NALYTICAL IRCLE - Fujifilm

70FM TLC -
-
DOWEX™ ICP-MS
® MycoTOOL PCR Mycoplasma Detection Kit NH
66 NMR qNMR “”

2015.9No.78ANALYTICAL CIRCLE
ANALYTICAL CIRCLE2015.9No.78
2. 3. p- 4. p-
:= a) 95:5 b) 90:10 c) 85:15 d) 80:20 (v/v)
UV254nm 10cm

a ::=8:2:1(v/v/v) 4- 1055 10cm
162

195-12871 70PF254() 0.75 10(20cm×20cm) 15,000
143-08641 100(2.5cm×6.6cm) 20,000
145-08721
NH260F254-
()
70 TLC- 70FM TLC - (λ=250 400nm)
520μm
7nm70
(254nm) (250400nm)
199-17813 10( 5cm×10cm) 2,900
193-17816 200( 5cm×10cm) 25,500
197-17814 100( 5cm×20cm) 22,500
193-17811
195-17871
192-17881

CHIRALPAK® AGP
Silodosin Ureif α1A- JP
CHIRALCEL® OJ-RH Rosuvastatin Calcium Crestor HMG-CoA EP
Abacavir Sulfate Ziagen HIV USP
Atorvastatin Calcium Lipitor HMG-CoA USP
Fulvestrant Faslodex USP
CROWNPAK® CR(+) Valacyclovir Hydrochloride Valtrex JP,USP
No. ()
307-31971 30713 CHIRALPAK® AGP 4.0×100mm 5μm 1 200,000
308-08051 17025 CHIRALCEL® OJ 4.6×250mm 10μm 1 180,000
305-07961 17724 CHIRALCEL® OJ-RH 4.6×150mm 5μm 1 165,000
CHIRALPAK® AGP 4.0×100mm
NaCl aq.(29g/L)/CH3OH
n-Hexane/ Diethylamine/C2H5OH
=93/10/ 7 (v/v/v)
Heptane / C2H5OH=17/ 3 (v/v)
0.8 mL/min
0.1TFA/CH3CN

Diphacinone Standard 045-33781 100mg 16,000

2-(Diphenylacetyl)indan-1,3-dione
C23H16O3
340.37
Flutolanil Metabolite M4 Standard M4 064-06481 50mg 30,000

α, α,α-Trifluoro-3’-hydroxy-o-toluanilide
Isoxaflutole Metabolite B Standard B 097-07111 100mg 30,000

2-Cyano-3-cyclopropyl-4-(2-methylsulphonyl-4-trifluoromethylphenyl)propane-1,3-dione

Ethyl O-[5-(2-Chloro-α,α,α-trifluoro-p-tolyloxy)-2-nitrobenzoyl]-DL-lactate

Methyl (E )-3-(Dimethoxyphosphinothioyloxy)-2-methylacrylate

4,4',6,6'-Tetramethyl-3,3'-ethylenedi-1,3,5-thiadiazinane-2-thione
C12H22N4S4

No. (
Vedaprofen Standard 227-02291 100mg 30,000

2-(4-Cyclohexylnaphthalen-1-yl)propanoic Acid
047-30441 100mg 10,000
092-03901 200mg 18,900
160-08871 100mg 10,500
K.M.)
Presep® RPP-WCX
Iminoctadine Diquat Paraquat
50 0.9986 80.5 0.9973 99.8 0.9955 88.5

NH
NH2NHNHNH
NH
NH2
A 150mM (pH 3.6)
6min.(5050)→7min.(8020)→17min.(8020)→
17.01min.(3070)→25min.(3070)

Time(min

W
D 41,000
HILIC
50mL 1mg/L
6
06
10% 9% 8% 7% 6% 5% 4% 3% 2% 1% 0%
80 120 80
Step 4 – 110 Step 5 – 25Step 3 – 150Step 2 – 110Step 1 – 25 0
25
50
75
100
ns e
4. 3
4. 4
4. 5
4. 2
O.Y.)
-
System Agilent 6890 GC with CTC PAL autosampler with Headspace system
Phase 25m 250μm ID 0.25μm BPX5 column
Sample 10ppm Hexane:Water sample incubated at 80
Initial Temp 40 Rate 1 20/minute Final Temp 100 Detector Type FID, 250 Carrier Gas He Injection Port Temp 140

()
Fig.2 1205

Fig.3


No.
(mL)
RSH
CAS No, ()
ASB-00001977-010 10mg 21,000
25mg 40,600
25mg 93,500
ASB-00005060-005 5mg 79,200
ASB-00005060-010 10mg 125,200
25mg 283,400
ASB-00005065-005 5mg 78,400
ASB-00005065-010 10mg 123,800
25mg 279,400
25mg 109,200
ASB-00005450-005 5mg 31,400
10mg 47,300
10mg 51,800
10mg 156,800
25mg 175,000
5mg 100,200

CAS No, ()
ASB-00010540-001 Jusneesiinol 216955-78-1 C20H14O7 RG 1mg 42,800
ASB-00010545-001 1mg 28,600
5mg 100,200
ASB-00010555-005 Justirumalin C20H12O7 SH 5mg 56,000
ASB-00012074-005 5mg 17,100
ASB-00012074-010 10mg 28,600
25mg 57,100
10mg 56,000
5mg 94,100
10mg 56,100
ASB-00016635-001 1mg 56,000
5mg 142,100
25mg 91,000
ASB-00016940-005 5mg 15,800
25mg 31,400
10mg 61,900
1g 910,000
1g 630,000
50mg 251,700
ASB-00019447-005 5mg 80,900
ASB-00019500-005 5mg 61,900
ASB-00019500-010 10mg 93,500
25mg 205,500
10mg 93,500
25mg 205,500
50mg 378,300
ASB-00020012-001 Taiwanin E Methyl Ester 30403-00-0 C21H14O7 RG 1mg 113,400
ASB-00020308-001 Tiruneesiin C24H28O8 RG 1mg 28,600
ASB-00023900-005 5mg 110,600
5mg×2 210,000
ChromaDex

U.TN.)

1. 1 2.(2) 5 () 3. 40 () 4. 10 () 5. 10 6. 10
No. ()
138-01836 500mL 680
013-00356 500mL 800
082-00426 500mL 830
198-01675 500g 780

(
)

(
293-76001 10 13,000
1 2 3 4

2 3 4 1 2 3 4
1 : 2 : a 2 : a 3 : b 1 : 2 : a
3 : b

(I. 401 II. 501)
30mL 120mL 500mL 3g

HPLCLC/MS 1HPLC(UV) HPLCHPLCUV/VIS PDAUV HPLC
LC/MSHPLCLC/MSHPLCLC/MS LC/MS
016-19854 100mL 2,300
012-19851 1L 7,100
062-04721 1L 7,000
n20 D 1.3431.346 1.3431.346 1.3431.346
0.1 0.05 0.05
0.005 0.001 0.001
(NH4 ppm 0.3 0.3

1ppm10ppm

No. ()
045-33041 100mL 4,000
500mL 6,000
500mL 4,400
500mL 5,100
500mL 7,600
500mL 5,310
500mL 4,800
500mL 4,150
18L
207-18701 100mL 2,800
500mL 4,900
No. ()
014-23461 100mL 1,800
016-23465 500mL 3,350
010-23463 3L 13,700
3L 14,000
3L 14,700
500mL 4,400
1ppm
No. ()
027-18361 100mL 2,300
029-18365 500mL 5,000
3L 17,000
3L 21,500
18L
048-32811 100mL 2,500
040-32815 500mL 7,000
3L 18,240
500mL 7,000
500mL 5,000
No. ()
139-17611 100mL 2,500
131-17615 500mL 5,700
9L
161-24845 500mL 4,200
3L 16,000
18L
205-17901 100mL 2,050
207-17905 500mL 4,300
209-17904 3L 15,200
18L
202-17911 100mL 1,850
204-17915 500mL 3,500
206-17914 3L 13,000

GPC
034-24541 1- GPC 1L 35,000
036-24481 1L

DOWEX™

(meq/mL)

(g/L)
pH

™ HCR-S Na 3001200μm: 90min. 44-52 1.9 800 0-14 120 A
™ ™ 650C(H) H 600700μm 46-51 2.0 785 0-14 120 A
™ C-10 Na 580680μm 40-45 2.2 845 0-14 130 A
/

(meq/mL)

(g/L)
pH

™ 66 3001200μm: 95min. 40-46 1.6 640 0-7 60 B
™ WBA 475575μm 50-60 1.3 640 0-7 100 A
™ ™ 77 475600μm 40-50 1.7 640 0-7 60 B
I

(meq/mL)

(g/L)
pH

™ A Cl 525625μm 50-60 1.3 670 0-14 100 A
™ MSA Cl 590690μm 56-66 1.1 670 0-14 100 A
™ ™ 550A(OH) OH 540640μm 55-65 1.0 660 0-14 60 A
II

(meq/mL)

(g/L)
pH

™ 22 Cl 3001200μm: 97min. 48-56 1.2 670 0-14 46 B
™ MSA-2 Cl 3001200μm: 90min. 48-56 1.1 670 0-14 70 A
™ A2 Cl 500600μm 45-54 1.2 690 0-14 70 A

()
357-14371 100mL 4,500
353-14373 ™ HCR-S

DOWEX™
() () (meq/mL) (g/cm3) DOWEX™ 50W×2 2 50-100 H 74-82 0.6 0.74 DOWEX™ 50W×2 2 100-200 H 74-82 0.6 0.74 DOWEX™ 50W×2 2 200-400 H 74-82 0.6 0.74 DOWEX™ 50W×4 4 50-100 H 64-72 1.1 0.77 DOWEX™ 50W×4 4 100-200 H 64-72 1.1 0.77 DOWEX™ 50W×4 4 200-400 H 64-72 1.1 0.77 DOWEX™ 50W×8 8 50-100 H 50-56 1.7 0.80 DOWEX™ 50W×8 8 100-200 H 50-58 1.7 0.80 DOWEX™ 50W×8 8 200-400 H 50-58 1.7 0.80 () () (meq/mL) (g/cm3) DOWEX™ 1×2 2 50-100 Cl 65-75 0.7 0.70 DOWEX™ 1×2 2 100-200 Cl 70-80 0.6 0.70 DOWEX™ 1×2 2 200-400 Cl 70-80 0.6 0.70 DOWEX™ 1×4 4 50-100 Cl 50min. 1.0 0.70 DOWEX™ 1×4 4 100-200 Cl 55-63 1.0 0.70 DOWEX™ 1×4 4 200-400 Cl 55-63 1.0 0.70 DOWEX™ 1×8 8 50-100 Cl 43-48 1.2 0.70 DOWEX™ 1×8 8 100-200 Cl 39-45 1.2 0.70 DOWEX™ 1×8 8 200-400 Cl 39-45 1.2 0.70
() 322-97561 100mL 7,000 324-97565
™ 50W×2 50-100 500mL 19,000
325-97551 100mL 7,000 327-97555
359-27261 100mL 7,000 351-27265
356-27271 100mL 7,000 358-27275
329-97571 100mL 7,000 321-97575
353-27281 100mL 7,000 355-27285
323-97591 100mL 7,000 325-97595
328-97541 100mL 7,000 320-97545
326-97581 100mL 7,000
500mL 19,000 323-97471 100mL 7,000 325-97475
™ 1×2 50-100 500mL 19,000
326-97461 100mL 7,000 328-97465
352-27251 100mL 7,000 354-27255
320-97481 100mL 7,000 322-97485
327-97511 100mL 7,000 329-97515
320-97501 100mL 7,000 322-97505
355-27241 100mL 7,000 357-27245
324-97521 100mL 7,000 326-97525
327-97491 100mL 7,000 329-97495
321-97531 100mL 7,000
500mL 19,000
DOWEX™2”X” DVB
50W : 1 :
™ 50W×8 : 8DVB ™ 1×4 : 4DVB

25 HNO3
Water tr.HF
10 HCl
25 HNO3
100 519-99651 ICP-MS-24N-0.01X-1 15,100
25 HNO3
25 HNO3
10 HCl
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
210 HNO3
Water dilute
100 511-99731 ICP-MS-36N-0.01X-1 12,200
25 HNO3
25 HNO3

μg/mL No.
25 HNO3
25 HNO3
100 ICP-MS-03N-0.01X-1 11,400
25 HNO3
25 HNO3
25 HNO3
210 HNO3
Water tr.
100 ICP-MS-08N-0.01X-1 11,400
25 HNO3
10,000 ICP-MS-08N-1 25,500
100 ICP-MS-09N-0.01X-1 11,400
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3

25 HNO3
Water
Water tr.HF
1040 HCl
25 HNO3
25 HNO3
25 HNO3
25 HNO3
100 556-00351 ICP-MS-64W-0.01X-1 12,200
Water tr.HF
Water tr.
100 550-00371 ICP-MS-67N-0.01X-1 12,200
25 HNO3
25 HNO3
25 HNO3
25 HNO3
25 HNO3
551-00421 ICP-MS-BLN-1 ICP-MS-5 100mL 10,800
ICP-MS-BLN-5 ICP-MS-5 500mL 15,100
ICP-MS-BLH-1 ICP-MS-5 100mL 10,100
ICP-MS-BLH-5 ICP-MS-5 500mL 15,100
ICP-MS-BLW-1 ICP-MS 100mL 10,100
550-00435 ICP-MS-BLW-5 ICP-MS 500mL 16,200
: 100mL : 100mL
Water tr. HF
10 HCl
Water
10 HCl
25 HNO3
25 HNO3
Water tr.HNO3
10 HCl
25 HNO3
10 HCl
25 HNO3
25 HNO3
25 HNO3
Water tr.HF
25 HNO3
25 HNO3


No. ()
307-30751 NIP-50-1.5 50 7,000
200 24,000
200 24,000
No. ()
303-95431 320102 100 9,000
300-95441 320103 100 12,000

G.YM.)
®
No. ()
304-96061 320302 50 8,000
301-96071 320402 240 9,600
308-96081 320403 240 12,000

®
®V
®SP
No. ()
389-01281 891390 20 8,800
385-01283 891391 V
100 25,000
100 28,000
382-01271 891300 1 8,000
(PP) 1 100mg
2 ()

MycoTOOL PCR Mycoplasma Detection Kit MycoTOOL PCR Mycoplasma Detection KitPCR
DNA”MycoTOOL Mycoplasma Detection Prep kit (Prep kit)”DNA
/

9:30 PCR
12:00 PCR
Prep kit Amp kit
Prep kit (10)
Proteinase K) 2×850μL Lysis Buffer 5×4mL Precipitation Reagent 5×6mL Washing Buffer 5×9mL Dissolution Buffer 10×1mL 45vials
2-10
Amp kit10
RM1a 5×45μL RRM1b 5×570μL MgCl2-Solution 5×600μL Primer Mix, Mycoplasma 5×40μL Primer Mix, GAPDH 5×30μL Detection Dye) 5×120μL PCR grade Water 5×1mL Dilution Buffer 5×1mL Negative Control 5×1mL Positive Control 5×55μL DNA Molecular 1×200μL Weight orange Marker

(15/)

M1 : 100bp Marker
M2 : 50bp Marker
NC : Negative Control

639-24991 05184592001 MycoTOOL PCR Mycoplasma Detection Prep kit 1kit 190,000
632-24981 05184240001 MycoTOOL PCR Mycoplasma Detection Amplification kit 1kit 260,000
632-25341 05619424001 MycoTOOL Carrier DNA 5×320μL 120,000
No. ()
636-25001 6495605001 MycoTOOL Real-Time PCR Kit 1kit 370,000
318-90041 5×TBE 1L 9,000

300-85671 NH O157 25 8,000
307-85681 NH O26 25 8,000
304-85691 NH O111 25 8,000
NH2!!

300-31581 NH 20 14,000
303-31691 NH 20 10,000
301-83141 NH 20 14,000

oui

11 150

1N105

108

Analytical Circle
Wako Bio Window Wako Organic Square

()
71 10

(KN.B.)
21
22
21
23
23
•Wako Chemicals USA, Inc. http://www.wakousa.com Head Office (Richmond, VA) Tel: +1-804-714-1920 Boston Sales Office (MA) Tel: +1-617-354-6772
•Wako Chemicals GmbH (Europe Office) http://www.wako-chemicals.de Tel: +49-2131-311-0
: 540-8605 1 2 TEL: 06-6203-1788 : 103-0023 1 TEL: 03-3270-8243
: 0120-052-099 : 0120-052-806
TEL: 092-622-1005 TEL: 082-285-6381 TEL: 052-772-0788 TEL: 0466-29-0351 TEL: 029-858-2278 TEL: 022-222-3072 TEL: 011-271-0285
…210 …20 …80
… … …
/moc.ukayis.www//:ptth moc.ukayis
… … …… … … … … … … … … …
DM
24
K.A.)
: 271013() 13:0017:00 : () 5
5CSJ2015 : / : : 2

NMR(qNMR) ""
NMR --

NH

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NALYTICAL IRCLE - Fujifilm