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    SIN FIN(USA) Limited.

    MMB EL BOLEO PROJECT

    Quality Plan

    Santa Rosalia Plant

    Baja Mexico

    1October

    2012Project Quality plan R Haye

    2March

    2013Project Quality plan R Haye

    3

    REV. DATE DESCRIPTION PREPARED BYCHECKED

    BY

    APPROVED

    BY

    This quality Plan represents work done by Sin Fin (USA) Limited. The work is based upon the project scope and designinformation as described herein and as provided by the owner. None of the above named parties or individuals shall be

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    SIN FINMMB EL BOLEO PROJECT

    (USA) LTD.NO: MMB 038-11liable, in negligence or otherwise, for any reliance which may be placed by any other party upon any representations

    contained herein.

    SIN FIN (USA)

    Field QA/QC

    Page

    1.0 Quality Control Policy 5

    1.1 Scope 5

    1.2 Purpose 51.3 Laboratory Standards 6

    1.4 Test Methods 6

    1.5 Operating Procedures 6

    1.6 Field Activities 7

    1.7 Notification of In-Process Changes 7

    2.0 Quality Control Organization 7

    2.1 Organizational Definitions 8

    2.2 Organizational Responsibility 92.3 Inspector Functions 9

    2.4 Certified Individual, Functions 9

    2.5 Training of Quality Control Personnel 10

    2.6 Training and Qualification of Certified Individuals11

    3.0 Contract Review & Design 11

    3.1 Minimum Documentation 11

    3.2 Document Distribution 11

    3.3 Authorized Inspector 123.4 Procedures 13

    3.5 Purchasing 13

    3.6 Vender Evaluation 14

    3.7 Non-Compliant Items/Materials. 14

    2

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    4.0 Materials 14

    4.1 Receiving Inspection 14

    4.2 Resins 15

    4.3 Reinforcements 154.4 Curing Agents 16

    4.5 Common Additives 17

    5.0 In-Process Inspection 18

    5.1 Procedures 18

    5.2 Resin Mixing 18

    5.3 Material Dispersion 19

    5.4 Component Fabrication 19

    5.5 Assembly 205.6 Nonconformance 21

    6.0 Finished Equipment Inspection 24

    6.1 Procedures 24

    6.2 Pressure Test 25

    6.3 Qualification of Secondary Bonders 25

    6.4 Access For Authorized Inspector 25

    7.0 Records Retention & Control 267.1 Scope 26

    7.2 Application 27

    7.3 Records Retention 27

    7.4 Procedures for Records Handling 27

    7.5 Acetone Sensitivity Test 28

    7.6 Barcol Hardness Measurement 29

    8.0 Lamination Procedure 29

    8.1 Surface Prep 308.2 Structural Layer 30

    8.3 Interior Layer Corrosion Resistant Barrier 30

    8.4 Inspection of Lamination Material 31

    9.0 Attachments

    9.1 Inspection Checklist 32

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    9.2 Barcol/Acetone Sensitivity Test Record 33

    9.3 Cut-Out Thickness Check 34

    9.4 Mat Reinforcement Log Sheet 35

    9.5 Fabric (Woven Roving) Reinforcement Log Sheet 36

    9.6 Common Additives Log Sheet 37

    9.7 Peel Bond Test Procedure 38

    9.8 Peel Test Report Form 39

    9.9 Resin Evaluation & Test Procedure 40

    9.10 Daily Resin Gel Test 41

    9.11 Resin Dispersment Sheet 42

    9.12 Non Conformity Correction Report 43-459.13 Inspection Test Plan 46-49

    9.14 Quality Assurance & Control Org Chart 50

    1.0 Quality Control Policy

    1.1 Scope

    This manual applies to the installation only of the

    fiberglass components at the MMB Santa Rosalia Plant

    Baja SUR Mexico. The work scope is for the field fiber

    glassing of the CCD THICKENERS, FRP LINERS AND

    LAUNDERS and the manufacturing of components.

    Purpose

    The purposes of the Quality Control Program are to:

    1.1.1 Ensure adherence to the rules and requirements of

    the Customer through processing of purchase

    orders, drawings, specifications, Users Basic

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    Requirements Specification (UBRS), and other

    documents at the field locations.

    1.1.2 Establish an inspection system to monitor thevariability of workmanship, processes and

    materials, in order to produce a consistent product.

    1.1.3 Establish and monitor the quality requirements

    related to the materials and services of vendors of

    subcontractors, based on surveillance and

    performance analysis.

    1.1.4 Provide a system for the detection of defect trends,

    and institute corrective measures.

    1.2 Laboratory Standards

    1.2.1 It shall be the responsibility of the Quality Control

    Manager to ensure that all equipment used in

    testing is in good working condition.

    1.2.2 All testing equipment will be regularly calibrated, in

    accordance with recognized national standards.

    Where no national standards exist, the basis for

    calibration shall be noted.

    1.2.3 Items tested with defective testing equipment shall

    be considered non-conforming, and shall be retestedafter (re)calibration of the testing equipment.

    1.3 Test Methods

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    Specific written inspection procedures will be followed,

    for all inspection and test operations.

    1.4 Operating Procedures.

    1.4.1 Parts will be made in accordance with the

    conditions specified by the Engineering Manager, as

    communicated on the approved shop drawings,

    (UBRS), and the inspection requirements check list.

    1.4.2 Approved Drawings and the inspection requirements

    check list shall be available to the Quality Controlpersonnel.

    1.4.3 Procedures shall be prepared and issued, as

    specified in section 3 of this manual.

    1.5 Field Activities

    The field activities performed by SIN FIN (USA) LTD shall

    be performed in accordance with the requirements of thisquality control manual. The program responsibilities,

    controls, documentation, and authorities shall apply.

    1.6 Notification of In-Process Changes

    1.6.1 If a change is necessary after the fabrication of an

    item has begun, the Engineering Manager shall

    issue a written stop work notification to theConstruction/Project Manager and the Quality

    Control Manager. The Quality Control Manager shall

    remove the item drawing, and the Construction

    Manager shall stop work in the area specified by the

    Engineering Manager.

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    1.6.2 The Engineering Manager shall process the change,

    as specified in section 3 of this quality control

    manual.

    2.0 Quality Control Organization

    Responsibility and authority for the implementation of

    procedures outlined in this manual shall rest with the

    Construction Manager or Project Manager...

    The Quality Control Manager shall have the organizational

    freedom to identify quality control problems and torecommend solutions. He/She has the responsibility to

    report directly to the Construction Manager or Project

    Manager matters concerning quality control.

    If differences cannot be resolved between Department

    Managers and the Quality Control Manager, they shall be

    brought to the attention of the Construction Manager or

    Project Manager for resolution. In all cases this manual

    shall prevail.

    2.1 Organizational Definitions

    The organization of the quality control department is the

    responsibility of the Quality Control Manager. This

    section sets forth:

    2.1.1 Where Quality Control inspector is referred to, it is

    understood to mean the inspector employed by SIN

    FIN (USA) LTD.

    2.1.2 Where Authorized Inspector is referred to, it is

    understood to mean the Inspector mutually agreed

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    inspector to ensure conformance to specifications.

    Functions include:

    a) Review of applicable drawings.b) Inspection of incoming raw materials and

    components.

    c) Providing Q.C. at various stages of the

    fabrication process.

    d) Determining product release or rejection.

    2.4 Certified Individual, Functions

    2.4.1 The Certified Individual shall:

    a) Perform an annual audit to verify that SIN FIN

    (USA) LTD. Quality Control System is current

    and is an effective operation;

    b) Verify that the qualifications of the Inspector

    and inspectorare in accordance with the SIN

    FIN (USA) LTD Quality Control System;c) Verify that corrective actions taken to resolve

    nonconformities are in accordance with the

    SIN FIN (USA) LTD. Quality Control Program;

    d) Verify that the responsibilities and activities of

    the Inspectorare in accordance with the

    requirements of the Standard;

    e) Verify that products are manufactured by

    qualified secondary bonders, and

    f) Sign the Inspectors Certification on theFabricators Data report and/or the

    Fabricators Partial Data Report.

    2.5 Training of Quality Control Personnel

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    2.5.1 Quality Control personnel shall be provided with

    training in the handling of inspection equipment and

    tools used by them in the inspection process.

    2.5.2 Quality Control personnel shall be provided with

    training in the implementing of Quality Control

    procedures and the recording, and interpretation of

    inspection data.

    2.5.3 Quality Control Personnel training shall be

    documented in a file maintained by the Q.C.

    Manager.

    2.6 Training and Qualification of Certified Individuals

    2.6.1 Certified Individuals shall be qualified using the

    following criteria:

    a) A minimum of two years experience with QC

    systems in the equipment fabrication industry.This experience need not be direct

    employment as QC department personnel.

    b) Initial attendance at one internal or external

    QC system audit, performed by qualified CI

    3.0 Contract Review and design

    3.0.1 The Customer job order comes from the Customers

    Purchasing Department. The Quality Control

    Manager will then prepare a project file.

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    3.1 Minimum Documentation

    As per agreement of Authorized Inspector

    3.2 Document Distribution

    3.2.1 Job order documents to be distributed include

    (UBRS) drawings, specifications and technical

    procedures.

    3.2.2 Preliminary design drawings shall be used only forthe following purposes;

    a) Review of construction details and

    requirements.

    b) Preparation of tooling for bonding.

    c) Purchase of raw materials.

    d) Fabrication of components, on a risk basis,

    subject to the express written approval of the

    Authorized Inspector.

    3.2.3 Fabrication details not shown on design drawings

    and details of design drawings, used for purchasing

    of subcontracted components, are to be assigned a

    sketch number and be placed in the file folder.

    3.3 Authorized Inspector

    3.3.1 The Authorized Inspector shall be mutually

    acceptable to SIN FIN (USA) LTD. and the Customer

    (user). This shall be determined during contract

    negotiations. If the Authorized Inspector is not

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    established by contract, then SIN FIN (USA) LTD.

    shall propose a Qualified Authorized Inspector,

    and obtain the customers concurrence prior to the

    start of fabrication.

    3.3.2 Any hold points will be chosen by the Authorized

    Inspector prier to work commencing.

    3.3.3 The Quality Control Manager shall keep the

    Authorized Inspector informed of the work progress

    and schedule, for hold point inspections.

    3.4 Procedures

    3.4.1 Technical procedures that effect the job

    requirements shall be prepared by the Engineering

    Department, and distributed to appropriate

    personnel.

    3.5 Purchasing

    3.5.1 Purchase orders are prepared by the Purchasing

    Department in accordance with a Bill of Materials.

    3.5.2 Stock materials, such as resin and reinforcement

    materials are detailed on equipment drawings.

    These materials are purchased by the Purchasing

    department.

    3.5.3 If the item to be purchased is a fabricated FRP part,

    it shall be furnished with a Partial Data Report and

    supporting documents, signed by the sub

    contractors Quality Control Manager.

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    3.5.4 Purchase order copies supplied to the receiving and

    Quality Control departments do not show pricing

    information.

    3.5.5 The Quality Control department retains all copies of

    purchase orders. These are NOT supplied to the

    user with the Fabricators Data Report.

    3.6 Vendor Evaluation

    The Quality Control Manager shall evaluate the Material

    Manufacturer by review of material inspections atreceiving. The Quality Control Manager maintains the

    records of these evaluations. Since only acceptable

    materials are used, the material Manufacturer is

    evaluated on each shipment. An annual report of these

    evaluations is prepared by the Quality Control Manager

    and distributed to appropriate management.

    3.7 Non-Compliant Items/Materials.

    All items/materials received, that are not in compliance

    with the purchasing and contract documents, shall not be

    accepted during the receiving inspection process, and

    shall not be used in the fabrication process. These

    items/materials shall be returned to the Vendor.

    4.0 Materials

    4.1 Receiving Inspection

    All resins, reinforcements, curing agents, purchased and

    sub vended items, and common additives shall be

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    received and checked under the control of the Quality

    Control Manager. The checks shall include:

    4.1.1 Check to assure they are the products ordered, bycomparing the items with the purchase order.

    4.1.2 Check for proper labeling:

    4.1.3 Manufacturers product name.

    A) Manufacturers Specific Product

    Identification (MSPI)

    4.1.4 Verify the receipt of a Manufacturers Certificate ofAnalysis or Certificate of Compliance as applicable

    for each lot received, when certificates are

    required. Verify that the lot number on the

    certificate matches that on the item(s).

    4.1.5 Check the packaging for visible damage.

    4.1.6 For acceptable items, sign and date the appropriate

    receiving documents, and forward to purchasing.

    4.1.7 Unacceptable items shall be handled as non-

    conforming.

    4.2 Resins

    The Quality Control Manager prior to use in the

    fabrication process shall review the results of the

    following inspection and confirm the Material Testreports specify the proper material.

    4.2.1 Check for normal color and clarity for the specific

    resin type, and that it is free of solids or gelled

    particles and contaminants of any type.

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    4.2.2 A sample from each resin lot shall be used for

    checking specific gravity, viscosity, and room

    temperature gel time; that they are within the resin

    manufactures specified range of limits. The resultsof these resin analysis shall be compared with the

    Resin Manufacturers Certificate of Analysis, and

    documented.

    4.2.3 Log the lot number and the date received for each

    lot, gel time, viscosity and specific gravity.

    4.2.4 The storage environment of the resin must be incompliance with the resin manufacturers

    recommendations.

    4.3 Reinforcements

    The results of the following shall be recorded by the

    Quality Control Manager on the reinforcement log sheets,

    prior to use in the fabrication process.

    4.3.1 All reinforcements shall be visually inspected under

    suitable overhead lighting, as they are dispersed for

    imperfections such as holes, cuts, thin spots,

    separation, and for contaminants such as

    inclusions, dirt, oil and grease. Dimensions,

    weights, and identifying numbers shall be recorded

    on Material Reinforcement Log Sheet.

    4.3.2 The storage environment of the reinforcement must

    be in compliance with the reinforcement

    manufacturers recommendations and all material

    supplied will be with certified material test report.

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    4.4 Curing Agents

    The results of the following shall be recorded by the

    Quality Control Manager on the Common

    Additives/Curing Agents log sheet, prior to use in

    the fabrication process.

    4.4.1 Check for stratification of material into two or more

    phases. In the case of liquids, they shall be free ofsediment or suspended solids.

    4.4.2 The curing activity of curing agents shall be tested

    generaly in accordance with ASME RTP-1, Appendix

    M-3, and Article E.

    4.4.3 The storage environment of the curing agent must

    be in compliance with the curing agent

    manufacturers recommendations.

    4.5 Common Additives

    The results of the following shall be recorded by the

    Quality Control Manager on the Common Additives/Curing

    Agents log sheet prior to use in the fabrication process.

    4.5.1 Record date received manufacturer, product name,

    quantity, and lot number. As additives are used,

    record the start use and end use dates.

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    4.5.2 The storage environment of common additives must

    be in compliance with the additive manufacturers

    recommendations.

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    5.0 In Process Inspection

    5.1 Procedures

    5.1.1 The Construction Manager is issued the Approved

    for Construction drawings from the Project

    Manager, and the Inspection requirements Checklist

    from the Quality Control Manager. These

    documents, together with the Construction/Project

    Managers file, authorize the fabrication process tobegin.

    5.1.2 All construction requirements shall be specified on

    the drawing, or on a document specified on the

    drawings.

    5.1.3 Preliminary activities that may proceed prior to the

    issue of Approved for Construction drawings are

    identified in 3.4.2.

    5.2 Resin Mixing

    The resin mixing and dispersion operator, on the Mixing

    Data sheet, shall record the following data.

    5.2.1 Resin promotion and primary preparation must bedone in the assigned resin mixing area.

    5.2.2 Formulas for each particular type of resin mixture

    are those recommended by the resin manufacturer

    or as predetermined by experience. The

    predetermined formulas shall be kept in a log book.

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    5.2.3 Resin mixing data shall be completed for each

    batch, and recorded on a mixing data sheet withreference to particular Job Number.

    5.3 Material Dispersion

    5.3.1 Resin shall be dispersed in containers clearly

    marked by the resin mixing and dispersion operator,

    identifying their contents. Resin type must beentered on the component data sheet for parts

    utilizing that resin.

    5.3.2 After materials have been fabricated, the identifying

    numbers of the materials used in their fabrication,

    shall be recorded.

    5.4 Component Fabrication

    The Quality Control Manager is responsible to have the

    following data recorded on the component data sheet

    prior to assembly.

    5.4.1 The types of materials used in fabrication shall be

    recorded, and verified as being correct.

    5.4.2 The lamination sequence of a particular component

    shall be recorded, and verified as being correct.

    5.4.3 Laminate sequences for standard flanges are not

    specifically recorded. Structural adequacy is

    determined by thickness checks.

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    5.5 Assembly

    The following inspections shall be done, and the data

    shall be recorded by the Quality Control Manager on the

    inspection checklist.

    5.5.1 All corrosion liners, and repairs to corrosion liners,

    shall be inspected on the molds by the Q.C.

    Department, prior to continuing the installationprocess. The installation department shall be

    immediately notified of the results of these

    inspections.

    5.5.2 Laminate sequence lay-ups shall be compared with

    the drawings, to ensure that all sequence layers are

    present and the proper materials are used.

    5.5.3 Inspect all equipment nozzles for the following,before installation:

    -Corrosion liner quality -Number and size of bolt holes

    -Flange and wall thickness -Bolt circle diameter

    -Spot facing of flange -Resin in bolt holes

    -Flange face drawback -Hub thickness

    -Nozzle identification -Hub shear length

    5.5.4 Inspect nozzle orientation and layout on allequipment before holes are cut for installation.

    5.5.5 Inspect corrosion liners completely for air,

    imperfections and inclusions, from the equipment

    interior immediately after the parts are removed

    from the mold.

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    5.5.6 Collect all nozzle cutouts and measure them for

    thickness. Confirm that the thicknesses are asspecified and record them on the quality control

    report. Retain cutouts for physical properties

    testing, as required, & review with the Authorized

    Inspector.

    5.5.7 Record laminate sequences for both interior and

    exterior body welds, when used.

    5.5.8 Record resin hardness (Barcol) readings.

    5.5.9 Inspect all equipment nozzles after initial

    installation (before the nozzle attachment welds are

    completed) for the following:

    a) Bolt holes straddle major centerlines.

    b) Orientation meets specification requirements.

    c) Elevation meets specification requirements.

    d) Projection meets specification requirements.e) Nozzles are square and level.

    5.6 Nonconformance

    5.6.1 When a nonconformance is detected, the item shall

    be tagged by the Quality Control Inspector and

    segregated, when practical. The Quality Control

    Inspector notifies the Quality Control Manager andthe Construction/Project Manager, and prepares the

    non-conformities correction report, and forwards

    the report to the Quality Control Manager. The

    detected nonconformance may be cause to reject

    items and/or initiate a vendor incident report. The

    Vendor Incident Report shall be used for receiving

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    inspection on material rejection prior too

    acceptance of the material.

    5.6.2 The Quality Control Manager may propose the

    following dispositions in lieu of forwarding the non-

    conformities correction report to the Engineering

    Manager.

    a) Return to vender

    b) Scrap.

    c) Repair visual defects (corrosion liner) or

    exterior cosmetic defects

    5.6.3 For all other dispositions, the report is forwarded to

    the Engineering Manager who provides the

    disposition. The registered Professional Engineer

    (RPE) shall approve all repairs affecting design and

    structure.

    5.6.4 Dispositions shall be one of the following:

    Use as is This is permitted when the item is in full

    compliance with the (UBRS) and the

    customer order.

    Repair The repair shall be fully described on the

    Nonconformity report. Only repairs,

    which are listed in RTP-1 M7 300, shallbe made. The Authorized Inspector shall

    approve the repair. The result of the

    repair shall make the part to be in

    accordance with the (UBRS) and the

    customer order. The Quality Control

    Inspector re inspects all repairs.

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    Return to vendor Applicable to purchased materials, which

    are found to be unacceptable for their

    intended use.

    Scrap Applicable when the nonconformity is not

    repairable or is found to be unacceptable

    for its intended use.

    Other Other information, not covered by the

    above listed categories.

    5.6.5 The disposition non conformity report is returned tothe Quality Control Inspector, who causes the

    action to be completed. When completed, the

    Quality Control Inspector signs and dates the Non

    conformity report, to record that the disposition has

    been satisfactorily completed. In the case of

    repair, the Authorized Inspector also signs and

    dates the completed disposition.

    5.6.6 The nonconformity report shall record as aminimum:

    a) Date of correction

    b) Specific location on the equipment

    c) Description of the nonconformance

    d) Method of correction

    e) Name of qualified laminator/secondary bonder

    who affected the repairf) Signatures of approvers

    5.6.7 The Engineering Manager shall reconcile any

    affected design documents, to reflect the current

    status.

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    6.0 Finished Equipment Inspection

    6.1 Procedures

    SIN FIN (USA) LTD. shall perform inspection of items

    being installed, as necessary to determine that the items

    are in compliance with the (UBRS) and the customer

    order. These inspections will be done by the Quality

    Control Inspector, and recorded on the inspection

    requirements checklist. When complete, the Quality

    Control Manager shall advise the Authorized Inspector

    that the item is complete, and ready for final inspection.The Quality Control Manager prepares the Data Report

    and the required supporting documentation. The Quality

    Control Manager certifies the data report Certificate of

    Compliance. All documents are then presented to the

    Authorized Inspector

    The Authorized Inspector performs the final inspection of

    the item(s) as required. SIN FIN (USA) LTD. shall make

    available its applicable inspection reports. TheAuthorized Inspector shall then record the results of

    his/her inspections on the SIN FIN (USA) LTD. reports.

    When the final inspection has been completed, the

    Authorized Inspector shall prepare a brief report

    summarizing his/her inspection activities and findings.

    He/she then submits a copy of this report to the SIN FIN

    (USA) LTD. Quality Control Manager as an attachment to

    the Certificate of Compliance. When satisfied that the

    item is fabricated within the requirements, the AuthorizedInspector signs and dates the Inspectors Certification,

    then returns it to the Quality Control Manager. Once

    these actions are completed, and all required testing, is

    complete, The Certified Individual then signs and dates

    the Contractors Certificate of Compliance, and the

    Inspectors Certification.

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    6.2 Pressure Test. (NOT APPLICABLE TO CONTRACT)

    6.3 Qualification of Secondary Bonders

    Secondary Bonders shall be qualified as required by

    ASME RTP 1, Appendix M-5 400.This meets or exceeds

    the requirements of ASME B-31-3. The Quality Control

    Manager shall select the personnel to be qualified and

    supply the necessary training. The qualification samples

    shall be inspected and tested by the Quality ControlManager. Test results shall be reviewed, and approved

    by signature and date, if acceptable. The Quality Control

    Manager shall maintain the qualification records. The

    Secondary Bonders names are recorded on applicable

    reports. The reports shall be available to all parties

    involved in the procurement and inspection activities.

    Secondary Bonders shall be re-qualified at a three year

    frequency, 18 months if inactive, or when the Quality

    Control Manager or Certified Individual has cause toquestion their ability to produce quality items.

    6.4 Access For Authorized Inspector

    6.4.1 The Authorized Inspector shall be allowed access to

    areas of the field, where the item is being installed,

    at any time during the process.

    6.4.2 The Authorized Inspector shall have access at anytime to all documents relating to the design and

    quality control of the item being installed.

    6.4.3 Access for final inspection to the inside and outside

    of the item being installed shall be arranged for the

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    Authorized Inspector, at a mutually agreed upon

    time.

    6.4.4 A clean safe working environment shall be provided

    for the Authorized Inspector, with adequate lighting,

    scaffolding, and other equipment required for

    access to inspect the item being installed.

    6.4.5 Adequate safety equipment, such as ventilation

    fans, shall be made available for the Authorized

    Inspector.

    7.0 Records Retention and Controls

    7.1 Scope

    7.1.1 This procedure shall ensure that the records

    retained, are complete and reliable.

    7.1.2 Inspection and testing records shall as a minimum,

    indicate the nature and number of observations

    made. All inspection documentation shall be clearly

    identified, indicating the job order number, part

    number, part description, or in any manner that will

    link the inspection results to a specific part.

    7.1.3 Records shall be available for review, as one of the

    principal forms of objective evidence of the qualityassurance program at SIN FIN (USA) LTD. office.

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    7.2 Application

    All records shall reflect the product conformance. The

    records shall reflect acceptability of the product, andworkmanship, and what action was taken to correct any

    non-conformity.

    7.3 Records Retention

    All records shall be retained by the quality control

    department for a period of not less than five (5) years, or

    longer as necessary for compliance of contractualrequirements.

    7.4 Procedures for Records Handling

    7.4.1 Records shall be identified and filed according to

    job order number.

    7.4.2 Any items supplied by sub venders shall be recordedby part number, with cross reference to the job

    order number.

    7.4.3 Records shall form an analysis basis, and

    management action regarding the quality assurance

    program.

    7.5 AcetoneSensitivity Test

    Should be applied to any secondary laminate surface,

    within the following parameters:

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    7.5.1 Perform three (3) tests per joint.

    7.5.2 Acetone used for testing must be clean.

    7.5.3 Acetone Testing Procedure (Note test location--

    elevation and radial location (in degrees--see

    drawings for reference) on the Acetone Sensitivity

    Report Form).

    7.5.4 Apply 5 drops of acetone to a small area of the

    laminate surface.

    7.5.5 With a clean finger, rub the acetone into the surface

    until the liquid evaporates.

    7.5.6 Check the laminate surface for tackiness.

    7.5.7 If the laminate feels tacky, note a fail on the test

    report. If not, indicate passage by checking OK on

    the report.

    7.5.8 Sign the report.

    7.60 Barcol Hardness Measurement ASTM D 2583

    .

    Following is a summary of the test method. Refer to the

    indicated ASTM for specific instructions on performing

    this test.

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    7.61 Fill out background information on the Barcol

    Hardness Report, including date of test, description of

    sample, and the specified Barcol for the test.

    7.62 Note and record the areas from which the readings

    have been taken (shell interior, bottom interior,

    overlays, etc.) in the boxes labeled A through H.

    7.63 Check the calibration of the Barcol Impressor with an

    aluminum calibration disc before taking any readings.

    7.64 Take ten (12) readings from each area listed. Record

    each reading in lines 1-12 on the report.

    7.65 Discard the lowest and highest readings, and average

    the remaining 10 readings.

    7.66 Compare the averages for each location to the

    specified Barcol for the test.

    7.67 Make a note of whether or not they conform. Make any

    necessary comments and sign.

    8.0 Lamination Procedure

    Laminating Construction shall be in accordance with the

    tabulated lay-up sequence according to the drawing or

    specifications provided by the client.

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    8.1 Surface Prep

    8.1.1 Surface material must be pre-ground with a 35-50grit sandpaper or equivalent before applying any

    structural material

    8.1.2 All holes or crevasses shall be filled with resin

    paste and left to exotherm and cool before applying

    structural lamination

    8.2 Structural Layer

    8.2.1 Application of the structural layer shall not alter the

    corrosion resistant barrier

    8.2.2 The first ply of the structural layer of the laminate

    shall be 1 or more plies of non-continuous glass

    fibers totaling 450 Gram per m comprised of

    Chopped Strand Mat and or Woven Roving or as per

    owner specification.

    8.2.3 Continue layup sequence of plies stated as perdrawing or specification supplied by owner

    8.2.4 After each layup sequence is applied allow to

    exotherm and cool before next layup sequence

    8.3 Interior Layer Corrosion Resistant Barrier

    8.3.1 The inner surface layer exposed to the contentsshall be a resin rich layer reinforced with a surface

    veil providing a thickness of minimum 0.25 mm

    0.50 mm or as per drawing or owner specification.

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    8.3.2 After corrosion barrier has reached its peak

    exotherm and cooled a resin rich wax coating will

    be applied to seal or protect the corrosion barrier.

    8.4 Inspection of Lamination Material

    8.4.1 All fiber material must be pre inspected and signed

    off by quality control before use of product

    8.4.2 All resin must have gel test and approved by quality

    control before use.

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    Attachment 9.1

    Inspection Checklist

    -

    Inspected Item Layout By

    (initial/date)Checked By

    (initial/date)Verified By

    (initial/date)

    Proper fit

    Pre groundbefore lay-up

    Nozzle size &

    orientation

    Elevation

    Material

    Lay up sequence

    Barcol

    Wax coat

    Paperwork

    completed

    ProjectNumber:

    CUSTOMER:Customer

    Number:Location

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    Turnover

    Comments:

    Attachment 9.2

    Barcol/Acetone Sensitivity

    Test Record

    Component:

    1

    2

    3

    4

    5

    6

    78

    9

    10

    11

    12

    ProjectNumber:

    CUSTOMER:CustomerNumber:

    EquipmentNumber:

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    Average

    Note: A minimum of 12 Barcol readings for each component is required for RTP 1 see 6-910

    ACETONE SENSITIVITY RECORD

    COMPONENT

    NUMBER

    DATE

    RESULT

    INITALS

    1Attachment 9.3

    Cut-Out Thickness Check

    Mk Qty Id Service Location DrawingThickness

    ActualThickness

    ProjectNumber:

    CUSTOMER:CustomerNumber:

    EquipmentNumber:

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    1

    1Attachment 9.4

    Mat Reinforcement Log Sheet

    Mat Manufacturer:

    Mat Nomenclature:

    Mat Treatment (if given)[Note 1]:

    Mat Weight [Note 2]:

    Q.C. File No.:

    ProjectNumber:

    CUSTOMER:CustomerNumber:

    EquipmentNumber:

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    RollNo.

    Reinforcement

    ProductionDate

    Lot No.[Note

    1]

    Width Weightof

    Sampl

    e3

    PropertyInspection3

    VisualInspectio

    n

    (if given) (grams) By Date By Date

    (3) Inspection Protocol: If no defects have been recorded in the previous 80 rolls,Sample the 1st roll on each skid. If defects are recorded, inspect every roll until 80rolls without defects have been recorded.Complete visual inspection for every roll as used.

    Comments on visual and packaging inspection (indicate which roll):

    Notes :( 1) Lot, batch, product code, or other label identification. (2)

    Manufacturers label weight.

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    1Attachment 9.5

    1Fabric (Woven Roving) Reinforcement Log Sheet

    Fabric Manufacturer:

    Fabric Nomenclature:

    Fabric Weight:

    Fabric Construction:

    Roll No.Reinforcem

    entProduction

    Date

    (if given)

    Lot No.[Note(1)]

    Width

    Weight

    Gram

    s3

    Construction3

    PropertyInspection

    Cols 4,5, and63

    VisualInspection

    1 2 3 4 5 6 By Date By Date

    (3) Inspection Protocol: If no defects have been recorded in the previous 80 rolls,Sample the 1st roll on each skid. If defects are recorded, inspect every roll until 80rolls without defects have been recorded.Complete visual inspection for every roll as used.

    Comments on visual and packaging inspection (indicate which roll):

    ProjectNumber:

    CUSTOMER:CustomerNumber:

    EquipmentNumber:

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    Notes:(1) Lot, batch, product code, or other label identification.

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    1Attachment 9.6

    1

    Common Additives Log Sheet

    Manufacturer: Raw Materials Inspection Inspector Date

    As Received

    Product Name:

    Lot Number:

    Additive Purpose:

    Manufacturer: Raw Materials Inspection Inspector Date

    As Received

    Product Name:

    Lot Number:

    Additive Purpose: Catalyst

    Manufacturer: Raw Materials Inspection Inspector Date

    As Received

    Product Name: I

    Lot Number:

    Additive Purpose:

    Manufacturer: Raw Materials Inspection Inspector Date

    As Received

    ProjectNumber:

    MMB 038-11

    CUSTOMER: MMB El Boleo MiningCustomerNumber:

    EquipmentNumber:

    CCD 01

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    Lot Number:

    Additive Purpose:

    Attachment 9.7 Peel Bond Test Procedure

    .

    General Method for Performing Peel Test

    A Peel Bond Test is performed to test secondary bondingperformance. It should also be run prior to the start of work toverify proper application technique.

    1: First the area to be bonded is properly prepared by grindingwith a 16 or 24 grit disk. This removes any paraffinatedresin/concrete laitance or contaminants. Or in the case of themoulded surfaces, it roughens the surface and exposes glassfibers.

    2: A piece of Mylar is taped over 1/2 of the area to be tested.Next a laminate is prepared consisting of 3 layers of 450 GramChopped Strand Matt cut to 150mm x 300mm along with a properamount of resin and catalyst.

    3: The glass is wet out and applied over the test area being carefulto center the laminate over the prepared area and the Mylar area,i.e., 150mm x 150mm over the Mylar and 150mm x 150mm over theprepared area.

    4: After the laminate has properly cured, the laminate is removedby lifting along the no bond (Mylar) side and pulling the laminatefree from the test area.

    5: If the laminate pops free from the test area with little or no fiberstearing, it has failed the test. The prepared area needs to beinspected to see if it was ground properly to the right profile andto see if all contaminants have been removed.

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    6: If the laminate tears loose exposing numerous fibers along thissubstrate, the test show that a proper bond has been achieved.

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    1Attachment 9.8

    Peel Test Report

    Location Accepted Rejected Comments

    Inspectors Name ____________________ Date:_____________________________

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    Attachment 9.9

    Resin Evaluation & Test Procedure ASTM D2471

    Following is a summary of the test method. Refer to the

    indicated ASTM for specific instructions on performing

    this test.

    Gel Time:

    Gel time is defined as the timer interval between the

    mixing of a resin with catalyst and promoter, and the

    point where the mixture becomes unworkable due to

    gelation. Gel time tests follow this procedure:

    1. Make a note of all information on the resin to be

    tested, including type of resin, resin manufacturer, date

    of manufacture, batch and drum numbers, and date of

    test. If required, note type of promotion and type of

    catalyst, including percent used in the test. Also, if

    required, include temperature at time of test.

    2. Set gel time counter to zero.

    3. a. When using a Gel Timer, weigh and place 100g

    sample of resin in a paper cup, measure and add an

    appropriate amount of catalyst and mix for at least one

    minute.

    b. When using a Hot Pot Gel Timer, set the thermostat

    at the desired test temperature (usually 20 deg. C to 25

    deg. C). Weight and place a 100g resin sample in an

    aluminum gel cap. Measure and add an appropriate

    amount of catalyst and mix for at least one minute.

    4. Place the sample in the gel timer.

    5. Insert a wire utensil and stir.

    6. When the resin gels, note the time shown on the

    counter and record it on the Resin Evaluation & Test Log.

    7. Record comments, if any, and sign the log.

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    1Attachment 9.10

    Resin Dispersement Sheet

    Project Number MMB 038/11

    Customer MMB El Boleo Mining

    Equipment Number CCD 01

    1Manufacturer: Ashland Chemicals Q.C. contact:

    Resin: Derakane 411-350 VE Address:

    Spindle No.: Telephone No.:

    Emergency telephone

    No.:

    Date Lot No.

    Gel Time @25oc

    (min)

    Viscosity

    @25oc (cps)

    Specific Gravity

    @25oc VisualExamination

    Manufacturers

    Specification

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    1Attachment 9.11

    Daily Resin Gel Test

    Resin Type: Derakane 411/350 VE

    Catalyst Used: _Norox 922H (Red) __

    Additives Amount

    Mass

    % Comments

    D 411/350 1000 gram 100%

    Cobalt (6%) 20 ml 2%

    BYK A 515 1.5 ml 0.15%

    2.4p (Acetyl Acetone) 0.2 ml 0.02%

    MEKP ( Norox) To be added for Gel test.

    Gel Test

    TimeofTest

    % ofCatalyst

    CatalystMass

    ResinMass

    RelativeHumidity

    AmbientTemp

    GelTime

    InspectorsInitials

    1.25% 1.25ml.

    100 Gr.

    Project

    Number:MMB 038/11

    CUSTOMER: MMB El Boleo MiningCustomerNumber:EquipmentNumber:

    CCD 01

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    Inspectors Name ____________________ Date:_____________________________

    Attachment 9.12

    Nonconformity Correction Report (Page 1 of 2)

    Project Number:

    Customer:

    Customer PO Number:

    Equipment Number:

    Sequence No.: Initiation Date:

    Description of equipment

    Work area or responsible laminator(s) or secondary bonder(s):

    Description of nonconformity (i.e. size, type, location, etc.):

    Identified by: Date:

    Method of repair or corrective action (Use back of form if necessary. If other attachments,sketches, or drawings are required, they must be referenced here and attached),

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    Check off approvals required (see ASME RTP-1, Appendix M-7 for stamped equipment):

    Registered Professional Design Engineer Date

    : Fabricators Engineering Manager Date

    :

    Inspector Date:

    Fabricators Quality Control Manager Date

    :

    Other Date

    Project Number:

    Customer:

    Customer PO Number:Equipment Number:

    Nonconformity Correction Report (Page 2 of 2)

    CorrectiveWorkdoneby:

    Name Title Employee

    No.

    Supervisorssignature:

    Date completed:

    Required quality control inspections and approvals (check off approvals required):

    Inspector Date

    :

    Fabricators Quality Control Manager Date

    :

    Other Date

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    :

    Date

    :

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    Attachment 9.13Project Number:

    Customer:

    Customer PO Number:

    Equipment Number:

    Receiving Inspection / Material Verification x 1Verify all resin and additives received comply topurchase orders x Standard 1

    Verify all glass received complies to purchase orders x 1

    Unacceptable material is reported to purchasing x 1 Purchasing to mark non conforming material as: use as

    is, rework, or return to vendor x1

    Lamination Process Inspection x

    Resin inspection as per field order x 1

    Fiberglass inspection as per field order x 1

    Resin Additives inspection as per field order x 1Final cure Thickness Dimensions, Appearance, BarcolHardness x 1

    Component inspection (covers, flanged nozzles,

    bosses, gussets, ribs, stiffeners, etc. X 3Submit Report x

    Assembly Inspection x

    Production layouts for flanged nozzles, fittings,manholes, vents, filling ports prior to bonding sub-assemblies, Assembly fixtures, leveling devices, Drill

    jigs properly oriented, Locating pins and stops usedproperly.

    x 3

    Sanding (applies to all sanded parts /areas) x

    Smooth surface, Critical wall thicknesses aremaintained after sanding, Areas requiring secondarybonding are completely sanded, Air bubbles have beensanded through are repaired

    x 1

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    Drilling x

    Drill patterns to match drawings, Jigs to matchdrawings, Resin wipe all holes, Exposed fibers are

    sealed, Check size, Check location, Check number,Check orientation x

    1

    Trimming x

    Trimmed to correct dimensional lines, Check fordelamination where trimmed, Resin wipe trimmededges are wiped to seal exposed fiber

    x 1

    Hydrostatic Testing (if required) 2

    Check pressure to meet specification 2

    Check vacuum to meet specification 2

    Log time test begins 2

    Log time test ends 2

    Check Hourly: 2

    Liquid level 2

    Pressure Gauge 2

    Submit Report 2

    Manway Covers and Fittings x 3

    Top Center Manway Covers, Smooth inner surface, Noentrapped air or dry spots, Hole pattern, Edge distance x 1

    Sidewall Manway Covers, Smooth inner surface, Boltpattern, O.D. Trimming, Thickness, No entrapped air ordry spots

    x 1

    Molded Fittings x Tie down brackets smooth, no dry spots, internal voidsor delamination x 3

    Fittings not meeting the above criteria may besubmitted for rework. x 3

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    Purchased Parts x

    Reinforced Plastic Sub Assemblies x

    Threaded assemblies have clean threads

    x

    Nipples, elbows, flange faces have no cracks, airpockets or damage of any kind, Ends are cut squareand smooth

    x

    Sub-Assemblies x Dimensions and angles meet engineering drawings,specifications and tolerances x

    Mating joints are fully and firmly seated, Evidence offiller squeeze out around circumference of joint x

    Cut edges are sanded and resin coated x Excess filler is removed from outside and inside

    assembly x

    Resin fillers are smooth, even and fully cured, no tackyor soft spots x

    Acceptable sub-assemblies marked OK,Unacceptable sub-assemblies marked REJECTED,Unacceptable sub-assemblies removed for rework ordisposal

    x

    Tank Bottoms x

    Material requirements are verified to drawing x Inspect surface preparation prior to application x

    Exterior surface has no protrusions above 1/8 x Seams and overlays are blended to form a smooth anduniform transition area x

    No voids or delaminations between liner and structurallaminate larger than visual inspection criteria. x

    Pits are filled prior to bottom installation x

    Submit Report x

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    Attachment 9.14

    George White

    Project Manager

    Robert Haye

    QA/QC(Manager)

    TBDField QAManager

    TBDQC Inspector