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Integrated Photonic Devices James Wilkinson Optoelectronics Research Centre University of Southampton, UK [email protected]

Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

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Page 1: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Integrated Photonic Devices

James Wilkinson

Optoelectronics Research Centre University of Southampton, UK

[email protected]

Page 2: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

The Birth of Integrated Photonics

High-index “channel” on or in a flat substrate

Light guided by total internal reflection

Optical circuits may be made

“Evanescent” field results at waveguide surface

High-index

guiding channel Substrate

Electric field strength

EAJ Marcatili, Bell Labs

1978

“In 1969 my friend and boss,

S.E. Miller had the wonderful

idea of fabricating the many

components of optical

transmitters and receivers on a

single substrate using well-

known photolithographic

techniques. These devices were

very small (a few microns

across), precise, insensitive to

mechanical and thermal

transients and, if fabricated in

large numbers, economical.”

Page 3: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Advantages of the Planar Configuration

• Robustly interconnected multiple devices with economy of mass-production

• Localisation of gain and nonlinearity for example by dopant diffusion

• Simple variation of guide geometry by photolithography

• Access to evanescent fields

• Stable long lengths in small area

• Distributed functions such as pump-coupling and filtering

Page 4: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Fabrication Facility Layout

Fibre and Novel

Glass Integrated

Photonics

Southampton

Nanofabrication

Centre

Biophotonics

Thick Film

Bioelectronics

FIB

Page 5: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Integrated Photonics Cleanrooms

• Class 1000 cleanroom

• Photolithography

• Dip-pen nanolithography

• Sputtering, e-beam and thermal evaporation

• Ion-beam deposition

• Diffusion to 2300oC

• Reactive ion etching

• Chemically-assisted ion beam etching

• Microscopy, profilometry & SEM

Page 6: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Photolithography

Karl-Suss MA6 double-sided aligner

Define surface structures, electrodes,

optical circuits

Wide range of substrates

Resists – almost anything you can spin:

PMMA, SU-8, carbon

nanotubes in polymer

Max substrate size 4” diameter

Min feature size <1 micron

Dip-pen down to 10nm dots…

Page 7: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Sputtering, ion-beam, e-beam and thermal evaporation

Thin films of almost any material you want!

• Silica

• Germania-doped silica

• Erbium-doped tantala

• Indium tin oxide

• Pyrex

• Gallium lanthanum sulphide glass

• Bismuthate glass

• Gold, chromium, aluminium, silver, nichrome ..

• Neodymium, erbium, thulium, ytterbium …

• Lutetium biphthalocyanine

• Alumina

• Magnesium fluoride

• Teflon

• Germanium telluride glass

Page 8: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Etch almost any material you want!

Ar ion mill eg sapphire

150mm collimated

(+ FIB in separate facility)

Reactive ion etch eg SiO2

HF etch glass

Etching: Ion-Beam, Reactive and Wet

Page 9: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Diffusion and annealing

Diffuse almost anything into anything else!

• ≤ 600oC Salt-melt diffusion in glass (Ar, N2, O2)

• ≤ 1200oC Ti/Er diffusion into lithium niobate (Ar, N2, O2)

• ≤ 1700oC Glass softening and annealing (Ar, N2, O2)

• ≤ 2300oC Ga/Ti diffusion into sapphire (Vacuum, Ar, N2)

Depth (m)

012

Ga counts normalised0

1

Page 10: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Characterisation

2-D and 1-D stylus profilometry

~ 1nm step height resolution

~ 2μm lateral resolution

Microscopy

4-point probe for film sheet resistance

SEM AFM Optical

Page 11: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Waveguide lasers and amplifiers

● Er/Yb borosilicate glass waveguide laser & amplifier with 3dB/cm gain

● Nd-diffused LiNbO3 coupled-cavity tunable waveguide laser

● Ti-diffused sapphire waveguide laser for broad tunability

● Nd-doped Ta2O5 rib waveguide laser for photonic crystals

Er-doped Ta2O5 rib waveguide lasers and amplifiers for compact circuits

Channel Width of Mask / µm

4 6 8 10 12 14 16 18 20 22

Incid

en

t T

hre

sh

old

Pu

mp

Po

we

r /

mW

0

20

40

60

80

100

120

6µm wide 12.5µm wide 20µm wide

Page 12: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Integrated multisensor system “AWACSS”

32 analyte glass fluorescence sensor chip Instrument to handle fluids and analyse data

Fluorescent molecules within evanescent field are excited by light in waveguide

Light emitted from fluorescent molecules on 32 spots is detected in instrument

Page 13: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Trapping and manipulation at a surface

Light in

Downward force

Lateral forces Detection

“Radiation pressure”

forces

v1

v2

Page 14: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Optical Organisation of Gold Nanoparticles

What? • 125nm radius gold spheres in water

• Trapped and propelled on waveguide

• Speeds up to 0.7mm per second

Waveguide

Why? • Separation of gold-tagged biomolecules

• Organisation of regular arrays

• Surface-enhanced Raman spectroscopy

Laser light into

waveguide

Page 15: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Amplifiers & lasers: Er, Yb & Nd-doped glass and Ta2O5 on silicon

Filters, mirrors & resonators: with F.Diaz URV Tarragona and M.N. Zervas

Schematic of EDWA integration Gain spectra of Er:Ta2O5 guides Lasing spectra of Er:Ta2O5

Bottle-resonator add/drop mux Epitaxial KY1-x-yGdxLuy(WO4)2

ring resonators

Waveguide grating reflection spectra for

Er laser mirrors

Ta2O5 rib waveguide

photonic crystal filter

Integrated Photonic Devices

Page 16: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Excitation & manipulation of spheres & cells

Microsphere fabrication & resonator self-assembly

with D. Hewak, P.N. Bartlett, & M.N. Zervas

Integrated μsphere lasers:

Add lasing function to passive circuits

1055 1060 1065 1070

0

200

400

600

0

30

60

90

120

0

50

100

150

200

250

(c) Waveguide outputT

E(1

,23

5)

TE

(1,2

36

)

TE

(1,2

37

)

TE

(1,2

38

)

TM

(2,2

28

)T

M(3

,22

1)

TM

(1,2

36

)

TM

(1,2

37

)

TM

(1,2

38

)

(b)

Wavelength (nm)

Lasin

g p

ow

er

spectr

al density (

nW

/nm

)

Side

(a) Top

Waveguide optophoresis:

Microsphere and biological cell manipulation

with O.G.Hellesø, Uni. Tromsø, Norway

High-Q chalcogenide spheres

Chemical/physical assembly

Self-assembled waveguide grating

Surface microsphere sorting

Loop for standing-wave trapping Waveguide-coupled laser spectra

Nd-doped microsphere laser

Page 17: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

Integrated Photonics for Bioanalysis

Wideband Integrated Photonics for Accessible Biomedical Diagnostics:

• Mid-IR materials

• On-chip spectroscopy and cytometry

• Nanostructured materials

• Point-of-care applications

32 analyte biosensor chip

Estrone, 2-4D, bisphenol A, simazine …

water pollution at LoD all below 20ng/L

Detector

Laser

Fibre

Microlens

Microchannel

Waveguide

Microchip

Optofluidic integration for microflow cytometers – planar kinoform lenses

Electrochemical plasmonics with Prof P.N. Bartlett, Chemistry

Page 18: Integrated Photonic Devices - cimp.soton.ac.uk films of almost any material you want! • Silica • Germania-doped silica • Erbium-doped tantala • Indium tin oxide ... erbium,

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