Embed Size (px)
Citation preview
MODEL 7800
SPECTROPHOTOMETER
(LCD TYPE)
INSTRUCTION MANUAL
JAPAN SPECTROSCOPIC CO.~ LTD.
2967-5, ISHIKANA-CHO, HACHIOJI CITY
TOKYO, JAPAN
July 1987
I
Pll.oduc:L6 /.>oid &.y J-(J./.)co, un.f..v,/.> o~e /.>peci/-Led, wz.e WOA/I.an.:ted tOIl. a peAiocL ot one yeall. to &.e -/!tee ot de-J.ec:L6 .m ma.i.vUa.Lo and lUoll.k.maJv,lUp . It any de-J.ec:L6 /.>houfd OCCUlt .m the pll.oduc:L6 duJt.mg tIU/.> peAiod ot WOA/I.anty, }Mco will Il.epa.ill. Oil. Il.epi.ace the detect.ive pall.t/.> tll.ee ot chall.ge. Ilowevel/., tIU/.> WOA/I.anty cLoe/.> /lot COVel/. to.teOIu.mg c(J./.)e/.>!
1) Detec:L6 cau/.>ed &.y m.i/.>opel/.at.ion. 2) i?epa.ill. Oil. mocL.i-J..icat.ion clone &.y othell. than J-M co OIl.
authoJt.ized agent. 3) LUe ot -J..ill.Utg/.> Oil. othell. /.>pwz.e palti/.> /.>uppi..ied &.y
othel/. than }Mco. 4-) Accident &.eyond OUlt Jte/.>poM.i&..ility. 5) D.i/.>MieIl. 6) COll.ll.o/.>.iO/l due to U/.>e ot .impll.Opel/. /.>oi.vent Oil.
/.>ampi.e.
7h.i/.> WOA/I.anty doe/.> not COVel/. palti/.> ruled &.ei.ow.
1) 7 UIlg/.>ien .iocL.ine i.amp, deuteAium i.amp, light /'>OUltce m.iJtJto/W, etc.
2) tU/.>e
tOll. any .inc1u.iJty Oil. Jteque<>t tOll. JtePa.ill. /.)el/.v.ice, contact yoUlt lASCD agent a-J.t= con~g the model. and /.>eIl..iai. num&.eIl. ot yoUlt -iMiAument.
l.
1-1
Table of Contents
UNPACKING & INSTALLATION .. .. .. . .. .. . . . ................ ..
Unpacking .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .......... ..
1-1-1 Unpacking the main unit
1-1-2 Unpacking and checking accessories
1-2 Installation ..................................................................
1-2-1 Installation requirements
1-2-2 Installation and connecting connectors
1-2-3 Loading heat-sensitive chart paper
2.
3.
3-1
3-2
SPECIFICATIONS .. .. .. .. .. ........................ ............ .................. ..
GENERAL DESCRI PTION OF INSTRUMENT
Optical System
System
3- 3 Program Structure
4. COMPONENTS & FUNCTIONS
4-1
4-2
4-3
5.
External View
Operation Panel
Rear Panel
TURNING ON " POWER" & STOP OF OPERATION
5-1 Turning on " Power " Switch
5- 2 Stop of Operation
6. MEASUREMENT METHOD
6-1 "1. Fix WL Meas" Measurement of Transmittance
Page
1
1
1
2
2
2
4
6
9
11
11
12
13
16
16
17
20
21
21
26
27
and Absorbance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
- i -
Page
6- 2 " 2. Ti me Scan 1 " Measurement of Change with
Time at Fixed Wavelength .. ...... .. ... . . ...... 29
6- 3 " 3. Q~anti Analy " Quantitative Analysis . .. .. 32
6-4 " 4 . Spectrum" Absorption Spectrum Measurement 47
6- 5 "5. Time SCan 2" Measurement of Change with
Time at Fixed Wavelength
7. METHOD OF SETTING PARAMETERS
8. DATA FILE AND PARAMETER FILE
8- 1 Data Fi l e
8- 2 Parameter File
9. "METHOD 21 " SETTING OF SPECTROPHOTOMETER
10. " METHOD 22 " SELF- DIAGNOSIS
11. " METHOD 23 " BASELINE CORRECTION AND WAVELENGTH
CORRECTION
12. "METHOD 31 " SETTING INPUT/OUTPUT DEVICES
1 2-1 Setting Parameters for RS - 232C Interface
13. "METHOD 32" POSITIONAL ADJUSTMENT OF THERMAL
PLOTTE;R HEAD
APPENDIX 1 REPLACEMENT AND POSITIONAL ADJUSTMENT
OF LIGH SOURCE
APPENDIX 2 RECORDER OUTPUT
APPENDIX 3 LIST OF DRAWINGS OF 7800
- ii -
48
52
59
59
61
64
67
69
71
74
76
1. UNPACKING & INSTALLATION
1-1 Unpacking
1-1-1 Unpack ing the main unit
Take out the main unit from the carton and check
that the serial number inscribed on the nameplate
on the right side of the main unit and that on the
inspection record are in agreement . Also check
the line voltage.
~------------~ MODEL Ubest - 30 I MFG. 1000332 ----+1---DATE 1986. OCT LINE VTG AC. 100V 50/60HZ
Jasco. B *?J·:l'tI~~it~tl
Japan Spectroscopic Co.,LTD
Nameplate
Serial numb er
Line voltage and frequency
Fig. 1-1 Hain unit and nameplate.
- 1 -
1-1-2 Unpacking and checking accessories
Take out accessories from the carton and check them
against Table 1-1. If any part is found missing or
damaged, please contact your l ocal JASCO distributor.
Table 1 - 1 List of Components
Component Q' ty Remarks
1 pc Holumium glass
Fuse 1 pc 2- ampere slO1' bIOI, f use
AC input cord
Allen wrench
Dust cover
Instruction manual
1 pc
1 pc
l ' s hee t
1 copy
2.5 mm
NOTE: If the printer (option) is ordered , the
following will be supplied with the printer,
which will be incorporated in the main unit.
o Heat sensi tive chart paper
o Chart paper bobbin
1- 2 Installation
1-2-1 Installation requirements
1 roll
1 pc
In installing the unit, observe the following condi
tions. If the unit is installed in a place that
does not meet with these condit i ons , the performance
may not be guaranteed. Also note that such an
- 2 -
installation may cause failure of the instrument.
(1) Small line voltage variation
The line voltage variation is preferably within
+5 % of the line voltage. The instrument will
not operate normally if it is more than +10 %
of your line voltage.
(2) Use a 3-pin grounded outlet (or with a ground
ing terminal).
If a 2-pin outlet is used, use the supplied 3P-
(3) Small temperatu~~ variation
The temperature variation is preferably 15°C to
25°C. The operating temperature range is 10°C
to 35°C.
(4) Humidity must be within the range of 35% to 85%.
High humidity will accelerate the deterioration
of optical elements. It is therefore recommended
to install the instrument in a place where humid
ity is lower than 60%.
(5) The atmospheric pressure must be 750 to 1060
millibar.
(6) No intense magnetism or source of high frequency
The instrument may not operate normally in the
vicinity of intense lines of magnetic force
or a source of high frequency.
(7) Small mechanical vibration
- 3 -
(8) Avoid installation in a dusty place or a place
where harmful gas such as corrosive gas or the
like is present.
(9) Install the instrument in a place not exposed
to direct sunlight.
(10) Install the instrument in a place not directly
blown with air from an air conditioner.
1-2-2 Installation and connecting connectors
Install the instrument on a bench or table measuring
600 mm wide and 550 mm deep, which withstands a weight
of 15 kg.
Ideally, provide a space behind the instrument to
allow access for inspection and maintenance. Fig. 1-2
shows the dime nsions of the instrument.
- 4 -
mn~mn
~ ~ ~ ~
Q
= Q ~
Q
~ ~
= = = Q
0
'" ".
II I)
478 9 5
Fig. 1- 2 Dimensional drawing.
After making sure the " POWER" switch at the bottom
of the right - hand side panel of the main unit is ln
the "OFF " position, connect connectors. Connect
one end of the AC input cord to "AC lOOV INLET" on
the rear of the main unit and t h e other e nd to your
outlet. The instrument can be grounded by plugging
the cable to a 3-pin outlet with a grounding terminal .
If your outlet has no grounding terminal, ground the
grounding terminal on the rear of the main unit
- 5 -
3-pin connector wit h grounding terminal
Fig. 1-3
I WARNING I (1) Make sure that the grounding wire of
the 3-pin outlet is grounded.
(2) Do not use a water supply pipe for
grounding because it is often made of
non-metal materials. Correctly ground
the instrument using the grounding
t e rminal on your power distribution
board. If it is not grounded , you may
receive an electric shock in case
insulation failure.
1-2-3 Loading heat-sensitive chart paper
CAUTIONS: (1) The heat-sensitive chart paper has
its face and back. Be sure to load
it so that print is made on the face.
(2) Be sure to load the chart paper before
using the printer . Operati o n without
loading chart paper may damage the
thermal head.
- 6 -
<Cautions in handling heat sensitive chart paper >
The heat sensitive chart paper will develop color
by heat. Color development is noticeable from
about 75°C . Use the following care in handling
the chart paper.
(1) Do not store it in a place where temperature
and/or humidity is high. Store it in a dark
place where temperature is lower than 30°C and
humidity lower than 60%.
(2) Use care not to wet the chart paper. If the
recording area is wetted with water, do not rub
the surface with force , but liqhtly press it
with tissue paper or the like and allow it to
dry.
(3) Do not rub chart paper with a hard ob j ect. If
rubbed , it may develop color by friction heat.
(4) Exposure to intense light for an extended time
after color has developed may fade it. Keep it
in a file, as and if necessary.
(5) For pasting, do not use a solvent-based paste.
Use of organic solvent may develop color.
Appropriate adhesives include starch-based paste ,
gum arabic , and poval-based or CMC - based
adhesive.
(6) Plasticizer may fade the recording area. Do not
- 7 -
stick cellophane tape directly to the recording
area or do not allow plastic film containing
much plasticizer to be in direct contact with
it for an extended time.
- 8 -
2. SPECIFICATIONS
Optical system
Light source
Light source changeover wavelength
Wavelength range
Concave diffraction grating
Double- beam single mono-
chromator
Deutrium discharge tube
(200 nm to 350 nm)
Tungsten iodine lamp
(330 to 1100 nm)
Wavelength can be selected
at 330 or 350 nm .
200 nm to 1100 nm
Wavelength repeatability: +0 . 1 nm
Wavelength accuracy
Spectrum band width
Wavelength display
Measurement range
Measurement display
Measurement reproducibility
+0.5 nm
3 nm , fixed
1000.0 nm (0.1 nm)
o to 2 Abs
0.0 to 200.0 %T
0.000 to 2.000 Abs
Can be displayed up to
OOO.OO %T , 0.0000 Abs by
changeover .
+0.001 Abs (0 to 0.5 Abs)
+0.002 Abs
0 . 5 to 1 Abs)
+0.15 %T
- 9 -
Measurement accuracy
Scan speed
Stray light
Baseline flatness
Baseline stability
Clock function
Detector
Line voltage
+0.005 Abs
(0 to 1 Abs)
±. 0.3%T
Checked by NBS SRM930D.
240, 480, 1200,
2400 nm/min
0.1 %
(220, 340 nm)
+0.001 Abs (200 to 1000 nm)
+0.001 Abs/day
Provided
Two silicon photocells
100, 115, 200, 220, 230,
240 volts
Dimensions and weight: 478 mm wide x 460 mm deep x
195 mm high, 15 kg.
- 10 -
3. GENERAL DESCRIPTION OF INSTRUMENT
3-1 Optical System
This instrument measures the absorption of a sample
in the ultraviolet/ visible/near infrared region of
200 to 1100 nm wavelengths to make quantitative
analysis. It can also measure the absorpiton spec
trum, as a matter of course.
Fig. 3-1 shows the optical system of this instrument.
It uses a deuterium lamp in the ultraviolet region
and a tungsten iodine lamp in the visible-to-near
infrared region as the light source. The light from
the light source, after passing through a high order
light cut-off filter, goes to the monochromator that
uses a concave diffraction grating. The light is
monochromated by the monochromator and is split into
two beams by the beam splitter. One of the beams
pass through the sample and the other the reference
sample such as a solvent or other and is incident on
the silicon photocell detector.
- 11 -
M2
D D
Ml: Tungsten iodine lamp
D2: Deuterium lamp
Ml to M4: Mirror
F: Filter
Sl, S2: Slit
G: Concave diffraction grating
BS: Beam splitter
D: Detector
Fig . 3- 1 Optical system.
3- 2 System
Fig. 3-2 shows the block diagram of this system.
After the light signal is converted into an electrica l
signal by the detector and amplified , it is subjected
to A-D conversion. The data thus converted is subjected
to necessary processing by a microcomputer and is
output.
- 12 -
WI
F SI G S2 D
o f1 0 ~ 1E--------11-+-0 --IU~-,Oc---B-<S ~
M D
D2 FI I.TElI 1M VEI. ENGTH CONTIWL CONTlWL
I I ~IA I N
LIGHT MAIN BOIIRO SOURCE 1/1' CONTROL I I I LIGHT POIjER AtIPL II'I ER PIINEL SOURCE IINO EXCHA NGE SUPPLY 11/0 CONVElH'EIl 1/F
Fig. 3- 2 Block diagram of the system.
3- 3 Program Structure
The programs include the following four .
(1) Standard measurement program
This program is supplied with the instrument as
standard and includes Methods 1 through 5.
Method 1 Measurement at fixed wavelength
( %T, Abs)
Method 2 Measurement of change with time at
fixed wavelength (stored in memory)
Method 3 Quantitative analysis
Method 4 Measurement of s pectrum data
Hethod 5 Measurement of change with time at
fixed wavelength (not stored in memory)
- 13 -
(2) Data processing program
This program comes with CRT. The following methods
are included.
Method 11: spectrum data processing
Addition, subtraction, multiplication,
division; differential processing;
smoothing processing; peak detection;
mode conversion; expansion and reduction
of scale; etc .
Method 15: Comment function
Method 16: Command link function (simple program
function)
NOTE: If CRT is not supplied, the memory program
will be supplied instead. This program
permits move of the memory contents, addition,
subtraction, multiplication, division, and
data printout.
(3) Program for setting the spectrophotometer and
control of the input/output unit.
1) Program for setting the spectrophotometer
Method 21: Setting of spectrophotometer
Method 22: Self-diagnosis
Method 23: Baseline correction and wavelength
correction
- 14 -
2) Program related to input/output unit
Method 31: Control of interface with options
Method 32: Positional adjustment of thermal
plotter head
(4) Application program (option)
Application programs are al l included in Method 50.
One program is stored on a piece of ROM cartridge
or floppy disk . The following programs are available.
o Wavelength program (spread sheet system)
o Printout of measurement data at fixed wave-
length intervals
o Kinetics (for enzyme routine)
o Kinetics (for enzyme study)
o Color difference calculation program
o Multi- component analysis program
o Differential quantitative analysis program
o Saving data and measurement parameters onto
floppy disk
o Dissolution test program
- 15 -
4. COMPONENTS & FUNCTIONS
4-1 External View
lI1W.W~ --
i ~ = = = ~ = = =
® = - W =
=
[I II ® CD
®
Fig. 4- 1
Component Function
~ Sample chamber Open the lid by sliding it, and a
cell holder will be in sight.
The beam on your side is the sample
beam and the one on the back side
is the reference beam .
~ Operation panel All operations are performed by
operating the keys on this panel.
(See 4- 2 . )
(2) LCD indicator The wavelength , absorbance, input
of parameters, etc. are displayed
on this indicator.
- 16 -
Component Function
o "Power " switch Located at the bottom of the right-
hand side panel of the instrument.
~ Light s ource unit
o Printer
The light source is located here.
Option. The printer prints out
parameters and measurement results
if supplied.
4-2 Operation Panel
A Print Lis'
Q ~
Key
"Method"
B Auto Zero
GQ~ ~ Display .... list
Fig. 4-2 Operation panel.
Function
This key selects the measurement method.
Pressing it causes the menu selection
mode.
- 17 -
Key
"File"
"Go to WL"
"Auto Zero"
"Print List"
"Print Data"
116, 'V , <J , 1> "
" Display List"
" Control "
[Contro l] [I>]
[Control] [<1]
Function
This key is used for storing parameter s
in the C- MOS RAM or calling them from it .
A wave l ength setting key.
(Ex.) 400 nm [Go to WL] [4 ] [ 0] [0] [Enter ]
A key for automatic setting of 100%T or
AbsO . Pressing this key starts execution
immediately.
A k ey for printing out the measurement
parameters of the method now selected.
Pressing the key starts execution
immediate l y.
A key for printing out the c urrently
displayed wavelength and measurement
value on the printer. Pressing the key
starts execution immediately.
A c ursor key.
A key for changing the measurement mode
of each method to the parameter setting
mode or , conversely, the parameter
setting mode to the measurement mode .
Pressing another key with this key held
down changes the functions of the key.
}
This key is used for shifting the wave
length to the shorte r wavelength side
- 18 -
Key
[Control] [ i!. ]
[Control] [ IJ ]
"Shift"
"Measure ll
"Stop"
"0 ... , 9,
11+, _
" II ,
"Enter II
IIClear"
" -+ 11
*
"Memory"
"
1"
Function
or the longer wavelength side.
}
These keys are used in feeding
winding the chart paper.
A key for options.
o r
A measurement start key. Pressing this
key starts execution.
Measurement suspension key. Pressing
this key during measurement suspends
measurement. It is also used for sus-
pending parameter setting and program
run.
Numerical keys, which are used for
k eying in numerals.
Keys for arithmetic operation such as
addition, subtraction, multiplication,
and division. (option)
Used as a delimiter in entering parameters.
Key for executing the inputting of numericals
values.
Used for cancelling an entered numerical value.
Used for moving the memory contents to
another memory.
Used for specifying a memory number.
- 19 -
4-3 Rear Panel
AC l00v Inlel 2A S8 Ground
£
3
Component
Sampler 1 F
4
Plolter IF
Fig. 4- 3 Rear panel.
Function
CRT IF
7
FDD IF
8
-l--I--{ 9
RS-232C IF
LC Net
10
CD "AC Inlet" Connect it to your outlet.
CD "SB Fuse: Slow blow fuse for the main unit.
(2) "Ground" A grounding terminal.
o "Recorder" An output terminal of the recorder.
o "Sampler IF" A connector to be connected to the
auto sampler, quick flow sampler,
etc.
CD "plotter IF" A connector to be connected to the
(2) "CRT IF"
CD " FDD IF"
o "RS-232C IF"
(9) "LC-Net:
plotter.
A connector to be connected to the CRT.
A connector to be connected to the
floppy disk driver.
A connector to be connected to the
RS -2 32C interface.
A connector for options.
- 20 -
5. TURNING ON "POWER" & STOP OF OPERATION
5-1 Turning on "Power" Switch
(1) Turn ON the "Power" switch at the bottom of the
right-hand side panel of the 7800. The LCD dis-
plays "Under Initialization", and automatic check
of the instrument is started, and the following
items are checked. Upon completion, the parameter
setting mode of "Method 1" (Fig. 5-1) is caused.
o Wavelength (Wavelength is checked)
o Lamp (Light source lights up)
o Lamp exchange (The light source mirror is
changed over.)
o Filter (Filter is changed over)
o Parameter (Measurement parameter is
initialized)
NOTE (1)
:tt: 1 : Pho to ~lode 1. (2) Abs
Fig. 5 - 1 Parameter setting mode of
"Method 1".
If a parameter has been stored in the para-
meter file 1, the " Method" in file 1 will
be called.
- 21 -
NOTE (2)
NOTE (3)
During initial check, LCD displays its
progress in sequence. If "Error" is dis -
played, operation stops at "Method 99 ".
In such a case, turn on the "Power" switch
again, locate the error, and decide whether
measurement is possible or not referring to
Table 5-1. If measurement is possible,
proceed to the next step.
If the Model 7800 is equipped with a plotter
and the plotter output of the parameter file
1 is set at "ON" (see "Method 31 "), turn on
the "Power" switch on the plotter before
turning on the "Power" switch on the 7800.
Otherwise, a parameter error will be dis
played and the operation will stop at "Method
99".
Table 5-1 Error Message and Criteria
of Measurement Feasibility
Filter error Measurement not feasible
Lamp Error Check the light source.
W lamp is lit:
- 22 -
Measurement is feasible
on the wavelength side
longer than 330 nm.
D2 lamp is lit: Measurement is feasible
on the wavelength side
shorter than 350 nm.
Both W and D2 lamps off: Measurement
not feasible
Lamp Exchange Error Measurement not feasible.
Wavelength Error Measurement not feasible.
Parameter Error Heasurement is feasible if the para-
meter setting can be done by key
input.
(2) Call the desired method by the following key operat i on.
CI) Press the [Method] key. LCD displays the menu
selection mode (Fig. 5-2).
~ On the display shown in Fig. 5-2, the method dis
play can b e c hanged in sequence with the cursor
keys ([ \7 ], [.':1 ]).
~ When the desired method is displayed, press the
[Enter] key.
NOTE: The method is affixed with a number. The
desired method can be called also by entering
that number, instead of pressing the cursor
key.
[Number ] [Enter]
- 23 -
The method display and its meaning are given in
Table 5- 2.
Table 5-2 Method Display and
its Meaning
Method LCD display
# 1 1. Fix WL Meas
# 2
# 3
# 4
# 5
#21
#22
#23
#31
#32
#50
2. Time Scan 1
3 . Quanti Analy
4. Spectrum
5. Time Scan 2
21. Internal
22. Self Diagnos
23. Correction
31. Output
32. Zero, Span
50. Application
Meaning
Measurement at fixed wavelength
( %T, Abs)
Measurement of change with time
at fixed wavelength (The result
is stored in memory.)
Quantitative analysis
Spectrum measurement
Measurement of change with time
at fixed wavelength
Initial control
Self- diagnosis
Baseline correction, wavelength
correction
Control of external devices
(option)
Zero and span adjustment of the
plotter
Application program
- 24 -
I tt1~ ; [ Enter]
Menu ~ #1 parameter setting mode (Par. 6-1) Fix WL Meas
[\7] S [.6.]
I tt~~ ; [ Enter]
Menu , #2 parameter setting mode (Par. 6-2) Time Scan 1
[\7] S [.6.] , [ Enter ]
tt99 ; ~lenu ~ #3 parameter setting mode (Par. 6- 3) 3. Quanti Analy
[\7] i [.6.]
I tt~~ ; [ Enter]
Menu , #4 parameter setting mode (Par. 6-4) Spectrum
[\7] ~ [,6,]
I tt99 ; [ Enter]
(Par. ~lenu ~ #5 parameter setting mode 6-5 ) Time Scan 2 5 ..
[.6.] [\7] [\7] t [.6.]
I tt99 ; [ Enter]
(Section 9) Menu ~ #21 menu mode Internal 21.
[\7] S [,6,]
I tt99 ;
II [ En ter ]
(Section 10) Menu , #22 menu mode Self Diagnos 22.
['01 t [.6.] V" ,
I tt99 ; I
[ En ter ] Menu , #23 menu mode (Section 11) Correc tion 23.
[\7] ~ [ ,6,]
I tt99 ; [ Enter]
Menu , #31 menu mode (Section 12) Ou tpu t 31.
[\7] S [,6,] [ En ter ]
tt99 ; Menu ~ #32 menu mode (Section 13) 32. Zero Span
[\7] t [.6.]
I tt99 ; I [ En ter ]
Menu , (Option) Appl ica tion 50 .
Fig. 5-2 Menu selection mode and key operation.
- 25 -
5- 2 Stop of Operation
After making sure there is nothing in the sample
chamber, turn OFF the " Power" switch. About 5 five
minutes later when the light source unit has cooled
down, put on the dust cover.
- 26 -
[Y']
6. MEASUREMENT METHOD
6-1 "1. Fix WL Meas" Measurement of Transmittance and
Absorbance
(1) Call Method 1.
Pressing keys [Method] [1] [Enter] causes the
parameter setting mode of 11ethod 1. Fig. 6-1
shows the LCD display and key operation in
Method 1.
:It 1 : Photo tlode [ Display List]
+-
l. (2) Abs I-
[Y'] l [6] [ Display Lis t ]
:It 1 : Cycle No :It 1 Wl 500.0nm 2. 1 i or [ Measure] 0.025 Abs
[6 ] [Y'] t [6] i <Measurement mode >
:It 1 : Sample No I--
3. 1 [ Go to I'll ] [Wavelength) [ Enter
[\7] t [6] [ Go to Wl ]
:It 1 : Print Out :It 1 Wl 500.0nm 4. (2) Off f--
. [Wavelength) ( En ter ].
<Parameter setting mode> <. Go to ill" . mode' > , Fig . 6-1 LCD display and key operation
in Method 1.
(2) Check and c hange the parameter in the parameter
setting mode shown in Fig. 6-1. Pressing the
- 27 -
cursor key ([ 6 ], [9 ]) to change the LCD display
as shown in the ' of igure, and check the displayed
value. For how to change, refer to Section 7.
NOTE: Measurement parameters are set as shown in
Fig. 6-1 as standard.
(3) Select the measurement wavelength by the following
key operation. Fig. 6-1 shows the change in the
LCD display when the key is operated.
[Go to WL] [Wavelength] [Enter] (Input range 200.0
to 1,100.0 nm)
After this operation , control immediately proceeds
to the selected wavelength.
NOTE (1): If the wavelength has already been set at
the desired wavelength, press [Display List]
to proceed to the measurement mode.
NOTE (2) Press [Auto Zero], as and if necessary.
Execution of "Auto Zero" takes several
seconds.
(4) Mount the sample in the sample chamber. The beam
on your side is the sample beam.
(5) Press the [Me asure] key. If the printer or plotter
is supplied, the result is printed out on it.
(6) If measurement is to be repeated under the same
conditions, repeat the steps in (4) and (5).
NOTE: To change the measurement parameter, press
- 28 -
[Display List).
The parameter setting mode is caused.
6- 2 "2. Time Scan 1" Measurement of Change with Time
at Fixed Wavelength
NOTE: The result obtained by measurement in this
method is stored in memory 1.
(1) Ca ll Method 2.
Pressing keys [Method) [2) [Enter) causes the
parameter setting mode of Method 1. Fig. 6-2
shows the LCD display and key operation in Method
2.
- 29 -
[6] [V']
:j::j: 2 : [ Display Lis
Photo Mode t ]
1. (2) Abs -
[V'] t [6J
:j::j: 2 : Lower Limit -
2. 0. 000 Abs
[V'J j [6]
:j::j: 2 : Upper Limi t r--3. 1. 000 Abs
['7] i [6] • [ Display Li s t ]
:j::j: 2 : Meas Time :j::j: 2 lolL 500.0nm 4. 30m ODs [ Measure] 0.026 Abs
[V'] t [6] <Measurement mode>
:j::j: 2 : Cycle No -
5. 1 [ Go to lolL ] [Waveleng thl [En ter 1
[V'] $ [6] [ Go to lolL ]
:j::j: 2 : Draw Axis ~ :j::j: 2 lolL 500.0nm 6. (2) On -[Wavel eng th 1 [ En ter 1 •
[V'] t [6] <" Go to lolL" mode ">
:j::j: 2 : Line Mode f--7. (1) Full
[V'J i [6]
:j::j:2 : Print Out 8. (3) Off -
<Parameter setting mode>
Fig. 6- 2 LCD display and key
operation in Method 2.
- 30 -
(2) Check and change parameters in the parameter
setting mode shown in Fig. 6- 2 . Press the cursor
key ([ tI ], [ 11 ]) to change the LCD display as shown
in t he figure and check the displayed value. For
how to change , refer to Section 7.
NOTE: The measurement parameters are set as shown
in Fig. 6- 2 as standard.
(3) Select the measurement wavelength by the following
key operation. Fig. 6-2 shows the change in the
LCD display when the key is operated.
[Go to WL] [Wavelength] [Enter] (Input range: 200.0
to 1,100.0 nm)
NOTE (l):
NOTE (2):
If the wavelength has already been set at
the desired wavelength, press [Display List ]
to proceed to the measurement mode.
Press [Auto Zero], as and if necessary.
Execution of "Auto Zero" takes several
seconds.
(4) Mount the sample in the sample chamber. The beam
on your side is the sample beam.
(5) Press the (Measure] key. The result is stored in
memory 1. If the plotter is supplied, the resu~t
is recorded on the plotter.
NOTE (1): To suspend operation during measurement ,
press the [Stop] key.
- 31 -
NOTE (2): If the data in memory 1 is needed, move
data to another memory in accordance with
8- 1.
NOTE (3): The chart speed when the plotter is inter-
fac e d depends on the "Measure Time".
Table 6 - 1 shows the relatio n.
Table 6- 3 Re l atio n between "Measure Time"
and Chart Speed
"Measure Time" " Cha rt Speed " sec/Data (min, sec) (rom/min)
166 m 41 s t o 333 m 20 s 1.2 10
66 m 41 s t o 166 m 40 s 2.4 5
33 m 21 s t o 66 m 40 s 6 2
16 m 41 s to 33 m 20 s 12 1
6 m 41 s to 16 m 40 s 24 0. 5
3 m 21 s to 6 m 40 s 60 0.2
1 m 41 s to 3 m 20 s 120 0.1
o m 01 s to 1 m 40 s 240 0.05
(6) To make measureme nt under t he same conditions ,
repeat the steps in (4) and (5).
NOTE: To change the measurement paramete rs, press
the [Display List]. The parameter sett ing
mod e is caused.
6 - 3 " 3. Quanti Analy " Quantitative .Analysis
This method is a mode for making quantitative analysis .
It permits two - wave l e ngth processing and three- wa ve
- 32 -
processing, in addition to one- wavelength processing.
Quantitive analysis can be made with high accuracy by
selecting a method suited to the sample condition out
of these three processing methods.
In preparaing calibration curves, calibration points
up to maXlmum 20 points are plotted and a calibration
curve suited to the purpose can be selected out of
the straight line passing through the zero point,
regression straight line and polygonal approximation
curve. If the slope of the calibration curve is known,
calculation of coefficients can be made by entering
the value.
Fig. 6-3 shows the flow of quantitative analysis.
I Set parameters in 7800 l 1
I Blank measurement of standard sample I
1 Input of concentration of standard sample and measurement of absorbance (input)
1 I Preparation of calibration curve l
1 I Blank measurement of sample I
1 I Sample measurement I
Fig. 6-3 Flow of quantitative analysis.
- 33 -
The structure of the mode of Method 3 is shown in
Fig. 6-4. In this method , the desired mode including
the menu mode can be called , as necessary. To perform
operation in sequence , press the [+] key, and control
proceeds to t h e next mode. To return to the preceding
mode, press the [-] key .
- 34 -
[ 1 ] [ Enter] Parameter se tting mode l. Wave leng th 1 [x] 2. Ijaveleng th 2 3. Wave length 3 4. Cycle No 5. Sample No 6. Print Out
[-] I [+ ]
Menu mode [ 2 ] [ En ter ] Cal ibration point i nput
~ l. Blank < 1 >
<2>
<3>
<4>
<5>
Conditions [x] 2. Conce and Abs
Standarts i [- ] ! [+ ]
Calib Curve Calibration curve
Meas Blank
Meas Sample <-
selection mode [ 3 ] [ Enter] l. Conc= a *Abs
2. Cone = a * Abs + b [x] 3. Li ne Segmen t
4. Conc= K * Abs +c
[ --:- ] i ! [ + ]
Blank m~asurernent [ 4 ] Enter] Samp le Blank
~
[x] i [ - ] ! [ +]
[ 5 ] [ En ter ] Sample measurement ~
[xJ
Fig. 6-4 Structu re of mode and key
operatio n in Method 3.
- 35 -
mode
mode
mode
[ - ] [ + ]
[6J
The key operating sequence is given below for each mode.
Call Method 3.
Pressing keys [Method ] [3] [Enter] causes the menu mode
in Method 3. Fig. 6 - 5 shows the LCD display and key
operation in the menu mode.
I :j:j: 3 : Menu
. < 1 > Condi ti ons
[V'J j [6J
I :j:j: 3 : Menu < 2 > Standards
[V'J i [6J
I :j:j: 3 : Menu < 3 > Ca lib Cur ve
[V'] [V'J j [6J
Menu Meas Blank
Menu Meas Sampl e
[ Enter J 1-------+ To parameter setting mode (1)
. [ Enter] To the calibration point i nput mode
for standard sample (2)
[ Enter J To the calibration curve -+ .
selection mode (3)
[ Enter] ~------------, To blank measurement mode (4)
[ En ter J ~------+ To sample measur·ement mode (5)
Fig. 6 - 5 LCD display and key operation
in the menu mode.
Display the desired mode with the cursor keys ([ 9].
[ 6]) in the menu mode in Fig. 6- 5, and press [Ente r ] .
The display changes to the desired mode.
- 36 -
NOTE (1): The display can be changed to the desired
mode also by entering a number «1 > to < 5»
in Fig . 6-5, instead of using the cursor
keys.
NOTE (2): Press the [Print List] key in the menu mode
in Fig. 6-5 or in the sample measurement
mode in Fig . 6-1 0, and al l quantitative
analysis parameters including the calibration
curves can be presented on the plotter or
printer . In other modes, the parameters
of that mode can be printed out.
Calibration curve can not be printed out
on the MTP-397.)
- 37 -
(1) Parameter s etti ng mode
[6]
Pressing ke ys [1] [Ente r] on the d i splay in Fig .
6- 5 ca us es the parameter setting mode in Fig. 6- 6 .
~ Iitr. [ En ter ] , 1 it r. Wave length 1 11ave leng th 1
500.0nm 1500.0nm [Have length] [ En te r 1
[\7] l [6]
1 it ~. : Wave I eng th 2 I [Enter] - I it r. Havelength 2
O.Onm -CHavelength] • O. Onm
[ En te r 1 [\7] ~ [6]
1 itf !la ve I eng th 3 I [ En ter ] -I it r. !lave length 3
O.Onm • [I,avclcngth] • O. Onm [ En te r 1
[\7] [\7] r [6]
1 it r. : I· [ En ted
~ Iitr. Cycle No. Cyc le No. 1
• 1 00 [ Enter] [\7] t [6]
I it g. : [ En ter ]
, I it g. Sampl e No . Sampl e No. 1
• 1 00 [ Enter] [\7] t [6]
~rint Out I ~ [ En ter ] it 3 : Print Ou t -
~ 6. (2) orr 6. • (2) Off [Number ] [ En ter 1
<Paramet er setting mode> <Par amet er input wait
Fig. 6- 6 LCD display and key operation
in parameter setting mode .
- 38 -
I
mode>
On the display in Fig. 6- 9, set parameters for
the 7800 , inc luding the quantitative analysis
wavelength. There are 3 quantitat ive analysis
wavelengths ( "Wavelength") 1, 2 and 3. Up to
what number the wavelength is to be set, 1, 2 or
3 , depends on the method of calculation.
Make setting as follows. Set unnecessary wave
lengths to zero.
l-wave length processing: wavelength 1
2-wavelength processing: wavelengths 1 and 2
3-wavelength processing: wavelengths 1 , 2 and 3
For the input method, refer to Section 7 . After
the input , proceed to the desired mode by the
following key operation .
o Standard sample calibration point input mode (2) [+]
o Sample measurement mode (5) [-]
o Menu mode [x]
(2) SEandard sample calibration point input mode
Pressing keys [2] [Enter] on the display in Fig.
6- 5 or pressing the [+] key on the display in
Fig. 6-6 causes the standard samp le calibration
point input mod e in Fig. 6- 7.
- 39 -
I
[ En ter ]
L:t:t:_23:-.-_S_t_an_d_ar_d_s __ ---' ~-----------l'1 :t:t: 3 . Blank O. 000 ~ .
[ Measure ] or
Standards Blank. 0.000
[Numeral] [ Enter J
I I ~- [ En ter ]
:t:t: 3 : Sd tandards . 2. Cone and Abs L-________ [ Stop]
[9] J [6]
<Calibration point input mode>
~ I :t:t:(r): ~one and Abs '
[9] t [6]
:t:t: 3 : Cone and Abs (2) •
[9] t [6] 1 ..... 0 ,, _____ -l
Abs I +r (3) :
\..IUIII.... (lIlU
• T
? :t:t: 3 : Cone and Abs
(20) • <Input wait mode>
Fig. 6-7 LCD display and key operat ion
in calibration point input mode.
This mode permits the following operation.
1. Input and measurement of standard sample blank
2. Input of standard sample concentration or
input of absorbance
1. Blank
a) Press the [Enter) key when "1. Blank" is dis-
played on the LCD. The input wait mode in
Fig. 6-7 will be selected.
- 40 -
b) Mount the standard sample blank in the sample
chamber and press the [Measure] key. Measure
ment is carried out and the initial display is
resumed.
NOTE: When the blank is known, input can be made
through the numeric keypad.
2. Conc and Abs
a) Pressing the [Enter] key when "Conc and Abs " is
displayed on the LCD causes the input wait mode
in Fig. 6- 7.
b) Key in the standard sample concentration sequentially
from (1). Press the (V) key to advance the number
or the (6 ) key to reverse it.
Example: (1) O. 5, (2) 1. 0, (3) 1.5
<Key operation >
NOTE:
c)
[ 0] [.] [5] [Enter]
[Il ] [1] [.] [0] [Enter]
[Il ] [1] [ .] [5] [Enter]
A maximum of 20 items can be entered.
After the concentration has been entered , press
keys [ ->< ] [1] or the [6 ] cursor key to resume
( 1) .
d) Mount the standard sample with concentration
(1) in the sample chamber and press the [Measure]
key. Measurement results will be displayed in
- 41 -
the Abs column. Advance the number to (2)
with a cursor key and make me asurement in the
same manner.
e) After all standard samples are measured,
press the [Stop] key.
play will be resumed.
"2. Conc and Abs " dis -
a) through e) describe the standard key operation
procedure. If the absorbance of the standard
sample is known, input can be made through the
numeric keypad or changed in case of erroneous
input or measurement. Operational rules for
this procedure are given below.
CD Moving the display number
[6 ] or [V]: moves one by one
[ + ] [Number] (1-20): moves to the desired number
CD Entering concentration and absorbance through
numeric keypad
[Concentration] [,] [Absorbance] [Enter]
G) Entering only absorbance through numeric keypad
[,] [Absorbance] [Enter]
G) Measuring only absorbance
[Measure]
GD Input of only concentration
[Concentration] [Enter]
- 42 -
G) Input of concentration and measurement of
absorbance
[Concentration] [,] [Measure]
G) Conversion between calibration point input
mode and input wait mode
[Enter ]: From the input mode to the input
wait mode
[Stop] : From the input wait mode to the
input mode
NOTE: Operate the keys in 0 to ® when the
desired number is displayed .
After all inputs in the calibration po int input
mode in Fig. 6-7 have been completed, se l ect the
desired mode by the following key operation.
o Calibration curve selection mode (3) [+]
o Parameter s etting mode (1) [-]
o Menu mode [x]
(3) Calibration curve selection mode
Pressing keys [3 ] [Enter ] on the display in Fig.
6-5 or the key [+] in Fig. 6-7 causes the calibra
tion curve selection mode in Fig. 6- 8.
- 43 -
[6J [V'J
:l:J: 3 : Calib Curve 1. Cone = a *Abs
[V'] i [6J
:l:J: 3 : Ca 1 i b Curve 2. Cone = a * Abs + b
[V'] S [6J
:l:J: 3 : Ca 1 i b Curve 3. Line Segment
[V'J ~ [6J
Calib Curve Cone =K*Abs+C
1
[ Enter]
~-------'
[ Enter J
[ Enter]
[ Enter J
[Nuiner all [ En ter J
Value a is displayed for several seconds.
Value a and b are displayed for several seconds.
:l:J:3 :K •
1 [Numeral] [ Enter J
1:l:J:3 :C •
<Input wait mode>
Fig. 6- 8 LCD display and key operation in
calibration curve selection mode.
In the calibration curve selection mode in Fig.
6-8, select a calibration curve out of 1 to 4
below.
1. Conc=a*Abs: straight line which passes the
point of origin
2. Conc=a*Abs+b: regression straight line
3. Line segment: polygonal approximation curve
4. Conc=K*Abs+C: preparing calibration curve
by keying in K and C
- 44 -
o To select any of I to 3, display the desired
item by keying [Number] [Enter ] or by pressing
cursor key [6 ] or [9 ], and press the [Enter]
key. Then a calibration curve will be prepared.
o Selecting 4 ([4] [Enter ], or [9 ] or [6 ] [Enter])
causes the K and C input wait mode. Key in K
and C according to the LCD display.
After the input has been completed, proceed to the
desired mode by the following key operation.
o Blank measurement mode (4) [+]
o Calibration point input mode (2) [-]
o Menu mode [x]
(4) Blank measurement mode
Pressing keys [4] [Enter ] on the display in Fig.
6-5 or pressing keys [Control] [+] in Fig. 6-8
causes the blank measurement mode in Fig. 6-9.
:l:t 3 Sample Blank 0.000 Abs
Fig. 6-9 Blank measurement mode .
In Pig. 6-9, mount the sample blank in the sample
chamber and press the [Measure ] key. Measurement
will be performed and the results displayed.
- 45 -
Upon completion of measurement, proceed to the
desired mode by the fo llowing key operation.
o Sample measurement mode (5) [+]
o Calibration curve selection mode (3) [-]
o Menu mode [* )
( 5 ) Samp l e measurement mode
Pressing keys [5) [Enter ) on the display in Fig.
6-5 or pressing the [+ ) key in Fig . 6- 9 causes
the sample measurement mode in Fig. 6-10.
[ Measure ] in :
i'lL 0.002 Abs 500.0 nm
:tt3 0.390 Abs 0.140 Cone
I i [ Measure ]
Fig. 6-1 0 Sampl e measurement mode .
In the sample measurement mode in Fig. 6-10, mount
a sample with unknown concentration in the sample
c h amber a nd press the [Measure) key. Measure-
ment results will be displayed on the LCD . Repeat
t h e opera tion in t h e same manner to start measur·e -
ment successively.
NOTE: To change the sample number on the display in
Fig. 6-10, press the [+) key. Control returns
t o the parameter setting mode in Fig. 6- 6.
- 46 -
6-4 "4. Spectrum" Absorption Spectrum Measurement
(1) Call Method 4
Pressing keys [Method ] [4] [Enter ] causes the para-
meter setting mode in Method 4. Fig. 6-11 shows
the LCD display and key operation in Method 4.
:j:j: 4 : Photo Mode ~
1. (2) Abs - [ Display Lis t ]
[V'] i [6]
:j:j: 4 : Start i'lL -2. 1l00.0~ [ Display List] :j:j: 4 : i'lL 500.0nm
0.025 Abs [V'J 1 [6 ] [ Measure]
<Heasur ement mode> :j:j: 4 : Eod i'lL f--
3. 200.0om [ Go to i'lL ] [Waveleng th) [ Enter]
[V'] 1 [6]
:j:j: 4 : i'lL Sca le f--4. (4) 50om/em [ Go to i'lL ] :j:j: 4 : i'lL 500.0om
~
[V'] 1 [6] ,
[Wavelength) [ En ter ] •
<" Go to \~II mode>
:j:j: 4 : Scan Speed 5. (4) 2400mm/m i I--
[6) [V' ) [V') 1 [6J
:j:j: 4 : Lower Limi t I-6. 0.000 Abs
[V'] 1 [6]
:j:j: 4 : Upper Limit f--7. 1. 000 Abs
[V'] 1 [6]
:j:j: 1\ : Cycle No I--8. 1 I
[V'] S [6J
:j:j: 4: Print Out -9. (3) Of f
[V'] 1 [6J
:j:j: 4 : Draw Axis f---10 . (2) On
[V'] t [6]
:j:j: 4 : Line 110de 11. (1) Full f--
<Parameter setting mode>
Fig. 6-11 LCD display and key operation in Method 4 .
- 47 -
(2) Check and change the parameters in the parameter
setting mode in Fig. 6-11. Press the cursor key
[6] or [~] to change the LCD display as shown in
the figure and check the displayed value. For
how to change, refer to Section 7.
NOTE: The measurement parameters are set as shown in
Fig. 6-11 as standard.
(3) Press the [Display List] key to proceed to the
measurement mode.
(4) Mount a sample in the sample chamber. The beam
on your side is the sample beam.
(5) Press the [Measure] key. The results will be
stored in memory 1 and printed out on a plotter,
if provided.
NOTE (1): To suspend the measurement, press the
[Stop] key.
NOTE (2) If data in memory 1 is necessary, move
the data to another memory referring
to 8-1.
(6) To continue measurement under the same conditions,
repeat steps (4) and (5).
6-5 "5. Time Scan 2" Measurement of Ohange with Time
at Fixed Wavelength
NOTE: Results obtained by measurement in this method
are not stored in memory.
- 48 -
(1) Call Method 5.
[6] (9
Pressing keys [Method ] [5] [Enter] causes the para-
meter setting mode of Method 5. Fig. 6-12 shows
)
the LCD display and key operation in Method 5.
:It 5 : Phot Mode [ Display Lis t ]
1. (2) fibs i---
[9 ] $ [6]
:It 5 : Lower Limit [ Display List] :It 5 : i'lL 500 .0nm 2. 0.000 Abs 0.000 Abs
or [ Measure] I t <Measurement mode [9] $ [6]
:It 5 : Upper Limit i--- [ Go to i'lL ] l ,W,.,,,., "" E. to< 3. 1. 000 fibs
[9] l [6]
>
:It 5 : Meas Time [ Go to WL ] :j:j: 5 : i'lL 500.0nm 4. 30mOOs •
[9] ; [6] [Wavelength] [ En ter ]
<"Go to i'lL" 'f:-I-'>
:It 5 : Cycle No 5. 1 f--
[9] t [6]
:It 5 : Draw Axis i---
6. (2) On
[9] l [6]
:It 5 : Lime Mode -7. (1) Full
[9] l [6]
:It 5 : Print Out f--
8. (1) On
.. . [9] j [6]
:It 5 : Chart Speed 9. (4) lOmm/min f--
Fig. 6-12 LCD display
<Parame·ter setting mode> and key operation
in Method 5.
- 49 -
]
(2) In the parameter setting mode in Fig. 6-12, check
and change the parameters. Press the cursor key
[ ~ ] or [V] to change the LCD display as shown in
the figure, and check the displayed value . For
how to change , refer to Section 7.
NOTE: The measurement parameters are set as shown in
Fig. 6-12 as standard.
(3) Set the measurement wavelength by the following
key operation. Fig. 6-12 shows how the LCD dis
play changes when keys are operated.
[Goto WL] [Wavelength] [Enter] (Input range: 200.0 to
1,100.0 nm)
The set wavelength is valid immediately after the
operation.
NOTE (1): If the desired wavelength has already been
set, press the [Display List] key to
proceed to the measurement mode.
NOTE (2) Press the [Auto Zero] key, as necessary.
It takes several seconds to execute
(4) Mount a sample in the sample chamber. The beam
on your side is the sample beam.
(5) Press the [Measure ] key. The result will be
recorded on a plotter, if provided.
- 50 -
(6) To make measurement under the same conditions ,
repeat steps (4) and (5).
NOTE : To change the measurement parameters , press
the [Disp l ay List) key. The parameter
setting mode wil l be caused.
- 51 -
7. METHOD OF SETTING PARAMETERS
[6]
Parameters for this instrument are set in the
parameter setting mode in respective methods.
Calling a method causes the parameter setting mode
for that meth od .
If , for example, keys [ ~Iethod ) [1) [Ente r) are pressed
to call Method 1, the parameter setting mode in
Fig. 7 - 1 will be displayed.
I~f. I· [ En ter ]
I~f. Photo Mode Photo Mode (2) Abs • (2) Abs
[Number] [ Enter] [V'] S [6]
[ En ter ] I ~ 1 : Cye! e No I ~ ~. Cycle No
• 1 2. 1 [ Enter] [Numeral ]
[V'] [V'] t [6] I [ En ter ] I ~l: Sample No I~l Sample No
1 ~[ NumeralJ [ • 1 En ter ]
[V'] t [6] [ En ter ]
~ I ~ 1. ~ 1~1 Prin tOut Print Out (2) 0 f f I 4. r:~) Off
[Number ] [ En ter ]
<Parameter setting mode> <Parameter input wait
Fig. 7- 1 LCD display and key operati?n
in setting parameters in
Method 1.
- 52 -
mode>
Basic rules in setting parameters are given below.
(1) Pressing the cursor key (6 ) or (V) in the
parameter setting mode changes the contents
of LCD display (see Fig. 7-1).
NOTE: Each parameter is affixed with a number.
The desired parameters can also be displayed
by pressing keys [Number] [Enter] .
(2) Pressing the [Enter] key when the desired
parameter is displayed causes the parameter
input wait mode.
(3) Pressing the [Enter] key after entering a
numerical value or number in the parameter
input wait mode resumes the parameter setting
mode, and the parameters can be changed.
(4) If a number (the number is affixed in a
parenthesis in the case of "Photo Hode " below,
for example , ) is to be entered in the parameter
input wait mode, operate the cursor key ([~],
[~]) to change the parameter. When the desired
parameter is displayed, press the [Enter] key.
Example: "1. Photo Hode"
- 53 ~
:IH:
1.
Photo Hode [<J] ~H : Pho to tlode [<J] :It 1 : Photo ~lode +--- to 4- ---..
1(1) T% [C>] 1. 1(2) Abs [C>] 1. 1(3)
t I
[<J]
[C>]
Fig. 7-2 Change of parameter input
wait mode for "Photo Mode".
(5) When entering a numerical value, key in a
value within the input range referring to
Table 7- 1.
For details of parameter contents, refer to
Table 7- 1.
Examples of change are given below.
[Example 1] Change "1. Photo mode" to "T%"
Key in as shown in Fig. 7- 3.
:It 1 : Pho to ~lode 1. (2) Abs
:It 1 : Pho to tlode 1. (1) T% L-____________ ~
[ En ter ] :It 1 : 1.
Photo Mode • (2) Abs
1 [<J]
[ En ter ] :It 1 : I'ho to Mode <-----I 1.. (1) T %
Fig. 7-3 LCD display and key operation
when changing "1. Photo Mode".
- 54 -
Sil
J
[Example 2] Setting "2. Cycle No." to 3 and
"Cyc l e time" to 2 minutes 30 seconds
Key in as shown in Fig. 7-4.
I :!:j: 21. Cycle No [ En ter ] :!:j: 1 : Cycle No
1 I-------~ 2. I 1 L-____________ ~
1 [3 ] [En ter ] (Number of times)
[2] [.] [3]
L:!:j: __ ~_. _: _C_y_cl_3e_N_o_2 _~_3_0S---, +-[_0_] __ [ _E_n_te_r_]_-----1IL:!:j:_~_. _~_y_C l_e_T_iO_m_~O_o_s__'1 (Time) - .
<Parameter setting mode> <Parameter i nput wait mod e>
Fig. 7- 4 LCD display and key operat i on
when changi ng " 2 . Cycle No . Time ".
NOTE: As a delimiter between minutes and seconds in
"Cyc l e Time ", "." is use d. When "Cycle No. " is
one, "Cyc l e Time " is unnecessary and, t herefore ,
pressing keys [1) [Enter ) resumes the parameter
setting mode.
The method of changing other parameters is the
same as shown in the above examples. Table 7-1
shows the parameter funct{ons, input range,
input method, etc. The input range of some
parameters is limited by the set values of other
parameters. (See Tables 7-2 and 7-3) Points to
be noted in entering parameters are given in
Notes 1 through 8.
- 55 -
Table 7- 1
Display Function Initial value Input range Input method Remarks
Photo Mode Measur ement mode (2) Abs (1) Transmittance %T , (2) Absorbance Abs, (3) Single beam SB Number
St.a r t WL Star t. wavelength (longer 1100 nm
wavelength side) 200 . 0 to 1100 .0 nm Numerical value See Note (1) .
End WL End wavelengt.h (shorter 200 nm
wavelength side)
WL Scale \~avelength scale (4) 50 nm/cm (1) 5, (2) 10, (3) 25 , (4) 50 nm/cm Number See Notes (1) and (2) .
Scan Speed Scan speed (4) 2400 nm! (1) 240 , (2) 480, (3) 1200, (4) 2 400 nm/min Number See Not.e (2) . min
Lower Limit Measurement range 0.000 Abs or (n) -500.0 t.o 500 . 0
(minimum value) O. O%T (ASS) - 5 . 000 to 5.000 Numerical value
Upper Limit Measurement r ange 1.000 Abs or (5. S) - 500.0 to 500 . 0
(maximum value) 100 . 0tT
Meas Time Measur ement time 999 min 59 sec 1 sec to 999 min 59 sec Numerical value
Cycle No . and Time Repeated measurement 1, Number of cycles 1 t.o 999, Time 1 sec to 999 min 59 sec Nume r ical value See Not.e (3) .
and time o min 00 sec
Chart Speed Chart speed (4) 10 mm/min (1) I, (2) 2 , (3) 5, (4) 10, (5) 20 , (6) 50, (7) 100 , Number "Met.hod 2" only
(8) 200 mm/min
Draw Axis Writing frame when (1) On (1) On, (2) Off , (3) Draw Number See Note (4) .
recorded on plotter
Line Mode Line drawing mode (1) Full (1) Full (full line); (2) Dott.ed (dotted line) ; (3) Br oken Number
(broken line); (4) Chain (one-point chain line); (5) Change
«1) to (4) are displayed sequentially)
Sample No . Sample number 1 o to 999 Numerical value See Note (5) .
Print out Printer and plotter (1) On (1) On , (2) Off Number
outputs (1) Seq (1) Seq (onQ writing) ; (2) Overlay (overlaid writing), Number "Method 2" ,
(3) Off "Method 4"
Aut.o Zero Setting of 100%T and Press the [ Au to Zero] key. as necessary . See Note (6).
Abs 0
Go to WL \.;ravelength sett i ng 500 nm 200 . 0 to 1100 . 0 nm Numer ical value Sett.ing with the
[ Go to WL ]key .
i See Note (7) . , -- .-
- 56 -
NOTE (1): The input range of the measurement wave -
length is 200.0 to 1,100.0 nm which, how-
ever , is limited by the WL scale as shown
in Table 7-2. If setting is made beyond
the restriction in Table 7-2, an error
will be displayed when the [Measure] key
is pressed.
Table 7- 2 " WL Scale" and Settable
Wavelength Range
-Have length Scale [nm/em] Settable wavelength range [nm]
5 200 or 10loler
10 200.1 to 400
25 400 . 1 to 900
50 400.1 to 900
NOTE (2): OWL Scale" is limited by "Scan Speed" as
shown in Table 7-3.
Table 7- 3 Relation between "S Can Speed " and
oWL Scale"
Scan Speed (nm/min) Data acquisition
Wavelength 240 480 1200 2400 interval in nm/data
Scale (nm/em)
5 0 X X X 0.1
10 0 0 X X 0.2
25 0 0 0 X 0.5
50 0 0 0 0 1.0
- 57 -
NOTE (3) Enter the number of cycles and press the
[Enter] key, and then key in time. Use
"." as a delimiter between min and sec
(see Example 2).
NOTE (4): Selecting" (3) Draw" immediately draws a
frame on the plotter.
NOTE (5): Sample number 999 is followed by O. The
NOTE (6)
sample number is incremented by 1 in each
measurement.
Pressing the [Auto Zero] key lights up the
"Measure" lamp and starts execution imme
diately. When it ends, the [Stop] lamp
lights up. It takes several seconds for
execution.
NOTE (7): The wavelength is set with the [Goto WL]
key. To set it at 310 nm, for example ,
key in as follows. When the input is
completed , execution starts immediately.
[Goto WL] [3] [1] [0] [Enter ]
NOTE (8): Parameters include those in "Method 3"
quantitative analysis, in addition to
those shown in Table 7-1. They are des
cribed in 6-3.
- 58 -
8. DATA FILE AND PARAHETER FILE
8-1 Data File
Data obtained by measurement in "Hethod 2" or "Method
4" is stored in memroy 1. If the next measurement is
made with the previous data stored in memory 1, the
previous data in memory 1 will be destroyed. If
necessary, move the data in memory 1 to another memory
by the following operation. There are 6 memories in
total and 6 pieces of data can be stored.
4-rule arithmetic operation can be made between a
memory and constant or between memories.
(1) Moving memory contents
[Memory) [ml) [ ->- ) [m2) [Enter)
ml, and m2: Memory numbers Input range: 1 to 6
Contents of memory ml are moved to memory m2 .
The LCD display c hanges with key operation as shown
in Fig. 8-1.
(Display in "Methods 1 to 5")
1 [ Memory J
:j:j: 4. 1. 2 3 4 5 6
• I [lJ [-J [2J
:j:j: 4. 1. 2 3 4 5 6 1 m 2 •
I . [ En ter J !
(Display in "Methods 1 to 5")
Fig. 8-1 LCD display when the (Memory) key is operated.
- 59 -:
NOTE: The number of the memory in which data is stored
is affixed with a period " II In Fig. 8-1, the
number is affixed to memory 1.
(2) Presenting memory contents on plotter
[Memory] [m] [Measure]
m: Memory number Input range: 1 to 6
Contents of memory m are presented to the plotter.
(3) 4-rule arithmetic operation between memory and
constant
[Memory] [ml] [+] ([-], [x] or [/]) [N] [ + ] [m2] [Enter]
ml and m2: Memory numbers Input range: 1 to 6
N: Constant Input range: 0 to 999.99
Calculation (addition, subtraction, multiplication
or division) is made between the contents of memory
ml and constant N, and the result is stored in memory
m2.
(4) 4-rule arithmetic operation between memories
[Memory] [ml] [+] [Memory] [m2] [ + ] [m3] [Enter]
[ -]
[x]
[!]
ml, m2 and m3: Memory numbers Input range: 1 to 6
Calculation (addition, subtraction, multiplication
or division) is made between contents of memories
ml and m2, and the result is stored in m3.
- 60 -
NOTE (1): The same parameter may be specified in ml,
m2 and m3. In that event , contents stored
in ml will be destroyed .
NOTE (2): If the attribute differs when making cal
culation between memories, an error message
will be displayed.
NOTE (3): If division is made by zero or if the result
of calculation has overflown, an error
message will be displayed.
8- 2 Parameter File
This instrument permits the selected parameters in
Methods 1 t h rough 5 , Hethod 21 and Method 31 to be
stored in one parameter file . Parameters are stored
in the C- MOS RAt1 backed up by battery . There are 5
parameter files in total , so that 5 different parameters
can be stored .
NOTE: If the RAM card (option) is provided , the number
of the parameter files will be 25. No.1 through
No.5 are the files provided in the main unit as
standard and No . 6 through No.25 are the files
for the RAr1 card.
(1) Storing parameters in file
Perform the following key operation in the desired
"r1ethod " .
[File] [n] [Enter]
- 61 -
n: File number Input range: 1 to 5
The LCD display changes with key operation as
shown in Fig. 8-2.
(Display of "Methods 1-5 " )
:tt4:. 1. 2
Fi l e ]
345
I [2] .------------------------
:tt4::2 1. 2 3 4 5
[ En ter ]
(Display of "Methods 1- 5")
Fig. 8- 2 LCD display when (File) key is pressed.
NOTE (1): The number of the file in which parameters
are stored is affixed with a period ".".
If the file is affixed with a period, "E 29"
will be displayed and , after a while , the
display of "Methods 1 to 5" will be resumed.
NOTE (2): If the RAM card is provided, files of 6 through
25 are disp l ayed by pressing the [ ~ ] or [6 ] key.
(2) Calling parameter from file
Perform the following key operation in "Method 1-5".
[File] Tn] [Measure]
- 62 -
n: File number Input range: 1 to 5
The parameter setting mode for the "Hethod " corres
ponding to the entered file number is selected.
(3) Transferring file contents
Perform the following key operation in "Methods
1-5".
[File] [nl] [ + ] [n2] [Enter]
nl and n2: File numbers Input range: 1 to 5
Contents of file nl are transferred to n2. After
making sure n2 is affixed with a period ".", press
the [S top ] key.
(4) Deleting file contents
Perform the following key operat i on in "Methods
1- 5" .
[File] [0] [ + ] [n] [Enter]
n: File number Input range: 1 to 5
The period " . " affixed to the number disappears
simultaneously with deletion of the contents of
file n. After making sure of it, press the [Stop]
key.
- 63 -
9. "METHOD 21 " SETTING OF SPECTROPHOTOMETER
[,0,]
"Method 21" permits selection of the light source,
setting of the light source changeover wavelength
and displayed data; change of the number of digits and
setting of date and hour.
Press keys [Method) [2) [1) [Enter ) to call "Method 21".
The menu mode in "Hethod 21" (Fig. 9-1) is caused.
-+ I :\:j:21: Lamp [ Enter]
, I :\:j:1~ : Lamp 1. (l) W&D2
• (l) W&D2
[Numeral] [ Enter] [9] t [,0,]
\ :\:j:~~ : Lamp Ex WL
I [ En ter ]
'\ :\:j:~~ : Lamp Ex i'lL
340.0 ' [Numeral) • 340.0 [ En ter )
[9) t [,0,)
I :\:j:21: Decimal [ En ter )
'\ tt~~ : Deci mal .1)4 digi ts . 3. (1) 4 digi ts
[Number) [ Enter) [9] [9] $ [,0,]
\ :\:j:21: Time I ' [ Enter)
'\ :\:j:~~ : Time
• (1) On 4. (1) On [Number) [ En ter )
<Menu mode> <Input wait mod e>
Fig. 9-1 LCD display and key operation
in "Method 21".
Parameters in the menu mode in Fig. 9-1 mean:
1. Selection of light source
2. Light source changeover wavelength
- 64 -
3. Number of digits of displayed data
4. Setting of built-in clock
These parameters can be changed in the same manner
as ordinary measurement parameters (see Section 7).
The parameter input range and input method are
briefly described below.
(1) "Lamp" Selection of light source
Input range: (1) W & D2 (both Wand D2 on);
(2) W (only Won); (3) D2 (only
D2 on); (4) No Lamp (both Wand
D2 off)
Input method: In numbers
Initial value: (1) W & D2
(2) "Lamp Ex WL": Light source changeover wavelength
Input range: 330 .0 to 350.0 nm
Input method : In numerical values
Initial value: 340 nm
(3) "Decima l" Number of digits of displayed data
Input range: (1) 4 digits; (2) 5 digits
Input method: In numbers
Initial value: (1) 4 digits
(4) "Time " Setting of built- in clock
Input range: (1) On; (2) Off; (3) Set
Input method: In numbers
Initial value: (1) On
- 65 -
Selecting "(3) Set" changes the . display as shown
in Fig. 9-2.
:f:j:21: Time Set 4. 187
Fig. 9-2 Time input wait mode.
Enter the year , month, date , hours and minutes in
2-digit value each, with commas "," as delimiters.
The display changes with the input.
Example: 15 hours 30 minutes on April 10, 1987
[8) [7) [,) [0) [4) [,) [1) [0) [,) [1) [5) [,) [3) [0] [Enter)
With completion of input, the display changes to
" 1 (1) On ". Pressing the [Enter) key again
changes the display to "(1) On".
NOTE: Be sure to follow the specified format in entry.
If " (3) Set" has been erroneously selected,
press the [Stop) key.
- 66 -
10. "METHOD 22" SELF-DIAGNOSIS
[6]
"Method 22 " makes self-diagnosis of the instrument.
Press keys [Me thod) [2) [2) [Enter) to call "Method 22 " .
The menu mode in "Method 22" in Fig. 1 0-1 is ·caused.
I ~ 212.: Check
· Wave l ength
[\7] 1 [6]
I :it 22: Check
· 2. Scan
[\7] [\7]! [6]
I :it 22: Check
· 3. Fi Iter
[\7] l [6]
I :it 22: Check
->. 4. Lamp
<Menu mode>
[ Enter]
[ Enter]
[ Enter]
[ Enter]
f "Measure" lamp is lit during execution.
l "Good " i s displayed after execution.
f ,"Measure" lamp is lit during execution.
1 ,ItGood ll is displayed after execution .
J Visually check the color of beam
l in sample chamber
(see operating procedu re).
f "Measure" lamp is lit during execution.
'\ "Good " is displayed after execution.
Fig. 10-1 LCD display and key operation
in "Method 22 " .
The parameters in the menu mode in Fig. 10-1 mean:
1. Wave l e ngth check
2. Wavelength drive c heck
3. Fi l ter check
4. Light source check
Press t h e [Enter) key when a parameter to be c hecked
- 67 -
is displayed. The "Measure" lamp lights when I, 2
or 4 is being executed, and "Good" or "Error" is
displayed at the end. If "Error" is displayed,
take actions according to Section 14. To check
"3. Filte r", proceed as follows.
["3. Filter" check]
(1) Press the [Enter] key when " 3 . Filter" is
displayed.
(2) Open the sample chamber lid, place a piece of
white paper in the sample beam, and visually
check that red light is there.
NOTE: It takes some time for the filter to move
after the [Enter] key is pressed.
(3) Press the [Enter] key. Make sur~ the beam color
changes to light blue.
(4) Thereafter, make sure each press on the [Enter]
key changes the beam color to violet, colorless
(invisible because it is ultraviolet light),
white and red again.
(5) Press the [Stop] key. After a while, LCD indi-
cates "Good".
NOTE: The "Me asure " lamp is lit while the operation
in (2), (3) and (4) is being performed.
- 68 -
11. "METHOD 23 " BASELINE CORRECTION AND WAVELENGTH
CORRECTION
"Method 23 " corrects the baseline or wave l ength.
Press keys [Method ] [ 2] [3] [Enter] to call "Me thod 23".
The menu mode of "Me thod 23" in Fig. 11-1 is caused.
[ En ter ]
I :j:j: 23 1:. Correct i on • I :j:j: 23: Correct i on
. Base line ~-----------<. . (2) Off '---________ ----1 [Number] [Enter]
['\7] i [ 6 ] [ En ter]
l_:j:j:_2_3_: __ c_or_r_e_c_ti_o_n __ ~ . _________________ ·~I :j:j:2.3: 2. Wavelength <- .
[Numer al) [ Enter]
Correction
<Menu mod e> <Input wait mode>
Fig. 11-1 LCD display and key operation In
"Method 23".
The parameters in Fig. 11-1 mean:
1 . Baseline correction
2. Wave l ength correction
The key operation is g i ven below.
(1) "Baselin e " Baseline correction
~ Press the [Enter) key wh en a baseline is dis
p layed . The display changes to t he input wait
mode in Fig. 11-1. The cursor [~] or [~ ] changes
the display as fo llows.
(' (1) On " ~ "( 2) Off " ~ " (3) Measure"']
- 69 -
(1) to (3) mean:
(1) Base l ine correction i s made using the
baseline stored in memory.
(2 ) Baseline correction is not made .
(3) The baseline is measured . In this case,
"(1) On" is set afte r measureme nt.
~ Press the [Enter ] key when the desired item is
displayed.
NOTE: Se l ecting "3. Measure " displays the measure-
ment state o f the baseline i n real time, and
the menu mode is resumed at the end.
(2) " 2. Wave l ength " Wavelength correction
CAUTION : Since the wavelength has been corrected
before s hipment from the factory, do not
make this operat i on unless the wave l e ngth
is deviated. For wavelength correction,
prepare a sample with a known wavelength
and proceed as follows.
(2) Measure the known sample in "1-1ethod 4".
CD Set the wavelength to the known peak position
by pressing keys [Control] [ ~] o r [CONTROL] [~] .
CD Call "Method 23 " and select " 2 . Havelength" to
cause the wavelength input wait mode in Fig. 11-1.
ei) Enter t h e known peak wavelength (true value).
With the input the menu mode is resumed.
- 70 -
12. "METHOD 31" SETTING INPUT/OUTPUT DEVICES
This method controls the thermal plotter, p rinter,
quick flow sampler or other external input/output
dev ices.
Press keys [Method ] [3] [1] [Enter] to call "Method 31".
The menu mode of "Method 31" in Fig. 12-1 is caused.
[6] [9]
I :t+31: Plotter I [ Enter J
, I :t+1~ : Plotter
[Number] [Enter J • (1) Off 1. (l) Off
[\7J 1 [6]
I :t+31: Prin ter I [ En ter ]
, I :t+~~ : Printer i'lL
, [Number] [ Enter] • (1) Off 2. (1) Off
[\7] t [6]
I :t+31: Recorder I [ En ter ] , I :t+~~ : Recorder
, [Number] • (l) Off 3. (1) Off [ Enter]
[9] l [6]
I :t+31: QFS Control I [ Enter]
, I :t+~~ : QFS Control
[Number] • (1) Off 4. (1) Off
[ En ter ] [\7] ~ [6]
I :t+31: RS-232C I , [ En ter ]
> I :t+31 : RS-232C I 5. (1) Off I 5. I (l) Off
I [Number) [ Enter]
<Menu mode> <Input wait mode>
Fig. 12-1 LCD display and key
operation is "Method 31".
- 71 -
The parameters in the menu mode in Fig. 12-1 mean:
1. Setting thermal plotter output
2. Setting printer output
3. Setting recorder output
4. Controlling quick flow sampler
5. Controlling RS-232C interface
These parameters can be changed in the same manner
as ordinary measurement parameters (see Section 7).
Here, the parameter input range and input method are
briefly described.
(1) "plotter" Setting thermal plotter output
Input range:
Input method:
Initial value:
(1) Off; (2) On
In numbers
(1) Off
(2) "Printer" Setting printer output
Input range: (1) Off; (2) On
Input method: In numbers
Initial value: (1) Off
(3) "Recorder" Setting recorder output
Input range:
Input method:
Initial value:
(1) Off; (2) On
In numbers
(1) Off
(4) "QFS Control" Controlling quick flow sampler
Input range: (1) Off; (2) On
Input method: In numbers
- 7 2 -
Initial value: (1) Off
NOTE: If "(2) On" is selected,the spectrophotometer
starts measurement by a star t signal from the
quick flow sampler. Upon completion of
measurement, an end signal is issued to the
quick flow sampler.
CAUTION: Be sure to set the input r ange at "(l)Off"
when the quick flow sampler is not used.
Otherwise, normal measurement may be
impossible.
(5) "RS-232C IF" Control of RS-232C interface
Input range: (1) Off; (2) On; (3) Set
In numbers Input method:
Initial value: (1) Off
(1) Off: RS-232C interface communication channel
is closed.
(2) On: RS-232C interface communication channel
is open. In this state, communication
with external devices is possible through
the RS-232C interface. In this state,
keys on the 7800 are not valid.
(3) Set: Sele cted when changing the parameters of
the RS-232C interface. If this is selected,
the menu mode for parameter input for the
RS-232C interface shown in Fig. 12-2 will
be caused.
- 73 -
12-1 Setting Parameters for RS-232C Interface
Select " 5. RS - 232C " in Fig. 12-1 and then" (3) Set",
and the menu mode in Fig. 12-2 will be caused.
[6]
I I [ En ter ]
tJ:31: Set Speed 1. (3) 9600 baud '
'------------' (Number] [ Enter J ['7J t [6J
I \ +-
[ En ter J tJ:31: Set Word
· 2. (2) 8 bi t '--------------' (Number] [ Enter J
['7] ['7] f [6]
I I +-
[ En ter ] tJ:31: Set Pari ty
· 3. (1) Even '-------------' [ Nu mb e r] [
, I tJ:311.: Se t Speed I
. • (3) 9600 ba ud
I tJ:3
21.: Set Word
: • (2) 8 bi t
, I tJ:331.: Set Pari ty
- • (l) Even L-__ ~_ _ ___ ~
L ['7] $ [6]
\
tJ:31: Stop Bit \ [EnterJ '\tJ:341.: Stop Bit
· 4. (1) 1 bi t ... , ----------1- • (1) 1 bi t '--------------' [Number] [ Enter]
<Menu mode> . <Input wai t mode>
Fig. 12-2 LCD display when entering
parameters for RS-232C interface.
The parameters in the menu mode in Fig. 12-2 mean:
1. Transfer speed
2 . Word length
3. Parity
4. Stop bit
These parameters can be changed in the same manner as
ordinary measuring parameters (see Section 7). Here,
- 74 -
the parameter input range and input method are briefly
described. With all inputs being completed, press the
[Method] key to resume the display in Fig. 12-1.
(1) "Speed " Transfer speed
Input range: (1) 38400, (2) 19200, (3) 9600,
(4) 4800, (5) 2400, (6) 1200,
(7) 600, (8) 300, (9) 150 baud
Input method: In numbers
Initial value: (3)9600 bauds
(2) "Word Length"
Input range:
Input method:
(1) 7 bits, (2) 8 bits
In numbers
Initial value: (2) 8 bits
(3) "Parity" Parity
Input range: ( 1) Even ; (2) Odd; (3) Non
Input method: In numbers
Initial value: (1) Even
(4) "Stop bit" Stop bit
Input range: (1) 1 bit; (2) 2 bits
Input method: In numbers
Initial value: (1)1 bit
NOTE: Pressing the [Method] key on the display in
Fig. 12-2 resumes t h e display in Fig. 12-1.
- 75 -
13. "METHOD 32" POSITIONAL ADJUSTMENT OF THERMAL PLOTTER
HEAD
Press keys [Method] [3] [2] [Enter] to call · "Method 32".
The menu mode in "Method 32" in Fig. 13-1 is caused.
tJ: 32 1.
tJ: 32 1.
LR Adjust • L Adj ust
[6] 1 (\7)
LR Adjust • R Adj ust
Fig. 13-1 LCD display in "Method 32".
(1) Press the [Enter] key on the display in Fig. 13-1
when "1 . • L Adjust" is displayed. The "Measure"
lamp lights up, the thermal plotter head moves to
the extreme left, recording starts, and the "PEN
ADJ" button becomes valid. In this state, adjust
the "PEN ADJ" button so that the plotter head is
positioned on the ruled l ine on the extreme left in
Fig. 13-2.
After the adjustment , press the [Stop] key.
(2) To adjust the head position at the extreme right,
display "2. • R Adjust " and press the [Enter]
key. "PEN ADJ " button · becomes valid. Hake
adjustment in the same manner as (1).
- 76 -
~lJ .!};.¢ PEN ADJ © HEAD
Thermal head connector
t:9db9lL-___ _ --'----_
Fig. 13-2 Switch position.
Left-side button moves the head to left
Right-side button: moves the head to right
- 77 -
LED
lJoo
APPENDIX 1 REPLACEMENT AND POSITIONAL ADJUSTMENT OF LIGHT
SOURCE
The life expectancy of the light source is approximately
1,000 hours for both the deuterium (D 2 ) lamp and tungsten
iodine (WI) lamp. After prolonged use of the lamp,
increased noise will appear on the data because of reduced
light quantity .
(1) Replacement of lamp
<Cautions in replacing light source>
1) The lamp is heated to a high temperature whi le it is
lit. Replace the lamp more than ten minutes after
turning OFF the light source.
2) Before replacing the lamp, turn OFF the "POWER" switch
and disconnect the AC power cord from the outlet.
3) In replacing the lamp, never loosen any screws except
the one to be loosened.
4) Wear clean cloth gloves when handling the lamp.
5) Never touch the mirror
6) If the lamp is contaminated, wipe it with gauze or the
like wetted with ethyl alcohol and then wipe with
clean dry gauze.
[Rep lacement of tungsten iodine (WI) lamp]
1) Slide the outer lid of the light source to remove it
and then remove the inner lid.
- 1 -
Fig. 1
2) pullout the WI lamp from the lamp connector.
3) Insert a new WI lamp into the connector. (Fig. 2)
loves
Fig . 2 Mounting WI lamp.
- 2 -
[Replacement of deuterium (D 2 ) lamp]
1) Slid'e the outer lid of the light source to remove it
and then remove the inner lid. (Refer to Fig. 1 . )
2) Disconnect the D2 lamp from the connector.
3) Insert a new D2 lamp into the connector. (Fig. 3)
Fig. 3 Mounting D2 lamp.
(2) Positional ad j ustment o f lamp
If the beam from the light source is not accurate l y
incident on the entrance slit, problems will occur such
as insufficient light quantity, curved baseline and
variations of the measurement values at the time of
changing over the light source. The light source
condenser mirror and light source need adjustment when
the light source is replaced.
I WARNING I (1) Never touch a lit lamp with naked hand.
- 3 -
(2) During adjustment, wear ordinary eyeglasses or
sunglasses to protect your eyes from
ultraviolet rays.
(3) Never touch the lead wire by hand or with a
screwdriver. Contact with the lead wire will
cause an electric shock.
CAUTION: Never loosen any screws except the one to be
loosened in adjustment. ,
[Angular adjustment of light source mirror with respect to
tungsten iodine (WI) lamp]
(1) Set the controls on the instrument in the following
position.
"POWER" switch
"Method (#)"
"Photometric Mode (Photo Mode)
"Go to WL"
ON
1
SB
: 500 nm
(2) Remove the rear panel of the light source unit.
(3) Press the [Display List] key. (With the LCD type)
(4) Slightly loosen the lock screw on the WI lamp side by
turning it counterclockwise with an Allen wrench, search
for a position where the data value (displayed on CRT
or LCD) becomes maximum by turning the stopper screw on
the WI lamp side, and tighten the lock screw. (Fig. 4)
- 4 -
WI lamp s ide D2 l amp s ide
St opper scr ew __ ~~~~~~~~~ Lock scr ew-- · Stopp er screw
<-Jr--~--' ____
Rear panel of light source unit
Fig. 4 Rear pane l of light source un i t .
Lock scr ew
(5 ) Insta ll the rear panel and the inner and outer l ids o f
the l ight source un i t i n t he or i g i na l position.
This comp l etes the ad jus t ment of the WI lamp.
[Angu l ar ad jus t ment of light source condenser mirror with
respect to D2 l amp ]
(1) Set the controls on the i nstrument i n t he f o llowing
pos i tion .
" POWER " switch ON
"Method (#)" 1
5 -
"Photometric Mode (Photo Mode)
"Go to WL"
SB (HT 400 V)
: 300 nm
(2) Remove the rear pane l of the light source unit.
(3) Press the [Display List] key. (With the LCD type)
(4) Slightly loosen the lock screw on the D2 lamp side by
turning it counterclockwise with an Allen wrench ,
search for a position where the data value (displayed
on CRT or LCD) becomes maximum by turning the stopper
screw on the D2 lamp side, and tighten the lock screw.
(Refer t o Fig. 4. )
(5) Install the rear panel and inner and outer lids of the
light source unit in the origina l position.
This completes the adjustment of the D2 lamp.
- 6 -
APPENDIX 2 ERROR MESSAGES
Table 1 shows the error messages and their meanings.
Parentheses ( are for the LCD type.
Table 1 Error Messages and Their Meanings.
Error message
Lamp Control Error!
(L01)
WL Range?
(E22)
Input Error
(E)
WL Scale? WL Range?
(E20 )
Upper?
(E23 )
Lower?
Meaning
Displayed if the l amp does not come
on when the l amp lighting operation
is performed in "Method 21 " or
"Method 22".
Disp l ayed if attempt is made to
make measurement by reversing the
setting of the start wavelength and
the end wavelength.
Displayed if a va lue out the input
range or a value inhibited to be
entered is entered.
Disp l ayed if attempt is made to make
measurement by setting a wavelength
scale or wavelength range out of the
allowable range. (Refer t6 Table 7-
2 in the 7800 manua l.)
Displayed if attempt is made to make
measurement by reversing the setting
- 7 -
Error message Meaning
of the "Upper Limit" and the "Lower
Limit".
WL Scale? Scan Speed? Displayed if attempt is made to make
(E2l)
SOl
L99
WOO
measurement by setting a wavelength
scale or scan speed out of the
allowable range. (Refer to Table 7-
3 in the 7800 manual.)
Displayed if the wavelength is not
scanned.
Displayed if the lamp cannot be set
in the status of the parameter in
the file when the parameter file is
called up.
Displayed if the wavelength cannot
be initialized in Method 22.
- 8 -
~- !
73
APPEND I X 2
MODEL ROU-398
RECORDER OUTPUT UNIT
INSTRUCTION MANUAL
JAPAN SPECTRO SCOPIC CO., LTD.
296 7-5 , I SHIKAWA- CHO, HACHIOJI CI TY
TOKYO , JAPAN
June 1987
1. UNPACKING & INSTALLATION
This unit has been installed in the Model 7800 before
shipment from the factory. Prior to operation, make
sure that it is installed in position. (check that
output terminal shown in Fig. 1-1 is provided on the
year panel of the 7800.)
SAMPLER IF
RECORDER
+ ©©
Fig. 1-1 Recorder output terminal.
2. SPECIFICATIONS
Output Power The upper limit and lower limit values
of the photometric values set by the
7800 are output from -1 to zero volt.
(Example) When the l ower limit value is 0.5 Abs
and the upper limit value is 1.5 Abs,
the output voltage is -0 .2 volt if the
data obtained is 0.7 Abs.
Output speed Output speed in memory (Methods 2 and 4)
- 1 -
Approx. 60 msec per piece of data
NOTE: This unit has no function to control start/stop of
the chart paper or to lift and lower the pen.
Stcmdard Accessories
One piece of recorder output cable
P/N5590-0294
3. GENERAL
Measurement values obtained by the spectrophotometer
can be output as analog signals by using this unit.
This function is valid in Methods 2, 4 and 5.
NOTE: Method 2: Measures data with time using memory
Method 4: Measures spectrum data using memory
Method 5: Measures data with time in real time
4. OPERATING PROCEDURE
4-1 Setting Output Device
The output device is set in "Method 31." Set each
device in the following position:
l. Plotter (1) Off
2 . Printer Either position of (1) Off! (2) On
3 . Recorder (2 ) On
4. QFS Either position of (1 ) Off/ (2) On
5. RS-232C Either position of (1) Off/(2) On
NOTE: If the plotter is set to (2 ) On " the signal will
be output not to recorder but to the plotter.
Then set "Print Out" (printer output) in the following
- 2 -
position in each method.
Method 2:
8. Print Out
Me thod 4: .
Either position of (1) Seq/(2) Overlay
11. Print Out: Either position of (1) Seq/(2) Overlay
Method 5:
9. Print Out: (1) On
4-2 Adjusting Zero position and Full Scale
(1) Set the following parameters as follows in Method 5.
Photometric Mode
Lower Limit
Upper Limit
(l) %T
lO %T
20%T
(2) Shut off the sample beam, make sure the %T indication
is lO%T or less and press the "Measure" key to adjust
the zero position of the recorder.
(3) Release the sample beam, make sure that the %T
indication is 20 %T or more, and adjust the full
scale (lVoutput) position . .
4-3 Measurement in Method 2
First, set parameters in Method 2 and press the [Measure]
key to store data with time into memory.
Then output the stored data to the recorder by pressing
keys [Memory] [n] [Measure ].
4-4 Measurement in Method 4
First, set parameters in Method 4 and press the [Mea s ure]
- 3 -
key to store spectrum data into memory.
Then output the stored data to the recorder by pressing
keys (Memory] (n] (Measure].
~. .. _.----.. _ .
....:.::-
':::j=.:" . • .... ... - = - = =-=-=t::.::t. .. -L :.:~_ :. - . _ ~; .: . :' --=-£..:::
, -
Wavelength 700 to 300 Range
Wavelength 10 Scale
Chart 50 Speed
Recorder lV Full Scale
Fig. 4-1 Output example of spectrum data
of holumium g lass .
4-5 Measurement in Method 5
nm/cm
nm/min
Set parameters in Method 5 and press the (Measure ] key,
and the data with time will be output to the recorder
in real time.
- 4 -
nm
APPENDIX 3
LIST OF DRAW I NGS FOR 7800
Drawing No Descript ion
6590- 500BA Electric wiring
6590- 501CA Power supply(2 sheets)
6590- 502CA Amp. & AID
6590- 503CA Main I/F( 2 sheets)
6590- 504CA Panel I/F( 2 sheets)
6590- 505CA Photo sense scan
6541-580CB L main board(4 sheets)
6541 - 574CB 60 PROM board
"
17
7-
Jl5
of!;
RE(
OUT
IlHP a. AID
roDC/Z84 liZ 2S0
FIt TfR
SCANtl'N. HOTOR -()]8
I'1A1N 1 IF
CA -
PHOTO
SEIo/SE S CItN
Z PIO' 750' __ -,
P~NEL i l F
H06?8180R
HAIN BOARD
,,,, " 'f 'll ' .. , sr--2~~ I I iK8
fCH>Z
1 ~ J I , I 35" pS4J -- l I I J _'_:J L _ __ _
SDtI'.l ..f7-tI()3 '-"0 r-l 12>
()~ LAt1P I 4 1524-0/1 ,
'7
716
613 2SO
717 ~ o~~.mf'OWfRSUPPLY C' I )3:>; 031
'5;1 Rut. ,..) ~,
>! o.}~'''' ,
,-,-}s PIO! e SllO.. o~ }JI05 0'
I l.Ir' fVfII 4-I
Ie (JjRD
DpTIIIN J
If' ,'"
1
4
~'Io'''' 5 L _ _ ..J
L-...J no.L---'j/o. .. ......... a.wL 8" ,... ...871 h ... + 30 ~. ,mt t-~, ®
.... _C:.I.100
"86· 'r . 10· "
o E
BlII8 0l~'(IN
6S'lO-S008A a!!I.4 ___ II
F
N
JAPAN SPECTROSCOPIC I;O .. lTO
JIS A3 (297X 420) A 1 B 1 E I c 1 0 I F
=:;==-~-:- : ElllI:5.t7'tI~IH*it~;f:t G
t
2
~
I
41
5
o R?I I b. sA S/Jj '" ~ ., "."., '" -, '0 '" "'" ~ N .0.0
,,.,~ , , ~ , ~ "" ... <- " •
~/OJ
FH/ Ff
• ~ "" >0" Em ~ , "
TD f);I LAt1'p
;; l,., '" --n _~ " _ " ,., . ~ ,.. --,-, - .--; " ,- "., ..2 + r ~ S , '_ "" " ~ f-.C:'-n" ~~. :' ,. ," '" , oZM ICOk, C.3Lt- - cs
.-' " 1:"
. ~~; It--~~-----t--~-C~--'--I R~ " 'W _ ,"
,. L--'---.:::
R30 t k: i)11 ~~~~~==~~~~~~~~~~~~~~~~~~~~~~~,~,~""~~~ bll D <-
IIC ,00 v
:rIO;
AlS" V <E
","", D.I - " , p,,-,,~- '" ;1H0-2'fv:.~"t--r=:-l L___ -"-=~_ I, 4S V , <c, '" ",. w, ", '"
.oo r[J7)Df /qa",u
, ------------,. '. .. , }.. lot ~
AC
(q.
1
I)f.J 1 . .3 V
,W "E RJJ ® @ (0Of/. ,0 v ZK
JIOI
I7V f.::..
'.... '''',--, H _ , " H~'~' 'jl"" ,,' " :
,,- ~ ( I", i h :! I' '"", ~q,vDZ I. " .. , " ' ,-, :;: ",',
EJI" ?l r.:;-:t:l c/,l. " f'l ~ CI' , H"V...l!:.
41~.o-r ,,. OV @
, I?V (j b t bd ;sv.L '" I T<1¥ 1 "4 I co CIS IN
PFc2 t1 17'. IC.3
" , , ,I If\ " , &.
2Sv 00,
, I
t D(' ~-15V , _ ......
/s(538 T [i/:;:5;~' ;,\.. (i' 0J ' .. ,2_
:r lOll
EI31'
1 !.'7i'~ I 1'''19, 7j?T&. 1tJ.\\,~L'. (1"·1IiLJ:r i'k = I 1 I E I = 1"""" m "'"' JO I "'''5 ~~".,,~, , 0" •• , 5 ,30 ' U beA.t 30 POiYE,R SUf?LY
~~n.- -1.""9 c-" ,- ~ 7)@itd"~ Iii" "" ,'" ~4 fO(If-*?~'9f'7.12 . 18·1 &.1(}':LAHI',6\· ·il!"~L..t::2.-,):tt' .... s I - Ir.:r?j:=! I
. . 'H~ ').-1.'=. ~ - --~ o.u_ t..... CH(CJ<lO 0"_ 0
00' U - A 11i i~, ;,.s- 1 () - .s 0 I C I)
"" .. , """"I ,,~" I.~ I """". ~ ... "'"'" ""'~ .""".1 IT Ai I "'''' ... ~,"'""," Yz 2~" .0000000tCO'00I<
8 1·1 DUE
~m ~I'j« iU!I ?"J .... t-~tljlf-·:;1" .... li iJffl ::a'lI - ,0. I ' ", , , , , ' , ' , ' , 1'~ I :;:II!! IZ:J· ""'lit\. (C~nEL
1
~
2 I--
3
I--
4
I--
5
t& JAPAN SPECTROSCOPIC CO .. LTD.
liS A3 1191)( H OI A~ B~ c~ D~ E~ E ~Pltft:l't::Z:III*it~Ht "
1"
2
7-
, ... -3
:r ~.
5
J / DZ A+ .,. 5'"
0 .... (:24
O( .ljv , ,
"(>
n.
Fl
4A
r - - -, Jill
: '2 ~ EI:JP !CURREN' LIMIT 13A '-I rSV . L - _ . - J r - - T,
RJ6 I 2W' a./A S'':- TI2 - !iO .2 I
3 1
2W 'I(
.. CUJ luI ;SOl > ~ : i;:"", $8540 S I .
Lf'Ic sw Pf/II ~ Sf/. flfl " I
J 10,/
EI ~p
A c '0 V
19
~ 'C " E 7 1 l _ _ J
DC -
pA 71S4() ., foUl) r -- l
r----------------~====!/I -'11
R47 I ,-__ ';'3'
~5 ON' '" .~ IN on
7 4- • tel4- ••• r/tlZ ~ ... ."
, ~" 2.J.)c
~-u-J 6,2'" ,,u.l. RU
~ • CZ!J CDr z~
cu "'k
R" ~~ .. R7.J cA-... <T'
." ,.'" {# • .,.
470 '/- : pt'1S L __ j
Sri
f1,3 !3A
'<5 J I(J/ ~w 02.
B OSil
~ . , I (41 f t ~"' I # I
16V , .. 47"'.1'4 510
9
kfYL-01. 7fT
DC+
DC
pc~
N" I Lf?: 2~O ~ :
t-i>t' '-- Nt,
". r--' I Jr I'~ I if ~ t>:t f/t.N lOO,j
3/" I I I I 4" , J z~ L. _ ...J 112' '1ID, +--__ h~--J
2SD
... ~w UJl
2
I. H VOLTMEADJ]
L '" ~:T i ....!F-r a.tlJ. Q z.sA/:J.2' __
£2 '2 -5"
...........-eJI 1 . J... . - 1
DZ! ~ Ii-J ~ ~r'I (A\ W.LAHP-DZI I!rf ,4 ;Zjlf ~I , , "H1 I N
N_ Z I~ ~~
<!~ f' 4-12 IIV .. -~
.reS 0,5 1(1() ;.t/l 78 S 40
<" of' IrfIN I'" ' A/V IN "IT
1 4 .... ~='--t----:t O¥
IO~ I.1'S
r. 2,1(. ;!'; S/f( ou Jlltl'
1 IT .. ... r--' L-{,,~6:
g.11 L. __ ~ Jl'.111t' 3106
EX lOp
r --~w;;W .... r--... I 2k C5"DY 1"6
:11,,6 L~~ Z.Z 21< .
I!IlOf UUIi!OIj Iw.INfP vDUAfftYU;1 ri.L4HPt-- W.t.,411P-1c6
DC /I v Ala 8N OoU( ."8- (~UJ8 Of.5CllII'1QOj
71J cpu
JIIO
EJ4P
TO HAIN I/p.
:T/05
TO HIRF'''' EyC/tAV9E.
;rIO 4
TO HIIOf'I<tI t..AH~
19 • .db. - D -" /ib· , • I~ . U beA t 19 A!\ - c - 30 pOWER SU?fl Y
~" t ICCO IO . ~ ~",-I ---I" 5690- • . {, S'lo_So I c t1 " . ~ - · - ~ eiWd"C n*
It!!... 8M "It .1!1e. .'" Jllil I}." "1'):"" •• "- ':tl'!.oI(;a1ll = It -lUt.Qorc£lotIOI jQ4,!t ~ ....... ' tL ''''l .... 1II.I.l.."f ~ 1( IS_~ .~ _1l0~._'" 1ol-, "'lCll r
~o fr~~ ,lIft'X.) au •• ~ 0..., ~-!II ,. %.
>\-(D'DI · ' A B c ' o I E F ' G
1
I-
2 I-
3
I-
4
I-
5
-$- ~
""-""oo '" 3
-$-4
5
~
JIS Al rz,J 7X . 20)
.... ~c,,'01)01
"*£010101
PH 2
" .It ~n
A I
.-"" I""· Sy.... (C~I.u.
A
B I CJ DJ
Ie 16
Hell 04
I I I ~I 5690 • ... "1'J;, .... /i- ~) 1" ;,/(
<'(11""" Antel l ~~-" 1"-
~ 001._
/" :~m[ffu! 'ff B C D
c! F Elllln:rt:L~1,;d~=>t-! G ,
.,. TL Iql C Z.3#(
~ lGll 'l ~ ~/' I c.' R2 1 Cf> ... 17. 7" I I
_---s.. 16
B" ~" ,- ..... COI LD
E
~II -, "* J.; •• Y':J
C2 reS/TeF r--, C f tH/6L ( 10 I
84 ji"T5O' < 9 I
"'5 Ap CL~ ( 7 : I( 8 I
I
ApEOC. <s: , I
IONd. CLOCK I( I I
cS eLlr , I
~61 I
Cf.l-1' eft I I Sy ., , (/3 '''''1
&.3V. I
"'! ! "''''9' I ~1J1 <:.<p L_J
!!Illti 1)(_""0.
730 1
14r FLA T CA IJLE
AHP ct 11/0
bSl0_S0.2CI! [ZI51 1t '!MO:"""':" I , •• , • X
F ~
~
2
I-
~
4 I-
5
<4-
1
, 2
-$-
/L Z 2OilO
"--3
-$-4
5
.JIo'~N ;:ore:.\". , tll ... .;) .... V,. ......... V., ~I .....
JIS Al !<I'l 7X 4lOl A I B I C I D I E I F ElJI(7.t:l'tJ:~l"':P:~iFt ~
10--'5D) +SV... LSIII-Ill _ _ _ _ "
Ilf > BREg, r 8' l o j P' RD III P8~ T¥I~
, 0
r-l /C ] PDt< 6
:J 201
rE!1t! _C:.,01 IS-lO ' OI-l
IS) 8 8"< leI I I In P-'iill t1 Ie) f LHtJ0628 IJJ ·AIP Jeo.2 .2
2A) 7iHT N'£!(I/,/2 1 IFJ ·A I U J .} 28) I'ilTl tP ZJ eLI<" TO;" ~(AA/ I I ,F-J CST ll .Q ,.
~<:) mg reB ,,4t.HN. 2" f>f' 1~5 I I IFJ csr u S S
31f > 7llT'7 L S 14-4/ ~, cUe I SCAN I I ~ .3__ • • 38) ~ ,2 IH I I ~,,c:s .. .. ~ 7 7
/CJ--'-L<S ,<3 '2( 1t
/CJ · J ( 7
"3 ·-<10 "j • 5" (. 9 I'" • '(/2 ,,, • ? < II
3C> !EM t::P~ IE5 , IFl ~ J 6 ~'F5 IC3 411) B'!lif IDJ I~+, .. cUt Z/ 5 I /C.3 0' pc" ~'" R,EOe. /FJ
~8) 7JC He7S .. c I I JJ I I 4C) Ii .. 6 1 ~ . I/O),I TCs/TCF/~J 2
SA) ljIH tI., COd ' I I i ~B) 7iIC I" 15 ..... IU I 9 ~tH/;r-, ..
sc) 'WiJ1T Ii! HI I I 6") N , l'll~::1---. •• ,~> 'liU /u TDH J _ I I
6C> 7liJhT IU --. I If_ leI 12 ,.3~ '.1 IFf 7.1> Q! IU ' ~ I . .,. : ,Ir '11
I <4-I I I 76) PI III 18.3 A " ~I Cl' 162 I I 111.1 182
'Ie) D% " .7202 I 7 i'ToZ" ,.., __ I gA) 1/1 /C5 I~' L __ 1 I I/ P" D < 14
69) H A B lP Iftl JC4- It 6 l EI p ·W! < 13 gc) IS '., ,." 11'''.1 1C8 81 55 I Ef p·d' (/6
911) R' ~ He II .. Z 'fl IE! /. 1.11.'" l EI f'Al (.15 98) 07 ,u f ,., IF-f. " .. z % .f ·EOe. IF2 lEI , ,sf (/6
9C).... • [(/2 161 IH - J c/' m CSl ( 17 lOA) 8 I $ AS. S 1t,1 lEt 11 pCf T fOl. IeB IF-l C;S3 <20 /OS)"2 ~ / D ",. l '., l£l I~ .. S .,Jr L..~ ,.N (Flo S ' ltp (/9
109 d.5 ,., zn' ", IU H ·U, <22 II Ii) d:f __ lit 10 -1 211. ~/QJ liZ RESer kZI
1/8) 1 5 I(f N4 __ ••• ., K2l,,qI /Ie) ", au IC5 I 212~.D - /Qj ~,2'1
tl~) "7 2 • ~ I
/2") . AI • ~"21 ,ole> If? __ • Ie 10 3 /.JA) "It! [0 " ,.,. D~ 5 HC.nN I I
138) 811 ~ I Xl l ~, $CAN IJ L_J
7# ~"~l £/1'
I.J C) 4" W '1 (~S u 1 If I :?C>z /I "ScAN 2Sf . zDS 1.-. If> AI" Ck ICf 1.2 5' " 1£1,1£2 :r 703
H~ AH- S z60S 1$ 2E$' lIa Wi ,e" OUT F up RAT (ABLE.
I<l.e) AIS .. z " u OZq 2Cl IU " ", !: Zr IS") AI6 J I. IFJ /U' lal lC s cucJ( IE' ( II
1$8) AI? .. 6 ~ IC" II. D ID$ L ,,2 6d~ --ISC) 1'1' 101 IC$ ICY frND
6/) Alt 7[)-IS/)'>------l J2lJ1
19 .IK - • - 8M GAll "lit. ___ loOt ~IBt. «5CIIIPTOI
19 Ii!-, - D -19 &. - c - /'fAIN [IF ,g" . r· ~ . U be~t 30 19 L!!'. - • - ~ ..
•• 5690-
1"' 1"· RIll. U lIfi. ~u 7 '):" .-•• ,t_ ~/ ~:"/( ~" .. - A
iI/II ~"'" JAs.ca OUWOI
_ ~1i. :~ n",. 'JT
n~ .- ItU CM(Qt(O
._, ~, n~
,6 .S.9,O,- ,5,o ,J,C,A , , f no... _~_. a Yz lCU'lll. V;/I""- Afft(1( ..... - --rU)~ ......... KI'U.I. ""'((1[0
A B C D E F ' G
1
~
2
I-
3
~
4
~
5
1
!1-2
"''''' 3
11-
5
""
JIS 4 3 1291X ~ 20) A B c
r--l 1 /0 N#FF Q. Dr /'I <ill 18)
JZ#4 : 9 I ~ I i AT r • z
EIIDf'l ? I He s - .~ I 6 > IV f1(JA{/ .HU $'1~f ' I-
:s>lhaow .111. 1(/3 5 1 ,> MWP IF.. :lFJ ___ 'i Q, • 0' L
I 3 ): 11 DP IF4- J:fJ rxlT I 1/.2>J l L __
. 2. T , ~ .. ru
, s.t/ruT
, I ::~'l . Jlo6 : 6> ~ , I I :-"J'I
I El", S > c·.OJ I II I :.,::t' _1_-
l4):r::w I. I J) off I 7> \/.2>---L __
r--, J .2.06 I I >-------,
Er +P: z >------; i • If< L __ ~ • I r--, I I
:~ J207 I
EUP: .ii,' I I I I ~ I I
S I I I
t:> L.. __ .J
IJr '!'ET 2£1
IS
2
,.
7 6 •
S I /~
~
-'--L-t. •
c 1,4
e9 RI
". '~I; ':"K i . _
~ SCAlI " 5 I I
ICI5
•
•
I",
•
•
o
l,oJ .-I • I ·
•
• h
......... . _.. ... . E F Sllt~ftII!iI.*:O(f<"t G
r-- ,
n; ,.-lL
. , I
"iT ~. 1 ,~ our " I
< I JZo~
) I
FLTibe 2
Ie IB "L"'" >
1:, rm. • -{l>o-
M V .e,:---rr
1'21
15
," UJ
00
I I
I £I6P
• I I
S I I , L __ -I
lI3 ~ r--' II j iiT{;iI c:: 5 I
.182 mowr <~! < J,..
.a. 1.1 Irs OUT I ;j' I <2: : E1SP ,--< I I
.,j,. L __ J
---OPTION -l ~'~e~: REC OUT
Id R2 Rr-I ,.21{ n 500 "ftv I I
PI .)~ ~~, ,00 I~ Ir.) '1"I~:lr . - - PA.O(IT
... \' I 6 ,2k
II I .7 J;1./0
EI2f
6 II< r---, > • N. 1::2 I I I I I I I
~ I I I.. __ ..J
~-I-; ;r Z'I 1J1~l;-~o'-~---111 ~ z j EIJf
i CJ2 '<3 I +IO~ LuJ ~
MAiN I/F I" 1 t 1 ": : : - • - B"~" " . ~ :1 1 I ~I -I""·~·l.' .tts ow.
U be4t 30
II ~ - • - ~titJ
alia oue".,OI
1---." 5690- • I "I!!1t:I 8ft &a~ If!~. 11~ jlft" ~U "I'):'" .. a.If- ~/;-:"'1C aM = " -I ._e41"01 Dolr, s. ..... rC ~['«L .:;(. Ul'fl"'Tt ISMIt -- _ltD Il:\I0III0...... w.-. anteu o
,s·[ O'o. ·. A B c o
"II
jil '1';.'
n. \ .. " ,_ CMtOO; to ." -, -f'~ {,5?o-.J"" tJ 3CIl
I ,Z/ ~ •• 4 'owa~-:" / 2
E F G
11
2
3
4
5
'-.)
J APAN SPf.CTHOS(.OI'LC t l J . .l.lU.
JIS AJ ( 297X~20 ) A~ a I C I D I E I F E1*:57;)'t::r:~l;;ot:~iii G
-$-~
<:;'''''''3'
-$-
~ -.., ~ - - 11Q.! - - - - - - -, Jil.!L' ,0 'k S -1 __ _ .)~."......... 1~
~S6 m, i' UIJ t> ! , __ __ b 0_"' _ ___ , : - I 17 ./ 2 <E---
~ I , • I ,p~~ H"" .~ TD -.& ./3<0--f Z 2 ·z 1'-.,2 DISPLAY V .. , Zl II<. ~.J .. 62iJ1J!.5..... ../1(-E-----
J , ·3 I S'd (LCD) .". Ifl' 14 /S<o--~,. fI • 4 I ,... 111632 l If S ~.J3 ./ 6 <E--~ 5 SH. ~ I j~ .,.5 I .It' 4 ---.l 4 12 /7~ ~ 6 ,'" It 6 I " ,,6 ~ ~ : If '.1... Ie II ,/ 8' ~ ~ I". I, 1 '1" ~. "...J vr /C<E--
> BC":ET IC' .,"1 ~ _ ~ _ =~ ~/"~ t4~ Qf ...£l...M.L J 1'" 9.1 I L - .J.J40$! PRINTER I 2/ PD~ 1#_ If. ,_ E "1 'cl'J$IrR ,1111110 YU5A
" Ps'> PC, HEAD cAl II( ,,,lI-Y r -..., 15 • I "l- "I , I" os "z I~ ~ , " ,.5' uL " ". '.-'~t1t I g , Z ISJ-, J2 2 2" IfJI/II ,It'' *~:Z LI IOIJ'"1l:iv IUS J I I I ' 17 II' 3 IF3- ,1 / ~ ,j' 1'.f_91/ U~ 2'10 QS : : I1TP201
I 10 ' <' ''' -cc " • Ie I ~'R" "'. I ." J. ... 0 I I -~'Z8 "" -(' Ip/'- 1 .5" PC 4 I~ T6 10k I RII'1e L- '~~/S~ """ ,'6 I :
I ? N' IF+- l' 6 S 2 'i1iiiE sw 1 ~ ct.! _ 1 ,,"k ',,",, ' ", 1 !...2tl' H-I J,Z. '" "I IFf- 2'1 6 (;.3 I .Q2. .......... 10k Tn .'t1/~ »1 RI3 1 y--' 2~O I I
" Po PO 50 7 oZ S5 10' ~'C"'5..., 1 <~' ['"' 'I >Ok J. R* .• ' ''l. ~"-VR .:-- ' I/If -It R» 7 t:1 . r t;II: .... ,s/58'1 .3 <E------Q T I 1.3 Po;;;;; p.Wlf "- l1li' ik<:" .. ~ J .; .s <i--? R
6 p,At, 1,,=-"5,- .. ..... ,1>5 ."£T _ .::.':. 3L r-<"~TR I '5 PO" , • T • AI CS _?7 ;:" Ii W ,J,. L --Jr4<>4:'-' ---' I ' I II P,A'" ,IT I" n sp
CS7 1I~'F5 'i.'m,,, ,A "",.6 ret; 1/8 . IF" r - - - - -14- - JI - - - - - - - - --, I?~~ I ,. ... or. " • PA.· I/<D. 1\ 1\ Aa>3". • ~ PD 120~ ""<t ~ I ", , ~ 2<"' YfjD Vee 119>.1o..Jj Q olL .. L _ j I JA'" ~ 20 1 2 z IJ < 2 ,eJID>2? !.2 .. IfC p" ,.
>.4' •• ., • .3' 2, <l EXT HENO/?Y /JIJIIRD AI/>l1- .iII.5?f~' >-.1. ...... l!. . !u ll<_ £P-15' A,i>Z ,S. .~
" loot, .. ~ 23 5 5 11 1.3< 5 AJj~Z.' ...Lj A ,.~ .lAS< ,. ~ ~, , JI x< ~ ~ ~ -e. ... N .." ~ .!l '<I t... ~ 1114>""" t3 ~ 11 f ' ,
... .? "? ? 17 lS< 1 V V \) V \;,i~, ~ V' ~ V V f!IO>JS • ' .. ,,' •
II .)oj ~ Ie 1, " L - - - ~ ~ ~ ().. to t... '() CtI 't- '1 ~ - - - - - _..J I "
'. ,AZ , ,u Z
I " '- IAl • -/~Z L/~l • 7 I"
I~ •
;]"401
,MID ~ I , liS . r _..1
II I "I , I" en RI7 IHI? /0/(
RV' CI 501( R6
O.I,/.e "n. SOc
1
I-
2
I-
~
II 3 1 .! 3 117 ~ ~ s , II ~~ f IIIlt ,,",s ;1'.i ,. A: , Ie 5
III e'I 5 I'C#. I~ 11'4 cut .. ", c~ J II i' , sLa )Ck~Y',.U L~ 7 JlT "
I I I z? I /I l<..uy { lA£
I I 5 .. ? M "0»,.. R' Li)l ~~, LDZ tELill
4 J.. tel ....f.:d.L
16Z p.W!t
, .. .fAt.
J.. • .. I, M,< ~., .. " '1- ,. 'r--'~~ Ie 3
'1.511311 R.' ". '11
II ,. RRSEr l~ REH T ,A:2. . ~l. ,,> ~8 TOk rfr
~ i4 "', !~ __ _ ~_ ~I< <r_1' ~. LrNoJP
II I • , E tN ~ tA. ,LE '-CII'SfR ,.,' r" 'CI'IS"
51 I" "" 8z55 T _ I .,,~ ,I " ,:~~ .. " <>3 15
20" •• oo,n::u_
.IS"(010'·'
" " " e M ~n
... "" In". SY __ tcurtl.
A
""" ...... OlI,. ........ " .... _ .... vo · ,I,.. .... ... llU
JIS "3 (291X4Z0) A B c o E F S*~:l'I::z:.'*:>1:~ft G
itA I
tl ,.,
I II ,-·1--, 1":';:1.-.., ,.,. -1- .... I' ......... 1-..... r1=-_ 11 -/U-3 ,- --,-- =- r--=1 __ r---=-::l __
ICS );-Kfyt '"'"I" I<~ • , " , ,.~ • 2 "c •
'. D °1Tl 11! t __ .j I. t ... _::Y. I t_ .. j I I'L5'I~u~ 12 [7--4 ,j,. Ie 7
RIO ,~
Z2000
3J ~A" 13 ," ~ Sl!lt-/t).f - :7
," ,., ~
t /"
:r J JI'
"' ~ 1*' --=- • II'
#
14
s: 5
I 19. - f - af:t 0Af1 ."8 ""'"" I!UIS DUClIPloClII •
I " - D - 19'1"1"" Ube.Lt" 30 "'I/NEt.. .1'''' Ii ... C _ T. /r
I ,19. - 8 - ~ ttl. l!!. !!! !!i~" 2.." I I '" 5690-2243.' 1<. ' ~ .t 6S9 0 _S0SLCI1 I!~ Bf:t &Z'! 1:!1i!. :,all Aft •• u ,.');... .. I./t- ~JT;.../( iI" = II - 4 l'" I , , , , , , l~cnOi I~I( ~ ....... ' C: lIY{L ·" ~""-&JTfr." 1S!.Ul1II ......... 1(0_110........ stNAl...lHfC:U fI 'rf . ~ alII',! I;IWQ ... __ .%. ~')
JAPAN SPECTROSCOPIC CO .. m>. JIS A4 1210X297) A I B I B~~;'tIJ!jH*it~it C In!!.., Sf.! Ic~ lI:9!lC. >Mill ~iT. ~111 7't) :..-t-:§:tlil "<-':rr'/I' i§1Il MOOIFICATIOH OA'" SYMBOL E C. LE.VEL SERIALAFF"ECTED IS5:UEA "'" ~IPHEO BOARO NUM8(R Sf RIAL AFFECTED
Ifill! 5690 A
19 . .&. - B -19 .& - c -19 Al\. - 0 -19 .& - E -
1 1 P so/ l? 6 S ~ 3 i! / J -E 17 P ~ 'I' 1\' \ 'I' 'I' ' . II'
f-
_ ~ 31 ~ $ ~""'~$">j, ~~"~~I~Q
---- <t Cil l-bl ~ "" I ~ I::l ,--- -l ~
1 Vee ".,If
" ? " 1<'1
Cl I I 200 .~ I -- - -lPCf r-~ 6.3VI , 2
I 1 _ ~ ,4P-fS04 J 2
-$- L_ - - -:3 _J 100)'1 I-z
I 6 RZ I I 2.7k.
1 I R3
I 3~~ _4 -l pe2 1 I r-~ 1 ~ Ir 1 Iii'-I S04-
I r-Z2000
1
L _ _____ J
" :2 3
"" 3 '::.I ~ I
R4 2.'1 k. I l-
I R~ I 1
I 3~-1:-lPC3 I r-1 _ IljP-IS04 , r- I -$- I L _____ ..J
Z ~ 'jL
I R6 ~ 2.'11< I 4
~ I 1 I-R7
I I 200 4 PC4 1 r-.,---- -i~'~04
I 1 3 L ---- _..J
2 ;3
~ I 118 Z. 'II(
, L_ ,
5 - -- - - ~D~.....I 5
8'f:t DATE tltt.:8 NAME 1Elt3.:8 DESCRIPTION
19 i(, • 7 . 1 . U beAt 30 PHOTO SENSE. SCAN
[=~ fl;J;)1 lill! IUt ~111 ORA""
,_ CHECKED .4.PPROVEO
6590-5 0 5CA l~
,,1:: I
\"'~ I I I I 1 I I I I I I 'X Ill1 i!ii. ~ cwo """"'"
-.S c.OIO I 2 A I B I c 9
'" ., ''''''' '' A I tl I C IDE F 8*?i:iitii'iH*~{~~i G i
j-a 'L I 2 i t..,rf~IL . (K26'18 U+3 I -~-~-, -'- nl ~,<:llII ~ ~ HIPE\! CH' PAl'?
( 8 • I> If I if' 1 rh c~~- rh C2'1 1111 CAl. IS '" I\~ 1'1 (
2 16 .. flC , ~ 105 CAIS S ~~p 5 9I.j
H WA IT "I I--11lLiAiT PI' CAli I~l ~ . ,*D-) I 11 jIl) tl2 Q ~ 8 lC.18 9 !*r~
IS1~8 A IP'> 2. TO. \ All 14
' t1I' - IbS lS I :TrAP ~._ I.. I, "'r~ lE I
13 . ~
CI!1I!; &1 M
RS1'!l<JIf3 ~D .. 6 DHC e
2t iQ.C2 / ' IX .l'" ,., . .3 670 Q q PAI7 12 1'-1< 1 2. ~ "" ~ . 1- H(74 p58Jb ) .~o t I pAIS
~\.C3 ~~R19 ~ ~ sal liP< = ~4.cq.
H·(~ S ~~.~ . ~ j(D "'H "i/ ~'"'" T :tV'D m¢'t<>--l ~ICZ . • '7 6 ~ T CI~ rl-. u IO~ Ril2 CA 14 .'8 1 ~ If! 1> m lOl 8 CA 13 V7. cry II' :.l 4.1 DO D3 ~AI
~,.rb '1 ~ l PA' "'" I O~OC D b oql~ M 1/ 32 ~" 3 D3 D~ ,; D 67J Q 13
12 "" 3'1 . ",. r D2 o m N = I'} ,;! ~ 3S .', u 19 ___ _ ~ tf .....,. CKS IOO~ r IS Or '/0 <J) /<¥t, mxs I RI! ~ 4- c" M - I 1 3~
J8 6 wR l,j 102 J,J:OZ v~ 2. VU: CKS cKS ....§... . ' If- 'v~_L~~D
IH- TR)(S nS 66 ~ 11181;-4-
41 IE:.. RX:; :! ORQ SIIML k'E-T eoA~12 14
401 , Ie 1. 4f:/ (Q ono..l'" 1'=1,
" ST
HD64180-RIF8
51 15
:: -: TX;;rl ~-S-1'd4~L = l~ ~2~3 ~~ = ·%;;··12.~l). ·STD.BD L'~AlrroARD (BAOI4-) " ~ n~3. ~ $£igd~. II~ KU ~u ~ ~,-,~ .~~" ' '!'"'''' [541 ' 580C '
•• 5690 2.2.7.3 • I ~ ;i" 0 - B " 'il!'" 8M Uti IU!&aa ~'" iUTe IJU 7'J:.- .... H-·;I"t";../i... = II - ~ Y;1lj.... '! " f ! , • , , I , I ~ r~oOof"CUOI 10&1, -n'u ..... -PC.lYl. ".filIAL .",rrr o1!10011t ""' • ... .. 1[0 _Il10 _III >("""'- ",'(CII II r'1!. ~ CilI1i." 0WI1"""1If~ /4
"' tOIOI · ' A I Be" D E F G
~ JAPAN SPEC",RQSCOl',C CO .. Llll
"" A "I ,,,, , ... ,~,, , " N.t. - - . -.-, ...... -~ .... _,_ .. ,. -
11-1' ~12~/;,s(t ~i)::l{4~ ~8 ~U44
M ~ IJ~S11ffi , 't .La
PAI6 ~ llf tyROIj flIli ." I>l 1'- moMes Al • L
'AI~ 3 A2 3 I . '6 .L....<, .. , o---fAJi 16 ~ II. CiWRS M I" I> • !I~~U)
5" "" 1 B It oiiIDii1 AI2 4 AI2 t» ~ ~12 Ym" 17 RAS ~ J )----l t Aq ; A, 0) ~ "'" 7 •
• A' !<) -.1 . FSH 1 r1 ~.,., 6 <02 B lfl ourlUp ... -.A7 :J )-.-!. 1 5 AS (I> ----l Vto 2! VBT,p HE>\ .1> "1%1 cAI3 ~ B .16 iiiJi1i3 • A+ (6) ----1 q'* lU) - :/4 -= CA/4 ,0 (') =i GIll> • I
cAIS 12 A ,,/11.. Ct) ..J 1.3 AIWq iOii"Q " 110 '" 17 AI (,) ~ MB&U4A .1l. lie. I~ .E,. RI 14- L~E~'7 AO 00) WR DI ~ 14 (II) --". -IOL()lFP) - I
! . ~ I (IV '---!1 "'3 I~~ DW '. [ ~ D2 15 PZ fll) :=:.1! III ~ ) D '7 b3 OS) ~ IPMll4<i' D3 II A~ I'I!> IB IIBT
v/l IB P4 (16) ------4 - 12L 02. 12 f.--I b~ (/7) ~ PI DS *5v"~3- 5V"
"'" " ~
>1'.'" VBT (2 BAT. 20 D6 (I~ -----L! ~ 104-D7 .<1 P7 (II) ~ 07 11~
If,\j[ I "V ><4 . l!>Isi.~.1 ov ~ 22 to ("') -IO~HFf' • ~ RTC
~ D6 '- __
AIO ... AID (l) --4 .0 RD l'IUS"3
"" ~ (>1.) ~ i{ WR ,0 ... 62l\2I -. ,. Ail (23) ~ ~II = z."Cf JijfZ"
11 '0 A1 (l~) . r---4.~' AI ~ <to.r I IAI I . AIO 18 >7 At (~ ~~ A.
PAI3 ,. AI3 "0) •• A""'2 I .. AI A I4Ii 2' A ~ "7) AD .. c>
~T " il( " . m!
L ';0 CV«)(,,)
. ! JU'2'" 1 <lIP ("") 104;r, "
Ie SOCl(tT 32p(ZQp) VBT
>01 ~ . zt3 I
(1115"-,
5\9, 10K
~
101 t'FAIL ,f! 1'3),2.51<.4£2
, - !
" . - • - Bf:t OUl .tII!. ........ Dn8 OUd''''0I
" - 0 - II,n.I2 .19· STD·BD L fIIA[N M~kP lPAoI4-) " - c -" - .2~ 3 • - ~ I .. , IIiO "" ;JU
~.- ,- C><IlOltO
~ bS4-I-5"80C 13 •• 5690 .. ~lL ~>!.-~~,,~~:;~,'oiii '%. iI:!1IiI ." "4 'Ir!l!lla .. m MIT_ ;JU "f'J;". ~I""-""':"'/( ;010 f.J1i.~!~:""".!:~ I I I I I . I
'.00)1",'001 ~ .. .. - (ell ....... «II>AI,. ""feTl ._, - "",""'0 ___
Sl-' &n'UT(C
. ... .. -A -B ~ , c -o , -E -F -G
JAPAN SPECTHOSCOPtC CQ..Ll D. ......... , .. ~,~ 'U .. , - - - - - . -,--..- -~-''- ,~ .. -... -., -
MB»f256 -IZP5l-q-8C X8/tt ' ' I "
, \
IS 2.. y ll.l. ~ - r-- - r-- r-- r--'- ;-- r-- r-- ;-- - - - r- - r--~ r - r - - r r r
t> 3 B I" aM r r - - r r 5 ~ .~ r - r r ~ ~ r 6 ' liz.. ~e r - r r - ~ ~ - r - -
0 /I
2 10 HCI5~ '~r r - r - ~ ~ - r - -W~r r - - - r - - ~ - - ~ -t I '
" 1(20 ~M r - r - - - r r - ~ r - ~-- A3 3 ~ r - r - - - r r r
~ SAA ~ - r - - - r r - r ~I m;r. I IS
Il> 7 I~C - r - - - r r -
AI2. , . ~ 40- ~~~~ - r - - - r r -~ 'I' - r r r r - -
\4 " f: ,.1 ~ r r r - ~ ~ - - - '-' P, 13 B
>E' ,~ r - r - ~ r - r - - ~ .2EZ S ' CI~ lclb ICI~ lOt )e13 tra2 e ll IUD rL~ J(~ lq u6 lC-~ [(9- (3 HZ P 114- II
~
1 Ib 10 ICI9 2 6 .> .> ":rF ":rF .. 'T -;jT ~T '-r¢- "IT' .[T 7~ >:16 'IT ' .> 4
- I' 15 4- HCI5'j PO J-~7 I~ J§..
.<--- . QL .EL- l£!. '~2 AihAJf1 ~ l2£~
~ ~L2L ffiViB,SUf'Fl'l' . £L - / " Sv-,
5v (:~ l. s' • <13 - I . *_639' /, I Icj)~f
qNf) ~~ '0 r
- _J rf,
H71flS-O
U'12.
I .
j !
19. • - , - 8f:t ~T( .lIts ~ ...... " fAts o[<.c~ .. '''''
" , , - 0 - ,,8:6,12- ,.2.D, .sTD. BD L~AIN BOARD ( BMI4-) " - c -" =~., .
~;id ~ tlifi IIU ;0 .. .~ ,-.... CO'lO -" 6541-5&0(5 •• 5690 l2'l~ A ,~
~ ~r!--.... 8N "' . 1:~12. .... RfiS ;0 .. 7'J;"'~.lilt ~J "";"'I~ ... a,1i.~ '-~"'':II I I , I I I 1?4 .... oOoI'.c::. It ... ~ .. ~, ...... fnl'llL ., ,, ..... ""f'.-I[ "~. - '''''''(0 .. _110",_" "'MAL "'(.-" r , \.,
.... . ft .. " • • -A n I;! -c -o -E -F G
"tv
t
2 1- -
" ... 3 "
r
4
JIS A3 1291XQOI
~HE AS
::r1.
J7
4~
. SA lvlE AS J \
.]'6
--'Ll
SfTHE SAI~ [-As As :r I J I
I5 I J4
c~ JLl - -- - --I -- r I IA'\ ~IA I
l~~
t<~ [CR., rU
SAME RI<lltT
.(1 C"'IS£»
!8IH,6Di705
J3
Ei ----, r- I
DR!liT )' /A I IAr I J1'Nji! )~
~..vvd {FDD'tfJ
sAME: R\GHT (IC'V~)
.. ' J2.
.JAf'AH SP~CTAOSCoPlC CO .. UD.
F S*jlft:Z:fiI I.:i1: fliit Q
liROO' fA BAcK: B
Jjr Si~
1§2B
»TI 2C 3A
"""""S 36 3C
a4~
~ 4C. ~ 5"A w1rr 56 MJ 5g~
/~/ ~ m& S6B I B~ D1 6C
,. DI ) 7A D2 )'7B D3 ) '1c. D4 ) 8A DS ) 8B D6 ) 8e 07 )'1 A
M q~ AI ) loA A2 < loB ~3 . 10C.
M ~::~ A7 ( lie A8 \ 12A A9 , 12.6
1 - , I I
I~~ ~vcc
I I
'1Dn( ~:1ND
I I
AIO · I2.C.
~I' ) :~~ : PAI~ 5 I~C. J I
1
PAlt ) t4A SSI I-PAIS S 14~ 060-
1 ~3 tlg6 ~A I170L I IS-B: 8 ISC. I
. ,6D I
1
~
2
~
3
~
4
~
5 ~Q~ __ I ....l oS
19 . • • - E - 8M ()'\ I( ."S ~......... fIlI rus Pl!o(:,,"', ....
: ::: = ~ =" If/, , 12. .)D. STD. BD lI·iAlN BoAR]) (BAoI4) I I " - 2:> ,-. - ~ eW ~Q n~ "" "'u . , , ~ ~." ,- .~~" .~, c 54- I t:- 8 0 CB
... 5690 22,).3 • I"" . 0 - J Ir!~ 8N aztt 21!1I!. 1I.Ift I:fifl ~u 7'):.-~"IiIf-·;JY::-/i ilJII = II - 1;tJ., , , , I ! , , , ! , I 't .•• ~ ... ~ "" ,,_ ".,~. .,_ "''''' ~o .~ ~.'" _~ ._0 "o~ ~""" "';"s.- ~ l!.- OJ .... - ._0 Z ~ lo.g • • A B c o E F G
~
-$-~
~ 3 1
-$-4
5
.u.I"Af~ ~ .. t:.C1HU::'COljIC CO_L10.
;.. 1 u __ 1 c I o I E I F SJl[~:l'tI I'IWr.it ~fi
'd>OI-O!D-I~Ot---.:, . -1£! J!! ....1ll
I
...1!r. ...1f! ~ 1/
'. ;;:t~--q I A~ t;\? ~rf.'=--'-' ttl A' -
;;t7i:--JJ '"-~;-":!t...._~ , A> ~~L-_tIN- 6 r,i1r..;;-_J I ' '> 5 4
3
/I
I>
IJ
»
"
) ,
: . , 1
,
" )
" t'
" ". " "
" 1
" " I' I
f-E-q"" 5'1 2
~mH
:r c. '1
Ae ilL- __ _ ''' I ~
p2 r--'~1!3! s.~ 3 j«
". :,~ '''' • ~s "Tn~ - 't 20 1f~ ~ S/I' 0 ,
46 011 sa - /Z "' ... '" - ~ " ~~ . - -".~ , . " ' ,~,.. ' 0- "'"
" • " '" I SV /D ~tk '13 II C'S3 25tlijiS
'", • , '"J
7D~'~U am " ,. "" . ' '" , " -
• PFAIL ....::L!!=-_ ,1---'
CK2&DS 2SK33('
U078 QI
14 ) 2 !AT ,J;Ll_ J2 1?182t-3
~~D
~. " -'A , - I , 1 - :in r.~'l MIll!. ~~"l !:lll -& cue·" ',,',
" I ...e.. ~r" ~.,q.o - 0 - ,,86 · 10 . IS . Stllll\MnL B01·«i. hOP Ro f-'\ BOA R i) " \Lf.. joP4 :-i.l-d. - .213' c -" .J.AI\ :riA~ - - . • - J.As.cD "" nil! ,U1 ~II
M 5690 , • ~~ ~~ I(-~~ jt~ ,6,5,4-.I ,- .5,'7 ,4-,C,8, U .. IBM I~~ In". ;.UI R'" o.u 7'J;" ~.til1 - ·:J "';"1\ U ::lr-Hl ... .;.:.·<_ ~O;.'IDO. ~n s ..... _ IC~LVl~ 'I."'~ •• ... ra . ~. ," ...... ' l OiOOlIIO_. " ... .0;. UY'{CT I O
wEalt 0*'1< _.,! • A I O'«>,' A B C 0
, E F
I-
2
I-
3 I-
4 I-
5
,
'~ c:
