42
Omar El Khatib Teaching and Research Assistant Cairo University Under Supervision of: Prof. Dr. Mohamed Helmy Sayyouh Prof. Dr. El Sayed El Tayeb Prof. Dr. Ahmed Hamdy El Banbi OGUFD SESSION 17 Abstract ID: 635 Development of a Predictive Model for Miscible EOR Processes

Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

  • Upload
    others

  • View
    2

  • Download
    0

Embed Size (px)

Citation preview

Page 1: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Omar El KhatibTeaching and Research Assistant

Cairo University

Under Supervision of:Prof. Dr. Mohamed Helmy SayyouhProf. Dr. El Sayed El TayebProf. Dr. Ahmed Hamdy El Banbi

OGUFDSESSION 17

Abstract ID: 635

Development of a Predictive Model for Miscible EOR Processes

Page 2: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Dedication

13/02/2017 2

Page 3: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Contents

1. Introduction & Background

2. Statement of the Problem

3. Objective

4. Model Development, Capabilities and Validation

5. Conclusions & Recommendations

6. Discussion

13/02/2017 3

Page 4: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

• Enhanced Oil Recovery (EOR) technology is gaining anincreasing importance due to the present difficulties indiscovering new reservoirs and the increasing energy needs

• In 2010, EGPC (Egyptian General Petroleum Corporation) hasdeveloped a strategic plan to evaluate the residual reserve inEgyptian mature reservoirs to determine the applicability ofthe different EOR methods.

• In 2014, EGPC signed a corporation protocol with MSRC, CairoUniversity to develop an EOR Map for all the reservoirs.

Introduction & Background

13/02/2017 4

Page 5: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

• In 2013, Cairo University Research Team developed a generalapplied research methodology to determine the most suitableEOR methods for any field.

• Predictive software package that is able to predict theperformance of different EOR methods is one of the toolsrequired for this methodology

• The software package includes the following EOR Methods:1. Chemical Flooding - Finished2. Miscible Flooding – In Progress3. Thermal Flooding – In Progress4. Unconventional EOR (Seismic) – In Progress

Introduction & Background

13/02/2017 5

Page 6: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

1. Analogical methods

2. Experimental methods

3. Mathematical methods (Analytical – Empirical – Material

Balance – Decline Curve Analysis)

4. Predictive methods (A combination of modelling approaches)

5. Numerical methods (Reservoir Simulation)

Modelling Approaches

Introduction & Background

13/02/2017 6

Page 7: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

1. Screening Guides (Initial indicator)

2. Predictive Models

3. Reservoir Simulation Software

Early Stage Studies for EOR Applications

Introduction & Background

13/02/2017 7

Page 8: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Early Stage Studies of EOR Applications

Screening Guides Predictive Models Reservoir Simulation

Advantages

• Simplest tool for applicability of EOR methods

• Consideration of reservoir and fluid properties and behavior

• Fast and simple prediction

• Most accurate method of reservoir performance

• Mixing and physics of fingers are considered

Disadvantages

• No consideration of any characteristic of fluids or the porous medium

• No indication of economic feasibility

• Assumptions made in their formulation

• Expensive and time consuming

• Lack of necessary data

Introduction & Background

13/02/2017 8

Page 9: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Introduction & Background

Miscible Predictive Models (Factors Affecting Miscible Displacement)

13/02/2017 9

Comparison

Items

Koval, E.

J., (1963)

Claridge,

E. L.,

(1972)

Paul, G.

W. et al.

(1984)

Walsh, M. P.

and Lake, L.

W. (1988)

Mollaei,

A.,

(2011)

Jain, L.,

(2013)

Heterogeneity √ √ √ N/A √ √

Viscous

fingering√ √ √ N/A √ √

Gravity

segregationN/A N/A √ N/A √ √

Loss of

miscibilityN/A N/A N/A N/A N/A N/A

Interference of

wavesN/A N/A N/A √ N/A √

Diffusion N/A N/A N/A N/A N/A N/A

Cross flow N/A N/A N/A N/A N/A N/A

Page 10: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Comparison

Items

Koval, E.

J.,

(1963)

Claridge,

E. L.,

(1972)

Paul, G.

W. et al.

(1984)

Walsh, M. P.

and Lake, L.

W. (1988)

Mollaei,

A.,

(2011)

Jain, L.,

(2013)

PatternLine

drive5-spot

Line drive

5 spotLine drive

Line

drive

Line

drive

Type of flow Diffuse Diffuse Diffuse Diffuse Segregat. Segreg.

Solvent type Any Any CO2 Any Any Any

Chase fluids N/A N/A N/A √ N/A N/A

Introduction & Background

Miscible Predictive Models (Injection Strategies)

13/02/2017 10

Page 11: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Statement of the Problem

As concluded from the literature survey, there is no model that

takes all factors, affecting EOR processes, into consideration.

In addition, commercial software covering this branch of models

are rare. Therefore, it is essential to develop a software package

that can quickly and effectively predict the performance of

different EOR methods by taking into consideration all the features

accompanying the process.

13/02/2017 11

Page 12: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Developing an effective screening

Tool

Developing predictive models for

EOR methods

Software package

Screening tool(Done)

Miscible model Thermal model Seismic model(In progress)

Chemical model (Done)

Pro

gre

ss B

ar

2015 2016 2017

13/02/2017

Statement of the Problem

12

Page 13: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Miscible displacement

model

13/02/2017

Developing an effective screening

Tool

Developing predictive models for

EOR methods

Software package

Statement of the Problem

13

Page 14: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Objective

The main target of the present work is to develop a rigorous

software package that can predict the performance of

miscible flooding without throwing away the advantages of

predictive models of fast calculations and easy use.

13/02/2017 14

Page 15: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Model Structure

13/02/2017 15

Page 16: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Model Capabilities

Injection Features

Pattern type Line Drive & 5-spot

Type of injection

(Continuous / WAG) & /

Chase Fluids with different injection strategies

Optimum WAG determination

Solvent type Any

Type of Reservoir

Stratification and heterogeneity

Stratified / Not stratified

Miscible Process Features

Effect of mobile water blocking

Considered / Not Considered

Effect of phase behavior

Considered / Not Considered

Viscous fingering Considered / Not Considered

13/02/2017 16

Page 17: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Model Approach

Recovery Factor = 𝐸𝑑𝑖𝑠𝑝𝑙𝑎𝑐𝑒𝑚𝑒𝑛𝑡 ∗ 𝐸𝑎𝑟𝑒𝑎𝑙 ∗ 𝐸𝑣𝑒𝑟𝑡𝑖𝑐𝑎𝑙

Fractional Flow Theory (Graphical)

Areal Sweep Models

Layered Calculations

13/02/2017 17

Page 18: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Fractional Flow Theory (Graphical)

𝜕𝑆𝑤𝜕𝑡𝐷

+𝜕𝑓𝑤𝜕𝑆𝑤

∗𝜕𝑆𝑤𝜕𝑥𝐷

= 0

1. Aqueous phase mass conservation equation:

2. Oleic phase mass conservation equation:

𝜕(𝐶𝑠𝑜𝑆𝑜)

𝜕𝑡𝐷+

𝜕(𝐶𝑠𝑜𝑓𝑜)

𝜕(𝐶𝑠𝑜𝑆𝑜)∗𝜕(𝐶𝑠𝑜𝑆𝑜)

𝜕𝑥𝐷= 0

13/02/2017 18

Model Approach

Page 19: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Fractional Flow Theory (Graphical)

13/02/2017 19

Model ApproachModel

Approach

Page 20: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Areal Sweep Efficiency

Mahaffey et al. Experimental model for 5-spot

13/02/2017 20

Model Approach

Page 21: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Vertical Sweep Efficiency

Vertical Sweep is considered by performing (Ed*EA) calculations on every layer and summing them up at the producer to reach the recovery efficiency

13/02/2017 21

Model Approach

Swept Zone

Non Swept Zone

Page 22: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Model Development

Assumptions

1. Isothermal porous medium 2. Independency of fluid properties on pressure3. Ideal mixing of fluids (Fluids don’t interact with the solid

phase)4. Negligible dispersion and diffusion 5. Presence of only oil and water at initial conditions6. Simultaneous injection of water with solvent or water with

chase fluid7. Two immiscible phases (aqueous and oleic)8. Full miscibility (First contact miscibility) of two components

(Solvent and oil) in the oleic phase

13/02/2017 22

Page 23: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Input Data

1. Relative permeability data

2. Fluid properties

3. Reservoir characteristics

4. Injection pattern provisions

5. Solvent specifications

13/02/2017 23

Model Development

Page 24: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Output Data

1. Oil production rate vs. time

2. Cumulative oil production vs. time

3. Water cut vs. time

13/02/2017 24

Model Development

Page 25: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Model Validation Cases

Input Data 1st Case 2nd Case

Type of injection Continuous injection Continuous injection

Pattern Line Drive 5-Spot

Injection rate (res bpd) 500 500Distance between producer & injector (ft)

4300 1320

Bo (res bbl/STB) 1.1 1.1Bw (res bbl/STB) 1 1Oil viscosity (cp) 1.5 1.5Water viscosity (cp) 1 1Solvent viscosity (cp) 0.3 0.3

13/02/2017 25

Page 26: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Model Validation Cases

13/02/2017 26

Input Data 1st Case 2nd CasePorosity (fraction) 0.18 0.18Pattern Area (ft2) 871200 871200

Swc 0.25 0.25Swi 0.25 0.25

Sorm 0.05 0.05Total thickness (ft) 20 20

Permeability insertion mode

Data points Data points

Page 27: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

1st Case (Line Drive →M =5)

13/02/2017 27

Model Validation Cases

0

50000

100000

150000

200000

250000

300000

350000

400000

450000

0 2000 4000 6000 8000

Cu

mu

lati

ve P

rod

uct

ion

, res

b

bl

Time, days

Walsh + Dyes - Program

Koval - Program

Eclipse

Page 28: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

1st Case (Line Drive →M =5)

13/02/2017 28

Model Validation Cases

0

100

200

300

400

500

600

0 2000 4000 6000 8000

Qo

, res

bp

d

Time, days

Walsh+Dyes - Program

Koval - Program

Eclipse

Page 29: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

2nd Case (5-spot →M =5)

13/02/2017 29

Model Validation Cases

0

50000

100000

150000

200000

250000

300000

350000

400000

450000

0 2000 4000 6000 8000

Cu

mu

lati

ve P

rod

uct

ion

, res

b

bl

Time, days

Walsh + Mahaffey - Program

Claridge - Program

Eclipse

Page 30: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

2nd Case (5-spot →M =5)

13/02/2017 30

Model Validation Cases

0

100

200

300

400

500

600

0 1000 2000 3000 4000 5000 6000 7000 8000

Qo

, res

bp

d

Time, days

Walsh +Mahaffey - Program

Claridge-Program

Eclipse

Page 31: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Model Validation Cases

Input Data 3rd Case 4th Case

Type of injection Continuous injection Continuous injection

Pattern Line Drive 5-Spot

Injection rate (res bpd) 500 500Distance between producer & injector (ft)

4300 1320

Bo (res bbl/STB) 1.1 1.1Bw (res bbl/STB) 1 1Oil viscosity (cp) 1.5 1.5Water viscosity (cp) 1 1Solvent viscosity (cp) 0.06 0.06

13/02/2017 31

Page 32: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

3rd Case (Line Drive →M =25)

13/02/2017 32

Model Validation Cases

0

50000

100000

150000

200000

250000

300000

350000

400000

450000

0 5000 10000 15000 20000

Cu

mu

lati

ve P

rod

uct

ion

, res

bb

l

Time, days

Koval - Program

Eclipse

Walsh + Dyes - Program

Page 33: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

3rd Case (Line Drive →M =25)

13/02/2017 33

Model Validation Cases

0

100

200

300

400

500

600

0 1000 2000 3000 4000

Qo

, res

bp

d

Time, days

Koval

Eclipse

Walsh + Dyes - Program -

Page 34: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

4th Case (5-spot →M =25)

13/02/2017 34

Model Validation Cases

0

50000

100000

150000

200000

250000

300000

350000

400000

450000

0 1000 2000 3000 4000 5000 6000 7000 8000

Cu

mu

lati

ve P

rod

uct

ion

, res

bb

l

Time,days

Claridge - Program

Eclipse

Walsh +Mahaffy - Program -

Page 35: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

4th Case (5-spot →M =25)

13/02/2017 35

Model Validation Cases

0

100

200

300

400

500

600

0 2000 4000 6000 8000 10000

Qo

, res

bp

d

Time, days

Claridge - Program

Eclipse

Walsh+Mahaffey - Program

Page 36: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Model Validation Cases

Layers 5th Case 6th Case

Oil viscosity (cp) 1.5 1.5Water viscosity (cp) 1 1Solvent viscosity (cp) 0.3 0.3

13/02/2017 36

Thickness Porosity Absolute Permeability20 0.18 1010 0.15 205 0.1 15

15 0.2 610 0.25 3

Page 37: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

5th Case (Line Drive - Layered →M =5)

13/02/2017 37

Model Validation Cases

0

200000

400000

600000

800000

1000000

1200000

1400000

0 5000 10000 15000 20000

Cu

mu

lati

ve O

il P

rod

uct

ion

, re

s b

bl

Time, days

Walsh+Dyes

Koval Layers only

Koval Vdp only

Eclipse

Page 38: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

5th Case (Line Drive - Layered →M =5)

13/02/2017 38

Model Validation Cases

0

200

400

600

800

1000

1200

0 500 1000 1500 2000 2500 3000 3500 4000

Qo

, res

bp

d

Time, days

Walsh+Dyes

Koval Layers only

Koval with Vdp only

Eclipse

Page 39: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

6th Case (5 Spot – Layered →M =5)

13/02/2017 39

Model Validation Cases

0

200000

400000

600000

800000

1000000

1200000

1400000

0 5000 10000 15000

Cu

mu

lati

ve P

rod

uct

ion

, res

b

bl

Time, days

Walsh + Mahaffey

Claridge

Claridge - no layering

Eclipse

Page 40: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

6th Case (5 Spot – Layered →M =5)

13/02/2017 40

Model Validation Cases

0

200

400

600

800

1000

1200

0 2000 4000 6000 8000

Qo

, res

bp

d

Time, days

Walsh + Mahaffey

Claridge

Claridge - no layering

Eclipse

Page 41: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

Conclusions & Recommendations

1. A predictive model of miscible flooding has beenconstructed and validated against reservoir simulator(Eclipse)

2. The model accounts for different injection and chase fluidsstrategies and considers factors like waves interference andloss of miscibility near the wellbore of the producer

3. The graphical solution of fractional flow theory is used todetermine displacement efficiency

4. Mahaffey’s areal sweep model is used for determination ofareal sweep efficiency in 5 spot and Dyes for line drive

5. The developed model may be extended further to accountfor other heterogeneity effects other than stratification (i.edispersion) and gravity segregation

13/02/2017 43

Page 42: Omar El Khatib Teaching and Research Assistant Cairo ... Koval, E. J., (1963) Claridge, E. L., (1972) Paul, G. W. et al. (1984) Walsh, M. P. and Lake, L. W. (1988) Mollaei, A., (2011)

THANK YOU

Omar El KhatibTeaching and Research Assistant

Cairo University