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ANALYTICAL REPORT
Job Number: 720-88635-1
Job Description: Soil Removal for HPNS Crime Lab
For:Engineering Remediation Resources Group.
456 Montgomery StreetSuite 900
San Francisco, CA 94104
Attention: Rima Chaib
_____________________________________________
Approved for release.Chenise Y Lambert-SykesProject Manager I10/22/2018 7:36 PM
Chenise Y Lambert-Sykes, Project Manager I13715 Rider Trail North, Earth City, MO, 63045
(314)298-8566 [email protected]
10/22/2018
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. Pursuant toNELAP, this report shall not be reproduced, except in full, without the written approval of the laboratory. This report isconfidential and is intended for the sole use of TestAmerica and its client. All questions regarding this report should bedirected to the TestAmerica Project Manager.
Louisiana Lab Certification ID (Non-Potable, Solid/Haz. Material): 106151Florida Lab Certification ID (Drinking Water): E87689.
TestAmerica Laboratories, Inc.
TestAmerica Pleasanton 1220 Quarry Lane, Pleasanton, CA 94566
Tel (925) 484-1919 Fax (925) 600-3002 www.testamericainc.com
Page 1 of 613
mailto:[email protected]://www.testamericainc.comhttp://
Table of ContentsCover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Default Detection Limits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83
Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 201
GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 201
Method 8260B Low Level . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 201Method 8260B Low Level QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 202Method 8260B Low Level Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 219Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 222
Method 8260B Low Level ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 222Method 8260B Low Level CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 248
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 260Method 8260B Low Level Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 260
Page 2 of 613
Table of ContentsMethod 8260B Low Level LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 263
Method 8260B Low Level Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 271Method 8260B Low Level Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 274
GC/MS Semi VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 275
Method 8270C . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 275Method 8270C QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 276Method 8270C Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 285Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 288
Method 8270C ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 288Method 8270C Resolution Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 297Method 8270C CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 298
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 303Method 8270C Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 303Method 8270C LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 306
Method 8270C Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 309Method 8270C Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 310
GC Semi VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 311
Method 8015B - DRO . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 311Method 8015B - DRO QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 312Method 8015B - DRO Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 317Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 318
Method 8015B - DRO ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 318Method 8015B - DRO CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 328
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 344Method 8015B - DRO Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 344Method 8015B - DRO LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 345
Page 3 of 613
Table of ContentsMethod 8015B - DRO MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 346
Method 8015B - DRO Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 348Method 8015B - DRO Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 352
Method 8081A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 353Method 8081A QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 354Method 8081A Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 365Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 366
Method 8081A ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 366Method 8081A PEM Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 398Method 8081A CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 402
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434Method 8081A Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434Method 8081A LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 436
Method 8081A Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 438Method 8081A Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 447
Method 8082 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 448Method 8082 QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 449Method 8082 Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 457Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458
Method 8082 ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458Method 8082 CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 478
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 506Method 8082 Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 506Method 8082 LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 507
Method 8082 Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 508Method 8082 Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 515
Page 4 of 613
Table of ContentsInorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 516
Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 516
Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 517
Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 518
Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 520Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 520Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 525Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 527Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 537Met MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 541Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 544Met Serial Dilution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 548
Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 549
Met IECF . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 557
Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 581
Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 583
Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 587
Met Internal Standards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 592
Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 594
Subcontracted Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 604
Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 609
Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 610
Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 613
Page 5 of 613
Definitions/GlossaryTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Qualifiers
GC/MS Semi VOA
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a
dilution may be flagged with a D.X Surrogate is outside control limits
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
B Compound was found in the blank and sample.
V Serial Dilution exceeds the control limits
^ ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Pleasanton
Page 6 of 613
CASE NARRATIVE
Client: Engineering Remediation Resources Group.
Project: Soil Removal for HPNS Crime Lab
Report Number: 720-88635-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a % solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.”
Any minimum detectable concentration (MDC), critical value (DLC), or Safe Drinking Water Act detection limit (SDWA DL) is sample-specific unless otherwise stated elsewhere in this narrative.
Reference the chain of custody and condition upon receipt report for any variations on receipt conditions and temperature of samples on receipt.
Manual Integrations were performed only when necessary and are in compliance with the laboratory’s standard operating procedure. Detailed information can be found in the raw data section of the level IV report.
The following clean-up methods for Organic analyses may have been used on the samples in this data set. Specific methods employed are documented on the batch extraction logs:
Method 3600C: CleanupMethod 3620C: Florisil CleanupMethod 3630C: Silica Gel CleanupMethod 3640A: Gel-Permeation CleanupMethod 3650B: Acid-Base Partition CleanupMethod 3660B: Sulfur CleanupMethod 3665A: Sulfuric Acid/Permanganate Cleanup
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPTThe samples were received on 09/18/2018; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 2.2 C.
VOLATILE ORGANIC COMPOUNDS (GC MS)Sample SFPD091818 (720-88635-1) was analyzed for volatile organic compounds (GC MS) in accordance with EPA SW-846 Method 8260B. The samples were analyzed on 10/01/2018.
Analytical Batch: 720-252546The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 720-252551 and analytical batch 720-252546 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated
Page 7 of 613
laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within acceptance limits. 720-88736-9 MS, 720-88736-9 MSD
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)Sample SFPD091818 (720-88635-1) was analyzed for semivolatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8270C. The samples were prepared on 09/21/2018 and analyzed on 09/26/2018.
Analytical Batch: 720-252166The following sample was diluted due to the abundance of non-target analytes: SFPD091818 (720-88635-1). Elevated reporting limits (RLs) are provided.
The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 720-251971 and analytical batch 720-252166 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.
The method blank for preparation batch 720-251971 and analytical batch 720-252166 contained Phenol, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 1,2-Dichlorobenzene, Isophorone, Hexachlorobutadiene, Acenaphthylene, Anthracene, Benzo[a]pyrene, Indeno[1,2,3-cd]pyrene, Pyridine and Nitrobenzene above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed. MB 720-251971/1-A
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
DIESEL RANGE ORGANICS (DRO) (GC)Sample SFPD091818 (720-88635-1) was analyzed for Diesel Range Organics (DRO) (GC) in accordance with SW 846. The samples were prepared on 09/26/2018 and analyzed on 09/28/2018.
720-252409The following samples required a dilution due to the nature of the sample matrix: SFPD091818 (720-88635-1), (720-88635-A-1-E MS) and (720-88635-A-1-F MSD). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.
p-Terphenyl failed the surrogate recovery criteria low for SFPD091818 (720-88635-1). p-Terphenyl failed the surrogate recovery criteria low for SFPD091818MS (720-88635-1MS). p-Terphenyl failed the surrogate recovery criteria low for SFPD091818MSD (720-88635-1MSD). Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHLORINATED PESTICIDESSample SFPD091818 (720-88635-1) was analyzed for chlorinated pesticides in accordance with EPA SW-846 Method 8081A. The samples were prepared on 09/21/2018 and analyzed on 09/25/2018.
The %RPD between the primary and confirmation column / detector exceeded 40% for 4,4'-DDD for the following sample: SFPD091818 (720-88635-1). The lower value(s) has been reported and qualified in accordance with the laboratory's SOP.
The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 720-251965 and analytical batch 720-252126 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS ) was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
POLYCHLORINATED BIPHENYLS (PCBS)Sample SFPD091818 (720-88635-1) was analyzed for polychlorinated biphenyls (PCBs) in accordance with EPA SW-846 Method 8082. The samples were prepared on 09/21/2018 and analyzed on 09/25/2018.
The following sample required a tetrabutylammonium sulfite (TBA) clean-up to reduce matrix interferences caused by sulfur: SFPD091818 (720-88635-1).
The following samples required a tetrabutylammonium sulfite (TBA) clean-up to reduce matrix interferences caused by sulfur: (LCS 720-251967/2-A), (MB 720-251967/1-A), (720-88674-A-5-I), (720-88674-A-5-G MS) and (720-88674-A-5-H MSD).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep Method 3546: Due to sample viscosities, these samples were volumed up to 2ml and 5ml. SFPD091818 (720-88635-1)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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METALS (ICP)Sample SFPD091818 (720-88635-1) was analyzed for Metals (ICP) in accordance with SW 846. The samples were leached on 09/24/2018, prepared on 09/28/2018 and analyzed on 09/29/2018.
The Leachate blank for preparation batch 720-251968 and 720-252432 and analytical batch 720-252520 contained As,Ba,Cd,Cr,Ni & Zn above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed. Blank LB4 720-251968/1-D
The serial dilution performed for the following sample associated with batch 720-252520 was outside control limits: (720-88635-B-1-H SD)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL METALS (ICP)Sample SFPD091818 (720-88635-1) was analyzed for total metals (ICP) in accordance with EPA SW-846 Method 6010B. The samples were prepared and analyzed on 09/28/2018.
The following sample was diluted due to the abundance of non-target analytes Fe, Ti: SFPD091818 (720-88635-1). Elevated reporting limits (RLs) are provided.
The method blank for preparation batch 720-252436 and analytical batch 720-252500 contained Cr above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed. MB 720-252436/1-A
The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 720-252436 and analytical batch 720-252500 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.
The serial dilution performed for the following sample associated with batch 720-252500 was outside control limits: (720-88784-A-1-G SD)
The ICSA/ICSAB for batch 720-252500 was outside the acceptance limits on the internal standard (IS).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
MERCURY (CVAA)Sample SFPD091818 (720-88635-1) was analyzed for Mercury (CVAA) in accordance with EPA SW-846 Method 7470A-CWET. The samples were leached on 09/24/2018, and prepared and analyzed on 10/02/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL MERCURYSample SFPD091818 (720-88635-1) was analyzed for total mercury in accordance with EPA SW-846 Method 7471A. The samples were prepared on 09/21/2018 and analyzed on 09/25/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SUBCONTRACTFecal Coliform: See Subcontract section of the report.
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Detection SummaryTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Client Sample ID: SFPD091818 Lab Sample ID: 720-88635-1
Anthracene
RL
0.27 mg/Kg
MDL
0.034
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA2J B0.046 8270C
Fluoranthene 0.27 mg/Kg0.060 Total/NA20.093 J 8270C
Pyrene 0.27 mg/Kg0.030 Total/NA20.088 J 8270C
Bis(2-ethylhexyl) phthalate 1.3 mg/Kg0.052 Total/NA20.39 J 8270C
Benzo[b]fluoranthene 0.27 mg/Kg0.076 Total/NA20.11 J 8270C
Benzo[a]pyrene 0.27 mg/Kg0.052 Total/NA20.14 J B 8270C
Diesel Range Organics [C10-C28] 9.8 mg/Kg3.7 Silica Gel
Cleanup
586 8015B
Motor Oil Range Organics [C24-C36] 240 mg/Kg49 Silica Gel
Cleanup
5480 8015B
4,4'-DDT 2.0 ug/Kg0.40 Total/NA123 8081A
4,4'-DDE 2.0 ug/Kg0.41 Total/NA14.6 8081A
4,4'-DDD 2.0 ug/Kg0.60 Total/NA11.7 J p 8081A
trans-Chlordane 2.0 ug/Kg0.45 Total/NA11.3 J 8081A
PCB-1260 49 ug/Kg5.2 Total/NA156 8082
Antimony 1.3 mg/Kg0.22 Total/NA40.35 J 6010B
Arsenic 2.6 mg/Kg0.22 Total/NA43.8 6010B
Barium 1.3 mg/Kg0.18 Total/NA485 6010B
Cadmium 0.32 mg/Kg0.032 Total/NA40.33 6010B
Chromium 1.3 mg/Kg0.14 Total/NA4140 B 6010B
Cobalt 0.52 mg/Kg0.052 Total/NA421 6010B
Copper 3.9 mg/Kg1.8 Total/NA431 6010B
Lead 1.3 mg/Kg0.27 Total/NA423 6010B
Molybdenum 1.3 mg/Kg0.17 Total/NA40.57 J 6010B
Nickel 1.3 mg/Kg0.13 Total/NA4230 6010B
Selenium 2.6 mg/Kg0.39 Total/NA41.1 J 6010B
Thallium 1.3 mg/Kg0.38 Total/NA41.6 6010B
Vanadium 1.3 mg/Kg0.18 Total/NA453 6010B
Zinc 3.9 mg/Kg1.6 Total/NA465 6010B
Antimony 0.10 mg/L0.041 STLC Citrate10.043 J 6010B
Arsenic 0.10 mg/L0.029 STLC Citrate10.11 B 6010B
Barium 0.50 mg/L0.016 STLC Citrate15.4 B 6010B
Cadmium 0.020 mg/L0.0021 STLC Citrate10.0066 J B 6010B
Chromium 0.10 mg/L0.0070 STLC Citrate11.0 B 6010B
Cobalt 0.020 mg/L0.0068 STLC Citrate10.74 6010B
Copper 0.20 mg/L0.037 STLC Citrate10.76 6010B
Lead 0.050 mg/L0.022 STLC Citrate11.2 6010B
Nickel 0.10 mg/L0.010 STLC Citrate14.9 B 6010B
Vanadium 0.10 mg/L0.0087 STLC Citrate10.45 6010B
Zinc 0.20 mg/L0.074 STLC Citrate11.8 B 6010B
Mercury 0.017 mg/Kg0.0025 Total/NA10.11 7471A
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.
Page 10 of 613
Client Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Lab Sample ID: 720-88635-1Client Sample ID: SFPD091818Matrix: SolidDate Collected: 09/18/18 15:17
Date Received: 09/18/18 18:18
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 0.75 ug/Kg 09/22/18 16:15 10/01/18 20:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.61 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,1,1-Trichloroethane ND
5.0 0.74 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,1,2,2-Tetrachloroethane ND
5.0 2.1 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,1,2-Trichloro-1,2,2-trifluoroethane ND
5.0 0.69 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,1,2-Trichloroethane ND
5.0 0.67 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,1-Dichloroethane ND
5.0 0.62 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,1-Dichloroethene ND
5.0 0.68 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,1-Dichloropropene ND
5.0 0.73 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,2,3-Trichlorobenzene ND
5.0 0.76 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,2,3-Trichloropropane ND
5.0 0.70 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,2,4-Trichlorobenzene ND
5.0 1.6 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,2,4-Trimethylbenzene ND
9.9 1.7 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,2-Dibromo-3-Chloropropane ND
5.0 0.67 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,2-Dichlorobenzene ND
5.0 0.75 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,2-Dichloroethane ND
5.0 0.62 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,2-Dichloropropane ND
5.0 0.64 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,3,5-Trimethylbenzene ND
5.0 0.71 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,3-Dichlorobenzene ND
5.0 0.72 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,3-Dichloropropane ND
5.0 0.70 ug/Kg 09/22/18 16:15 10/01/18 20:05 11,4-Dichlorobenzene ND
5.0 2.0 ug/Kg 09/22/18 16:15 10/01/18 20:05 12,2-Dichloropropane ND
50 21 ug/Kg 09/22/18 16:15 10/01/18 20:05 12-Butanone (MEK) ND
5.0 0.64 ug/Kg 09/22/18 16:15 10/01/18 20:05 12-Chlorotoluene ND
50 9.9 ug/Kg 09/22/18 16:15 10/01/18 20:05 12-Hexanone ND
5.0 0.67 ug/Kg 09/22/18 16:15 10/01/18 20:05 14-Chlorotoluene ND
5.0 2.5 ug/Kg 09/22/18 16:15 10/01/18 20:05 14-Isopropyltoluene ND
50 9.9 ug/Kg 09/22/18 16:15 10/01/18 20:05 14-Methyl-2-pentanone (MIBK) ND
50 38 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Acetone ND
5.0 0.64 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Benzene ND
5.0 0.78 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Bromobenzene ND
5.0 2.0 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Bromoform ND
9.9 0.78 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Bromomethane ND
5.0 2.0 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Carbon disulfide ND
5.0 0.62 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Carbon tetrachloride ND
5.0 0.68 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Chlorobenzene ND
20 0.71 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Chlorobromomethane ND
5.0 0.70 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Chlorodibromomethane ND
9.9 0.56 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Chloroethane ND
5.0 0.65 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Chloroform ND
9.9 0.78 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Chloromethane ND
5.0 0.67 ug/Kg 09/22/18 16:15 10/01/18 20:05 1cis-1,2-Dichloroethene ND
5.0 0.68 ug/Kg 09/22/18 16:15 10/01/18 20:05 1cis-1,3-Dichloropropene ND
9.9 0.85 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Dibromomethane ND
5.0 0.71 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Dichlorobromomethane ND
9.9 0.78 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Dichlorodifluoromethane ND
5.0 0.74 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Ethylbenzene ND
5.0 1.4 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Ethylene Dibromide ND
250 99 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Gasoline Range Organics (GRO)
-C4-C12
ND
TestAmerica Pleasanton
Page 11 of 613
Client Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Lab Sample ID: 720-88635-1Client Sample ID: SFPD091818Matrix: SolidDate Collected: 09/18/18 15:17
Date Received: 09/18/18 18:18
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
Hexachlorobutadiene ND 5.0 0.89 ug/Kg 09/22/18 16:15 10/01/18 20:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.67 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Isopropylbenzene ND
5.0 1.2 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Methyl tert-butyl ether ND
9.9 5.6 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Methylene Chloride ND
9.9 1.5 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Naphthalene ND
5.0 0.99 ug/Kg 09/22/18 16:15 10/01/18 20:05 1n-Butylbenzene ND
5.0 0.65 ug/Kg 09/22/18 16:15 10/01/18 20:05 1N-Propylbenzene ND
5.0 0.71 ug/Kg 09/22/18 16:15 10/01/18 20:05 1sec-Butylbenzene ND
5.0 0.62 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Styrene ND
5.0 0.72 ug/Kg 09/22/18 16:15 10/01/18 20:05 1tert-Butylbenzene ND
5.0 0.66 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Tetrachloroethene ND
5.0 0.70 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Toluene ND
5.0 0.74 ug/Kg 09/22/18 16:15 10/01/18 20:05 1trans-1,2-Dichloroethene ND
5.0 0.66 ug/Kg 09/22/18 16:15 10/01/18 20:05 1trans-1,3-Dichloropropene ND
5.0 0.62 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Trichloroethene ND
5.0 0.56 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Trichlorofluoromethane ND
20 5.0 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Vinyl acetate ND
5.0 0.72 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Vinyl chloride ND
5.0 1.2 ug/Kg 09/22/18 16:15 10/01/18 20:05 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr) 109 60 - 140 09/22/18 16:15 10/01/18 20:05 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene 95 09/22/18 16:15 10/01/18 20:05 145 - 131
Toluene-d8 (Surr) 95 09/22/18 16:15 10/01/18 20:05 158 - 140
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Phenol ND 0.27 0.044 mg/Kg 09/21/18 13:13 09/26/18 00:06 2
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.27 0.056 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Bis(2-chloroethyl)ether ND
0.27 0.029 mg/Kg 09/21/18 13:13 09/26/18 00:06 22-Chlorophenol ND
0.27 0.032 mg/Kg 09/21/18 13:13 09/26/18 00:06 21,3-Dichlorobenzene ND
0.27 0.072 mg/Kg 09/21/18 13:13 09/26/18 00:06 21,4-Dichlorobenzene ND
0.68 0.041 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Benzyl alcohol ND
0.27 0.037 mg/Kg 09/21/18 13:13 09/26/18 00:06 21,2-Dichlorobenzene ND
0.27 0.040 mg/Kg 09/21/18 13:13 09/26/18 00:06 22-Methylphenol ND
0.27 0.076 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Methylphenol, 3 & 4 ND
0.52 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 2N-Nitrosodi-n-propylamine ND
0.52 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Hexachloroethane ND
0.27 0.11 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Nitrobenzene ND
0.27 0.037 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Isophorone ND
0.52 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 22-Nitrophenol ND
0.52 0.22 mg/Kg 09/21/18 13:13 09/26/18 00:06 22,4-Dimethylphenol ND
0.68 0.044 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Bis(2-chloroethoxy)methane ND
1.3 0.036 mg/Kg 09/21/18 13:13 09/26/18 00:06 22,4-Dichlorophenol ND
0.27 0.056 mg/Kg 09/21/18 13:13 09/26/18 00:06 21,2,4-Trichlorobenzene ND
0.52 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Naphthalene ND
0.68 0.035 mg/Kg 09/21/18 13:13 09/26/18 00:06 24-Chloroaniline ND
0.27 0.040 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Hexachlorobutadiene ND
0.68 0.044 mg/Kg 09/21/18 13:13 09/26/18 00:06 24-Chloro-3-methylphenol ND
0.27 0.048 mg/Kg 09/21/18 13:13 09/26/18 00:06 22-Methylnaphthalene ND
TestAmerica Pleasanton
Page 12 of 613
Client Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Lab Sample ID: 720-88635-1Client Sample ID: SFPD091818Matrix: SolidDate Collected: 09/18/18 15:17
Date Received: 09/18/18 18:18
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Hexachlorocyclopentadiene ND 0.68 0.22 mg/Kg 09/21/18 13:13 09/26/18 00:06 2
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.68 0.080 mg/Kg 09/21/18 13:13 09/26/18 00:06 22,4,6-Trichlorophenol ND
0.27 0.033 mg/Kg 09/21/18 13:13 09/26/18 00:06 22,4,5-Trichlorophenol ND
0.27 0.038 mg/Kg 09/21/18 13:13 09/26/18 00:06 22-Chloronaphthalene ND
1.3 0.27 mg/Kg 09/21/18 13:13 09/26/18 00:06 22-Nitroaniline ND
0.68 0.048 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Dimethyl phthalate ND
0.27 0.044 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Acenaphthylene ND
0.68 0.31 mg/Kg 09/21/18 13:13 09/26/18 00:06 23-Nitroaniline ND
0.27 0.030 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Acenaphthene ND
2.6 0.52 mg/Kg 09/21/18 13:13 09/26/18 00:06 22,4-Dinitrophenol ND
1.3 0.27 mg/Kg 09/21/18 13:13 09/26/18 00:06 24-Nitrophenol ND
0.27 0.044 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Dibenzofuran ND
0.52 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 22,4-Dinitrotoluene ND
0.52 0.27 mg/Kg 09/21/18 13:13 09/26/18 00:06 22,6-Dinitrotoluene ND
0.68 0.037 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Diethyl phthalate ND
0.68 0.048 mg/Kg 09/21/18 13:13 09/26/18 00:06 24-Chlorophenyl phenyl ether ND
0.27 0.032 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Fluorene ND
1.3 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 24-Nitroaniline ND
1.3 0.27 mg/Kg 09/21/18 13:13 09/26/18 00:06 22-Methyl-4,6-dinitrophenol ND
0.27 0.031 mg/Kg 09/21/18 13:13 09/26/18 00:06 2N-Nitrosodiphenylamine ND
0.68 0.040 mg/Kg 09/21/18 13:13 09/26/18 00:06 24-Bromophenyl phenyl ether ND
0.52 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Hexachlorobenzene ND
1.3 0.52 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Pentachlorophenol ND
0.52 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Phenanthrene ND
0.27 0.034 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Anthracene 0.046 J B
0.68 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Di-n-butyl phthalate ND
0.27 0.060 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Fluoranthene 0.093 J
0.27 0.030 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Pyrene 0.088 J
0.68 0.044 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Butyl benzyl phthalate ND
0.68 0.080 mg/Kg 09/21/18 13:13 09/26/18 00:06 23,3'-Dichlorobenzidine ND
1.3 0.14 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Benzo[a]anthracene ND
1.3 0.052 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Bis(2-ethylhexyl) phthalate 0.39 J
0.52 0.26 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Chrysene ND
0.68 0.038 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Di-n-octyl phthalate ND
0.27 0.076 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Benzo[b]fluoranthene 0.11 J
0.27 0.052 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Benzo[a]pyrene 0.14 J B
0.27 0.11 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Benzo[k]fluoranthene ND
0.27 0.10 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Indeno[1,2,3-cd]pyrene ND
0.52 0.16 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Benzo[g,h,i]perylene ND
1.3 0.27 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Benzoic acid ND
0.27 0.048 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Azobenzene ND
0.27 0.12 mg/Kg 09/21/18 13:13 09/26/18 00:06 2Dibenz(a,h)anthracene ND
Nitrobenzene-d5 57 21 - 98 09/21/18 13:13 09/26/18 00:06 2
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 69 09/21/18 13:13 09/26/18 00:06 230 - 112
Terphenyl-d14 86 09/21/18 13:13 09/26/18 00:06 259 - 134
2-Fluorophenol 72 09/21/18 13:13 09/26/18 00:06 228 - 98
Phenol-d5 77 09/21/18 13:13 09/26/18 00:06 223 - 101
2,4,6-Tribromophenol 82 09/21/18 13:13 09/26/18 00:06 237 - 114
TestAmerica Pleasanton
Page 13 of 613
Client Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel CleanupRL MDL
Diesel Range Organics [C10-C28] 86 9.8 3.7 mg/Kg 09/26/18 15:51 09/28/18 13:19 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
240 49 mg/Kg 09/26/18 15:51 09/28/18 13:19 5Motor Oil Range Organics [C24-C36]
480
p-Terphenyl 0 D X 38 - 148 09/26/18 15:51 09/28/18 13:19 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8081A - Organochlorine Pesticides (GC)RL MDL
Aldrin ND 2.0 0.49 ug/Kg 09/21/18 15:11 09/25/18 21:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.0 0.58 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Dieldrin ND
2.0 0.62 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Endrin aldehyde ND
2.0 0.45 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Endrin ND
2.0 0.32 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Endrin ketone ND
2.0 0.45 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Heptachlor ND
2.0 0.34 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Heptachlor epoxide ND
2.0 0.40 ug/Kg 09/21/18 15:11 09/25/18 21:27 14,4'-DDT 23
2.0 0.41 ug/Kg 09/21/18 15:11 09/25/18 21:27 14,4'-DDE 4.6
2.0 0.60 ug/Kg 09/21/18 15:11 09/25/18 21:27 14,4'-DDD 1.7 J p
2.0 0.31 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Endosulfan I ND
2.0 0.48 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Endosulfan II ND
2.0 0.54 ug/Kg 09/21/18 15:11 09/25/18 21:27 1alpha-BHC ND
2.0 0.35 ug/Kg 09/21/18 15:11 09/25/18 21:27 1beta-BHC ND
2.0 0.62 ug/Kg 09/21/18 15:11 09/25/18 21:27 1gamma-BHC (Lindane) ND
2.0 0.43 ug/Kg 09/21/18 15:11 09/25/18 21:27 1delta-BHC ND
2.0 0.37 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Endosulfan sulfate ND
2.0 0.67 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Methoxychlor ND
39 6.7 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Toxaphene ND
39 3.1 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Chlordane (technical) ND
2.0 0.39 ug/Kg 09/21/18 15:11 09/25/18 21:27 1cis-Chlordane ND
2.0 0.45 ug/Kg 09/21/18 15:11 09/25/18 21:27 1trans-Chlordane 1.3 J
2.0 2.0 ug/Kg 09/21/18 15:11 09/25/18 21:27 1Hexachlorobenzene ND
Tetrachloro-m-xylene 85 21 - 145 09/21/18 15:11 09/25/18 21:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 83 09/21/18 15:11 09/25/18 21:27 121 - 136
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL
PCB-1016 ND 49 1.8 ug/Kg 09/21/18 15:07 09/25/18 15:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
49 1.8 ug/Kg 09/21/18 15:07 09/25/18 15:26 1PCB-1221 ND
49 1.8 ug/Kg 09/21/18 15:07 09/25/18 15:26 1PCB-1232 ND
49 1.8 ug/Kg 09/21/18 15:07 09/25/18 15:26 1PCB-1242 ND
49 1.8 ug/Kg 09/21/18 15:07 09/25/18 15:26 1PCB-1248 ND
49 1.8 ug/Kg 09/21/18 15:07 09/25/18 15:26 1PCB-1254 ND
49 5.2 ug/Kg 09/21/18 15:07 09/25/18 15:26 1PCB-1260 56
Tetrachloro-m-xylene 110 45 - 132 09/21/18 15:07 09/25/18 15:26 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 91 09/21/18 15:07 09/25/18 15:26 142 - 146
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.35 J 1.3 0.22 mg/Kg 09/28/18 10:42 09/28/18 18:21 4
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.6 0.22 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Arsenic 3.8
TestAmerica Pleasanton
Page 14 of 613
Client Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Lab Sample ID: 720-88635-1Client Sample ID: SFPD091818Matrix: SolidDate Collected: 09/18/18 15:17
Date Received: 09/18/18 18:18
Method: 6010B - Metals (ICP) (Continued)RL MDL
Barium 85 1.3 0.18 mg/Kg 09/28/18 10:42 09/28/18 18:21 4
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.26 0.084 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Beryllium ND
0.32 0.032 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Cadmium 0.33
1.3 0.14 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Chromium 140 B
0.52 0.052 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Cobalt 21
3.9 1.8 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Copper 31
1.3 0.27 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Lead 23
1.3 0.17 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Molybdenum 0.57 J
1.3 0.13 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Nickel 230
2.6 0.39 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Selenium 1.1 J
0.65 0.13 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Silver ND
1.3 0.38 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Thallium 1.6
1.3 0.18 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Vanadium 53
3.9 1.6 mg/Kg 09/28/18 10:42 09/28/18 18:21 4Zinc 65
Method: 6010B - Metals (ICP) - STLC CitrateRL MDL
Antimony 0.043 J 0.10 0.041 mg/L 09/28/18 09:43 09/29/18 13:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.029 mg/L 09/28/18 09:43 09/29/18 13:35 1Arsenic 0.11 B
0.50 0.016 mg/L 09/28/18 09:43 09/29/18 13:35 1Barium 5.4 B
0.020 0.0059 mg/L 09/28/18 09:43 09/29/18 13:35 1Beryllium ND
0.020 0.0021 mg/L 09/28/18 09:43 09/29/18 13:35 1Cadmium 0.0066 J B
0.10 0.0070 mg/L 09/28/18 09:43 09/29/18 13:35 1Chromium 1.0 B
0.020 0.0068 mg/L 09/28/18 09:43 09/29/18 13:35 1Cobalt 0.74
0.20 0.037 mg/L 09/28/18 09:43 09/29/18 13:35 1Copper 0.76
0.050 0.022 mg/L 09/28/18 09:43 09/29/18 13:35 1Lead 1.2
0.10 0.029 mg/L 09/28/18 09:43 09/29/18 13:35 1Molybdenum ND
0.10 0.010 mg/L 09/28/18 09:43 09/29/18 13:35 1Nickel 4.9 B
0.20 0.046 mg/L 09/28/18 09:43 09/29/18 13:35 1Selenium ND
0.050 0.020 mg/L 09/28/18 09:43 09/29/18 13:35 1Silver ND
0.10 0.035 mg/L 09/28/18 09:43 09/29/18 13:35 1Thallium ND
0.10 0.0087 mg/L 09/28/18 09:43 09/29/18 13:35 1Vanadium 0.45
0.20 0.074 mg/L 09/28/18 09:43 09/29/18 13:35 1Zinc 1.8 B
Method: 7470A - Mercury (CVAA) - STLC CitrateRL MDL
Mercury ND 0.0050 0.0025 mg/L 10/02/18 10:28 10/02/18 16:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.11 0.017 0.0025 mg/Kg 09/21/18 11:26 09/25/18 12:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Pleasanton
Page 15 of 613
Default Detection LimitsClient: Engineering Remediation Resources Group. TestAmerica Job ID: 720-88635-1Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep: 5030B
5.01,1,1,2-Tetrachloroethane ug/Kg
Analyte Units MethodMDLRL
0.76 8260B
5.01,1,1-Trichloroethane ug/Kg0.61 8260B
5.01,1,2,2-Tetrachloroethane ug/Kg0.75 8260B
5.01,1,2-Trichloro-1,2,2-trifluoroethane ug/Kg2.1 8260B
5.01,1,2-Trichloroethane ug/Kg0.70 8260B
5.01,1-Dichloroethane ug/Kg0.68 8260B
5.01,1-Dichloroethene ug/Kg0.62 8260B
5.01,1-Dichloropropene ug/Kg0.69 8260B
5.01,2,3-Trichlorobenzene ug/Kg0.74 8260B
5.01,2,3-Trichloropropane ug/Kg0.77 8260B
5.01,2,4-Trichlorobenzene ug/Kg0.71 8260B
5.01,2,4-Trimethylbenzene ug/Kg1.6 8260B
101,2-Dibromo-3-Chloropropane ug/Kg1.7 8260B
5.01,2-Dichlorobenzene ug/Kg0.68 8260B
5.01,2-Dichloroethane ug/Kg0.76 8260B
5.01,2-Dichloropropane ug/Kg0.63 8260B
5.01,3,5-Trimethylbenzene ug/Kg0.65 8260B
5.01,3-Dichlorobenzene ug/Kg0.72 8260B
5.01,3-Dichloropropane ug/Kg0.73 8260B
5.01,4-Dichlorobenzene ug/Kg0.71 8260B
5.02,2-Dichloropropane ug/Kg2.0 8260B
502-Butanone (MEK) ug/Kg21 8260B
5.02-Chlorotoluene ug/Kg0.65 8260B
502-Hexanone ug/Kg10 8260B
5.04-Chlorotoluene ug/Kg0.68 8260B
5.04-Isopropyltoluene ug/Kg2.5 8260B
504-Methyl-2-pentanone (MIBK) ug/Kg10 8260B
50Acetone ug/Kg38 8260B
5.0Benzene ug/Kg0.65 8260B
5.0Bromobenzene ug/Kg0.79 8260B
5.0Bromoform ug/Kg2.0 8260B
10Bromomethane ug/Kg0.79 8260B
5.0Carbon disulfide ug/Kg2.0 8260B
5.0Carbon tetrachloride ug/Kg0.62 8260B
5.0Chlorobenzene ug/Kg0.69 8260B
20Chlorobromomethane ug/Kg0.72 8260B
5.0Chlorodibromomethane ug/Kg0.71 8260B
10Chloroethane ug/Kg0.56 8260B
5.0Chloroform ug/Kg0.66 8260B
10Chloromethane ug/Kg0.79 8260B
5.0cis-1,2-Dichloroethene ug/Kg0.68 8260B
5.0cis-1,3-Dichloropropene ug/Kg0.69 8260B
10Dibromomethane ug/Kg0.86 8260B
5.0Dichlorobromomethane ug/Kg0.72 8260B
10Dichlorodifluoromethane ug/Kg0.79 8260B
5.0Ethylbenzene ug/Kg0.75 8260B
5.0Ethylene Dibromide ug/Kg1.4 8260B
250Gasoline Range Organics (GRO)-C4-C12 ug/Kg100 8260B
5.0Hexachlorobutadiene ug/Kg0.90 8260B
5.0Isopropylbenzene ug/Kg0.68 8260B
5.0Methyl tert-butyl ether ug/Kg1.2 8260B
TestAmerica Pleasanton
Page 16 of 613
Default Detection LimitsClient: Engineering Remediation Resources Group. TestAmerica Job ID: 720-88635-1Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)Prep: 5030B
10Methylene Chloride ug/Kg
Analyte Units MethodMDLRL
5.6 8260B
10Naphthalene ug/Kg1.5 8260B
5.0n-Butylbenzene ug/Kg1.0 8260B
5.0N-Propylbenzene ug/Kg0.66 8260B
5.0sec-Butylbenzene ug/Kg0.72 8260B
5.0Styrene ug/Kg0.63 8260B
5.0tert-Butylbenzene ug/Kg0.73 8260B
5.0Tetrachloroethene ug/Kg0.67 8260B
5.0Toluene ug/Kg0.71 8260B
5.0trans-1,2-Dichloroethene ug/Kg0.75 8260B
5.0trans-1,3-Dichloropropene ug/Kg0.67 8260B
5.0Trichloroethene ug/Kg0.63 8260B
5.0Trichlorofluoromethane ug/Kg0.56 8260B
20Vinyl acetate ug/Kg5.0 8260B
5.0Vinyl chloride ug/Kg0.73 8260B
5.0Xylenes, Total ug/Kg1.2 8260B
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep: 3546
0.0671,2,4-Trichlorobenzene mg/Kg
Analyte Units MethodMDLRL
0.014 8270C
0.0671,2-Dichlorobenzene mg/Kg0.0094 8270C
0.0671,3-Dichlorobenzene mg/Kg0.0080 8270C
0.0671,4-Dichlorobenzene mg/Kg0.018 8270C
0.0672,4,5-Trichlorophenol mg/Kg0.0084 8270C
0.172,4,6-Trichlorophenol mg/Kg0.020 8270C
0.332,4-Dichlorophenol mg/Kg0.0090 8270C
0.132,4-Dimethylphenol mg/Kg0.054 8270C
0.662,4-Dinitrophenol mg/Kg0.13 8270C
0.132,4-Dinitrotoluene mg/Kg0.066 8270C
0.132,6-Dinitrotoluene mg/Kg0.068 8270C
0.0672-Chloronaphthalene mg/Kg0.0096 8270C
0.0672-Chlorophenol mg/Kg0.0074 8270C
0.332-Methyl-4,6-dinitrophenol mg/Kg0.068 8270C
0.0672-Methylnaphthalene mg/Kg0.012 8270C
0.0672-Methylphenol mg/Kg0.010 8270C
0.332-Nitroaniline mg/Kg0.068 8270C
0.132-Nitrophenol mg/Kg0.066 8270C
0.173,3'-Dichlorobenzidine mg/Kg0.020 8270C
0.173-Nitroaniline mg/Kg0.078 8270C
0.174-Bromophenyl phenyl ether mg/Kg0.010 8270C
0.174-Chloro-3-methylphenol mg/Kg0.011 8270C
0.174-Chloroaniline mg/Kg0.0088 8270C
0.174-Chlorophenyl phenyl ether mg/Kg0.012 8270C
0.334-Nitroaniline mg/Kg0.066 8270C
0.334-Nitrophenol mg/Kg0.068 8270C
0.067Acenaphthene mg/Kg0.0076 8270C
0.067Acenaphthylene mg/Kg0.011 8270C
0.067Anthracene mg/Kg0.0086 8270C
0.067Azobenzene mg/Kg0.012 8270C
TestAmerica Pleasanton
Page 17 of 613
Default Detection LimitsClient: Engineering Remediation Resources Group. TestAmerica Job ID: 720-88635-1Project/Site: Soil Removal for HPNS Crime Lab
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)Prep: 3546
0.33Benzo[a]anthracene mg/Kg
Analyte Units MethodMDLRL
0.036 8270C
0.067Benzo[a]pyrene mg/Kg0.013 8270C
0.067Benzo[b]fluoranthene mg/Kg0.019 8270C
0.13Benzo[g,h,i]perylene mg/Kg0.040 8270C
0.067Benzo[k]fluoranthene mg/Kg0.028 8270C
0.33Benzoic acid mg/Kg0.068 8270C
0.17Benzyl alcohol mg/Kg0.010 8270C
0.17Bis(2-chloroethoxy)methane mg/Kg0.011 8270C
0.067Bis(2-chloroethyl)ether mg/Kg0.014 8270C
0.33Bis(2-ethylhexyl) phthalate mg/Kg0.013 8270C
0.17Butyl benzyl phthalate mg/Kg0.011 8270C
0.13Chrysene mg/Kg0.066 8270C
0.067Dibenz(a,h)anthracene mg/Kg0.030 8270C
0.067Dibenzofuran mg/Kg0.011 8270C
0.17Diethyl phthalate mg/Kg0.0094 8270C
0.17Dimethyl phthalate mg/Kg0.012 8270C
0.17Di-n-butyl phthalate mg/Kg0.066 8270C
0.17Di-n-octyl phthalate mg/Kg0.0096 8270C
0.067Fluoranthene mg/Kg0.015 8270C
0.067Fluorene mg/Kg0.0080 8270C
0.13Hexachlorobenzene mg/Kg0.066 8270C
0.067Hexachlorobutadiene mg/Kg0.010 8270C
0.17Hexachlorocyclopentadiene mg/Kg0.054 8270C
0.13Hexachloroethane mg/Kg0.066 8270C
0.067Indeno[1,2,3-cd]pyrene mg/Kg0.026 8270C
0.067Isophorone mg/Kg0.0094 8270C
0.067Methylphenol, 3 & 4 mg/Kg0.019 8270C
0.13Naphthalene mg/Kg0.066 8270C
0.067Nitrobenzene mg/Kg0.028 8270C
0.13N-Nitrosodi-n-propylamine mg/Kg0.066 8270C
0.067N-Nitrosodiphenylamine mg/Kg0.0078 8270C
0.33Pentachlorophenol mg/Kg0.13 8270C
0.13Phenanthrene mg/Kg0.066 8270C
0.067Phenol mg/Kg0.011 8270C
0.067Pyrene mg/Kg0.0076 8270C
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel CleanupPrep: 3546
2.0Diesel Range Organics [C10-C28] mg/Kg
Analyte Units MethodMDLRL
0.75 8015B
50Motor Oil Range Organics [C24-C36] mg/Kg10 8015B
Method: 8081A - Organochlorine Pesticides (GC)Prep: 3546
2.04,4'-DDD ug/Kg
Analyte Units MethodMDLRL
0.61 8081A
2.04,4'-DDE ug/Kg0.42 8081A
2.04,4'-DDT ug/Kg0.41 8081A
2.0Aldrin ug/Kg0.50 8081A
2.0alpha-BHC ug/Kg0.55 8081A
TestAmerica Pleasanton
Page 18 of 613
Default Detection LimitsClient: Engineering Remediation Resources Group. TestAmerica Job ID: 720-88635-1Project/Site: Soil Removal for HPNS Crime Lab
Method: 8081A - Organochlorine Pesticides (GC) (Continued)Prep: 3546
2.0beta-BHC ug/Kg
Analyte Units MethodMDLRL
0.36 8081A
40Chlordane (technical) ug/Kg3.2 8081A
2.0cis-Chlordane ug/Kg0.40 8081A
2.0delta-BHC ug/Kg0.44 8081A
2.0Dieldrin ug/Kg0.59 8081A
2.0Endosulfan I ug/Kg0.32 8081A
2.0Endosulfan II ug/Kg0.49 8081A
2.0Endosulfan sulfate ug/Kg0.38 8081A
2.0Endrin ug/Kg0.46 8081A
2.0Endrin aldehyde ug/Kg0.63 8081A
2.0Endrin ketone ug/Kg0.33 8081A
2.0gamma-BHC (Lindane) ug/Kg0.63 8081A
2.0Heptachlor ug/Kg0.46 8081A
2.0Heptachlor epoxide ug/Kg0.35 8081A
2.0Hexachlorobenzene ug/Kg2.0 8081A
2.0Methoxychlor ug/Kg0.68 8081A
40Toxaphene ug/Kg6.8 8081A
2.0trans-Chlordane ug/Kg0.46 8081A
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep: 3546
50PCB-1016 ug/Kg
Analyte Units MethodMDLRL
1.8 8082
50PCB-1221 ug/Kg1.8 8082
50PCB-1232 ug/Kg1.8 8082
50PCB-1242 ug/Kg1.8 8082
50PCB-1248 ug/Kg1.8 8082
50PCB-1254 ug/Kg1.8 8082
50PCB-1260 ug/Kg5.3 8082
Method: 6010B - Metals (ICP)Prep: 3050B
0.50Antimony mg/Kg
Analyte Units MethodMDLRL
0.083 6010B
1.0Arsenic mg/Kg0.085 6010B
0.50Barium mg/Kg0.071 6010B
0.10Beryllium mg/Kg0.033 6010B
0.13Cadmium mg/Kg0.012 6010B
0.50Chromium mg/Kg0.053 6010B
0.20Cobalt mg/Kg0.020 6010B
1.5Copper mg/Kg0.71 6010B
0.50Lead mg/Kg0.11 6010B
0.50Molybdenum mg/Kg0.064 6010B
0.50Nickel mg/Kg0.051 6010B
1.0Selenium mg/Kg0.15 6010B
0.25Silver mg/Kg0.051 6010B
0.50Thallium mg/Kg0.15 6010B
0.50Vanadium mg/Kg0.068 6010B
1.5Zinc mg/Kg0.64 6010B
TestAmerica Pleasanton
Page 19 of 613
Default Detection LimitsClient: Engineering Remediation Resources Group. TestAmerica Job ID: 720-88635-1Project/Site: Soil Removal for HPNS Crime Lab
Method: 6010B - Metals (ICP) - STLC CitratePrep: 3005ALeach: CA WET Citrate
0.010Antimony mg/L
Analyte Units MethodMDLRL
0.0041 6010B
0.010Arsenic mg/L0.0029 6010B
0.050Barium mg/L0.0016 6010B
0.0020Beryllium mg/L0.00059 6010B
0.0020Cadmium mg/L0.00021 6010B
0.010Chromium mg/L0.00070 6010B
0.0020Cobalt mg/L0.00068 6010B
0.020Copper mg/L0.0037 6010B
0.0050Lead mg/L0.0022 6010B
0.010Molybdenum mg/L0.0029 6010B
0.010Nickel mg/L0.0010 6010B
0.020Selenium mg/L0.0046 6010B
0.0050Silver mg/L0.0020 6010B
0.010Thallium mg/L0.0035 6010B
0.010Vanadium mg/L0.00087 6010B
0.020Zinc mg/L0.0074 6010B
Method: 7470A - Mercury (CVAA) - STLC CitratePrep: 7470ALeach: CA WET Citrate
0.00020Mercury mg/L
Analyte Units MethodMDLRL
0.00010 7470A
Method: 7471A - Mercury (CVAA)Prep: 7471A
0.017Mercury mg/Kg
Analyte Units MethodMDLRL
0.0025 7471A
TestAmerica Pleasanton
Page 20 of 613
Surrogate SummaryTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (60-140) (45-131) (58-140)
DCA BFB TOL
109 95 95720-88635-1
Percent Surrogate Recovery (Acceptance Limits)
SFPD091818
101 99 100LCS 720-252546/5 Lab Control Sample
104 101 99LCS 720-252546/7 Lab Control Sample
101 99 101LCSD 720-252546/6 Lab Control Sample Dup
100 101 97LCSD 720-252546/8 Lab Control Sample Dup
99 100 98MB 720-252546/4 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene
TOL = Toluene-d8 (Surr)
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (21-98) (30-112) (59-134) (28-98) (23-101) (37-114)
NBZ FBP TPHL 2FP PHL TBP
57 69 86 72 77 82720-88635-1
Percent Surrogate Recovery (Acceptance Limits)
SFPD091818
70 83 90 7978 76LCS 720-251971/2-A Lab Control Sample
65 72 92 7675 61MB 720-251971/1-A Method Blank
Surrogate Legend
NBZ = Nitrobenzene-d5
FBP = 2-Fluorobiphenyl
TPHL = Terphenyl-d14
2FP = 2-Fluorophenol
PHL = Phenol-d5
TBP = 2,4,6-Tribromophenol
Method: 8015B - Diesel Range Organics (DRO) (GC)Prep Type: Silica Gel CleanupMatrix: Solid
Lab Sample ID Client Sample ID (38-148)
TPH1
0 D X720-88635-1
Percent Surrogate Recovery (Acceptance Limits)
SFPD091818
0 D X720-88635-1 MS SFPD091818
0 D X720-88635-1 MSD SFPD091818
88LCS 720-252275/2-A Lab Control Sample
97MB 720-252275/1-A Method Blank
Surrogate Legend
TPH = p-Terphenyl
TestAmerica Pleasanton
Page 21 of 613
Surrogate SummaryTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8081A - Organochlorine Pesticides (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (21-145) (21-136)
TCX1 DCBP1
85 83720-88635-1
Percent Surrogate Recovery (Acceptance Limits)
SFPD091818
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCBP = DCB Decachlorobiphenyl
Method: 8081A - Organochlorine Pesticides (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (21-145) (21-136)
TCX2 DCBP1
86 111LCS 720-251965/2-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCBP = DCB Decachlorobiphenyl
Method: 8081A - Organochlorine Pesticides (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (21-145) (21-136)
TCX2 DCBP2
79 105MB 720-251965/1-A
Percent Surrogate Recovery (Acceptance Limits)
Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCBP = DCB Decachlorobiphenyl
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (45-132) (42-146)
TCX1 DCBP1
110 91720-88635-1
Percent Surrogate Recovery (Acceptance Limits)
SFPD091818
80 106LCS 720-251967/2-A Lab Control Sample
80 111MB 720-251967/1-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCBP = DCB Decachlorobiphenyl
TestAmerica Pleasanton
Page 22 of 613
QC Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 720-252546/4Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 0.76 ug/Kg 10/01/18 11:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.615.0 ug/Kg 10/01/18 11:43 11,1,1-Trichloroethane
ND 0.755.0 ug/Kg 10/01/18 11:43 11,1,2,2-Tetrachloroethane
ND 2.15.0 ug/Kg 10/01/18 11:43 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.705.0 ug/Kg 10/01/18 11:43 11,1,2-Trichloroethane
ND 0.685.0 ug/Kg 10/01/18 11:43 11,1-Dichloroethane
ND 0.625.0 ug/Kg 10/01/18 11:43 11,1-Dichloroethene
ND 0.695.0 ug/Kg 10/01/18 11:43 11,1-Dichloropropene
ND 0.745.0 ug/Kg 10/01/18 11:43 11,2,3-Trichlorobenzene
ND 0.775.0 ug/Kg 10/01/18 11:43 11,2,3-Trichloropropane
ND 0.715.0 ug/Kg 10/01/18 11:43 11,2,4-Trichlorobenzene
ND 1.65.0 ug/Kg 10/01/18 11:43 11,2,4-Trimethylbenzene
ND 1.710 ug/Kg 10/01/18 11:43 11,2-Dibromo-3-Chloropropane
ND 0.685.0 ug/Kg 10/01/18 11:43 11,2-Dichlorobenzene
ND 0.765.0 ug/Kg 10/01/18 11:43 11,2-Dichloroethane
ND 0.635.0 ug/Kg 10/01/18 11:43 11,2-Dichloropropane
ND 0.655.0 ug/Kg 10/01/18 11:43 11,3,5-Trimethylbenzene
ND 0.725.0 ug/Kg 10/01/18 11:43 11,3-Dichlorobenzene
ND 0.735.0 ug/Kg 10/01/18 11:43 11,3-Dichloropropane
ND 0.715.0 ug/Kg 10/01/18 11:43 11,4-Dichlorobenzene
ND 2.05.0 ug/Kg 10/01/18 11:43 12,2-Dichloropropane
ND 2150 ug/Kg 10/01/18 11:43 12-Butanone (MEK)
ND 0.655.0 ug/Kg 10/01/18 11:43 12-Chlorotoluene
ND 1050 ug/Kg 10/01/18 11:43 12-Hexanone
ND 0.685.0 ug/Kg 10/01/18 11:43 14-Chlorotoluene
ND 2.55.0 ug/Kg 10/01/18 11:43 14-Isopropyltoluene
ND 1050 ug/Kg 10/01/18 11:43 14-Methyl-2-pentanone (MIBK)
ND 3850 ug/Kg 10/01/18 11:43 1Acetone
ND 0.655.0 ug/Kg 10/01/18 11:43 1Benzene
ND 0.795.0 ug/Kg 10/01/18 11:43 1Bromobenzene
ND 2.05.0 ug/Kg 10/01/18 11:43 1Bromoform
ND 0.7910 ug/Kg 10/01/18 11:43 1Bromomethane
ND 2.05.0 ug/Kg 10/01/18 11:43 1Carbon disulfide
ND 0.625.0 ug/Kg 10/01/18 11:43 1Carbon tetrachloride
ND 0.695.0 ug/Kg 10/01/18 11:43 1Chlorobenzene
ND 0.7220 ug/Kg 10/01/18 11:43 1Chlorobromomethane
ND 0.715.0 ug/Kg 10/01/18 11:43 1Chlorodibromomethane
ND 0.5610 ug/Kg 10/01/18 11:43 1Chloroethane
ND 0.665.0 ug/Kg 10/01/18 11:43 1Chloroform
ND 0.7910 ug/Kg 10/01/18 11:43 1Chloromethane
ND 0.685.0 ug/Kg 10/01/18 11:43 1cis-1,2-Dichloroethene
ND 0.695.0 ug/Kg 10/01/18 11:43 1cis-1,3-Dichloropropene
ND 0.8610 ug/Kg 10/01/18 11:43 1Dibromomethane
ND 0.725.0 ug/Kg 10/01/18 11:43 1Dichlorobromomethane
ND 0.7910 ug/Kg 10/01/18 11:43 1Dichlorodifluoromethane
ND 0.755.0 ug/Kg 10/01/18 11:43 1Ethylbenzene
ND 1.45.0 ug/Kg 10/01/18 11:43 1Ethylene Dibromide
TestAmerica Pleasanton
Page 23 of 613
QC Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 720-252546/4Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
RL MDL
Gasoline Range Organics (GRO)
-C4-C12
ND 250 100 ug/Kg 10/01/18 11:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.905.0 ug/Kg 10/01/18 11:43 1Hexachlorobutadiene
ND 0.685.0 ug/Kg 10/01/18 11:43 1Isopropylbenzene
ND 1.25.0 ug/Kg 10/01/18 11:43 1Methyl tert-butyl ether
ND 5.610 ug/Kg 10/01/18 11:43 1Methylene Chloride
ND 1.510 ug/Kg 10/01/18 11:43 1Naphthalene
ND 1.05.0 ug/Kg 10/01/18 11:43 1n-Butylbenzene
ND 0.665.0 ug/Kg 10/01/18 11:43 1N-Propylbenzene
ND 0.725.0 ug/Kg 10/01/18 11:43 1sec-Butylbenzene
ND 0.635.0 ug/Kg 10/01/18 11:43 1Styrene
ND 0.735.0 ug/Kg 10/01/18 11:43 1tert-Butylbenzene
ND 0.675.0 ug/Kg 10/01/18 11:43 1Tetrachloroethene
ND 0.715.0 ug/Kg 10/01/18 11:43 1Toluene
ND 0.755.0 ug/Kg 10/01/18 11:43 1trans-1,2-Dichloroethene
ND 0.675.0 ug/Kg 10/01/18 11:43 1trans-1,3-Dichloropropene
ND 0.635.0 ug/Kg 10/01/18 11:43 1Trichloroethene
ND 0.565.0 ug/Kg 10/01/18 11:43 1Trichlorofluoromethane
ND 5.020 ug/Kg 10/01/18 11:43 1Vinyl acetate
ND 0.735.0 ug/Kg 10/01/18 11:43 1Vinyl chloride
ND 1.25.0 ug/Kg 10/01/18 11:43 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr) 99 60 - 140 10/01/18 11:43 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
100 10/01/18 11:43 14-Bromofluorobenzene 45 - 131
98 10/01/18 11:43 1Toluene-d8 (Surr) 58 - 140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-252546/5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
1,1,1,2-Tetrachloroethane 50.0 54.0 ug/Kg 108 70 - 130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 51.3 ug/Kg 103 70 - 130
1,1,2,2-Tetrachloroethane 50.0 51.3 ug/Kg 103 70 - 146
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 55.4 ug/Kg 111 60 - 140
1,1,2-Trichloroethane 50.0 56.0 ug/Kg 112 70 - 130
1,1-Dichloroethane 50.0 49.6 ug/Kg 99 70 - 130
1,1-Dichloroethene 50.0 48.7 ug/Kg 97 74 - 122
1,1-Dichloropropene 50.0 48.6 ug/Kg 97 70 - 130
1,2,3-Trichlorobenzene 50.0 55.3 ug/Kg 111 60 - 140
1,2,3-Trichloropropane 50.0 53.4 ug/Kg 107 70 - 146
1,2,4-Trichlorobenzene 50.0 54.6 ug/Kg 109 60 - 140
1,2,4-Trimethylbenzene 50.0 49.5 ug/Kg 99 70 - 130
1,2-Dibromo-3-Chloropropane 50.0 53.8 ug/Kg 108 60 - 145
1,2-Dichlorobenzene 50.0 51.9 ug/Kg 104 70 - 130
1,2-Dichloroethane 50.0 51.5 ug/Kg 103 70 - 130
TestAmerica Pleasanton
Page 24 of 613
QC Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-252546/5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
1,2-Dichloropropane 50.0 51.9 ug/Kg 104 73 - 127
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,3,5-Trimethylbenzene 50.0 49.5 ug/Kg 99 70 - 131
1,3-Dichlorobenzene 50.0 50.5 ug/Kg 101 70 - 131
1,3-Dichloropropane 50.0 54.4 ug/Kg 109 70 - 140
1,4-Dichlorobenzene 50.0 50.6 ug/Kg 101 70 - 130
2,2-Dichloropropane 50.0 50.5 ug/Kg 101 70 - 162
2-Butanone (MEK) 250 256 ug/Kg 103 59 - 159
2-Chlorotoluene 50.0 48.4 ug/Kg 97 70 - 138
2-Hexanone 250 249 ug/Kg 100 62 - 158
4-Chlorotoluene 50.0 48.7 ug/Kg 97 70 - 136
4-Isopropyltoluene 50.0 50.7 ug/Kg 101 70 - 133
4-Methyl-2-pentanone (MIBK) 250 255 ug/Kg 102 60 - 160
Acetone 250 236 ug/Kg 94 30 - 162
Benzene 50.0 48.6 ug/Kg 97 70 - 130
Bromobenzene 50.0 51.0 ug/Kg 102 70 - 130
Bromoform 50.0 58.9 ug/Kg 118 59 - 158
Bromomethane 50.0 56.7 ug/Kg 113 59 - 132
Carbon disulfide 50.0 46.4 ug/Kg 93 60 - 140
Carbon tetrachloride 50.0 50.9 ug/Kg 102 70 - 142
Chlorobenzene 50.0 50.8 ug/Kg 102 70 - 130
Chlorobromomethane 50.0 55.0 ug/Kg 110 70 - 130
Chlorodibromomethane 50.0 58.4 ug/Kg 117 70 - 146
Chloroethane 50.0 51.4 ug/Kg 103 65 - 130
Chloroform 50.0 50.6 ug/Kg 101 77 - 127
Chloromethane 50.0 54.0 ug/Kg 108 55 - 140
cis-1,2-Dichloroethene 50.0 49.4 ug/Kg 99 70 - 138
cis-1,3-Dichloropropene 50.0 57.0 ug/Kg 114 68 - 147
Dibromomethane 50.0 52.8 ug/Kg 106 70 - 139
Dichlorobromomethane 50.0 53.7 ug/Kg 107 70 - 140
Dichlorodifluoromethane 50.0 62.7 ug/Kg 125 37 - 158
Ethylbenzene 50.0 49.3 ug/Kg 99 80 - 137
Ethylene Dibromide 50.0 55.9 ug/Kg 112 70 - 140
Hexachlorobutadiene 50.0 55.2 ug/Kg 110 70 - 132
Isopropylbenzene 50.0 51.3 ug/Kg 103 70 - 130
Methyl tert-butyl ether 50.0 60.0 ug/Kg 120 70 - 144
Methylene Chloride 50.0 51.2 ug/Kg 102 70 - 134
m-Xylene & p-Xylene 50.0 49.7 ug/Kg 99 70 - 146
Naphthalene 50.0 53.4 ug/Kg 107 60 - 147
n-Butylbenzene 50.0 48.8 ug/Kg 98 70 - 142
N-Propylbenzene 50.0 48.3 ug/Kg 97 70 - 130
o-Xylene 50.0 50.6 ug/Kg 101 70 - 140
sec-Butylbenzene 50.0 49.6 ug/Kg 99 70 - 136
Styrene 50.0 50.8 ug/Kg 102 70 - 130
tert-Butylbenzene 50.0 49.8 ug/Kg 100 70 - 130
Tetrachloroethene 50.0 52.7 ug/Kg 105 70 - 132
Toluene 50.0 48.9 ug/Kg 98 75 - 120
trans-1,2-Dichloroethene 50.0 49.7 ug/Kg 99 67 - 130
trans-1,3-Dichloropropene 50.0 55.4 ug/Kg 111 70 - 155
TestAmerica Pleasanton
Page 25 of 613
QC Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-252546/5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
Trichloroethene 50.0 51.4 ug/Kg 103 70 - 133
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Trichlorofluoromethane 50.0 54.9 ug/Kg 110 60 - 140
Vinyl acetate 50.0 51.2 ug/Kg 102 38 - 176
Vinyl chloride 50.0 52.9 ug/Kg 106 58 - 125
Xylenes, Total 100 100 ug/Kg 100 70 - 146
1,2-Dichloroethane-d4 (Surr) 60 - 140
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
994-Bromofluorobenzene 45 - 131
100Toluene-d8 (Surr) 58 - 140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-252546/7Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
Gasoline Range Organics (GRO)
-C4-C12
1000 942 ug/Kg 94 70 - 122
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane-d4 (Surr) 60 - 140
Surrogate
104
LCS LCS
Qualifier Limits%Recovery
1014-Bromofluorobenzene 45 - 131
99Toluene-d8 (Surr) 58 - 140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 720-252546/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
1,1,1,2-Tetrachloroethane 50.0 54.5 ug/Kg 109 70 - 130 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 51.6 ug/Kg 103 70 - 130 0 20
1,1,2,2-Tetrachloroethane 50.0 51.4 ug/Kg 103 70 - 146 0 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 55.0 ug/Kg 110 60 - 140 1 20
1,1,2-Trichloroethane 50.0 56.9 ug/Kg 114 70 - 130 2 20
1,1-Dichloroethane 50.0 49.9 ug/Kg 100 70 - 130 1 20
1,1-Dichloroethene 50.0 51.2 ug/Kg 102 74 - 122 5 20
1,1-Dichloropropene 50.0 48.5 ug/Kg 97 70 - 130 0 20
1,2,3-Trichlorobenzene 50.0 55.6 ug/Kg 111 60 - 140 1 20
1,2,3-Trichloropropane 50.0 54.0 ug/Kg 108 70 - 146 1 20
1,2,4-Trichlorobenzene 50.0 54.9 ug/Kg 110 60 - 140 1 20
1,2,4-Trimethylbenzene 50.0 50.2 ug/Kg 100 70 - 130 2 20
1,2-Dibromo-3-Chloropropane 50.0 54.5 ug/Kg 109 60 - 145 1 20
1,2-Dichlorobenzene 50.0 52.8 ug/Kg 106 70 - 130 2 20
1,2-Dichloroethane 50.0 51.6 ug/Kg 103 70 - 130 0 20
1,2-Dichloropropane 50.0 52.2 ug/Kg 104 73 - 127 1 20
1,3,5-Trimethylbenzene 50.0 50.3 ug/Kg 101 70 - 131 2 20
1,3-Dichlorobenzene 50.0 51.4 ug/Kg 103 70 - 131 2 20
TestAmerica Pleasanton
Page 26 of 613
QC Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 720-252546/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
1,3-Dichloropropane 50.0 55.0 ug/Kg 110 70 - 140 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,4-Dichlorobenzene 50.0 51.6 ug/Kg 103 70 - 130 2 20
2,2-Dichloropropane 50.0 50.1 ug/Kg 100 70 - 162 1 20
2-Butanone (MEK) 250 262 ug/Kg 105 59 - 159 2 20
2-Chlorotoluene 50.0 49.0 ug/Kg 98 70 - 138 1 20
2-Hexanone 250 253 ug/Kg 101 62 - 158 1 20
4-Chlorotoluene 50.0 49.5 ug/Kg 99 70 - 136 2 20
4-Isopropyltoluene 50.0 51.3 ug/Kg 103 70 - 133 1 20
4-Methyl-2-pentanone (MIBK) 250 255 ug/Kg 102 60 - 160 0 20
Acetone 250 248 ug/Kg 99 30 - 162 5 30
Benzene 50.0 48.5 ug/Kg 97 70 - 130 0 20
Bromobenzene 50.0 51.5 ug/Kg 103 70 - 130 1 20
Bromoform 50.0 59.6 ug/Kg 119 59 - 158 1 20
Bromomethane 50.0 56.8 ug/Kg 114 59 - 132 0 20
Carbon disulfide 50.0 46.5 ug/Kg 93 60 - 140 0 20
Carbon tetrachloride 50.0 50.9 ug/Kg 102 70 - 142 0 20
Chlorobenzene 50.0 50.9 ug/Kg 102 70 - 130 0 20
Chlorobromomethane 50.0 55.2 ug/Kg 110 70 - 130 0 20
Chlorodibromomethane 50.0 59.4 ug/Kg 119 70 - 146 2 20
Chloroethane 50.0 51.7 ug/Kg 103 65 - 130 0 20
Chloroform 50.0 50.7 ug/Kg 101 77 - 127 0 20
Chloromethane 50.0 51.1 ug/Kg 102 55 - 140 5 20
cis-1,2-Dichloroethene 50.0 48.9 ug/Kg 98 70 - 138 1 20
cis-1,3-Dichloropropene 50.0 57.9 ug/Kg 116 68 - 147 2 20
Dibromomethane 50.0 53.0 ug/Kg 106 70 - 139 0 20
Dichlorobromomethane 50.0 54.0 ug/Kg 108 70 - 140 1 20
Dichlorodifluoromethane 50.0 61.7 ug/Kg 123 37 - 158 1 20
Ethylbenzene 50.0 49.9 ug/Kg 100 80 - 137 1 20
Ethylene Dibromide 50.0 56.5 ug/Kg 113 70 - 140 1 20
Hexachlorobutadiene 50.0 54.7 ug/Kg 109 70 - 132 1 20
Isopropylbenzene 50.0 51.5 ug/Kg 103 70 - 130 0 20
Methyl tert-butyl ether 50.0 59.7 ug/Kg 119 70 - 144 0 20
Methylene Chloride 50.0 50.7 ug/Kg 101 70 - 134 1 20
m-Xylene & p-Xylene 50.0 50.3 ug/Kg 101 70 - 146 1 20
Naphthalene 50.0 53.9 ug/Kg 108 60 - 147 1 20
n-Butylbenzene 50.0 49.3 ug/Kg 99 70 - 142 1 20
N-Propylbenzene 50.0 48.9 ug/Kg 98 70 - 130 1 20
o-Xylene 50.0 50.7 ug/Kg 101 70 - 140 0 20
sec-Butylbenzene 50.0 49.9 ug/Kg 100 70 - 136 1 20
Styrene 50.0 51.1 ug/Kg 102 70 - 130 1 20
tert-Butylbenzene 50.0 50.2 ug/Kg 100 70 - 130 1 20
Tetrachloroethene 50.0 53.1 ug/Kg 106 70 - 132 1 20
Toluene 50.0 49.7 ug/Kg 99 75 - 120 2 20
trans-1,2-Dichloroethene 50.0 50.0 ug/Kg 100 67 - 130 1 20
trans-1,3-Dichloropropene 50.0 56.2 ug/Kg 112 70 - 155 1 20
Trichloroethene 50.0 51.8 ug/Kg 104 70 - 133 1 20
Trichlorofluoromethane 50.0 54.0 ug/Kg 108 60 - 140 2 20
Vinyl acetate 50.0 50.8 ug/Kg 102 38 - 176 1 20
TestAmerica Pleasanton
Page 27 of 613
QC Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 720-252546/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
Vinyl chloride 50.0 52.8 ug/Kg 106 58 - 125 0 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Xylenes, Total 100 101 ug/Kg 101 70 - 146 1 20
1,2-Dichloroethane-d4 (Surr) 60 - 140
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
994-Bromofluorobenzene 45 - 131
101Toluene-d8 (Surr) 58 - 140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 720-252546/8Matrix: Solid Prep Type: Total/NAAnalysis Batch: 252546
Gasoline Range Organics (GRO)
-C4-C12
1000 916 ug/Kg 92 70 - 122 3 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,2-Dichloroethane-d4 (Surr) 60 - 140
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
1014-Bromofluorobenzene 45 - 131
97Toluene-d8 (Surr) 58 - 140
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 720-251971/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 252166 Prep Batch: 251971
RL MDL
Phenol 0.0177 J 0.067 0.011 mg/Kg 09/21/18 13:13 09/25/18 20:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0140.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Bis(2-chloroethyl)ether
ND 0.00740.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 12-Chlorophenol
0.0190 J 0.00800.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 11,3-Dichlorobenzene
0.0194 J 0.0180.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 11,4-Dichlorobenzene
ND 0.0100.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Benzyl alcohol
0.0157 J 0.00940.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 11,2-Dichlorobenzene
ND 0.0100.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 12-Methylphenol
ND 0.0190.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Methylphenol, 3 & 4
ND 0.0660.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 1N-Nitrosodi-n-propylamine
ND 0.0660.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Hexachloroethane
0.0344 J 0.0280.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Nitrobenzene
0.0212 J 0.00940.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Isophorone
ND 0.0660.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 12-Nitrophenol
ND 0.0540.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 12,4-Dimethylphenol
ND 0.0110.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Bis(2-chloroethoxy)methane
ND 0.00900.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 12,4-Dichlorophenol
ND 0.0140.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 11,2,4-Trichlorobenzene
ND 0.0660.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Naphthalene
ND 0.00880.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 14-Chloroaniline
TestAmerica Pleasanton
Page 28 of 613
QC Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 720-251971/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 252166 Prep Batch: 251971
RL MDL
Hexachlorobutadiene 0.0126 J 0.067 0.010 mg/Kg 09/21/18 13:13 09/25/18 20:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0110.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 14-Chloro-3-methylphenol
ND 0.0120.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 12-Methylnaphthalene
ND 0.0540.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Hexachlorocyclopentadiene
ND 0.0200.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 12,4,6-Trichlorophenol
ND 0.00840.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 12,4,5-Trichlorophenol
ND 0.00960.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 12-Chloronaphthalene
ND 0.0680.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 12-Nitroaniline
ND 0.0120.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Dimethyl phthalate
0.0200 J 0.0110.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Acenaphthylene
ND 0.0780.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 13-Nitroaniline
ND 0.00760.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Acenaphthene
ND 0.130.66 mg/Kg 09/21/18 13:13 09/25/18 20:23 12,4-Dinitrophenol
ND 0.0680.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 14-Nitrophenol
ND 0.0110.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Dibenzofuran
ND 0.0660.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 12,4-Dinitrotoluene
ND 0.0680.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 12,6-Dinitrotoluene
ND 0.00940.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Diethyl phthalate
ND 0.0120.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 14-Chlorophenyl phenyl ether
ND 0.00800.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Fluorene
ND 0.0660.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 14-Nitroaniline
ND 0.0680.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 12-Methyl-4,6-dinitrophenol
ND 0.00780.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1N-Nitrosodiphenylamine
ND 0.0100.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 14-Bromophenyl phenyl ether
ND 0.0660.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Hexachlorobenzene
ND 0.130.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Pentachlorophenol
ND 0.0660.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Phenanthrene
0.00946 J 0.00860.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Anthracene
ND 0.0660.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Di-n-butyl phthalate
ND 0.0150.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Fluoranthene
ND 0.00760.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Pyrene
ND 0.0110.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Butyl benzyl phthalate
ND 0.0200.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 13,3'-Dichlorobenzidine
ND 0.0360.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Benzo[a]anthracene
ND 0.0130.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Bis(2-ethylhexyl) phthalate
ND 0.0660.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Chrysene
ND 0.00960.17 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Di-n-octyl phthalate
ND 0.0190.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Benzo[b]fluoranthene
0.0295 J 0.0130.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Benzo[a]pyrene
ND 0.0280.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Benzo[k]fluoranthene
0.0284 J 0.0260.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Indeno[1,2,3-cd]pyrene
ND 0.0400.13 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Benzo[g,h,i]perylene
ND 0.0680.33 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Benzoic acid
ND 0.0120.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Azobenzene
ND 0.0300.067 mg/Kg 09/21/18 13:13 09/25/18 20:23 1Dibenz(a,h)anthracene
Nitrobenzene-d5 65 21 - 98 09/25/18 20:23 1
MB MB
Surrogate
09/21/18 13:13
Dil FacPrepared AnalyzedQualifier Limits%Recovery
TestAmerica Pleasanton
Page 29 of 613
QC Sample ResultsTestAmerica Job ID: 720-88635-1Client: Engineering Remediation Resources Group.
Project/Site: Soil Removal for HPNS Crime Lab
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 720-251971/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 252166 Prep Batch: 251971
2-Fluorobiphenyl 72 30 - 112 09/25/18 20:23 1
MB MB
Surrogate
09/21/18 13:13
Dil FacPrepared AnalyzedQualifier Limits%Recovery
92 09/21/18 13:13 09/25/18 20:23 1Terphenyl-d14 59 - 134
75 09/21/18 13:13 09/25/18 20:23 12-Fluorophenol 28 - 98
76 09/21/18 13:13 09/25/18 20:23 1Phenol-d5 23 - 101
61 09/21/18 13:13 09/25/18 20:23 12,4,6-Tribromophenol 37 - 114
Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-251971/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 252166 Prep Batch: 251971
Phenol 2.67 2.05 mg/Kg 77 48 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Bis(2-chloroethyl)ether 2.67 1.92 mg/Kg 72 40 - 110
2-Chlorophenol 2.67 2.21 mg/Kg 83 45 - 110
1,3-Dichlorobenzene 2.67 1.92 mg/Kg 72 38 - 110
1