risk of solvent evaporation.
Not available for standard-mouth vials.
Tapered Inserts - Mandrel vs. Pulled Point
Tapered glass inserts are manufactured in differ-
ent ways. The point can either be flame-drawn
and pulled (pulled point) or shaped over a die
(mandrel point). The pulled point is less costly to
produce, while the mandrel point typically has
more accurate dimensional tolerances. Mandrel Point Pulled Point
Inserts: A) Flat Bottom B) Pulled Point C)
Mandrel Point D) TriSpring Glass E) Tri-
Spring Plastic F) Hanging
A B C D E F
Hanging insert; Hanging insert in wide-
mouth screw vial.
063181
146 Chromatography Research Supplies, Inc.
Vials
Other 12 x 32 mm Vials
12 x 32 mm Shell Vial, Insert
and Plug Cap
Shell Vials 1.8 mL Capacity
• Inexpensive alternative to crimp-top or screw-top vials; just push in the cap.
• Can be used in most autosamplers except robot arm types, and autosamplers that pressurize the vial. (Not usable with Agilent 7673/83A and 1090A autosamplers.)
• Polyethylene plug cap included; the needle pierces the cap directly.
• Type 1 borosilicate glass.
Inserts
• Inserts fit into a special collar in the plug cap, for sampling of very small samples.
• 250 µL insert is flat-bottom; 100 µL insert is tapered-bottom.
Description Qty. Item No.
2 mL Clear Shell Vial with Plug Cap 200/pk 123332
2 mL Amber Shell Vial with Plug Cap 200/pk 123362
250 µl Insert 100/pk 053101
100 µl Conical Insert 100/pk 053151
Silanized Vial 1.8 mL Capacity
• Vials have very low chemical absorption, for special applications.
• Screw vial has a standard mouth (8-425) and uses 8 mm caps; see page 140.
• Type 1 borosilicate glass.
Description Qty. Item No.
1.8 mL Clear Screw Vial, Silanized 100/pk 123208
123332 123362
123208
www.chromres.com 147
Vials
Other 12 x 32 mm Vials
0.7 mL Crimp Vial,
“12 x 32 mm” SleeveDescription Qty. Item No.
0.7 mL Amber Crimp Vial 100/pk 073251
Combo-Pack 100/pk 073281
(Vial, Cap and Std Seal)
8 mm Crimp Cap and Std Seal 100/pk 308001
8 mm Crimp Cap and Seal TT 100/pk 308401
Support Sleeves 25/pk 303005
Tapered Crimp Vial and “12 x 32 mm” Sleeve 0.7 mL Capacity
• Vial measures 7 x 32 mm and fits into a 12 x 32 mm PTFE sleeve.
• Vial uses standard 8 mm crimp caps and seals.
• Type 1 borosilicate glass.
Support Sleeve
• Mimics 12 x 32 mm vials; reusable. Made from PTFE.
Caps and Seals
• Cap is made from lacquered aluminum with an open-hole design.
• The Standard Seal is good for routine use; PTFE/rubber. Resealable.
• Seal TT is a premium-grade septum made by coating pure silicone on both sides
with 0.08 mm PTFE, to minimize coring.
148 Chromatography Research Supplies, Inc.
Vials
15 x 45 mm Screw-Top Vials
Inserts for 4 mL Wisp®-type Vial
A) 084201 B) 063951 C) 063551 D) 300501
4.0 mL Vials
• Ideal for your most demanding sampling needs.
• Recommended for pH-sensitive work and other highly
critical applications.
• Type 1 borosilicate glass.
Caps and Seals
• Screw top vials use caps and seals listed at right,
page 149.
Description Qty. Item No.
4.0 mL Clear Screw Top Vial 100/pk 154505
Combo-Pack 100/pk 154525(Clear Vial, Cap and Seal ST)
Combo-Pack T 100/pk 154545
(Clear Vial, Cap & Seal PTFE)
4.0 mL Amber Screw Top Vial 100/pk 154515
Combo-Pack A 100/pk 154535
(Amber Vial, Cap and Seal ST)
Description Qty. Item No.
1.2 mL Shell Insert for 4 mL Vial 100/pk 084201
300 µl Tapered Insert* 100/pk 063951
250 µl Tapered Insert, Polyethylene* 100/pk 063551
50 mm Spring, Steel 100/pk 300501
TriSpring Insert, 300 µl 100/pk 063961
TriSpring Insert, 250 µl, Polypropylene 100/pk 063971
*Requires spring for support
Pre-Assembled Vials
• Vials come completely assembled, with cap and PTFE/silicone seal.
• Type 1 borosilicate glass.
Description Qty. Item No.
4.0 mL Vial, Cap & Seal ST 100/pk 154565
4.0 mL Vial, Cap & Seal PTFE 100/pk 154575
Inserts
• Allow small-volume sampling in 15 x 45 mm vials.
• Shell insert fits directly into the vial. 8 x 42 mm.
• Tapered glass (6 x 41 mm) and tapered polyethylene (6 x 35 mm) inserts require
a spring for support; the spring is reusable.
• TriSpring inserts have a plastic support spring permanently attached, to center
the insert and act as a shock absorber to prevent needle damage.
• Type 1 borosilicate glass, except as noted.
154505 154515
A B C D
154565
063961 063971
www.chromres.com 149
Vials
15 x 45 mm Screw-Top Vials
Description Qty. Item No.
4 mL Clear Labeled Screw Vial 100/pk 154555
Combo Pack L 100/pk 154595
(Labeled Vial, Cap & PTFE/Silicone seal)
Combo Pack LT 100/pk 154615
(Labeled Vial, Cap & PTFE seal)
4 mL Amber Labeled Screw Vial 100/pk 154515L
Clear Graduated Screw Vial 100/pk 154506
Amber Graduated Screw Vial 100/pk 154507
Screw-Top Vial with Label 4 mL Capacity
• Mark vials with an ordinary pen or pencil on permanent ceramic patch.
• Graduated-label vials show approximate volume of contents.
• 13-425 threads.
• Vials use the caps and seals listed below.
• Type 1 borosilicate glass.
Description Material Qty. Item No.
12 mm Screw Cap Polypropylene 100/pk 312115
12 mm Silicone Seal ST PTFE/Silicone 100/pk 312515
12 mm Seal PTFE PTFE 100/pk 312005
12 mm TruSeal™ PTFE/Silicone 100/pk 312565
12 mm Seal TT PTFE/Silicone/PTFE 100/pk 311715
Caps and Seals for 15 x 45 mm Screw-Top Vials
• Caps are made from polypropylene; open-hole design.
• 12 mm caps (13-425 threads) fit the threads of 15 x 45 mm vials.
Silicone Seal is 1.5 mm thick silicone faced on one side with 0.08 mm of PTFE. Resealable.
PTFE Seal is a 12 mm x 0.25 mm thick disk of pure PTFE. For one-time use; not resealable.
Similar to Waters Part No. 73018.
Seal TT is our premium silicone seal coated on both sides with a 0.08 mm thick layer of
PTFE. Resealable. Double layer of PTFE minimizes coring.
TruSeal™ This is a silicone seal for routine sampling. These seals offer reduced permeability
and lower bleed than natural rubber, and resist degradation from –68°C to +250°C. The PTFE
layer is 0.08 mm thick.
12 mm Seals:
ST, TT, PTFE
312565
312115
154506 154507
154555 154515L
150 Chromatography Research Supplies, Inc.
Vials
15 x 45 mm Vials
Description Qty. Item No.
2.5 mL Polypropylene Screw Top Vial 100/pk 154655
2.5 mL Polypropylene Crimp Top Vial 100/pk 154561
Combo-Pack Poly T 100/pk 154675
(2.5 mL Poly Screw Vial, Cap and Seal PTFE)
13 mm Crimp Cap & PTFE/Rubber Seal 100/pk 313001
250 µl Tapered Insert for 100/pk 063551
2.5 mL Poly Vials (requires spring support)
50 mm Spring, Steel 100/pk 300501
Reduced-Volume Polypropylene Vials 2.5 mL Capacity
• 15 x 45 mm polypropylene vial fits WISP® and other autosamplers directly.
• Reduced volume and non-ionic makes it ideal for IC and HPLC applications.
• Interior is tapered at the bottom to allow nearly complete sample withdrawal.
Insert
• Use with the 2.5 mL vials for sampling small volumes.
• Spring is automatically adjusted to the center of the vial.
• Polyethylene.
Caps and Seals: The screw-top polypropylene vial uses the same 12 mm (13-425) screw
caps and seals as listed on page 149. The Crimp-Top Poly Vial uses standard 13 mm alu-
minum crimp caps and seals.
Description Material Qty. Item No.
1.2mL Poly Screw Top Vial Polypropylene 100/pk 154645
Reduced-Volume Polypropylene Vials 1.2 mL Capacity
• Screw-top polypropylene vial fits WISP® and other autosamplers directly.
• Reduced volume and non-ionic makes it ideal for IC and HPLC applications.
• Interior is tapered at the bottom to allow nearly complete sample withdrawal.
• Uses the same 12 mm screw caps and seals as listed on page 149.
Description Qty. Item No.
4.0 mL Shell Vial with Plug 200/pk 154541
1.2 mL Flat-Bottom Insert 100/pk 084201
3.0 mL Tapered Polypropylene Shell 100/pk 154562
Vial & Plug Cap
Shell Vials with Caps and Insert
154562
154561
154645
Shell Vials 4 mL Capacity
• No need to crimp or assemble screw caps.
• Polyethylene plug cap included; just push in to seal.
• Type 1 borosilicate glass.
• The polypropylene Shell Vial has a tapered bottom, for small-volume sampling;
3 mL capacity.
Insert
• For glass shell vials. 1.2 mL capacity; dimensions 8 x 42 mm.
• Type 1 borosilicate glass. 154541
www.chromres.com 151
Vials
Sample Vials; TOC Vials
Vials for Shimadzu ASI-5000 5 mL Capacity
• Designed for use in the Shimadzu model ASI-5000.
• 12 x 96 mm.
• Type 1 borosilicate glass.
Description Qty. Item No.
5 mL Vial, Auto Sample Inj. 100/pk 129610
Screw
Size Dia x Ht, mm Cap Size Qty. Item No.
Clear Sample Vials
1.8 mL 12 x 32 8-425 100/pk 123205
4 mL 15 x 45 13-425 100/pk 154505
8 mL 17 x 60 15-425 200/pk 176003
12 mL 19 x 65 15-425 200/pk 196503
16 mL 21 x 70 18-400 200/pk 217003
24 mL 27 x 57 24-400 100/pk 275705
40 mL 27 x 98 24-400 100/pk 279505
Amber Sample Vials
1.8 mL 12 x 32 8-425 100/pk 123215
4 mL 15 x 45 13-425 100/pk 154515
40 mL 27 x 98 24-400 100/pk 279515
PTFE Lined Screw Caps• Solid (no-hole) replacement screw caps for all of our sample vials and jars.
• PTFE-faced foam seals are ultrasonically bonded to the inside of the caps.
• Not autoclavable.
Description Qty. Item No.
8-425 Thread Screw Cap 100/pk 309925
13-425 Thread Screw Cap 100/pk 309935
15-425 Thread Screw Cap 100/pk 520110
18-400 Thread Screw Cap 100/pk 520310
24-400 Thread Screw Cap 100/pk 520510
38-400 Thread Screw Cap 100/pk 520810
48-400 Thread Screw Cap 100/pk 521110
Sample Vials
• Ideal for sample storage; available in several sizes.
• Vials are made from Type 1 borosilicate glass.
• Use PTFE-lined screw caps shown below.
129610
PTFE Lined Screw Caps
Sample Vials
152 Chromatography Research Supplies, Inc.
Vials
Headspace Vials - Crimp Top
Rounded-Bottom Vials 6 mL, 10 mL, 20 mL and 27 mL Capacity
• Vial lip has a beveled shape (slightly raised inner edge) for
better, tighter seals; see illustration.
• Type 1 borosilicate glass.
• Dimensions are: 6 mL, 23 x 38 mm; 10 mL, 23 x 46 mm;
20 mL, 23 x 75 mm; 27 mm, 30 x 60 mm.
• Vials use standard 20 mm aluminum crimp caps and seals
shown on next page.
Flat Bottom Vials 10 mL, 20 mL Capacity
• Flat-bottom headspace vials for those who cannot use the rounded-bottom style.
• Vials use standard 20 mm aluminum crimp caps and seals and are the same
dimension as round bottom vials listed above.
• Type 1 borosilicate glass.
Precision Electronic Crimpers and Decappers
• Available in rechargeable hand-held, or heavy-duty bench-top models.
• Easy to use; hand-held model has a comfortable, ergonomic grip.
• Adjustable crimping force for consistent, reproducible crimps or decap operations.
• Fits standard aluminum headspace caps and seals.
See pages 136 and 137 for complete information.
Description Qty. Item No.
10 mL Headspace Vial 100/pk 224604
20 mL Headspace Vial 200/pk 237504
6 mL, 10 mL, 27 mL, 20 mL Headspace Vials
Decapping 20 mm caps is easy as...
Precision Electronic Crimper
one
two
three!
Description Qty. Item No.
6 mL Headspace Vial (flat bottom) 100/pk 223801
Combo-Pack 6 100/pk 223821
(6 mL Headspace Vial, Crimp Cap & Septum 3)
10 mL Headspace Vial 100/pk 224601
Combo-Pack 10 100/pk 224621
(10 mL Headspace Vial, Crimp Cap and Septum 3)
20 mL Headspace Vial 100/pk 237501
Combo-Pack 20 100/pk 237521
(20 mL Headspace Vial, Crimp Cap and Septum 3)
27 mL Headspace Vial 100/pk 306001
www.chromres.com 153
Vials
Headspace Vials - Crimp Top
Bellows Seal; Septum 3; Chlorobutyl Seal
Description Qty. Item No.
20 mm Crimp Cap 100/pk 320001
20 mm Safety Crimp Cap 100/pk 320301
20 mm Magnetic Crimp Cap* 100/pk 320605
20 mm Magnetic Ring Crimp Cap† 100/pk 320607
20 mm Seals
All of our headspace seals are 20 mm diameter. For pre-stuffed caps with seals see next page.
Septum 3 Pure silicone rubber, 3 mm thick, coated with 0.13 mm of PTFE.
Septum 2 2.4 mm thick silicone faced with 0.25 mm of PTFE.
Preconditioned Septa for Headspace This is a 20 mm version of our popular seal for soil
sampling. Suitable for your most sensitive analysis; it is pre-conditioned to be free from
volatiles. 0.13 mm layer of PTFE on silicone; 3 mm total thickness.
Chlorobutyl Septum (gray) This is made from pure chlorobutyl rubber, 3 mm thick. It is low
in cost for routine use. Chlorobutyl rubber has greater high-temperature stability compared
with standard butyl rubber.
Butyl Septum (black) Available pre-stuffed in the standard aluminum cap; see next page.
Bellows Seal Chlorobutyl rubber faced with PTFE for superior sample protection. Only PTFE
contacts the sample, while the soft outer ring of rubber makes a tight seal.
20 mm Caps
Standard Cap Made from lacquered aluminum with an open hole design. It fits the 6 mL, 10
mL, 20 mL and 27 mL headspace vials.
Safety Cap Specially designed to vent high-pressure gas at approximately 5 bar (78 psi).
The Safety Cap is made from aluminum.
Magnetic Cap This nickel plated steel cap is for use with autosamplers made by Leap and
CTC, and other autosamplers using a magnetic pick-up arm. May be used with the HD
Electronic Crimper; not suitable for use with the rechargeable 20 mm Electronic Crimper or
Electronic Decapper.
Magnetic Ring Crimp Cap This is a 20 mm aluminum crimp cap, pre-assembled with an
internal steel ring. The steel ring allows use with magnetic pick-up autosamplers while the alu-
minum cap can be crimped with the rechargeable 20 mm Electronic Crimper, the HD Crimper
and other standard crimping tools.
* Not suitable for use with the 20 mm Electronic Crimper or Decapper. Can be crimped with
the HD Crimper, see page 137.
† May be used with the 20 mm Electronic Crimper.
20 mm Magnetic, Standard, and Safety
Crimp Caps
20 mm Magnetic Ring Crimp Cap
Soil Sample Septa for
Headspace
Description Qty. Item No.
20 mm Septum 3 100/pk 320101
20 mm Preconditioned Septa for Headspace 100/pk 320545
20 mm Septum 2 100/pk 320201
20 mm Chlorobutyl Septum (Gray) 100/pk 320401
20 mm Bellows Seal 100/pk 320501
Septum 2
154 Chromatography Research Supplies, Inc.
Vials
Headspace Vials - Crimp Top
320121
320221
320222
320223
320122
320123
320421
320521
20 mm Pre-Stuffed Caps and Seals
Seals are pre-stuffed for added convenience and lower contamination risk. These fit all stan-
dard 6, 10, 20 and 27 mL headspace vials. Aluminum caps may be crimped using the 20 mm
Electronic Crimper, see page 136.
Standard Cap Made from lacquered aluminum; open hole design.
Safety Cap Specially designed to vent high-pressure gas at approximately 5 bar (78 psi).
The Safety Cap is made from aluminum.
Magnetic Cap Made from nickel-plated steel for use with magnetic pick-up arm autosam-
plers. Not suitable for use with the rechargeable 20 mm Electronic Crimper or Electronic
Decapper. May be used with the Heavy Duty Crimper.
Septum 3 Pure silicone rubber, 3 mm thick, coated with 0.13 mm of PTFE.
Septum 2 2.4 mm thick silicone faced with 0.25 mm of PTFE.
Butyl Septum (black) Standard butyl rubber (not chlorobutyl) available pre-stuffed in the alu-
minum cap. Good for routine use.
Bellows Seal Chlorobutyl rubber faced with PTFE for superior sample protection. Only PTFE
contacts the sample, while the outer ring of rubber makes a tight seal.
Description Qty. Item No.
Seals Pre-Stuffed in 20 mm Crimp Caps
20 mm Septum 3 / Standard Aluminum Crimp Cap 100/pk 320121
20 mm Septum 3 / Safety Crimp Cap 100/pk 320122
20 mm Septum 3 / Magnetic Crimp Cap* 100/pk 320123
20 mm Septum 2 / Standard Aluminum Crimp Cap 100/pk 320221
20 mm Septum 2 / Safety Crimp Cap 100/pk 320222
20 mm Septum 2 / Magnetic Crimp Cap* 100/pk 320223
20 mm Black Butyl Septum / Standard Al. Crimp Cap 100/pk 320421
20 mm Bellows Seal / Standard Aluminum Crimp Cap 100/pk 320521
* Not suitable for use with the 20 mm Electronic Crimper or Decapper. Can be crimped with
the HD Crimper, see page 137.
www.chromres.com 155
Vials
Headspace Vials - Screw Top
Precision-Thread Vials 10 mL and 20 mL Capacity
• Recommended for CTC instruments.
• Made from borosilicate glass.
These are an alternative to crimp-top headspace vials, which can be difficult to crimp manual-
ly when steel caps are used. The precision thread design allows a leak-tight seal with moder-
ate twisting force. Since they do not require crimpers or decappers, samples can be taken
and sealed in the field without the need for sample transfer in the lab. Waste solvent disposal
is also easy. Vials can be used either for traditional headspace analyses or SPME. Use with
magnetic screw caps and seals shown below. Vials have rounded bottoms and 18 mm diame-
ter necks. Dimensions: 10 mL vials, 46 x 23 mm; 20 mL vials, 76 mm x 23 mm.
Description Qty. Item No.
10 mL Screw Thread Headspace Vial, Clear 100/pk 224608
Combo-Pack 10 100/pk 224611
(10 mL Screw Thread Headspace Vial,
Magnetic Cap and blue PTFE/white Silicone Seal)
10 mL Screw Thread Headspace Vial, Amber 100/pk 224609
20 mL Screw Thread Headspace Vial, Clear 100/pk 237508
Combo-Pack 20 100/pk 237511
(20 mL Screw Thread Headspace Vial,
Magnetic Cap and blue PTFE/white Silicone Seal)
20 mL Screw Thread Headspace Vial, Amber 100/pk 237509
Description Thickness Shore A Qty. Item No.
Screw Cap, white PTFE/Blue silicone 1.3 mm 35 100/pk 320125
Screw Cap, gray PTFE/Red butyl rubber 1.6 mm 55 100/pk 320128
Screw Cap, red PTFE/White silicone 1.3 mm 45 100/pk 320124
Screw Cap, blue PTFE/White silicone 1.5 mm 55 100/pk 320126
Magnetic Precision-Thread Screw Caps with Seals
• Use with Precision-Thread Vials above.
• Flat upper surface assures strong magnetic bond.
• Seals available in a range of hardnesses.
• 8 mm center hole also suitable for SPME.
Precision-thread magnetic screw caps present a convenient alternative to crimp-cap designs.
Caps come with 18 mm liners already installed. Liners are available in a range of hardnesses,
as measured by Shore A durometer. Liners are thinner than typical crimp-top headspace liner
seals, so they may be more easily pierced by SPME sampling systems.
320125
237508 237509
224608 224609
320128
320124
320126
Description Qty. Item No.
24 mL Clear EPA Vial 100/pk 275705
Combo-Pack 24 (Clear Vial, Cap & Septum) 100/pk 275725
24 mL Amber EPA Vial 100/pk 275805
Combo-Pack 24A (Amber Vial, Cap & Septum) 100/pk 275905
40 mL Clear EPA Vial 100/pk 279505
Combo-Pack 40 (40 mL Vial, Cap & Septum) 100/pk 279525
40 mL Amber EPA Vial 100/pk 279515
Combo-Pack 40A (40 mL Amber Vial, Cap & Septum) 100/pk 279535
60 mL Clear EPA Vial 144/pk 271406
24 mm Screw Cap, 24-400 100/pk 324115
24 mm Screw Cap, 24-414 100/pk 324114
22 mm Standard Seal, PTFE/silicone (0.13 mm PTFE) 100/pk 322515
22 mm PTFE/silicone Seal, (0.25 mm PTFE) 100/pk 322516
22 mm PTFE disk 100/pk 322005
Pre-Assembled 24-400 Screw Cap and Seal 100/pk 324415
Bulk EPA Vials
• Meet specifications for water sampling under EPA 40 CFR, pts. 136 and 141.
• Type 1 borosilicate glass.
• Dimensions: 24 mL vials - 27 x 57 mm; 40 mL vials - 27 x 95 mm; 60 mL vials -
27 x 135 mm.
• All have 24-400 threads and use 24 mm screw caps with 22 mm seals.
Caps
• 24-400 or 24-414 threads; made from polypropylene. Both fit 24-400 thread vials.
The 24-414 thread caps are deeper, and are recommended for use with thick
seals.
• Open-hole design.
Seals
• All seals for headspace are 22 mm diameter and come 100/pk.
• Seals are made from silicone with a PTFE layer. Total thickness 3 mm.
• Available with 0.13 mm or 0.25 mm thick PTFE.
Bulk Pack EPA Vials
Soil Sample Septa
These GC-quality septa have been specially developed for purge-and-trap analysis using soil
sample jars in DynaSoils®, DynaTrap® and similar instruments. Septa are 22 mm diameter
and 3 mm thick, coated on one side with 0.13 mm of PTFE. They are conditioned to be free of
volatiles, and can be stored indefinitely at 80° C - ready for use anytime.
Description Qty. Item No.
Soil Sample Septa, 22 mm 100/pk 322545
322545
322515
322516
322005
279505 279515
324115
156 Chromatography Research Supplies, Inc.
Vials
EPA Sampling Vials—24, 40 and 60 mL
www.chromres.com 157
Vials
EPA Sampling Vials—24, 40 and 60 mL
Precleaned Vials• Precleaned EPA vials come pre-assembled with cap and PTFE/silicone seal.
• 24mL vials measure 27 x 57 mm; 40 mL vials measure 27 x 98 mm.
• Vials are cleaned to Protocol B as specified in the EPA “Specifications and
Guidance for Contaminant-Free Sample Containers.”
• Type 1 borosilicate glass.
Description Qty. Item No.
Clear 24 mL EPA Vials, Precleaned 72/pk 275825
Amber 24 mL EPA Vials, Precleaned 72/pk 275835
Clear 40 mL EPA Vials, Precleaned 72/pk 279825
Amber 40 mL EPA Vials, Precleaned 72/pk 279835
Clear 60 mL EPA Vials, Precleaned 72/pk 271425
Amber 60 mL EPA Vials, Precleaned 72/pk 271435
Precleaned EPA Vials
Pre-Assembled Vials
• Vial is completely pre-assembled, with PTFE/silicone seal and open-hole cap.
• The seal is bonded to the open-hole polypropylene cap using a proprietary
process without glue, so it cannot fall out.
• Vials are made from type 1 borosilicate glass.
Description Qty. Item No.
24 mL EPA Vials, Pre-Assembled 100/pk 275745
40 mL EPA Vials, Pre-Assembled 100/pk 279545
Description Qty. Item No.
24 mm Pre-assembled EPA Cap 100/pk 324415
EPA Vial Screw Caps, Prestuffed with Seal
• Can be heated to 125°C for preparation per EPA protocols, or for autoclaving.
• The PTFE/silicone seal is welded to the polypropylene cap so it cannot fall out.
• Fits 24, 40 and 60 mL EPA Vials. 24-414 threads.
324415
Vial Rack For EPA Vials
This polypropylene rack holds 50, 40 mL EPA vials. It is autoclavable at 121°C for 20 minutes.
Racks have an alpha-numeric indexed vial grid for convenient sample identification and are
stackable, with openings in the well bottoms for drainage. 63/4" x 13" x 11/4".
Description Qty. Item No.
50 Position Rack for EPA Vials 5/pk 868806868806
158 Chromatography Research Supplies, Inc.
Vials
Other Vials
Soil Sample Jars 120 mL Capacity
Clear Jars for soil sampling. Soil sample jars are supplied with caps; caps have 48-400
threads and are lined with PTFE for sample protection. Caps are also available separately.
Jars are without graduations.
Description Qty. Item No.
120 mL Soil Jar 24/pk 472305
Caps, PTFE lined, 48-400 100/pk 521110
Description Thread Size Qty. Item No.
0.1 mL Reaction Vials 8-425 12/pk 099400
0.3 mL Reaction Vials 13-425 12/pk 099410
1.0 mL Reaction Vials 13-425 12/pk 099420
3.0 mL Reaction Vials 20-400 12/pk 099430
5.0 mL Reaction Vials 20-400 12/pk 099440
10.0 mL Reaction Vials 24-400 12/pk 099450
Reaction Vials
These minivials are useful for micro and semi-micro scale reactions or concentration work.
The vials have thick walls, conical tapered interiors and come complete with PTFE-faced sili-
cone liners and open-hole screw caps. Vials have graduation marks (0.1 mL and 0.3 mL vials
are not graduated), and are made from Type 1 borosilicate glass.
099440
472305
099420
www.chromres.com 159
Vials
Other Vials
PTFE Lined Screw Caps
PTFE Lined Screw Caps
• Recommended for storage of samples in EPA vials.
• PTFE-faced foam seals are fixed to the inside of the caps.
• Not autoclavable.
• 24-400 threads.
Description Qty. Item No.
24-400 Thread Screw Cap 100/pk 520510
Soil Sample Septa
• GC-quality septa; specially developed for purge-and-trap analysis using soil sam-
ple jars in DynaSoils®, DynaTrap® and similar instruments.
• Conditioned to be free of volatiles.
• Also superior for EPA sampling.
• 22 mm diameter and 3 mm thick, coated on one side with 0.13 mm of PTFE.
Description Qty. Item No.
Soil Sample Septa, 22 mm 100/pk 322545
322545
160 Chromatography Research Supplies, Inc.
Vials
Crimp Caps and Seals - 8 mm, 11 mm
Description Qty. Item No.
8 mm Blank Crimp Cap 100/pk 308501
8 mm Crimp Cap & Std Seal 100/pk 308001
8 mm Crimp Cap & Std Seal, Red 100/pk 308001R
8 mm Crimp Cap & Std Seal, Green 100/pk 308001G
8 mm Crimp Cap & Std Seal, Blue 100/pk 308001B
8 mm Crimp Cap & Std Seal, Gold 100/pk 308001GO
8 mm Crimp Cap & Seal S 100/pk 308201
8 mm Cap & Seal TT 100/pk 308401
8 mm Cap & TruSeal™ 100/pk 308231
11 mm Blank Crimp Cap 100/pk 311501
11 mm Crimp Cap & Std Seal 100/pk 311001
11 mm Crimp Cap & Std Seal, Red 100/pk 311001R
11 mm Crimp Cap & Std Seal, Green 100/pk 311001G
11 mm Crimp Cap & Std Seal, Blue 100/pk 311001B
11 mm Crimp Cap & Std Seal, Gold 100/pk 311001GO
11 mm Crimp Cap & Seal S 100/pk 311201
11 mm Cap & Seal TT 100/pk 311401
11 mm Cap & TruSeal™ 100/pk 311231
Description Qty. Item No.
7.5 mm Seal PTFE 100/pk 307001
10 mm Seal PTFE 100/pk 310001
8 mm Caps and Seals These fit all standard 6-, 7- and 8 mm- diameter crimp-
top vials, and others with 8 mm lips. Caps with standard seals are available plain or in red,
green, blue and gold.
11 mm Caps and Seals These fit all common 12 x 32 mm (1.8 mL) crimp vials,
both standard and wide mouth. Caps with standard seals are available plain or in red, green,
blue and gold.
Blank Crimp Caps• Made from lacquered aluminum for good crimping properties with low cost.
• Open-hole design.
Crimp Caps Pre-stuffed with Seals• Use the same lacquered aluminum crimp cap as above.
• Pre-stuffed with the following seals:
Standard Seal Rubber, 1 mm thick, faced on one side with a 0.03 mm layer of PTFE for
sample protection.
Seal S A quality PTFE/silicone seal; silicone offers good sealing properties.
Seal TT Our premium-grade silicone seal, coated on both sides with a 0.08 mm layer of
PTFE. Minimizes coring and the resulting inlet plugging.
TruSeal™ Our PTFE/silicone seal that costs just pennies more than rubber. It offers reduced
permeability and lower bleed, and resists degradation from –68°C to +250°C. The silicone is
softer than in many seals, so lower crimp force is needed. TruSeals have a 0.08 mm thick
layer of PTFE on 1.1 mm thick silicone.
Seal PTFE
• Disks of pure PTFE, 0.25 mm thick.
• Easy to penetrate and inexpensive for one-time use. Not resealable.
• The 7.5 mm seal fits 8 mm crimp caps; the 10 mm seal fits 11 mm crimp caps.
308001
311001
311231
311501
310001
www.chromres.com 161
Vials
Screw Caps and Seals, Open Hole
Screw Caps, Polypropylene8 mm Screw Cap 8-425 threads. Fits standard-mouth 12 x 32 mm vials.
8 mm Wide Lip Screw Cap 8-425 threads. Specially designed for Shimadzu, Hitachi and
Jasco autosamplers. It fits standard 12 x 32 mm vials, but is made with a wider outer lip.
10 mm Screw Cap 10-425 threads. Fits wide-mouth 12 x 32 mm vials.
12 mm Screw Cap 13-425 threads. Fits standard 15 x 45 mm (4 mL Wisp) vials.
Seals• 8 mm Seals fit 8 mm, 8-425 thread screw caps.
• 9 mm Seals fit 10 mm, 10-425 thread screw caps.
• 12 mm Seals fit 12 mm, 13-425 thread screw caps.
Silicone Seal ST (Red) This is our standard seal for screw-top vials, offering good perform-
ance at low cost. White silicone layered with 0.08 mm of red PTFE. 1.5 mm thick.
Silicone Seal (Cream) Similar to our red silicone seal, except that the PTFE is 0.13 mm
thick for added protection. Cream-colored PTFE on white silicone.
Seal TT Pure silicone rubber coated on both sides with a 0.08 mm layer of PTFE. Preferred
by many because it minimizes coring and inlet plugging.
TruSeal™ Quality silicone septum faced with a 0.08 mm layer of PTFE. The TruSeal features
reduced permeability and lower bleed than rubber. Total thickness 1.1 mm.
Slit Seal Designed for Shimadzu, Hitachi and Jasco autosamplers. Pre-scored for easy sam-
ple needle penetration; it is made from PTFE layered on pure silicone. This seal can also be
used with other autosamplers for a lower sampling pressure.
Seal PTFE Disks of pure PTFE, 0.25 mm thick. Easy to penetrate, but cannot be resealed.
The 7.5 mm size fits 8 mm crimp caps.
Seal ST
Cream Seal
TruSeal
Slit Seal
Seal PTFE
Seal TT
308115 309115
310115
312115
Description Qty. Item No.
Caps
8 mm Black Screw Cap 100/pk 308115
8 mm Wide-Lip Screw Cap 100/pk 309115
10 mm Black Screw Cap 100/pk 310115
12 mm Black Screw Cap 100/pk 312115
12 mm White Screw Cap 100/pk 312415
Seals
8 mm Silicone Seal ST (Red) 100/pk 308515
8 mm Cream Silicone Seal 100/pk 308915
8 mm Seal TT 100/pk 308715
8 mm TruSeal™ 100/pk 308565
8 mm Slit Seal 100/pk 309715
7.5 mm Seal PTFE 100/pk 307001
9 mm Seal ST(Red) 100/pk 310515
9 mm Seal TT 100/pk 310615
9 mm Slit Seal 100/pk 310815
9 mm Seal PTFE 100/pk 310005
12 mm Silicone Seal ST (Red) 100/pk 312515
12 mm Cream Silicone Seal 100/pk 312915
12 mm Seal TT 100/pk 311715
12 mm TruSeal™ 100/pk 312565
12 mm Seal PTFE 100/pk 312005
162 Chromatography Research Supplies, Inc.
Vials
Screw Caps, Pre-Assembled
Description Qty. Item No.
8 mm Open-Hole Preassembled 100/pk 309525
Screw Cap & PTFE/Silicone Seal
8 mm Pierceable Screw Cap 100/pk 309915
8 mm Solid Phenolic Cap / PTFE Liner 100/pk 309925
Caps are available either open-hole for autosampler use, or solid (no-hole) for storing sam-
ples. They are made from polypropylene, or phenolic where noted. Choose the seal material
that is best for your sampling needs.
Pierceable Screw Caps for autosampler use are designed for fast and easy sample prepara-
tion; there are no seals to assemble. A 0.25 mm thick polypropylene seal is molded directly
into the cap, so it can’t fall out. Concentric raised ridges at the contact point with the vial
ensure a positive seal. Low cost for single-time use.
Polyethylene Plugs are suitable for most vials and autosamplers. Many people find them
easier to work with than crimp- or screw-caps; just push into the vial. Do not use polyethylene
plugs with systems that pressurize the vial.
Seal ST These are silicone faced with PTFE; only the PTFE contacts your sample.
8 mm Screw Caps, 8-425 ThreadsPreassembled for all common 12 x 32 mm Standard-Mouth Vials
Description Qty. Item No.
Plug 11-2 100/pk 311021
Plug 8-1 100/pk 308021
12 mm Screw Caps, 13-425 ThreadsPreassembled; fit 15 x 45 mm autosampler vials
Open-Hole and Solid Pre-assembled
Screw Caps
Pierceable Screw Caps
Polyethylene Plug Caps
Polyethylene Plug Caps
These are for use with screw-top or crimp-top vials; not for use with shell vials. (For replace-
ment shell vial plugs, see listings with the respective shell vials.) Do not use with systems that
pressurize the vial. Plug 11-2 fits 12 x 32 mm standard mouth vials, pages 132 and 140. Plug
8-1 fits 7 x 40 mm and 8 x 30 mm vials, page 129.
Description Qty. Item No.
12 mm Pierceable Screw Cap 100/pk 312815
12 mm Solid Phenolic Cap/ PTFE Liner 100/pk 309935
www.chromres.com 163
Vials
Accessories - Crimpers
Manual Crimpers
Precision-crafted hand operated crimpers are used to secure aluminum caps to autosampler
vials. They are easy to use and durable for years of dependable service. Crimper jaws are
made of steel. An adjustable stop in the handle can be set to give the same sealing tightness
every time. Available in four sizes: 8 mm for all crimp-top vials using 8 mm caps; 11 mm for
all vials using 11 mm caps (includes standard- and wide-mouth 12 x 32 mm crimp vials); 13
mm and 20 mm (for crimp-top headspace vials).
Description Item No.
8 mm Precision Crimper 308000
11 mm Precision Crimper 311000
13 mm Precision Crimper 313000
20 mm Precision Crimper 320000
Precision Decappers
Remove caps quickly and easily; avoids broken vials and sharp aluminum. Our precision
decappers are made with steel jaws for toughness and years of use. Simply hold the cap in
the decapper, squeeze, and the cap pulls off effortlessly. A necessity when dangerous sam-
ples must be collected before discarding vials. Available in four popular sizes: 8 mm for all
crimp-top vials using 8 mm caps; 11 mm for all vials using 11 mm caps (includes standard-
and wide-mouth 12 x 32 mm crimp vials); 13 mm and 20 mm (for crimp-top headspace vials).
Description Item No.
8 mm Precision Decapper 308040
11 mm Precision Decapper 311040
13 mm Precision Decapper 313040
20 mm Precision Decapper 320040
CRS Rechargeable Crimpers and Decappers
These precision, rechargeable tools are available for 8, 11, 13 and 20 mm crimp caps. The
Electronic Crimper allows hundreds of reproducible crimps from one charge, and has an easi-
ly-set, adjustable crimping force.
For more information, see pages 136 - 137.
PTFE Lined Screw Caps
CRS offers solid (no-hole) replacement screw caps for all of the sample vials and jars we sell.
They have PTFE-faced foam seals fixed to the inside of the caps. Not autoclavable.
Description Qty. Item No.
8-425 Thread Screw Cap 100/pk 309925
13-425 Thread Screw Cap 100/pk 309935
15-425 Thread Screw Cap 100/pk 520110
18-400 Thread Screw Cap 100/pk 520310
24-400 Thread Screw Cap 100/pk 520510
311000
311040
164 Chromatography Research Supplies, Inc.
Vials
Accessories
Autosampler Vial Holder
Our unique vial holder is fabricated from spongy foam plastic, to hold vials for filling, sample
prep or storage. Low enough in price to replace if they become contaminated. Holds 12–15
mm diameter vials. Also suitable for test tubes and reaction vials.
Vial Holders
Vial holders provide a convenient and accessible way to store samples. They are clear poly-
styrene cases with hinged lids, with alpha-numeric indexing for positive sample identification.
The vial holder will hold 40 to 60 vials in individual partitions. Foam inserts are included.
Vial Racks For Autosampler, Headspace and EPA Vials
These plastic racks are available with either 36 or 50 positions. The 36 position rack holds 6,
10 or 20 mL headspace vials, while the 50 position racks accommodate either 50, 40 mL EPA
vials or 50, 1.8 mL vials. Polypropylene racks are autoclavable at 121°C for 20 minutes, while
the polyethylene rack cannot be autoclaved. Racks have an alpha-numeric indexed vial grid
for convenient sample identification and are stackable. Polypropylene racks have openings in
the well bottoms for drainage. The 36 position rack measures 35/8" x 123/4" x 11/8". The 50
position rack for EPA vials measures 63/4" x 13" x 11/4". The 50 position rack for 1.8 mL vials
measures 4" x 7 5/8" x 1 1/8".
Description Material Qty. Item No.
36 Position Rack for Headspace Vials Polypropylene 5/pk 868805
50 Position Rack for 1.8 mL Vials Polyethylene 5/pk 868850
50 Position Rack for EPA Vials Polypropylene 5/pk 868806
Description Qty. Item No.
Holder for 60 Vials up to 13 x 50 mm 1/pk 228778
6-Pack of Above Holder 6/pk 228779
Holder for 40 Vials up to 16 x 50 mm 1/pk 228780
6-Pack of Above Holder 6/pk 228781
Description Qty. Item No.
Foam Vial Holders Large-hole 5/pk 330850
868850
www.chromres.com 165
Vials
Accessories
6-Port Mini-Vap
This concentrator/evaporator handles up to six miniature vials or containers simultaneously. It
comes with six stainless steel needles, a nickel-plated needle valve, and 3 feet of plastic tub-
ing. The needle valve allows fine control of nitrogen or dry air flow for the evaporator.
Instructions included.
Description Item No.
6-Port Mini-Vap 201006
Vibrograver
The Burgess Vibrograver permanently engraves all hard and semi-hard surfaces.
Recommended for marking column tags and tools. Just write on the item to be engraved as with
a pencil. The etched information cannot be erased, wiped off, or rubbed out.
Description Item No.
Vibrograver, 120V 486211
Vibrograver, 220V 486212
Spare Diamond Tip 486213
Spare Carbide Tip 486214
Reaction Vials, 5 mL and 1 mL
Description Thread Size Qty. Item No.
0.1 mL reaction vials 8-425 12/pk 099400
0.3 mL reaction vials 13-425 12/pk 099410
1.0 mL reaction vials 13-425 12/pk 099420
3.0 mL reaction vials 20-400 12/pk 099430
5.0 mL reaction vials 20-400 12/pk 099440
10.0 mL reaction vials 24-400 12/pk 099450
Reaction Vials
These are useful for micro and semi-micro scale reactions or concentration work. The Vials
have thick walls, conical tapered interiors and come complete with PTFE-faced silicone liners
and open-hole screw caps. Vials have graduation marks (0.1 mL and 0.3 mL vials are not grad-
uated), and come 12 per package. Made from borosilicate glass.