IR 03037850/2014001 on 7/15/14, 08/18/14 and 8/25/14, CB&I ... · Overload Light: @ Adjusted 0 Not Adj. REMARKS: Does Instrument Meet Final Acceptance Criteria?: Calibration Sticker

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR

Owner: Gl

DATE: 11116/12

TECH: E.M. Glenn

2360 SERIAL# 278541

LOCATION: Griffin lnst

DATE LAST CAL EXPIRES: 11/16/12

Reason For Calibration: (!) Due For Calibration i 0 Repai~ (See Remarks)

0 Other (See Remarks) 0 Due and Repair (See Remarks)

NIST TRACEABLE EQUIPMENT USED DURING CALIBRATION

MODEL: M-500 SERIAL#: 114512 CAL. DUE: 09/26/13

~ Audio Response ~ Geotropism CABLE LENGTH: 39"

CONDITION: Sat

NEW BATIERIES:

HV (+/-10%) AS FOUND HV

500 V: 500

1000 V: 1000

1500 V: 1500

x.1 or x1

x1 or x10

x10 or x100

AF MECHANICAL ZERO:

0 Yes (!) No

AS LEFT HV

A. F.

A. F.

A.F.

0 AL MECHANICAL ZERO:

BA TIERY CHECK: Sat

WINDOW SETIINGS:

BT (3.5 mV +/- 1 mV):

BW (30 mV +1-3 mV):

AT (120 mV +/-10 mV) :

A. F.

3.5

31

120

A.L

A. F.

A. F.

A. F.

Is the As Found Data Within 20% of the Set Point?: (!) Yes 0 No

Overload Light: @ Adjusted 0 Not Adj.

REMARKS:

Does Instrument Meet Final Acceptance Criteria? :

Calibration Sticker Attached?:

Date Instrument Is Due For Next Calibration:

INSTRUMENT MARRIED WITH 43-93

(!) Yes

(!) Yes

11/16/13

#PR311203

0 No

0 No

0

Performed/Reviewed by: Date: 11/16/2012 Entered by: d~ Initials

Calillratoons penormed to ANSI N323A·1 997 standards.

~~ GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR 43-93 PROBE# PR311203

Owner: Gl

DATE:

TECH:

11/16/12

E.M. Glenn

LOCATION:

DATE LAST CAL EXPIRES:

Griffin lnst

11116/12

REASON FOR CALIBRATION:

(!) Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair

CABLE LENGTH: 39" INPUT SENSITIVITY: dual

NIST TRACEABLE EQUIPMENT AND STANDARDS USED DURING CALIBRATION

MODEL: 2360 SERIAL#: 278541 CAL DUE: 11/16/13

NIST TRACEABLE SOURCES USED

Source Number Isotope 4 pi Activity Assay Date 2 pi Activity

OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16.700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm

Efficiencies from last cal.:

Condition: (!) Sat 0 Unsat Pu: 22.49% Th: 20.99% Sr: 35.98%

Tc ss: 18.44% C14: Tc Ni :

As Found (AF) Efficiencies:

HV /Vernier. Tc-99 Source Response Pu-239 Source Background (CPM): iTc-99 Source Response Nickel (CPM): Response (CPM): Stainless Steel (CPM):

Ach. B ch. j Net Eft. Ach. B ch. I Net Eft. Ach. B ch. Ach. B ch. j Net Eft. 775/ NIA I 4220 : 462 22.80%1 2 263 ' 28 3315 17.64%

i

Net A to B B to A Xtalk: Xtalk: <10% <1%

4.5% <1%

Pu239 Tc99 Ni Tc99 ss Th-230 Sr90 ~

AFCPM: 4220 3315 3416 3367

AF 4 pi eft: 22.80% 17.64% 20.44% 34.52%

AF 2 pi eff: 45.02% 28.26% 41.79% 49.37%

Is as found efficiency within 20% of the efficiency from the last cal? (!) Yes 0 No (See Remarks)

Nore· llrhe as found ~ala rs Within 10% of the last callbratton and the B-A Xtalk is <1% and the A·E' Xtalk is <10%. then the technteian may NIA the plateau seclion and go dnectly to remarks.

GRIFFIN INSTRUMENTS

PROBE#: PR311203 Date: 11116/12

PLATEAU AND SET POINT DATA

I HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B I B to A X talk: J SS(CPM): Response (CPM): Xtalk: <10% <1%

Ach. I B ch. I Net Elf. A ch. l B ch.j Net Eff. Ach. J B ch.

N/A

Alpha /Beta Bkg (cpm) 2 263 HV I Vernier Pu-239 Tc-99 Nl Tc-99 SS Th-230 C-14 Sr-90

775 / N/A CPM: 4220 3315 3416 3367

4 pi AL Efficiencies: 22.80% 17.64% 20.44% 34.52%

2 piAL Efficiencies: 45.02% 28.26% 41.79% 49.37%

REMARKS:

Does Instrument Meet Final Acceptance Criteria?: (!) Yes 0 No

0 No Cal ibration Sticker Attached?: (!> Yes

Date Instrument is Due For Next Calibration: 11/16/13

INSTRUMENT MARRIED WITH 2360 #278541

Performed/Reviewed by: Date: 11 /16/2012 Entered by: cff1: Initials

2 pi efficiencies denolod In Italics. C•libratlons performed to ANSI N323A·1997 atandords.

2

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR 2360 SERIAL# 278554

Owner: Gt

DATE: 11/08/12 LOCATION: Griffin lnst

TECH: Joanne Glenn DATE LAST CAL EXPIRES: 11/29/12

Reason For Calibration :

MODEL: 500-2

~ Audio Response

(!) Due For Calibration

0 other (See Remarks)

0 Repair (See Remarks)

0 Due and Repair (See Remarks)


SERIAL#: 284951 CAL. DUE: 12/28/12

~ Geotropism CABLE LENGTH: 39"

CONDITION: Sat AF MECHANICAL ZERO: 0 AL MECHANICAL ZERO: 0

NEW BATTERIES: 0 -----------

HV [+/-10%) AS FOUND HV

500V: 500

1000 V: 1000

1500 V: 1500

Yes (!) No --- --

AS LEFTHV

A. F.

A. F.

A. F.

BATTERY CHECK: Sat

WINDOW SETTINGS:

BT (3.5 mV +/- 1 mV):

BW (30 mV +/-3 mV):

AT (120 mV +/-10 mV):

3.5

30

120

A. F.

A. F.

A. F.

SCALE RATE CPM AS FOUND o/o ERROR AS LEFT o/o ERROR AS FOUND % ERROR AS LEFT o/o ERROR

x.1 or x1 100 100 0.0% A. F.

250 250 0.0% A. F.

400 400 0.0% A. F.

x1 or 1000 1000 0.0% A. F. x10 2500 2500 0.0% A. F.

4000 4000 0.0% A. F.

x10 or 10K 10 K 0.0% AF. x100 25K 25 K 0.0% A. F.

40K 40 K 0.0% A. F.

x100 or 100K 100 K 0.0% A. F. x1000 250K 250 K 0.0% A. F.

-400K 400 K 0.0% A. F.


Overload Light: (!) Adjusted. 0 Not Adj .

REMARKS:





Performed/Reviewed by:

(!) Yes

(!) Yes

11/08/13

# PR270010

Date: 11/8/2012

0 No

0 No

Entered by:Linitials

Calibrations performed to ANSI N323A·1997 standards.

GRIFFIN INSTRUMENTS


Owner: Gl --------------- ------------ --- -- -- - ---------DATE: LOCATION:

TECH:

11/08/12

Joanne Glenn DATE LAST CAL EXPIRES:

Griffin lnst

11/29/12

REASON FOR CALl BRA TION:

@ Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair



MODEL: 2360 SERIAL#: 278554 CAL. DUE: 11/08113 --·----- ------------------- -- - - --- ----



OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16,700 dpm 06/15/09 8,170 cpm

2696-00 Pu239 18,500 dpm 06/15/09 9,370 cpm

2697-00 Sr90 12,200 dpm 06/15/09 8,530 cpm

--------- ----- ---- --Efficiencies from last cal.:

Condition: (!) Sat 0 Unsat Pu: L __ 22. 5~% Th=l~ ~ Sr: [ --:?"3.!ml.]

Tcss: J ~~~ C14: [ ____ - J TcNif·-- __ i As Found (AF) Efficiencies:

:-·-H_V_/ _V_er-ni-e-r: ...,.,..fr -(C-99 Source Response I Pu-239 Source -l~BaokQ<O""d (CPM)o r .c-99 Source Response I j JJ _ Nickel (CPM): Response (CPM): Stainless Steel (CPM):

- A ch. IJ8ctt-:- I Net Eff.l A ch. T B ch.j Net Eff. A ch. ~h. A ch. J j B ch . I Net Eff. j

lr-_-_~_77~5-=-1-N_/_A_-:.__-:-__ ,I __ _.I_ -- 4004 _j_ 495 j21 .59~ =---~-- L 262 - , 16''1 3116 Tt6. 50°/~

~et A to B B to A Xtalk: -

talk: <1 Oo/o <1 o/0 '

- 5-:-s%-----'r---- <1% .J ( ______ - ------- J

Tc99 ss Th-230

AFCPM: r-·3410 ! _____ I

AF 4 pi eff: r·-35:-o1%- 1

AF 2 pi eff: [_~C!:~~~~ I ---J L ___ _

Is as found efficiency within 20% of the efficiency from the last cal? ~ Yes 0 No (See Remarks)

Note: tithe as found data is withon 10'" of the last calibration and the B-A Xtait< Is <1'.1. and the A·B Xtalk is <10'A. then the tachnicoan may NIA the plateau section and go directly to remarl<s.

-

GRIFFIN INSTRUMENTS

PROBE #: PR27001 0 Date: 11/08112


HV I Vernier: Tc-99 Source Response SS (CPM):

Ach. B ch. Net Eff.

650 4 176 0.9%

700 10 1172 6.4%

750 20 2165 11 .7%

775 28 2915 15.3%

800 58 3325 17.6%

Alpha I Beta Bkg (cpm) 9 HV I Vernier Pu-239

7751 N/A CPM: 3939

4 piAL Efficiencies: 21.24%


Pu-239 Source Background (CPM): Net A to B Response (CPM):

Ach. B ch . l Net Eff.

629 580

2584 353

3608 344

3939 557

4090 578

275

l£:ll1:fi

3.4%

13.9%

19.5%

21 .2%

22.1%

Tc-99 ss

2915

15.26%

24.44%

Xtalk: < 10%

Ach. B ch .

2 6

7

9

10

Th-230

3230

19.29%

39.42%

27 46.8%

71 9.8%

149 5.1%

275 6.7%

275 6.9%

---- ---

B to A Xtalk: <1 o/o

2.27%

<1%

<1%

<1%

1.74%

Sr-90

3378

34.51%

49.35%

I

'·

..... Desogner and Manufacturer

Scient ifoc or~~ fndustriol lns:rvments CERTIFICATE OF CALIBRATION

Not used until 11/28/11

__ ....,.;...,_,..'-'-'-'""""""""""""c.c.e."-'-'-'"-"-'""-'---- Model 2

__ _,L,u,d,'"'lu"'m-'-'-'M""e""o,_s.,u"'re~m~e""n""ts..._,"'-l n""c.,.._· __ Model 43-93

~&LlUDLUM MEASUREMENTS, INC. POST OFFICE BOX 8 10 PH. 325-235-5494

501 OAK STREET FAX NO. 325-235-4672

SWEETWATER. TEXAS 79556. U.S.A.

ORDER NO. 20186632

Serial No. _ n_xs-_k_,Z-:::._ _____ _

Serial No. ff<....._3.__,1LL'IJ.I....._.~--_____ _

Col. Dote -------'--"-'-.=..;'-'-'----- Col Due Do te _____ 1,_,6""·N~o.:..v-'-'-l _.,2 ___ Col. Interval 1 Year Meterfoce __ _,2,_,0._.2'"'·8...,5._,5,___

:r.eck mark applies to applicable instr. and/or de tector lAW mfg. spec. T. ___ 7_L °F RH 29 % Alt ___ 702JL mm Hg

fJ' New Instrument Instrument Received 0 Within Toler. +-10% 0 10-20% O Out of Tal. O Requiring Repair 0 Other-See comments

Rf Mechanical cl:: . R:f Meter Zeroed O Bac kground Subtract 0 Input Sens. Linearity 0 F/S Resp. ck 0 Rese l ck. ~ Window Operation ~ Geotropism Rf Audio ck. Rf Alarm Setting ck. Rf Batt. c k. (Min . Volt). _ __.,2'-".2~VDC @/ RS-232 Port OK

:0'Colibrafed in ac cordance wit11 LMI SOP 14.8 rev 12/05/89. 0 Calibrated in accordance will1 LMI SOP 14.9 rev 02/07/97.

nslrument Volt Set __ 6J.L V

GZi HV Readout (2 points) Ref./lnst. _ _,5,00.,__ / _Jj Z.., __ v Ref./lnst. _ l.S.QQ___ 1 !tl'i 1 v

Firmware Version : 39010N Alpha Threshold: 120mv Beta Threshold: 3.5mv Beta Window: 30mv Overload set with Am241 , 91 mdpm

Instrument calibrated with a

High voltage set with detector

39" cable . connected.

COMMENTS:

(EEPROM Settings)

User Time: .....!..! ~.0:.._ ____ _

Alpha Alarm: 999999 Bela Alarm: 999999 A/B Alarm: 999999

Model2360 Dote: __Jf---'-'..fq_/_Ul'-'-1'-l ____ _

Calibration Dote Due: J_Jbtl.

G; 'bra!Jon· GM detectors pos1toooed perpenditula; to source except for M 44-9 '"which the front of probe f<r.es source

RANGE/MULTIPLIER _x1.QQQ__

xlOOO

_A]__O'-----xl

REFERENCE CAL. POINT

__ ___AOQk.c .........,'--------lOOkcpm 40kcpm

____ 4J~c_pOLL.L_ _____ _

_______ 1~k~cp~m~---------

----~~QOcR~----------lOOcpm

•uncerto.nty W1lh1n ~ 10% C .F. within± 20%

REFERENCE INSTRUMENT CAL. POINT RECEIVED

INSTRUMENT METER READING'

Digital Readout __ 4_QQk.c_p.m... ~~~

_J_.,~_(oJ f./00 ((?}

Ol<CR.C!L __ _::4Lbk:<;.R!IL _____AQQ._c.Qill_

---~QIIL --"'-'<L.W

'{ (t!)_

INSTRUMENT REC'D "AS FOUND READING"

INSTRUMENT METER READING*

Log Sc ale

REFERENCE CAL. POINT

A Range(s) Calibrated Electronically

INSTRUMENT INSTRUMENT RECEIVED METER READING•

Lvdlvm Measure ents I<'IC cerllloes 1n01 I he cove rnsl!vrnenl nos been co,bfo ted by standards traceable to the Notoonoi lnslitule of Standards a. d Jechnotogy or to the coo Oflan 1oo t1hes of omor tnternotoonol Slonooros Orgomatoon memoers. or nove been derived frorn occcoted ,·elves of noMoi pl'ly~COI co•Siontl or hove oeen aeuved oy •ne ro11o 1ype of co'o ot on I llntoues I he col•broloon systemcontorms to tne reqvirements of ANSI/NCSL Z.S·t0-1 ·199• ond ANSI N323-1978 State ol Texos Calibration license No . L0-1963

Reference Instruments and/or Sources: 0 73410 11 31 0 781 0 059 0 280 0 60646 0 70897 0 P.o-226 S/N Y982

Cs-1 37 Gamma S/N 0 11 62 0 G 11 2 0 M565

.o.lpho S/N ___ __,_P_,u,_.,2~3.t..9 _,#c.::!4><3:.c37'-----

0 5105 0 1008 0 1879 0 E552 0 E551 0 720 0 734 0 1616 0 Neutron Am-241 Be~/ 1-304

LoY' ~ Beta S/N ___ Tc 9 :1635/83.~¥.90 'f.J 0 Other

' 500 S/N ___ ..,381 20 0 Osc illoscope S/N. _________ _ Gf Mullime ter S/N 84260 131

Calibrated By: __ _ __ _.k.eJj::..!~'-L~· .rt_ta.~,-- -----· Dote - #..:h.V_,.c::'..LL( -----------

Reviewed By: flt_~ ~--- Dote j J{;rnJ_f_( ____ _ I

AC Ins o· Passed Oielec nc ('·it-Pot} ono Cont•nu•ty es

Only n Foiled· -----

fus c rtJII.co· s c no· e teoroctvc:eo except n tvtl wJthOtJl tne .vt Hen oor~a. o~ lu t.:m MeO!.u>crnents:. l"lc rf)o,_. rn· tOO·•nolt ~ .. , .. ~ 1 , , 2.

GRIFFIN INSTRUMENTS


Owner: Gl

DATE: LOCATION: Griffin lnst

TECH:

11/28/11

E.M. Glenn DATE LAST CAL EXPIRES:


Due For Calibration Repair (See Remarks) • Other (See Remarks) Due and Repair






OOTC470-0654 Tc99 ss 17.300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16.700 dpm 06/16/09 8.170 cpm

2696-00 Pu239 18,500 dpm 12/02109 9,370 cpm

2697-00 Sr90 12.200 dpm 03/01/00 8.530 cpm


Condition: • Sat Unsat Pu: Th: Sr:

Tc ss: C14: Tc Ni:


HV /Vernier: Tc-99 Source Response Nickel (CPM):

Pu-239 Source Response (CPM):

Background (CPM): lrc-99 Source Response Stainless Steel (CPM):

A ch. B ch. jNet EtC A ch. B ch. j Net Eff. A ch . B ch. I A ch . . , B ch . !Net Eff.

r . 1

Net A to B B to A X talk: Xtalk: <10% <1%

AFCPM:

AF 4 pi eft:

AF 2 pi eff:

Is as found efficiency within 20% of the efficiency from the last cal? Yes • No (See Remarks)

Note If the as rouno data is Within tO% of the last calibration and me B-A Xtalk 1s <1% and the A·B Xtatk IS <10%. then the techn:c.an may NIA the plateau sect1on and go dtrectly 10 remarks

GRIFFIN INSTRUMENTS

PROBE#: PR311154 Date: 11128111


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B 8 toAXtalk:

I SS (CPM): Response (CPM): Xtalk: <10% <1%

A ch. 8 ch. Net Eff. Ach. B ch. 1 Net Eff. A ch . l B ch .

700 7 2186 12.0% 3814 280 20.6% 2 108 4.3% <1%

725 6 2719 14.7% 4128 309 22.3% 0 170 3.3% <1%

750 7 3100 16.6% 4214 387 22.8% 0 228 3.6% <1%

775 8 3420 18.6% 4363 458 23.6% 0 207 5.4% <1%

800 11 3618 19.5% 4211 559 22.7% 3 249 6.9% <1%

825 11 3652 19.5% 4368 819 23.6% 3 272 11 .1% <1%

Alpha I Beta Bkg (cpm} 0 225 HV /Vernier Pu-239 Tc-99 Ni Tc-99 55 Th-230 C-14 Sr-90

7751 N/A CPM: 4213 3527 3627 3513

4 piAL Efficiencies: 22.77% 19.09% 21.72% 35.69% 2 piAL Efficiencies: 44.96% 30.57% 44.39% 51.05%

REMARKS: New instrument. Cal due 11/16112 to match the box.

Does Instrument Meet Final Acceptance Criteria?: • Yes No

Calibration Sticker Attached?: Yes No



Performed/Reviewed by: Date: 11/28/2011 Entered by: cfC: Initials

2 pi afficioncles denoted in italics. Calibrations performed to ANSI N323A·1997 standards.

2

GRIFFIN INSTRUMENTS


Owner: Gl

DATE: 11/16/12

TECH: E.M. Glenn

2360 SERIAL# 278562



Reason For Calibration: (!) Due For Calibration

0 Other (See Remarks)




MODEL: M-500 SERIAL#: 114512 CAL DUE: 09126/13


CONDITION: Sat

NEW BATTERIES:

HV (+/-10%) AS FOUND HV

500 V: 500

1000 V: 1000

1500 V: 1500

x1 or x10

AF MECHANICAL ZERO:

0 Yes (!) No

AS LEFTHV

A. F.

A. F.

A. F.


BATTERY CHECK: Sat

WINDOW SETTINGS: A. F. A.L.

BT (3.5 mV +/- 1 mV): 3.5 A. F.

BW (30 mV +/-3 mV): 30 A. F.

AT (120 mV +/-10 mV): 120 A.F.


Overload Light: (!) Adjusted 0 Not Adj.

REMARKS:



Date Instrument is Due For Next Calibration:


(!) Yes

(!) Yes

11/16/13

#PR311154

0 No

0 No

0

Performed/Reviewed by: Date: 11/16/2012 Entered by: c{l;::: Initials

Calibrations pertormed to ANSI N323A·1997 standards.

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR PROBE# PR311154

Owner: Gl

DATE:

TECH:

11/16/12

E.M. Glenn

LOCATION:

DATE LAST CAL EXPIRES: I

Gri ffin Ins!

11/16/12


C!> Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair



MODEL: 2360 SERIAL#: 278562 CAL. DUE: 11/16/13



OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94THI70-1593 Th230 16.700 dpm 06/16/09 8,170 cpm

2596-00 Pu239 18.500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03101100 8,530 cpm


Condition: G!) Sat 0 Unsat Pu: 22.77% Th: 21.72% Sr: 35.69%

Tc ss: 19.09% C14: TcNi:


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): ITc-99 Source Response Nickel (CPM): Response (CPM). I Stainless Steel (CPM):

j Net Eff. B ch. j Net Eff. I

Ach. B ch. Ach. Ach . 8 ch. A ch. 8 ch. I Net Eff. 7751 N/A I 3753 1 428 ·;w.29%1 0 229 24 1 3191 17.12%

Net A to B B loA Xtalk: Xtalk: <10% <1%

5.0% <.1%

Pu239 Tc99 Ni Tc99 ss lh-230 Sr90 C-14

AFCPM: 3753 3191 3255 3364

AF 4 pi eff: 20.29% 17.12% 19.49% 34.86%

AF 2 pieff: 40.05% 27.43% 39.84% 49.86%

Is as found efficiency within 20% of the efficiency from the last cal? G!) Yes 0 No (See Remarks)

Note: If the as found data is with1n 10% of the lasl cal ibration and the B-A Xtalk 1s <1% and ~he 1\·8 Xtalit ts <10%. then the technician may NJA the plateau secbon and go dnectty to remarks_

GRIFFIN INSTRUMENTS

PROBE#: PR311154 Date: 11/16/12


HV /Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B B toAXtalk:

J SS (CPM). Response (CPfv1): 1Xtalk: <10% <1%

Ach. B ch. Net Eff. Ach. B ch. 1 Net Eff. Ach. B ch.

750 10 2891 15.7% 3840 344 20.8% 0 178 4.1% <1%

775 8 3400 18.4% 3928 449 21.2% 0 220 5.5% <1%

BOO 12 3617 19.5% 4132 655 22.3% 0 238 9.4% <1%

Alpha I Beta Bkg (cpm) 222 HV I Vernier Pu-239 Tc-99 Ni Tc-99 55 Th-230 C-14 Sr-90

7751 N/A CPM: 3948 3371 3079 3335



REMARKS:

Does Instrument Meet Final Acceptance Criteria?: (!) Yes

(!) Yes

0 No

0 No Calibration Sticker Attached?:



Performed/Reviewed by: Date: 11/16/2012 Entered by: cf'C: Initials

2 pi efficlenclos donotod in il21ica. Calibrations performed to ANSI N323A·1997 stlndards .

2

Safety and Ecology Corpr.ration 2800 Solway Road

Knoxville, TN 37931

Calibration Certificate

SEC PROCEDURE

Calibration Certificate for LV-1,Seria/ # 003573, Bar Code# ,Propehy # SEC-6839

Date: 05/09/13 Date Last Cal. Expires: 11/19/13 I Technician : Jeffrey Knight

I

SEC-IS-409 Rev 3

Location: 9999, Reason For Calibration: Due for Calibration I I

EQUIPMENT USED DURING CALIBRA,lTION I

MODEL: D-812 V.2 SERIAL#: 3531 CAL. DUE: 11/20113

MODEL: SERIAL#: CAL DUE:

AS FOUND DATA AF Physical Condition SAT AS LEFT DATA

As Found Calibrator Flow Indication: 64 LPM

A~ Left Instrument Flow Indication:

Ak Left Calibrator Flow Indication: I 0 CFM

As Found Instrument Flow Indication: 64 LPM

Unit of Measure: (!' LPM

Reproducibility 60 LPM 60 LPM 60 LPM Average:

CALIBRATION DATA TARGET VALUE

30.00 LPM

50.00 LPM

70.00 LPM

~ Are the Individual Counts Withini 10% of the Average?

AIR SAMPLER READING 1 ALIBRATOR READING

30.00 LPM

50.00 LPM

70 .00 LPM

I 3o.oo !

50.60

70.10

LPM

LPM

LPM

60 LPM

60 LPM

60.00 LPM

ERROR%

0.00% LPM

1.20% LPM

0.14% LPM

Air Sampler Setting 60.00 ~ Is Error Within 10%?

Reproducibility 60 LPM 60 LPM I 60 LPM Average:

~ Are the Individual Counts i ithin 10% of the Average?

0 Use Manufacturers Indication @ Use Corrected Marking 0 NIA

Model . Bar Code #:

60.00 LPM

Air Sampler rotameter reading:

Comments: Married as a set with:

~ Does Instrument Meet Final Acceptance Criteria? I ate Instrument is Due For Next Calibration: I

Reviewed by: z:?:?~

~ Calibration Sticker Attached?

05/09/14

Date: yf,..,.l] Printed Name:

5/912013 Page 1 of 1

GRIFFIN INSTRUMENTS

CALl BRA TION CERTIFICATE FOR Owner: DENUKE

2929 SERIAL# 171583 06-00148

DATE: 09/08111 LOCATION: Griffin lnst·

TECH: E.M. Glenn DATE LAST CAL EXPIRES: 10/22/10

Reason For Cal ibration : • • Due For Calibration' Repair (See Remarks)

CABLE LENGTH: 39" Other (See Remarks) Due and Repair (See Remarks)




Condition: • • Sat Unsat M Mechanical Zero: 0

AL Mechanical Zero: 0

Seeler Function Check AsFou.nd As Lett

Beta Channel Window (~-50 mV): ~-~7 AF.

Alpha Channel Window (175 mV. 120 for 3030): 170 A. F.

Alpha Counts w/Pulser@ 10.000 CPM: 9.992 A. F. 'Y. Error: 0.1%

Beta Counts w/Pulser@ 1 0.000 CPM: 9.992 A.F. 'Y. Error: 0.1 'Y.

HIGH-VOLTAGE POWER SUPLY CAL (2929 only)

1 KV Reading (R-5 on HV Board): A. F.

-Mex HV (1500 V +): •• • Sat Unsat

REMARKS:

Does Instrument Meet Final Acceptance Criteria?: • • Yes

-Calibration Sticker Attached?: , . Yes No


INSTRUMENT MARRIED WITH 43-10-1 # PR119312

Performed/Reviewed by: Date: 9/8/2011 Entered by: cf'.C-. Initials

Calib(a!Jons performed to ANSI NJZJA-1997 standards.

GRIFFIN INSTRUMENTS

PROBE#: PR179312 Date: 09/08/11


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B B toAXtalk: j SS (CPM): Response (CPM): Xtalk: <10% <1%

A ch. I B ch . Net Eff. Ach. B ch. I Net Eff. Ach. B ch .

800/3.27 1 3596 20.6% 7139 178 38.6% 0 38 1.9% <1%

850/3.48 1 4361 25.0% 7174 210 38.8% 0 43 2.3% <1%

900/3.68 0 4526 25.8% 7425 432 40.1% 0 54 4.8% <1%

950/3.91 1 103

Alpha I Beta Bkg (cpm) 63 HV I Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

875/3.56 CPM: 7269 4351 5977 6131 3962

4 pi AL Efficiencies: 39.29% 24.79% 35.78% 12.44% 42.16%


REMARKS:

Does Instrument Meet Final Acceptance Criteria? : '.! ' Yes • • No

Calibration Sticker Attached?: ! l Yes No



Performed/Reviewed by: Date: 9/8/2011 Entered by: C'f'C. Initials

2 pi efficiencies denoted in italics. Calibrations performed to ANSI N323A·1997 standards.

2

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR 43-10-1 PROBE# PR179312

Owner: DENUKE

DATE:

TECH:

09/08/11

E.M. Glenn

LOCATION:



Griffin lnst

10122/10

•:!1 Due For Calibration ,~' Repair (See Remarks) •:::> Other (See Remarks)

I I

( Due and Repair

CABLE LENGTH: 39• INPUT SENSITJVITY: dual




Source Number Isotope

OOTC470-0654 Tc99 SS

2697-00 Sr90

PX 726 C14

2696-00 Pu239

94 TH4 70-1593 Th230

. Condition: .. Sat Unsat


4 pi Activity

17,300 dpm

12,200 dpm

48,780 dpm

18,500 dpm

16,700 dpm

Pu: I

Assay Date 2 pi Activity

06/15/09 10,800 cpm

03/01/00 8,530 cpm

01/21/08 18,660 cpm

12/02/09 9,370 cpm

06/16/09 8,170 cpm


38.34%1 Th: j

23.36%1 C14:1

36.91% Sr: l 42.41%1

10.10%! Tc Ni:''-----'

HV I Vernier. ,Tc-99 Source Response 11 Background {CPM): Tc-99 Source Response 1 I Nickel (CPM): Stainless Steel (CPM): 1

I A ch. I! B ch. j,_N_et_E_ff-'.j'--:::-:-=-::--.-:::-::-:--'-:-::-::-::::-:c::t--::----i---::c::---r--c:--'-I--B .... c=-h-. + N-::-e-::-t E,ff,-:..~.1 875 I 3.56 - i I ' I 26.08%1

I Net A to B : B to A X talk: Xtalk: <10% <1%

3.0% <1%

Pu239 Tc99 Nl Tc99 ss Th-230 Sr90 C-14

AFCPM: 7176 4571 3761 6242 1 AF 4 pi eff: ' 38.79% ~08% I 40.03% 12.68%

-AF 2pi eff: 76.58% I I 41.78% 73.46% 57.25% 33.14%

Is as found efficiency within 20% of the efficiency from the last cal? ! ' Yes No (See Remarks)

Note: If lhe as lound data is w11hin HI% of lhe las! cahbrat1on and lhe B-A Xtalk 1s <1% and the A-B Xtalk IS <10%. then the techr1ie1an may NJA the plateau section and go d"ectly to remarl<s.

GRIFFIN INSTRUMENTS

\LIBRATION CERTIFICATE FOR Owner: DENUKE

2929 SERIAL# 171583 06-00148


TECH: E.M. Glenn DATE LAST CAL EXPIRES: 09108112

Reason For Calibration: (!) Due For Calibration 0 Repair (See Remarks)

CABLE LENGTH: 39" 0 Other (See Remarks) 0 Due and Repair (See Remarks) - -




Condition: (!) Sat 0 Unsat AF Mechanical Zero: 0


Scaler. function Check

Beta Channel Window (4-50 mV):

Alpha Channel Window (175 mV, 120 for 3030):

Alpha Counts w/Putser@ 10,000 CPM:

·eta Counts w/Pulser@ 10,000 CPM:

As Found As Left

4-48 A. F.

175 A. F.

9,994 A.F.

9.994 A.F.

HIGH VQLTAGEPOWER SUPLV CAL (2929 only)

1 KV Reading (R-5 on HV Board): A.F.

(!) Sat 0 Unsat Max HV (1500 V .-):

REMARKS:

Does Instrument Meet Final Acceptance Criteria?:



INSTRUMENT MARRIED WITH 43-10-1


(!) Yes

(!) Yes

08/03/13

0 No

0 No

#PR179312

Date: 8/312012

%Error: 0.1%

%Error: 0.1%

Entered by: cf'a' Initials

Cahnra110ns performed lo ANSI N323A-1997 slandards

GRIFFIN INSTRUMENTS

PROBE#: PR179312 Date: 08/03/12


I HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B l B to A Xtalk: SS (CPM): Respons~ (CPM):

Ach. B ch. Net Eff. Ach. B ch. I Net Eff. Ach.

N/A

Alpha I Beta Bkg (cpm) 59 HV /Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230

875/3.56 CPM: 7177 4383 5732

4 pi AL Efficiencies: 38.79% 24.99% 34.32%

2 piAL Efficiencies: 76.58% 40.04% 70.15%

REMARKS:


@ Yes

0 No



INSTRUMENT MARRIED WITH 2929 # 171583

Performed/Reviewed by: Date: 8/3/2012

Xtalk: <10% <1%

B ch.

C-14 Sr-90

6428 3682

13.06% 40.05%

34.13% 57.28%

Entered by: cf(!:! Initials

I

2 pi efficiencioa denoted tn Italics . Calibrations performed to ANSI N323A-1997 standards.

2

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

08/03/12

E.M. Glenn

LOCATION:


Griffin lnsl

09/08/12


C!J Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair






OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10.800 cpm

94TH470-1593 Th230 16.700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm PX726 C14 48,780 dpm 01/21/08 18,660 cpm


Condition: @ Sat 0 Unsat Pu: 39.29% Th: 35.78% Sr: 42.16%

Tc ss: 24.79% C14: 12.44% Tc Ni:


HV /Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): ITc-99 Source Response Nickel (CPM): Response (CPM): Stainless Steel (CPM):

Ach. B ch. !Net Eft. Ach . B ch. I Net Eft. Ach. Bch. A ch. B ch. I Net Eft. 875/3.56 I 7177

r 38.79%1 o 1 4383 24.99% 299 59


3.2% <1%

Pu239 Tc99 Ni Tc99 ss Th-230 Sr90 ..£:!!

AFCPM: 7177 4383 5732 3682 6428

AF 4 pi eft: 38.79% 24.99% 34.32% 40.05% 13.06%

AF 2 pi eff: 76.58% 40.04% 70.15% 57.28% 34.13%


Note. lithe as found data rs W>th•n 10% of the last calibration and the B·A Xtallc rs <1% and the A·B Xtalk is <10%, 1hen lhe tcchnicl<ln may N/A lhe plateau section and go d irec~y to remarks

·---GRIFFIN INSTRUMENTS


Owner: Gl

DATE: 11/08/12

TECH: Joanne Glenn

2360 SERIAL#

LOCATION:


278589

Griffin Ins!

11/29/12


0 Other ~ee Remarks) 0 Due and Repair (See Remarks)


MODEL: 500-2 SERIAL#: 284951 CAL. DUE: 12/28/12


CONDITION: Sat AF MECHANICAL ZERO: 0 AL MECHANICAL ZERO:

NEW BATIERIES: 0 Yes (!) No BATIERY CHECK: Sat

HV 1+/-10%) AS FOUND HV AS LEFTHV

500 V: 500 A. F.

1000 V: 1000 A. F.

1500 V: 1500 A. F.

WINDOW SETIINGS:

BT (3.5 mV +/- 1 mV):

BW (30 mV +/-3 mV):

AT (120 mV +/-10 mV):

A. F.

3.5

30

120

A.L.

AF

A. F.

A. F.

0

~ RATECPM AS FOUND % ERROR AS LEFT % ERROR AS FOUND % ERROR AS LEFT % ERROR

x.1 or x1 100 100 0.0% A. F.

250 250 0.0% A. F. 400 400 0.0% A. F.

x1 or 1000 1000 0.0% A. F. x10 2500 2500 0.0% A. F.

4000 4000 0.0% A. F.

x10 or 10K 10 K 0.0% A. F. x100 25K 25 K 0.0% A. F.

40K 40 K 0.0% A. F. -x100 or 100K 100 K 0.0% A. F. ·-x1DOO 250K 250 K 0.0% A. F.

40DK 400 K 0.0% A. F.

Overload Light:

Is the As Found Data Within 20% of the Set Point?:

(!) Adjustedd - Not Adj.

REMARKS:






(!) Yes

@ Yes

11/08/13

# PR200119

Date: 11/8/2012

(!) Yes

0 No

0 No

0 No

Entered by: q? Initials

Calibratoons performed to ANSI N323A-1997 standards.

GRIFFIN INSTRUMENTS


Owner: Gl

DATE:

TECH:

11/08/12

Joanne Glenn

LOCATION:



Griffin lnst

11/29/12

<!> Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair

CABLE LENGTH: 39" INPUT SENSITIVITY: dual -----------·


MODEL: 2360 SERIAL#: 278589

----·---NIST TRACEABLE SOURCES USED

Source Number Isotope 4 pi Activity

OOTC470-0654 Tc99 SS 17.300 dpm

94TH470-1593 Th230 16,700 dpm

2696-00 Pu239 18,500dpm

2697-00 Sr90 12,200 dpm

CAL. DUE:

Assay Date

06115/09

06116/09

12/02/09

03/01/00

11/08/13

2 pi A.ctlvlty

10,800 cpm

8,170 cpm

9,370 cpm

8,530 cpm


Condition: (!) Sat 0 Unsat Pu: ~ 21_:_?.:% Th: ' - 19.87•io] Sr: [ 30.25%

Tc ss:L - 12.61o;~ C14: l _ __] Tc Nl:[__ J


~ HV I Vernier: 7

c-99 Source Response lj--Pu-239 s;urce - I Background (CPM): T;-99 Source Response 1 ' Nickel (CPM): jl Response (CPM): Stainless Steel (CPM): j _ ~-=- Ach. -B9~ _1~t_Ef!:1 A_~· l§ chj ~et-~!.!J ·Ach.

1

. Be~. IAch.J B _ch . - i~!_!Eff.( L 8oo _~ ____ L _____ L _ 3985_ [ 543 121.53%[_ __ ~ ~ _1 _ __2l_ [ 2435_ 13.04%

Net A to B B to A XtaJk:l Xtalk: <10% <1%

c 8.4% --~ ::% J

AFCPM:

AF 4 pi eff:

AF 2 pleff:

Is as found efficiency within 20% of the efficiency from the last cal?

[ __ ! r==-:J [ --~ ····-- __ ______j

(!) Yes 0 No (See Remarks)

Note. If the as found data is within 10% of the laJI calibration and the B·AXIalk is <1% and tho A·B Xtalk is <10'4. then the technician may NIA the plateau section and go directly 10 rematks.

GRIFFIN INSTRUMENTS

PROBE#: PR200119 Date: 11/08112


I HV I Vernier: Tc-99 Source Response SS (CPM}:

A ch. 1 8 ch. I Net Eft.

N/A

Alpha I Beta Bkg (cpm) 2

HV I Vernier Pu-239

800/ N/A CPM: 3985


2 pi AL Efficiencies: 42.51%

REMARKS:

Pu-239 Source Background (CPM}: Response (CPM}:

A ch. I B ch . l Net Eft. A ch. I B ch.

179 Tc-99 Ni Tc-99 SS Th-230

3111 2435

13.04%

20.89%

18.62%

38.05%

Net A to 8 I 8 to A Xtalk: I Xtalk: <10% <1%

Sr-90

2797

29.11%

41.64%


(!) Yes

0 No




Performed/Reviewed by: Date: 11/8/2012 Entered by:~lnitials 2 pi efficiencies denoted In Italics. CalibraUons performed to ANSI N323A·1997 standards.

2

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR Owner: DENUKE

2929 SERIAL# 171592


TECH: E.M. Glenn DATE LAST CAL EXPIRES: 03/26/11 I


CABLE LENGTH: 39" 0 Other (See Remarks) 0 Due and Repair (See Remarks)






Scaler Function Che<:k As Found As Left

Beta Channel Window (4-50 mV): 4-48 A. F.

Alpha Channel Window (175 mV, 120 for 3030): 170 A. F.

Alpha Counts w/Pulser@ 10,000 CPM: 9,971 A. F.

Beta Counts w/Pulser@ 10,000 CPM: 9,972 A. F.

HIGH VOLTAGE POWER SUPL Y CAL. (2929 only)

1 KV Reading (R-5 on HV Board): A. F.

(!) Sat 0 Unsat Max HV (1500 V +):

REMARKS:






(!) Yes

(!) Yes

01/09/13

0 No

0 No

# PR175878

Date: 1/9/2012

'Yo Error: 0.3%

%Error: 0.3%

Entered by:~lnltlals

CalibrattOnS performed to ANSI N323A-1997 standards.

GRIFFIN INSTRUMENTS

CALl BRA TION CERTIFICATE FOR 43-10-1 PROBE# PR175878

Owner: DENUKE

DATE: LOCATION:

TECH:

01/09/12


Griffin lnst

03/26/11

I REASON FOR CALIBRATION:

@ I Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair






OOTC4 70-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH4 70-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm

PX 726 C14 48,780 dpm 01/21/08 18,660 cpm


Condition: Sat 0 Unsat Pu: I

Tc ss:

~.82°/~ .- -,

Th: 34.77% Sr: 41.64%1

20.46%j C14: [ ___ 6.03%; Tc Ni: L __ _


-HV I Vernier: rc-99 Source Response j' Pu-239 Source Background (CPM): Tc-99 Source Response I

Stainless Steel (CPM): 1

Nickel (CPM): 1

Response (CPM): ,

A ch. B ch. Net Eff. A ch. 6 ch. j Net Eff . . : A ch. .

975 I 3.96 I 1 6832 203 j36~93%f 0 -l Net A to B B to A Xtalk: Xtalk: <10% <1% ~·---- 1 2.3% <1%

Pu239 Tc99 Ni Tc99 ss Th-230

AF CPM: I 6632 - 1- 3560 5619 ----I

36.93% 20.33% - 33.65%- I

6 ch .

43

Sr90

3913

42.18%

.. -~ - fl A ch. . B ch. Net Eff.

o_ _ f 3560 20.~0/o~

C-14

3333

6.74% AF 4 pi eff: ~- -

AF 2 pi eff: 72.91% ' _E:_S~ l 68.78% iio-:33%' 17.63% J --

Is as found efficiency within 20% of the efficiency from the last cal? @ Yes 0 No (See Remarks)

Note: If the as found data Is within 10% of the last calibration and the B·A Xtalk is <1% and lhe A-B Xtalk is <10'.0, then the technician may NIA the plateau section and go directly to ramarl<s.

GRIFFIN INSTRUMENTS

PROBE#: PR175878

Date: 01/09/12


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B B to A Xtalk: SS (CPM}: Response (CPM): Xtalk: <10% <1%

Ach. B ch . Net Eff. Ach. B ch . 1 Net Eff. Ach. I B ch .

N/A

Alpha I Beta Bkg (cpm) 0 43 HV lVernier Pu-239 Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

975/3.96 CPM: 6832 3560 5619 3333 3913

4 piAL Efficiencies: 36.93% 20.33% 33.65% 6.74% 42.18% 2 piAL Efficiencies: 72.91% 32.56% 68.78% 17.63% 60.33%

REMARKS:

Does Instrument Meet Final Acceptance Criteria?: @ Yes

@ Yes

0 No




Performed/Reviewed by: Date: 1 /9/2012 Entered by :~lnitials 2 pi efficiencies denoled in italics . Calibrations performed to ANSI N323A·1997 standards.

2

I

GRIFFIN INSTRUMENTS


....

DATE: 11/08/12

TECH: E.M. Glenn

Reason For Calibration:

LV-1 SERIAL# 003598 09-00345

GENERAL INf'ORMATION

LOCATION: Griffin Ins!

DATE LAST CAL EXPIRES: 08119/10

0 Repair (See Remarks) (!) Due For Calibration

____ 0 Other (See Remark~~ __ ...:0=--Due and Repair (See Remarks)


MODEL: C-828 SERIAL#: 1768

MODEL: SERIAL#:

~: - ~se&,r19.N 2: -~~--: Physical Condition: (!) Sat 0 Unsat

Air Sampler Set At Midpoint Flow: (!) Yes 0 No

Is the Actual Reading w/in 20% of the Indicated Volume on the Air Sampler?:

3 Collections - (Minutes or Flow):: 40 40

Are the Individual Collections w/in 10% of the Average?:

r:· SECTiqN~ S: TARGET VALUE

Is Error Within 10% ?:

Warm Up Delay:

30

1. __ 4o _ _.l 1 -w--j ---' ~--!

60 i -70'

.__ I (!) Yes 0 No

NA Seconds

DISPLAY SETTING

30

L 40

60 j

[_~ Default Mode:

Keypad:

REMARKS: Calibrated using FP-47M filter paper. Cal range 30-80 LPM.





(!) Yes

(!) Yes

11/08/13

0 No

0 No

Date: 11 /8/2012

CAL. DUE: 06/28/13

CAL DUE:

Flow: 40 LPM

Actual Flow: 40

(!) Yes 0 No

40 Avg. 40

(!) Yes 0 No

N/A

CALIBRATOR READING

30J 40

50

60 ,--:-· I 70

., . '

Target Volume:

0 On 0 Off (!) N/A

N/A cu. ft.

Entered by: d'2:: Initials

'

GRIFFIN INSTRUMENTS


DATE:

LV-1

LOCATION:

SERIAL# 003599 09-00346

TECH:

11/08112 1


Reason For Calibration : @ Due For Calibration

0 Other (See Remarks) - -- - ---


0 Due and Repair (Se..:_ Remarks)

NISTTRACEABLE EQUIPMENT USED DURING CALIBRATION

MODEL: C-828

MODEL:

Physical Condition: @ Sat

Air Sampler Set At Midpoint Flow:

SERIAL#:

SERIAL#:

0 Unsat

@ Yes

1768

0 No

Is tho Actual Reading w/in 20% of the Indicated Volume on the Air Sampler? :

3 Collections- (Minutes or Flow):: 40 40

Are the Individual Collections w/in 10% of the Average?:

Is Error Within 10%?:

Warm Up Delay:

[_40

r-so J [ _::_Go J l 70 J

@ Yes 0 No

NA Seconds

DISPLAY SETTING

[ j oJ ~

40 J '

IY~I I~ !_ 7<:_ I

Default Mode:

Keypad:

REMARKS; Calibrated usi'lg FP--47M filter paper. Cal range 30-80 LPM.

Does Instrument Meet Finol Acceptance Criteria?:

Ca:ibralion Sticker Attached?:

Date Instrument is Due For Next Ca libration:


@ Yes

@ Yes

11/08/13

0 No

0 No

Date: 1118/2012

@

40

@

N/A

CAL DUE: 06/28/13

CAL DUE:

Flow: 40LPM

Actual Flow: 43

Yes 0 No

Avg. 40

Yes 0 No

CALIBRATOR READING

r3Q I I __ _

L: 40 l [ so::J L so.=J 1 --7o ]

Target Volume:

0 On 0 Off @ N/A

N/A cu. ft.

Entered by: cf~ Initials

I

1

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR 2224 SERIAL#

Owner: DENUKE ----------------------------

DATE: 09/1 0/1 1 LOCATION:

TECH: E.M. Glenn DATE LAST CAL EXPIRES:

114606 06-00120

Griffin lnst

I Reason For Calibration :

I Due For Calibration Repair (See Remarks)

; , Other (See Remarks) _: Due and Repair (See Remarks) --~------ --------~



~ Audio Response fiZJ Geotropism CABLE LENGTH: 39"

CONDITION : Sat AF MECHANICAL ZERO: 0 AL MECHANICAL ZERO: 0

NEW BATTERIES: Yes 1!1 No BATTERY CHECK: Sat -------- ---------------------- -------------

HV {+1-10%} AS FOUND HV AS LEFTHV WINDOW SETTINGS: A.F. A.L.

SOOV: 500 A.F. BT (3.5 mV +I· 1 mV): 3.5 A.F.

1000 V: 1000 A. F. BW (30 mV +1-3 mV): 30 A.F.

1500 V: 1500 A. F. AT (120 mV +1-10 mV): 120 A.F. -

RATE METER .. .... A; -·~~

SCALER SCALE RATE CPM AS FOUND %ERROR AS LEFT %ERROR AS FOUND % ERROR AS LEFT% ERROR

x.1 or x1 100 100 0.0% A. F. .. · ' . 250 250 0.0% A. F. 251 I 0.4% I A. F. I 400 400 0.0% A. F. ' ...

x1 or 1000 1000 0.0% A. F. ·. x10 2500 2500 0.0% A. F. ... .

' •.. ,. ·- ~.,

4000 4000 0.0% A. F. .,

' .. , . : .. ' t;. -.;; . ~

x10 or 10K 10 K 0.0% A. F. "' .- : x100 25K 25 0.0% A. F.

.. . •. . K ~ . ,,; .. . ..

40K 40 K 0.0% A. F. .. . -~-

' ; x100 or 100K 100 K 0.0% A. F. .. . . x1000 250K 250 K 0.0% A. F. - . ' .

< -~. · ..• b · .. ,., .. ;. 400K 400 K 0.0% A. F. .... ~- . .•

'

-Is the As Found Data Within 20% 9f the Set Point?: ! ' Yes No

Overload Light: ! · Adjusted '= Not Adj.

REMARKS: Removed from storage. Calibrated as a unit.

-Does Instrument Meet Final Acceptance Criteria?: • Yes No

Calibration Sticker Attached?: • Yes No

Date Instrument is Due For Next Calibration: 09/10112

INSTRUMENT MARRIED WITH 43-89 #PR127990

~d. PerformedfReviewed by: f9. ®IL ~fen.,. Date: 9/10/2011 Entered by: cf;:: Initials

Calibrations performed to ANSI N323A·1997 siandards.

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR 43-89

owner: DENUKE

DATE: 09/10/11 LOCATION:

PROBE# PR127990 06-00133

Griffin lnst

TECH: Joanne Glenn DATE LAST CAL EXPIRES:

@ Due For Calibration

I REASON FOR CALIBRATION:

0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair






OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH4 70-1593 Th230 16,700 dpm 06/16/09 8,1 70 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm


Condition: (!) Sat 0 Unsat Pu: Th:._l __ _, Sr: j ~~

Tc ss: ._l __ _,I C14: I O.Oo%1 Tc Ni: jl_ _ _ ....J


l HV 1 Vernier: Jr c-99 Source Response Pu-239 Source Background (CPM): Tc-99 Source Response I Nickel (CPM): Response (CPM): Stainless Steel (CPM):

I A ch. II B ch. !Net Eff. A ch. I B ch. I Net Eff. Ach. I B ch. A ch. II B ch. I Net Eff.J -I N/A I I I I I I I I



AFCPM: I I I I I I AF 4 pi eff: I I I I II AF2 pi eff: I I I I I I

Is as found efficiency within 20% of the efficiency from the last cal? 0 Yes @ No (See Remarks)

Note: H the es found data is within 10% of the lest calibra6on and the B-A Xlalk is <1% and the A-B Xlalk is <10%, then the te::hniQan may N/A the plateau section and go directly to ramatl<.s.

GRIFFIN INSTRUMENTS

PROBE#: PR127990 Date: 09/10/1 1


I HV I Vernier: Tc-99 Source Response I SS (CPM):

Pu-239 Source Background (CPM): Net A to B B toAXtalk: Response (CPM): Xtalk: <10% <1%

Ach. I B ch. Net Eff. Ach. B ch. I Net Eff. Ach. B ch.

650 5 988 5.3% 2430 298 13.1% 1

700 7 1995 10.5% 3305 557 17.9% 0

750 3352 1281 18.1% 1

Alpha I Beta Bkg (cpm) 3 167 HVIVemier Pu-239 Tc-99 Ni Tc-99 SS

700 I NIA CPM: 3261



REMARKS: As found off scale - replaced mylar.


· Calibration Sticker Attached?:


INSTRUMENT MARRIED WITH 2224


· 2 pi e!ficlencles denoted In ltallcs.

(!) Yes

(!) Yes

09110/12

2147

11.45%

18.33%

0 No

0 No

# 114606

Date: 9/10/201 1

2

76 8.4% <1%

170 10.5% <1%

281 23.0%

Th-230 C-14 Sr-90

2741 2647

16.40% 26.81%

33.51% 38.35%

Enter~d by:.£__1nitials

Calibrations pelfonned to ANSI N323A·1997 standards.

I

GRIFFIN INSTRUMENTS

. CALl BRA TION CERTIFICATE FOR 43-89 PROBE# PR127990

06-00133

I I !

I

Owner: DENUKE

DATE:

TECH:

01/05/12

Joanne Glenn

LOCATION:


I

Griffin lnst

09/10/12

REASON FOR CALIBRATION: 1J Due For Calibration (_! , Repair (See Remarks) 1C' Other (See Remarks) 0 Due and Repair


NISTTRACEABLE EQUIPMENT AND STANDARDS USED DURING CALIBRATION




OOTC4 70-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12102109 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm


Condition: ~~ Sat 0 Unsat Pu: 17.61%1 Th:! 16.40%1 Sr: l 25.81%!

Tc Ni:! ----'


HV /Vernier: lt c-99 Source Response 'I Pu-239 Source Background (CPM): Tc-99 Source Response I 1 j Nickel (CPM): 1 Response (CPM): Stainless Steel (CPM):

A ch. II B ch. I Net Eff. A ch. I 8 ch. I Net Eff. A ch . I 8 ch. Ach.l l Bch. INetEff. l

700 IN/A I I I 0 I 0 j O.OO% 0 I 0 0 I 0 ! O.OO% j

Net A to 8 1 8 to A Xtalk: Xtalk: <10% I <1%

#Num! <1%

Pu239 Tc99 Ni Tc99 ss Th-230 Sr90 C-14

AFCPM: 0 0 I i 0 0

AF 4 pi eff: 0.00% 0.00% I 0.00% 0.00%

AF2pieff: 0.00% 0.00% I I 0.00% 0.00%

Is as found efficiency within 20% of the efficiency from the last cal? ~ Yes ~!l No (See Remarks)

Note. tr the as found data is within 1 0'4 of the last calibration and the B-A Xtalk ts <1% and the A·B Xtalk is <10%. then t he techn1cian may N/A the plateau section and go d"ectly to remarks.

Safety and Ecology Corporation sEc PROCEDURE

2800 Solway Road

Knoxville, TN 37931


Calibration Certificate for LV-1,Serial # 003787, Bar Code# ,Property# SEC-7252

Date: 05/0911 3 Date last Cal. Expires: 06/13/1 3 Technician : Jeffrey Knight

location : 1,03361 , Reason For Calibration: #Error I

EQUIPMENT USED DURING CALIBRATION

SEC-IS-409 Rev 3

MODEL: 0 -812 V.2 SERIAL#: 3531 CAL. DUE: 11/20/1 3

MODEL:

AS FOUND DATA

As Found Instrument Flow Indication:

As Found Calibrator Flow Indication:

SERIAL#:

AF Physical Cond it ion SAT

60 LPM

60 LPM

CAL DUE:

AS LEFT DATA

As Left Instrument Flow Indication:

As left Calibrator Flow Indication:

Unit of Measure: @ LPM 0 CFM

Reproducibility 60 LPM 60 LPM 60 LPM Average :

~ Are the Individual Counts Within 10% of the Average?

CALIBRATION DATA TARGET VALUE AIR SAMPLER READING CALIBRATOR READING

30.00 LPM 30.00 LPM 30.80 LPM

50.00 LPM 50.00 LPM 49.70 LPM

70.00 LPM 70.00 LPM 70.40 LPM

60 LPM

60 LPM

60.00 LPM

ERROR%

2.67% LPM

0.60% LPM

0.57% LPM

Air Sampler Setting 60.00 l.J Is Error Within 10%?

Reproducibility 60 LPM 60 LPM 60 LPM Average: 60.00 LPM


Air Sampler rotameter reading: 0 Use Manufacturers Indication (!; Use Corrected Marking 0 NIA

Comments: Married as a set with : Model Bar Code#:

V Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

····~·· ·'JjJ.;I Printed Name· r Kn1ght


Reviewedby: ~~Date: >-~--(}

51912013 Page 1 of 1

GRIFFIN INSTRUMENTS


DATE: 09/1 0/1 1

TECH: E.M. Glenn

Reason For Calibration :

2224 SERIAL#

LOCATION :


119790 06-00136

Griffin lnst

0 Repair (See Remarks) 0 Due For Cal ibration

(!) Other (See Remarks) 0 Due and Repair (See Remarks)




CONDITION : Sat AF MECHANICAL ZERO: 0 AL MECHANICAL ZERO: 0

NEW BA ITERIES: 0 Yes (!) No BAITERY CHECK: Sat

HV {+/-10%} AS FOUND HV AS LEFTHV WINDOW SEITINGS: A. F. A.L.

500 V: 500 A. F. BT (3.5 mV +/- 1 mV): 3.5 A. F.

1000 V: 1000 A. F. BW (30 mV +/-3 mV): 30 A. F.

1500 V: 1475 A. F. AT (120 mV +/-10 mV): 125 120

RATE METER SCALER SCALE RATE CPM AS FOUND % ERROR AS LEFT % ERROR AS FOUND % ERROR AS LEFT % ERROR

x.1 orx1 100 100 0.0% A. F.

250 250 0.0% A. F.

400 400 0.0% A. F.

x1 or 1000 1000 0.0% A. F. x10 2500 2500 0.0% A. F.

4000 4000 0.0% A.F.

x10 or 10K 10 K 0.0% A. F. x100 25K 25 K 0.0% A. F.

40K 40 K 0.0% A.F.

x100 or 100K 100 K 0.0% A. F. x1000 250K 250 K 0.0% A. F.

400K 400 K 0.0% A.F.


Overload Light: (!) Adjusted 0 Not Adj .

REMARKS: No previous data. Removed from storage. Calibrate as a unit.






(!) Yes

(!) Yes

09/10/12

#PR152461

Date: 9/10/2011

250 I

(!) Yes

0 No

0 No

0.0% I A. F. I

.

0 No

Entered by: ~ Initials

Cahbrahons performed to ANSI N323A-1997 standards

GRIFFIN INSTRUMENTS

CALl BRA TION CERTIFICATE FOR 43-89 PROBE# PR152461 09-00320

Owner: DENUKE

DATE:

TECH:

09/10/11

Joanne Glenn

LOCATION:


Griffin lnst

04121/10

R.EASON FOR CALIBRATION:







OOTC470-0654 Tc99 ss 17,300 dpm 06/15/09 10,800 cpm

94TH47Q-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm


Pu: Th:j :==~

Sr: l :==~

Condition: @ Sat 0 Unsat


I HV /Vernier: r c-99 Source Response Nickel (CPM):

A ch. II 8 ch. !Net Eft. i I I I

Pu239 Tc99 Ni

AFCPM: I I AF 4 pi eft: I I AF2pi eff: I I

Tcss:t_l __ _JI C14: ~_1 _ _ -J Tc Ni: ~'--------'

Pu-239 Source Background (CPM): Tc-99 Source Response l Response (CPM): Stainless Steel (CPM):

A ch. I B ch. I Net Eft. Ach. I B ch. A ch. ll B ch. I Net Ett:j

I I I I I I

Net A to 8 8 to A Xtalk: Xtalk: <:10% <:1%

Tc99 ss Th-230 Sr90

II II I :======:' I I I I I I I

I I I I L =:=J ~--]


Nota: ~ ll1e as found data is within 10% of lhe last calibnttion and ll1e B-A Xtall< is <1% and lhB A-B X!alk i• <10%, then lhe technician may NJA the plateau section and go directly to rematl<s.

?

GRIFFIN INSTRUMENTS

PROBE#: PR152461 Date: 09/10/11


HV /Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): NetAtoB B to A Xtalk: I SS (CPM): Response (CPM):

Ach. B ch. Net Eft. Ach. B ch. I Net Eff. Ach. B ch.

550 5 1533 8.3% 3220 404 17.4% 0

575 13 2162 11.4% 3360 520 18.1% 3

600 0

Alpha I Beta Bkg (cprn) 3 187

HV /Vernier f!!:ill Tc-99 Nl Tc-99 SS Th-230

575/ N/A CPM: 3360 2162

4 pi AL Efficiencies: 18.15% 11.42%

2 pi AL Efflclencfes: 35.75% 18.29%

REMARKS: No previous cal data. As found off scale - replaced mylar.






@ Yes

@ Yes

09/10/12

0 No

0 No

# 119790

Date: 9/1 0/2011

2859

17.10%

34.96%

96

187

311

Xtalk: <10% <1%

8.7% <1%

9.0% <1%

C-14 Sr-90

2557

25.62% -

36.65%

Entered by: cf) Initials

2 pi efficiencies denoted in italics. Calibrations performed to ANSI N323A-1997 standards.

2

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR 43-89 PROBE# PR152461 09-00320

Owner: DENUKE

DATE:

TECH:

12/31/11

E.M. Glenn

LOCATION:


Griffin Ins!

09/10/12


0 Due For Calibration @ Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair

CABLE LENGTH: 39'' INPUT SENSITIVITY: dual





OOTC4 70-0654 Tc99 ss 17,300 dpm 06/15/09 10,800 cpm

94TH4 70-1593 Th230 16,700 dpm 06116/09 8,170 cpm

2696-00 Pu239 18.500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm

Efficiencies from last cal. :


Tc ss: 11.42% C14: TcNi:


HV I Vernier: 'Tc-99 Source Response Pu-239 Source Background (CPM): r c-99 Source Response Nickel (CPM): Response (CPM): Stainless Steel (CPM):

Ach. B ch. jNet Etf.' Ach. I B ch . J Net Eff. 1 Ach. B ch. A ch, B ch . jNet Eff.

575/ NIA I ., r 3520 . 762 t19.03%f 0 309 1 13 1 2514 112.75%

Net A to 8 B to AXtalk: Xtalk: <10% <1 o/o

11.4% <1 o/o


AFCPM: 3520 2514 2846 2975

AF 4 pi eff: 19.03% 12.75% 17.04% 29.00%

AF 2 pi eff: 37.57% 20.42% 34.83% 41.48%


Note- lithe as round data 1S W11h1n 10".1. or the last cahbrauon and the B· A Xta lk 1S <1•.!. and the A-8 Xtalk 1s <10%. then the IC"..I'lmc1an may NIA the plateau sect1on and go directly to remarks

GRIFFIN INSTRUMENTS

PROBE#: PR152461 Date: 12/31/11


I HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B B to A Xtalk: SS (CPM): Response (CPM): Xtalk: <10% <1%

Ach. B ch . Net Eff. A ch. B ch . I Net Eff. Ach. I B ch .

500 3 475 2.5% 1955 337 10.6% 1 47 12.9% <1%

525 10 1090 5.8% 2785 353 15.1% 0 88 8.7% <1%

550 7 1517 8.1% 3139 423 17.0% 0 121 8.8% <1%

575 17 2086 10.8% 3390 540 18.3% 1 210 8.9% <1%

600 8 3001 15.6% 3484 1029 18.8% 1 309 17.1% <1%

Alpha I Beta Bkg (cpm) 1 210 HV I Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

575/ NIA CPM: 3390 2086 2708 2558



REMARKS: A.F. off scale- replaced mylar. A. F. data taken after mylar change. Re-plateaued due to poor uniformity. Cal due 09/10/12 to match the meter.






2 pi cfficlcncic5 denoted In Italics.

(!) Yes

(!) Yes

09/10/12

0 No

0 No

# 119790

Date: 12131/2011

2

Entered by: ~C, Initials


I

GRIFFIN INSTRUMENTS

CALl BRA TION CERTIFICATE FOR

Owner: DENUKE

DATE: 08/04/12

TECH: Joanne Glenn

2224 SERIAL#

LOCATION:

119790 06-00136

Griffin Ins!


I (!) Due For Calibration 0 Repair (See Remark~) Reason For Calibration:



MODEL: 500-2 SERIAL#: 284951 CAL. DUE: 12/28112

0 Audio Response ~ Geotropism CABLE LENGTH: 39"

CONDITION: Worn AF MECHANICAL ZERO: 0 AL MECHANICAL ZERO: 0

NEW BATTERIES: 0 Yes (!) No BATTERY CHECK: Sat

HV (+/-10"[o} AS FOUND HV AS LEFT HV WINDOW SETTINGS: A.F. A.L.

500 V: 500 A. F. BT (3 .5 mV +/- 1 mV): 3.5 A. F.

1000V: 1000 A. F. BW (30 mV +/-3 mV): 30 A. F.

1500 V: 1500 A. F. AT (120 mV +/-10 mV): 110 120

RATE METER SCALER SCALE RATE CPM AS FOUND % ERROR AS LEFT % ERROR AS FOUND % ERROR AS LEFT % ERROR

x.1 or x1 100 100 0.0% A. F.

250 250 0.0% A. F.

400 400 0.0% A. F.

x1 or 1000 1000 0.0% A. F. x10 2500 2500 0.0% A. F.

4000 4000 0.0% A. F.

x10 or 10K 10 K 0.0% A. F. x100 25K 25 K 0.0% A.F.

40K 40 K 0.0% A. F.

x100 or 100K 100 K 0.0% A. F. x1000 250K 250 K 0.0% A. F.

400K 400 K 0.0% A. F.

Overload Light:


(!) - Adjusted 0 Not Adj.

REMARKS:






(!) Yes

(!) Yes

08/04/13

# PR152461

Date: 8/4/2012

250 I

@ Yes

0 No

0 No

0.0% I A. F. I

0 No

Entered by:~lnitials

Calibrations performed to ANSI N323A-1997 standards.

Owner: DENUKE

DATE:

TECH:

08/04/12

Joanne Glenn

GRIFFIN INSTRUMENTS

43-89 PROBE#

LOCATION:


PR152461 09-00320


Griffin lnst

09/10/12

I

0 ouJ and Repair (!) Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks)






OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18.500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530cpm



Tc ss: 10.84% C14: Tc Ni:


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): r c-99 Source Response Nickel (CPM): Response (CPM): Stainless Steel (CPM):

A ch . B ch . ]Net Eff~ A «h. ' B ch. j Net Eff . . A ch. B ch. A ch . B ch. ]Net Eff.1

575/ N/A I l 3049 ' 595 116.48%: 0 246 1 s 1908 1 9.61%


10.3% <1%


AFCPM: 3049 1908 2487 2542

AF 4 pi eff: 16.48% 9.61% 14.89% 25.38%

AF2 pi eff: 32.54% 15.39% 30.44% 36.30%


Note If the as found data IS withtn 10% of the last calibration and the B-A Xtalk IS < 1% and the A·B Xtalk IS <1 0%. then the techmc•an may NJA the plateau sectiOn and go O•rectly to remarks.

GRIFFIN INSTRUMENTS

PROBE#: PR152461 Date: 08104/12

\ PLATEAU AND SET POINT DATA

HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM) : Net A to B B to AXtalk: I SS (CPM): Response (CPM): Xtalk: <10% <1%

Ach. Bch. Net Eff. A ch. I B ch . l Net Eff. A ch. J B ch .

575 16 775 4.0% 2131 350 11 .5% 0

600 36 1553 7.8% 2890 525 15.6% 1

625 10 1713 8.6% 3013 532 16.3% 1

650 11 1795 8.9% 3239 545 17.5% 1

660 16 1843 9.2% 3226 534 17.4% 0

Alpha I Beta Bkg (cpm) 0 258 HV /Vernier Pu-239 Tc-99 Ni Tc-99 SS

660 /N/A CPM: 3226



REMARKS: Replaced PMT and damaged scintillator.





Perfonned/Reviewed by:

2 pi efficiencies denoted in Italics.

@ Yes

@ Yes

08/04/13

1843

9.16%

14.68%

0 No

0 No

# 119790

Date: 8/4/2012

2

91 10.8% <1%

208 9.9% <1%

232 9.1 % <1%

254 8.2% <1%

258 7.9% <1%

Th-230 C-14 Sr-90

2561 2183

15.34% 21 .28%

31.35% 30.43%

Entered by:~lnitials


I

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE: 08/04/12

2224

LOCATION :

SERIAL# 119790 06-00136

Griffin lnst

TECH: Joanne Glenn DATE LAST CAL EXPIRES: 09/10/12 I

Reason For Calibration: (!) Due For Calibration / 0 Repair (See Remarks)

Q _2the~(See Remarks)


MODEL: 500-2 SERIAL#: 284951 CAL. DUE: 12/28112

'll"i Audio Response Geotropism CABLE LENGTH: 39"

CONDITION: Worn AF MECHANICAL ZERO: 0 AL MECHANICAL ZERO:

NEW BATIERIES: 0 Yes (!) No BATIERY CHECK: Sat -HV 1+/-10%) AS FOUND HV AS LEFT HV WINDOW SETIINGS: A. F.

500 V: 500 A.F. BT (3.5 mV +/- 1 mV): 3.5

1000 V: 1000 A. F. BW (30 mV +/-3 mV): 30

1500 V: 1500 A. F. AT (120 mV +/-10 mV): 110

x.1 or x1 100 100 0.0% A. F.

250 250 0.0% A. F. 400 400 0.0% A. F.

x1 or 1000 1000 0.0% A. F. x10 2500 2500 0.0% A. F.

4000 4000 0.0% A. F.

x10 or 10K 10 K 0.0% A. F. x100 25K 25 K 0.0% A. F.

40K 40 K 0.0% A. F.

x100 or 100K 100 K 0.0% A.F x1000 :!SOK 250 !: 0.0% (I -•• a .

400K 400 K 0.0% A. F.

Is the As Found Data Within 20% of the Set Point?: (!) Yes

@ ---- 0 Overload Light: Adjusted Not Adj.

REMARKS:





(!) Yes

(!) Yes

08/04/13

#PR152461

0 No

0 No

&b

A. F.

A. F.

120

0 No

0

Performed/Reviewed by: Date: 8/4/2012 Entered b~lnltlals

Calibrnlions performod to ANSI N323A·1997 srondan:!s.

Instrument Setup Sheet

INSTRUMENT# MODEL PROBE CAL DUE HIGH VOLTAGE

\ b a4aL.t '13-~ <6-'i-13 hbcJ SERIAL# N/A N/A

11~1,0 P~ I;~Yb/ (AQ>u239/240 I A2 Pu239/240 I (.B~c 99 I 82 Tc99 I Gl Cs137 I G2 Cs137 63724-570 I 63723-570 I 92TC4701425 I 92TC4701422 I 07-00236 I o1-oo239

BACKGROUND a / ~ Pu 239 eff: 1 '). '"ft4 t Tc99 eff:

0 I &1\ 17~ 1q1s

{J) I 3oS lSo I~G? ·

0 I d.1JO I b~ l~~q

0 I r;;.~:J. ISO \q So

(J I d.~3 I~ l? 19~S

0 I 'J.<i>'J. \ 4b l9Si 0 I ~51 \ t.f 5 \<11~

\ I 3,~ I '1 b \Cbbd.

\ I ?.93 'L.\ i lq\'6 0 I J.qi \ 11 \~1S

I DATE:

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

43-89

LOCATION:

PROBE# PR152461 09-00320

TECH:

08/04/12


Griffin lnst

09/10/12







Soun;e Number lsotcpa 4 pi 'Activlty Assay Date · 2 pi AQUVIty

OOTC470·0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm '

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696·00 Pu239 18,500dpm 12/02/09 9.370 cpm

2697·00 Sr90 12.200 dpm 03/01/00 8,530 cpm


Condition: (!) Sat 0 Unsat Pu: ' 18.32%] Th:j 16.21%j sr:l2~l

Tc ss f _10.~4·~] C14: [ -·-J Tc Ni: J I As Found (AF) Efficiencies:

HV /Vernier:

I - 575/ N/A

AFCPM:

AF 4 pi eft:

AF 2pl eff:

r.t:"-jTc-99 Source Response I Pu-239 Source jf Nickel (CPM): _ .. ~onse (C~M) : _ j Background (CPM): 'rc-99-So~rce Response j

Stainless Steel (CPM:J

I A ~h. 1

._ B ch. Net E~~t_~~1~hl jNe. t ~~- _ 3049 595 16.48% --- ..• - - - ----- ... _

A ch. B ch. _A_ ch-:-1 !J c~ rNet E_ff.: 0 -r=-24.f___ . 5_ .. 1908 ~1.o/o I

[-3a~l [-- 1

(J_f4B~;;- l I __ J

~~ Net A to a ' slo A xialk:---'1 Xtalk: <10% 1 <1%

L 10.3% L -:2_% I

9.61% .., ['14--:89%

[ 2542

L 25.3BU

~~~0% l

[ =-=j L-1 I


Nolo; II !he asfounddalo 15wi\hin 10% ollhe lastca!ibralion and lho 8 -AXIalk I• <1% and lho A·B Xlall< is <IO'Io, lhon lho lochnieianmoy N/A lho plaleou section and go dlloclly lo remarks.

GRIFFIN INSTRUMENTS

PROBE#: PR152461 Date: 08/04/12


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B B to AXtalk: SS (CPM): Response (CPM): Xtalk: <10% <1%

Ach. B ch. Net Eft. Ach. B ch. I Net Eff. Ach. Bch.

575 16 775 4.0% 2131 350 11.5% 0

600 36 1553 7.8% 2890 525 15.6% 1

625 10 1713 8.6% 3013 532 16.3% 1

650 11 1795 8.9% 3239 545 17.5% 1

660 16 1843 9.2% 3226 534 17.4% 0 ____ .,. .•. ·- - -~--

~

----···- --

Alpha I Beta Bkg (cpm) 0 258 HV lVernier fl.!.:m Tc-99 Nl Tc-99 ~s

660/ NJA CPM: 3226



REMARKS: Replaced PMT and damaged scintillator.




INSTRUMENT MARRIED WITH 22.24


2 pi efficiencies denolod In llallco,

@ Yes

@ Yes

08104113

1843

9.16%

14.68%

0 No

0 No

# 119790

Date: 8/4/2012

2

91 10.8% <1%

208 9.9% <1%

232 9.1% <1%

254 8.2% <1%

258 7.9% <1%

Th-230 C-14 Sr-90

2561 2183

15.34% 21.28%

31.35% 30.43%

Entered by:~lnitlals

CoUbratlons performed to ANSI N323A-19t7 atandards.

J


2800 Solway Road

Knoxville, TN 37931

.Calibration Certificate


Date: 05/09/13 Date last Cal. Expires: 08/15/13 Technician : Jeffrey Knight

SEC-IS-409 Rev 3

location: 9999, Reason For Calibration : Due for Calibration


MODEL: D-812 V.2 SERIAL#: 3531 CAL DUE: 11/20/13

MODEL:

AS FOUND DATA



SERIAL#:

AF Physical Condition SAT

60 LPM

60 LPM

CAL DUE:

AS LEFT DATA

As left Instrument Flow Indication:

As Left Calibrator Flow Indication:

Unit of Measure: (;) LPM 0 CFM




30.00 LPM 30.00 LPM 28.40 LPM

50.00 LPM 50.00 LPM 49.70 LPM

70.00 LPM 70.00 LPM 70.10 LPM

60 LPM

60 LPM

60.00 LPM

ERROR%

5.33% LPM

0.60% LPM

0.14% LPM




Air Sampler rotameter reading: 0 Use Manufacturers Indication C!: Use Corrected Marking 0 N/A

Comments: Married as a set with: Model Bar Code#:

[7 Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

ate Instrument is Due For Next Calibration: 05/09/14

Performed by:~-HilAT'--~~------ Reviewedby: ~Date: J-f-/J Printed Name:

51912013 Page 1 of 1

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE: 09/09/11

TECH: Joanne Glenn

2224 SERIAL#

LOCATION:


119809 06-00134

Griffin lnst

03/22/11




MODEL: M-500 SERIAL#: 114512 CAL. DUE: OB/24112


CONDITION: Worn

NEW BATTERIES:

HV (+1-10%) AS FOUND HV

500 V: 500

1000 V: 1000

1500 V: 1500

x.1 orx1

x1 or x10

x10 or x100

AF MECHANICAL ZERO:

(!) Yes 0 No

AS LEFT HV

A. F.

A. F.

A. F.


BATTERY CHECK: Sat

WINDOW SETTINGS:

BT (3.5 mV +1- 1 mV}:

BW (30 mV +1-3 mV):

AT (120 mV +1-10 mV):

A. F.

3.5

29

120

A.L.

A.F .

30

A. F.



REMARKS:





@ Yes

@ Yes

09109112

#PR130517

0 No

0 No

0

Performed/Reviewed by: Date: 9/9/2011 Entered by: c;{t:.. Initials

Calibrations performed 10 ANSI N323A-1997 standards.

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

09/09/11

Joanne Glenn

LOCATION:


Griffin lnst

03122111


@ Due For Calibration I .







OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16.700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12102/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm


@ Sat 0 Unsat Sr: j 26.47%j

Tc Ni: '--1 - ---'

Condition: Pu: 19.15%J Th: j

:==::~ Tc ss: j 9.5o%j C14: ._I __ ____,


I HV /Vernier: lc-99 Source Response Pu-239 Source Background (CPM): Tc-99 Source Response

Nickel (CPM): Response (CPM): Stainless Steel (CPM):

A ch. I I B ch . I Net Eff. A ch. I B ch. I Net Eff. Ach. I B ch. Ach. ll Bch. INetEff.l

I 650 J I 3297 1 465 117.82% 0 I 223 2 I 1796 l 9.oa%

Net A to B B to AXtalk: Xtalk: <10% <1%

6.8% <1%


AFCPM: 3297 I I II 1796 II 2799 2493

AF 4 pi eff: 17.82% I [ I 9.09% I I 16.76% 24.54%

AF 2pieff: 35.19% I I I I 14.56% I I 34.26% 35.10%

Is as found efficiency within 20"/o of the efficiency from the last cal? @ Yes 0 No (See Remarks)

Note: If the as found data is within 10% of the last calibration and the B-A Xtalk is <1% and the A·B Xtalk is <10%, then the tedmlcian may N/A the plateau section end go directly to remar1cs.

GRIFFIN INSTRUMENTS

PROBE#: PR130517 Date: 09/09/11


HV /Vernier: Tc-99 Source Response Pu-239 Source Background {CPM): Net A to B B to AXtalk: SS {CPM): Response (CPM): Xtalk: <10% <1%

Ach. B ch. Net Eff. Ach. B ch. I Net Eff. Ach. Bch.

650 2 1796 9.1% 3297 465 17.8% 0

675 0

Alpha I Beta Bkg (cpm) 2 238 HV /Vernier Pu-239 Tc-99 Ni Tc-99 SS

650/ N/A CPM: 3280 2059



REMARKS: Replaced mylar due to off scale as found readings.




I


Perfonned/Reviewed by:

2 pi efliclenc:les denoted In Italics.

(!) Yes

(!) Yes

09109/12

0 No

0 No

# 119809

Date: 9/912011

2

223 6.8% <1%

462

Th-230 C-14 Sr-90

2768 2720

16.56% 26.84%

33.86% 38.38%

Entered by:.£._1nitials


I

PROBE REPAIR ONLY

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

01/04/12

Joanne Glenn

LOCATION:


I

Griffin lnst

09/09/12


0 Due For Calibration C!> Repair (See Remar~s) 0 Other (See Remarks) 0 Due and Repair






OOTC470-0654 Tc99 SS J7,300dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm


Condition: @ Sat 0 Unsat Pu: 17.72%j Th:l 16.56%1 Sr: J 26.84%j

Tc ss: j 10.53%1 C14: J Tc Ni: j.__ _ __,


I HV /Vernier: ~c-99 Source Response I Pu-239 Source Background (CPM): Tc-99 Source Response I

Nickel (CPM): Response (CPM): I Stainless Steel (CPM):

A ch. II B ch. I Net Eff. A ch. I B ch. J Net Eff. Ach. I Bch. A ch. II B ch. I Net Eff. J

I 650/ N/A I I 0 1 3327 1 o.oo% 0 I 9 0 I 7 l-0.01% 1

I Net A to B B toAXtalk: Xtalk: <10% <1%

I 100.0%

Pu239 Tc99 Ni Tc99 ss Th-230 s~o C-14

AFCPM: 0 I I II 7 I I 0 9

AF 4 pi eft: 0.00% I I I I ..{).01% I I 0.00% 0.00%

AF 2pi eff: 0.00% I I I I -0.02% I I 0.00% 0.00%

Is as found efficiency within 20% of the efficiency from the last cal? 0 Yes (!> No (See Remarks)

Note: If the as found data is within 10% of the last calibration and the B-AXtalk is <1% end the A· B Xtalk is <10%, then the technician may NJAthe plateau section and go directly to remarks.

GRIFFIN INSTRUMENTS

PROBE#: PR130517 Date: 01/04/12


HV I Vernier: Tc-99 Source Response Pu-239 Source j Background (CPM): Net A to B B to A Xtalk: SS (CPM): Response (CPM): Xtalk: <10% <1%

Ach. B ch. Net Eff. Ach. B ch. J Net Eff. Ach. B ch.

725 12 512 2.7% 2610 292 14.1% 2 42 8.7% <1%

750 16 873 4.7% 2970 314 16.0% 2 55 8.0% <1%

775 8 1209 6.4% 3213 318 17.4% 3 99 6.4% <1%

800 14 1443 7.7% 3331 391 18.0% 3 119 7.5% <1%

825 10 2175 11.4% 3462 458 18.7% 3 195 7.1% <1%

850 9 2595 13.6% 3521 735 19.0% 4 240 12.3% <1%

Alpha I Beta Bkg (cpm) 2 176 HV /Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

825/ N/A CPM: 3529 2015 2781 2660

4 pi AL Efficiencies: 19.06% 10.63% 16.64% 27.07% 2 piAL Efficiencies: 37.64% 17.03% 34.01% 38.72%'

REMARKS: Replaced nicked mylar. No response - replaced PMT. Cal due 09109/12 to match the box.





Performeci/Reviewed by:

2 pi ollicloncies denoted In Italics.

f~l Yes

(!) Yes

09/09/12

0 No

0 No

#119809

Date: 1/4/2012

2

Entered by: c!};t. Initials

Callbn~tions performed to ANSI N323A-1997 standards.

I

PROBE REPAIR ONLY

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

05/03112

E.M. Glenn

LOCATION:


I

Griffin lnst

09/09112


0 Due For Calibration (!) Repair (See Remarks) I 0 Other (See Remarks) 0 Due and Repair



MODEL: 2224 SERIAL#: 119809 CAL. DUE: 09/09112



OOTC470-0654 Tc99 SS 17,300 dpm 06115109 10,800 cpm

94TH470-1 593 Th230 16,700 dpm 06/1 6/09 8,170 cpm

2696-00 Pu239 18.500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03101/00 8,530 cpm

Efficiencies from last cal.: --~ -


Tc ss: 10.63% C14: TcNi:


HV I Vernier: Tc-99 Source Response I Pu-239 Source Background (CPM): lTc-99 Source Response Nickel (CPM): Response (CPM): . Stainless Steel (CPM):

A ch . Bch. jNet Eff~ Ach. 1 B ch. j N!t Eff.· A ch . B ch. A ch . B ch. jNet Eff.

825 I NIA .,

3164 309 17.1 0°/ol 1 149 i 20 l 1371 7.06%


4.8% <1%


AF CPM: 3164 1371 2689 1916

AF 4 pi eff: 17.10% 7.06% 16.10% 19.41%

AF 2 pi eff: 33.76% 11.31% 32.90% 21.77%

Is as found efficiency within 20% of the efficiency from the last cal? 0 Yes (!) No (See Remarks)

Noto If tho as found data IS wrth1n 10% of the last cahbrahon and the B·A Xtalk 1s <1°.i. and the A-8 Xtalk is <1 O'A. . then the techn1C1an may N/A the plateau sectoon and go dorectly to rematks

GRIFFIN INSTRUMENTS

PROBE#: PR130517 Date: 05103/12


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): ~etA to B B to A Xtalk: SS (CPM): Response (CPM): X alk: <10% <1%

A ch. B ch . Net Eff. Ach. B ch. I Net Eff. A ch. I B ch .

800 15 964 5.1% 2968 268 16.0% 1 86 5.8% <1%

825 27 1273 6.8% 3209 362 17.3% 2 99 7.6% <1%

850 13 1510 7.9% 3341 363 18.1% 0 140 6.3% <1%

875 13 1687 8.8% 3536 402 19.1% 0 161 6.4% <1%

900 27 2161 11 .4% 3542 499 19.1% 0 186 8.1% <1%

925 3544 719 19.2% 0 208 12.6% <1%

Alpha I Beta Bkg (cpm) 180

HV I Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

9001 N/A CPM: 3492 2159 2894 2628


2 piAL Efficiencies : 37.26% 18.32% 35.41% 38.47%

REMARKS: Turned in due to low source check. Re-plateaued. Cal due 09109112 to match the meter.






2 pi efficiencies d&notcd in italics.

@ Yes

@ Yes

09/09/12

0 No

0 No

# 119809

Date: 5/3/2012

2

Entered by : ~c;:_ Initials


I

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR Owner: Gl

2929 SERIAL# 160005

------------- -----DATE: 01/19/12 LOCATION: Griffin lnst


Reason For Calibration: Due For Calibration I Repair (See Remarks)

-CABLE LENGTH: 39" • • Other (See Remarks) Due and Repair (See Remarks) - -NIST TRACEABLE EQUIPMENT USED DURING CALl BRA TION



Condition: Unsat AF Mechanical Zero: 0


Scaler Function Check

Bela Channel Window (4· 50 mV):

Alpha Channel Window (175 mV. 120 for 3030):

Alpha Counts wtpulser @ 1 0.000 CPM:

Beto Counts w{Pulser@ 1 0.000 CPM:

As Found

4-46

175

9.966

9.989

HIGH VOLTAGE POWER SUPl Y CAL (2929 only)

1 KV Reading (R-5 on HV Board) :

Max HV (1500 V +): ; Sat

REMARKS: Re-calibrated for rental.

Does Instrument Meet Final Acceptance Criteria?: • Yes

Calibration Sticker Attached?: • Yes


INSTRUMENT MARRIED WITH 43-10-1 #PR164048

No

No

Performed/Reviewed by; Date: 1/19/2012

As left

4· 50

AF.

AF.

A. F.

A.F

Unsat

%Error: 0.1 %

%Error: 0.1%

dC Entered by:_·_._lnitlals

Cahbtations performed to ANSI N323A-1997 standards

,/ '::>

GRIFFIN INSTRUMENTS


Owner: Gl ---------- -------

DATE:

TECH:

01/19/12

E.M. Glenn

LOCATION:


Griffin lnst

05/31/12


Due For Calibration • ·· Repair (See Remarks) Other (See Remarks) 1_ Due and Repair



MODEL: 2929 SERIAL#: · 160005 CAL. DUE: 01/19/13 ------




94 TH4 70-1593 Th230

2696-00 Pu239

2697-00 Sr90

PX 726 C14

Condition: • Sat Unsat


HV I Vernier: - Tc-99 Source Response Nickel (CPM):

·A~ Bch.

850 I 3.49 I

Pu239 Tc99 Ni

-----AFCPM: 6529

---- - ' AF 4 pi eff: 35.29%

AF 2 pi eff: 69.68% I -~-·--- -- --

4 pi Activity Assay Date 2 pi Activity

17,300 dpm 06/15/09 10.800 cpm

16,700 dpm 06/16/09 8,170 cpm

18,500 dpm 12/02/09 9,370 cpm

12.200 dpm 03{01/00 8,530cpm

48,780 dpm 01/21/08 18,660 cpm


Pu: 37.54% Th: 34.99% Sr: 41 .57%

Tc ss : 22.05% C14: L--~ Tc Ni: . _ __ _


Background (CPM): Tc-99 Source Response Stainless Steel (CPM):

A ch.--8 ch." j Net Eff.l

_ __. ___ __.._1_ ...1-_3_990 2.73%1

- ---Net A to B 1 B to A Xtalk: Xtalk: <10% <1%

- ---3.2% <1%

Tc99 ss Ih:lli Sr90 C-14

-----3990 5348 3886 4280

-----··--· ·------22.73% 32.02% L__!1_.72% --·, 8.66%

----- - ---36.41% 65.46% 59.67% --22. 63~

·-- -- --------'

Is as found efficiency within 20% of the efficiency from the last cal? ! Yes No (See Remarks)

Note: If the as founo data os w1trun 10% of the last calibratoon and !he B-A XlaiK IS <1% and the A·B Xtalk os <1 0%, tnen the ted'lnJCian may NJA the plateau sect•on and go directly to remarl<s.

GRIFFIN INSTRUMENTS

PROBE#: PR164048 Date: 01119/12


HV I Vernier: Tc-99 Source Response Pur239 Source Background (CPM): Net A to B B toAXtalk:

I SS (CPM): Response (CPM): Xtalk: <10% <1%

A ch. 1 B ch . Net Eff. Ach. B ch. J Net Eff. A ch. B ch.

750/3.06 3 2357 13.5% 5637 358 30.5% 1 30 5.5% <1%

800/3.26 0 3000 17.1% 6116 291 33.1 o/o 1 39 4.0% <1%

850/3.47 1 3824 21 .9% 6531 253 35.3% 0 42 3.1% <1%

875/3.52 0 3940 22.4% 6529 278 35.3% 0 57 3.3% <1%

900/3.67 0 4389 25.0% 6518 404 35.2% 2 67 4.9% <1%

92513.79 1 102

·---


875/3.52 CPM: 6529 3940 5244 4595 3814

4 pi AL Efficiencies: 35.29% 22.45% 31.40% 9.30% 40.95% 2 piAL Efficiencies: 69.68% 35.95% 64.19% 24.32% 58.57%

REMARKS: Replaced torn mylar. A. F. data taken after repair. Re-plateaued.

Does Instrument Meet Final Acceptance Criteria?: • ' Yes No

Calibration Sticker Attached?; -•• · Yes ,-' No




2 pi efficiencies denoted in italics. Callb<ations performed to ANSI N323A-1997 standallls .

2

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR LV-1 SERIAL# 004044

Owner: Gl

GENERAL INFORMATION


TECH: Joanne Glenn DATE LAST CAL EXPIRES: 08/23/13




MODEL: C-828 SERIAL#: 1768 CAL. DUE:

AS FOUND DATA

Physical Condition: (!) Sat 0 Unsat

(!) Yes

Flow: 50 LPM

Air Sampler Set At Midpoint Flow: 0 No Actual Flow:

Is the Actual Reading w/in 20% of the Indicated Volume on the Air Sampler?: (!) Yes

3 Collections- (Minutes or Flow):: 50 50 50 Avg.

Are the Individual Collections w/in 10% of the Average?: (!) Yes

CALIBRATION DATA

TARGET VALUE DISPLAY SETTING

30

40

50

60

70

80

Leak Test (if required): 0 Sat

REMARKS:




30

40

50

60

70

80

(!) N/A

(!) Yes

(!) Yes

05/03/14

CALIBRATOR READING

30

40

50

60

70

80

F1lter Paper Used:

0 No

0 No

0 No

0 No

FP47M

06/28/13

50

50

Is Error Within 10%?:

(!) Yes 0 No

Performed/Reviewed by: Date: 5/3/2013 Entered by: ___ lnitials

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR LV-1 SERIAL#

Owner Gl

DATE:

TECH:

05108?3

Joanne Glenn

GENERAL INFORMATION

LOCATION :


004045

Gnff•n lnst

08/23113

Reason For Calibration: ~' Due For Calibration :; Repair (See Remarks)

:J Other (See Remarks) :::) Due and Repair (See Remarks)


MODEL: C-828 SERIAL#: 1768 CAL. DUE:

AS FOUND DATA

Physical Condition: '3 Sat C Unsat Flow: 50 LPM

Air Sampler Set At Midpoint Flow: (~ Yes No Actual Flow:

Is the Actual Reading wlin 20% of the Indicated Volume on the Atr Sampler?:

3 Collections- (Minutes or Flow):: 50 so Are the lndivtdual Collections wlin 10% of the Average? :

C!· Yes

50

~~ Yes

CALIBRATION DATA

Avg.

TARGET VALUE DISPLAY SEITING CALIBRATOR READING

30

40

50

60

70

80

.-, ,-

30

40

50

60

70

80

30

40

50

60

iO

80

r, '-)

,-., "-·

No

No

06/28113

50

50

Is Error Within 10% ?:

(_!;, Yes 0 No

Leak Test (if required) : '-• Sat ,., NIA Filter Paper Used: FP 47M

REMARKS

Does Instrument Meet Final Acceptance Ctltena? .:!) Yes ( ,_ No

Calibration Sltcker Attached?. •:!' Yes No

Date Instrument ts Due For Next Calibration 05108114

P<:rforme(VRevtewed by: Date: 5/8/2013 Entered by:~lnitials

GRIFFIN INSTRUMENTS

CALIBRATION CERTIFICATE FOR MICRO REM SERIAL# Owner: DENUKE

2023 08-00281

-------------------DATE: 08/21/12 LOCATION: Griffin lnst

TECH: Joanne Glenn I


REASON FOR C~UBRATION: Due for Calibration

NIST TRACEABLE EQUIPMENT AND SOURCES USED DURING CALIBRATION

PULSER MODEL: MP-2 PULSER SERIAL: 1000 PULSER CAL DUE: 07/19/13

SOURCE NUMBE 10250 ISOTOPE: Cs137 ASSAY DATE: 08/30/07

Geotropism TEMP 52.3 F BARO PRESS: 29.29" HUMIDITY 48%

I 0 ---~ --rli 0 ""'" I A.F.Data 1A.F. Vo ERROR , I A.l.Data ,A.l. Vo ER~ -- uR{fir ----- --------·---- ···-··-- ··- ---------------- --------------

!xO.~ Sci!~~*. ,

ixo.1 ~t:aia

lrt"Sc;"Ie* 1~..?~~~-J

mR{hr

~iQ"_~9''~- - J

~~0 Sc~J~--- ~ lx1Q _Sca_le i

rii.9o seal~ .~ r -·-- ·- · - 1

[x~OO .~cale 1 ,.---------· -·-1

l~~_9_Q_$c~l~ -r --··- - --- -l

t£0!)_Q ~-~~~_j r------~~~J lxlOOO Scale I l_ -·-·-- -- ---

l19. ... -~ i16Q __ _j

:g_,~!L_~ i035--l :!~L __ j

~~2 -=--= )L ___ J ~l7 ---~-] j-o·--·-=J :w-s-1 J§.L_J

cs:o~] r--s.ooAJ , __ 3_.1~

[ -- 5.0o/~l

I 1o.o%1 1 6.3°fol L------- - ---~

[_ o.o%1 ~ .. -~- S.0%1 , --::-:-.:-:1 [__ __ 3.1%1

~~---; ~,;. __ , ___ ., __ _ 16.£_ IA.F. l [6£, _~

[L-=--=-:-.J [9 l :1.6 I c==:; [lQ.s·--l ~--. J [M.:__] :A. F~ ___ j ~~· --=:·~--


@ Yes 0 No, See Remarks

REMARKS:




(!) Yes

(!) Yes

08/21/13

0 No

0 No

.- I L ___ _ ,--~

r-~ _ __j

0.0°~

o.o%1 o.o%1

j 0.0~ C s.o%1 r--o.o%1 '------=-=-=--= [ ____ _]

:J ==== -l ·------'

Performed/Reviewed by: $"""""" gr...... cfJ Date: 8121/2012

*Pulsed Scale

Entered by: cf Initials


Thermo Fisher SCIENTIFIC


Tbe wodd leader in serving science

Report Number MicroRem-2023 Page 1 of 2

Instrument Serial Number

Test Equipment

Calibration Standards

Micro Rem LE 2023 FLUKE 8010A S/N 2650076 Cal Due:10 Nov 11 FLUKE 80K-40 S/N HVP-003 Cal Due:02 Feb 12 MP-2 S/N 174 Cal Due: 9 May 12 Cs-137 1 OmCi S/N 733 Cal Due 23 Jan 12 Cs-137 10Ci S/N 375 Cal Due 23 Jan 12

Environmental Conditions Temperature 23.6"C Relative Humidity 46% Barometric Pressure 29.88 inHg

Range Calibration Point Reading X.1 1600 CPM 16 1-1Rem/hr X.1 400 CPM 4 1-1Rem/hr X1 16K CPM 160 uRem/hr X1 4KCPM 40 1-1Rem/hr X1 .16 mR/hr (*140) 160 1.1Rem/hr

X10 1.6 mR/hr 1600 uRem/hr X10 .4 mRihr 400 )JRem/hr

X100 16 mR/hr 16000 uRem/hr X100 4 mR/hr 4000 )JRem/hr

X1000 160 mRihr 160000 uRem/hr X1000 40 mR/hr 40000 )JRem/hr

(*) Received readings out of specifications.

Received condition 0 In tolerance ~ Out of tolerance

Calibration standards used have calibration traceable to N.I.S.T.

Date: 11-Aug-11

P.O. Number:

RMSI Depot Ser~ice Center Environmenlal lnslrumenls

1154

312 Miami St. Wesl Columbia, SC 29170

(600) 274-421Z (803) 822-80531ax

VNIVI.Ihei/JlO.COnl ~ n -4--·0.L ~ ( hI 1~-~-l(

Certificate of Test & Calibration & Conformance

Thermo Fisher Scientific certifies that the items in this report were inspected, tested and calibrated (as indicated on page 1 of this form} and found to meet all documented requirements for quality and performance under Thermo Fisher Scientifics ISO 9001:2000 Certified Quality Management System inspection and test procedures and in compliance with ISO 17025 and ANSI I NCSL Z540 and all requirements of Customer PO.

GENERAL: All calibrations performed at Thermo Fisher Scientific are' performed within the following environmental conditions: Temperature: 22±4 •c (72±6 °F) Humidity: Greater than 15% but less than 65% relative humidity. Barometric Pressure: As measured at 236 ASL (760 mm Hg nominal). Test equipment: All test equipment calibrations are traceable to NIST and equipment is re-certified annually. Radiation Sources: All radiation sources have emission rates or exposure intensities that are traceable to NIST and are re-certified at least annually (photon calibrations are re-r.ertified every six months).

ACCURACY OF CALIBRATION: Calibrations are performed per the methods and requirements stated in ANSI N323 unless the customer and Thermo Fisher Scientific have agreed to a different standard. Some instrumentation is inherently Incapable of meeting this requirement and the calibration will meet the technical specification as slated in the equipment's technical literature.

NOTIFICATION OF ERRORS: If any errors are detected in Thermo Fisher Scientifics calibrations, Thermo Fisher Scientific will notify the customer and meet any other reporting requirements.

DO NOT REPRODUCE: This report shall not be reproduced except in full without the written approval of Thermo Fisher Scientific.

INFORMATION ON TECHNICAL ASPECTS OF A CALIBRATION: Information on a calibration may be obtained from Thermo Fisher Scientifics Quality Assurance Manager or the Depot Operations Supervisor:

QA Manager One Thermo Fisher Way Oakwood Village, OH 44146-6519 Phone: (440) 703-1400 Fax: (440) 703-1596

Depot Operations Supervisor 312 Miami Street West Columbia, SC 29170 Phone: (803) 822-8843 Fax: {803) 822-8053

Statement of the Uncertainty of Measurement

ESTIMATED UNCERTAINTIES IN REFERENCE FIELD MEASUREMENTS UNCERTAINTIES IN GAMMA REFERENCE FIELD MEASUREMENTS

THESE UNCERTAINTIES ARE CALCULATED FOR THE WORST CASE CONDITION

TRANSFER STANDARD INSTRUMENT

Radiation Field Calibration

ENVIRONMENTAL EFFECTS

Pressure (not correcting for barometer error} 0.4mm/760mm Temperature (not correcting thermometer) 0.2°C@22°C

RADIATION FIELD ERRORS Error in established source to reference distance Reproducibility of the position of the test instrument Vs. the reference instrument Source position reproducibility Exposure time Source decay corrections Beam size and uniformity

Subtotal: Transfer Standard Instrument Subtotal: Environmental Effects Subtotal: Radiation Field Errors

Total for Source Calibration:

TOTALS

max(%}

1.00

0.1 1.1

1.3 0.04

1.3 0.1 0.4 1.4

1.00 1.1 2.4

2.8

typ(%)

1.00

0.1 1.1

0.6 0.04

0.6 0.1 0.4 1.1

1.00 1.1 1.5

2.4

Form 57-045 Rev2 Page2

GRIFFIN INSTRUMENTS

.;AUBRATION CERTIFICATE FOR Owner: DENUKE

2929 SERIAL# 160026 06-00150

DATE: 09/08/11 LOCATION: · Griffin Jnst


Reason For Calibration: • • Due For Calibration 1 1 Repair (See Remarks)

CABLE LENGTH: 39" Other (See Remarks) --"----

Due and Repair (See Remarks) ----- - ---- --'----


MODEL: M-500 SERIAL#: 134715 CAL DUE: 04/13/12


Condition: !! Sat Unset AF Mechenical Zero: 0

AL Mechanical Zero: 0 ---------------------Seeler Function Check

Bete Channel Window (4-50 mV):

Alpha ChBnnel Window (175 mV. 120 for 3030):

Alpha Counts wfPulser@ 1 0.000 CPM:

Beta Counts w/Pulser@ 1 0.000 CPM:

. As Found

4-50

165

9.985

9.985

HIGH VOLTAGE P9WER ~UPL Y CAL. (2929 -only)

1 KV Reading (R-5 on HV Boerd): 0.975

Mex HV (1500 V +): ! ' Sat

REMARKS:

Does Instrument Meet Final Acceptance Criteria?: ! Yes

Calibration Sticker Attached?: ; Yes



No

No


As left

A. F.

175

A. F.

A. F.

Unset

%Error: 0.2%

%Error: 0.2%

Entered by: cf(7-. Initials

Calibrat1ons per1ormed to ANSI N323A-1997 standards.

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

09/08/11

E.M. Glenn

LOCATION:


Griffin lnst

06/29/10

I ' •

1 Due For Calibration (J Repair (See Remarks) ,:.) Other (See Remarks) () Due anb Repair






Source Number Isotope 4 pi Activity Assay Date 2 pi Activity OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm

PX 726 C14 48,780 dpm 01/21/08 18,660 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

94 TH4 70-1593 Th230 16,700 dpm 06/16/09 8,1 70 cpm

Efficiencies from last caL:

Condition: Sat Unsat Pu: sr:f Th: j :=====: Tc ss:L ____ I C14: LI __ -----' TcNi :


HV I Vernier: ITc-99 ~ource Response 1

II N1ckel (CPM): 1

Net A to B l B to A Xtalk: Xtalk: <10% <1%

AFCPM: ; -------1

AF 4 pi eft: - J

AF 2pi eff:

Is as found efficiency within 20% of the efficiency from the last cal? Yes ·~ ' No (See Remarks)

Note: If lhe as found daY! 1s within 10% of the last calibration and the 6-A Xtalk 1s <1% and the A-6 Xtalk is <10%, then the technician may N/A lhe plateau sect ion and go dtreclly to remarks.

GRIFFIN INSTRUMENTS

PROBE#: PR164051 Date: 09/08/11


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B B to A Xtalk:

J SS (CPM): Response (CPM): Xtalk: <10% <1%

Ach. B ch. Net Eff. Ach. B ch. I Net Eff. Ach. B ch .

650/2.63 1 1318 7.5% 4712 658 25.5% 0 13 12.0% <1%

700/2.85 0 2407 13.7% 5989 526 32.4% 0 45 7.4% <1%

750/3.06 1 3318 18.8% 6494 422 35.1% 0 57 5.3% <1%

775/3.13 0 3599 20.5% 6579 443 35.6% 1 55 5.6% <1%

800/3.26 0 4119 23.5% 6602 450 35.7% 0 52 5.7% <1%

825/3.36 0 93

Alpha I Beta Bkg (cpm) 55 HV /Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

775/3.13 CPM: 6579 3599 5120 3394 3971


2 piAL Efficiencies: 70.05% 32.81% 62.66% 17.89% 60.56%

REMARKS: No previous data.

Does Instrument Meet Final Acceptance Criteria?: -•• Yes No

Calibration Sticker Attached?: •• Yes No



Performed/Reviewed by: Date: 9/8/2011 Entered by: ~ Initials

2 pi efficiencies denoted in italics. Calibl"l!tions performod to ANSI N323A-1997 standards.

2

GRIFFIN INSTRUMENTS

ALIBRATION CERTIFICATE FOR Owner: DENUKE

2929 SERIAL# 160026 06-00150

DATE: 08103/12 LOCATION: Griffin Ins!

TECH: E.M Glenn DATE LAST CAL EXPIRES: 09/08/12


CABLE LENGTH: 39"

0 Due For Cal ibration

0 Other (See Remarks)

I

lo Repair (See Remarks)

(!) Due and Re~~(~ee Remarks)









Alpha Counts w/Pulser@ 10,000 CPM:

:leta Counts w/Pulser@ 10,000 CPM:

As. found

4-50

175

9,982

9,982

As Left

A.F.

A. F.

A. F.

A. F.

HIGH VOLTAGE. POWER SUPLY CAL (2929 only)

1 KV Reading (R-5 on HV Board):

Max HV (1500 V +):

A .F.

(!) Sat 0 Unsat

REMARKS: Replaced broken volume pot and missing knob for alpha channel.






(!) Yes

(!) Yes

08/03/13

0 No

0 No

#PR164051

Date: 813/2012

%Error: 0.2%

"'o Error: 0.2%

Entered by: cfC/ Initials

Cahbra1100s performed 10 ANSI N323A-1 997 standards

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

08/03/12

E.M. Glenn

LOCATION:


Griffin lnst

09/08/12

REASON FOR CALIBRAHON:

<!> Due For Calibration I







OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12.200 dpm 03/01/00 8,530 cpm

PX 726 C14 48,780 dpm 01/21/08 18,660 cpm

Efficiencies from last cal .:


Tc ss: 20.49% C14: 6.85% Tc Ni:


HV /Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): ITc-99 Source Response Nickel (CPM): Response (CPM): I Stainless Steel {CPM):

!Net Elf. B ch. I Net Elf. I

Ach. B ch. Ach. A ch. Bch. A ch. B ch. I Net Eff. 775/3.13 6423 I 443 34.71%1 1 47 0 l 3736 21 .34%


5.8% <1%

Pu239 ~ ~ !h.:ill Sr90 C-14

AF CPM: 6423 3736 5157 3973 3641

AF 4 pi eff: 34.71% 21 .34% 30.87% 43.39% 7.37%

AF2 pi eff: 68.54% 34.18% 63.11% 62.07% 19.26%


Note: If the os found data 1s Wlthon 10'k of the last calibratiOn and the B·A Xtalk IS <1% and the A-B X\alk IS <1 0%, then the techniCian may N/A \he plateau see11on and go d~tectly to remarks

~~f(~. ... \~ N r · .,, •. t;: ~~g· ...

GRIFFIN INSTRUMENTS

PROBE#: PR164051 Date: 08/03/12


I HV I Vernier: Tc-99 Source Response Pu-239 Sour~e Background (CPM): Net A to B B toAXtalk: Response (CPM): SS (CPM)·

I

A ch. B ch. Net Eff. A ch . B ch. I Net Elf. Ach.

NIA

Alpha I Beta Bkg (cpm) 47 HV I Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230

775 I 3.13 CPM: 6423 3738 5157



REMARKS:


G) Yes

0 No

0 No Calibration Sticker Al1ached?:

Date Instrument is Due For Next Calibration: 08103113



Xtalk: <10% <1%

8 ch.

C-14 Sr-90

3641 3973

7.37% 43.39%

19.26% 62.07%

Entered by: C-q;~ Initials

I

2 pi officionc:ios donotod in italics . C~librationa parfonnod to ANSI N323A-1997 sundardo.

2

GRIFFIN INSTRUMENTS


- --·---------DATE: 09/08111

TECH: E.M. Glenn 1

I -

2929 SERIAL#

LOCATION:

149124 06-00152

Griffin lnst


Reason For Calibration: • Due For Calibration Repair (See Remarks)

CABLE LENGTH: 39" Other (See Remarks) Due and Repair (See Remarks) _ ___:_ __ _ NIST TRACEABLE EQUIPMENT USED DURING CALIBRATION



Condition: • · Sat -.

• . Unset M Mechanical Zero: 0


Scaler Function Che~ .


Alpha Channel Window (175 mV. 120 for 3030):

Alpha Counts w/P~Iser@ 10.000 CPM:

Beta Counts w/Pulser@ 1 0.000 CPM:

4-48

180

9.975

9.977

HIGH VOLT !>-GE POWER su'Pi_ Y-CAL (2~29 on_ly),


Max HV (1500 V +): • Sat ,

REMARKS:

-Does Instrument Meet Final Ac~ptance Criteria?: • Yes No

Calibration Sticker Attached?: • Yes No

Date Instrument is Due For Next Calibration: 09/08112



-------·-----------

As left

A. F.

A. F.

AF.

A. F.

A. F.

Unset

%Erro r: 03%

%Error: 0.2%

Entered by: e':t:. Initials

Calibrations performed to ANSI N323A-1997 standaras.

GRIFFIN INSTRUMENTS

PROBE#: PR156596

Date: 09108111


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM}: Net A to B B to A Xtalk: I . SS (CPM): Response (CPM): Xtalk: <10% <1%

Ach. B ch . Net Eff. Ach. B ch. J Net Eff. A ch. B ch.

N/A

----··------------- ··-····-------------··--·--- --·-··-··-·

Alpha I Beta Bkg (cpm) 0 58 HV I Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

825/3.42 CPM: 6749 4742 5604 5671 4156



REMARKS:

Does Instrument Meet Final Acceptance Criteria?: • Yes No

Calibration Sticker Attached?: • ; Yes No



Performed/Reviewed by: Date: 9/8/2011 Entered by: ~ Initials


2

GRIFFIN INSTRUMENTS

CALl BRA TION CERTIFICATE FOR 43-10-1 PROBE#

Owner: DENUKE

DATE:

TECH:

i

09/08/11

E.M. Glenn

LOCATION:



PR156596

Griffin lnst

07/05/11

~~ Due For Calibration ' ' Repair {See Remarks) ~ Other (See Remarks) ·= l Due and Repair



MODEL: 2929

Source Number

OOTC470-0654

2697-00

PX726

2696-00

94TH470-1593

SERIAL#: 149124


Isotope

Tc99 ss Sr90

C14

Pu239

Th230

4 pi Activity

17,300 dpm

12,200 dpm

48,780dpm

18,500 dpm

16,700 dpm

-------

CAL DUE:

Assay Date

06/15/09

03/01/00

01/21/08

12/02/09

06/16/09

09/08/12

2 pi Activity

10,800 cpm

8,530 cpm

18,660 cpm

9,370 cpm

8,170 cpm


Condition: .. Sat ~~ Unsat Pu: ; 36.68%1 Th: j 34.77%1

Tc ss: ! 27.10%1 C14: 1 11.04%1 Tc Ni: jL - - --'


Tc-99 Source Response '! Pu-239 Source~·-· Background (CPM): ___ I, Nickel (CPM): Response (CP,M):

1

!A ch. ! B ch. fNetEtf1-ACil':l~ NetEffT

HV I Vernier:

=::==.8..,..2_5-_,-3~._4-~-_-L_ I_ 6749

1 Net A to B 1 B to A Xtalk: Xtalk: <10% <1%

3.4% <1%

AFCPM: 5749 ~'---

4742 5604 4156 5671 -, -----, L--------~__...;

-------~. 36.48% AF 4 pi eff:

·-·--- -27.08% 33.56% __j 44.31% 11.51%

AF 2 pi eff: 72.03% ; I -- _j 43.37% 68.59% !6£37% - 30.08%

Is as found efficiency within 20% of the efficiency from the last cal? - ~ Yes _. No (See Remarks)

Note: If the as found data 1s with1n 1 0'.4 of the last calibrat ion and the B-A Xtalk IS <1% and the A-8 Xtatk is <1 0%, then the technician may NIA the plateau se::lion and go directly to remarks.

GRIFFIN INSTRUMENTS


2929 SERIAL# 149124 06-00152




CABLE LENGTH: 39"

0 Due For Calibration

~ Other {See Remarks)






Condition: ~ Sat 0 Unsat AF Mechanical Zero: 0






Beta Counts w/Pulser@ 10,000 CPM:

HIGH VOLTAGE POWER SUPLY CAL (2929 only)


As Found As Left

4-49 A. F.

180 A.F.

9,986 A. F.

9,988 A. F.

A. F.

Max HV {1500 V +): ~ Sat 0 Unsat

REMARKS: Probe repair.






~ Yes

~ Yes

06113/13

0 No

0 No

# PR156596

Date: 6/13/2012

%Error: 0.1%

%Error: 0.1%

Entered by: ~tE.. Initials

Calibrations performed to ANSI N323A-1997 standards

GRIFFIN INSTRUMENTS


2929 SERIAL# 149124 06-00152


TECH: Joanne Glenn DATE LAS~ CAL EXPIRES: 06/13/13

@ Due For Calibration 0 Repair (See Remarks) Reason For Calibration:









Alpha Channel Window (175 mV, 120 for 3030) :





As Found

4-48

173

9.952

9.952

0.995

As Left

A. F.

A.F

A. F.

A. F.

A. F.

Max HV (1500 V +): (!) Sat 0 Unsat

REMARKS:

Does Instrument Meet Final Acceptance Criteria?·

Calibrallon Sticker Attached?:

Date Instrument is Due For Next Calibration.


Performed/Reviewed by :

(!) Yes

@ Yes

04/27/14

0 No

0 No

# PR156596

Date: 4/27/2013

%Error: 0.5%

"!.Error: 0.5%

Entered by:~lnitlals

Cahbn>!>c~ performeo 10 ANSI N32JA-1997 standards

GRIFFIN INSTRUMENTS


Owner: OENUKE

DATE: LOCATION:

TECH:

04/27/13


Gri ffin lnst

06/13/13


0 Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) C!J Due and Repair






OOTC470-0654 Tc99 SS 17.300 dpm 06/15/09 10.800 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500dpm 12/02/09 9,370 cpm

2697-00 Sr90 12.200 dpm 03/01/00 8.530 cpm

PX 726 C14 48,780dpm 01121108 18,660 cpm


Condition: ~_.. Sat 0 Unsat Pu: 33 77% Th: 30.38% Sr: 41 .34%

Tc ss: 26.06% C14: 11.59% Tc Ni:


HV / Vemier: Tc-99 Source Response Pu-239 Source Nickel (CPM): Response (CPM) :

Background (CPM): Tc-99 Source Response Stainless Steel (CPM):

Ach B ch Net Eft. A ch. _ B ch . 1 Net Elf.

340 ,34 .29%

A ch. B ch. A ch. B ch. r Net Eff.

4669 26.66% 850/3 45 6344 56

Net A to B B to A Xta lk: Xtalk: <10% <1%

4.3% <1%


AF CPM: 6344 4669 5138 3693 5824

AF 4 pi eff: 34.29% 26.66% 30.76% 40.85% 11.82%

AF 2 pi eff: 67.69% 42.71% 62.88% 58.43% 30.91%

Is as found efficiency within 20% of the efficiency from the last cal? (~ Yes C No (See Remarks)

Note If tne as found data,. w.tn•n 10'4 of tno last cahbfallon anc tne S-A X talk •S <1 % and the A·B Xtalk os <IO'Yo rlten me tec71noctan may NIA the pta:eau sec;,on and go d1rec:1y to remarks

GRIFFIN INSTRUMENTS

PROBE#: PR156596 Date: 04/27/13

PLATEAU AND SET POINT DATA I I HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B B to AXtalk:

SS (CPM): Response (CPM): Xta lk: <10% <1%

A ch. B ch . Net Eft. A ch. B ch. I Nel Eft. A ch. B ch.

N/A


850/3.45 CPM: 6259 4632 4856 5478 3787

4 piAL Efficiencies: 33.83% 26.40% 29.08% 11 .10% 41.81%


REMARKS: Replaced broken tube holder.

Does Instrument Meet Final Acceptance Criteria?: (!J Yes

@ Yes

0 No

0 No Calibration Sticker Attached? ·



Perfonned/Reviewed by: Date: 4/27/2013 Entered by:~lnitials

2 pi efficiencies denoted in italies. Colibratiom• performed to ANSI N323A-1997 standards.

2

GRIFFIN INSTRUMENTS

PROBE#: PR156596 Date: 06/13/12


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): I

Net A to B B toAXtalk: SS (CPM): Response (CPM): Xtalk: <10% <1%

Ach. B ch. Net Eff. Ach. B ch. I Net Eff. Ach. B ch.

775/3.20 0 4289 24.5% 5789 357 31 .3% 0 51 5.0% <1%

800/3.29 0 4443 25.4% 6103 323 33.0% 0 43 4.4% <1%

825/3.38 0 4644 26.6% 6222 336 33.6% 0 50 4.4% <1%

850/3.45 0 4553 26.0% 6298 310 34.0% 0 51 3.9% <1%

875/3.54 0 4713 27.0% 6550 303 35.4% 1 47 3.8% <1%

900/3.67 1 111

Alpha I Beta Bkg (cpm) 51 HV /Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

850 I 3.45 CPM: 6248 4559 5074 5703 3806

4 pi AL Efficiencies: 33.77% 26.06% 30.38% 11.59% 41 .34%


REMARKS: Tagged out "Torn Mylar". Replaced mylar. Replaced missing drawer spacer strip and missing knob.






(!) Yes

@ Yes

06/13113

0 No

0 No

# 149124

Date: 6113/2012 Entered by: c!'Cf. Initials

I

2 pi efficiMcies denoted In Italics. Calibration& performed to ANSI N323A·1997 s~ndards.

2

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE: 08/04112

TECH: Joanne Glenn

2224 SERIAL#

LOCATION:

119809 06-00134

Griffin Ins!


Reason For Calibration: (!) Due For Calibration ~ Repair (See Remarks)


NIST TRACEABLE EQUIPMENT USED DURING CALl BRA TION



CONDITION: Worn AF MECHANICAL ZERO:

NEW BATTERIES: 0 Yes (!) No

HV (+/-10%1 AS FOUND HV AS LEFT HV

A. F. 500 V: 500

1000 V: 1000 A. F.

1500 V: 1500 A. F.

RATE METER

0 AL MECHANICAL ZERO: 0

BATTERY CHECK: Sat

WINDOW SETTINGS: A.F. A.L.

BT (3.5 mV +/- 1 mV): 3.5 A. F.

BW (30 mV +/-3 mV): 30 A. F.

AT (120 mV +/-10 mV): 120 AF.

SCALER SCALE RATE CPM AS FOUND % ERROR AS LEFT % ERROR AS FOUND % ERROR AS LEFT % ERROR

x.1 or x1 100 100 0.0% A. F.

250 250 0.0% A. F.

400 400 0.0% A.F.

x1 or 1000 1000 0.0% A. F. x10 2500 2500 0.0% A. F.

4000 4000 0.0% A. F.

x10 or 10K 10 K 0.0% A. F. x100 25K 25 K 0.0% A. F.

40K 40 K 0.0% A. F.

x100 or 100K 100 K 0.0% A. F. x1000 250K 250 K 0.0% A. F.

400K 400 K 0.0% A. F.

Overload Light:


@ Adjusted 0 Not Adj.

REMARKS:





PerformediReviewed by:

(!) Yes

(!) Yes

08104113

# PR130517

Date: 814/2012

250 I

(!) Yes

0 No

0 No

0.0% I A.F. I

0 No

Entered byEr__lnitials


GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

43-89

LOCATION:

PROBE# PR130517 06-00141

TECH:

08/04/12


Griffin lnst

09/09/12


<!> Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair



MODEL: 2224 SERIAL#: 119809 CAL. DUE: 08/04/13 - -



OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8.170 cpm

2696-00 Pu239 18,500dpm 12/02/09 9,370 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530cpm



Tc ss: 12.44% C14: TcNi: ·


HV /Vernier: Tc-99 Source Response Pu-239 Source Nickel (CPM): Response (CPM):

• • L:,

Background (CPM): rTc-99 Source Response Stainless Steel (CPM):

A ch . 8 ch. 1Net Eft. A ch. j B ch. j Net Eft.· A ch. B ch. . A ch. -- B ch. [Net Efi [ _1 0 . , 2338 .12.03% 900 /N/A . [_3373 l 413 j18.23%[ o - 1 256

Net A to B B to AXtalk: Xtalk: <10% <1%

4.4%

f.!!ill ~ Tc99 ss Th-230 §!22 £:.1!

AFCPM: 3373 2338 2785 2659

AF 4 pi eff: 18.23% 12.03% 16.68% 26.56%

- -AF 2 pi eff: 36.00% 19.28% 34.09% 37.99%


Note: If tne as found data •• Wtthtn 10".4 of the last cahb<abon and the B·A Xtalk is <1'4 and the A-B Xtalk is <10'4. then the technician may N/A the plateau section and go d~rea ly to remarl<s

GRIFFIN INSTRUMENTS

PROBE#: PR130517 Date: 08/04/12


I HV I Vernier: Tc-99 Source Response 9u-239 Source Background (CPM): Net A to B B to AXtalk: SS (CPM): Response (CPM): Xtalk: <10% <1%

A ch. B ch. Net Eff. Ach. B ch. 1 Net Eff. Ach. B ch .

N/A


900 / N/A CPM: 3373 2338 2785 2659



REMARKS: As found off scale - replaced mylar.


@ Yes

0 No




Perfonmed/Reviewed by: Date: 8/4/2012 Entered by:.£.__1nitials

2 pi effi~ion~les denoted In italics. Calibrations performed to ANSI N323A·1 997 standards.

2

I

#/4 GRIFFIN INSTRUMENTS


Owner: DENUKE

2224 SERIAL# 119809 06-00134

DATE: 04/26113 LOCATION: Griffin lnst

TECH: 1 E M Glenn DATE LAST CAL EXPIRES: 08/04113

I Reason For Carbration: 1!' Due For Calibration Repair (See Remarks)

,) Other (See Remarks I ,·) Due and Repair (See Remarlls)


MODEL: M-500 SERIAL#: 114512 CAL DUE: 09126/13

:.1 Audio Response !;.!, Geotropism CABLE LENGTH: 39"

CONDITION: Sat AF MEC~ANICAl ZERO: 0 AL MECHANICAl ZERO: 0

NEW BATTERIES: Yes ; No BATTERY CHECK: Sa!

HV {+/-10%} AS FOUND HV AS l EFT HV WINDOW SETTINGS. A. F. A.L .

500 V: 500 A.F. BT (3.5 mV +/- 1 mV): 35 A.F

1000 V: 10CO AF BW (30 mV +/-3 mV): 30 A.F

1500 V: 1500 A.F AT (120 mV +/-10 mV): 120 A.F

RATE METER SCALER SCALE RATE CPM AS FOUND %ERROR AS LEFT %ERROR AS FOUND %ERROR AS LEFT % ERROR

x.1 or x1 100 100 00% A. F. f-

250 250 0.0% AF

400 400 00% AF

x1 or 1000 1000 0.0% AF x10 2500 2500 00% AF

4000 4000 0.0% A.F

x10 or I 101( 10 K 00% AF x100 25K 25 1< 00% .AF

40K 40 K 00% A.F

x100 or ·100K 100 ~ 00% A.r x1000 2.SOK 250 ~ 0 0% AF

400K 400 K 0.0% AF .


Overload Laght: o";, AdjUSted ·"" Not Adj

REMARKS




•NSTRUMENT MARRIED WITH 43-89

Performed/Reviewed by: t9.01L ~l.~.,~e

:~ Yes

• .!. Yes

04126/14

t: PR130517

Date: d/2e12013

250 I 00% I AF. I

. . :;,

""

..:•

.:;t· Yes ) No

No

Enhored by: c.if'i,;: Initials

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

04/26113

EM. Glenn

LOCATION :


Griffin tnst

08/04/13

REASON FOR CALl BRA TION:

(: Due For Calibratjon 0 Repair {See Remarks) 0 Other (See Remarks) (!; Due and Repair


NIST TRACEABLE EQUIPMENT AND STANDARDS USED DURING .CALIBRATION





94TH470-1593 Th230

2696-00 Pu239

2697·00 Sr90

Condition: (!) Sat 0 Unsat

As Found {AF) Efficiencies:

HV I Vernter·

900 I NIA

AFCPM:

AF 4 pi eft:

AF 2 pi eff:

Tc-99 Source Response Nickel (CPM):

A ch. B ch. Net Eft.


17.300 dpm 06/1 5/09 10.800cpm

16,700 dpm 06/1 6109 8,170 cpm

18,500 dpm 12/02/09 9.370 cpm

12.200 dpm 03/G l/00 8.530 cpm


Pu: 18.23% Th: 16.66% Sr: 26 56%

Tc ss: 12 03% C14: Tc Nl:


Background (CPM)· Tc-99 Source Response Stainless Steel (CPM)

A ch. B ch. Net Elf Ach. B ch. A ch. B ch, Net Eft

Net '' to B B to A Xtaik· Xtalk: <1 0% <: 1%

Is as found efficiency within 20% of the efficiency from I he last cal? 0 Yes (!) No (See Remarks)

Note 1f tne as l:>und da~a os wrthon 10% of tne last C<llollrat>on and the 8-A Xtall< os <1% anc toe A-8 Xtallc os <10%. then the '""""'c .. r. may N/A tne plateau oectKJn and go d•tcctty to rcrn-afks

GRIFFIN INS1RUMENTS

PROBE#: PR130517 Date 04125113


I HI/ I Vermer i Tc-99 Sour;;e Response 1 SS fCPM)

Pu-239 Sour~e Response 1CPMl.

! Background (CPM)· Net A to B I B to A Xtalk. I Xtalk : <10% <1% J

,__A_c_h _ _._ I_B_ch __ _,_IN_e_t __ E_tt ...... f_ A_c_h __ _:. r,_B_ch___,- 1,_1'.:~ cff. ! A ch. 1 B ch.

7 ~579 ls.4~ 3~1~ i :il:l rr1, 4% 11=- 1

6 200b 106% r-33s!: 4ss~£!:J%j 2

800

825

850 8 2421 12.7% 3544 53ti 191°/., 3 ···-- --

. .-._,_

Alpha I Beta Bkg (cpm) 1 217 HV /Vernier Pu-239 Tc-99 Ni lc-99 SS

850 I NJA CPM: 3544 2421

4 pl Al Effic iencies: 19.14% 12.74%

2 piAL Efficiencies: 37.79% 20.41%

REMARKS. A F off scale Replaced mylar

Does Instrument Meet Final Acceptance Criteria?. @ Yes

~ ~~ Yes

0 No

Calibration Sticker Attached?; :_) No



Performed/Reviewed by: Oate: 4/26/2013

2 pi effit 1oncie-s denoted in ibJies.

2

126 7.3% <1%

~72 8.5% <1%

217 8 .2% <1%

~ C-14 Sr-90

2745 2729

16.42% 28.21%

33.56% 40.35%

Entered by:_ cz!'C: Initials

Calibration• performed to ANSI N32;)A-1g,7 slilndords.

GRIFFIN INSTRUMENTS


DATE: 09/08/11

TECH: E.M. Glenn

2929 SERIAL#

------- ---- -----LOCATION:


I

167850 06-00154

Griffin lnst

08/17/10

Reason For Calibration: . , Due For Calibration Repair (See Remarks)

CABLE LENGTH: 39" Other (See Remarks) Due and Repair (See Remarks)




Condition: · ! Sat ~~ Unset AF Mechanical Zero: 0


Scaler Function' Check -


Alpha Channel Window (175 mY. 120 for 3030):

Alpha Counts w/Pulser@ 10.000 CPM:·

Beta Counts w/Pulser @ 1 0.000 CPM:

As Found

4.2-50

175

10.000

10.001

HIGH VOLTAGE P._OWER SUPL '(C:AL (2929 only) .. '

1 KV Reeding (R-5 on HV Board):

Max HV (1500 V •): • Sat _

REMARKS:

Does Instrument Meet Final Acceptance Criteria?: · • Yes No

Calibration Sticker Attached?: · • Yes No




As Left ·

A. F.

A. F.

A. F.

AF.

A. F.

Unse.t

%Error: 0.0%

%Error: 0.0%

Entered by: c'?G...Initials

Calibrations performed to ANSI N323A·1997 st;lndards

GRIFFIN INSTRUMENTS


Owner: DEN U KE ---· ---- --·

DATE:

TECH:

09/08/11

EM. Glenn

' • · Due For Calibration

CABLE LENGTH: 39"

LOCATION:



' Repair (See Remarks) Other (See Remarks)

INPUT SENSITIVITY: dual

Griffin lnst

08/17/10

' ' Due and Repair




Source Number Isotope 4 pi Activity Assay Date 2 pi Activity OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

2697-00 Sr90 12,200 dpm 03/01/00 8,530 cpm

PX726 C14 48,780 dpm 01/21/08 18,660 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm


Condition: .. Sat Unsat Pu: 36.72% Th:' 34.62%! Sr: l 43.09%,

Tc ss:· 26.04%1 C14: 10.58%1 Tc Ni: 1

---~


~-----,.------,---,.----~ ~--· ----HV I Vernier: 'Tc-99 Source Response Pu-239 Source Background (CPM): Tc-99 Source Response I

..---:.---1 850/3.44

AF CPM:

AF 4 pi eff:

AF 2 pi eff:

1 i Nickel (CPM): Response (CPM): Stainless Steel (CPM): '

J A ch. ll B c~~L A ch. 1 B ch. Net EffJ A ch_:_-,------r--,--'+----c~:-+Net Eft. j i r , 1 . 6693 _ 423 36.18%r o 124.90%~

Net A to B I B to A Xtalk: ~

Xtalk: <10% <1% --- - <1%~ 5.2%


-·----- - -··-·-, [5356~ 6693 4365 5543 4011

- --- ------36.18% t____ ___ 24.90% 33.19% 42.74% 10.86% -----

------. - --- r 71.43% 39.88% 67.85% 61.13% 28.39% -----· ~------~..i --·----- ---· -

Is as found efficiency within 20% of the· efficiency from the last cal? -• Yes No (See Remarks)

Note· If the as found data is Within 10% of the last calibration and the B·A Xtalk is <1% and the A·B Xtalk IS <10%. then the ted'IOJC!an may N/A the plateau se::i1on an d go directly to remarks.

·~;s§~t(" .. ~~ ~ ~ ·~1 ... ' -\ ,l_. . ,. ~9'.s .

GRIFFIN INSTRUMENTS

PROBE#: PR174808 Date: 09/08/11


I HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B I B to A Xtalk/ I SS (CPM): Response (CPM}: Xtalk: <10% <1%

A ch . j B ch . jNet Eff. A ch. I B ch.l Net Eff. Ach. I B ch.

750/3.04 0 3089 17.7% 6262 443 33.8% 0 28 6.2% <1%

800/3.24 0 3692 21 .1% 6569 412 35.5% 1 44 5.3% <1%

825/3.38 1 4014 22.8% 6516 403 35.2% 0 68 4.9% <1%

850/3.44 1 4252 24.3% 6691 424 36.2% 0 50 5.3% <1%

875/3.50 0 135

--·----Alpha I Beta Bkg (cpm) 0 68

HV /Vernier Pu-239 Tc-99 Ni Tc-99 ss Th-230 C-14 Sr-90

825/3.38 CPM: 6516 4014 5345 4860 3885

4 pi Al Efficiencies: 35.22% 22.81% 32.01% 9.82% 41 .27%


REMARKS:

Does Instrument Meet Final Acceptance Criteria?: ·• • Yes ' • No

Calibration Sticker Attached?: '..! ' Yes No



Performed/Reviewed by: Date: 9/8/2011 Entered by: ce'C:: Initials


2

GRIFFIN INSTRUMENTS


2929 SERIAL# 167850 06-00154




CABLE LENGTH: 39"


(!) Other (See Remarks)




MODEL: M-500 SERIAL#: 114512 CAL DUE: 08/24/12


Condition : (!) Sat 0 Unsat AF Mechanical Zero: 5







HIGH VOLTAGE POWER.SUPLY CAL. (2929 only)


As Found

4.2-50

180

9,996

9,997

0.975

As Left

4-50

175

A. F.

A. F.

Max HV (1500 V +): @ Sat 0 Unsat

REMARKS: Probe repair. Replaced missing time select knob.


Calibration Sticker Attached? :




(!) Yes

(!) Yes

06/13/13

0 No

0 No

# PR174808

Date: 6/13/2012

"'o Error: 0.0%

"'o Error: 0.0%

Entered by: etC! Initials

Calibrations performed to ANSI N323A·1997 standards

GRIFFIN INSTRUMENTS


owner: DENUKE

DATE: LOCATION:

TECH:

06/13/12


Griffin lnst

09/08/12


REASON FOR CALIBRATION: I (!) Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair




----NIST TRACEABLE SOURCES USED


OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm

2696-00 Pu239 18,500 dpm 12/02/09 9,370 cpm

2697-00 Sr90 12.200 dpm 03/01/00 8,530 cpm

PX 726 C14 48,780dpm 01/21/08 18,660 cpm



Tc ss: 22.81% C14: 9.82% Tc Ni:


HV I Vernier: Tc-99 Source Response Pu-239 Source ' Nickel (CPM): 1 Response (CPM):

Background {CPM):

ITc-99 Source Response Stainless Steel (CPM):

A ch. B ch. l Net Eff." A ch. I B ch.I Net Eff.··

I _. J , I I A ch. B ch. A ch. - 8 ch. rNet Eff. I -, t· ; 825 I 3.38

Net A to 8 8 to A Xtalk: Xtalk: <10% <1%

AFCPM:

AF 4 pi eff:

AF 2 pi eff:


Nota If tho as found data is wilhin 100.4 of the last calibration and the B·A Xtall< os <I% and the A-B Xtalk is <10%. then the technician may N/A the plateau section and go direct ly to remarks.

GRIFFIN INSTRUMENTS

PROBE#: PR174808 Date: 06/13/12


l HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Net A to B B to AXtalk: SS (CPM): Response (CPM):

Ach. B ch. !Net Eff. Ach. B ch. I Net Eff. Ach. B ch.

775/3.17 0 3684 21 .0% 6294 222 34.0% 0 46

800/3.29 1 3979 22.7% 6341 231 34.3% 0 55

825/3.39 0 4204 24.0% 6350 200 34 .3% 2 48

850/3.50 0 4542 26:0% 6700 211 36.2% 0 46

875/3.58 0 4369 24.9% 6674 253 36.1% 1 55

900/3.70 0 82

-- -

Alpha I Beta Bkg (cpm) 48 HV /Vernier Pu-239 Tc-99 Ni Tc-99 SS Th-230

850/3.50 CPM: 6589 4417 5507

4 ·piAL Efficiencies: 35.61% 25.25% 32.97%

2 pi AL Efficiencies: 70.31% 40.45% 67.39%

REMARKS: Turned in due to erratic response. Replaced torn mylar and damaged scintillator.






(!) Yes

(!) Yes

06/13/13

0 No

0 No

# 167850

Date: 6/1312012

Xtalk: <10% <1%

2.7% <1%

2.7% <1%

2.3% <1%

2.4% <1%

2.9% <1%

C-14 Sr-90

5500 3856

11.18% 41 .92%

29.22% 59.96%

Entered by: c f'C?. Initials

I

2 pi efficiencies denoted In italics. Calibrations petfonned to ANSI N323A·1997 standards.

2

GRIFFIN INSTRUMENTS


2929 SERIAL# 167850 06-00154

DATE: 04/26/13 LOCATION : Griffin lnst

TECH: Joanne Glenn I DATE LAST CAL EXPIRES: 0611 3/13

~ Due For Calibration 0 Repair (See Remarks) Reason For Calibration :



MODEL: 500-2 SERIAL#: 284951 CAL. DUE: 01 /07/14

MODEL: SERIAL#: CAL DUE :

Condition: ~ Sat 0 Unsat AF Mechanical Zero: 0


Sealer Functlon Cheek

Beta Channel Window (4·50 mV):

Alpha Channel Window (175 mV, 120 for 3030) :





As Found As Left

4-49 A. F.

170 A.F

9,929 A.F.

9,929

0.980 A .F

Max HV (1500 V +): (!) Sat 0 Unsat

REMARKS.

Does Instrument Meet Final Acceptance Criteria?·

Calibration Sticker Attached?·

Date Instrument is Due For Next Calibration



(!) Yes

@ Yes

04/26/14

0 No

0 No

# PR174808

Date: 4/26/2013

%Error: 0.7%

%Error: 0.7%

E.ntered by:~lnitials

Cnl ocratoo~s pe!iormed :o ANSI N32".A l 997 slan<lards

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

I

04/26/13

Joanne Glenn LOCATION: Griffin lnsl


REASON FOR CALIBRATION: C!l Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair





Source Number Isotope OOTC47Q-0654 Tc99 SS

94TH470-1593 Th230

2696-00 Pu239 2697-00 Sr90

PX 726 C14



4 pi Activity

17.300 dpm

16.700 dpm

18,500 dpm

12,200 dpm

48.760 dpm

Pu:

Tc ss:

Assay Date

06/15109

06/16/09

12/02/09

03/01/00

01/21/08

2 pi Activity


35.61% Th: 32.97%: Sr:

25.25% C14: ' 11 .18%' Tc Ni:

10.800 cpm

8.170 cpm

9.370cpm

8.530 cpm

18.660 cpr:n

41.92%

HV /Vernier: Tc-99 Source Response Pu-239 Source Background (CPM): Tc-99 Source Response Stainless Steel (CPM):

850/3.50

AF CPM:

AF 4 pi eft:

AF 2 pi eft: ·

Nickel (CPM): Response (CPM):

A ch . - Bch.- [Net Eft:- -.c.. ch. Is ch. L-Net Eft. A ch. B ch.

r j • --'--64-95 . • --- • 204 ..1!35.11% 0 66

Net A to B BtoAXtalk: Xtalk: <10% <1%

2.1% <1%

Pu239 Tc99 Ni Tc99 ss Th-230 Sr90

6495 4355 5295 3780

35.11% 24.79% 31 .71 ~. 41.72%

I 69.32% 39.71% 64.81% 59.66%

A ch . ·a C'h. fN!t Eff.

0 4355 24.79%

~

4974

10.06%

26.30%


N0111. ~ the as found data ~ Wlthtn 10% of tho last c.ahbrahon and the B·A Xla!lo. 1$ <1% and the A-B Xla~k 1S <10%. then tne ~ecr.n•oan may NIA In& plateau sect•cm and go d1rodfy to romarks

GRIFFIN INSTRUMENTS

PROBE#: PR174808 Date 04/26/13


HV I Vernier: Tc-99 Source Response Pu-239 Source Background (CPM)· Net A to B B to AXtalk· SS (CPM): Response (CPM):

Ach. B ch Net Eff. A ch . B ch. I Net Eff. Ach.

NIA

Alpha I Beta Bkg (cpm) 0 66 HV /Vernier Pu-239 Tc-99 Ni T10-9~ s~ Th-230

850 / 3.50 CPM: 6495 4355 5295

4 piAL Efficiencies: 35.11% 24.79% 31 .71%

2 piAL Efficfencies: 69.32% 39.71% 64.81%

REMARKS:


@ Yes

04/26/14

0 No

0 No Calibration Sticker Attached?·




Xta lk: <10% <1%

B ch.

C-14 Sr-90

4974 3780

10.06% 41 .72%

26.30% 59.66%

Entered by:.q2._tnltials

I

2 p i efficiencies denoted In llallc s.. Calibrations performed to ANSI N323A·1997 standards.

2


2800 Solway Road

Knoxville, TN 37931


Calibration Certificate for LV-1,Serial # 003872, Bar Code# ,Prope?y # SEC-7373

Date: 05/09/13 Jeffrey Knight

SEC-IS-409 Rev 3

Location: 9999.

Date Last Cal. Expires: 10/30/13 j Technician :

Reason For Calibration: Due for Calibration


MODEL: D-812 V.2 SERIAL#: 3531 CAL. DUE: 11/20/13

MODEL:

AS FOUND OAT A



SERIAL#:

AF Physical Condition SAT

60 LPM

60 LPM

CAL DUE:

AS LEFT DATA

As Left Instrument Flow Indication:

As Left Calibrator Flow Indication :

Unit of Measure: '~ LPM () CFM


y Are the lndi.vidual Counts Within 10% of the Average?


30.00 LPM 30.00 LPM 30.70 LPM

50.00 LPM 50.00 LPM 49.20 LPM

70.00 LPM 70.00 LPM 70.40 LPM

60 LPM

60 LPM

60.00 LPM

ERROR%

2.33% LPM

1.60% LPM

0.57% LPM




Air Sampler rotameter reading: 0 Use Manufacturers Indication (!) Use Corrected Marking :] N/A


~ Does Instrument Meet Final Acceptance Criteria? :;zj Calibration Sticker Attached?

Date Instrument is Due For Next Calibration: _GS/09/14 _

Perlo<med '''/#.- Re•lewed by' ~ D"e' s;;-f -13 Printed Name: ey n ght

5/9/2013 Page 1 of 1


2800 Solway Road

Knoxville, TN 37931



Date: 05/09/13 Date Last Cal. Expires: 08f15/13 Technician : Jeffrey Knight

SEC-IS-409 Rev 3

Location : 9999. Reason Fol Calibration: Due for Calibration

EQUIPMENT USED DURING CALIBRATION I

MODEL: D-812 V.2 SERIAL#: 3531 CAL. DUE: 11/20/13



As Found Instrument Flow Indication: 58 LPM As Left Instrument Flow Indication:

As Found Calibrator Flow Indication: 58 LPM As Left Calibrator Flow Indication:

Unit of Measure: <!J LPM .:J CFM




30.00 LPM 30.00 LPM 29.60 LPM

50.00 LPM 50.00 LPM 50.90 LPM

70.00 LPM 70.00 LPM 69.10 LPM

60 LPM

60 LPM

60.00 LPM

ERROR%

1.33% LPM

1.80% LPM

1.29% LPM

Air Sampler Setting 60.00 -' Is Error Within 10%?



Air Sampler rotometer reading: 0 Use Manufacturers Indication ~ Use Corrected Marking 0 N/A


~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

05/09/14 ate Instrument is Due For Next Calibration:

Pertormedby~· -H~~~~-------------- Reviewed by: ~Date: J~?-7J Printed Name:

519/2013 Page 1 of 1

Safety and Ecology Cor'fration sEc PROCEDURE

2800 Solway Road

Knoxville, TN 37931


Calibration Certificate for LV-1,Serial # 003873, Bar Code# ,Propettll y # SEC-7375

Date: 05/09/13 Date Last Cal. Expires : 06/26/13 Technician : Jeffrey Knight

SEC-IS-409 Rev 3

Location : 9999. Reason r or Calibration : Due for Calibration


MODEL: D-812 V.2 SERIAL#: 3531 CAL DUE: 11/20/1 3





60 LPM

60 LPM

~ Left Instrument Flow Indication :

As Left Calibrator Flow Indication:

Unit of Measure: ~ LPM 0 CFM

60 LPM

60 LPM



CALIBRATION DATA TARGET VALUE AIR SAMPLER READING CALIBRATOR READING ERROR%

30.00 LPM 30.00 LPM 30.60 LPM 2.00% LPM

50.00 LPM 50.00 LPM 49.50 LPM 1.00% LPM

70.00 LPM 70.00 LPM 70.20 LPM 0.29% LPM

Air Sampler Setting 60 .00 ~ Is Error Within 10%?

Reproducibility 60 LPM 60 LPM 60 LPM Average : 60.00 LPM


Air Sampler rotameter reading : 0 Use Manufacturers Indication (!) Use Corrected Marking 0 N/A


~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

05/09(14 Date Instrument is Due For Next Calibration :

Perto~od by.I!J;f!; Printed Name: y n1ght

Reviewed by:_-~.~~:.z....-=L=t-:_q::>.c.=----Date: Y!-/J

51912013 Page 1 of 1

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE: 09/09/11

TECH: E.M. Glenn

2224-1 SERIAL#

LOCATION:

DATE LAST CAL EXPIRES :

257959 09-00327

Griffin lnst

08/17/10

Reason For Calibration: •f!J Due For Calibration n Repair (See Remarks)

Other (See Remarks) (; Due and Repair (See Remarks)




CONDITION: Sat AF MECHANICAL ZERO: 0 AL MECHANICAL ZERO: 0

NEW BATTERIES: Yes ·! • No BATTERY CHECK: Sat

HV {+/-10%1 AS FOUND HV AS LEFTHV WINDOW SETTINGS: A.F. A.l.

SOOV: 500 A.F . BT (3.5 mV +/- 1 mV): 3.5 A.F.

1000 V: 1000 A. F. BW (30 mV +/-3 mV): 30 A.F.

1500 V: 1500 A. F. AT (120 mV +/-10 mV): 110 120

·RATE METER - : SCALER SCALE RATE CPM AS FOUND %ERROR AS LEFT %ERROR AS FOUND %ERROR AS LEFT% ERROR

x.1 or x1 200 200 0.0% A. F. 500 500 0.0% A, F. 501 I 0.2% I A. F. I 800 800 0.0% A. F. .,

x1 or 2000 2000 0.0% A. F. - -x10 ~

' .. 5000 5000 0.0% A. F. 0 -- . :..· .,

~ . -8000 8000 0 .0% A. F. ' . -

•.: : . / .~ . . -x10 or 20K 20 K 0.0% A. F. . ; '· ' .. c.· ·' " x100

. . . SDK 50 K 0.0% A. F. I .. ~ : . - -80K 80 K 0.0% A. F. . . ..

~ •·. : x100 or 200K 200 K 0.0% A. F. ., .. I

' ... •. x1000 50 0K 500 K 0.0% A. F. - ... ..

BOOK 800 K 0.0% A.F. ~'- . ;;-' ''•

Is the As Found Data Within 20% of the Set Point?: -~ · Yes

Overload Lig,ht: , . , Adjusted • • NotAdj.

REMARKS:


Calibration Sticker Attached?: ' ! 1 Yes No



Performed/Reviewed by: Date: 9/9/2011 Entered by: c?.'C · Initials

Calibrations performed to ANSI N323A-1997 stan<Sards.

GRIFFIN INSTRUMENTS


09-00328

I

Owner: DENUKE

DATE:

TECH:

09/09/11

Joanne Glenn



(!) Due For Calibration REASON FOR CALIBRATION: !

0 Repair (See Remarks) 0 Other.(See Remarks) 0 Due and Repair



MODEL,: 2224-1 SERIAL#: 257959 CAL. DUE: 09/09/12


Source Number Isotope 4 pi Activity Assay Date 2 pi_ Activity OOTC470-0654 Tc99 SS 17,300 dpm 06/15/09 10,800 cpm

94TH470-1593 Th230 16,700 dpm 06/16/09 8,170 cpm 2696-00 Pu239 18,500 dpm 12/02109 9.370 cpm 2697-00 Sr90 12,200 dpm 03/01/00 8.530 cpm


Condition: (!) Sat 0 Unsat Pu: 21 .93%1 Th:l 19.32%1 Sr: l 31 .76%j

Tc ss: l 14.62%1 C14: 1 Tc Ni:'--1 __ _____,


HV 1 vernier: lrc-99 Source Response I Pu-239 Source Background (CPM): Tc-99 Source Response I Nickel (CPM): Response (CPM): Stainless Steel (CPM):

Ach. I B ch. A ch. II B ch . !Net Eff.l I A ch. II B ch. INet Eff. A ch. _I B ch. j Net Eff.

L 650/N/A J I I 3993 l 424 ]21.58% 0 I 146 6 I 2n1 !15.17%1

Net A to 13 B toAXtalk: Xtalk: <10% <1%

6.5% <1%


AF CPM: 3993 I I I I 2771 II 3193 3251

AF 4 pi eff: 21.58% I I I I 15.17% "] [}i"i'io/.- 1 33.57%

AF 2pi eff: 42.61% I I I I 24.31% I I 39.08% 48.01%


Note: If the as found data is within 10% of the last calibration and the B·A Xtalk is <1% and the A·B Xtalk is <10%, then the technician may NIA the platoau section and go directly to rama11<s. •

GRIFFIN INSTRUMENTS

PROBE#: PR278242 Date: 09109111


HV !Vernier: Tc-99 Source Response Pu-239 Source i Background (CPM): NetAtoB B to AXtalk: SS (CPM): Response (CPM): Xtalk: <10% <1%

Ach. B ch. Net Eft. A ch. I B ch . l Net Eff. Ach. B ch.

NIA

Alpha I Beta Bkg (cpm) 0 146 HV I Vernier El!.:lli Tc-99 Ni Tc-99 SS Th-230 C-14 Sr-90

650 IN/A CPM: 3993 2771 3193 3251



REMARKS:


@ Yes

0 No


Date Instrument is Due For Next Calibration: 09109112

INSTRUMENT MARRIED WITH 2224-1 # 257959

Performed/Reviewed by: Date: 9/9/2011 Entered by:~lnitials

2 pi efficiencies denoted in lta.lica. Callbr.tlons perfonned to ANSI N32lA·1997 standards.

2

I

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE: 08123112

TECH: E.M. Glenn

2224-1 SERIAL# 257959 09-00327

----·-··--·--------------LOCATION: Griffin lnst

DATE LAST CAL EXPIRES: 09/09112


0 Other (See Remarks) 0 Due and Repair (See Remarks) ----NIST TRACEABLE EQUIPMENT USED DURING CALIBRATION

MODEL: M-500 SERIAL#: 134715 CAL. DUE: 04/16113


CO!I!DIT!ON: Sat

NEW BATTERIES:

HV {+/-10%)

500 V:

1000 V:

1500 V:

AS FOUND HV

x1 or x10

500

1000

1500

AF MECHANICAL ZERO:

0 Yes (!) No

AS LEFT HV

A. F.

A. F.

A. F.

0 AL MECHANICAL ZERO: 0

BATTERY CHECK: Sat

WINDOW SETTINGS : A. F. A.L.

BT (3.5 mV +/- 1 mV): 3.5 AF.

BW (30 mV +/-3 mV): 29 A.F.

AT (120 mV +/-10 mV): 120 A .F.

SGALER


Overload Light: (!) Adjusted 0 Not Adj .

REMARKS:




INSTRUMENT MARRIED WITH 43·93

cfC. Performed/Reviewed by: f9.®1L. ~~

@ Yes

(!) Yes

08/23/13

#PR278242

Date: 8/23/2012

0 No

0 No

Entered by: e(Cf. Initials

Calibrations performed to ANS! N323A-1997 standards.

GRIFFIN INSTRUMENTS


Owner: DENUKE

DATE:

TECH:

08123112

E.M. Glenn

LOCATION:


Griffin Ins!

09/09/12





MODEL: 2224-1 SERIAL#: 257959 CAL DUE: 08/23/13


Source Number !sotope


94TH470-1593 Th230

2696-00 Pu239

2697-00 Sr90



HVIVemier:

650 I NIA

AFCPM:

AF 4 pi eft:

AF2pieff:


A ch. B ch. I Net Eft:'. I .

Pu239 Tc99 Ni

3942

21.30%

42.06%

4 p1 Activity Assay Date 2 pi Activity

17.300 d?m 06115/09 10,800cpm

16,700 dpm 06/1 6109 8,170cpm

18.SOO dpm 12/02/09 9,370 cpm

12,200 dpm 03/01/00 8,530 cpm


Pu: 21.58% Th: 19.12% Sr: 33.57%

Tc ss: 15.17% C14: , , Tc Ni:


Background (CPM):

ITc-99 Source Response Stainless Steel (CPM):

A ch. 8 ch . I Net Eff.

3942 588 .. Z1 .30%J

A ch. B ch.

332

A ch. 8 ch. J Net Eff.

I 16 I 2875 14.70%

r-Iel A to 8 B toAXtalk: Xlalk: <10% <1%

5 .1% <1%

Tc99 ss Th-230 Sr90 C-14

2875 3194 3370

14.70% 19.1 2% 33.58%

23.55% 39.08% 48.03%

Is as found efficiency within 20% of the efficiency irom the last cal? (!) Yes 0 No (See Remarks)

Note: If the as found data is Within 10% oi the last calibra1ion and tl"-.c B·A Xtaik •s ..: ~ 0k. and the A-8 X talk lS '1 0%, then the technician may N/A the plateau section and gc d11ectly to remarks.

GRIFFIN INSTRUMENTS


HV / Vernier: Tc-99 Source Response Pu-239 Source Response Background (CPM): SS (CPM):

Ach. B ch. 1 Net Eff.

600 8 1159 6.1%

625 9 1769 9.3%

650 13 2305 12.5%

675 11 2748 14.9%

Alpha /Beta Bkg (cpm) 0 HV /Vernier Pu-239

675 / N/A CPM: 3870

4 piAL Efficiencies: 20.92% 2 piAL Efficiencies: 41.30%

REMARKS:




(CPM):

Ach. B ch. 1 Net Eft. Ach. I 2560 371 13.8% 0

3253 399 17.6% 1

3666 381 19.8% 0

3870 429 20.9% 0

i I 'I

171 Tc-39 Ni Tc-99 SS

@ Yes

@ Yes

08/23/13

2748

14.90%

23.86%

0 No

0 No

I

Th-230

3186

19.08%

39.00%

INSTRUMENT MARRIED WITH 2.224-1 #257959

Performed/Reviewed by : . Date: 8123/2012

B ch .

101

160

140

171

PROBE#: PR278242

Date: 08123112

Net A to 8 B to A XtaJk: Xtalk: <10% <1%

9.5% <1%

6.8% <1%

6.2% <1%

6.3% <1% ,

I I I

C-14 Sr-90

3103

32.41%

46.35%

Entered by: &Initials

2 pi cffidencfe& OOnotod in italics. Colllbrations perfOrmed to ANSI N323A·1 '~7 standards.

2

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Ff .11

GRIFFIN INSTRUMENTS


Owner: DENUKE --~

DATE: I 08/23/1 2

2224-1 SERIAL#

LOCATION:


257959 09-00327

Griffin lnsl

09/09/12 TECH: I E.M. Glenn

Reason For Calibration: @ Due For Calibration 0 Repair (See Remarks)

0 Other (See Remarks} 0 Due and Repair (See Remarks) __ ;;;:.__


MODEL: M-500 SERIAL#: 134715 .CAL. DUE: 04/16/1 3


CONDIT! ON: Sat AF MECHANICAL ZERO: 0 AL MECHANICAL ZERO: 0

NEW BATTERIES: 0 Yes @ No BATTERY CHECK: Sat

HV (+/-10%} AS FOUND HV AS LEFTHV WINDOW SETTINGS: A.F. A.L.

500 V: 500 A.F. BT (3.5 mV +/- 1 mV): 3.5 A.F.

1000V: 1000 A. F. BW (30 mV +/-3 mV): 29 A. F.

1500 V: 1500 A. F. AT (120 mV +/-10 mV): 120 A. F.

RATE METER -SCALER SCALE RATE CPM AS FOUND %ERROR AS LEFT % ERROR AS FOUND % ERROR AS LEFT% ERROR

x.1 orx1 200 200 0.0% A. F.

500 500 0.0% A. F.

800 800 0.0% A. F.

x1 or 2000 2000 0.0% A. F. x10 5000 5000 0.0% A. F.

8000 8000 0.0% A. F.

x10 or 20K 20 K 0.0% A. F. x100 50K 50 K 0.0% A. F.

80K 80 K 0.0% A. F.

x100 or 200K 200 K 0.0% A. F. x1000 50 0K 500 K 0.0% A. F.

BOOK 800 K 0.0% A. F.



REMARKS:


Calibration Sticker Attached?: (!) Yes



c.i'c. Performed/Reviewed by: 6>.®1L §jfem• Date: 8/23/2012

499

@ Yes

0 No

0 No

0 No

c/.a:. Entered by: __ ' _Initials

C~hbrotiDn$ porlormGd 1o ANSI N323A-1997 stondards.

GRIFFIN INSTRUMENTS


09-00328 Owner: DENUKE

I DATE:

TECH:

06/23/12

E.M. Glenn

LOCATION:


Griffin Ins!

09/09/12


C!l Due For Calibration 0 Repair (See Remarks) 0 Other (See Remarks) 0 Due and Repair


NISTTRACEABLE EQUIPMENT AND STANDARDS USED DURING CALIBRATION

MODEL: 2224-1 SERIAL#: 257959 CAL DUE: 08/23/13




94TH470-1593 Th230

2696-00 Pu239

2697-00 Sr90

Condition: (!) Sat 0 Unsat


HV /Vernier:

650 I NIA

AFCPM:

AF 4 pi eff:

AF 2 pi eff:


: A ch. B ch. !Net Eff.·, ' I .

Pu239 Tc99 Ni

3942

21 .30%

42.06%


17,300 dpm 06/15/09 10,800 cpm

16.700dpm 06/16/09 8,170 cpm

18,500 dpm 12102/09 9,370 cpm

12.200 dpm 03/01/00 8,530 cpm


Pu: 21 .58% Th:1 19.12% Sr. 33.57%

Tess : 15.17% C14: TeNt::


Background (CPM}:

ITc-99 Source Response Stainless Steel (CPM}:

A ch. . B ch. I Net Eft.

3942 ; 588 ~1 .30%1 A ch . B ch. A ch. • B ch. !Net Eft. '

i 16 1 2875 14.70% 1 332

Net A to B B to A Xtalk: Xtalk: <10% <1 %

6.1% <1%

Tc99 ss Th-230 Sr90 C-14

2875 3194 3370

14.70% 19.12% 33.58%

• I 23.55% 39.08% 48.03%


Nolo; If tho as foun~ data Is \Whin 10% of the lost ea!<bnlhon and the 8-A Xto!k is <1% and the A·B Xlalk IS <10%,111on the technician may N/A tho plateau section and go directly lo remorks_

I

I I

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GRIFFIN INSTRUMENTS

PLJTEAU AND SET POINT DATA

HV I Vernier: Tc-99 Source Response Pu-239 Source Response Background (CPM): SS (CPM):

Ach. Bch. Net Eff.

600 8 1159 6.1%

625 9 1769 9.3%

650 13 2305 12.5%

675 11 2748 14.9%

Alpha I Beta Bkg (cpm) 0 HVIVernl~r Pu-239

6751 N/A CPM: 3870



REMARKS:


CaHbralion Slicker Attached?:


(CPM):

Ach. B ch. J Net Eff. Ach. I 2560 371 13.8% 0

3253 399 17.6% 1

3666 381 19.8% 0

3870 429 20.9% 0

i

171 Tc-99 Ni ~

@ Yes

@ Yes

08/23/13

2748

14.90%

23.86%

0 No

0 No

Th-230

3186

19.08%

39.00%

INSTRUMENT MARRIED WITH 2224-1 #257959

Performed/Reviewed by: . Date: 812312012

Bch.

101

160

140

171

PROBE#: PR278242

Date: 08123/12

NetAtoB B toAXtalk: Xtalk: <10% <1%

9.5% <1%

6.8% <1%

6.2".4 <1%

6.3% <1%

£:1! §!:22

3103

32.41%

46.35%

Entered by: ~Initials 2 pi emcloncleo do noted In ltallco. CollbroUono performed !o ANSI N323A·1117 •tandords.

2

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Documents

IR 03037850/2014001 on 7/15/14, 08/18/14 and 8/25/14, CB&I ... · Overload Light: @ Adjusted 0 Not Adj. REMARKS: Does Instrument Meet Final Acceptance Criteria?: Calibration Sticker