14
Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. इंटरनेट मानक !ान $ एक न’ भारत का +नम-णSatyanarayan Gangaram Pitroda “Invent a New India Using Knowledge” प0रा1 को छोड न’ 5 तरफJawaharlal Nehru “Step Out From the Old to the New” जान1 का अ+धकार, जी1 का अ+धकारMazdoor Kisan Shakti Sangathan “The Right to Information, The Right to Live” !ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता ह Bharthari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” IS 5642 (1991): Permeable sintered metal materials - Determination of density,oil content,and open porosity [MTD 25: Powder Metallurgical Materials and Products]

IS 5642 (1991): Permeable sintered metal materials - … · 2018-11-15 · IS 5642 : 1991 IS0 2738 : 1987 5.7 Pyknometer, of sufficient capacity, complying with the requirements of

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Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.

इंटरनेट मानक

“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru

“Step Out From the Old to the New”

“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan

“The Right to Information, The Right to Live”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

“Invent a New India Using Knowledge”

है”ह”ह

IS 5642 (1991): Permeable sintered metal materials -Determination of density,oil content,and open porosity [MTD25: Powder Metallurgical Materials and Products]

IS 6642 : 1991 IS0 2738 : 1987

Indian Standard

PERMEABLE WNTERED METAL MATERIALS - DETERMINATION OF DENSITY, OIL CONTENT, AND OPEN POROSITY

( Second Revision )

UDC 669-492-2-l 38.8 : 531,754

0 BIS 1991

BUREAU OF INDIAN STANDARDS MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG

NEW DELHI 110002

June 1991 Price Group 5

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As in the Original Standard, this Page is Intentionally Left Blank

IS 5642 : 1991 IS0 2730 : ‘1907

1 Scope and field of application

This International Standard specifies methods of determining

the density, oil content, and open ~porosity of, permeable

sintered metal materials.

It applies in particular to porous metal bearings and tostruc-

tural parts produced by pressing, and sintering metal powders.

2 References

IS0 758, Liquid chemical products for industrial use - Deter- mination of density at 20 T.

IS0 3448, Industrial liquid lubricants - IS0 viscosity classifica- tion.

IS0 3507, Fyknometers.

IS0 4495, Lubricated metallic powders - Determination of lubricant content - Soxhlet extraction method.

3 Symbols and designations

Symbol

ml

m2 m3 m4

m5

43

mw

V

Qw Ql Q2

QL

Table 1

Designation

Initial mass of the test piece

Maas of the test piece after oil extraction and drying

Mass of the fully impregnated test piece

Mass of the test piece and filled pyknometer with the test piece outside the pyknometer

Mass of the test piece and filled pyknometer with the test piece inside the pyknometer

Mass of the fully or partially impregnated test piece plus supporting device (for example suspension wire) weighed in air

Mass df the fully or partially impreghated test piece plus supporting device (for example suspension wire) weighed in water

Volume of the test piece

Density of the water used

Density of the oil initially in the test piecet)

Density of the impregnating oil usedt)

Density of the liquid in the pyknometer

Unit

g

g

g

1) The oil density is~assumed to be known or, if not, to be determined according to IS0 758.

3

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IS 5642 : 1991 IS0 2738 : 1987

5.7 Pyknometer, of sufficient capacity, complying with the requirements of IS0 3507.

6 Test piece

6.1 If possible, the test piece shall be tested whole. If this is not possible, the test piece shall be cut or broken into smaller ~parts to facilitate the various operations; all the parts shall be subjected to the density determination. The density of the test piece shall be determined from the total mass and the total volume.

6.2 If the test piece is too small to be measured easily, either a number of test pieces shall be tested together to obtain the average value, or the pyknometer method shall be used (see 7.6.8).

NOTE - In general, this is the case when the individual pieces have a volume less than 0,5 cm3.

6.3 The surface of the test piece shall be free of adhering dirt, grease, or other foreign material.

6.4 The surface of the test piece shall be free from surplus oil, for example that held by capillary action or surface tension. When removing any such surplus oil with an oil-absorbent material, care shall be taken to avoid removing oil-contained in the pores.

NOTE - The presence of surplus oil on the surface of the test piece is most likely to occur after the full impregnation treatment.

7 Test procedures

7.1 Determination of the initial mass of the test piece

Weigh the test piece in the condition in which it was received, to obtain rn,.

NOTE - If the test piece is known to contain no oil, the procedures described in 7.2 and 7.3 are omitted. In this case, ml is substituted for mg in the formulae given in 8.1 and 8.3.

7.2 Removal of oil from the test piece by solvent extraction

Approximately 3 h of soaking and about 10 solvent changes are required to remove the oil from test pieces of average density

and small wall thickness. For thick walls and high density, up to

24 h are sometimes required.

NOTE - The Soxhlet extractor is a convenient apparatus for soaking the test piece in warm freshly distilled oil solvent. The distillation rate determines the number of cycles and hence the number of solvent changes that occur.

A suitable Soxhlet unit is described in IS0 4495.

l 1 mm2/s = 1 cSt

Continue the extraction to constant mass after evaporation of the solvent left in the pores.

NOTE - Experience will indicate the best extraction time and distilla- tion rate to use.

Dry the test piece to constant mass (i.e. until the reduction in mass produced by the’ last extraction does not exceed 0,055 % 1 at a temperature of 26 OC above the boiling point of the sol- vent, then cool in a desiccator and weigh.

Choose the solvent so that complete dissolution of the oil is ensured. This requirement shall be tested for separately. The solvent used shall be stated in the test report.

For practical control purposes, other methods for removing the

oil may be used (such as heating in a protective atmosphere). In cases of dispute, the Soxhlet extraction method shall be the reference method.

7.3 Determination of the mass of the dried test piece

Weigh the test piece after solvent extraction and drying obtain rn2.

7.4 impregnation with oil and surface coating

to

7.4.1 Full impregnation (for determination of the open poro- sity)

Submerge the test piece in oil, contained in any suitable vessel capable of withstanding a vacuum. Reduce the pressure on the surface of the oil to between 1 and 10 MPa.

Continue the vacuum treatment until no further bubbles appear on the surface of the oil.

Restore the pressure in the vacuum chamber to that of the ~ambient atmosphere. Allow the test piece to remain submerged in the oil for a period which is not less than the period of the vacuum treatment.

NOTE - For the majority of porous metals a single vacuum treatment

is sufficient to ensure full impregnation. In some cases a second

vacuum treatment is necessary to achieve ful! impregnation. This can

be established by reducing the pressure a second time, and if no

further air bubbles appear, it can be safely assumed that the first

treatment has achieved full impregnation.

The oil shall be completely immiscible with water and shall wet the porous metal.

NOTE - Generally, the oil shall have a viscosity at 20 ‘-‘C of between 50

and 500 mm?,* which is in the range IS0 VG 22 to VG 150, as speci-

fied in IS0 3445. With a low-viscosity oil, impregnation is faster than

with a high-viscosity oil.

Remove the test piece from the oil, allow to drain and remove the surplus surface oil as described in 6.4.

IS 5642 : 1991 IS0 2738 : 1987

7.4.2 Partial impregnation (suitable for determination of the volume)

The requirements of the oil are the same as stated in 7.4.1.

Submerge the test piece in hot oil (65 ZL 5 OC) until no further air bubbles appear. Cool the test piece to room temperature whilst still submerged in oil by removing it froin the hot oil and quickly transferring it to cold oil. Remove the cooled test piece from the cold oil, allow to drain and remove the surplus surface oil as described in 6.4.

7.4.3 Surface coating methods (suitable for determination of the volume)

Coat the -porous surface of the test piece with a film that prevents, by surface tension, the water from entering the -pores.

The following techniques have been found to be suitable for particular types of porous metal. However, before any are used, the effectiveness oj the technique with respect to the type and shape of porous metal must first be established.

7.4.3.1 Petroleum jelly

Smear the surface of the test piece with petroleum jelly and remove any~excess.

7.4.3.2 Silicones

Many~silicone fluids produce surface films which are not wetted by water. Dip the test piece into either the silicone fluid or a dilute solution of the silicone fluid in a suitable solvent and dry to constant mass.

7.4.3.3 Paraffin wax

Dip the test piece into a 5 % solution of paraffin wax in a suitable solvent and dry to constant mass.

7.5 Determination of the mass of the fully impregnated test piece

Weigh the test piece after full oil impregnation to obtain m3.

7.6 Determination of the volume of the test piece

7.6.1 Determine the volume, V, of the test piece by weighing in air to obtain m,, and then submerge in water or other liquid of known density to obtain m,. Calculate the volume of the test piece by dividing the mass of displaced liquid by the densi- ty of the liquid.

7.6.2 With porous metals, it is essential that the liquid used is not absorbed by the pores. For this reason, the pores are im- pregnated with oil, and water is usually used as the test liquid, but it is not always necessary to impregnate a test apiece fully. However, in order to ensure that no water enters the pores when the test piece is submerged in the water, the test piece

may be partially impregnated or surface coated as described in 7.4.2 and 7.4.3. As a reference method, the test piece shall be fully impregnated with oil as described in 7.4.1.

NOTE - After weighing in water, the test piece should be reweighed in air (having removed any adhering water), to confirm that no water has been absorbed.

7.6.3 Figures 1,2 and 3 show methods of suspending the test piece during weighing. In general, the mass and volume of the device should be as small as possible.

7.6.4 The test piece can be suspended from _a piece of thin wire, and the total mass of the test piece and wire determined in air and in water. Allowance is made for the volume of the wire submerged in the water, but this is often insignificantly small when compared with the volume of the test piece. This allowance can be made by weighing the wire in air and then when submerged to the correct depth in water. Alternatively, the length of wire which is submerged can be measured, and the correction made based on the known volume of a unit length of wire.

7.6.5 Ensure that all air bubbles are removed from the surface of the test piece and the supporting device. It is permissible to add a few drops of wetting agent to the water. (See 5.4.)

7.6.6 The test piece and the water shall be at the same temperature. The normal test temperature is between 18 and 22 “C and the density, Q,, of pure water in this range may be taken as 0,997 g/cm? For temperatures outside this range, the water density shall be determined.

7.6.7 The volume, V, in cubic centimetres, is given by the equation

7.6.6 The volume can be determined using a pyknometer filled with a liquid of known density eV Impregnate the test piece fully with oil (see 7.4). Weigh the filled pyknometer together with the test piece outside the pyknometer, to obtain

1114.

Place the test piece in the pyknometer, ensuring that the test piece and the liquid are at the reference temperature as specified in IS0 3507. Remove any entrapped air by shaking. Top up the pyknometer with the liquid and replace the stopper. Remove all liquid from the outside of the pyknometer with an absorbent material, taking particular care over the region where the stopper and the neck meet. Leave until last the removal of the drop of liquid left on the stopper. Weigh the filled pyknometer, with the test piece inside it, to obtain ms

The volume, V, in cubic centimetres, is given by the equation

v= m4 - m5

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IS 5642 : 1991 IS0 2738 : 1987

__,_- -- ~- -- &

al Weighing in air bi Weighing in water

Figure 1

4 .___ I -- ~- - --_ __- ~_

Figure 2

E!D I

I \

b -.--- - __ _-- _ _~_ _ -.___.

--& ----- !j; Wcighlng m water

a) Welghing in air b) Weiqhlng XI water

Figure 3

8

L 1st

ISI

ISI

IS0 VISCOSITY CLASSIFICATION WITH CORRESPONDING KINEMATIC VISCOSITIES AT VARIOUS TEMPERATURES

FOR DIFFERING VISCOSITY INDICES

IS0

viscosity grade

Kinematic

viscosity

range

cSt at 40 “C

Approximate kinematic viscosity at other temperatures for different values of viscosity index

Viscosity ifiili!x 0 Viscosity illtlcx 50 Viscosity index .- 95

cst at 20 “c CSI ntt37.8 ‘C, cSt at 5O’C cst at 20 c cSt nt 37.8 ‘C cst at 50 “c cSt at 20 “C cSt at 37.8 “C cSt at 50 “C

OVG2 1 !jf, 3.12 17.87 3.G7) (7.05 7.52) (1.69 7.03) 12.u7 3.W) 17 .O!i 7.571 f 1 .r;n 7.03) 17.97 3.71) (2,OG 7.57) (1.69 7.03)

OVG3 2.88 .- 3.52 (4.60 -- 5.991 (3,02 3,711 (2.37 2.03) (4.59 - 5.92) 13.02 3.701 (2,313 2.84) (4,58 5.83) - (3.01 - 3.69) 12.39 2.86)

OVG5 4.14 - 5.06 (7.39 - 9.60) (4.38 - 5.38) (3.27 3.91) (7.25 9.35) (4.37 5.37) (3.29 - 3.95) (7.09 9,031 l4.36 - - 5.351 (3.32 -- 3.99)

0 VG 7 6.17 1,411 (17.3 1G.f)) If;.!;!; Il,O!il Pl.r;n 5.571 f 1 1 .!) l!r,3) W,‘,? Il,OI 1 (1,lN !i fi I , ) (11.4 14.41 win 1.W~ 14,1G 5 IT) .

D VG 10 9.00. 11.0 20.2 .. 25,9 9.73 17.0 6.53 7.R3 19.1 74.5 !).filI ,i) 1 1 fiJi5 I .!I!) 114.1 23.1 9.G4 .. 11.8 G.7G 8.14

DVG15 13.5 - 16.5 33.5 - 43.0 14.7 - 18.1 9.43 .- 11.3 31 .G -~ 40.6 14.7 18.0 9.62 -- 11.5 29.8 38.3 14.6 -- - 17.9 9.80 11.8

3VG22 19.8 - 24,2 54.2 - 69.8 21.8 - 26.8 13.3 - 16.0 51.0 -- 65.8 26.G 21.7 13.G lG.3 48.0 61.7 21.6 - - 26.5 13,9- 16.6

OVG32 28.8 - 35.2 87.7 - 115 32.0 -. 39.4 18.6 - 22.2 82.6 - 108 31.9 39.2 19.0 - 22.6 76.9 98.7 31.7 - -- 38.9 19.4 - 23.3

DVG46 41.4 - 50.6 144 - 189 46.6 - 57.4 25.5 - 30.3 133 - 172 - 46.3 56,9 26.1 - 31.3 120 153 45.9 - - 56.3 27.0 - 32.5

3VG68 61.2 - 74.8 242 - 315 69.8 - 85.8 35.9 - 42.8 2j9 - 283 69.2 .- 85.0 37,l - 44.4 193 - 244 68.4 - 83.9 38.7 - 46.6

3 VG 100 90.0 - 110 402 - 520 104 - 127 50.4 - 60.3 356 - 454 103 --- 126 52.4 - 63.0 303 383 101 - - 124 55.3 - 66.6

3 VG 150 135 - 165 672 - 862 157 - 194 72.5 - 86.9 583 - 743 155 - 191 75.9 -91,2 486 614 153 - - 188 80.6 - 97,l

1 VG 220 198 - 242 1 080 - 1 390 233 - 286 102 - 123 927 -- 1 180 230 282 108 - 129 761 .- 964 226 - 277 115 - 138

1 VG 320 288 - 352 1 720 - 2 210 341 -419 144 - 172 1 4GO .- 1870 337 414 151 .- 182 1 .--

41’4 - 506

180 1 500 331 - 4OG lG3.m 196

IVG460 2 700 - 3 480 495 - 608 199 - 239 2 290 - 2 930 488 - 599 210 - 252 1810-2300 478 - 587 228 - 274

IVG680 612 -- 748 4 420 - 5 680 739 - 908 283 - 339 3 700 - 4 740 728 894 300 - 360 2 - 3 880 650 712 - 874 326 - 393

1 VG 1 060 900--l 100 7 170 -9230 1 100 - 1 350 400 -. 479 5 9GO 7 G40 i 080 1 330 475 509 4 1 550 5 780 050 - 1 290 4GG -~- 560

1 VG 1 500 1 350 1 650 11900 - 15400 1 GGO -- 2 040 575 G88 9850. 12GO0 1640 7010 G13 734 7 1 390 9 400 590 1 9GO G76 812

NOTE - Values in pnrcnthescs have been derived by extrapolation and are approximate

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