MATIL MATERIALS TEST AND INOVATION ...matil.org/Uploads/pdf/cetam_web1-en.pdfDoç. Dr. Hüseyin SOYKAN General Manager MATIL MATERIALS TEST AND INOVATION LABORATORIES CO. Matil Material

Doç. Dr. Hüseyin SOYKAN

General Manager

MATIL MATERIALS TEST AND INOVATION LABORATORIES CO.

Matil Material Test and Inovation Laboratory Inc. has been established in order to perform activities in

vocational and technical education fields with R&D, inovation, accredited testanalysis, product compatibility

evaluation since end of 2012.

Established to today, MATİL Inc. which creates awareness with sectorial works to organize, perform

activities in order to increase in competitive power and continuing sustainability of steel sector.

Steel Test and Research Center which established by our company is to be national laboratory to represent

with independent and objective services ;also, to supply with international test services to sector and to

execute for global scale studies in scope of R&D and inovation studies not to depend on any corporation and

association. Matil Inc. aims at contributing to development for related sectors while technological solution

are represented for all metals in particular to steel by means of getting into a partnership with independent

product certification and compatibility evaluation corporations.

Best Regards

MATIL MATERIALS TEST AND INOVATION LABORATORIES CO.

POLICY OF LABORATORY

MATİL Material Testing and Innovation Laboratories Inc. As a laboratory, our policy is to present the test

/ analysis services applied in metallic and nonmetallic materials in a timely, error-free and reliable man-

ner by demonstrating good professional and technical practices and fulfilling the requirements stipulated

by the test / analysis method.

Test / analysis services use national and / or international standard test / analysis methods and valida-

tion studies are made in case of changes in test / analysis methods.

For this purpose, a Quality Management System in accordance with TS EN ISO / IEC 17025 was es-

tablished in the laboratory and the documents stipulated by the standard were published and put into

practice. It is imperative that all laboratory staff learn these documents and conduct test / analysis work

in accordance with the policies, procedures and principles set forth in these documents.

The goal of our laboratory is to prevent customer complaints with the help of cooperation with cus-

tomers, to fulfill customer expectations, and therefore to do all necessary work to increase customer

satisfaction. Impartiality, independence, honesty, confidentiality, reliability and quality are the basic

principles of our laboratory.

MATİL Material Testing and Innovation Laboratories Inc. As senior management; We pledge that we

will implement and continuously improve the Quality Management System in accordance with TS EN

ISO / IEC 17025 standard, customer requirements, legal requirements and TURKAK guidelines with the

contribution of all personnel

Mechanical Test Laboratory 2500 kN Tensile Test Machine ......................................................................................................6

600 kN Tensile Test Machine ........................................................................................................7

Charpy Impact TEST Machine .......................................................................................................8

High Frequency Fatigue Test Machine ..........................................................................................9

Low Frequency Fatigue Test Machine ........................................................................................10

Rib Geometry Test Machine ........................................................................................................11

Bend - Rebend Test Machine ......................................................................................................12

CHEMICAL AND COALANALYS IS LABORATORY ...................................

Chemical Analys is Test Machine ...............................................................................................14

Moisture, ASH, Volatile Matter Analysis .....................................................................................15

Carbon-Sulphur-Hydrogen Analyser .............................................................................................16

Calorimeter Test Instrument .......................................................................................................17

Microstructure and Material Analysis laboratory Metallographical Specimen Preparation Devices ..........................................................................19

Optical Microscope .....................................................................................................................20

Stereo Microscope ......................................................................................................................21

Scanning Electron Microscope (SEM) ........................................................................................22

Brinell Hardness Test Machine ...................................................................................................23

Universal Hardness Machine ......................................................................................................24

MicroHardness Test Machine .....................................................................................................25

Jominy Test Machine ..................................................................................................................26

PILOT SCALE STEEL PRODUCTION AND SIMULATION LABORATORY Melting Furnace .........................................................................................................................28

Annealing Furnace ......................................................................................................................29

Rolling Simulators ......................................................................................................................30

Thermochemical Simulation Software ..........................................................................................31

MINERAL PROCESSING LABORATORY Mineral Processing Instruments ................................................................................................33

LABORATORY MACHINE LIST

MechanicalTest Laboratory

2500 kN Tensile Test Machine

Zwick 2500E

Deney StandartlarıISO 6892 – 1EN ISO 15630 - 1 -2 -3ASTM E8 / A370

ISO 15835 – 2ASME Section IXAWS D1.1/D1.1M

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ApplicationsFlat Products Round Materials / Rebars• •

Sample TypesProfileSteel BladesWireFlat productsWelded Materials

CoilRound BarsPipesBulon pipes

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Technical Properties2500 kN load capacity

Accurate Yield strength,tensile strength, elongationmeasurements

1 to 100 mm flat and6-100 mm arası roundsamples’ test

Class 0.5 sensitivity

Full otomatic contact typeekstansometer

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Ürün StandartlarıTS 708BS 4449BS 6744BS 4482BS 4483ASTM A615/615M - A

706/706MDIN 488NEN 6008 / BRL 0501NBN A 24 -301NF A35 - 80 -1

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* These tests will be performed by accreditation according to TS EN ISO/IEC 17025 standard.

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600 kN Tensile Test Machine

Zwick 600E

Test StandardsISO 6892 – 1EN ISO 15630 - 1 -2 -3ASTM E8 / A370

ISO 15835 – 2ASME Section IXAWS D1.1/D1.1M

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ApplicationsFlat ProductsRound Materials / RebarsWirePipe & Tubes

Bolts & NutsWelded Materials Tensile & Bending

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Sample TypesRebarProfileSteel BladesWireFlat productsWelded Materials

CoilRound BarsPipesBulon pipesBolts & Nuts

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Technical Properties600 kN Load Capacity

30 kN loadcell for 0,1 to 10 mm wire and sheet metal tests

M6 – M8 – M10- M12 – M14 - M16 bolts (upper diameters with long products only)

0 to 100 mm flat and8-65 mm arası roundsamples’ test

3 Point Bend Test 50/60/74/96/108/120/132/150/160/168/192/200/224 mm radius

600 kN commpression capacity

Class 0.5 sensitivity

Full otomatic contact type ekstansometer

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Product StandardsTS 708BS 4449BS 6744BS 4482ASTM A615/615M - A 706/706M

BS 4483DIN 488NEN 6008 / BRL 0501NBN A 24 -301NF A35 - 80 -1

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Charpy Impact TEST Machine

Zwick/Roell RKP 450

Test StandardsTS-EN ISO 148-1 ASTM E 23••

ApplicationsStructure SteelsHardening Steels

Oil Pipe LinesSpecial projects

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Sample TypesV-notch sample U-notch sample• •

Technical Properties450 joule capacity

-80 to +70 °C sample conditioning

V & U notch tests

Optical Measurement sytem check for samples

2 & 8 mm hit anvil

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High Frequency Fatigue Test Machine

Zwick Vibrophore 500

Test StandardsEN ISO 15630-1DIN 50100EN ISO 15835BS 4449/TS 708

BRL 0501EN 10080DIN 488-2BS 6744

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ApplicationsRebarBolts

Round bar (prepared samples)

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Sample TypesRebar Bolts• •

Technical PropertiesM5, M6, M8, M10, M12, M14, M16, M20, M24 & M30 bolt’s fatigue

500 kN loadcell capacity

Ø8 -40 rebar fatigue

Class 0,5 sensitivity

Resonation type 35 to 300 Hz frequency working bandwith

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Low Frequency Fatigue Test Machine

Zwick Z1200H

Test StandardsPN-H-93220UNE 36065SI 739

EN ISO 15835SI 4446

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ApplicationsDeformation Controlled Rebar fatigue tests

Special designed test on flat products.

• •

Numune Tipleri

Technical Properties 1200 kN Load Cell capacity Static, 850 kN Load Cell capacity Dynamic tests

±9 mm, total18 mm stroke

1-3 Hz frequency with up to 10 cycles of one block

Ø5,5-60 mm rebar gripping

1- 75 mm flat product gripping

Full otomatic contact type ekstansometer

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•Up to Ø60 mm rebar

Round Bar

Hot & Cold Rolled flat products

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Sample Types

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*Hot & Cold Deformed Rebar•

Sample Types

Rib Geometry Test Machine

ECM RM 303

Test StandardsEN ISO 15630 - 1 •

ApplicationsRebar•

Product StandardsTS 708BS 4449DIN 488NEN 6008 / BRL 0501

NBN A 24 -301NF A35 - 80 -1ASTM A615/615M - A 706/706M

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Technical PropertiesØ8-50 mm rebar measurements.

Longitudinal rib width and height measurement

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Bend - Rebend Test Machine

RebarFlat productsRound Bars

PipesBulon Pipes

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Sample Types

Göçmaksan BD-60

ApplicationsRebarRound MaterialsPipes

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Test StandardsEN ISO 15630 - 1 -2 -3ASTM A370

EN ISO 7438••

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Product StandardsTS 708BS 4449BS 6744BS 4482BS 4483DIN 488-2

ASTM A615/615M - A 706/706MNEN 6008 / BRL 0501NBN A 24 -301NF A35 - 80 -1

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Technical PropertiesBend & Rebend tests for rebar up to 50 mm diameter.

Mandrel diameter up to 350 mm

Artificial aging furnace for rebend tests.

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CHEMICAL AND COAL ANALYSIS LABORATORY

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CHEMICAL ANALYSIS TEST MACHINE

ARL-iSPARK 8860 Optical EmissionSpectrometer

Technical PropertiesOptimal sensivity, stability, accuracy with ultra multiple phototube technology

Trace analysis of 33 element (Fe, Al, As, B, Bi, C, Ca, Ce, Co, Cr, Cu, La, Mg, Mn, Mo,Nb, Ni, P, Pb, S, Sb, Se, Si, Sn, Ta, Te, Ti, V, W, Zn, Zr, N, O)

Ppm level C, N and O concentration trace analysis

About a limit of 1,5 ppm in B for low alloy steels term analysis run

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Test StandardsASTM E 1806 ISO 14284 ASTM E 415

ASTM E 1086 ASTM E2209ASTM E1999

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Applications in Test MachineLow alloy and plain carbon steelStainless steelResulfurized SteelChromium Steel

Chromium and NickelHigh Manganase SteelTool SteelCast Iron

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Test Sample PropertiesAnalysis Service about 8 mm diameter and 0,8 mm thickness

Analysis service pin sample• •


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MOISTURE, ASH, VOLATILE MATTER ANALYSIS

ELTRA-Thermostep Makro TGA

Test StandardsASTM D7582 ASTM D7348•

Technical PropertiesUp to 5 g sample analysis with 0,1 mg resolution and with ultimate technology

High performance and long-term stability with encapsulated cell

Fast heating rates total power of 5400 W

Operation up to 1000 ºC from room temperature in steps of 1 ºC

Measurement up to 19 samples in one analysis cycle

Automatic placing with separate carousel for crucible lid

Monitoring integrated balance, heating and weighing with programmable furnace

Measurement moisture, ash, volatile matter in one analysis cycle

Fast result with short analysis time and simple operation principle

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ApplicationsMeasurement of moisture, ash, volatile matter in coal and coke

LOI in solid fuel residual/Katı yakıt atıklarda kızdırma kaybı

Analysis of residual moisture and LOI in cement

Analysis of ash and moisture content in paper

Analysis of loss in massDetermination of ash and moisture in flour

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*Test Sample Properties

250 μm of particul size of cokecoalsecondary fuels,

gypsum,flour,plastics and ceramics

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CARBON-SULPHUR-HYDROGEN ANALYSER

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ELTRA-CHS 580

Principal ApplicationsC-H-S determination in coke and coalS determination in oil and petroleumC-S determination in orga-nic waste and sludgeC-S determination in solid fuel waste

C-H-S determination in asphalt, rubber and plastics C-H-S determination in carbon black and graphiteC-H-S determination in calcium carbonate, cement, limestone, gypsum and wood

•

ApplicationsCoke and coalOil, asphalt and rubberCarbon and sulphur in ashGraphiteCalcium carbonate

LimeCementGypsiumPlasticWood

• •

Test StandardsASTM D 5373 ASTM D 4239 ASTM D 5016 ASTM D 1619 ASTM D 5291

ASTM D 1552 EN ISO 10694 EN ISO 15178 TS 12089 EN 13137

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Technical PropertiesFast, sensitive, precise and reliable element determinationAnalysis in low portion (100-500 mg)Operation up to 1550 ºC temperatureAnalysis in solid and liquid materials

Carbon, sulphur and hydrogen determination in organic samples 5-100% carbon determination 0,005-2% sulphur determination 0,01-15% hydrogen determination

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Calorimeter Test Instrument

IKA-C1 Calorimeter

ApplicationsCalorific analysis in all coke and coal typesCalorific analysis of jet fuel such as keroseneCalorific analaysis in liquid fuel such as diesel, oil, biodieselCalorific analysis of biological fuels

Calorific analysis in cereal and cropCalorific analysis in cement, food, solid residual and residual derived

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Numune TipleriToz boyutundaki kok, kömür, ikincil yakıt, cips, plastik ve seramik gibi katı malzemelerin analizi

Kerosen, jet yakıtları gibi sıvı hidrokarbonların analizi

• •

Test StandardsISO 1928 DIN 51900

ASTM D 240 •••

Technical PpopertiesAnalysis according to static jackets method

Analysis up to 40.000 joule heat capacity

Analysis result up to 20 minutes

22 ºC and 30 ºC operation run

Analysis up to 40 bar

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Microstructure and Material Analysis laboratory

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Metallographical Specimen Preparation Devices

Metkon SERVOCUT 301-AA Automatic Abrasive Cutting Machine

Metkon ECOPRESS 50 Mounting Machine

Metkon FORCIPOL 2V Grinding and Polishing Machine

Test StandardsASTM E3 •

Applications in Test MachineMetallographical examina-tion preparation for steels and other metallic materials

Precision cutting of the materials

Preparation materials for Scanning Electron Micros-cope with the conducted mounting

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Technical PropertiesAutomatic driven table-fe-ed cutting systems; variable cutting force, pulse cutting mode accurate and mo-torized positioning of the specimen in X and Y axis

Z-axis Chop cutting: The specimen is clamped and the cut-off wheel approac-hes the specimen

The advantage of combining different cutting techniques and methods into the samemachine to obtain superior cut surfaces for a broad range of heavy duty cutting applications on metals, plastics, and ceramics

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Technical PropertiesAutomatic digital mounting press with hydraulic pressu-re at 30 mm specimens

Adjustable: Pressure, Mol-ding Temperature, Heating and Cooling Time

Suitable for all current hot mounting materials used in metallography

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Technical PropertiesMetallographical Grinding and Polishing Machine, 250 mm Double Wheel system

Adjustable in grinding speed, time and water cooling

Automatic Specimen Mover microprocessor controlled, pneumatically adjustable individualforce loading system, upto 6 specimens

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Optical Microscope

Carl Zeiss – Axio Imager M2M Metalurji Mikroskobu

Test StandardsASTM E381 ASTM E112ASTM E45ISO 4967EN 10247

DIN 50602ISO 643DIN 50601ASTM 1382

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Applications in Test Machine

Metallographical Examinations for failure analysis

Determining Average Grain SizePhase analysis

Determining the Inclusion Content of Steel•

Technical PropertiesMotorised turret and Z axis focus

Contrasting Modules: Brightfield, Darkfield, Polarization

Led lighting and 5 MP CCD Camera

Apochromath optical system: 5x, 10x, 20x, 50x, 100x

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Stereo Microscope

Carl Zeiss – Stemi 305 Stereo Microscope

Applications in Test MachineMacro Examinations for failure analysis•

Technical PropertiesLed-ring lighting

10X/23mm oculer

0.8x, 1x, 2x, 3x, 4x zoom

5Mp CMOS camera

200 Lp/mm - resolution 2.5 micron

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Scanning Electron Microscope (SEM)

Carl Zeiss – EVO MA 10Scanning Electron Microscop

Applications in Test Machine

Image analysis of the metallic materials and cha-racterization

With the help of the EDX detector; elemantal com-position analysis of the specimens

Phase, Microstructure, Inc-lusion and Failure analysis of the metallic materials

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Technical PropertiesTungsten filament sourced analysis

Imaging wit the Secondary and Back-Scatter detectors

Advanced chemical analysis with EDX detector

Working distance of 8,5 mm and 25 mm2 imaging area

Specimen analysis up to 100 height and 120 mm diameter

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Brinell Hardness Test Machine

Bulut Makina – BMS 3000 Brinell Hardness Test Machine

Test StandardsEN ISO 6506-1 ASTM E-10 • •

Applications in Test MachineHardness test on the iron based and non-iron based metallic materials

Hardness test of the cast-iron materials

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Technical PropertiesBetween 187,5-3000 kg.f loadcell controlled Brinell Hardness tests

Turret controlled objective and indenter system

Computer controlled test load and precise measu-rement of the indentation diameter

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Universal Hardness Machine

Bulut Makina- Unibul Universal Hardness Test

Test StandardsEN ISO 6506 EN ISO 6507 EN ISO 6508

ASTM E-92 ASTM E-18ASTM E-10

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Hardness test of the he-at-treated materials

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Technical PropertiesHardness test for: Rockwell, Brinell and Vickers methods

Between 3-187,5 kg.f load-cell controlled tests

Turret controlled 2,5X, 5X ve 10X objectives

Computer controlled test load and objective selection

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MicroHardness Test Machine

Zwick – ZHVuM Mirco -Hardness Test Machine


Hardness test of the heat treated and coated materials

• • Test StandardsEN ISO 6507-1ASTM E92

ASTM E384 ••

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Technical PropertiesBetween 10-2000 gr.f Vickers Micro Hardness tests

10x, 40x ve 100x objectives

100x100mm stage and X-Y 25x25mm digital micrometer control

Motorised turret system for the intender and the objec-tives

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Jominy Test Machine

Bulut Makina – Jominy Test Machine

Applications in Test MachineDetermining Hardenability of Steel with the jominy test

Point measured Rockwell Hardness graphic of the test specimens

• •Test Standards

ASTM A255 EN ISO 642• •

Technical PropertiesHeat treatment up to 1000 C

Closed loop cooling unit

Jominy hardness test aparatus for the steel materials

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PILOT SCALE STEEL PRODUCTION AND

SIMULATION LABORATORY

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Melting Furnace

5M-50kW All kinds of steels, alloy

steel, stainless steel, pig iron casting can be reached by means of 50 kg capacity Induction Furnace having 50 kW power supply. Apart

from ferrous, melting of ot-hers, like aluminium, copper, brass and bronze can also be studied ther fore further researches.

Technical PropertiesCapable of melting 50 kg liquid metal

Proper for alloy development studies

Availability of different shape casting

Favorable for search for steel parts

Billet 20 mm x 20 mm x 300 mm

Slab 20 mm x 100 mm 200 mm

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Annealing Furnace

Alser Teknik - Protherm HLF190

Principal ApplicationsAnnealing process before rollingHeat treatment to all metal materials

Heat treatment to glass and etc materials

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•Laboratory scale (12 lt)

small furnace is suitable for annealing of Billet and Slabmodels which are manu-factured in melting furnace in which up to 20 pieces can be heat treated. For larger

amounts and big pieces big furnace (187 lt) can be used. Water-quenching, oil-quen-ching as well as controlled cooling can be achieved for developing various heat tre-atment strategies.

Technical PropertiesHeat Treatment till 1300 ºC

Possibility of working with 1 ºC sensitivity

Programmable temperature and time control

50 cm x 50 cm x 75 cm: 187 lt volume

20 cm x 20 cm x 30 cm: 12 lt volume

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Rolling Simulators

Pilot Scale Long and Flat Product Rolling Systems

Principal Applications

Ferrous and nonferrous long and flat metals•

Sample TypesDiameter of 1-20 mm long metals

Thickness of 1-20 mm flat metals

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Technical PropertiesManufacture of both long and flat products can be simulated

Up to 22 mm hot Rolling

Possibility of cold Rolling till 1 mm

Working of metals other than steel for product and process developments

Monitoring load, reduction ratio and roller revolution rate

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By means of two individual machines designed by MATİL, research and development and

innovative studies can be utilized for progressing steel sector.

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THERMOCHEMICAL SIMULATION SOFTWARE

FactSAGE Thermochemical CalculationFactSage is a thermochemi-

cal database software basis Windows, performingthermodynamics calculates, represent as a table and graph, especially FactSage admit of surveying in detail to gase-slag-metal interaction (including in thermochemical and viscosity values) at high temperature process such as

blast furnace, arc furnace, and the other seconder metalurgy, having iron-steel and slag databases, capable including in sintering process ;in addition, all pirometalurgical process calculating, hydrometalurgical and pirometalurgical process calculatings due to recycle study.

Technical PropertiesProper to modelling chemi-cal reaction equations

Proper to modelling Slag viscosity

Proper to modelling Phase durability diagrams

Proper to modelling Eh-pH diagrams

Proper to modelling Comp-lex balance calculations Proper to modelling oxide, melting of salt and alloy phase diagrams

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MINERAL PROCESSING LABORATORY

MINERAL PROCESSING INSTRUMENTS

Test Center TC A017 Sieve Shaker

Test Center TC A004-01 Disc Mill

Technical PropertiesSieve analysis at 50 -100-212-250-300-400-500 micron size

Sieve Analyses

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Principal ApplicationsCrushing, grinding end sieving applications of coal and coke

Crushing, grinding end sieving applications of bagasse and biomass

Crushing, grinding end sieving applications of ore and aggregate

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Test Center TC A004 Jaw Crusher

Technical PropertiesCrushing of 0-100 mm size of materials with adjustable jaw structure 0,75 kW engine power

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Technical PropertiesGrindability of 0-1000 micron hard materials

Grinding at micron sizes

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Test Standarts ASTM D2013 TS 4744 ASTM D346 ISO 18283 ISO 589• • • • •* * *

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Number of TR10/15/GPD-CM/0001 Steel Test and Research Center (STAREC) Project has been supported by ISTKA.

This publication’s content which is prepared in scope of Istanbul Development Agency Controlled Support do not represent to Istanbul Development Agency and Republic of Turkey Ministry of Development ideas and/or only responsibility in content

belong to Steel Exporter’s Association.

İTÜ Ayazağa Maslak Kampüsü No:2 34469 Maslak-Sarıyer/İSTANBUL : 0212 286 33 80 - : 0212 286 33 60

: [email protected] - : matil.org

Steel Test and Research Center

Documents

MATIL MATERIALS TEST AND INOVATION ...matil.org/Uploads/pdf/cetam_web1-en.pdfDoç. Dr. Hüseyin SOYKAN General Manager MATIL MATERIALS TEST AND INOVATION LABORATORIES CO. Matil Material