34
) .u .a January 24, 1987 u.s.!.P.A. !nvt ronaaatal Sarvteat lunch Ln:in1ton, HA Attn : Prank Lilley Dear Prank 1 Enc:loaad are copha of tnforaatton eoncarntnc tha "vault" aad aurroundtna area at tha Myaua Chaatcal Stta in Aahlancl, Haaaachuaatta. In addition, tha followtna tnforaatton haa bean IJttractad froa vartou1 lftlinaartnc reporta oa tha valtavataa· traataaant ayataa at tha etta: - 1 O!QI report by Irian Kelleher (1910) atatad that ( tha collection pit ••• rephcad betvaan 1965 and 1961, thh hu not bean conftraad - a 1965 plan by llooafield Phnta lhow the inflow and outflow for the colhetton baata h at ita ':J aortharn and - tnforaatton fro• Stlavn O'Connor (lyacol) tadtcatad that a ureu erack (1/16") nhtl on tha aorth of the butn - a 1972 report bJ lunnala atatad that tha collection hdn is approxi•atelr 37 ' x 77 ' xI' (14,000 cubic. feet) - aerial photoa indicate the baain ••• covered batvea n 1979 and 1981 If I unc.o•er anr additiond pertinent infor•ation 1 vill forward it to rou. In the •eanti•a, should you have any quaationa, don ' t haaitata to ca.ll •• at 935-1160.

LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

  • Upload
    others

  • View
    1

  • Download
    0

Embed Size (px)

Citation preview

Page 1: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) u a

January 24 1987

usPA nvt ronaaatal Sarvteat lunch Lnin1ton HA

Attn Prank Lilley

Dear Prank 1

Encloaad are copha of tnforaatton eoncarntnc tha vault aad aurroundtna area at tha Myaua Chaatcal Stta in Aahlancl Haaaachuaatta

In addition tha followtna tnforaatton haa bean IJttractad froa vartou1 lftlinaartnc reporta oa tha valtavataamiddot traataaant ayataa at tha etta

- 1 OQI report by Irian Kelleher (1910) atatad that (tha collection pit bullbullbull rephcad betvaan 1965 and 1961 thh hu not bean conftraad

- a 1965 plan by llooafield bull Phnta lhow the inflow and outflow for the colhetton baata h at itaJ aortharn and

- tnforaatton frobull Stlavn OConnor (lyacol) tadtcatad that a ureu erack (116) nhtl on tha aorth tU~ of the butn

- a 1972 report bJ lunnala atatad that tha collection hdn is approxibullatelr 37 x 77 xI (14000 cubic feet)

- aerial photoa indicate the baain bullbullbull covered batvean 1979 and 1981

If I uncobuller anr additiond pertinent inforbullation 1 vill forward it to rou In the bulleantibulla should you have any quaationa don t haaitata to call bullbull at 935-1160

)

I

=

oi

4shy

)

I I I I

1UtS ~- 11111

-r

140

I l__

JillurbullIImiddotfrrl

II

IfIll f fl

I z z N n

X

~ n

~ i 0

) _-- -_

l_

111011bull

Richard Batea

Richard J DeLuca

NYANZA Chemical Site Groundwater Sampling

814BS

L Chappell R Cleary w Siok T Schleaaer lt Burger

MEMOIWIDUM

bull ~~- _middotbull bull - ~~te ~~middot~J~middot middot~ J f~ CCI

lQEt~c~middot ~~a_ 1~n

I

On AUu8t 2 1985 Wehran Engineerin waa taaked by the MUaachuaetta Department of Environmental Quality Enineerinq (MDQE) to collect aix groundwater aamplea at the NYANZA Chemical aite located in Mhlancl Maaaachuaetta On Auquat 5 1985 Wehran attenced a meeting with the IIDampQamp Taak Manager to define the auaplin requirnta

Wahran ampnginHrinqa aaraplinq tau at with MDEOI repreaentativea on AU9IIIt 7 1115 at the NYANZA Chemical aite at 8 30 am The Wehran aupliq tea cooailted of R J DeLuca JD Graa an4 Mr Richter IIDIQI rapraHntativea wra Lynna Chappell and Pat Donahue Upon cbeckin9 in with the property ownerbull the Wehran aamplift9 tau and MDIQI ~ncecl the aampla collection The clataib of the aampla collection per well are ictentifiecl in Attachment I A blank waa alao collected in be field fra deioniamped water and aaained nlllber MW-10

The weather durinv the aampJaple collection vaa partly cloucly with teraturea in the aidcUe eoI A brief rainahover occured during the a-le collection the duration waa approxtately five llinutea ampaiDfa 1 for the previoua abc cSaya in Au9llt totaled 0 28 incbea aa reported by the Worceatar Airport

Channel 7 Neva arrivecl at Wall 8 and filme4 the aampling crew durinq well purvinq however dicl not requeat any information from Whran lllployeea MDIQI paraonnal handled the cOftlftlftication vith the neva media

Sample collection waa completed by the end of the day on Auguat 7 1915 Samplebull were placed on ice upon collection and kept cool until daliverecl to the laboratory on Auquat 8 1985 All aamplea numberbull were recorded on chain of cu1tody form numbera 432 4363 and 4364 and all aaplea ware placed in a cooler with chain of cuatody tapa (No 30640) Samplebull were relinquiahad to ERT at 1050 on Auguat 8 1985 Three aarnplaa could not be field filtered poaaibly due to the nature of the contaminanta however all aamplea were filtered in the laboratory to provide di11olvad metal concentrations The following attachments are provided bullbull part of this product

Attachment I Fielcl Data Swnnary Attachment II Boring Logs and Wall Construction Attachment III Analytical Resulta

v Attachment IV Health ancl Safety Plan Attachment v Personnel and Equipment

middotmiddot (

(

ATlACIIIIZIIT I

rield Datbull a-ry

C middot C

(l jlTE NAMpound1 Nyanza CheMiCal

8

Wll Dtter

Well DetJih jJJ 0 n btl9W tgg or geeing

etattc wLbull jl OS n belqw 99 pf eeinp

ca

aackaround a PM

acUng bull sg co - at 3 tncfl above top of caetng

I --1amp fOI Calculating fbullebullbull petbull

Matte HaO Volue cu

ure - abullbullcY bull ta CO lUI

Y bull 38911 ua OlU eofdud t vUy - Ul79 UlllhOe

pH - s 9av bull sas 3V bull 175 gallons

Notbullbullbull llood recharge

Puraed collected tn 70 gallon drUM Wter very cUbulleolored having a dark red tint lldth the conetstency of vegetable ot 1

l

(

0S ITE NAMpoundbull _

4 0 f belpw SAP pf SAliDAWll Depth

4 11 n belpn tee gt seeingltatie WL

WAter ColUIIFI

fl elf J)tSA POtMula for C l culat i ng Sta U c HaO Yol __ U ) CJ Y bull a CO lUI

QONiuct iY U y - M l O Ulllhoev bull oM a cubull o t63

- bull a v bull a ~ 216

Purged bullater collctci in 70 gallon dru HNu reacUnabull Not in the drUM bull Mater was pou1ed into the drU bullbullcclbulld

eo PPfllbull Water wabull vry di~lo-cl a dark red tint with the cotbullteney of vegetable oil

8ailci well dry approMiMamptely 1 yenoluMe ce gallons)

Allow Nell to recharge for 20 etnutbullbullmiddot

Wter lel after lechargbull 27 n bttlow top of caeing

laUH Nell dry agatn- alloecl well to recharge for

4S etnutbullbullmiddot

Tot a l volu- purged 11 gallonbullmiddot

SAMple collected at 1245 honlbull

lti~l=t (~ Jfill

I z OJgt ltz ~~ lgt O or

~ z~ ~n

~I ~a~

~

ill ini

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 2: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

)

I

=

oi

4shy

)

I I I I

1UtS ~- 11111

-r

140

I l__

JillurbullIImiddotfrrl

II

IfIll f fl

I z z N n

X

~ n

~ i 0

) _-- -_

l_

111011bull

Richard Batea

Richard J DeLuca

NYANZA Chemical Site Groundwater Sampling

814BS

L Chappell R Cleary w Siok T Schleaaer lt Burger

MEMOIWIDUM

bull ~~- _middotbull bull - ~~te ~~middot~J~middot middot~ J f~ CCI

lQEt~c~middot ~~a_ 1~n

I

On AUu8t 2 1985 Wehran Engineerin waa taaked by the MUaachuaetta Department of Environmental Quality Enineerinq (MDQE) to collect aix groundwater aamplea at the NYANZA Chemical aite located in Mhlancl Maaaachuaetta On Auquat 5 1985 Wehran attenced a meeting with the IIDampQamp Taak Manager to define the auaplin requirnta

Wahran ampnginHrinqa aaraplinq tau at with MDEOI repreaentativea on AU9IIIt 7 1115 at the NYANZA Chemical aite at 8 30 am The Wehran aupliq tea cooailted of R J DeLuca JD Graa an4 Mr Richter IIDIQI rapraHntativea wra Lynna Chappell and Pat Donahue Upon cbeckin9 in with the property ownerbull the Wehran aamplift9 tau and MDIQI ~ncecl the aampla collection The clataib of the aampla collection per well are ictentifiecl in Attachment I A blank waa alao collected in be field fra deioniamped water and aaained nlllber MW-10

The weather durinv the aampJaple collection vaa partly cloucly with teraturea in the aidcUe eoI A brief rainahover occured during the a-le collection the duration waa approxtately five llinutea ampaiDfa 1 for the previoua abc cSaya in Au9llt totaled 0 28 incbea aa reported by the Worceatar Airport

Channel 7 Neva arrivecl at Wall 8 and filme4 the aampling crew durinq well purvinq however dicl not requeat any information from Whran lllployeea MDIQI paraonnal handled the cOftlftlftication vith the neva media

Sample collection waa completed by the end of the day on Auguat 7 1915 Samplebull were placed on ice upon collection and kept cool until daliverecl to the laboratory on Auquat 8 1985 All aamplea numberbull were recorded on chain of cu1tody form numbera 432 4363 and 4364 and all aaplea ware placed in a cooler with chain of cuatody tapa (No 30640) Samplebull were relinquiahad to ERT at 1050 on Auguat 8 1985 Three aarnplaa could not be field filtered poaaibly due to the nature of the contaminanta however all aamplea were filtered in the laboratory to provide di11olvad metal concentrations The following attachments are provided bullbull part of this product

Attachment I Fielcl Data Swnnary Attachment II Boring Logs and Wall Construction Attachment III Analytical Resulta

v Attachment IV Health ancl Safety Plan Attachment v Personnel and Equipment

middotmiddot (

(

ATlACIIIIZIIT I

rield Datbull a-ry

C middot C

(l jlTE NAMpound1 Nyanza CheMiCal

8

Wll Dtter

Well DetJih jJJ 0 n btl9W tgg or geeing

etattc wLbull jl OS n belqw 99 pf eeinp

ca

aackaround a PM

acUng bull sg co - at 3 tncfl above top of caetng

I --1amp fOI Calculating fbullebullbull petbull

Matte HaO Volue cu

ure - abullbullcY bull ta CO lUI

Y bull 38911 ua OlU eofdud t vUy - Ul79 UlllhOe

pH - s 9av bull sas 3V bull 175 gallons

Notbullbullbull llood recharge

Puraed collected tn 70 gallon drUM Wter very cUbulleolored having a dark red tint lldth the conetstency of vegetable ot 1

l

(

0S ITE NAMpoundbull _

4 0 f belpw SAP pf SAliDAWll Depth

4 11 n belpn tee gt seeingltatie WL

WAter ColUIIFI

fl elf J)tSA POtMula for C l culat i ng Sta U c HaO Yol __ U ) CJ Y bull a CO lUI

QONiuct iY U y - M l O Ulllhoev bull oM a cubull o t63

- bull a v bull a ~ 216

Purged bullater collctci in 70 gallon dru HNu reacUnabull Not in the drUM bull Mater was pou1ed into the drU bullbullcclbulld

eo PPfllbull Water wabull vry di~lo-cl a dark red tint with the cotbullteney of vegetable oil

8ailci well dry approMiMamptely 1 yenoluMe ce gallons)

Allow Nell to recharge for 20 etnutbullbullmiddot

Wter lel after lechargbull 27 n bttlow top of caeing

laUH Nell dry agatn- alloecl well to recharge for

4S etnutbullbullmiddot

Tot a l volu- purged 11 gallonbullmiddot

SAMple collected at 1245 honlbull

lti~l=t (~ Jfill

I z OJgt ltz ~~ lgt O or

~ z~ ~n

~I ~a~

~

ill ini

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 3: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

)

I I I I

1UtS ~- 11111

-r

140

I l__

JillurbullIImiddotfrrl

II

IfIll f fl

I z z N n

X

~ n

~ i 0

) _-- -_

l_

111011bull

Richard Batea

Richard J DeLuca

NYANZA Chemical Site Groundwater Sampling

814BS

L Chappell R Cleary w Siok T Schleaaer lt Burger

MEMOIWIDUM

bull ~~- _middotbull bull - ~~te ~~middot~J~middot middot~ J f~ CCI

lQEt~c~middot ~~a_ 1~n

I

On AUu8t 2 1985 Wehran Engineerin waa taaked by the MUaachuaetta Department of Environmental Quality Enineerinq (MDQE) to collect aix groundwater aamplea at the NYANZA Chemical aite located in Mhlancl Maaaachuaetta On Auquat 5 1985 Wehran attenced a meeting with the IIDampQamp Taak Manager to define the auaplin requirnta

Wahran ampnginHrinqa aaraplinq tau at with MDEOI repreaentativea on AU9IIIt 7 1115 at the NYANZA Chemical aite at 8 30 am The Wehran aupliq tea cooailted of R J DeLuca JD Graa an4 Mr Richter IIDIQI rapraHntativea wra Lynna Chappell and Pat Donahue Upon cbeckin9 in with the property ownerbull the Wehran aamplift9 tau and MDIQI ~ncecl the aampla collection The clataib of the aampla collection per well are ictentifiecl in Attachment I A blank waa alao collected in be field fra deioniamped water and aaained nlllber MW-10

The weather durinv the aampJaple collection vaa partly cloucly with teraturea in the aidcUe eoI A brief rainahover occured during the a-le collection the duration waa approxtately five llinutea ampaiDfa 1 for the previoua abc cSaya in Au9llt totaled 0 28 incbea aa reported by the Worceatar Airport

Channel 7 Neva arrivecl at Wall 8 and filme4 the aampling crew durinq well purvinq however dicl not requeat any information from Whran lllployeea MDIQI paraonnal handled the cOftlftlftication vith the neva media

Sample collection waa completed by the end of the day on Auguat 7 1915 Samplebull were placed on ice upon collection and kept cool until daliverecl to the laboratory on Auquat 8 1985 All aamplea numberbull were recorded on chain of cu1tody form numbera 432 4363 and 4364 and all aaplea ware placed in a cooler with chain of cuatody tapa (No 30640) Samplebull were relinquiahad to ERT at 1050 on Auguat 8 1985 Three aarnplaa could not be field filtered poaaibly due to the nature of the contaminanta however all aamplea were filtered in the laboratory to provide di11olvad metal concentrations The following attachments are provided bullbull part of this product

Attachment I Fielcl Data Swnnary Attachment II Boring Logs and Wall Construction Attachment III Analytical Resulta

v Attachment IV Health ancl Safety Plan Attachment v Personnel and Equipment

middotmiddot (

(

ATlACIIIIZIIT I

rield Datbull a-ry

C middot C

(l jlTE NAMpound1 Nyanza CheMiCal

8

Wll Dtter

Well DetJih jJJ 0 n btl9W tgg or geeing

etattc wLbull jl OS n belqw 99 pf eeinp

ca

aackaround a PM

acUng bull sg co - at 3 tncfl above top of caetng

I --1amp fOI Calculating fbullebullbull petbull

Matte HaO Volue cu

ure - abullbullcY bull ta CO lUI

Y bull 38911 ua OlU eofdud t vUy - Ul79 UlllhOe

pH - s 9av bull sas 3V bull 175 gallons

Notbullbullbull llood recharge

Puraed collected tn 70 gallon drUM Wter very cUbulleolored having a dark red tint lldth the conetstency of vegetable ot 1

l

(

0S ITE NAMpoundbull _

4 0 f belpw SAP pf SAliDAWll Depth

4 11 n belpn tee gt seeingltatie WL

WAter ColUIIFI

fl elf J)tSA POtMula for C l culat i ng Sta U c HaO Yol __ U ) CJ Y bull a CO lUI

QONiuct iY U y - M l O Ulllhoev bull oM a cubull o t63

- bull a v bull a ~ 216

Purged bullater collctci in 70 gallon dru HNu reacUnabull Not in the drUM bull Mater was pou1ed into the drU bullbullcclbulld

eo PPfllbull Water wabull vry di~lo-cl a dark red tint with the cotbullteney of vegetable oil

8ailci well dry approMiMamptely 1 yenoluMe ce gallons)

Allow Nell to recharge for 20 etnutbullbullmiddot

Wter lel after lechargbull 27 n bttlow top of caeing

laUH Nell dry agatn- alloecl well to recharge for

4S etnutbullbullmiddot

Tot a l volu- purged 11 gallonbullmiddot

SAMple collected at 1245 honlbull

lti~l=t (~ Jfill

I z OJgt ltz ~~ lgt O or

~ z~ ~n

~I ~a~

~

ill ini

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 4: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

I I I I

1UtS ~- 11111

-r

140

I l__

JillurbullIImiddotfrrl

II

IfIll f fl

I z z N n

X

~ n

~ i 0

) _-- -_

l_

111011bull

Richard Batea

Richard J DeLuca

NYANZA Chemical Site Groundwater Sampling

814BS

L Chappell R Cleary w Siok T Schleaaer lt Burger

MEMOIWIDUM

bull ~~- _middotbull bull - ~~te ~~middot~J~middot middot~ J f~ CCI

lQEt~c~middot ~~a_ 1~n

I

On AUu8t 2 1985 Wehran Engineerin waa taaked by the MUaachuaetta Department of Environmental Quality Enineerinq (MDQE) to collect aix groundwater aamplea at the NYANZA Chemical aite located in Mhlancl Maaaachuaetta On Auquat 5 1985 Wehran attenced a meeting with the IIDampQamp Taak Manager to define the auaplin requirnta

Wahran ampnginHrinqa aaraplinq tau at with MDEOI repreaentativea on AU9IIIt 7 1115 at the NYANZA Chemical aite at 8 30 am The Wehran aupliq tea cooailted of R J DeLuca JD Graa an4 Mr Richter IIDIQI rapraHntativea wra Lynna Chappell and Pat Donahue Upon cbeckin9 in with the property ownerbull the Wehran aamplift9 tau and MDIQI ~ncecl the aampla collection The clataib of the aampla collection per well are ictentifiecl in Attachment I A blank waa alao collected in be field fra deioniamped water and aaained nlllber MW-10

The weather durinv the aampJaple collection vaa partly cloucly with teraturea in the aidcUe eoI A brief rainahover occured during the a-le collection the duration waa approxtately five llinutea ampaiDfa 1 for the previoua abc cSaya in Au9llt totaled 0 28 incbea aa reported by the Worceatar Airport

Channel 7 Neva arrivecl at Wall 8 and filme4 the aampling crew durinq well purvinq however dicl not requeat any information from Whran lllployeea MDIQI paraonnal handled the cOftlftlftication vith the neva media

Sample collection waa completed by the end of the day on Auguat 7 1915 Samplebull were placed on ice upon collection and kept cool until daliverecl to the laboratory on Auquat 8 1985 All aamplea numberbull were recorded on chain of cu1tody form numbera 432 4363 and 4364 and all aaplea ware placed in a cooler with chain of cuatody tapa (No 30640) Samplebull were relinquiahad to ERT at 1050 on Auguat 8 1985 Three aarnplaa could not be field filtered poaaibly due to the nature of the contaminanta however all aamplea were filtered in the laboratory to provide di11olvad metal concentrations The following attachments are provided bullbull part of this product

Attachment I Fielcl Data Swnnary Attachment II Boring Logs and Wall Construction Attachment III Analytical Resulta

v Attachment IV Health ancl Safety Plan Attachment v Personnel and Equipment

middotmiddot (

(

ATlACIIIIZIIT I

rield Datbull a-ry

C middot C

(l jlTE NAMpound1 Nyanza CheMiCal

8

Wll Dtter

Well DetJih jJJ 0 n btl9W tgg or geeing

etattc wLbull jl OS n belqw 99 pf eeinp

ca

aackaround a PM

acUng bull sg co - at 3 tncfl above top of caetng

I --1amp fOI Calculating fbullebullbull petbull

Matte HaO Volue cu

ure - abullbullcY bull ta CO lUI

Y bull 38911 ua OlU eofdud t vUy - Ul79 UlllhOe

pH - s 9av bull sas 3V bull 175 gallons

Notbullbullbull llood recharge

Puraed collected tn 70 gallon drUM Wter very cUbulleolored having a dark red tint lldth the conetstency of vegetable ot 1

l

(

0S ITE NAMpoundbull _

4 0 f belpw SAP pf SAliDAWll Depth

4 11 n belpn tee gt seeingltatie WL

WAter ColUIIFI

fl elf J)tSA POtMula for C l culat i ng Sta U c HaO Yol __ U ) CJ Y bull a CO lUI

QONiuct iY U y - M l O Ulllhoev bull oM a cubull o t63

- bull a v bull a ~ 216

Purged bullater collctci in 70 gallon dru HNu reacUnabull Not in the drUM bull Mater was pou1ed into the drU bullbullcclbulld

eo PPfllbull Water wabull vry di~lo-cl a dark red tint with the cotbullteney of vegetable oil

8ailci well dry approMiMamptely 1 yenoluMe ce gallons)

Allow Nell to recharge for 20 etnutbullbullmiddot

Wter lel after lechargbull 27 n bttlow top of caeing

laUH Nell dry agatn- alloecl well to recharge for

4S etnutbullbullmiddot

Tot a l volu- purged 11 gallonbullmiddot

SAMple collected at 1245 honlbull

lti~l=t (~ Jfill

I z OJgt ltz ~~ lgt O or

~ z~ ~n

~I ~a~

~

ill ini

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 5: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) _-- -_

l_

111011bull

Richard Batea

Richard J DeLuca

NYANZA Chemical Site Groundwater Sampling

814BS

L Chappell R Cleary w Siok T Schleaaer lt Burger

MEMOIWIDUM

bull ~~- _middotbull bull - ~~te ~~middot~J~middot middot~ J f~ CCI

lQEt~c~middot ~~a_ 1~n

I

On AUu8t 2 1985 Wehran Engineerin waa taaked by the MUaachuaetta Department of Environmental Quality Enineerinq (MDQE) to collect aix groundwater aamplea at the NYANZA Chemical aite located in Mhlancl Maaaachuaetta On Auquat 5 1985 Wehran attenced a meeting with the IIDampQamp Taak Manager to define the auaplin requirnta

Wahran ampnginHrinqa aaraplinq tau at with MDEOI repreaentativea on AU9IIIt 7 1115 at the NYANZA Chemical aite at 8 30 am The Wehran aupliq tea cooailted of R J DeLuca JD Graa an4 Mr Richter IIDIQI rapraHntativea wra Lynna Chappell and Pat Donahue Upon cbeckin9 in with the property ownerbull the Wehran aamplift9 tau and MDIQI ~ncecl the aampla collection The clataib of the aampla collection per well are ictentifiecl in Attachment I A blank waa alao collected in be field fra deioniamped water and aaained nlllber MW-10

The weather durinv the aampJaple collection vaa partly cloucly with teraturea in the aidcUe eoI A brief rainahover occured during the a-le collection the duration waa approxtately five llinutea ampaiDfa 1 for the previoua abc cSaya in Au9llt totaled 0 28 incbea aa reported by the Worceatar Airport

Channel 7 Neva arrivecl at Wall 8 and filme4 the aampling crew durinq well purvinq however dicl not requeat any information from Whran lllployeea MDIQI paraonnal handled the cOftlftlftication vith the neva media

Sample collection waa completed by the end of the day on Auguat 7 1915 Samplebull were placed on ice upon collection and kept cool until daliverecl to the laboratory on Auquat 8 1985 All aamplea numberbull were recorded on chain of cu1tody form numbera 432 4363 and 4364 and all aaplea ware placed in a cooler with chain of cuatody tapa (No 30640) Samplebull were relinquiahad to ERT at 1050 on Auguat 8 1985 Three aarnplaa could not be field filtered poaaibly due to the nature of the contaminanta however all aamplea were filtered in the laboratory to provide di11olvad metal concentrations The following attachments are provided bullbull part of this product

Attachment I Fielcl Data Swnnary Attachment II Boring Logs and Wall Construction Attachment III Analytical Resulta

v Attachment IV Health ancl Safety Plan Attachment v Personnel and Equipment

middotmiddot (

(

ATlACIIIIZIIT I

rield Datbull a-ry

C middot C

(l jlTE NAMpound1 Nyanza CheMiCal

8

Wll Dtter

Well DetJih jJJ 0 n btl9W tgg or geeing

etattc wLbull jl OS n belqw 99 pf eeinp

ca

aackaround a PM

acUng bull sg co - at 3 tncfl above top of caetng

I --1amp fOI Calculating fbullebullbull petbull

Matte HaO Volue cu

ure - abullbullcY bull ta CO lUI

Y bull 38911 ua OlU eofdud t vUy - Ul79 UlllhOe

pH - s 9av bull sas 3V bull 175 gallons

Notbullbullbull llood recharge

Puraed collected tn 70 gallon drUM Wter very cUbulleolored having a dark red tint lldth the conetstency of vegetable ot 1

l

(

0S ITE NAMpoundbull _

4 0 f belpw SAP pf SAliDAWll Depth

4 11 n belpn tee gt seeingltatie WL

WAter ColUIIFI

fl elf J)tSA POtMula for C l culat i ng Sta U c HaO Yol __ U ) CJ Y bull a CO lUI

QONiuct iY U y - M l O Ulllhoev bull oM a cubull o t63

- bull a v bull a ~ 216

Purged bullater collctci in 70 gallon dru HNu reacUnabull Not in the drUM bull Mater was pou1ed into the drU bullbullcclbulld

eo PPfllbull Water wabull vry di~lo-cl a dark red tint with the cotbullteney of vegetable oil

8ailci well dry approMiMamptely 1 yenoluMe ce gallons)

Allow Nell to recharge for 20 etnutbullbullmiddot

Wter lel after lechargbull 27 n bttlow top of caeing

laUH Nell dry agatn- alloecl well to recharge for

4S etnutbullbullmiddot

Tot a l volu- purged 11 gallonbullmiddot

SAMple collected at 1245 honlbull

lti~l=t (~ Jfill

I z OJgt ltz ~~ lgt O or

~ z~ ~n

~I ~a~

~

ill ini

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 6: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

middotmiddot (

(

ATlACIIIIZIIT I

rield Datbull a-ry

C middot C

(l jlTE NAMpound1 Nyanza CheMiCal

8

Wll Dtter

Well DetJih jJJ 0 n btl9W tgg or geeing

etattc wLbull jl OS n belqw 99 pf eeinp

ca

aackaround a PM

acUng bull sg co - at 3 tncfl above top of caetng

I --1amp fOI Calculating fbullebullbull petbull

Matte HaO Volue cu

ure - abullbullcY bull ta CO lUI

Y bull 38911 ua OlU eofdud t vUy - Ul79 UlllhOe

pH - s 9av bull sas 3V bull 175 gallons

Notbullbullbull llood recharge

Puraed collected tn 70 gallon drUM Wter very cUbulleolored having a dark red tint lldth the conetstency of vegetable ot 1

l

(

0S ITE NAMpoundbull _

4 0 f belpw SAP pf SAliDAWll Depth

4 11 n belpn tee gt seeingltatie WL

WAter ColUIIFI

fl elf J)tSA POtMula for C l culat i ng Sta U c HaO Yol __ U ) CJ Y bull a CO lUI

QONiuct iY U y - M l O Ulllhoev bull oM a cubull o t63

- bull a v bull a ~ 216

Purged bullater collctci in 70 gallon dru HNu reacUnabull Not in the drUM bull Mater was pou1ed into the drU bullbullcclbulld

eo PPfllbull Water wabull vry di~lo-cl a dark red tint with the cotbullteney of vegetable oil

8ailci well dry approMiMamptely 1 yenoluMe ce gallons)

Allow Nell to recharge for 20 etnutbullbullmiddot

Wter lel after lechargbull 27 n bttlow top of caeing

laUH Nell dry agatn- alloecl well to recharge for

4S etnutbullbullmiddot

Tot a l volu- purged 11 gallonbullmiddot

SAMple collected at 1245 honlbull

lti~l=t (~ Jfill

I z OJgt ltz ~~ lgt O or

~ z~ ~n

~I ~a~

~

ill ini

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 7: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

C middot C

(l jlTE NAMpound1 Nyanza CheMiCal

8

Wll Dtter

Well DetJih jJJ 0 n btl9W tgg or geeing

etattc wLbull jl OS n belqw 99 pf eeinp

ca

aackaround a PM

acUng bull sg co - at 3 tncfl above top of caetng

I --1amp fOI Calculating fbullebullbull petbull

Matte HaO Volue cu

ure - abullbullcY bull ta CO lUI

Y bull 38911 ua OlU eofdud t vUy - Ul79 UlllhOe

pH - s 9av bull sas 3V bull 175 gallons

Notbullbullbull llood recharge

Puraed collected tn 70 gallon drUM Wter very cUbulleolored having a dark red tint lldth the conetstency of vegetable ot 1

l

(

0S ITE NAMpoundbull _

4 0 f belpw SAP pf SAliDAWll Depth

4 11 n belpn tee gt seeingltatie WL

WAter ColUIIFI

fl elf J)tSA POtMula for C l culat i ng Sta U c HaO Yol __ U ) CJ Y bull a CO lUI

QONiuct iY U y - M l O Ulllhoev bull oM a cubull o t63

- bull a v bull a ~ 216

Purged bullater collctci in 70 gallon dru HNu reacUnabull Not in the drUM bull Mater was pou1ed into the drU bullbullcclbulld

eo PPfllbull Water wabull vry di~lo-cl a dark red tint with the cotbullteney of vegetable oil

8ailci well dry approMiMamptely 1 yenoluMe ce gallons)

Allow Nell to recharge for 20 etnutbullbullmiddot

Wter lel after lechargbull 27 n bttlow top of caeing

laUH Nell dry agatn- alloecl well to recharge for

4S etnutbullbullmiddot

Tot a l volu- purged 11 gallonbullmiddot

SAMple collected at 1245 honlbull

lti~l=t (~ Jfill

I z OJgt ltz ~~ lgt O or

~ z~ ~n

~I ~a~

~

ill ini

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 8: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

l

(

0S ITE NAMpoundbull _

4 0 f belpw SAP pf SAliDAWll Depth

4 11 n belpn tee gt seeingltatie WL

WAter ColUIIFI

fl elf J)tSA POtMula for C l culat i ng Sta U c HaO Yol __ U ) CJ Y bull a CO lUI

QONiuct iY U y - M l O Ulllhoev bull oM a cubull o t63

- bull a v bull a ~ 216

Purged bullater collctci in 70 gallon dru HNu reacUnabull Not in the drUM bull Mater was pou1ed into the drU bullbullcclbulld

eo PPfllbull Water wabull vry di~lo-cl a dark red tint with the cotbullteney of vegetable oil

8ailci well dry approMiMamptely 1 yenoluMe ce gallons)

Allow Nell to recharge for 20 etnutbullbullmiddot

Wter lel after lechargbull 27 n bttlow top of caeing

laUH Nell dry agatn- alloecl well to recharge for

4S etnutbullbullmiddot

Tot a l volu- purged 11 gallonbullmiddot

SAMple collected at 1245 honlbull

lti~l=t (~ Jfill

I z OJgt ltz ~~ lgt O or

~ z~ ~n

~I ~a~

~

ill ini

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 9: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

middot

r

( bull TE NAME s Nybullnzbull cneeual =_

sectAMonUoling WU Nu111ber

Wll Ditel

11 n helew tqg pf seaampngWll Opth

static wLbull I n twtqw tee e sbullbullnbull

Colurt bull Jl cu

_ _CJPIIIM__ at 3 itch attovbull top of c-aet

r t tot Caleulatil field pete

ftattc HIO Vol__ cu

V bull ta IOIUI

v bull a11 cubull o1n conciiampCtivUy - R3 _

v 10 pH - amp4

Total vo1~ purgH 4 gall~middotNotbullbullbull Good -cherabull

SaMpl collctci et 1100 hourbullbull

Metalbull bullbullbullple wee tibullld tl Uered

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 10: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

l

bull IJir=t SITE NAME1 (~r

Monitoring Well NuMber ___ii_

_amp1n_ ~ 2 bull RacUue -1JJl_Cr)

11 tt belqw toe or seeingWell Opth

4 7 ft bslptt tgg gf s eeingltaUc wL uLlttl

ebull at 3 ln aDovbull top of caalngI 9

field Qetatrorwula for Calculating ftaUc HaO Vol- CU

t perature - ss-e cV bull a CO tUraquo

conductivity - 0 vbullaa~ cubulloau pH -6 1111v bull atA 1a11one

Well wes bail~ dry after l voluMeNotbullbullbull

laUed u dry again

Total volue purge-d 4 2 gallona

Weter vbullry turbid

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 11: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) middotmiddotmiddot-middot

( ( fpound NAMpound1 Nyenze Chbullbulllcel

Well Dlter

Well Depth J 9 ft belpw top gf seeing

8teUe WL amp ~ ft belptt tgp of sewing

fleld htePort~ule for Clcvleting

eUc HaO Vol- UJ

middot-perobulltu - 15 c bull (OlU

tOftduet 1y l ty - 940 v bull bullmiddotbull cua otu pH- bullbull ~

y bullbullbull bullbull

3Y bull tas

Since HNu reedingbull could not be ~o~eed to detert~~iIW the level of resplretory protection the hight deg bullpeel fled in the safety plan was used

Purged 11 S gallons froM well end placed into e 30 gallon drUM supplied by Nyecol

fltetels bullbullbullPlbull bullbullbull not field filtered

Water very discolored Dark red tint with the constsency of vegetable oil

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 12: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

c

( S llE NAIIE I Nyaroze CnettllCfl6

lfil flq 10t Jlur

ltatic wLbull 4 I ft JIJAt

ColUIIft 11 middot~ Jw1(11 Sllltk~-5

kckground A

Reading _JJPIIIIL- at 3 irch- atovbull top of caeing

~OIttUll foro CalculaUng hatte He0 VOlshy U)

field Qetl

Y bull a COlU

Y bull u 1 cua o tu conductlvUy - 1104 lllhOS

pH - 62

~ bull 5 7 gallons

11 on belQM top qf seeing

)

Well bailct dry - purged 3 gallons

Total -ount purgH lt 4 gallons

Water level 8 f-t tlow top of cas i ng - u saMpled at 1420 hourbull

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 13: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

l

-

r

ATTACDPr II

Drillillll Lo9bull AD4 llonitoring well conotruction

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 14: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) I =~W

___ -middotmiddotmiddot I

I

iIi J i ~ ~~ shy1 ~middotmiddot)ll

1 II

1iu-

1-shy1=shy1shy

~~ ~ D

I I I I

~ ~

j I

i1--

1shy

I

1shy _Wii

~r c -~==middot==-middota==

i I I

I J I

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 15: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) c Itil

(1

r--middot rt~l Ilftbullf

~---middot- u

I-shy

Ii I i I I

I

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 16: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

l

c

-middot __ ~shy-middot

m ____ ~imr--=-rmiddot- j ~----middot-middot I

bullI -ur-=-

1-- 1-- - ~--shy

I

Itil rr~ ( ~~middotmiddot I

X

i

c

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 17: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) middot

I I

I l

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 18: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) middotmiddotmiddot

y c

( TrST IOftiHONbull MWmiddotII hIIILampbullt JaaaL - ~~ = -zu -~hmiddotbullbull middot obullcJIIIUII- 1-bullu obull bullbull bullbull rem ~ _

=--~-shyr=-~---shy

=-~-----middot--shy=-

0 -=~~ I ~IIIIILIIIt -middot ~ plusmn- ~ -Mir I - = ~

y i

I

middotI I

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 19: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

(

ATTACDDT III

Alldytical oulta

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 20: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

(

l ANALYSIS OP WATER SAMPLES FRQM M)EQE - 0501 SITE ASHlNil NASSAQIUSE1TS

illz ~-ltltI ~~ lgtO

~iliERT No 0201-350 MJlt Mus Pit 0236Sl76middot050101 ZM

MO

~ItAuaust 15 INS ~l MCII

~1

~

0 ~

Propond for

l J DIWCA lfiiiWI INGl-ING U Pine StreH Peabody No 01 t60

Prepared by

ANALYTICAL CHEMISTRY LAIORATORY Environ-ental Research TeeMoloiY Inc

6g6 Vir11n1a Road Concord Masnchu tts 01742

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 21: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

l IN11UJOUCTION

1h11 report represents tha results of analysis conducted on a

sarias of Watr receivS by the ERT Laboratory on Aupst bullbull 1915

1ha suplu wan to ba analyred for volatile oraanic copowwb

(includinc -tbfl ethyl kltone) bull utract~le oraanic coounds

(includina aniline) and uhcted tal parueurs

Sple Receipt and Chain of CUstodr

Routine iupeetion of the suplas revealed thbull to ba packqed

properly and received in aood conditi on eorb on of bullbullbull labels

whh IICCOIIIpUYina chain of cUstody ncordl verified tuple identification

IIDd Ulamplyab nquqted Upon receipt infomation tro the subaitted

saplu wu recorded iD the Maatar Los look ud ulipM DT lAboratory

CoDtrol Tbqa W~iqu~ auple labalt wen affbbulls to nqectiva

apla CODUiun subseqlltly utilhecl throufbout the laboratory

aallil procMurel for positive traceability

Analrticampl ProcecWna

11te watern ualyampN accordiaa to procedure~ u outlined

b tba tonowtac IPA nfftfttu

~ ~ 5

Volatile Oqlllic 624

~

Extractable 625

Oraanic

eopoa

Sleeti4 Metalt 200 7

Quality Control Procedures c Standard quality control procedures vera illplbullented for all

analyses Labo~atory bullethod blanks and laboratory identifiM control

I I

ifIJill ~~u~bull rrbull(Ifbullbull

f fl

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 22: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) auplu wen ualyamped concurrently with the subaitted saple1 1be

nsults of the quality control anamplyaea wen nvievtd by the laboratory

quality ~trol coordinator to insure COIpliampnce with tltabihhed

control tiattt

Reaulu of Aulrsis

Result auartaa are pnaanted in tha attached tables Methyl

Ethyl amptoae (JreJ) vas not datactad b any of tha aubaitted suplea

Allilina wu qualitativly identified in (6) of the (7) subaitted

auples Seaiquantitative concantratioftl of anllina an presentee

ill parutheJtl

0

IJi rr (middot~middot

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 23: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

bullbull

) ~

n (

( ~

middot----

20560

10

IDL IDL

L

-- ~ - -

I

illz lt-lt OJgt2tS63 ltZ lgtN rJgt

11 lgtOor OIl HJ ZH HOIDL

IDL ~It 0

IDL ~~ Hill ~f ill r 0~ ~

IDL

18 Dr

-( (

SIHNY OF AJWY1ICAL RESULTS

lASENEUTRAL ElnACTAILE (1)

Client DEQE NASSFIT middot

Suplin1 Location Ashland MA

Suplina Date 17IS

ERTHo Deletion 2854S 28541 DSS1 2t557 28S54

Client Icleatiftcation Lioit SA sc 61 6A

ParaMter IIitJ=CIlroroethyl) ether 10 ul1 67 IDL IDL IDL IDL13-Dichlonbeubullbull IDL IDL IDLIDL IDL1 ltt-Dichlorobeubullbull 1to 3170 48 331 2-Dicblorobeubullbull 530 11400 130 240 40lb(2-Qlorobopzopyl) ether

I IDL

I LT l-Mo shyN-NttfOHdi-M-propyl aaine NitnNu- 38700boploo IDL IDLlllpltthalbullbull 31 middot 124-Trichlorobaane 2foHuadamplorobutu- IDL -Jiloroqcl-tobullli-lb(ZmiddotCUo~) shy2-CialCIIalshy_ 2_6-Dlaitntolueu

24-Dillitrotolu Pluorue j4-Qlorophenylphenyl ether Oiethyl phthalate N-nttrobullocllphenyl aaine

l IS

4-lroophenylphenyl ether Hxachlorobenune otthyl phtbalau

170 L fL IDL

11 13 IDL BDL

L

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 24: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

ltilt (bull

iliz illlt~gtN rgt

gt0 ~iii MJt

c SLMUJlY OF ANALYTICAL RESULTS

( lASENEUTRAL EXTRACTABLI (2)

Client DEQE MASSFIT Saapliq Location Ashland MA SUpUq Date 1715

DT No Deletion zgsbulls 2UU Clint ldMtification Uoit

Parauter JiipoundEiiiiiiaPbeaampDthreaa Di-a-butyl phthalatePluoruu tyl btuyl pbtbalatl leu (a)utbncbulleJCbrytene TS J-DicUombeluictiu 25 ua1 llo(2-othy1b01J1) pbtboioto Di-octyl phtbamplau loalo(b)l(k) fluoroatbo loalo(l) shy1_(123-cd)pyroao Dibluo(ah)udarac -o(pl)porylbullbull I lallloa HA

atlltt reported in ua1 (part per bill ion)

IOL bull hlov Detection Liait u reported

M bull Not Applicable flaquo) - Not Detected

SA sc

BDL

I16

T (170) (3t0)

29551 lA

8 L

(360)

(

2DS54 2i557 2DS60 29563 6A 61 10 II

I ~ IDL

(340) (ltO) ND

I L

ZM MO

~~ 0

IIi ~lii1 iliooi ~

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 25: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

S~Y OF ANAJYTICAJ RESIJLTS ACID EX11lACTAILE COOQJIGS

Client DEQI NASSPIT SUplina middotLocatioft Ashland MA SUpUnc Date 1785

ERT No DetectioD 28545 29548 29551 ns54 U557 29560 29565

Client Identification Llbullit SA SC lA 6A 61 10

11 1 11

11

Ph-1 2-Qlorophtool L L bull L bull L IL middotr Z-Hitloph-1 24middotDlbulltllflpheaol 24-Dichlorophaol 4-0lloro-3-Metbylphenol Z6-TIIclllonphono1 24-Dillltrophaol middot-Hitzoph-1 10 uc1 2-Mttbyl-46-Dinftrophenol SO ul1 ochl~1 10 uc1

lesults reported iD ua1 (part per bUUoa)

IDL bull lelow Dehetion Ualt u reported

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 26: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

bullbull

( SIMIARY OF ANALYTICAL cLTS

VOLATILE ORGANIC CQ4PQINDS

l Client DEQE Nasa Slina Location Aohland SUpline Date 1715

ERT No 2t547 Client Identification MW-SA

~

Mttbylene Qloride 92 1 1-Dichloroethylene BDL 1 1-Diehloroethane BDL Trau-12-Dichloroethylne 31 Qlorofon BDL 12-Dichloroethue 1 11-hidloroetbaae Cllorotbae

Viayl dlloride middot-Qaloroethue Carbon tetnchloride TridlorofluoroMthane lrodichloiGMtbue 12-Dicholoropropane Tnaa-1 S-Dicbloroproene TlicllloroetllJlae Dlb-loshy112-hiclloroetbau Cil-lS-Didalorapropene 2-QlorMtb)l vinyl ether lrofon Tetrachloroethylene Toluene QJorobbullnne ISO Ethyl benzene IDL 11 2 2-Tetrachloroethane IDL

ttflw-1--shy

Fit

2~550

middotSC

BDL IDL IDL 110 18

r460

BDL 620 BDL

l 20

1100 IDL BDL

29553 Nf- IA

100 IDL IDL 190 BDL

soo IDL

280 IDL IDL

2t556 - 6A

120 IDL IDL 100 BDL

50 IOL IOL 100 IDL

1130 BDL BDL

ResultJ nported in uampfl (part per billion)

IDL bull Below Detection Ualt 10 ua1

1te n~r ILl Mlz kXl Cllo~7lt 12+---lt zoo

i~~~~middotI

29562 2i565 -10 middotII

110 110 IDL 111 IDL BDL IDL BDL

_C IDL

l ~

I BDL

f (1 0 112 J-lt OJgtltZ JgtN rgt

IQ ~J z~ ~n

~~ 0

~~ ~ ~1

~ ~

29559 - 61

BDL IDL IDL 300

T 50

IOL

-l r980 IDL BDL

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 27: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) ~

)I

sect -middotyen

~ ~

~~

8-

lf

lllllfllll

~~

00

00

0

00

l 0

00

00

0

00

~ ~llli~JJ

5~

lil 1H

iliOili

N

~~

~ lil m

o

II I II

0 ~~~

0n

~~

~h

ii~iiiiiiii ~~

~

n ~~

o -gt

r

v ~

J ~L

I iia

oo

loo

o Ui

N

~

~ j

o

iw

iIi

I

j

~~~~N~lc

ii i

~~ ~

i l t1

i

li~ ~

s

ll e~

~

~ middot

j~~

liliii 0~ -middot

s I

j 1

H

3 t

~

~

l e

u bull

bull i

ic-plusmn ~

I

-~~ ie ~ II lilb

IIaU

10

lll-6

8ll

Hr

i )

-_

_)

)

I I ~ I

1 1till U~~~~

f

~~~~~ f fl I

z z N nr ~ n r ~ ~ 0 i

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 28: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

NoTICE ifi-f~~~-II lese Clear than this NYANZA CHEMICAL WAS TE DUHP notice itmiddot Is due to t he REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 29: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

NOTICE Wt~f~~-la ltaa Cltar than this NYANZA CHEMICAL WASTE DUMP notice Itmiddot II due to the REMOVAL ADMINISTRATIVE RECORD quality of the document being filmed NYA 004

middot~ __

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 30: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

NOnCE iit-r~~=-1bull le11 clear than thla NYANZA CHEMICAL WASTE DUMP notice It middot Ia due to the REMOVAL ADMINISTRATIVE RECORD quality of the document

NYA 004 being fllmod

middot--

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 31: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

r

ATTACIIMDIr IV

Health aD4 Safety Plan

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 32: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

) shy

-

SITE HAllE Nr anu Chemfcal Corp DATE August 6 1985 (

TASK IWIAGpoundR Jar Deluca Lynne Chappe11

SITE DESCRIPTION Tht Nyenza Chemical site 1s located on the 35 acre tract of land

whch 1s bordered by wetllnds The sftt 1s currently an fndustrtal part but wu

foiMrly a chltlical Mnufacturer During operttfon the f(yanza plant was reported

to hevt burfed solvents and tal sludges on portions of the property

SITE HEALTH I SAFm IHFDIU4ATOft

-QlL

2400 ppoo s SITpound PERSDHAL PRDTECTIOII REQUIREMENT

level of ProtOKtlon

c =+=

SITE CONTINGENCY PLAN

Acute Jnstnt

tUPlPL~llt~~ L D-1-s 907 WUCM diif vtwtt~ Jll tm as ww tJB reiDftOry 1couth ~

ContfRIfCY

llportant Phone Numbers

Response L 2001 7Ur -ur

c

Police Fire Dept Hotltll DeptPotson Center Sttto Spill Contractor HOEQE Aft)ulance

6171881- 1212 - 617 881-2323 - 617 881- 2353 - 617 223-2120

bull 617~585-5111 - Clun Htrbor - 617 292- 5831 Inc - 617 881-2323

~

llehrtn Engl noorlng rut Hlntgor ~ eLflJ 12 L HOEQE Site Hlntgor

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 33: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

r

AlACIIIISIIT V

hraonnel aD4 ampqu1s-ent Break4oWn

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826
Page 34: LETTER REGARDING TRANSMITTAL OF VAULT AREA …l_ 1'11011• Richard Batea . Richard . J. DeLuca . NYANZA Chemical Site . Groundwater Sampling . 8/14/BS . L. Chappell . R. Cleary

~

Peraonnel and Reaponaibilitietl

aJ DeLuca Taak Manager reaponaible for all data collection and aamplinq

JD Gram Samplinq crew reaponaibility for collectinq qroundwater aaraplea and Health and Safety officer

M r Richter Sampling crew reaponaible for collecting qroun4water tamplea

lgviwpt Ybullt4 PuriM Sampling

1111a lbotoioniaer

p8 Mter

CODductivity Meter

~ter

fefflon lampiloro I 4 l

Filter Apparatua

rour WhHl Drive Vehicle

Lfboratory tnalytif Reaueated

Volatile Organic Caapoundaincluclinq Methyl Ethyl Jtetone

aaaeNeutral Extractablebull includin9 Anilino

11 Drinking Water Metal

  1. barcode 579826
  2. barcodetext SDMS Doc ID 579826