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Transport of Static and Fal
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cs Study on the Liquid Entrapment and Melt Transport of Static
and Falling-Film Melt Crystallization - Industrial &
Engineering Chemistry Research (ACS Publications)
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Abstract
Kinetics Study on the Liquid Entrapment and Melt Transport of
Static
and Falling-Film Melt Crystallization
Xiaobin Jiang , Baohong Hou , Yingying Zhao ,
ingkang Wang*, and Meijing Zhang
School of Chemical Engineering and Technology,
tate Research Center of Industrialization for
Crystallization Technology, Tianjin University, Tianjin
00072, Peoples Republic of China
Engineering Research Center of Seawater Utilization
Technology of Ministry of Education, Hebei University
of Technology, Tianjin 300130, Peoples Republic of
China
nd. Eng. Chem. Res., 2012, 51 (13), pp 50375044
DOI: 10.1021/ie202615b
ublication Date (Web): March 9, 2012
Copyright 2012 American Chemical Society
Tel.: +86 02227405754 . Fax: +86-22-27374971. E-
mail: [email protected].
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History
Published In IssueApril 04, 2012
Article ASAPMarch 22, 2012
Just Accepted ManuscriptMarch 09, 2012
Received: November 13, 2011Accepted: March 08, 2012Revised:
March 07, 2012
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Section: Industrial Inorganic Chemicals
Experiments were carried out to study the kinetics of crystal
growth and the sweating
process in two kinds of melt crystallization modes: static melt
crystallization (SMC) and
falling-film melt crystallization (FFMC). The system utilized in
this paper was hyperpure
phosphoric acid with water and trace amounts of metal ions as
impurities. The kinetic
experimental data of crystal growth, liquid entrapment, and the
melt-transport process were
well fitted by power function equations (R2 > 0.947). The
fractal and porous media theories
were introduced to improve the model of melt transport and
explain the difference between
the two modes. The separation efficiencies of SMC and FFMC on
different ion impurities
were compared. The SMC mode separated calcium and ferrum ions
with higher efficiency
than the FFMC mode, while the FFMC mode separated sodium and
magnesium ions better
than the SMC mode. A combined operation mode was suggested to
prepare hyperpure
phosphoric acid in industrial applications.
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