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1 On the Prediction of Long-term Creep-Failure of GRP Pipes in Aqueous Environment R. M. Guedes 1 , Alcides Sá 2 , Hugo Faria 2 1 Departamento de Engenharia Mecânica e Gestão Industrial, Faculdade de Engenharia da Universidade do Porto, Rua Dr. Roberto Frias s/n, 4200-465 Porto, Portugal 2 INEGI, Instituto de Engenharia Mecânica e Gestão Industrial, Portugal Abstract The aim of this work was to study the long-term failure of GRP (Glass Fiber Reinforced Polymer) pipes under the influence of moisture absorption. These pipes are used in water transportation which has an important effect on the mechanical properties of the polymeric matrix. The GRP pipes are usually tested under ring deflection or internal pressure conditions. This study presents and analyzes experimental creep-rupture data obtained from standard test methods under ring deflection conditions. This loading configuration simulates in laboratory the conditions verified in a sub-soil installation. The creep testing was carried out under constant dead weight on unconditioned and preconditioned samples in a submerged condition. The diametrical deflection of samples was measured periodically and the time to failure of each sample was recorded. The main purpose of this work was to determine the short and long-term rupture energies of GRP pipes and assess the influence of moisture preconditioning on those values. The observed failure mode was always the same. It was concluded that the energy at failure decreases with time. The influence of the preconditioning on the creep- rupture of GRP pipes was considered negligible. Different time-dependent failure models were described and used for long-term extrapolation of the experimental data. The maximum strain at failure decreased about 12% from 0.1 to 1000 hours of creep testing. Furthermore data extrapolation to 50 years predicts a reduction of strength of about 60%, founded on the most conservative time-dependent failure criterion. Keywords: GRP pipes; Creep rupture; Mechanical testing; Fracture; Energy.

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Page 1: On the Prediction of Long-term Creep-Failure of GRP Pipes

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On the Prediction of Long-term Creep-Failure of GRP Pipes

in Aqueous Environment

R. M. Guedes1, Alcides Sá2, Hugo Faria2

1Departamento de Engenharia Mecânica e Gestão Industrial, Faculdade de Engenharia

da Universidade do Porto, Rua Dr. Roberto Frias s/n, 4200-465 Porto, Portugal 2INEGI, Instituto de Engenharia Mecânica e Gestão Industrial, Portugal

Abstract

The aim of this work was to study the long-term failure of GRP (Glass Fiber Reinforced

Polymer) pipes under the influence of moisture absorption. These pipes are used in

water transportation which has an important effect on the mechanical properties of the

polymeric matrix. The GRP pipes are usually tested under ring deflection or internal

pressure conditions. This study presents and analyzes experimental creep-rupture data

obtained from standard test methods under ring deflection conditions. This loading

configuration simulates in laboratory the conditions verified in a sub-soil installation.

The creep testing was carried out under constant dead weight on unconditioned and

preconditioned samples in a submerged condition. The diametrical deflection of

samples was measured periodically and the time to failure of each sample was recorded.

The main purpose of this work was to determine the short and long-term rupture

energies of GRP pipes and assess the influence of moisture preconditioning on those

values. The observed failure mode was always the same. It was concluded that the

energy at failure decreases with time. The influence of the preconditioning on the creep-

rupture of GRP pipes was considered negligible. Different time-dependent failure

models were described and used for long-term extrapolation of the experimental data.

The maximum strain at failure decreased about 12% from 0.1 to 1000 hours of creep

testing. Furthermore data extrapolation to 50 years predicts a reduction of strength of

about 60%, founded on the most conservative time-dependent failure criterion.

Keywords: GRP pipes; Creep rupture; Mechanical testing; Fracture; Energy.

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1. Introduction

In recent years materials that possess high specific strength and specific modulus were

developed to fulfil the need for advanced lightweight structures. Fibre reinforced

plastics (FRP) have these characteristics, and are being used as primary as well as

secondary load carrying members in civil engineering structures. Consequently, the

development of testing procedures to predict the lifetimes of materials in extreme

service environments is becoming a high priority.

The problem tackle in this paper deals with durability issue which is usually associated

to different important fields of research. Those include viscoelastic effects, damage

initiation and propagation, environmental effects and glass-fiber stress corrosion. The

last case has been well studied and several models, based on fracture mechanics, have

been presented to model the propagation of a stress-corrosion crack in a glass fibre and

predict the time to failure in different environments [1-10].

High-performance polymer composites exhibit a time-dependent degradation in

modulus (creep or stress relaxation) and strength (creep rupture) as a consequence of the

viscoelasticity of the polymer matrix [11, 12]. One of the most important aspects of

long-term durability and dimensional stability of these materials is their long-term creep

behaviour. Prediction of long-term integrity of any polymeric composite structure

depends on the viscoelastic properties of these materials [11-13]. However, long-term

properties prediction of GRP pipes remains a difficult task because extensive long-term

mechanical tests on the components are required [14].

Yet the structural applications of composite materials in civil construction are becoming

more important. One major application is on rehabilitation in renewal of the structural

inventory, to repair or strengthen. The success of these applications has promoted the

development of new solutions based on FRP (Fiber-Reinforced Polymers). Although

these new products may promise a better mechanical performance on a long-term basis,

the lack of a historical record leads to overdesigned structures. The main reason is

because durability factors, usually determined after long-term experimental tests,

depend on each material system.

On the other hand the full comprehension of internal material changes from microscopic

scale up to the full structure length is far from being well known. The interaction

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between of different mechanisms acting at different scale levels is extremely complex

and not yet fully understood.

Glass fibre reinforced plastic pipes are composite constructions consisting of short

and/or long glass fibre and thermoset materials such as unsaturated polyester or

vinylester as their main components. These pipes are normally produced through

centrifugal casting and/or filament winding of long fibres. GRP pipes are an alternative

to traditional pipes in metallic materials where corrosion, weight and environmental

effects limit the use of this kind of materials. For this reason they are being widely used.

Their good specific mechanical properties deserve a special attention in several

applications. GRP pipes have applications in pressure pipeline as well as in drainage

sewerage piping systems. In these applications the pipe is in contact with various fluids

that, in some cases may have aggressive effects on the material components of the pipe

[12-15]. GRP pipes are frequently used in water transportation and it is widely

recognized that water as a pronounced effect on the mechanical properties and on the

structure of fibre reinforced polymer materials [16-20]. One of the most important

factors which affect the creep behaviour of these materials is moisture. Water penetrates

the resin and attacks the matrix, the reinforcement and the interface of several

composite materials [21]. Some of the hygrothermal aging effects are reversible like the

effect on Tg (reversible when the material dries) and others are not like the plasticization

of the matrix and post-cure reactions [18].

Farshad [22] performed diametrical compression creep tests on GRP pipes. Prior to

creep testing in submerged conditions the samples were conditioned in water at ambient

temperature. During the testing period, diametrical deflection of samples was measured

and the time to failure of each sample was recorded. The long-term tests showed that,

for the pipes tested, the strength corresponding to 1000 testing hours was about 60% of

the short-term strength. Moreover, extrapolation of the data to 50 years showed a

reduction of strength by about 55%.

Nishizaki [20] studied the effects of water on the durability of pultruded glass-fibre

reinforced polymers (GFRP) with vinylester resin for applications in normal air

conditions. Deterioration tests, including both immersion and atmosphere conditions at

various temperatures, were conducted to investigate the deterioration characteristics of

pultruded GFRP after being permeated by water. The bending strength of the GFRP was

reduced. The reductions in bending strength were larger in a 60ºC water immersion

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condition compared to both 60ºC moist-atmosphere condition and a 40ºC water

immersion condition.

The purpose of the present work was to determine and compare lifetimes of GRP pipes

under various loading levels. The observed failure mode was always the same, fiber

breakage, and always localized in the same region. This fact allowed the calculation of

the local failure energy from the experimental data. This failure energy decreased as

lifetime increased and the influence of preconditioning was considered negligible.

Different time-dependent failure criteria were used to model the GRP lifetimes with

reasonable success. Data extrapolation to 50 years predicts a reduction of strength by

about 60%. Furthermore maximum strain at failure decreased about 12% from 0.1 to

1000 hours of creep testing.

2. Time-dependent failure criteria

As the computing power capabilities improve more complex micro-mechanical

models can be solved to predict the creep and creep rupture of real polymers and

polymer matrix composites. These local and direct analyses of the defects initiation and

growth have shown promising results [23]. This type of analysis has the advantage to

allow a deeper understanding of the mechanisms responsible for the rupture and the

creep-rupture. Nevertheless the global and homogeneous analysis, simpler to formulate

and solve, is still more appropriated for practical applications. One of the first

theoretical attempts to include time on a material strength formulation was developed

by Reiner and Weissenberg [24] for viscoelastic materials. Briefly, the Reiner-

Weissenberg criterion [24] states that the work done during the loading by external

forces on a viscoelastic material is converted into a stored part (potential energy) and a

dissipated part (loss energy). The criterion says that the instant of failure depends on a

conjunction between distortional free energy and dissipated energy, a threshold value of

the distortional energy is the governing quantity.

Let us assume that the unidirectional strain response of a linear viscoelastic material,

under arbitrarily stress σ(t), is given by the power law as,

( ) ( ) ( )0 1 0

0

nt t

t D t D dσ ττε σ τ

τ τ∂ −= + ∂

∫ (1)

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where D0, D1, n are material constants; and τ0 represents the time unity (equal to

1second or 1hour or 1day, etc.).

The free stored energy, using Hunter [25] formulation, is given by

( ) ( ) ( ) ( ) ( ) ( ) 2 1 21 20 1 1 2 0 0

0 1 2

1 1 2

2 2

nt t

s

tW t t t D t D d d

σ τ σ ττ τε σ σ τ ττ τ τ

∂ ∂ − −= − − ∂ ∂ ∫ ∫ . (2)

The total energy is defined as,

( ) ( ) ( )

0

t

tW t dε τ

σ τ ττ

∂=

∂∫ . (3)

Accordingly these time-dependent failure criteria [26] predict the lifetime under

constant load, as a function of the applied load σ0 and the creep strength under

instantaneous condition σR:

Reiner-Weissenberg Criterion (R-W), states that ( ) 20

2s R

DW t σ≤ ,

11 10

0 1

1 11

2 2

nnf nn

t D

Dτ γ = − −

. (4)

Maximum Work Stress Criterion (MWS), states that ( ) 20

2t R

DW t σ≤ ,

1 1

0

0 1

1 11

2

nf n

t D

Dτ γ

= −

. (5)

Maximum Strain Criterion (MS), states that ( ) 0 Rt Dε σ≤ ,

1 1

0

0 1

11

nf n

t D

Dτ γ

= −

. (6)

Modified Reiner-Weissenberg Criterion (MR-W), states that ( ) ( )0

2t R

DW t tσ σ ≤

,

11 10

0 1

1 11

2 2

nnf nn

t D

Dτ γ = − −

. (7)

where 2 20 Rγ σ σ= .

Another possible approach is based on the kinetic rate theory of fracture. Based on this

Zurkov [27] used a simple relationship to predict lifetime of several different materials

(except for very small stresses) in terms of a constant stress level σ,

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( )0 0expft t U kTγσ= − . (8)

where t0 is a constant on the order of the molecular oscillation period of 10-13s, k is the

Boltzmann constant, T is the absolute temperature, U0 is a constant for each material

regardless its structure and treatment and γ depends on the previous treatments of the

material and varies over a wide range for different materials.

3. Materials

The GRP pipes used on the experimental program were produced by centrifugal casting.

The pipes are composed by unsaturated polyester reinforced with fibreglass filled with

sand. The mechanical properties provided by the manufacturer are described on Table I.

Accordingly with the manufacturer the pipe wall is made up of three different major

layers, each one possessing different properties according to its functions. Moreover the

pipe wall is composed by an inner layer which provides the chemical resistance, by a

mechanical resistant layer, and a top coat. The specimens used in creep tests are

depicted in Figure 1.

Burn-off tests were made according to the standard procedure NP 2216 1988 on 10

specimens removed from the pipes in order to analyse the components and the structure

of the specimens. The structure of the pipes is heterogeneous and it is constituted by

roving, random matt, polyester resin and sand according to the values displayed on

Table II. Ten plies were observed each one composed by a sub-layer of roving in the

hoop direction and another sub-layer of random matt as depicted in Figure 2. The matrix

is composed of a mixture of polyester resin with sand particles of small size distributed

uniformly.

The glass transition temperature (Tg) of the composite was measured, using a DMTA

machine of the Polymer Laboratories®, as 106.5ºC (±3.4ºC) for the unconditioned

specimens. The glass transition temperature was identified as the peak of loss modulus

measured at 1Hz. The measured glass transition temperature of the conditioned

specimens in water at 50ºC was 100.8ºC (±8.7ºC).

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4. Methods

Prior to testing, samples were stored at room temperature of 20–25 °C and 50% relative

humidity. Care was taken to prepare and maintain the pipe samples free of scratches. A

number of selected specimens were conditioned in a container filled with tap water. The

hoop edges were not protected to prevent water ingress.

The creep tests were carried out following to the European standard EN 1227:1997 [28].

This standard is used to determine the long-term ultimate relative ring deflection under

wet conditions on glass-reinforced thermosetting plastics (GRP) pipes. The

experimental creep tests were carried out applying a dead weight to the specimen

submerged in water at room temperature. The deflection was measured periodically and

the failure time recorded. The test set-up is depicted in Figure 3a and 3b.

Creep tests were preformed on 18 unconditioned specimens using several load levels

(10 to 14 KN) [28]. Creep tests were also performed on specimens preconditioned in

water at 50ºC. After the preconditioning the specimens were tested in the same

conditions, i.e. submerged in water at room temperature. In Table III are listed all the

specimens tested, with the load level and the applied preconditioning conditions.

The deflection was measured with a deflection dial gauge with a precision of ±0.01mm.

Since the load was applied with a beam bar there were no local indentations to account

for.

5. Data reduction schemes

The observed failure mode was always the same, fibre breakage, and always in the same

points, as shown in Figure 4. This is in strict accordance with the theoretical analysis

[29] which predicts the higher tensile stress in such points. Therefore these points were

considered the critical points where the failure always takes place, under ring deflection.

Consequently all the stress-strain analysis developed is focused in those points.

Furthermore it is assumed that the material is linear viscoelastic until failure to keep the

calculations simple.

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In this particular case, a very flexible structure, large defections occur well before

failure takes place. Therefore the circumferential elastic modulus E, function of the

applied load P and the maximum deflection W of a pipe with an average radius R and

with a thickness h, must be calculated taking into account the geometrical nonlinearity

[29]:

max

max

Eσε

= , (9)

where

( )2

1 121max P

bR h Rσ

π

= ± +

,

( )( )2

4

8max

hWRRW

επ ξ

≅ ±− +

with ( ) ( )22 21208 128

9

WW

Rξ π α π ≅ − + −

and α π= ,

which reduces to the linear relationship when 0α = . In Figure 5 is depicted the strain

calculated using the linear and the non-linear relationships against the strain measured,

using an electrical strain gauge. One should note that the strain gauge fail before the

pipe collapsed. It is clear that the non-linear relationship must be used, almost from the

beginning, to obtain the correct maximum strains from the maximum deflection.

The strain gauges were only used in static testes. They were placed in the tensile

stresses sides where the maximum strain was verified, i.e. along the loading line. This

was done to check the accuracy of the equation (9).Five specimens were tested with

strain gauges with a good repeatability.

During the creep test the load is prescribed as constant and the maximum deflection

( )W t becomes time dependent as well the modulus ( )E t which can be obtained from

the previous elastic solution assuming a linear viscoelastic behavior and applying the

Elastic-Viscoelastic Correspondence Principle [30] as

( ) ( )max

max

E tt

σε

= . (10)

In fact this is not the real relaxation modulus but the reciprocal of creep compliance.

The relaxation modulus can be obtained using the simple approach suggested by Park et

al. [31]. However in this case the differences were negligible. Finally the creep

compliance is given by

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( ) ( ) 0 10

1n

tD t D D

E t τ

= = +

, (11)

where D0, D1, n are material constants; and τ0 represents the time unity (equal to

1second or 1hour or 1day, etc.). This expression is usually designated as the power law

and allows the creep compliance representation of many polymers and polymer based

composites materials in a time scale of practical interest [32].

6. Experimental results

In this section the creep and lifetimes results are presented. The objective is to assess the

long-term prediction methodologies and the hygrothermal effects due to the

preconditioning. Since the material presents initial stiffness variability, of ±0.61 GPa for

unconditioned specimens and ±0.75GPa for the conditioned specimens in water at 50ºC,

the creep compliance was normalized to the initial value D0 calculated at 0.01hours

which corresponds to initial creep deflection. This was done to compare more easily the

creep data.

Creep tests

Unconditioned specimens

The measured average initial modulus of the unconditioned specimens was 10.48

(±0.61) GPa. The circumferential normalized creep compliance of some unconditioned

specimens against the power law equation is depicted in Figure 6.

Specimens preconditioned at 50ºC

The average initial circumferential modulus of the preconditioned specimens in water at

50ºC was 10.05 (±0.75) GPa. The circumferential normalized creep compliance of some

specimens preconditioned against the power is depicted in Figure 7. It seems reasonable

to assume that the creep compliance of the preconditioned specimens follow the same

power law used to describe the creep compliance of the unconditioned specimens.

Although some objections may be pointed against this assumption, it has the advantage

to simplify the subsequent calculations and analysis.

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Lifetime results

The creep tests were initiated using a loading rate as slow as necessary to obtain the

desired creep load in 3 min (±0.5 min). Under creep loading conditions the short-term

(<0.1 h) failures take place at stress levels close to 165MPa.

Therefore the reference value of the creep strength was chosen to be165MPa. In Figures

8 and 9 are represented the maximum applied stress and the strain at failure,

respectively, against the lifetime. Three preconditioned specimens, indicated by arrows,

did not fail after 5000 hours when the test was stopped.

The Zurkov type relationship [27] fits reasonably the experimental data with a squared

correlation coefficient of 0.72. The “low” value of the correlation coefficient reflects the

scatter of the creep rupture data, which is typical of creep rupture in general. The data

extrapolation for 50 years gives a maximum stress limit of 103 MPa. This represents a

strength reduction of 37% compared against the reference strength (165MPa). Although

slightly different curves were determined for the unconditioned and preconditioned

specimens as depicted in Figure 8, the influence of the preconditioning on lifetime was

considered negligible. The main effect was a drop of 4% in the initial modulus. A

decrease on the maximum strain at failure was detected, 12% after 1000 hours and, by

extrapolation, 17% after 50 years.

7. Discussion of results

Both conditioned and unconditioned creep specimens were tested under the same load

and environment conditions. When comparing the instantaneous modulus (elastic) and

the creep compliance we can conclude that the preconditioning caused a 4% drop of the

elastic modulus but did not affect the viscoelastic behaviour. Nevertheless the reduced

number of preconditioned specimens tested as well the applied reduced stress range is

no sufficient to draw definitive conclusions.

The lifetime expressions previously summarized depended on the viscoelastic properties

and on the creep strength under instantaneous condition. Moreover these expressions

depend on the rate between the viscoelastic and elastic compliance parameters (D1/D0).

From the creep tests this ratio was determined as 0.030. However, for the lifetime

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prediction, it was verified that the ratio D1/D0 should be larger, i.e. 0.08. One

explanation for this can be attributed to the linear viscoelastic assumption. Since the

stress state is not uniform, the stress influence over the creep compliance is averaged

when linear viscoelastic behaviour is presumed. Therefore one should expect higher

creep compliance values at the critical points, since the stress acts as an accelerator

factor on the viscoelastic behaviour [32]. The creep strength under instantaneous

condition was determined to be 165MPa. The viscoelastic parameters are summarized in

Table IV.

If we consider the normalized rupture free energy as

20

2

ff

R

ww

D σ= , (12)

and the normalized applied stress as

00

R

σσσ

= , (13)

then it is possible to rewrite all the previous criteria in an non-dimensional form.

Reiner-Weissenberg Criterion (R-W):

1fw = . (14)

Maximum Work Stress Criterion (MWS):

( )2 102 1 2n n

fw σ −= + − . (15)

Maximum Strain Criterion (MS):

( ) ( )20 02 1 2 2n n

fw σ σ= − + − . (16)

Modified Reiner-Weissenberg Criterion (MR-W):

0fw σ= . (17)

If we plot the experimental data against the theoretical values, calculated using the

values in Table IV, it became quite clear that the R-W criterion is not appropriated for

the present case, as depicted in Figure 10.

In Figure 11 are depicted the theoretical lifetime predictions against the experimental

results. As it was expected from the previous analysis the R-W criterion is not well

suited for this case. All the other models follow quite well the experimental data. Table

V summarizes the lifetime predictions for each theoretical approach. The maximum

strain criterion is more conservative when compared against the other models.

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In this case it seems appropriate to apply the MS criterion. The criterion can be

rewritten as follows

1

max 0 0

0 1 0

f nt D

D

ε στ σ −=

. (18)

Now using the MS criterion and considering a 50 year (438,000 hours) lifetime

prediction we obtain 79MPa and 68MPa for εmax=0.0160 and for εmax =0.0135,

respectively, see also Figure 12. These lifetime predictions imply a creep strength

reduction between 52 and 59 %, respectively.

Before closing this section something more has to be said about the preconditioned

effect. Although the preconditioning in water at 50ºC appeared to be irrelevant some

extra phenomena may occur. One phenomenon developed at high temperatures is the

post-curing process and the other is the acceleration of the ageing effect. In both cases

the outcome would be an increase of stiffness and strength. This in part would

compensate the stiffness decrease due to the water uptake. However neither the post-

curing process nor the ageing effect were measured or taken into account in this study.

8. Conclusions

Creep tests were performed on GRP pipes in order to determine the long-term creep

compliance and creep-rupture. It was observed that preconditioning in water at 50ºC

had a small influence on the initial stiffness of GRP pipes, a decrease of about 4%.

Furthermore the creep and creep-rupture behaviour in aqueous environment of

preconditioned and unconditioned GRP pipes under lateral deflection was very similar.

Not quite surprisingly Zurkov [27] type relationship was able to fit the entire lifetime

experimental data with a reasonably correlation. Other lifetime models based on

different time-dependent failure criteria, which depend on the viscoelastic properties

and on the creep strength under instantaneous conditions, were briefly presented and

successfully applied, with the exception of Reiner-Weissenberg criterion. Moreover it

was verified that the maximum strain criterion was the most conservative criterion of

all. On that ground and considering a 50 year lifetime, a strength reduction of about

60% was predicted.

Acknowledgements

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The research hereby presented was supported by Fundação para a Ciência e Tecnologia

(Ministério da Ciência e do Ensino Superior) through project POCTI/EME/47734/2002.

The authors acknowledge the support of Dr. João Rodrigues (INEGI) who performed

and analyzed all the burn-off tests.

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materials. Rheol Leaflet 1939;10:12–20. 25. Hunter, S. C., Tentative Equations for the Propagation of Stress, Strain and

Temperature Fields in Viscoelastic Solids, J Mech Phys Solids 1961;9(1):39-51

Page 15: On the Prediction of Long-term Creep-Failure of GRP Pipes

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26. R.M. Guedes. Mathematical analysis of energies for viscoelastic materials and energy based failure criteria for creep loading. Mechanics of Time-Dependent Materials 2004;8(2):169-192.

27. Zhurkov, SN, Kinetic Concept of the Strength of Solids, International Journal of

Fracture Mechanics 1965;1(4):311. 28. Faria H. Failure Analysis of GRP Pipes Under Compressive Ring Loads. MSc

Thesis, Faculdade de Engenharia da Universidade do Porto; 2005. 29. Guedes RM. Stress–strain analysis of a cylindrical pipe subjected to a transverse

load and large deflections. Compos Struct (2008), doi:10.1016/j.compstruct.2008.03.031.

30. Guedes RM, Marques AT, Cardon A. Creep or Relaxation Master Curves

Calculated from Experimental Dynamic Viscoelastic Function. Science and Engineering of Composite Materials 1998;7 (3):259-267.

31. Park SW, Kim YR. Interconversion between relaxation modulus and creep

compliance for viscoelastic solids. Journal of Materials in Civil Engineering 1999;11(1): 76-82.

32. Findley WN, Lai JS and Onaran K. Creep and Relaxation of Nonlinear Viscoelastic

Materials. Dover Publications, New York;1989.

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Figure Captions

Figure 1 – Creep specimens.

Figure 2 – Detail of the ply reinforcement composed of roving in the hoop direction and

random matt.

Figure 3 – Creep test apparatus; a) during load calibration and b) submerged in a tank

during creep tests.

Figure 4 – The GRP pipe failure mode under ring deflection.

Figure 5 – Comparison between the measured strain and the strain calculated using

linear and non-linear relationships.

Figure 6 – Normalized creep compliance of GRP pipes under ring deflection, without

preconditioning.

Figure 7 – Normalized creep compliance of preconditioned GRP pipes under ring

deflection.

Figure 8 – Lifetime GRP pipes under ring deflection versus the maximum applied

stress.

Figure 9 – Lifetime GRP pipes under ring deflection versus the maximum strain at

failure.

Figure 10 – Normalised free energy at failure versus normalised stress for the

experimental data and theoretical models.

Figure 11 – Experimental lifetime and theoretical predictions for GRP pipes under ring

deflection.

Figure 12 – Lifetime prediction of GRP pipes under ring deflection using the maximum

strain criterion, considering two extreme values.

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List of Tables

Page 18: On the Prediction of Long-term Creep-Failure of GRP Pipes

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Table I – Properties of the pipes provided by the manufacturer.

EHoop (MPa) ERadial (MPa) ELongitudinal (MPa)

10547 3808 3808

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Table II – Relative composition of GRP pipes for mass content (%).

Constituents Average values Standard deviation

Polyester (matrix) 35.65 0.41

Roving 10.41 1.51

Matt 12.66 0.88

Sand 41.28 2.54

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Table III – Creep specimens with the correspondent load and preconditioning.

Specimen Nº Preconditioning Load (N)

C36 No 12196

C46 No 11831

C47 No 12087

C55 No 12400

C56 No 12400

C38 No 10643

C50 No 10380

C52 No 10431

C39a No 12719

C48 No 12830

C49 No 12692

C51 No 13638

C57 No 13088

C39b No 13970

C45 No 14420

C58 No 13988

C53 No 11411

C54 No 11139

C88 50ºC during 4920 hours + 3000 hours at dry air 11096

C89 50ºC during 4920 hours + 3000 hours at dry air 11096

C92 50ºC during 4920 hours + 3000 hours at dry air 11353

C90 50ºC during 7112 hours 9865

C91 50ºC during 7112 hours 10567

C93 50ºC during 10800 hours 9084

C94 50ºC during 10800 hours 10059

C95 50ºC during 10800 hours 11358

Page 21: On the Prediction of Long-term Creep-Failure of GRP Pipes

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Table IV – Viscoelastic properties and strength under instantaneous conditions.

D1/D0 D1/D0* n σR

MPa 0.030 0.080 0.200 165 *Value used for lifetime prediction

Page 22: On the Prediction of Long-term Creep-Failure of GRP Pipes

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Table V – Lifetime theoretical predictions.

Failure Criteria

Maximum Stress 1000 h 1 year 50 years

R-W 146 138 119 MR-W 130 116 86 MSW 129 117 93 MS 125 110 79

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List of Figures

Page 24: On the Prediction of Long-term Creep-Failure of GRP Pipes

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12mm

R250mm

300mm

Figure 1 – Creep specimens.

Page 25: On the Prediction of Long-term Creep-Failure of GRP Pipes

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Figure 2 – Detail of the ply reinforcement composed of roving in the hoop direction and

random matt.

Page 26: On the Prediction of Long-term Creep-Failure of GRP Pipes

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(a) (b)

Figure 3 – Creep test apparatus; a) during load calibration and b) submerged in a tank during creep tests.

Page 27: On the Prediction of Long-term Creep-Failure of GRP Pipes

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Figure 4 – The GRP pipe failure mode under ring deflection.

Page 28: On the Prediction of Long-term Creep-Failure of GRP Pipes

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0

50

100

150

200

250

300

0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04

Strain

Str

ess

(MP

a)

Strain gauge

Linear calculation

Non-linear calculation

Strain gauge failure

Pipe failure

Figure 5 – Comparison between the measured strain and the strain calculated using

linear and non-linear relationships.

Page 29: On the Prediction of Long-term Creep-Failure of GRP Pipes

29

0.90

1.00

1.10

1.20

0.01 0.1 1 10 100 1000 10000

Time (hours)

Cre

ep C

ompl

ianc

e C

(t)/

C0 Not Precond.( ) 1

0 0 0

1n

D t D t

D D τ

= +

11 0 0 00.030, 0.20, 1h, 110475MPaD D n Dτ −= = = =

Figure 6 – Normalized creep compliance of GRP pipes under ring deflection, without

preconditioning.

Page 30: On the Prediction of Long-term Creep-Failure of GRP Pipes

30

0.90

1.00

1.10

1.20

0.01 0.1 1 10 100 1000 10000

Time (hours)

Cre

ep C

ompl

ianc

e C

(t)/

C0

Precond.( ) 1

0 0 0

1n

D t D t

D D τ

= +

11 0 0 00.030, 0.20, 1h, 110050MPaD D n Dτ −= = = =

Figure 7 – Normalized creep compliance of preconditioned GRP pipes under ring

deflection.

Page 31: On the Prediction of Long-term Creep-Failure of GRP Pipes

31

60

100

140

180

0.01 0.1 1 10 100 1000 10000 100000 1E+06

Time to Failure (hour)

Str

ess

(MP

a) Not Precond

Precond.

Zurkov (Not Precond.)

Zurkov (Precond.)

15624.09

00

e , 1 hour, 0.72ftσ

τ ρτ

= = =

15324.87

00

e , 1 hour, 0.72ftσ

τ ρτ

= = =

Figure 8 – Lifetime GRP pipes under ring deflection versus the maximum applied

Page 32: On the Prediction of Long-term Creep-Failure of GRP Pipes

32

0.000

0.004

0.008

0.012

0.016

0.020

0.01 0.1 1 10 100 1000 10000 100000

Time (hour)

Max

. Str

ain

at F

ailu

re

PrecondNot Precond

0.0108

2max 0

0

0.0154 , 1 hour, 0.257tε τ ρ

τ

= = =

Figure 9 – Lifetime GRP pipes under ring deflection versus the maximum strain at

failure.

Page 33: On the Prediction of Long-term Creep-Failure of GRP Pipes

33

0.0

0.2

0.4

0.6

0.8

1.0

0.0 0.2 0.4 0.6 0.8 1.0

Normalised Stress

Nor

mal

ised

Fai

lure

Fre

e E

nerg

y

Experim.R-WMR-WMSWMS

Figure 10 – Normalised free energy at failure versus normalised stress for the

experimental data and theoretical models.

Page 34: On the Prediction of Long-term Creep-Failure of GRP Pipes

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60

100

140

180

0.01 0.1 1 10 100 1000 10000 100000 1E+06

Time to Failure (hour)

Str

ess

(MP

a)

Not Precond

Precond.R-W

MR-W

MSW

MS

Figure 11 – Experimental lifetime and theoretical predictions for GRP pipes under ring

deflection.

Page 35: On the Prediction of Long-term Creep-Failure of GRP Pipes

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60

100

140

180

0.01 0.1 1 10 100 1000 10000 100000 1E+06

Time to Failure (hour)

Str

ess

(MP

a)

Not Precond

Precond.

εmax=0.0135

εmax=0.0160

Figure 12 – Lifetime prediction of GRP pipes under ring deflection using the maximum

strain criterion, considering two extreme values.